#------------------------------------------------------------------------------
#$Date: 2016-03-25 23:30:47 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180042 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/36/7033670.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7033670
loop_
_publ_author_name
'Vrána, Jan'
'Jambor, Roman'
'R°užička, Aleš'
'Alonso, Mercedes'
'De Proft, Frank'
'Lyčka, Antonín'
'Dostál, Libor'
_publ_section_title
;
 Reactivity of bis(organoamino)phosphanes with magnesium(ii) compounds.
;
_journal_issue                   10
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              4533
_journal_page_last               4545
_journal_paper_doi               10.1039/c4dt03929g
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C52 H62 Mg2 N4 O4 P2, 2(C6 H6)'
_chemical_formula_sum            'C64 H74 Mg2 N4 O4 P2'
_chemical_formula_weight         1073.83
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2014-12-17 deposited with the CCDC.
2015-01-16 downloaded from the CCDC.
;
_cell_angle_alpha                97.586(5)
_cell_angle_beta                 91.018(5)
_cell_angle_gamma                110.470(4)
_cell_formula_units_Z            1
_cell_length_a                   10.9041(7)
_cell_length_b                   11.0920(5)
_cell_length_c                   12.5151(8)
_cell_measurement_reflns_used    27333
_cell_measurement_temperature    150(1)
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      1
_cell_volume                     1402.35(15)
_computing_cell_refinement       'COLLECT and DENZO'
_computing_data_collection
'COLLECT (Hooft, 1998) and DENZO (Otwinowski & Minor, 1997)'
_computing_data_reduction        'COLLECT and DENZO'
_computing_molecular_graphics    'PLATON (Spek, 2003)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SIR92 (Altomare et al., 1994)'
_diffrn_ambient_temperature      150(1)
_diffrn_detector_area_resol_mean 9.091
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker Nonius KappaCCD area detector'
_diffrn_measurement_method       'φ and ω scans to fill the Ewald sphere'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0348
_diffrn_reflns_av_sigmaI/netI    0.0242
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            27272
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         2.89
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.153
_exptl_absorpt_correction_T_max  0.971
_exptl_absorpt_correction_T_min  0.957
_exptl_absorpt_correction_type   integration
_exptl_absorpt_process_details
;
Gaussian integration (Coppens, 1970)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.272
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             572
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.31
_exptl_crystal_size_min          0.25
_refine_diff_density_max         0.493
_refine_diff_density_min         -0.413
_refine_diff_density_rms         0.057
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.087
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     343
_refine_ls_number_reflns         6421
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.087
_refine_ls_R_factor_all          0.0541
_refine_ls_R_factor_gt           0.0415
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0402P)²+1.0720P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0993
_refine_ls_wR_factor_ref         0.1100
_reflns_number_gt                5404
_reflns_number_total             6421
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4dt03929g2.cif
_cod_data_source_block           shelxl
_cod_depositor_comments
'Adding full bibliography for 7033670--7033677.cif.'
_cod_original_cell_volume        1402.33(14)
_cod_database_code               7033670
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
P1 P 0.66016(4) 0.42501(4) 0.13177(3) 0.01803(10) Uani 1 1 d .
Mg1 Mg 0.40705(5) 0.44589(5) 0.09364(4) 0.01686(12) Uani 1 1 d .
O1 O 0.41459(11) 0.56227(11) 0.24057(9) 0.0218(2) Uani 1 1 d .
N2 N 0.50252(13) 0.33073(13) 0.14625(10) 0.0189(3) Uani 1 1 d .
N1 N 0.62725(13) 0.54368(12) 0.07328(10) 0.0176(3) Uani 1 1 d .
O2 O 0.20629(11) 0.34217(12) 0.11742(10) 0.0253(3) Uani 1 1 d .
C1 C 0.71118(15) 0.33235(15) 0.01888(13) 0.0197(3) Uani 1 1 d .
C7 C 0.68369(15) 0.67180(15) 0.13118(12) 0.0185(3) Uani 1 1 d .
C13 C 0.47950(16) 0.24256(15) 0.21882(12) 0.0198(3) Uani 1 1 d .
C6 C 0.82597(16) 0.39416(17) -0.03050(13) 0.0236(3) Uani 1 1 d .
H6 H 0.8673 0.4839 -0.0146 0.028 Uiso 1 1 d R
C18 C 0.35300(17) 0.18920(16) 0.25531(14) 0.0238(3) Uani 1 1 d .
H18 H 0.2859 0.2134 0.2293 0.029 Uiso 1 1 d R
C5 C 0.87916(17) 0.32319(19) -0.10299(14) 0.0285(4) Uani 1 1 d .
H5 H 0.9553 0.3656 -0.1354 0.034 Uiso 1 1 d R
C2 C 0.65255(16) 0.19734(16) -0.00607(14) 0.0238(3) Uani 1 1 d .
H2 H 0.5768 0.1542 0.0265 0.029 Uiso 1 1 d R
C16 C 0.4222(2) 0.06345(17) 0.37015(14) 0.0313(4) Uani 1 1 d .
H16 H 0.4037 0.0056 0.4202 0.038 Uiso 1 1 d R
C12 C 0.79190(16) 0.71458(16) 0.20733(13) 0.0239(3) Uani 1 1 d .
H12 H 0.8318 0.6568 0.2230 0.029 Uiso 1 1 d R
C17 C 0.32544(19) 0.10159(17) 0.32874(14) 0.0287(4) Uani 1 1 d .
H17 H 0.2406 0.0680 0.3507 0.034 Uiso 1 1 d R
C3 C 0.70554(18) 0.12619(17) -0.07911(15) 0.0294(4) Uani 1 1 d .
H3 H 0.6648 0.0364 -0.0956 0.035 Uiso 1 1 d R
C21 C 0.4671(2) 0.74666(19) 0.37270(16) 0.0373(4) Uani 1 1 d .
H21A H 0.4284 0.8017 0.4157 0.045 Uiso 1 1 d R
H21B H 0.5556 0.7987 0.3584 0.045 Uiso 1 1 d R
C22 C 0.38525(18) 0.68038(17) 0.26973(14) 0.0276(4) Uani 1 1 d .
H22A H 0.2927 0.6597 0.2807 0.033 Uiso 1 1 d R
H22B H 0.4087 0.7355 0.2137 0.033 Uiso 1 1 d R
C19 C 0.47804(19) 0.53764(18) 0.33510(13) 0.0270(4) Uani 1 1 d .
H19A H 0.5695 0.5512 0.3243 0.032 Uiso 1 1 d R
H19B H 0.4344 0.4490 0.3486 0.032 Uiso 1 1 d R
C8 C 0.62978(16) 0.76457(16) 0.11035(13) 0.0229(3) Uani 1 1 d .
H8 H 0.5583 0.7399 0.0602 0.028 Uiso 1 1 d R
C4 C 0.81902(19) 0.18938(19) -0.12731(15) 0.0313(4) Uani 1 1 d .
H4 H 0.8550 0.1421 -0.1758 0.038 Uiso 1 1 d R
C20 C 0.4664(2) 0.63354(19) 0.42828(15) 0.0343(4) Uani 1 1 d .
H20A H 0.5399 0.6586 0.4816 0.041 Uiso 1 1 d R
H20B H 0.3852 0.5982 0.4629 0.041 Uiso 1 1 d R
C14 C 0.57613(18) 0.20038(17) 0.26127(14) 0.0267(4) Uani 1 1 d .
H14 H 0.6611 0.2319 0.2393 0.032 Uiso 1 1 d R
C9 C 0.67951(18) 0.89198(17) 0.16212(14) 0.0280(4) Uani 1 1 d .
H9 H 0.6421 0.9514 0.1456 0.034 Uiso 1 1 d R
C11 C 0.84034(18) 0.84200(17) 0.25940(14) 0.0298(4) Uani 1 1 d .
H11 H 0.9118 0.8679 0.3098 0.036 Uiso 1 1 d R
C15 C 0.5466(2) 0.11326(19) 0.33551(15) 0.0323(4) Uani 1 1 d .
H15 H 0.6124 0.0878 0.3623 0.039 Uiso 1 1 d R
C10 C 0.78474(18) 0.93161(17) 0.23798(14) 0.0298(4) Uani 1 1 d .
H10 H 0.8174 1.0165 0.2741 0.036 Uiso 1 1 d R
C26 C 0.13165(18) 0.37309(19) 0.20511(16) 0.0324(4) Uani 1 1 d .
H26A H 0.1312 0.4606 0.2065 0.039 Uiso 1 1 d R
H26B H 0.1693 0.3671 0.2741 0.039 Uiso 1 1 d R
C23 C 0.12749(19) 0.2180(2) 0.05459(16) 0.0403(5) Uani 1 1 d .
H23A H 0.1795 0.1632 0.0396 0.048 Uiso 1 1 d R
H23B H 0.0933 0.2308 -0.0134 0.048 Uiso 1 1 d R
C25 C -0.00630(19) 0.2742(2) 0.18230(18) 0.0414(5) Uani 1 1 d .
H25A H -0.0598 0.3042 0.1373 0.050 Uiso 1 1 d R
H25B H -0.0483 0.2553 0.2489 0.050 Uiso 1 1 d R
C24 C 0.0170(2) 0.1568(2) 0.12377(17) 0.0431(5) Uani 1 1 d .
H24A H -0.0606 0.0988 0.0799 0.052 Uiso 1 1 d R
H24B H 0.0428 0.1091 0.1740 0.052 Uiso 1 1 d R
C28 C 0.0331(3) 0.1780(3) 0.4604(2) 0.0573(7) Uani 1 1 d .
H28 H 0.0450 0.1113 0.4134 0.069 Uiso 1 1 d R
C27 C -0.0859(3) 0.1604(4) 0.4984(2) 0.0696(8) Uani 1 1 d .
H27 H -0.1548 0.0817 0.4787 0.084 Uiso 1 1 d R
C29 C 0.1359(3) 0.2911(3) 0.4894(2) 0.0570(7) Uani 1 1 d .
H29 H 0.2176 0.3002 0.4635 0.068 Uiso 1 1 d R
C30 C 0.1207(3) 0.3928(3) 0.5560(2) 0.0686(8) Uani 1 1 d .
H30 H 0.1907 0.4708 0.5752 0.082 Uiso 1 1 d R
C31 C -0.0027(4) 0.3748(4) 0.5947(3) 0.0954(12) Uani 1 1 d .
H31 H -0.0166 0.4421 0.6394 0.114 Uiso 1 1 d R
C32 C -0.1033(4) 0.2578(5) 0.5651(3) 0.1015(14) Uani 1 1 d .
H32 H -0.1851 0.2451 0.5921 0.122 Uiso 1 1 d R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
0 -1 0 0.128
0 1 0 0.192
1 0 0 0.124
-1 0 0 0.093
0 0 1 0.124
0 0 -1 0.101
0 1 -1 0.181
1 -1 0 0.157
-1 1 0 0.178
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 P1 N1 97.57(6) . .
N2 P1 C1 104.16(7) . .
N1 P1 C1 103.80(7) . .
N2 P1 Mg1 44.96(5) . .
N1 P1 Mg1 52.77(5) . .
C1 P1 Mg1 114.66(5) . .
N2 Mg1 O1 98.30(5) . .
N2 Mg1 O2 103.12(5) . .
O1 Mg1 O2 87.39(5) . .
N2 Mg1 N1 123.46(5) . 2_665
O1 Mg1 N1 136.05(5) . 2_665
O2 Mg1 N1 95.01(5) . 2_665
N2 Mg1 N1 72.06(5) . .
O1 Mg1 N1 93.40(5) . .
O2 Mg1 N1 175.19(5) . .
N1 Mg1 N1 87.73(5) 2_665 .
N2 Mg1 P1 35.48(4) . .
O1 Mg1 P1 95.24(4) . .
O2 Mg1 P1 138.52(4) . .
N1 Mg1 P1 110.50(4) 2_665 .
N1 Mg1 P1 36.69(3) . .
N2 Mg1 Mg1 98.49(4) . 2_665
O1 Mg1 Mg1 121.59(4) . 2_665
O2 Mg1 Mg1 140.67(4) . 2_665
N1 Mg1 Mg1 45.81(4) 2_665 2_665
N1 Mg1 Mg1 41.92(3) . 2_665
P1 Mg1 Mg1 70.04(2) . 2_665
C22 O1 C19 108.71(12) . .
C22 O1 Mg1 133.01(10) . .
C19 O1 Mg1 117.65(9) . .
C13 N2 P1 118.36(11) . .
C13 N2 Mg1 135.86(11) . .
P1 N2 Mg1 99.56(6) . .
C7 N1 P1 115.04(10) . .
C7 N1 Mg1 109.37(9) . 2_665
P1 N1 Mg1 129.71(7) . 2_665
C7 N1 Mg1 113.89(9) . .
P1 N1 Mg1 90.55(6) . .
Mg1 N1 Mg1 92.27(5) 2_665 .
C26 O2 C23 108.89(13) . .
C26 O2 Mg1 126.59(11) . .
C23 O2 Mg1 124.08(11) . .
C2 C1 C6 118.07(14) . .
C2 C1 P1 121.64(12) . .
C6 C1 P1 119.27(12) . .
C8 C7 C12 116.52(15) . .
C8 C7 N1 118.26(14) . .
C12 C7 N1 125.22(14) . .
N2 C13 C18 119.86(14) . .
N2 C13 C14 124.35(15) . .
C18 C13 C14 115.79(14) . .
C5 C6 C1 120.87(16) . .
C5 C6 H6 119.5 . .
C1 C6 H6 119.7 . .
C17 C18 C13 121.98(16) . .
C17 C18 H18 119.0 . .
C13 C18 H18 119.0 . .
C4 C5 C6 120.21(16) . .
C4 C5 H5 119.8 . .
C6 C5 H5 120.0 . .
C3 C2 C1 121.08(16) . .
C3 C2 H2 119.4 . .
C1 C2 H2 119.5 . .
C15 C16 C17 118.36(16) . .
C15 C16 H16 120.8 . .
C17 C16 H16 120.8 . .
C11 C12 C7 120.96(16) . .
C11 C12 H12 119.4 . .
C7 C12 H12 119.6 . .
C16 C17 C18 121.02(17) . .
C16 C17 H17 119.4 . .
C18 C17 H17 119.6 . .
C4 C3 C2 119.89(16) . .
C4 C3 H3 120.0 . .
C2 C3 H3 120.1 . .
C22 C21 C20 102.65(15) . .
C22 C21 H21A 111.3 . .
C20 C21 H21A 111.3 . .
C22 C21 H21B 111.3 . .
C20 C21 H21B 111.0 . .
H21A C21 H21B 109.2 . .
O1 C22 C21 104.97(14) . .
O1 C22 H22A 110.9 . .
C21 C22 H22A 110.7 . .
O1 C22 H22B 110.7 . .
C21 C22 H22B 110.7 . .
H22A C22 H22B 108.8 . .
O1 C19 C20 105.66(14) . .
O1 C19 H19A 110.6 . .
C20 C19 H19A 110.5 . .
O1 C19 H19B 110.6 . .
C20 C19 H19B 110.7 . .
H19A C19 H19B 108.8 . .
C9 C8 C7 122.12(16) . .
C9 C8 H8 118.9 . .
C7 C8 H8 118.9 . .
C3 C4 C5 119.87(16) . .
C3 C4 H4 120.1 . .
C5 C4 H4 120.0 . .
C19 C20 C21 102.10(15) . .
C19 C20 H20A 111.4 . .
C21 C20 H20A 111.5 . .
C19 C20 H20B 111.3 . .
C21 C20 H20B 111.2 . .
H20A C20 H20B 109.2 . .
C15 C14 C13 121.29(17) . .
C15 C14 H14 119.4 . .
C13 C14 H14 119.3 . .
C10 C9 C8 120.46(17) . .
C10 C9 H9 119.7 . .
C8 C9 H9 119.8 . .
C10 C11 C12 121.42(17) . .
C10 C11 H11 119.2 . .
C12 C11 H11 119.4 . .
C16 C15 C14 121.55(17) . .
C16 C15 H15 119.2 . .
C14 C15 H15 119.2 . .
C9 C10 C11 118.50(16) . .
C9 C10 H10 120.8 . .
C11 C10 H10 120.7 . .
O2 C26 C25 105.82(16) . .
O2 C26 H26A 110.4 . .
C25 C26 H26A 110.4 . .
O2 C26 H26B 110.7 . .
C25 C26 H26B 110.8 . .
H26A C26 H26B 108.7 . .
O2 C23 C24 105.53(16) . .
O2 C23 H23A 110.6 . .
C24 C23 H23A 110.6 . .
O2 C23 H23B 110.7 . .
C24 C23 H23B 110.7 . .
H23A C23 H23B 108.8 . .
C24 C25 C26 102.47(16) . .
C24 C25 H25A 111.3 . .
C26 C25 H25A 111.5 . .
C24 C25 H25B 111.2 . .
C26 C25 H25B 111.1 . .
H25A C25 H25B 109.2 . .
C23 C24 C25 102.17(17) . .
C23 C24 H24A 111.4 . .
C25 C24 H24A 111.3 . .
C23 C24 H24B 111.3 . .
C25 C24 H24B 111.4 . .
H24A C24 H24B 109.2 . .
C27 C28 C29 121.3(3) . .
C27 C28 H28 119.3 . .
C29 C28 H28 119.3 . .
C32 C27 C28 119.1(3) . .
C32 C27 H27 120.7 . .
C28 C27 H27 120.2 . .
C28 C29 C30 120.8(3) . .
C28 C29 H29 119.8 . .
C30 C29 H29 119.4 . .
C29 C30 C31 117.8(3) . .
C29 C30 H30 121.0 . .
C31 C30 H30 121.2 . .
C32 C31 C30 119.4(3) . .
C32 C31 H31 120.6 . .
C30 C31 H31 120.0 . .
C27 C32 C31 121.5(3) . .
C27 C32 H32 119.0 . .
C31 C32 H32 119.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
P1 N2 1.6985(14) .
P1 N1 1.7242(13) .
P1 C1 1.8456(16) .
P1 Mg1 2.8859(7) .
Mg1 N2 2.0680(14) .
Mg1 O1 2.0852(12) .
Mg1 O2 2.1345(12) .
Mg1 N1 2.1409(14) 2_665
Mg1 N1 2.2978(14) .
Mg1 Mg1 3.2020(10) 2_665
O1 C22 1.4571(19) .
O1 C19 1.4633(19) .
N2 C13 1.384(2) .
N1 C7 1.4227(19) .
N1 Mg1 2.1408(14) 2_665
O2 C26 1.453(2) .
O2 C23 1.455(2) .
C1 C2 1.396(2) .
C1 C6 1.399(2) .
C7 C8 1.400(2) .
C7 C12 1.405(2) .
C13 C18 1.409(2) .
C13 C14 1.415(2) .
C6 C5 1.389(2) .
C6 H6 0.9300 .
C18 C17 1.386(2) .
C18 H18 0.9300 .
C5 C4 1.385(3) .
C5 H5 0.9300 .
C2 C3 1.393(2) .
C2 H2 0.9301 .
C16 C15 1.376(3) .
C16 C17 1.383(3) .
C16 H16 0.9301 .
C12 C11 1.387(2) .
C12 H12 0.9300 .
C17 H17 0.9299 .
C3 C4 1.385(3) .
C3 H3 0.9299 .
C21 C22 1.499(3) .
C21 C20 1.511(3) .
C21 H21A 0.9701 .
C21 H21B 0.9699 .
C22 H22A 0.9700 .
C22 H22B 0.9699 .
C19 C20 1.510(2) .
C19 H19A 0.9699 .
C19 H19B 0.9700 .
C8 C9 1.386(2) .
C8 H8 0.9300 .
C4 H4 0.9300 .
C20 H20A 0.9700 .
C20 H20B 0.9700 .
C14 C15 1.390(2) .
C14 H14 0.9300 .
C9 C10 1.382(3) .
C9 H9 0.9300 .
C11 C10 1.383(3) .
C11 H11 0.9299 .
C15 H15 0.9301 .
C10 H10 0.9300 .
C26 C25 1.515(3) .
C26 H26A 0.9700 .
C26 H26B 0.9700 .
C23 C24 1.511(3) .
C23 H23A 0.9701 .
C23 H23B 0.9700 .
C25 C24 1.511(3) .
C25 H25A 0.9701 .
C25 H25B 0.9701 .
C24 H24A 0.9700 .
C24 H24B 0.9700 .
C28 C27 1.348(4) .
C28 C29 1.358(4) .
C28 H28 0.9301 .
C27 C32 1.346(5) .
C27 H27 0.9300 .
C29 C30 1.372(4) .
C29 H29 0.9300 .
C30 C31 1.396(5) .
C30 H30 0.9300 .
C31 C32 1.374(6) .
C31 H31 0.9301 .
C32 H32 0.9299 .
