#------------------------------------------------------------------------------
#$Date: 2016-03-25 23:23:56 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180037 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/31/7033190.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7033190
loop_
_publ_author_name
'Zhang, Xiu-Mei'
'Li, Peng'
'Gao, Wei'
'Liu, Jie-Ping'
'Gao, En-Qing'
_publ_section_title
;
 3D Co(II) coordination polymer with ferrimagnetic-like layers based on
 azide and tetrazolate bridges showing slow magnetic dynamics.
;
_journal_issue                   2
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              511
_journal_page_last               514
_journal_paper_doi               10.1039/c4dt03332a
_journal_volume                  44
_journal_year                    2015
_chemical_formula_sum            'C36 H24 Co6 N48'
_chemical_formula_weight         1482.61
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                107.263(2)
_cell_angle_beta                 106.136(2)
_cell_angle_gamma                90.3700(10)
_cell_formula_units_Z            1
_cell_length_a                   10.5940(8)
_cell_length_b                   10.7589(9)
_cell_length_c                   13.1841(11)
_cell_measurement_temperature    298(2)
_cell_volume                     1372.00(19)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.968
_diffrn_measured_fraction_theta_max 0.968
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.1982
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            4688
_diffrn_reflns_theta_full        25.02
_diffrn_reflns_theta_max         25.02
_diffrn_reflns_theta_min         2.96
_diffrn_standards_decay_%        2.5
_exptl_absorpt_coefficient_mu    1.853
_exptl_absorpt_correction_T_max  0.9130
_exptl_absorpt_correction_T_min  0.7814
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.794
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             738
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.195
_refine_diff_density_min         -2.986
_refine_diff_density_rms         0.232
_refine_ls_extinction_coef       0.000(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.902
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     411
_refine_ls_number_reflns         4688
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      0.906
_refine_ls_R_factor_all          0.1684
_refine_ls_R_factor_gt           0.1043
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1797P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2501
_refine_ls_wR_factor_ref         0.2902
_reflns_number_gt                2429
_reflns_number_total             4688
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4dt03332a2.cif
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 7033190.cif.
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7033190
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Co3 Co 0.19941(17) 0.53348(17) 0.33045(15) 0.0189(5) Uani 1 1 d .
Co2 Co 0.21228(17) 0.41759(17) 0.03551(15) 0.0184(5) Uani 1 1 d .
Co1 Co 0.5000 0.5000 0.0000 0.0196(7) Uani 1 2 d S
Co4 Co 0.5000 0.5000 0.5000 0.0162(6) Uani 1 2 d S
N1 N 0.5061(11) 0.4859(11) 0.1690(9) 0.021(3) Uani 1 1 d .
N2 N 0.3816(10) 0.4868(10) 0.1745(10) 0.019(3) Uani 1 1 d .
N3 N 0.3805(10) 0.5130(11) 0.2765(9) 0.020(3) Uani 1 1 d .
N4 N 0.5046(10) 0.5286(11) 0.3432(9) 0.021(3) Uani 1 1 d .
N5 N 1.0029(11) 0.5250(11) 0.3548(10) 0.024(3) Uani 1 1 d .
N6 N 0.1699(11) 0.2214(11) 0.3158(10) 0.022(3) Uani 1 1 d .
N7 N 0.2379(11) 0.3412(11) 0.3505(10) 0.026(3) Uani 1 1 d .
N8 N 0.3616(11) 0.3324(11) 0.4046(10) 0.022(3) Uani 1 1 d .
N9 N 0.3777(11) 0.2134(11) 0.4122(10) 0.024(3) Uani 1 1 d .
N11 N 0.1808(11) 0.7273(11) 0.0209(11) 0.028(3) Uani 1 1 d .
N12 N 0.2448(11) 0.6178(11) 0.0215(10) 0.024(3) Uani 1 1 d .
N13 N 0.3672(11) 0.6470(11) 0.0261(10) 0.023(3) Uani 1 1 d .
N14 N 0.3901(11) 0.7712(11) 0.0311(10) 0.024(3) Uani 1 1 d .
N16 N 0.1107(11) 0.4680(12) 0.1569(11) 0.033(3) Uani 1 1 d D
N17 N 0.0310(12) 0.5603(12) 0.1290(11) 0.036(3) Uani 1 1 d D
N18 N -0.0350(11) 0.6363(12) 0.0889(11) 0.034(3) Uani 1 1 d D
N19 N 0.3301(11) 0.6010(10) 0.4917(9) 0.021(3) Uani 1 1 d D
N20 N 0.3250(13) 0.6997(12) 0.5639(11) 0.035(3) Uani 1 1 d D
N21 N 0.3187(19) 0.7908(15) 0.6335(14) 0.075(6) Uani 1 1 d D
N22 N 0.3326(11) 0.3725(11) -0.0648(10) 0.027(3) Uani 1 1 d .
N23 N 0.3105(14) 0.2717(15) -0.1463(13) 0.045(4) Uani 1 1 d .
N24 N 0.286(2) 0.179(2) -0.2319(19) 0.098(7) Uani 1 1 d .
C1 C 0.5811(12) 0.5124(14) 0.2767(12) 0.020(3) Uani 1 1 d .
C4 C 0.9185(14) 0.4148(14) 0.2781(13) 0.030(4) Uani 1 1 d .
H4A H 0.9555 0.3431 0.2419 0.036 Uiso 1 1 calc R
C3 C 0.7886(13) 0.4105(13) 0.2562(12) 0.023(3) Uani 1 1 d .
H3A H 0.7362 0.3365 0.2050 0.028 Uiso 1 1 calc R
C2 C 0.7289(12) 0.5164(14) 0.3094(12) 0.019(3) Uani 1 1 d .
C6 C 0.8088(13) 0.6172(14) 0.3912(12) 0.026(3) Uani 1 1 d .
H6A H 0.7740 0.6837 0.4355 0.031 Uiso 1 1 calc R
C5 C 0.9471(14) 0.6182(15) 0.4071(13) 0.029(4) Uani 1 1 d .
H5A H 1.0008 0.6911 0.4588 0.035 Uiso 1 1 calc R
C7 C 0.2595(13) 0.1471(13) 0.3582(12) 0.023(3) Uani 1 1 d .
C13 C 0.2750(14) 0.8177(13) 0.0304(12) 0.021(3) Uani 1 1 d .
C8 C 0.2369(14) 0.0085(13) 0.3487(13) 0.026(3) Uani 1 1 d .
C9 C 0.3399(15) -0.0643(14) 0.3637(14) 0.034(4) Uani 1 1 d .
H9A H 0.4251 -0.0279 0.3769 0.040 Uiso 1 1 calc R
C12 C 0.1114(15) -0.0576(14) 0.3202(13) 0.032(4) Uani 1 1 d .
H12A H 0.0363 -0.0145 0.3035 0.039 Uiso 1 1 calc R
C11 C 0.0994(14) -0.1851(14) 0.3167(12) 0.028(4) Uani 1 1 d .
H11A H 0.0148 -0.2254 0.2993 0.033 Uiso 1 1 calc R
N10 N 0.2011(12) -0.2556(12) 0.3368(10) 0.032(3) Uani 1 1 d .
C10 C 0.3188(15) -0.1916(14) 0.3595(13) 0.031(4) Uani 1 1 d .
H10A H 0.3926 -0.2372 0.3737 0.037 Uiso 1 1 calc R
C14 C 0.2512(15) 0.9508(15) 0.0329(15) 0.038(4) Uani 1 1 d .
C15 C 0.3501(17) 1.0490(15) 0.0919(15) 0.047(5) Uani 1 1 d .
H15A H 0.4310 1.0296 0.1311 0.057 Uiso 1 1 calc R
C18 C 0.1378(17) 0.9873(16) -0.0376(17) 0.052(5) Uani 1 1 d .
H18A H 0.0726 0.9238 -0.0894 0.062 Uiso 1 1 calc R
C17 C 0.1267(18) 1.1205(17) -0.0275(17) 0.053(5) Uani 1 1 d .
H17A H 0.0513 1.1435 -0.0715 0.063 Uiso 1 1 calc R
C16 C 0.3316(16) 1.1777(16) 0.0942(15) 0.043(5) Uani 1 1 d .
H16A H 0.4030 1.2403 0.1344 0.052 Uiso 1 1 calc R
N15 N 0.2223(12) 1.2179(12) 0.0446(11) 0.030(3) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N19 Co3 N16 165.9(4) . .
N19 Co3 N7 83.2(4) . .
N16 Co3 N7 97.0(4) . .
N19 Co3 N5 104.6(4) . 1_455
N16 Co3 N5 89.5(5) . 1_455
N7 Co3 N5 93.4(4) . 1_455
N19 Co3 N3 84.9(4) . .
N16 Co3 N3 81.1(4) . .
N7 Co3 N3 82.9(4) . .
N5 Co3 N3 169.3(4) 1_455 .
N19 Co3 N10 85.9(4) . 1_565
N16 Co3 N10 92.4(4) . 1_565
N7 Co3 N10 168.0(4) . 1_565
N5 Co3 N10 94.1(5) 1_455 1_565
N3 Co3 N10 91.3(4) . 1_565
N22 Co2 N18 97.1(5) . 2_565
N22 Co2 N16 172.4(5) . .
N18 Co2 N16 90.4(5) 2_565 .
N22 Co2 N2 89.1(5) . .
N18 Co2 N2 173.4(5) 2_565 .
N16 Co2 N2 83.5(4) . .
N22 Co2 N15 87.3(5) . 1_545
N18 Co2 N15 91.1(5) 2_565 1_545
N16 Co2 N15 91.4(5) . 1_545
N2 Co2 N15 91.7(4) . 1_545
N22 Co2 N12 82.1(4) . .
N18 Co2 N12 96.0(4) 2_565 .
N16 Co2 N12 98.3(4) . .
N2 Co2 N12 82.2(4) . .
N15 Co2 N12 167.8(4) 1_545 .
N22 Co1 N22 180.000(1) 2_665 .
N22 Co1 N13 84.6(5) 2_665 2_665
N22 Co1 N13 95.4(5) . 2_665
N22 Co1 N13 95.4(5) 2_665 .
N22 Co1 N13 84.6(5) . .
N13 Co1 N13 180.0(7) 2_665 .
N22 Co1 N1 92.1(4) 2_665 .
N22 Co1 N1 87.9(4) . .
N13 Co1 N1 93.2(4) 2_665 .
N13 Co1 N1 86.8(4) . .
N22 Co1 N1 87.9(4) 2_665 2_665
N22 Co1 N1 92.1(4) . 2_665
N13 Co1 N1 86.8(4) 2_665 2_665
N13 Co1 N1 93.2(4) . 2_665
N1 Co1 N1 180.0(5) . 2_665
N19 Co4 N19 180.000(2) 2_666 .
N19 Co4 N8 83.9(4) 2_666 2_666
N19 Co4 N8 96.1(4) . 2_666
N19 Co4 N8 96.1(4) 2_666 .
N19 Co4 N8 83.9(4) . .
N8 Co4 N8 180.000(1) 2_666 .
N19 Co4 N4 88.5(4) 2_666 2_666
N19 Co4 N4 91.5(4) . 2_666
N8 Co4 N4 88.0(4) 2_666 2_666
N8 Co4 N4 92.0(4) . 2_666
N19 Co4 N4 91.5(4) 2_666 .
N19 Co4 N4 88.5(4) . .
N8 Co4 N4 92.0(4) 2_666 .
N8 Co4 N4 88.0(4) . .
N4 Co4 N4 180.000(1) 2_666 .
N2 N1 C1 104.2(11) . .
N2 N1 Co1 107.0(7) . .
C1 N1 Co1 145.2(9) . .
N3 N2 N1 110.3(10) . .
N3 N2 Co2 124.1(8) . .
N1 N2 Co2 124.5(9) . .
N2 N3 N4 109.6(10) . .
N2 N3 Co3 124.3(8) . .
N4 N3 Co3 126.0(9) . .
C1 N4 N3 105.6(11) . .
C1 N4 Co4 140.6(9) . .
N3 N4 Co4 108.6(8) . .
C5 N5 C4 116.4(12) . .
C5 N5 Co3 128.2(10) . 1_655
C4 N5 Co3 112.9(9) . 1_655
C7 N6 N7 103.6(10) . .
N8 N7 N6 108.4(10) . .
N8 N7 Co3 114.5(8) . .
N6 N7 Co3 136.9(9) . .
N9 N8 N7 111.1(10) . .
N9 N8 Co4 124.4(8) . .
N7 N8 Co4 122.9(9) . .
N8 N9 C7 104.4(10) . .
C13 N11 N12 104.2(11) . .
N13 N12 N11 107.1(10) . .
N13 N12 Co2 112.6(8) . .
N11 N12 Co2 139.9(9) . .
N12 N13 N14 112.4(11) . .
N12 N13 Co1 121.8(8) . .
N14 N13 Co1 125.0(8) . .
C13 N14 N13 103.1(10) . .
N17 N16 Co3 108.1(9) . .
N17 N16 Co2 104.4(9) . .
Co3 N16 Co2 125.6(5) . .
N18 N17 N16 170.0(15) . .
N17 N18 Co2 124.4(10) . 2_565
N20 N19 Co3 126.3(10) . .
N20 N19 Co4 122.3(10) . .
Co3 N19 Co4 109.8(5) . .
N21 N20 N19 178.0(18) . .
N23 N22 Co2 122.6(10) . .
N23 N22 Co1 126.3(11) . .
Co2 N22 Co1 110.6(6) . .
N24 N23 N22 174.9(19) . .
N4 C1 N1 110.4(11) . .
N4 C1 C2 127.1(12) . .
N1 C1 C2 122.5(12) . .
C3 C4 N5 122.0(13) . .
C3 C4 H4A 119.0 . .
N5 C4 H4A 119.0 . .
C4 C3 C2 120.8(13) . .
C4 C3 H3A 119.6 . .
C2 C3 H3A 119.6 . .
C6 C2 C3 117.8(12) . .
C6 C2 C1 122.8(13) . .
C3 C2 C1 119.4(12) . .
C2 C6 C5 118.1(13) . .
C2 C6 H6A 120.9 . .
C5 C6 H6A 120.9 . .
N5 C5 C6 124.3(14) . .
N5 C5 H5A 117.8 . .
C6 C5 H5A 117.8 . .
N9 C7 N6 112.4(11) . .
N9 C7 C8 120.9(12) . .
N6 C7 C8 126.7(11) . .
N14 C13 N11 113.2(12) . .
N14 C13 C14 123.2(12) . .
N11 C13 C14 123.5(12) . .
C9 C8 C12 115.9(13) . .
C9 C8 C7 120.2(12) . .
C12 C8 C7 123.8(13) . .
C8 C9 C10 119.9(14) . .
C8 C9 H9A 120.0 . .
C10 C9 H9A 120.0 . .
C11 C12 C8 120.0(14) . .
C11 C12 H12A 120.0 . .
C8 C12 H12A 120.0 . .
N10 C11 C12 124.2(13) . .
N10 C11 H11A 117.9 . .
C12 C11 H11A 117.9 . .
C10 N10 C11 114.4(12) . .
C10 N10 Co3 116.6(10) . 1_545
C11 N10 Co3 129.0(9) . 1_545
N10 C10 C9 125.4(14) . .
N10 C10 H10A 117.3 . .
C9 C10 H10A 117.3 . .
C15 C14 C18 115.1(14) . .
C15 C14 C13 119.4(14) . .
C18 C14 C13 124.7(14) . .
C14 C15 C16 120.9(15) . .
C14 C15 H15A 119.5 . .
C16 C15 H15A 119.5 . .
C17 C18 C14 119.2(15) . .
C17 C18 H18A 120.4 . .
C14 C18 H18A 120.4 . .
N15 C17 C18 122.8(16) . .
N15 C17 H17A 118.6 . .
C18 C17 H17A 118.6 . .
N15 C16 C15 125.5(15) . .
N15 C16 H16A 117.3 . .
C15 C16 H16A 117.3 . .
C16 N15 C17 115.2(14) . .
C16 N15 Co2 122.1(10) . 1_565
C17 N15 Co2 120.1(10) . 1_565
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Co3 N19 2.097(11) .
Co3 N16 2.111(13) .
Co3 N7 2.189(11) .
Co3 N5 2.198(11) 1_455
Co3 N3 2.215(11) .
Co3 N10 2.245(12) 1_565
Co2 N22 2.043(13) .
Co2 N18 2.065(12) 2_565
Co2 N16 2.113(14) .
Co2 N2 2.116(11) .
Co2 N15 2.188(12) 1_545
Co2 N12 2.249(11) .
Co1 N22 2.046(11) 2_665
Co1 N22 2.046(11) .
Co1 N13 2.139(11) 2_665
Co1 N13 2.139(11) .
Co1 N1 2.261(11) .
Co1 N1 2.261(11) 2_665
Co4 N19 2.102(11) 2_666
Co4 N19 2.102(11) .
Co4 N8 2.140(11) 2_666
Co4 N8 2.140(11) .
Co4 N4 2.193(11) 2_666
Co4 N4 2.193(11) .
N1 N2 1.340(15) .
N1 C1 1.363(17) .
N2 N3 1.294(14) .
N3 N4 1.340(14) .
N4 C1 1.327(17) .
N5 C5 1.286(19) .
N5 C4 1.414(17) .
N5 Co3 2.198(11) 1_655
N6 C7 1.353(16) .
N6 N7 1.358(15) .
N7 N8 1.325(15) .
N8 N9 1.323(15) .
N9 C7 1.333(16) .
N11 C13 1.343(16) .
N11 N12 1.364(15) .
N12 N13 1.312(15) .
N13 N14 1.336(15) .
N14 C13 1.319(17) .
N16 N17 1.374(12) .
N17 N18 1.223(12) .
N18 Co2 2.065(12) 2_565
N19 N20 1.211(12) .
N20 N21 1.144(13) .
N22 N23 1.245(18) .
N23 N24 1.23(2) .
C1 C2 1.501(17) .
C4 C3 1.323(19) .
C4 H4A 0.9300 .
C3 C2 1.40(2) .
C3 H3A 0.9300 .
C2 C6 1.357(19) .
C6 C5 1.421(19) .
C6 H6A 0.9300 .
C5 H5A 0.9300 .
C7 C8 1.471(18) .
C13 C14 1.448(19) .
C8 C9 1.35(2) .
C8 C12 1.403(19) .
C9 C10 1.369(19) .
C9 H9A 0.9300 .
C12 C11 1.362(19) .
C12 H12A 0.9300 .
C11 N10 1.333(18) .
C11 H11A 0.9300 .
N10 C10 1.333(18) .
N10 Co3 2.245(12) 1_545
C10 H10A 0.9300 .
C14 C15 1.37(2) .
C14 C18 1.44(2) .
C15 C16 1.39(2) .
C15 H15A 0.9300 .
C18 C17 1.41(2) .
C18 H18A 0.9300 .
C17 N15 1.37(2) .
C17 H17A 0.9300 .
C16 N15 1.307(19) .
C16 H16A 0.9300 .
N15 Co2 2.188(12) 1_565
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N22 Co1 N1 N2 138.9(8) 2_665 .
N22 Co1 N1 N2 -41.1(8) . .
N13 Co1 N1 N2 -136.4(8) 2_665 .
N13 Co1 N1 N2 43.6(8) . .
N1 Co1 N1 N2 -59(100) 2_665 .
N22 Co1 N1 C1 -13.4(17) 2_665 .
N22 Co1 N1 C1 166.6(17) . .
N13 Co1 N1 C1 71.3(17) 2_665 .
N13 Co1 N1 C1 -108.7(17) . .
N1 Co1 N1 C1 148(100) 2_665 .
C1 N1 N2 N3 0.7(13) . .
Co1 N1 N2 N3 -163.5(8) . .
C1 N1 N2 Co2 -167.7(8) . .
Co1 N1 N2 Co2 28.2(10) . .
N22 Co2 N2 N3 -167.2(10) . .
N18 Co2 N2 N3 35(4) 2_565 .
N16 Co2 N2 N3 11.3(10) . .
N15 Co2 N2 N3 -79.9(10) 1_545 .
N12 Co2 N2 N3 110.7(10) . .
N22 Co2 N2 N1 -0.4(10) . .
N18 Co2 N2 N1 -158(4) 2_565 .
N16 Co2 N2 N1 178.1(10) . .
N15 Co2 N2 N1 86.9(10) 1_545 .
N12 Co2 N2 N1 -82.6(9) . .
N1 N2 N3 N4 -0.9(13) . .
Co2 N2 N3 N4 167.5(8) . .
N1 N2 N3 Co3 177.5(8) . .
Co2 N2 N3 Co3 -14.1(13) . .
N19 Co3 N3 N2 -170.8(10) . .
N16 Co3 N3 N2 7.2(10) . .
N7 Co3 N3 N2 105.4(10) . .
N5 Co3 N3 N2 35(3) 1_455 .
N10 Co3 N3 N2 -85.1(10) 1_565 .
N19 Co3 N3 N4 7.3(10) . .
N16 Co3 N3 N4 -174.7(11) . .
N7 Co3 N3 N4 -76.4(10) . .
N5 Co3 N3 N4 -147(2) 1_455 .
N10 Co3 N3 N4 93.1(10) 1_565 .
N2 N3 N4 C1 0.8(14) . .
Co3 N3 N4 C1 -177.6(9) . .
N2 N3 N4 Co4 -159.2(8) . .
Co3 N3 N4 Co4 22.4(12) . .
N19 Co4 N4 C1 -8.2(15) 2_666 .
N19 Co4 N4 C1 171.8(15) . .
N8 Co4 N4 C1 75.7(15) 2_666 .
N8 Co4 N4 C1 -104.3(15) . .
N4 Co4 N4 C1 -161(100) 2_666 .
N19 Co4 N4 N3 140.6(9) 2_666 .
N19 Co4 N4 N3 -39.4(9) . .
N8 Co4 N4 N3 -135.5(9) 2_666 .
N8 Co4 N4 N3 44.5(9) . .
N4 Co4 N4 N3 -12(100) 2_666 .
C7 N6 N7 N8 3.2(15) . .
C7 N6 N7 Co3 178.1(11) . .
N19 Co3 N7 N8 -38.1(10) . .
N16 Co3 N7 N8 127.7(10) . .
N5 Co3 N7 N8 -142.4(10) 1_455 .
N3 Co3 N7 N8 47.6(10) . .
N10 Co3 N7 N8 -14(3) 1_565 .
N19 Co3 N7 N6 147.2(14) . .
N16 Co3 N7 N6 -47.0(14) . .
N5 Co3 N7 N6 42.9(14) 1_455 .
N3 Co3 N7 N6 -127.1(14) . .
N10 Co3 N7 N6 171.5(19) 1_565 .
N6 N7 N8 N9 -3.0(16) . .
Co3 N7 N8 N9 -179.2(8) . .
N6 N7 N8 Co4 -168.9(8) . .
Co3 N7 N8 Co4 14.9(13) . .
N19 Co4 N8 N9 33.1(11) 2_666 .
N19 Co4 N8 N9 -146.9(11) . .
N8 Co4 N8 N9 -144(100) 2_666 .
N4 Co4 N8 N9 -55.7(11) 2_666 .
N4 Co4 N8 N9 124.3(11) . .
N19 Co4 N8 N7 -162.9(11) 2_666 .
N19 Co4 N8 N7 17.1(11) . .
N8 Co4 N8 N7 20(100) 2_666 .
N4 Co4 N8 N7 108.3(11) 2_666 .
N4 Co4 N8 N7 -71.7(11) . .
N7 N8 N9 C7 1.5(16) . .
Co4 N8 N9 C7 167.1(10) . .
C13 N11 N12 N13 -2.7(15) . .
C13 N11 N12 Co2 168.6(12) . .
N22 Co2 N12 N13 -40.4(9) . .
N18 Co2 N12 N13 -136.8(10) 2_565 .
N16 Co2 N12 N13 131.9(9) . .
N2 Co2 N12 N13 49.7(9) . .
N15 Co2 N12 N13 -11(3) 1_545 .
N22 Co2 N12 N11 148.6(16) . .
N18 Co2 N12 N11 52.3(16) 2_565 .
N16 Co2 N12 N11 -39.0(16) . .
N2 Co2 N12 N11 -121.2(15) . .
N15 Co2 N12 N11 178.3(19) 1_545 .
N11 N12 N13 N14 1.3(15) . .
Co2 N12 N13 N14 -172.6(9) . .
N11 N12 N13 Co1 -168.9(9) . .
Co2 N12 N13 Co1 17.2(12) . .
N22 Co1 N13 N12 -164.6(10) 2_665 .
N22 Co1 N13 N12 15.4(10) . .
N13 Co1 N13 N12 14(100) 2_665 .
N1 Co1 N13 N12 -72.7(10) . .
N1 Co1 N13 N12 107.3(10) 2_665 .
N22 Co1 N13 N14 26.5(11) 2_665 .
N22 Co1 N13 N14 -153.5(11) . .
N13 Co1 N13 N14 -155(100) 2_665 .
N1 Co1 N13 N14 118.3(11) . .
N1 Co1 N13 N14 -61.7(11) 2_665 .
N12 N13 N14 C13 0.6(15) . .
Co1 N13 N14 C13 170.5(9) . .
N19 Co3 N16 N17 -114.0(17) . .
N7 Co3 N16 N17 156.2(9) . .
N5 Co3 N16 N17 62.8(10) 1_455 .
N3 Co3 N16 N17 -122.2(10) . .
N10 Co3 N16 N17 -31.3(10) 1_565 .
N19 Co3 N16 Co2 10(2) . .
N7 Co3 N16 Co2 -80.0(7) . .
N5 Co3 N16 Co2 -173.4(7) 1_455 .
N3 Co3 N16 Co2 1.6(6) . .
N10 Co3 N16 Co2 92.5(7) 1_565 .
N22 Co2 N16 N17 131(3) . .
N18 Co2 N16 N17 -57.7(9) 2_565 .
N2 Co2 N16 N17 119.6(9) . .
N15 Co2 N16 N17 -148.8(9) 1_545 .
N12 Co2 N16 N17 38.5(9) . .
N22 Co2 N16 Co3 6(4) . .
N18 Co2 N16 Co3 177.0(7) 2_565 .
N2 Co2 N16 Co3 -5.8(6) . .
N15 Co2 N16 Co3 85.8(7) 1_545 .
N12 Co2 N16 Co3 -86.9(7) . .
Co3 N16 N17 N18 149(8) . .
Co2 N16 N17 N18 13(8) . .
N16 N17 N18 Co2 74(8) . 2_565
N16 Co3 N19 N20 122.4(18) . .
N7 Co3 N19 N20 -146.1(12) . .
N5 Co3 N19 N20 -54.4(12) 1_455 .
N3 Co3 N19 N20 130.5(12) . .
N10 Co3 N19 N20 38.8(12) 1_565 .
N16 Co3 N19 Co4 -43.3(19) . .
N7 Co3 N19 Co4 48.3(5) . .
N5 Co3 N19 Co4 140.0(5) 1_455 .
N3 Co3 N19 Co4 -35.2(5) . .
N10 Co3 N19 Co4 -126.8(5) 1_565 .
N19 Co4 N19 N20 -174(100) 2_666 .
N8 Co4 N19 N20 -29.3(12) 2_666 .
N8 Co4 N19 N20 150.7(12) . .
N4 Co4 N19 N20 58.9(11) 2_666 .
N4 Co4 N19 N20 -121.1(11) . .
N19 Co4 N19 Co3 -8(100) 2_666 .
N8 Co4 N19 Co3 137.0(5) 2_666 .
N8 Co4 N19 Co3 -43.0(5) . .
N4 Co4 N19 Co3 -134.8(5) 2_666 .
N4 Co4 N19 Co3 45.2(5) . .
Co3 N19 N20 N21 102(53) . .
Co4 N19 N20 N21 -94(53) . .
N18 Co2 N22 N23 -41.6(12) 2_565 .
N16 Co2 N22 N23 130(3) . .
N2 Co2 N22 N23 141.0(12) . .
N15 Co2 N22 N23 49.3(12) 1_545 .
N12 Co2 N22 N23 -136.7(12) . .
N18 Co2 N22 Co1 145.9(6) 2_565 .
N16 Co2 N22 Co1 -43(4) . .
N2 Co2 N22 Co1 -31.5(5) . .
N15 Co2 N22 Co1 -123.2(6) 1_545 .
N12 Co2 N22 Co1 50.8(5) . .
N22 Co1 N22 N23 140(100) 2_665 .
N13 Co1 N22 N23 -37.6(13) 2_665 .
N13 Co1 N22 N23 142.4(13) . .
N1 Co1 N22 N23 -130.6(13) . .
N1 Co1 N22 N23 49.4(13) 2_665 .
N22 Co1 N22 Co2 -48(100) 2_665 .
N13 Co1 N22 Co2 134.6(5) 2_665 .
N13 Co1 N22 Co2 -45.4(5) . .
N1 Co1 N22 Co2 41.6(5) . .
N1 Co1 N22 Co2 -138.4(5) 2_665 .
Co2 N22 N23 N24 108(21) . .
Co1 N22 N23 N24 -81(21) . .
N3 N4 C1 N1 -0.3(15) . .
Co4 N4 C1 N1 149.0(11) . .
N3 N4 C1 C2 -178.3(13) . .
Co4 N4 C1 C2 -29(2) . .
N2 N1 C1 N4 -0.2(14) . .
Co1 N1 C1 N4 152.6(11) . .
N2 N1 C1 C2 177.8(12) . .
Co1 N1 C1 C2 -29(2) . .
C5 N5 C4 C3 4(2) . .
Co3 N5 C4 C3 -159.6(12) 1_655 .
N5 C4 C3 C2 0(2) . .
C4 C3 C2 C6 -6(2) . .
C4 C3 C2 C1 175.6(14) . .
N4 C1 C2 C6 -52(2) . .
N1 C1 C2 C6 130.2(15) . .
N4 C1 C2 C3 126.0(15) . .
N1 C1 C2 C3 -51.7(18) . .
C3 C2 C6 C5 9(2) . .
C1 C2 C6 C5 -173.1(13) . .
C4 N5 C5 C6 -1(2) . .
Co3 N5 C5 C6 159.5(11) 1_655 .
C2 C6 C5 N5 -5(2) . .
N8 N9 C7 N6 0.7(17) . .
N8 N9 C7 C8 -179.7(13) . .
N7 N6 C7 N9 -2.4(17) . .
N7 N6 C7 C8 178.0(14) . .
N13 N14 C13 N11 -2.5(16) . .
N13 N14 C13 C14 -179.0(14) . .
N12 N11 C13 N14 3.3(17) . .
N12 N11 C13 C14 179.8(14) . .
N9 C7 C8 C9 -20(2) . .
N6 C7 C8 C9 159.5(16) . .
N9 C7 C8 C12 162.5(16) . .
N6 C7 C8 C12 -18(2) . .
C12 C8 C9 C10 -5(2) . .
C7 C8 C9 C10 177.2(15) . .
C9 C8 C12 C11 5(2) . .
C7 C8 C12 C11 -177.8(15) . .
C8 C12 C11 N10 -2(2) . .
C12 C11 N10 C10 -1(2) . .
C12 C11 N10 Co3 -178.2(12) . 1_545
C11 N10 C10 C9 0(2) . .
Co3 N10 C10 C9 177.9(13) 1_545 .
C8 C9 C10 N10 3(3) . .
N14 C13 C14 C15 -35(2) . .
N11 C13 C14 C15 149.2(17) . .
N14 C13 C14 C18 134.0(18) . .
N11 C13 C14 C18 -42(3) . .
C18 C14 C15 C16 9(3) . .
C13 C14 C15 C16 178.6(16) . .
C15 C14 C18 C17 -10(3) . .
C13 C14 C18 C17 -179.6(17) . .
C14 C18 C17 N15 2(3) . .
C14 C15 C16 N15 1(3) . .
C15 C16 N15 C17 -10(3) . .
C15 C16 N15 Co2 -171.7(15) . 1_565
C18 C17 N15 C16 8(3) . .
C18 C17 N15 Co2 169.9(15) . 1_565
