#------------------------------------------------------------------------------
#$Date: 2016-03-25 23:13:35 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180030 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/24/7032486.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7032486
loop_
_publ_author_name
'Han, Min-Le'
'Duan, Ya-Ping'
'Li, Dong-Sheng'
'Xu, Guo-Wang'
'Wu, Ya-Pan'
'Zhao, Jun'
_publ_section_title
;
 A series of divalent metal coordination polymers based on isomeric
 tetracarboxylic acids: synthesis, structures and magnetic properties.
;
_journal_issue                   46
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              17519
_journal_page_last               17527
_journal_paper_doi               10.1039/c4dt01946f
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C22 H20 Co2 O13'
_chemical_formula_weight         610.24
_chemical_name_systematic
;

 ?

;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 97.852(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.444(8)
_cell_length_b                   6.526(4)
_cell_length_c                   23.959(13)
_cell_measurement_reflns_used    5479
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      2.1
_cell_volume                     2237(2)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0675
_diffrn_reflns_av_sigmaI/netI    0.0503
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            23097
_diffrn_reflns_theta_full        27.56
_diffrn_reflns_theta_max         27.56
_diffrn_reflns_theta_min         2.85
_exptl_absorpt_coefficient_mu    1.557
_exptl_absorpt_correction_T_max  0.7888
_exptl_absorpt_correction_T_min  0.7563
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.812
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             1240
_exptl_crystal_size_max          0.19
_exptl_crystal_size_mid          0.17
_exptl_crystal_size_min          0.16
_refine_diff_density_max         0.660
_refine_diff_density_min         -0.576
_refine_diff_density_rms         0.078
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.030
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     337
_refine_ls_number_reflns         5179
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.030
_refine_ls_R_factor_all          0.0497
_refine_ls_R_factor_gt           0.0387
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0517P)²+1.0439P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1011
_refine_ls_wR_factor_ref         0.1080
_reflns_number_gt                4285
_reflns_number_total             5179
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4dt01946f2.cif
_cod_data_source_block           z
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 7032483--7032487.cif.

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'none' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7032486
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Co1 Co 1.0000 -0.5000 0.5000 0.02212(13) Uani 1 2 d S
Co2 Co 0.5000 0.0000 0.5000 0.01569(12) Uani 1 2 d S
Co3 Co 0.39620(2) 0.49977(4) 0.475038(13) 0.01757(10) Uani 1 1 d .
O1 O 0.83652(16) -0.5734(3) 0.39062(8) 0.0396(5) Uani 1 1 d .
O2 O 0.87466(14) -0.3619(3) 0.46279(7) 0.0346(5) Uani 1 1 d .
O3 O 0.65134(12) -0.3758(2) 0.45327(7) 0.0253(4) Uani 1 1 d .
O4 O 0.62894(13) -0.0436(2) 0.47086(7) 0.0249(4) Uani 1 1 d .
O5 O 0.91373(17) -0.2384(3) 0.12186(9) 0.0480(6) Uani 1 1 d .
H5D H 0.9250 -0.2935 0.0928 0.072 Uiso 1 1 calc R
O6 O 0.94104(15) 0.0489(3) 0.07520(8) 0.0375(5) Uani 1 1 d .
O7 O 0.58430(14) 0.1274(3) 0.10215(7) 0.0291(4) Uani 1 1 d .
O8 O 0.56897(14) 0.4616(3) 0.08283(7) 0.0281(4) Uani 1 1 d .
O9 O 0.95103(14) -0.7791(3) 0.46730(8) 0.0344(4) Uani 1 1 d .
H9B H 0.9217 -0.8728 0.4822 0.052 Uiso 1 1 d R
H9A H 0.9069 -0.7419 0.4422 0.052 Uiso 1 1 d R
O10 O 0.51142(11) 0.3058(2) 0.47661(6) 0.0175(3) Uani 1 1 d .
H10D H 0.5290 0.3058 0.4385 0.026 Uiso 1 1 d R
O11 O 0.31000(13) 0.2869(3) 0.42131(8) 0.0335(4) Uani 1 1 d .
H11A H 0.3403 0.1779 0.4167 0.050 Uiso 1 1 d R
H11B H 0.2973 0.3450 0.3894 0.050 Uiso 1 1 d R
O12 O 0.27959(13) 0.7020(3) 0.48113(10) 0.0417(5) Uani 1 1 d .
H12B H 0.2997 0.7975 0.5037 0.063 Uiso 1 1 d R
H12A H 0.2457 0.6351 0.5011 0.063 Uiso 1 1 d R
O13 O 0.85991(16) 0.5465(3) 0.02995(9) 0.0439(5) Uani 1 1 d .
H13B H 0.8051 0.5188 0.0367 0.066 Uiso 1 1 d R
H13A H 0.8650 0.6240 0.0020 0.066 Uiso 1 1 d R
C1 C 0.83438(16) -0.4040(4) 0.41331(10) 0.0217(5) Uani 1 1 d .
C2 C 0.78599(16) -0.2294(3) 0.37955(9) 0.0190(4) Uani 1 1 d .
C3 C 0.70777(16) -0.1271(3) 0.39403(9) 0.0187(4) Uani 1 1 d .
C4 C 0.65958(15) -0.1885(3) 0.44324(9) 0.0182(4) Uani 1 1 d .
C5 C 0.66859(16) 0.0324(3) 0.35996(10) 0.0193(5) Uani 1 1 d .
H5 H 0.6157 0.0980 0.3694 0.023 Uiso 1 1 calc R
C6 C 0.70576(16) 0.0967(3) 0.31255(9) 0.0192(5) Uani 1 1 d .
C7 C 0.78860(17) 0.0040(3) 0.30051(10) 0.0205(5) Uani 1 1 d .
C8 C 0.82571(16) -0.1613(4) 0.33310(10) 0.0223(5) Uani 1 1 d .
H8 H 0.8783 -0.2277 0.3236 0.027 Uiso 1 1 calc R
C9 C 0.83983(17) 0.0929(4) 0.25594(10) 0.0226(5) Uani 1 1 d .
C10 C 0.85843(18) -0.0195(4) 0.20960(11) 0.0242(5) Uani 1 1 d .
H10 H 0.8423 -0.1574 0.2065 0.029 Uiso 1 1 calc R
C11 C 0.90148(17) 0.0751(4) 0.16757(10) 0.0243(5) Uani 1 1 d .
C12 C 0.92063(18) -0.0398(4) 0.11702(11) 0.0278(5) Uani 1 1 d .
C13 C 0.92647(18) 0.2803(4) 0.17222(11) 0.0283(5) Uani 1 1 d .
H13 H 0.9529 0.3440 0.1435 0.034 Uiso 1 1 calc R
C14 C 0.91202(19) 0.3896(4) 0.21959(11) 0.0311(6) Uani 1 1 d .
H14 H 0.9314 0.5252 0.2237 0.037 Uiso 1 1 calc R
C15 C 0.86845(18) 0.2965(4) 0.26109(11) 0.0284(5) Uani 1 1 d .
H15 H 0.8582 0.3711 0.2927 0.034 Uiso 1 1 calc R
C16 C 0.65770(16) 0.2546(3) 0.27403(9) 0.0195(5) Uani 1 1 d .
C17 C 0.63914(16) 0.2135(3) 0.21644(9) 0.0205(5) Uani 1 1 d .
H17 H 0.6529 0.0847 0.2032 0.025 Uiso 1 1 calc R
C18 C 0.60043(16) 0.3614(3) 0.17841(9) 0.0199(4) Uani 1 1 d .
C19 C 0.58310(16) 0.3117(3) 0.11645(9) 0.0200(5) Uani 1 1 d .
C20 C 0.57899(18) 0.5548(4) 0.19873(10) 0.0242(5) Uani 1 1 d .
H20 H 0.5553 0.6568 0.1737 0.029 Uiso 1 1 calc R
C21 C 0.59295(18) 0.5939(4) 0.25597(10) 0.0266(5) Uani 1 1 d .
H21 H 0.5762 0.7205 0.2693 0.032 Uiso 1 1 calc R
C22 C 0.63194(17) 0.4452(4) 0.29379(10) 0.0243(5) Uani 1 1 d .
H22 H 0.6409 0.4726 0.3322 0.029 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O9 Co1 O9 180.00(5) 3_746 .
O9 Co1 O2 89.24(8) 3_746 3_746
O9 Co1 O2 90.76(8) . 3_746
O9 Co1 O2 90.76(8) 3_746 .
O9 Co1 O2 89.24(8) . .
O2 Co1 O2 180.00(9) 3_746 .
O9 Co1 O6 91.89(8) 3_746 2_745
O9 Co1 O6 88.11(8) . 2_745
O2 Co1 O6 90.13(9) 3_746 2_745
O2 Co1 O6 89.87(9) . 2_745
O9 Co1 O6 88.11(8) 3_746 4_556
O9 Co1 O6 91.89(8) . 4_556
O2 Co1 O6 89.87(9) 3_746 4_556
O2 Co1 O6 90.13(9) . 4_556
O6 Co1 O6 180.000(1) 2_745 4_556
O10 Co2 O10 180.00(2) . 3_656
O10 Co2 O4 86.21(6) . .
O10 Co2 O4 93.79(6) 3_656 .
O10 Co2 O4 93.79(6) . 3_656
O10 Co2 O4 86.21(6) 3_656 3_656
O4 Co2 O4 180.00(9) . 3_656
O10 Co2 O8 84.58(6) . 2_645
O10 Co2 O8 95.42(6) 3_656 2_645
O4 Co2 O8 89.85(8) . 2_645
O4 Co2 O8 90.15(8) 3_656 2_645
O10 Co2 O8 95.42(6) . 4_566
O10 Co2 O8 84.58(6) 3_656 4_566
O4 Co2 O8 90.15(8) . 4_566
O4 Co2 O8 89.85(8) 3_656 4_566
O8 Co2 O8 180.0 2_645 4_566
O10 Co3 O7 95.53(7) 3_666 2_655
O10 Co3 O10 84.87(7) 3_666 .
O7 Co3 O10 93.12(7) 2_655 .
O10 Co3 O3 92.08(7) 3_666 3_656
O7 Co3 O3 168.77(7) 2_655 3_656
O10 Co3 O3 95.78(7) . 3_656
O10 Co3 O12 92.09(8) 3_666 .
O7 Co3 O12 90.97(8) 2_655 .
O10 Co3 O12 175.12(7) . .
O3 Co3 O12 80.49(8) 3_656 .
O10 Co3 O11 175.04(7) 3_666 .
O7 Co3 O11 82.26(8) 2_655 .
O10 Co3 O11 90.80(7) . .
O3 Co3 O11 90.76(8) 3_656 .
O12 Co3 O11 92.39(9) . .
C1 O2 Co1 123.83(16) . .
C4 O3 Co3 125.66(15) . 3_656
C4 O4 Co2 131.65(15) . .
C12 O5 H5D 109.5 . .
C12 O6 Co1 142.4(2) . 2_755
C19 O7 Co3 129.52(15) . 2_645
C19 O8 Co2 134.79(16) . 2_655
Co1 O9 H9B 129.6 . .
Co1 O9 H9A 101.6 . .
H9B O9 H9A 97.8 . .
Co3 O10 Co2 120.23(8) 3_666 .
Co3 O10 Co3 95.13(7) 3_666 .
Co2 O10 Co3 119.55(8) . .
Co3 O10 H10D 106.9 3_666 .
Co2 O10 H10D 106.9 . .
Co3 O10 H10D 106.9 . .
Co3 O11 H11A 110.5 . .
Co3 O11 H11B 106.5 . .
H11A O11 H11B 107.9 . .
Co3 O12 H12B 106.8 . .
Co3 O12 H12A 103.8 . .
H12B O12 H12A 101.1 . .
H13B O13 H13A 117.4 . .
O1 C1 O2 124.5(2) . .
O1 C1 C2 118.5(2) . .
O2 C1 C2 117.0(2) . .
C8 C2 C3 118.8(2) . .
C8 C2 C1 117.2(2) . .
C3 C2 C1 123.9(2) . .
C5 C3 C2 119.3(2) . .
C5 C3 C4 117.6(2) . .
C2 C3 C4 123.0(2) . .
O3 C4 O4 125.3(2) . .
O3 C4 C3 118.42(19) . .
O4 C4 C3 116.29(19) . .
C6 C5 C3 122.3(2) . .
C6 C5 H5 118.9 . .
C3 C5 H5 118.9 . .
C5 C6 C7 118.3(2) . .
C5 C6 C16 121.1(2) . .
C7 C6 C16 120.5(2) . .
C8 C7 C6 119.4(2) . .
C8 C7 C9 120.6(2) . .
C6 C7 C9 119.8(2) . .
C2 C8 C7 121.7(2) . .
C2 C8 H8 119.2 . .
C7 C8 H8 119.2 . .
C10 C9 C15 119.2(2) . .
C10 C9 C7 122.3(2) . .
C15 C9 C7 118.4(2) . .
C9 C10 C11 119.8(2) . .
C9 C10 H10 120.1 . .
C11 C10 H10 120.1 . .
C13 C11 C10 120.3(2) . .
C13 C11 C12 118.6(2) . .
C10 C11 C12 121.1(2) . .
O6 C12 O5 124.8(3) . .
O6 C12 C11 121.4(3) . .
O5 C12 C11 113.8(2) . .
C14 C13 C11 119.9(2) . .
C14 C13 H13 120.1 . .
C11 C13 H13 120.1 . .
C13 C14 C15 119.8(2) . .
C13 C14 H14 120.1 . .
C15 C14 H14 120.1 . .
C14 C15 C9 120.8(2) . .
C14 C15 H15 119.6 . .
C9 C15 H15 119.6 . .
C17 C16 C22 118.8(2) . .
C17 C16 C6 119.3(2) . .
C22 C16 C6 121.9(2) . .
C18 C17 C16 121.4(2) . .
C18 C17 H17 119.3 . .
C16 C17 H17 119.3 . .
C17 C18 C20 119.0(2) . .
C17 C18 C19 119.6(2) . .
C20 C18 C19 121.4(2) . .
O7 C19 O8 125.1(2) . .
O7 C19 C18 118.0(2) . .
O8 C19 C18 116.8(2) . .
C21 C20 C18 120.1(2) . .
C21 C20 H20 120.0 . .
C18 C20 H20 120.0 . .
C20 C21 C22 120.5(2) . .
C20 C21 H21 119.7 . .
C22 C21 H21 119.7 . .
C21 C22 C16 120.1(2) . .
C21 C22 H22 119.9 . .
C16 C22 H22 119.9 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Co1 O9 2.069(2) 3_746
Co1 O9 2.069(2) .
Co1 O2 2.108(2) 3_746
Co1 O2 2.108(2) .
Co1 O6 2.120(2) 2_745
Co1 O6 2.120(2) 4_556
Co2 O10 2.0853(18) .
Co2 O10 2.0853(18) 3_656
Co2 O4 2.0958(19) .
Co2 O4 2.0958(19) 3_656
Co2 O8 2.110(2) 2_645
Co2 O8 2.110(2) 4_566
Co3 O10 2.0761(17) 3_666
Co3 O7 2.0821(19) 2_655
Co3 O10 2.0873(18) .
Co3 O3 2.0974(18) 3_656
Co3 O12 2.160(2) .
Co3 O11 2.1678(19) .
O1 C1 1.234(3) .
O2 C1 1.277(3) .
O3 C4 1.255(3) .
O3 Co3 2.0974(18) 3_656
O4 C4 1.268(3) .
O5 C12 1.307(3) .
O5 H5D 0.8200 .
O6 C12 1.227(3) .
O6 Co1 2.120(2) 2_755
O7 C19 1.251(3) .
O7 Co3 2.0821(19) 2_645
O8 C19 1.266(3) .
O8 Co2 2.110(2) 2_655
O9 H9B 0.8500 .
O9 H9A 0.8499 .
O10 Co3 2.0761(17) 3_666
O10 H10D 0.9800 .
O11 H11A 0.8500 .
O11 H11B 0.8502 .
O12 H12B 0.8499 .
O12 H12A 0.8500 .
O13 H13B 0.8499 .
O13 H13A 0.8501 .
C1 C2 1.512(3) .
C2 C8 1.393(3) .
C2 C3 1.396(3) .
C3 C5 1.395(3) .
C3 C4 1.503(3) .
C5 C6 1.386(3) .
C5 H5 0.9300 .
C6 C7 1.405(3) .
C6 C16 1.490(3) .
C7 C8 1.395(3) .
C7 C9 1.497(3) .
C8 H8 0.9300 .
C9 C10 1.387(3) .
C9 C15 1.392(4) .
C10 C11 1.397(3) .
C10 H10 0.9300 .
C11 C13 1.387(4) .
C11 C12 1.482(4) .
C13 C14 1.380(4) .
C13 H13 0.9300 .
C14 C15 1.387(4) .
C14 H14 0.9300 .
C15 H15 0.9300 .
C16 C17 1.395(3) .
C16 C22 1.399(3) .
C17 C18 1.391(3) .
C17 H17 0.9300 .
C18 C20 1.402(3) .
C18 C19 1.506(3) .
C20 C21 1.382(3) .
C20 H20 0.9300 .
C21 C22 1.393(3) .
C21 H21 0.9300 .
C22 H22 0.9300 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O9 Co1 O2 C1 138.5(2) 3_746 .
O9 Co1 O2 C1 -41.5(2) . .
O2 Co1 O2 C1 -74(100) 3_746 .
O6 Co1 O2 C1 46.6(2) 2_745 .
O6 Co1 O2 C1 -133.4(2) 4_556 .
O10 Co2 O4 C4 -140.0(2) . .
O10 Co2 O4 C4 40.0(2) 3_656 .
O4 Co2 O4 C4 -43(100) 3_656 .
O8 Co2 O4 C4 -55.4(2) 2_645 .
O8 Co2 O4 C4 124.6(2) 4_566 .
O10 Co2 O10 Co3 143(100) 3_656 3_666
O4 Co2 O10 Co3 -74.50(9) . 3_666
O4 Co2 O10 Co3 105.50(9) 3_656 3_666
O8 Co2 O10 Co3 -164.71(9) 2_645 3_666
O8 Co2 O10 Co3 15.29(9) 4_566 3_666
O10 Co2 O10 Co3 27(100) 3_656 .
O4 Co2 O10 Co3 168.81(9) . .
O4 Co2 O10 Co3 -11.19(9) 3_656 .
O8 Co2 O10 Co3 78.60(9) 2_645 .
O8 Co2 O10 Co3 -101.40(9) 4_566 .
O10 Co3 O10 Co3 0.0 3_666 3_666
O7 Co3 O10 Co3 95.28(7) 2_655 3_666
O3 Co3 O10 Co3 -91.58(7) 3_656 3_666
O12 Co3 O10 Co3 -51.6(8) . 3_666
O11 Co3 O10 Co3 177.58(7) . 3_666
O10 Co3 O10 Co2 129.19(11) 3_666 .
O7 Co3 O10 Co2 -135.53(8) 2_655 .
O3 Co3 O10 Co2 37.61(9) 3_656 .
O12 Co3 O10 Co2 77.5(8) . .
O11 Co3 O10 Co2 -53.24(9) . .
Co1 O2 C1 O1 31.6(4) . .
Co1 O2 C1 C2 -144.59(17) . .
O1 C1 C2 C8 -65.7(3) . .
O2 C1 C2 C8 110.7(3) . .
O1 C1 C2 C3 117.9(3) . .
O2 C1 C2 C3 -65.7(3) . .
C8 C2 C3 C5 3.5(3) . .
C1 C2 C3 C5 179.9(2) . .
C8 C2 C3 C4 179.9(2) . .
C1 C2 C3 C4 -3.8(4) . .
Co3 O3 C4 O4 -10.0(3) 3_656 .
Co3 O3 C4 C3 171.24(15) 3_656 .
Co2 O4 C4 O3 -45.6(3) . .
Co2 O4 C4 C3 133.21(18) . .
C5 C3 C4 O3 137.8(2) . .
C2 C3 C4 O3 -38.6(3) . .
C5 C3 C4 O4 -41.0(3) . .
C2 C3 C4 O4 142.5(2) . .
C2 C3 C5 C6 -1.4(4) . .
C4 C3 C5 C6 -177.9(2) . .
C3 C5 C6 C7 -3.4(3) . .
C3 C5 C6 C16 174.4(2) . .
C5 C6 C7 C8 6.0(3) . .
C16 C6 C7 C8 -171.9(2) . .
C5 C6 C7 C9 -169.4(2) . .
C16 C6 C7 C9 12.7(3) . .
C3 C2 C8 C7 -0.9(4) . .
C1 C2 C8 C7 -177.5(2) . .
C6 C7 C8 C2 -4.0(4) . .
C9 C7 C8 C2 171.4(2) . .
C8 C7 C9 C10 62.6(3) . .
C6 C7 C9 C10 -122.1(3) . .
C8 C7 C9 C15 -118.3(3) . .
C6 C7 C9 C15 57.0(3) . .
C15 C9 C10 C11 -3.0(4) . .
C7 C9 C10 C11 176.1(2) . .
C9 C10 C11 C13 0.6(4) . .
C9 C10 C11 C12 -178.8(2) . .
Co1 O6 C12 O5 -16.4(5) 2_755 .
Co1 O6 C12 C11 163.5(2) 2_755 .
C13 C11 C12 O6 -13.9(4) . .
C10 C11 C12 O6 165.5(3) . .
C13 C11 C12 O5 166.0(2) . .
C10 C11 C12 O5 -14.6(4) . .
C10 C11 C13 C14 2.5(4) . .
C12 C11 C13 C14 -178.1(2) . .
C11 C13 C14 C15 -3.1(4) . .
C13 C14 C15 C9 0.7(4) . .
C10 C9 C15 C14 2.4(4) . .
C7 C9 C15 C14 -176.8(2) . .
C5 C6 C16 C17 -127.6(2) . .
C7 C6 C16 C17 50.2(3) . .
C5 C6 C16 C22 53.5(3) . .
C7 C6 C16 C22 -128.7(3) . .
C22 C16 C17 C18 3.5(4) . .
C6 C16 C17 C18 -175.4(2) . .
C16 C17 C18 C20 -0.6(4) . .
C16 C17 C18 C19 178.9(2) . .
Co3 O7 C19 O8 20.0(4) 2_645 .
Co3 O7 C19 C18 -159.48(16) 2_645 .
Co2 O8 C19 O7 24.9(4) 2_655 .
Co2 O8 C19 C18 -155.57(17) 2_655 .
C17 C18 C19 O7 15.7(3) . .
C20 C18 C19 O7 -164.8(2) . .
C17 C18 C19 O8 -163.9(2) . .
C20 C18 C19 O8 15.6(3) . .
C17 C18 C20 C21 -2.5(4) . .
C19 C18 C20 C21 178.0(2) . .
C18 C20 C21 C22 2.7(4) . .
C20 C21 C22 C16 0.3(4) . .
C17 C16 C22 C21 -3.3(4) . .
C6 C16 C22 C21 175.6(2) . .
