#------------------------------------------------------------------------------
#$Date: 2016-03-25 23:42:20 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180050 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/44/7034496.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7034496
loop_
_publ_author_name
'Dinca, Alina S.'
'Shova, Sergiu'
'Ion, Adrian E.'
'Maxim, Catalin'
'Lloret, Francesc'
'Julve, Miguel'
'Andruh, Marius'
_publ_section_title
;
 Ascorbic acid decomposition into oxalate ions: a simple synthetic route
 towards oxalato-bridged heterometallic 3d-4f clusters.
;
_journal_issue                   16
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7148
_journal_page_last               7151
_journal_paper_doi               10.1039/c5dt00778j
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C138 H138 Cu6 Dy6 N12 O60, 5(H2 O)'
_chemical_formula_sum            'C138 H148 Cu6 Dy6 N12 O65'
_chemical_formula_weight         4370.92
_chemical_name_systematic
;
 ? 
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2015-03-15
_audit_creation_method
;
Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
;
_audit_update_record
;
2015-03-19 deposited with the CCDC.
2015-03-20 downloaded from the CCDC.
;
_cell_angle_alpha                116.101(3)
_cell_angle_beta                 100.935(3)
_cell_angle_gamma                92.943(2)
_cell_formula_units_Z            1
_cell_length_a                   15.0763(4)
_cell_length_b                   18.9062(6)
_cell_length_c                   19.3431(6)
_cell_measurement_reflns_used    7943
_cell_measurement_temperature    173.00(14)
_cell_measurement_theta_max      24.7780
_cell_measurement_theta_min      1.6080
_cell_volume                     4804.2(3)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
;
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2008)'
_computing_structure_solution    'SIR2004 (Burla et al., 2007)'
_diffrn_ambient_temperature      173.00(14)
_diffrn_detector_area_resol_mean 16.1593
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_details
;
  1 omega  -76.00    1.00   1.0000   80.0000
omega____ theta____ kappa____ phi______ frames
    -      -14.0914  -57.0000  -60.0000 77

  2 omega  -77.00   -9.00   1.0000   80.0000
omega____ theta____ kappa____ phi______ frames
    -      -14.0914  -57.0000  150.0000 68

  3 omega  -80.00  -13.00   1.0000   80.0000
omega____ theta____ kappa____ phi______ frames
    -      -14.0914  -57.0000   90.0000 67

  4 omega  -10.00   22.00   1.0000   80.0000
omega____ theta____ kappa____ phi______ frames
    -      -14.0914  -99.0000    0.0000 32

  5 omega  -17.00   34.00   1.0000   80.0000
omega____ theta____ kappa____ phi______ frames
    -      -14.0914   38.0000   60.0000 51

  6 omega  -39.00   52.00   1.0000   80.0000
omega____ theta____ kappa____ phi______ frames
    -      -14.0914   77.0000 -120.0000 91
;
_diffrn_measurement_device_type  'Xcalibur, Eos'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_UB_11      -0.0432830000
_diffrn_orient_matrix_UB_12      -0.0194324000
_diffrn_orient_matrix_UB_13      -0.0033826000
_diffrn_orient_matrix_UB_21      0.0068978000
_diffrn_orient_matrix_UB_22      -0.0348994000
_diffrn_orient_matrix_UB_23      -0.0321251000
_diffrn_orient_matrix_UB_31      0.0207373000
_diffrn_orient_matrix_UB_32      -0.0138388000
_diffrn_orient_matrix_UB_33      0.0268862000
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0605
_diffrn_reflns_av_unetI/netI     0.1367
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            42447
_diffrn_reflns_theta_full        23.26
_diffrn_reflns_theta_max         23.26
_diffrn_reflns_theta_min         1.80
_diffrn_source                   'Enhance (Mo) X-ray Source'
_exptl_absorpt_coefficient_mu    3.029
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.56702
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            'clear dark green'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   dark
_exptl_crystal_colour_primary    green
_exptl_crystal_density_diffrn    1.511
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2150
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_refine_diff_density_max         1.975
_refine_diff_density_min         -1.030
_refine_diff_density_rms         0.175
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.000
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1035
_refine_ls_number_reflns         13698
_refine_ls_number_restraints     19
_refine_ls_restrained_S_all      0.999
_refine_ls_R_factor_all          0.0868
_refine_ls_R_factor_gt           0.0583
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0857P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1423
_refine_ls_wR_factor_ref         0.1551
_reflns_number_gt                9526
_reflns_number_total             13698
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5dt00778j2.cif
_cod_data_source_block           shi_2413_maan
_cod_depositor_comments
'Adding full bibliography for 7034494--7034500.cif.'
_cod_database_code               7034496
#BEGIN Tags that were not found in dictionaries:
_chemical_oxdiff_formula         'C138 H144 Dy6 N12 Cu6 O63'
_chemical_oxdiff_usercomment     Cu6Dy6Asc_894
_reflns_odcompleteness_completeness 99.92
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     26.32
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, {H3WA,H3WB} of O3W, {H4WA,H4WB} of O4W, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups, {H2WA,H2WB} of O2W, {H1WA,H1WB} of O1W
2. Restrained distances
 C69-C68 \\sim C69X-C68
 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
Uanis(C18) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C69X) \\sim Ueq, Uanis(C69) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C69) = Uanis(C69X)
4. Others
 Fixed Sof: C69X(0.5) H69A(0.5) H69B(0.5) H69C(0.5) C69(0.5) H69D(0.5)
 H69E(0.5) H69F(0.5) O3W(0.4) H3WA(0.4) H3WB(0.4) O4W(0.4) H4WA(0.4) H4WB(0.4)
 O2W(0.7) H2WA(0.7) H2WB(0.7)
5.a Riding coordinates:
 C69X(H69A,H69B,H69C), C69(H69D,H69E,H69F), O3W(H3WA,H3WB), O4W(H4WA,H4WB),
 O2W(H2WA,H2WB)
5.b Free rotating group:
 O1W(H1WA,H1WB)
5.c Secondary CH2 refined with riding coordinates:
 C9(H9A,H9B), C10(H10A,H10B), C11(H11A,H11B), C34(H34A,H34B), C35(H35A,H35B),
 C36(H36A,H36B), C53(H53A,H53B), C54(H54A,H54B), C55(H55A,H55B)
5.d Aromatic/amide H refined with riding coordinates:
 C3(H3), C4(H4), C5(H5), C8(H8), C12(H12), C14(H14), C15(H15), C16(H16),
 C28(H28), C29(H29), C30(H30), C33(H33), C37(H37), C39(H39), C40(H40), C41(H41),
  C47(H47), C48(H48), C49(H49), C52(H52), C56(H56), C58(H58), C59(H59), C60(H60)
5.e Idealised Me refined as rotating group:
 C1(H1A,H1B,H1C), C19(H19A,H19B,H19C), C26(H26A,H26B,H26C), C44(H44A,H44B,
 H44C), C45(H45A,H45B,H45C), C63(H63A,H63B,H63C), C65(H65A,H65B,H65C), C67(H67A,
 H67B,H67C)
;
_olex2_submission_special_instructions 'No special instructions were received'
#END Tags that were not found in dictionaries
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 'x, y, z'
2 '-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
C1 C 0.8748(7) 0.7845(8) 0.6908(7) 0.054(4) Uani 1 d . . . .
H1A H 0.8326 0.8220 0.6981 0.081 Uiso 1 calc . . GR .
H1B H 0.8495 0.7404 0.6967 0.081 Uiso 1 calc . . GR .
H1C H 0.8856 0.7656 0.6387 0.081 Uiso 1 calc . . GR .
C2 C 0.9571(7) 0.8436(6) 0.8265(6) 0.032(3) Uani 1 d . . . .
C3 C 0.8778(8) 0.8387(8) 0.8532(7) 0.046(3) Uani 1 d . . . .
H3 H 0.8203 0.8209 0.8185 0.056 Uiso 1 calc . . R .
C4 C 0.8888(9) 0.8618(8) 0.9344(8) 0.058(4) Uani 1 d . . . .
H4 H 0.8372 0.8602 0.9538 0.069 Uiso 1 calc . . R .
C5 C 0.9725(9) 0.8865(7) 0.9856(8) 0.051(3) Uani 1 d . . . .
H5 H 0.9775 0.8990 1.0385 0.061 Uiso 1 calc . . R .
C6 C 1.0503(8) 0.8931(7) 0.9591(7) 0.039(3) Uani 1 d . . . .
C7 C 1.0433(8) 0.8739(7) 0.8771(6) 0.041(3) Uani 1 d . . . .
C8 C 1.1378(9) 0.9133(7) 1.0134(6) 0.043(3) Uani 1 d . . . .
H8 H 1.1369 0.9125 1.0610 0.052 Uiso 1 calc . . R .
C9 C 1.2982(9) 0.9414(8) 1.0657(7) 0.054(4) Uani 1 d . . . .
H9A H 1.3354 0.9009 1.0421 0.065 Uiso 1 calc . . R .
H9B H 1.2795 0.9337 1.1076 0.065 Uiso 1 calc . . R .
C10 C 1.3546(8) 1.0233(9) 1.1009(7) 0.056(4) Uani 1 d . . . .
H10A H 1.3162 1.0631 1.1229 0.067 Uiso 1 calc . . R .
H10B H 1.4038 1.0289 1.1442 0.067 Uiso 1 calc . . R .
C11 C 1.3942(8) 1.0402(10) 1.0458(8) 0.065(4) Uani 1 d . . . .
H11A H 1.4272 0.9975 1.0187 0.077 Uiso 1 calc . . R .
H11B H 1.4375 1.0893 1.0749 0.077 Uiso 1 calc . . R .
C12 C 1.3228(7) 1.1160(8) 0.9886(7) 0.046(3) Uani 1 d . . . .
H12 H 1.3664 1.1572 1.0288 0.056 Uiso 1 calc . . R .
C13 C 1.2593(7) 1.1363(7) 0.9324(6) 0.033(3) Uani 1 d . . . .
C14 C 1.2586(7) 1.2162(7) 0.9508(7) 0.040(3) Uani 1 d . . . .
H14 H 1.2911 1.2562 0.9998 0.048 Uiso 1 calc . . R .
C15 C 1.2097(8) 1.2348(7) 0.8957(8) 0.049(3) Uani 1 d . . . .
H15 H 1.2073 1.2881 0.9085 0.059 Uiso 1 calc . . R .
C16 C 1.1632(7) 1.1761(7) 0.8209(7) 0.038(3) Uani 1 d . . . .
H16 H 1.1309 1.1892 0.7832 0.046 Uiso 1 calc . . R .
C17 C 1.1668(6) 1.0990(6) 0.8050(6) 0.025(2) Uani 1 d . . . .
C18 C 1.2101(6) 1.0749(7) 0.8599(6) 0.028(2) Uani 1 d . . . U
C19 C 1.1027(7) 1.0507(7) 0.6643(6) 0.036(3) Uani 1 d . . . .
H19A H 1.0887 1.0014 0.6162 0.053 Uiso 1 calc . . GR .
H19B H 1.1526 1.0840 0.6638 0.053 Uiso 1 calc . . GR .
H19C H 1.0500 1.0775 0.6683 0.053 Uiso 1 calc . . GR .
C20 C 0.9442(7) 1.0064(6) 0.7755(6) 0.026(2) Uani 1 d . . . .
C21 C 0.9182(7) 0.9607(6) 0.6830(6) 0.025(2) Uani 1 d . . . .
C22 C 1.1090(6) 0.8180(6) 0.5523(6) 0.025(2) Uani 1 d . . . .
C23 C 1.0549(6) 0.7518(6) 0.5621(6) 0.026(2) Uani 1 d . . . .
C24 C 0.9271(6) 1.2001(6) 0.6952(6) 0.026(2) Uani 1 d . . . .
C25 C 0.8404(7) 1.2385(6) 0.6939(6) 0.029(3) Uani 1 d . . . .
C26 C 0.9544(7) 1.2412(7) 0.8990(6) 0.042(3) Uani 1 d . . . .
H26A H 0.9890 1.2087 0.8634 0.064 Uiso 1 calc . . GR .
H26B H 0.9713 1.2392 0.9484 0.064 Uiso 1 calc . . GR .
H26C H 0.9669 1.2953 0.9081 0.064 Uiso 1 calc . . GR .
C27 C 0.7997(7) 1.2475(6) 0.9080(6) 0.032(3) Uani 1 d . . . .
C28 C 0.8238(8) 1.3157(8) 0.9790(9) 0.057(4) Uani 1 d . . . .
H28 H 0.8843 1.3407 0.9981 0.069 Uiso 1 calc . . R .
C29 C 0.7585(9) 1.3496(8) 1.0246(8) 0.057(4) Uani 1 d . . . .
H29 H 0.7753 1.3952 1.0731 0.068 Uiso 1 calc . . R .
C30 C 0.6705(8) 1.3114(8) 0.9934(7) 0.060(4) Uani 1 d . . . .
H30 H 0.6266 1.3327 1.0214 0.072 Uiso 1 calc . . R .
C31 C 0.6427(8) 1.2412(7) 0.9205(7) 0.046(3) Uani 1 d . . . .
C32 C 0.7090(7) 1.2100(7) 0.8765(7) 0.037(3) Uani 1 d . . . .
C33 C 0.5507(8) 1.1988(8) 0.8967(8) 0.048(3) Uani 1 d . . . .
H33 H 0.5147 1.2178 0.9332 0.058 Uiso 1 calc . . R .
C34 C 0.4222(8) 1.0990(8) 0.8229(7) 0.055(4) Uani 1 d . . . .
H34A H 0.3872 1.1394 0.8510 0.066 Uiso 1 calc . . R .
H34B H 0.4291 1.0640 0.8475 0.066 Uiso 1 calc . . R .
C35 C 0.3705(7) 1.0517(8) 0.7386(7) 0.050(3) Uani 1 d . . . .
H35A H 0.3086 1.0334 0.7371 0.060 Uiso 1 calc . . R .
H35B H 0.3991 1.0052 0.7132 0.060 Uiso 1 calc . . R .
C36 C 0.3672(7) 1.1005(8) 0.6916(8) 0.054(4) Uani 1 d . . . .
H36A H 0.3164 1.0767 0.6454 0.065 Uiso 1 calc . . R .
H36B H 0.3588 1.1547 0.7246 0.065 Uiso 1 calc . . R .
C37 C 0.4516(8) 1.1031(7) 0.5994(7) 0.040(3) Uani 1 d . . . .
H37 H 0.3948 1.1062 0.5730 0.048 Uiso 1 calc . . R .
C38 C 0.5243(6) 1.1014(6) 0.5628(6) 0.025(2) Uani 1 d . . . .
C39 C 0.5076(8) 1.1079(7) 0.4914(6) 0.037(3) Uani 1 d . . . .
H39 H 0.4489 1.1127 0.4698 0.045 Uiso 1 calc . . R .
C40 C 0.5748(7) 1.1074(6) 0.4537(6) 0.035(3) Uani 1 d . . . .
H40 H 0.5634 1.1156 0.4090 0.043 Uiso 1 calc . . R .
C41 C 0.6613(7) 1.0944(6) 0.4822(6) 0.031(3) Uani 1 d . . . .
H41 H 0.7071 1.0922 0.4555 0.037 Uiso 1 calc . . R .
C42 C 0.6787(7) 1.0850(6) 0.5488(6) 0.033(3) Uani 1 d . . . .
C43 C 0.6122(7) 1.0884(6) 0.5917(6) 0.032(3) Uani 1 d . . . .
C44 C 0.8223(7) 1.0389(7) 0.5275(6) 0.036(3) Uani 1 d . . . .
H44A H 0.8419 1.0817 0.5172 0.054 Uiso 1 calc . . GR .
H44B H 0.7925 0.9935 0.4785 0.054 Uiso 1 calc . . GR .
H44C H 0.8744 1.0250 0.5532 0.054 Uiso 1 calc . . GR .
C45 C 0.9255(8) 0.8632(6) 0.4639(7) 0.043(3) Uani 1 d . . . .
H45A H 0.9318 0.8889 0.5202 0.065 Uiso 1 calc . . GR .
H45B H 0.8729 0.8771 0.4389 0.065 Uiso 1 calc . . GR .
H45C H 0.9792 0.8804 0.4521 0.065 Uiso 1 calc . . GR .
C46 C 0.8307(8) 0.7425(7) 0.4315(7) 0.040(3) Uani 1 d . . . .
C47 C 0.7693(8) 0.7822(8) 0.4742(7) 0.047(3) Uani 1 d . . . .
H47 H 0.7836 0.8361 0.5100 0.056 Uiso 1 calc . . R .
C48 C 0.6824(9) 0.7369(9) 0.4613(9) 0.065(4) Uani 1 d . . . .
H48 H 0.6388 0.7627 0.4873 0.078 Uiso 1 calc . . R .
C49 C 0.6639(9) 0.6607(9) 0.4138(10) 0.067(4) Uani 1 d . . . .
H49 H 0.6071 0.6337 0.4071 0.081 Uiso 1 calc . . R .
C50 C 0.7261(8) 0.6173(7) 0.3721(7) 0.046(3) Uani 1 d . . . .
C51 C 0.8125(7) 0.6611(7) 0.3832(6) 0.033(3) Uani 1 d . . . .
C52 C 0.6993(9) 0.5346(9) 0.3180(9) 0.058(4) Uani 1 d . . . .
H52 H 0.6377 0.5145 0.3059 0.070 Uiso 1 calc . . R .
C53 C 0.7050(9) 0.4008(8) 0.2249(9) 0.071(4) Uani 1 d . . . .
H53A H 0.6398 0.3969 0.2217 0.085 Uiso 1 calc . . R .
H53B H 0.7139 0.3897 0.1729 0.085 Uiso 1 calc . . R .
C54 C 0.7411(12) 0.3409(9) 0.2464(11) 0.087(5) Uani 1 d . . . .
H54A H 0.7031 0.2898 0.2114 0.104 Uiso 1 calc . . R .
H54B H 0.7355 0.3546 0.2998 0.104 Uiso 1 calc . . R .
C55 C 0.8377(11) 0.3316(8) 0.2432(11) 0.088(5) Uani 1 d . . . .
H55A H 0.8450 0.3204 0.1908 0.105 Uiso 1 calc . . R .
H55B H 0.8526 0.2866 0.2523 0.105 Uiso 1 calc . . R .
C56 C 0.9681(9) 0.3976(7) 0.3526(9) 0.054(4) Uani 1 d . . . .
H56 H 0.9641 0.3485 0.3529 0.065 Uiso 1 calc . . R .
C57 C 1.0467(9) 0.4552(7) 0.4064(7) 0.047(3) Uani 1 d . . . .
C58 C 1.1049(10) 0.4400(9) 0.4595(8) 0.061(4) Uani 1 d . . . .
H58 H 1.0897 0.3935 0.4629 0.073 Uiso 1 calc . . R .
C59 C 1.1840(11) 0.4885(9) 0.5077(9) 0.070(4) Uani 1 d . . . .
H59 H 1.2199 0.4775 0.5455 0.084 Uiso 1 calc . . R .
C60 C 1.2091(8) 0.5551(8) 0.4987(7) 0.050(3) Uani 1 d . . . .
H60 H 1.2653 0.5872 0.5275 0.060 Uiso 1 calc . . R .
C61 C 1.1518(8) 0.5733(7) 0.4479(7) 0.047(3) Uani 1 d . . . .
C62 C 1.0665(7) 0.5273(6) 0.4010(7) 0.034(3) Uani 1 d . . . .
C63 C 1.2596(8) 0.6875(8) 0.4756(8) 0.058(4) Uani 1 d . . . .
H63A H 1.2639 0.7331 0.4661 0.087 Uiso 1 calc . . GR .
H63B H 1.3062 0.6563 0.4570 0.087 Uiso 1 calc . . GR .
H63C H 1.2677 0.7048 0.5314 0.087 Uiso 1 calc . . GR .
C64 C 1.3086(7) 0.8521(7) 0.7818(8) 0.040(3) Uani 1 d . . . .
C65 C 1.3892(8) 0.8281(9) 0.7449(8) 0.064(4) Uani 1 d . . . .
H65A H 1.3683 0.7840 0.6929 0.097 Uiso 1 calc . . GR .
H65B H 1.4322 0.8127 0.7772 0.097 Uiso 1 calc . . GR .
H65C H 1.4183 0.8723 0.7413 0.097 Uiso 1 calc . . GR .
C66 C 0.6326(8) 0.9450(7) 0.7108(6) 0.031(3) Uani 1 d . . . .
C67 C 0.6206(8) 0.8562(7) 0.6836(7) 0.049(3) Uani 1 d . . . .
H67A H 0.6302 0.8464 0.7289 0.074 Uiso 1 calc . . GR .
H67B H 0.6642 0.8332 0.6530 0.074 Uiso 1 calc . . GR .
H67C H 0.5598 0.8326 0.6516 0.074 Uiso 1 calc . . GR .
C68 C 0.9418(10) 0.5460(8) 0.1838(8) 0.060(4) Uani 1 d . . D .
Cu1 Cu 1.22789(8) 0.95561(8) 0.91670(7) 0.0326(3) Uani 1 d . . . .
Cu2 Cu 0.56754(8) 1.10049(8) 0.73811(7) 0.0314(3) Uani 1 d . . . .
Cu3 Cu 0.88496(10) 0.50922(8) 0.30689(9) 0.0430(4) Uani 1 d . . . .
Dy1 Dy 1.09777(3) 0.89763(3) 0.73276(3) 0.02543(15) Uani 1 d . . . .
Dy2 Dy 0.78789(3) 1.09188(3) 0.72429(3) 0.02564(15) Uani 1 d . . . .
Dy3 Dy 1.03024(3) 0.68204(3) 0.37430(3) 0.03043(16) Uani 1 d . . . .
N1 N 1.3224(6) 1.0482(6) 0.9864(5) 0.037(2) Uani 1 d . . . .
N2 N 1.2174(7) 0.9323(6) 1.0057(5) 0.040(2) Uani 1 d . . . .
N3 N 0.5135(6) 1.1380(6) 0.8306(6) 0.041(2) Uani 1 d . . . .
N4 N 0.4553(6) 1.1009(5) 0.6666(5) 0.036(2) Uani 1 d . . . .
N5 N 0.7511(7) 0.4851(6) 0.2842(6) 0.052(3) Uani 1 d A . . .
N6 N 0.9027(8) 0.4054(6) 0.3041(7) 0.057(3) Uani 1 d A . . .
O1 O 1.2067(4) 0.9980(4) 0.8387(4) 0.0301(17) Uani 1 d . . . .
O2 O 1.1156(4) 0.8811(4) 0.8493(4) 0.0306(17) Uani 1 d . . . .
O3 O 1.1278(4) 1.0348(4) 0.7314(4) 0.0309(17) Uani 1 d . . . .
O4 O 0.9580(5) 0.8219(4) 0.7480(4) 0.0343(17) Uani 1 d . . . .
O5 O 1.0105(5) 0.9909(4) 0.8106(4) 0.0323(17) Uani 1 d . . . .
O6 O 0.9664(4) 0.9084(4) 0.6530(4) 0.0305(17) Uani 1 d . . . .
O7 O 0.8964(4) 1.0584(4) 0.8069(4) 0.0262(16) Uani 1 d . . . .
O8 O 0.8555(4) 0.9806(4) 0.6479(4) 0.0281(16) Uani 1 d . . . .
O9 O 1.0513(4) 0.7663(4) 0.6299(4) 0.0295(17) Uani 1 d . . . .
O10 O 1.1416(4) 0.8802(4) 0.6128(4) 0.0263(16) Uani 1 d . . . .
O11 O 1.0180(5) 0.6889(4) 0.4985(4) 0.0345(18) Uani 1 d A . . .
O12 O 1.1149(5) 0.8000(4) 0.4824(4) 0.0325(17) Uani 1 d A . . .
O13 O 0.9252(4) 1.1459(4) 0.7147(4) 0.0297(17) Uani 1 d . . . .
O14 O 0.7779(4) 1.2146(4) 0.7155(4) 0.0321(17) Uani 1 d . . . .
O15 O 1.1601(5) 0.7106(4) 0.3305(4) 0.0329(17) Uani 1 d . . . .
O16 O 1.0070(4) 0.7746(4) 0.3235(4) 0.0294(16) Uani 1 d . . . .
O17 O 0.6354(4) 1.0786(4) 0.6568(4) 0.0257(16) Uani 1 d . . . .
O18 O 0.6907(4) 1.1444(4) 0.8090(4) 0.0282(16) Uani 1 d . . . .
O19 O 0.7590(5) 1.0640(5) 0.5784(4) 0.0355(18) Uani 1 d . . . .
O20 O 0.8592(4) 1.2123(4) 0.8651(4) 0.0340(18) Uani 1 d . . . .
O21 O 1.0170(5) 0.5483(4) 0.3537(4) 0.0345(18) Uani 1 d A . . .
O22 O 0.8763(5) 0.6250(4) 0.3484(4) 0.0369(18) Uani 1 d A . . .
O23 O 1.1706(5) 0.6395(4) 0.4339(4) 0.042(2) Uani 1 d A . . .
O24 O 0.9146(5) 0.7778(4) 0.4348(4) 0.0415(19) Uani 1 d A . . .
O25 O 1.2341(5) 0.8449(4) 0.7369(4) 0.0364(18) Uani 1 d . . . .
O26 O 1.3219(5) 0.8803(5) 0.8569(5) 0.051(2) Uani 1 d . . . .
O27 O 0.5644(5) 0.9796(4) 0.7226(4) 0.0346(18) Uani 1 d . . . .
O28 O 0.7104(5) 0.9777(4) 0.7181(4) 0.0377(19) Uani 1 d . . . .
O29 O 0.8947(6) 0.4931(5) 0.1896(5) 0.061(2) Uani 1 d A . . .
O30 O 0.9916(5) 0.6062(4) 0.2381(4) 0.0414(19) Uani 1 d A . . .
C69X C 0.964(2) 0.5245(18) 0.1010(12) 0.057(7) Uani 0.50 d A 1 D U
H69A H 0.9512 0.5682 0.0899 0.085 Uiso 0.50 d A 1 R .
H69B H 1.0265 0.5166 0.0991 0.085 Uiso 0.50 d A 1 R .
H69C H 0.9238 0.4769 0.0622 0.085 Uiso 0.50 d A 1 R .
C69 C 0.920(2) 0.5429(19) 0.0993(12) 0.057(7) Uani 0.50 d A 2 D U
H69D H 0.8889 0.5867 0.1026 0.085 Uiso 0.50 d A 2 R .
H69E H 0.9759 0.5474 0.0829 0.085 Uiso 0.50 d A 2 R .
H69F H 0.8822 0.4935 0.0613 0.085 Uiso 0.50 d A 2 R .
O3W O 1.1411(19) 1.3990(17) 1.1714(18) 0.103(9) Uiso 0.40 d . . . .
H3WA H 1.0843 1.3786 1.1553 0.123 Uiso 0.40 d . . R .
H3WB H 1.1657 1.4161 1.2210 0.123 Uiso 0.40 d . . R .
O4W O 0.553(2) 0.5927(18) 0.5966(19) 0.114(10) Uiso 0.40 d . . . .
H4WA H 0.5477 0.5900 0.5523 0.137 Uiso 0.40 d . . R .
H4WB H 0.5050 0.6146 0.6070 0.137 Uiso 0.40 d . . R .
O2W O 1.4584(12) 1.3044(12) 1.1225(12) 0.128(7) Uiso 0.70 d . . . .
H2WA H 1.5152 1.3133 1.1439 0.193 Uiso 0.70 d . . R .
H2WB H 1.4492 1.2726 1.0733 0.193 Uiso 0.70 d . . R .
O1W O 1.4387(7) 0.8232(8) 0.9456(7) 0.088(3) Uani 1 d . . . .
H1WA H 1.3825 0.8232 0.9281 0.132 Uiso 1 d . . G .
H1WB H 1.4692 0.8254 0.9137 0.132 Uiso 1 d . . G .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
H1A C1 H1B 109.5 . .
H1A C1 H1C 109.5 . .
H1B C1 H1C 109.5 . .
O4 C1 H1A 109.5 . .
O4 C1 H1B 109.5 . .
O4 C1 H1C 109.5 . .
C7 C2 C3 122.9(10) . .
C7 C2 O4 112.8(9) . .
O4 C2 C3 124.3(9) . .
C2 C3 H3 121.4 . .
C2 C3 C4 117.2(11) . .
C4 C3 H3 121.4 . .
C3 C4 H4 118.9 . .
C5 C4 C3 122.2(11) . .
C5 C4 H4 118.9 . .
C4 C5 H5 119.9 . .
C4 C5 C6 120.2(11) . .
C6 C5 H5 119.9 . .
C5 C6 C7 120.4(11) . .
C5 C6 C8 118.5(11) . .
C8 C6 C7 120.9(11) . .
C2 C7 C6 116.9(10) . .
O2 C7 C2 120.4(9) . .
O2 C7 C6 122.7(10) . .
C6 C8 H8 115.3 . .
N2 C8 C6 129.4(10) . .
N2 C8 H8 115.3 . .
H9A C9 H9B 108.0 . .
C10 C9 H9A 109.4 . .
C10 C9 H9B 109.4 . .
N2 C9 H9A 109.4 . .
N2 C9 H9B 109.4 . .
N2 C9 C10 111.2(9) . .
C9 C10 H10A 108.5 . .
C9 C10 H10B 108.5 . .
H10A C10 H10B 107.5 . .
C11 C10 C9 115.3(12) . .
C11 C10 H10A 108.5 . .
C11 C10 H10B 108.5 . .
C10 C11 H11A 109.4 . .
C10 C11 H11B 109.4 . .
C10 C11 N1 111.2(9) . .
H11A C11 H11B 108.0 . .
N1 C11 H11A 109.4 . .
N1 C11 H11B 109.4 . .
C13 C12 H12 117.0 . .
N1 C12 H12 117.0 . .
N1 C12 C13 126.1(11) . .
C14 C13 C12 118.6(10) . .
C14 C13 C18 121.9(10) . .
C18 C13 C12 119.2(10) . .
C13 C14 H14 120.5 . .
C15 C14 C13 118.9(11) . .
C15 C14 H14 120.5 . .
C14 C15 H15 119.1 . .
C14 C15 C16 121.7(11) . .
C16 C15 H15 119.1 . .
C15 C16 H16 121.3 . .
C17 C16 C15 117.4(10) . .
C17 C16 H16 121.3 . .
C16 C17 C18 124.4(10) . .
C16 C17 O3 123.4(9) . .
O3 C17 C18 112.3(9) . .
C13 C18 C17 115.5(10) . .
O1 C18 C13 125.2(9) . .
O1 C18 C17 119.2(9) . .
H19A C19 H19B 109.5 . .
H19A C19 H19C 109.5 . .
H19B C19 H19C 109.5 . .
O3 C19 H19A 109.5 . .
O3 C19 H19B 109.5 . .
O3 C19 H19C 109.5 . .
O5 C20 C21 118.0(10) . .
O5 C20 O7 125.8(10) . .
O7 C20 C21 116.1(9) . .
O6 C21 C20 115.0(9) . .
O8 C21 C20 117.7(10) . .
O8 C21 O6 127.3(9) . .
O10 C22 C23 116.7(9) . .
O10 C22 O12 128.0(9) . .
O12 C22 C23 115.2(9) . .
O9 C23 C22 116.7(10) . .
O9 C23 O11 127.2(9) . .
O11 C23 C22 116.1(8) . .
O13 C24 C25 115.8(8) . .
O13 C24 O16 125.9(9) . 2_776
O16 C24 C25 118.3(9) 2_776 .
O14 C25 C24 116.9(8) . .
O14 C25 O15 127.2(10) . 2_776
O15 C25 C24 115.8(9) 2_776 .
H26A C26 H26B 109.5 . .
H26A C26 H26C 109.5 . .
H26B C26 H26C 109.5 . .
O20 C26 H26A 109.5 . .
O20 C26 H26B 109.5 . .
O20 C26 H26C 109.5 . .
C28 C27 C32 120.4(11) . .
O20 C27 C28 123.8(10) . .
O20 C27 C32 115.8(10) . .
C27 C28 H28 119.0 . .
C27 C28 C29 122.0(11) . .
C29 C28 H28 119.0 . .
C28 C29 H29 121.7 . .
C30 C29 C28 116.7(12) . .
C30 C29 H29 121.7 . .
C29 C30 H30 118.4 . .
C29 C30 C31 123.2(12) . .
C31 C30 H30 118.4 . .
C30 C31 C33 119.6(11) . .
C32 C31 C30 118.5(10) . .
C32 C31 C33 121.7(11) . .
C27 C32 C31 119.1(11) . .
O18 C32 C27 117.4(10) . .
O18 C32 C31 123.4(9) . .
C31 C33 H33 116.5 . .
N3 C33 C31 126.9(11) . .
N3 C33 H33 116.5 . .
H34A C34 H34B 107.8 . .
C35 C34 H34A 109.1 . .
C35 C34 H34B 109.1 . .
N3 C34 H34A 109.1 . .
N3 C34 H34B 109.1 . .
N3 C34 C35 112.5(9) . .
C34 C35 H35A 109.1 . .
C34 C35 H35B 109.1 . .
C34 C35 C36 112.5(11) . .
H35A C35 H35B 107.8 . .
C36 C35 H35A 109.1 . .
C36 C35 H35B 109.1 . .
C35 C36 H36A 110.0 . .
C35 C36 H36B 110.0 . .
H36A C36 H36B 108.3 . .
N4 C36 C35 108.6(9) . .
N4 C36 H36A 110.0 . .
N4 C36 H36B 110.0 . .
C38 C37 H37 116.4 . .
N4 C37 H37 116.4 . .
N4 C37 C38 127.1(10) . .
C37 C38 C39 118.8(9) . .
C37 C38 C43 122.7(9) . .
C43 C38 C39 118.4(9) . .
C38 C39 H39 119.1 . .
C40 C39 C38 121.7(10) . .
C40 C39 H39 119.1 . .
C39 C40 H40 120.2 . .
C39 C40 C41 119.6(9) . .
C41 C40 H40 120.2 . .
C40 C41 H41 119.9 . .
C42 C41 C40 120.1(9) . .
C42 C41 H41 119.9 . .
C41 C42 C43 122.3(9) . .
C41 C42 O19 125.2(9) . .
O19 C42 C43 112.3(8) . .
C42 C43 C38 117.8(9) . .
O17 C43 C38 124.0(9) . .
O17 C43 C42 118.2(9) . .
H44A C44 H44B 109.5 . .
H44A C44 H44C 109.5 . .
H44B C44 H44C 109.5 . .
O19 C44 H44A 109.5 . .
O19 C44 H44B 109.5 . .
O19 C44 H44C 109.5 . .
H45A C45 H45B 109.5 . .
H45A C45 H45C 109.5 . .
H45B C45 H45C 109.5 . .
O24 C45 H45A 109.5 . .
O24 C45 H45B 109.5 . .
O24 C45 H45C 109.5 . .
C51 C46 C47 121.1(11) . .
O24 C46 C47 124.7(11) . .
O24 C46 C51 114.2(10) . .
C46 C47 H47 121.2 . .
C46 C47 C48 117.7(12) . .
C48 C47 H47 121.2 . .
C47 C48 H48 119.4 . .
C49 C48 C47 121.2(13) . .
C49 C48 H48 119.4 . .
C48 C49 H49 118.5 . .
C48 C49 C50 122.9(12) . .
C50 C49 H49 118.5 . .
C49 C50 C51 116.9(12) . .
C49 C50 C52 119.7(12) . .
C52 C50 C51 123.2(11) . .
C46 C51 C50 120.0(10) . .
O22 C51 C46 118.8(9) . .
O22 C51 C50 121.3(11) . .
C50 C52 H52 116.6 . .
N5 C52 C50 126.9(12) . .
N5 C52 H52 116.6 . .
H53A C53 H53B 107.9 . .
C54 C53 H53A 109.1 . .
C54 C53 H53B 109.1 . .
C54 C53 N5 112.3(12) . .
N5 C53 H53A 109.1 . .
N5 C53 H53B 109.1 . .
C53 C54 H54A 108.3 . .
C53 C54 H54B 108.3 . .
C53 C54 C55 115.9(13) . .
H54A C54 H54B 107.4 . .
C55 C54 H54A 108.3 . .
C55 C54 H54B 108.3 . .
C54 C55 H55A 109.3 . .
C54 C55 H55B 109.3 . .
C54 C55 N6 111.7(13) . .
H55A C55 H55B 107.9 . .
N6 C55 H55A 109.3 . .
N6 C55 H55B 109.3 . .
C57 C56 H56 115.8 . .
N6 C56 H56 115.8 . .
N6 C56 C57 128.3(11) . .
C58 C57 C56 120.6(12) . .
C58 C57 C62 119.7(12) . .
C62 C57 C56 119.6(11) . .
C57 C58 H58 118.0 . .
C57 C58 C59 123.9(13) . .
C59 C58 H58 118.0 . .
C58 C59 H59 121.2 . .
C58 C59 C60 117.6(12) . .
C60 C59 H59 121.2 . .
C59 C60 H60 120.0 . .
C61 C60 C59 119.9(12) . .
C61 C60 H60 120.0 . .
C60 C61 C62 123.8(10) . .
C60 C61 O23 124.7(11) . .
C62 C61 O23 111.5(9) . .
C61 C62 C57 114.6(10) . .
O21 C62 C57 125.4(10) . .
O21 C62 C61 119.8(9) . .
H63A C63 H63B 109.5 . .
H63A C63 H63C 109.5 . .
H63B C63 H63C 109.5 . .
O23 C63 H63A 109.5 . .
O23 C63 H63B 109.5 . .
O23 C63 H63C 109.5 . .
O25 C64 C65 117.5(11) . .
O25 C64 O26 124.3(11) . .
O26 C64 C65 118.1(10) . .
C64 C65 H65A 109.5 . .
C64 C65 H65B 109.5 . .
C64 C65 H65C 109.5 . .
H65A C65 H65B 109.5 . .
H65A C65 H65C 109.5 . .
H65B C65 H65C 109.5 . .
O27 C66 C67 118.1(10) . .
O28 C66 C67 116.7(10) . .
O28 C66 O27 125.1(10) . .
C66 C67 H67A 109.5 . .
C66 C67 H67B 109.5 . .
C66 C67 H67C 109.5 . .
H67A C67 H67B 109.5 . .
H67A C67 H67C 109.5 . .
H67B C67 H67C 109.5 . .
O29 C68 C69X 117.7(16) . .
O29 C68 C69 115.2(16) . .
O30 C68 O29 127.5(12) . .
O30 C68 C69X 112.4(15) . .
O30 C68 C69 116.3(15) . .
C69 C68 C69X 28.1(14) . .
N1 Cu1 N2 91.8(4) . .
N1 Cu1 O1 89.1(3) . .
N1 Cu1 O2 167.2(4) . .
N1 Cu1 O26 94.9(4) . .
N2 Cu1 O26 106.2(3) . .
O1 Cu1 N2 161.9(4) . .
O1 Cu1 O26 91.8(3) . .
O2 Cu1 N2 91.1(3) . .
O2 Cu1 O1 84.3(3) . .
O2 Cu1 O26 96.2(3) . .
N3 Cu2 N4 93.6(4) . .
N3 Cu2 O18 90.1(3) . .
N3 Cu2 O27 94.7(3) . .
N4 Cu2 O18 155.1(3) . .
N4 Cu2 O27 106.6(3) . .
O17 Cu2 N3 170.9(4) . .
O17 Cu2 N4 91.2(3) . .
O17 Cu2 O18 82.4(3) . .
O17 Cu2 O27 91.4(3) . .
O18 Cu2 O27 97.6(3) . .
N5 Cu3 N6 93.1(4) . .
N5 Cu3 O21 167.3(4) . .
N5 Cu3 O22 89.7(4) . .
N5 Cu3 O29 97.5(4) . .
N6 Cu3 O21 90.0(4) . .
N6 Cu3 O22 160.7(4) . .
N6 Cu3 O29 104.4(4) . .
O21 Cu3 O22 83.4(3) . .
O21 Cu3 O29 93.6(3) . .
O22 Cu3 O29 94.1(3) . .
O1 Dy1 O2 68.3(2) . .
O1 Dy1 O3 62.2(2) . .
O1 Dy1 O4 124.5(2) . .
O1 Dy1 O5 75.1(2) . .
O1 Dy1 O6 129.6(2) . .
O1 Dy1 O9 151.9(2) . .
O1 Dy1 O10 106.8(2) . .
O2 Dy1 O3 124.6(2) . .
O2 Dy1 O4 62.5(2) . .
O2 Dy1 O5 75.9(2) . .
O2 Dy1 O10 152.2(2) . .
O4 Dy1 O3 133.7(2) . .
O5 Dy1 O3 69.1(2) . .
O5 Dy1 O4 69.7(2) . .
O5 Dy1 O10 130.5(2) . .
O6 Dy1 O2 130.1(2) . .
O6 Dy1 O3 72.8(2) . .
O6 Dy1 O4 73.0(2) . .
O6 Dy1 O5 68.3(2) . .
O6 Dy1 O9 77.0(2) . .
O6 Dy1 O10 75.0(2) . .
O9 Dy1 O2 103.3(2) . .
O9 Dy1 O3 132.1(2) . .
O9 Dy1 O4 66.8(2) . .
O9 Dy1 O5 130.4(2) . .
O9 Dy1 O10 67.7(2) . .
O10 Dy1 O3 69.1(2) . .
O10 Dy1 O4 128.8(2) . .
O25 Dy1 O1 73.6(2) . .
O25 Dy1 O2 77.4(2) . .
O25 Dy1 O3 109.2(2) . .
O25 Dy1 O4 116.6(2) . .
O25 Dy1 O5 144.6(2) . .
O25 Dy1 O6 146.7(2) . .
O25 Dy1 O9 78.4(2) . .
O25 Dy1 O10 75.0(2) . .
O7 Dy2 O8 68.7(2) . .
O7 Dy2 O14 131.2(2) . .
O7 Dy2 O19 134.2(2) . .
O7 Dy2 O20 66.4(2) . .
O8 Dy2 O14 128.5(2) . .
O8 Dy2 O19 68.2(2) . .
O8 Dy2 O20 128.8(2) . .
O13 Dy2 O7 78.7(2) . .
O13 Dy2 O8 74.2(2) . .
O13 Dy2 O14 67.3(2) . .
O13 Dy2 O17 131.2(2) . .
O13 Dy2 O19 75.7(2) . .
O13 Dy2 O20 74.2(2) . .
O13 Dy2 O28 143.9(2) . .
O14 Dy2 O19 70.1(2) . .
O14 Dy2 O20 71.2(2) . .
O17 Dy2 O7 149.5(2) . .
O17 Dy2 O8 109.5(2) . .
O17 Dy2 O14 75.1(2) . .
O17 Dy2 O19 62.6(2) . .
O17 Dy2 O20 121.6(2) . .
O18 Dy2 O7 98.7(2) . .
O18 Dy2 O8 149.0(2) . .
O18 Dy2 O13 132.8(2) . .
O18 Dy2 O14 81.5(2) . .
O18 Dy2 O17 66.7(2) . .
O18 Dy2 O19 126.4(2) . .
O18 Dy2 O20 62.3(2) . .
O18 Dy2 O28 77.2(2) . .
O19 Dy2 O20 137.7(2) . .
O28 Dy2 O7 76.7(2) . .
O28 Dy2 O8 72.4(2) . .
O28 Dy2 O14 147.5(2) . .
O28 Dy2 O17 74.0(2) . .
O28 Dy2 O19 103.8(2) . .
O28 Dy2 O20 118.0(2) . .
O11 Dy3 O15 131.2(2) . .
O11 Dy3 O23 69.7(2) . .
O11 Dy3 O24 69.1(2) . .
O12 Dy3 O11 68.1(2) . .
O12 Dy3 O15 75.3(2) . .
O12 Dy3 O16 79.1(2) . .
O12 Dy3 O21 130.6(2) . .
O12 Dy3 O22 129.4(2) . .
O12 Dy3 O23 74.4(2) . .
O12 Dy3 O24 71.9(2) . .
O15 Dy3 O23 70.1(2) . .
O15 Dy3 O24 127.9(2) . .
O16 Dy3 O11 131.1(2) . .
O16 Dy3 O15 68.1(2) . .
O16 Dy3 O21 149.7(2) . .
O16 Dy3 O22 99.6(2) . .
O16 Dy3 O23 134.7(2) . .
O16 Dy3 O24 66.8(2) . .
O21 Dy3 O11 74.6(2) . .
O21 Dy3 O15 109.4(2) . .
O21 Dy3 O23 62.8(2) . .
O21 Dy3 O24 122.7(2) . .
O22 Dy3 O11 76.8(2) . .
O22 Dy3 O15 151.4(2) . .
O22 Dy3 O21 67.7(2) . .
O22 Dy3 O23 125.6(2) . .
O22 Dy3 O24 62.0(2) . .
O23 Dy3 O24 133.9(2) . .
O30 Dy3 O11 145.9(2) . .
O30 Dy3 O12 145.9(2) . .
O30 Dy3 O15 74.8(2) . .
O30 Dy3 O16 74.8(2) . .
O30 Dy3 O21 75.5(2) . .
O30 Dy3 O22 77.0(2) . .
O30 Dy3 O23 109.9(3) . .
O30 Dy3 O24 115.7(3) . .
C11 N1 Cu1 117.8(8) . .
C12 N1 C11 117.3(10) . .
C12 N1 Cu1 124.6(8) . .
C8 N2 C9 119.2(9) . .
C8 N2 Cu1 119.8(8) . .
C9 N2 Cu1 120.9(8) . .
C33 N3 C34 117.3(10) . .
C33 N3 Cu2 123.2(7) . .
C34 N3 Cu2 119.3(8) . .
C36 N4 Cu2 117.8(7) . .
C37 N4 C36 116.9(10) . .
C37 N4 Cu2 125.3(7) . .
C52 N5 C53 116.9(11) . .
C52 N5 Cu3 124.8(9) . .
C53 N5 Cu3 118.2(9) . .
C55 N6 Cu3 119.4(10) . .
C56 N6 C55 117.9(11) . .
C56 N6 Cu3 122.7(9) . .
C18 O1 Cu1 122.7(6) . .
C18 O1 Dy1 124.5(6) . .
Cu1 O1 Dy1 102.5(3) . .
C7 O2 Cu1 122.5(7) . .
C7 O2 Dy1 120.4(6) . .
Cu1 O2 Dy1 101.8(3) . .
C17 O3 C19 117.8(8) . .
C17 O3 Dy1 115.0(5) . .
C19 O3 Dy1 127.0(6) . .
C1 O4 Dy1 126.2(6) . .
C2 O4 C1 117.2(8) . .
C2 O4 Dy1 113.3(6) . .
C20 O5 Dy1 117.9(6) . .
C21 O6 Dy1 120.2(6) . .
C20 O7 Dy2 118.7(6) . .
C21 O8 Dy2 118.2(6) . .
C23 O9 Dy1 119.5(6) . .
C22 O10 Dy1 117.5(6) . .
C23 O11 Dy3 119.0(6) . .
C22 O12 Dy3 120.8(6) . .
C24 O13 Dy2 120.4(6) . .
C25 O14 Dy2 116.8(6) . .
C25 O15 Dy3 119.1(7) 2_776 .
C24 O16 Dy3 118.1(6) 2_776 .
C43 O17 Cu2 127.1(6) . .
C43 O17 Dy2 123.7(6) . .
Cu2 O17 Dy2 103.6(3) . .
C32 O18 Cu2 123.9(7) . .
C32 O18 Dy2 127.4(6) . .
Cu2 O18 Dy2 103.5(3) . .
C42 O19 C44 116.5(7) . .
C42 O19 Dy2 116.0(6) . .
C44 O19 Dy2 126.9(6) . .
C26 O20 Dy2 125.6(6) . .
C27 O20 C26 118.4(9) . .
C27 O20 Dy2 116.0(6) . .
C62 O21 Cu3 124.1(6) . .
C62 O21 Dy3 122.3(6) . .
Cu3 O21 Dy3 102.8(3) . .
C51 O22 Cu3 125.9(6) . .
C51 O22 Dy3 126.4(7) . .
Cu3 O22 Dy3 102.2(3) . .
C61 O23 C63 115.6(9) . .
C61 O23 Dy3 115.0(6) . .
C63 O23 Dy3 126.6(6) . .
C45 O24 Dy3 127.1(6) . .
C46 O24 C45 115.8(9) . .
C46 O24 Dy3 116.8(6) . .
C64 O25 Dy1 142.6(8) . .
C64 O26 Cu1 118.8(7) . .
C66 O27 Cu2 120.5(6) . .
C66 O28 Dy2 142.7(7) . .
C68 O29 Cu3 119.4(9) . .
C68 O30 Dy3 142.9(7) . .
C68 C69X H69A 106.0 . .
C68 C69X H69B 114.8 . .
C68 C69X H69C 107.5 . .
C68 C69X H69E 133.3 . .
C68 C69X H69F 94.3 . .
H69A C69X H69B 109.4 . .
H69A C69X H69C 109.5 . .
H69A C69X H69E 34.0 . .
H69A C69X H69F 84.4 . .
H69B C69X H69C 109.5 . .
H69B C69X H69E 78.0 . .
H69B C69X H69F 141.2 . .
H69C C69X H69E 109.4 . .
H69C C69X H69F 33.6 . .
H69E C69X H69F 100.8 . .
C68 C69 H69A 120.5 . .
C68 C69 H69B 82.7 . .
C68 C69 H69C 98.5 . .
C68 C69 H69D 107.9 . .
C68 C69 H69E 110.8 . .
C68 C69 H69F 109.6 . .
H69A C69 H69B 67.2 . .
H69A C69 H69C 110.4 . .
H69A C69 H69D 75.0 . .
H69A C69 H69E 34.6 . .
H69A C69 H69F 125.6 . .
H69B C69 H69C 63.6 . .
H69B C69 H69D 140.4 . .
H69B C69 H69E 34.9 . .
H69B C69 H69F 101.8 . .
H69C C69 H69D 145.5 . .
H69C C69 H69E 80.2 . .
H69C C69 H69F 38.6 . .
H69D C69 H69E 109.5 . .
H69D C69 H69F 109.5 . .
H69E C69 H69F 109.5 . .
H3WA O3W H3WB 117.1 . .
H4WA O4W H4WB 97.5 . .
H2WA O2W H2WB 109.5 . .
H1WA O1W H1WB 109.4 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 H1A 0.9600 .
C1 H1B 0.9600 .
C1 H1C 0.9600 .
C1 O4 1.411(12) .
C2 C3 1.404(14) .
C2 C7 1.387(15) .
C2 O4 1.390(12) .
C3 H3 0.9300 .
C3 C4 1.406(16) .
C4 H4 0.9300 .
C4 C5 1.359(17) .
C5 H5 0.9300 .
C5 C6 1.387(15) .
C6 C7 1.445(15) .
C6 C8 1.434(16) .
C7 O2 1.329(12) .
C8 H8 0.9300 .
C8 N2 1.289(14) .
C9 H9A 0.9700 .
C9 H9B 0.9700 .
C9 C10 1.518(17) .
C9 N2 1.459(14) .
C10 H10A 0.9700 .
C10 H10B 0.9700 .
C10 C11 1.455(15) .
C11 H11A 0.9700 .
C11 H11B 0.9700 .
C11 N1 1.487(13) .
C12 H12 0.9300 .
C12 C13 1.501(15) .
C12 N1 1.264(15) .
C13 C14 1.392(15) .
C13 C18 1.396(14) .
C14 H14 0.9300 .
C14 C15 1.364(16) .
C15 H15 0.9300 .
C15 C16 1.393(16) .
C16 H16 0.9300 .
C16 C17 1.357(14) .
C17 C18 1.398(13) .
C17 O3 1.391(11) .
C18 O1 1.321(12) .
C19 H19A 0.9600 .
C19 H19B 0.9600 .
C19 H19C 0.9600 .
C19 O3 1.446(11) .
C20 C21 1.562(14) .
C20 O5 1.222(11) .
C20 O7 1.252(12) .
C21 O6 1.252(12) .
C21 O8 1.232(11) .
C22 C23 1.559(13) .
C22 O10 1.226(11) .
C22 O12 1.264(11) .
C23 O9 1.228(11) .
C23 O11 1.274(12) .
C24 C25 1.529(14) .
C24 O13 1.240(11) .
C24 O16 1.259(11) 2_776
C25 O14 1.241(11) .
C25 O15 1.244(11) 2_776
C26 H26A 0.9600 .
C26 H26B 0.9600 .
C26 H26C 0.9600 .
C26 O20 1.427(11) .
C27 C28 1.373(16) .
C27 C32 1.397(14) .
C27 O20 1.339(12) .
C28 H28 0.9300 .
C28 C29 1.433(17) .
C29 H29 0.9300 .
C29 C30 1.364(16) .
C30 H30 0.9300 .
C30 C31 1.413(16) .
C31 C32 1.419(15) .
C31 C33 1.448(16) .
C32 O18 1.313(13) .
C33 H33 0.9300 .
C33 N3 1.280(14) .
C34 H34A 0.9700 .
C34 H34B 0.9700 .
C34 C35 1.493(16) .
C34 N3 1.478(13) .
C35 H35A 0.9700 .
C35 H35B 0.9700 .
C35 C36 1.550(16) .
C36 H36A 0.9700 .
C36 H36B 0.9700 .
C36 N4 1.498(13) .
C37 H37 0.9300 .
C37 C38 1.406(14) .
C37 N4 1.310(13) .
C38 C39 1.418(13) .
C38 C43 1.414(14) .
C39 H39 0.9300 .
C39 C40 1.355(14) .
C40 H40 0.9300 .
C40 C41 1.394(14) .
C41 H41 0.9300 .
C41 C42 1.355(13) .
C42 C43 1.405(14) .
C42 O19 1.392(12) .
C43 O17 1.338(12) .
C44 H44A 0.9600 .
C44 H44B 0.9600 .
C44 H44C 0.9600 .
C44 O19 1.447(11) .
C45 H45A 0.9600 .
C45 H45B 0.9600 .
C45 H45C 0.9600 .
C45 O24 1.445(12) .
C46 C47 1.384(15) .
C46 C51 1.383(15) .
C46 O24 1.377(13) .
C47 H47 0.9300 .
C47 C48 1.444(17) .
C48 H48 0.9300 .
C48 C49 1.302(18) .
C49 H49 0.9300 .
C49 C50 1.410(17) .
C50 C51 1.434(15) .
C50 C52 1.428(18) .
C51 O22 1.323(12) .
C52 H52 0.9300 .
C52 N5 1.281(16) .
C53 H53A 0.9700 .
C53 H53B 0.9700 .
C53 C54 1.464(19) .
C53 N5 1.522(15) .
C54 H54A 0.9700 .
C54 H54B 0.9700 .
C54 C55 1.49(2) .
C55 H55A 0.9700 .
C55 H55B 0.9700 .
C55 N6 1.508(17) .
C56 H56 0.9300 .
C56 C57 1.441(18) .
C56 N6 1.287(16) .
C57 C58 1.361(17) .
C57 C62 1.433(14) .
C58 H58 0.9300 .
C58 C59 1.358(18) .
C59 H59 0.9300 .
C59 C60 1.390(16) .
C60 H60 0.9300 .
C60 C61 1.355(15) .
C61 C62 1.408(15) .
C61 O23 1.418(12) .
C62 O21 1.280(12) .
C63 H63A 0.9600 .
C63 H63B 0.9600 .
C63 H63C 0.9600 .
C63 O23 1.447(12) .
C64 C65 1.515(15) .
C64 O25 1.242(12) .
C64 O26 1.278(14) .
C65 H65A 0.9600 .
C65 H65B 0.9600 .
C65 H65C 0.9600 .
C66 C67 1.510(15) .
C66 O27 1.252(12) .
C66 O28 1.249(12) .
C67 H67A 0.9600 .
C67 H67B 0.9600 .
C67 H67C 0.9600 .
C68 O29 1.254(14) .
C68 O30 1.235(14) .
C68 C69X 1.579(19) .
C68 C69 1.579(19) .
Cu1 N1 1.962(9) .
Cu1 N2 1.987(8) .
Cu1 O1 1.981(6) .
Cu1 O2 1.963(7) .
Cu1 O26 2.180(8) .
Cu2 N3 1.965(9) .
Cu2 N4 1.974(9) .
Cu2 O17 1.942(6) .
Cu2 O18 1.973(7) .
Cu2 O27 2.167(7) .
Cu3 N5 1.967(11) .
Cu3 N6 1.973(10) .
Cu3 O21 1.977(7) .
Cu3 O22 1.994(7) .
Cu3 O29 2.188(8) .
Dy1 O1 2.341(7) .
Dy1 O2 2.377(6) .
Dy1 O3 2.621(7) .
Dy1 O4 2.622(6) .
Dy1 O5 2.400(7) .
Dy1 O6 2.346(6) .
Dy1 O9 2.358(7) .
Dy1 O10 2.421(6) .
Dy1 O25 2.334(7) .
Dy2 O7 2.375(6) .
Dy2 O8 2.388(7) .
Dy2 O13 2.337(6) .
Dy2 O14 2.410(7) .
Dy2 O17 2.359(6) .
Dy2 O18 2.333(7) .
Dy2 O19 2.576(6) .
Dy2 O20 2.634(7) .
Dy2 O28 2.346(6) .
Dy3 O11 2.391(6) .
Dy3 O12 2.359(7) .
Dy3 O15 2.401(7) .
Dy3 O16 2.367(6) .
Dy3 O21 2.371(6) .
Dy3 O22 2.372(7) .
Dy3 O23 2.553(7) .
Dy3 O24 2.631(7) .
Dy3 O30 2.311(7) .
O15 C25 1.244(11) 2_776
O16 C24 1.259(11) 2_776
C69X H69A 0.9607 .
C69X H69B 0.9602 .
C69X H69C 0.9608 .
C69X H69E 0.6982 .
C69X H69F 1.2801 .
C69 H69A 0.7487 .
C69 H69C 1.1425 .
C69 H69D 0.9599 .
C69 H69E 0.9603 .
C69 H69F 0.9614 .
O3W H3WA 0.8587 .
O3W H3WB 0.8606 .
O4W H4WA 0.8239 .
O4W H4WB 0.8628 .
O2W H2WA 0.8499 .
O2W H2WB 0.8509 .
O1W H1WA 0.8509 .
O1W H1WB 0.8507 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C2 C3 C4 C5 -1.3(19) . .
C2 C7 O2 Cu1 157.4(8) . .
C2 C7 O2 Dy1 26.6(13) . .
C3 C2 C7 C6 6.3(17) . .
C3 C2 C7 O2 -176.4(10) . .
C3 C2 O4 C1 -7.3(15) . .
C3 C2 O4 Dy1 153.4(9) . .
C3 C4 C5 C6 3(2) . .
C4 C5 C6 C7 0.0(18) . .
C4 C5 C6 C8 -175.2(12) . .
C5 C6 C7 C2 -4.5(17) . .
C5 C6 C7 O2 178.2(10) . .
C5 C6 C8 N2 -170.3(12) . .
C6 C7 O2 Cu1 -25.4(14) . .
C6 C7 O2 Dy1 -156.3(8) . .
C6 C8 N2 C9 -172.9(12) . .
C6 C8 N2 Cu1 11.1(17) . .
C7 C2 C3 C4 -3.5(17) . .
C7 C2 O4 C1 175.0(10) . .
C7 C2 O4 Dy1 -24.3(11) . .
C7 C6 C8 N2 14.5(19) . .
C8 C6 C7 C2 170.6(10) . .
C8 C6 C7 O2 -6.7(17) . .
C9 C10 C11 N1 69.2(15) . .
C10 C9 N2 C8 -123.7(12) . .
C10 C9 N2 Cu1 52.2(13) . .
C10 C11 N1 C12 113.8(13) . .
C10 C11 N1 Cu1 -60.9(14) . .
C12 C13 C14 C15 172.1(9) . .
C12 C13 C18 C17 -168.0(8) . .
C12 C13 C18 O1 7.6(14) . .
C13 C12 N1 C11 177.3(10) . .
C13 C12 N1 Cu1 -8.4(16) . .
C13 C14 C15 C16 -2.3(17) . .
C13 C18 O1 Cu1 25.2(12) . .
C13 C18 O1 Dy1 164.0(7) . .
C14 C13 C18 C17 5.1(14) . .
C14 C13 C18 O1 -179.3(9) . .
C14 C15 C16 C17 1.3(16) . .
C15 C16 C17 C18 3.3(15) . .
C15 C16 C17 O3 -176.4(9) . .
C16 C17 C18 C13 -6.4(14) . .
C16 C17 C18 O1 177.8(9) . .
C16 C17 O3 C19 15.9(13) . .
C16 C17 O3 Dy1 -160.1(8) . .
C17 C18 O1 Cu1 -159.4(6) . .
C17 C18 O1 Dy1 -20.6(11) . .
C18 C13 C14 C15 -1.1(16) . .
C18 C17 O3 C19 -163.8(8) . .
C18 C17 O3 Dy1 20.2(9) . .
C20 C21 O6 Dy1 -8.8(10) . .
C20 C21 O8 Dy2 3.9(10) . .
C21 C20 O5 Dy1 3.4(11) . .
C21 C20 O7 Dy2 -7.7(10) . .
C22 C23 O9 Dy1 12.4(11) . .
C22 C23 O11 Dy3 -2.6(11) . .
C23 C22 O10 Dy1 -9.0(11) . .
C23 C22 O12 Dy3 8.8(11) . .
C24 C25 O14 Dy2 -14.8(11) . .
C25 C24 O13 Dy2 11.2(12) . .
C27 C28 C29 C30 -1(2) . .
C27 C32 O18 Cu2 -160.2(7) . .
C27 C32 O18 Dy2 -10.1(13) . .
C28 C27 C32 C31 -2.8(16) . .
C28 C27 C32 O18 -179.0(10) . .
C28 C27 O20 C26 7.8(15) . .
C28 C27 O20 Dy2 -173.3(9) . .
C28 C29 C30 C31 1(2) . .
C29 C30 C31 C32 -2(2) . .
C29 C30 C31 C33 172.0(13) . .
C30 C31 C32 C27 2.8(17) . .
C30 C31 C32 O18 178.7(11) . .
C30 C31 C33 N3 174.8(13) . .
C31 C32 O18 Cu2 23.8(14) . .
C31 C32 O18 Dy2 174.0(8) . .
C31 C33 N3 C34 173.1(12) . .
C31 C33 N3 Cu2 -11.9(18) . .
C32 C27 C28 C29 2.0(18) . .
C32 C27 O20 C26 -171.5(9) . .
C32 C27 O20 Dy2 7.4(11) . .
C32 C31 C33 N3 -11(2) . .
C33 C31 C32 C27 -171.1(11) . .
C33 C31 C32 O18 4.8(18) . .
C34 C35 C36 N4 80.9(13) . .
C35 C34 N3 C33 157.7(12) . .
C35 C34 N3 Cu2 -17.6(14) . .
C35 C36 N4 C37 147.9(10) . .
C35 C36 N4 Cu2 -33.4(12) . .
C37 C38 C39 C40 179.4(10) . .
C37 C38 C43 C42 177.7(10) . .
C37 C38 C43 O17 -1.7(16) . .
C38 C37 N4 C36 -177.8(10) . .
C38 C37 N4 Cu2 3.6(16) . .
C38 C39 C40 C41 4.7(16) . .
C38 C43 O17 Cu2 -13.5(14) . .
C38 C43 O17 Dy2 -162.7(7) . .
C39 C38 C43 C42 1.7(14) . .
C39 C38 C43 O17 -177.7(9) . .
C39 C40 C41 C42 -2.2(16) . .
C40 C41 C42 C43 -0.5(16) . .
C40 C41 C42 O19 173.4(10) . .
C41 C42 C43 C38 0.7(15) . .
C41 C42 C43 O17 -179.9(10) . .
C41 C42 O19 C44 -9.8(15) . .
C41 C42 O19 Dy2 162.5(9) . .
C42 C43 O17 Cu2 167.0(7) . .
C42 C43 O17 Dy2 17.9(12) . .
C43 C38 C39 C40 -4.5(15) . .
C43 C42 O19 C44 164.6(9) . .
C43 C42 O19 Dy2 -23.2(10) . .
C46 C47 C48 C49 3(2) . .
C46 C51 O22 Cu3 158.6(7) . .
C46 C51 O22 Dy3 9.6(13) . .
C47 C46 C51 C50 4.6(16) . .
C47 C46 C51 O22 -174.8(10) . .
C47 C46 O24 C45 -20.3(15) . .
C47 C46 O24 Dy3 165.7(9) . .
C47 C48 C49 C50 0(2) . .
C48 C49 C50 C51 -1(2) . .
C48 C49 C50 C52 -176.8(14) . .
C49 C50 C51 C46 -1.5(17) . .
C49 C50 C51 O22 177.9(11) . .
C49 C50 C52 N5 -169.8(13) . .
C50 C51 O22 Cu3 -20.8(14) . .
C50 C51 O22 Dy3 -169.8(7) . .
C50 C52 N5 C53 -176.5(12) . .
C50 C52 N5 Cu3 6.2(19) . .
C51 C46 C47 C48 -5.3(17) . .
C51 C46 O24 C45 162.1(9) . .
C51 C46 O24 Dy3 -11.9(11) . .
C51 C50 C52 N5 14(2) . .
C52 C50 C51 C46 174.4(11) . .
C52 C50 C51 O22 -6.2(17) . .
C53 C54 C55 N6 65.7(19) . .
C54 C53 N5 C52 -121.6(14) . .
C54 C53 N5 Cu3 55.9(15) . .
C54 C55 N6 C56 125.6(14) . .
C54 C55 N6 Cu3 -54.4(15) . .
C56 C57 C58 C59 174.7(13) . .
C56 C57 C62 C61 -170.8(11) . .
C56 C57 C62 O21 3.7(18) . .
C57 C56 N6 C55 168.6(12) . .
C57 C56 N6 Cu3 -11.3(19) . .
C57 C58 C59 C60 -4(2) . .
C57 C62 O21 Cu3 23.2(15) . .
C57 C62 O21 Dy3 161.4(9) . .
C58 C57 C62 C61 5.7(17) . .
C58 C57 C62 O21 -179.8(11) . .
C58 C59 C60 C61 6(2) . .
C59 C60 C61 C62 -1(2) . .
C59 C60 C61 O23 -179.8(12) . .
C60 C61 C62 C57 -4.3(18) . .
C60 C61 C62 O21 -179.1(11) . .
C60 C61 O23 C63 2.7(17) . .
C60 C61 O23 Dy3 -159.7(10) . .
C61 C62 O21 Cu3 -162.6(8) . .
C61 C62 O21 Dy3 -24.4(14) . .
C62 C57 C58 C59 -2(2) . .
C62 C61 O23 C63 -176.0(10) . .
C62 C61 O23 Dy3 21.6(12) . .
C65 C64 O25 Dy1 -151.5(9) . .
C65 C64 O26 Cu1 156.9(8) . .
C67 C66 O27 Cu2 -167.5(7) . .
C67 C66 O28 Dy2 159.8(8) . .
N1 C12 C13 C14 169.4(11) . .
N1 C12 C13 C18 -17.2(16) . .
N1 Cu1 N2 C8 136.8(9) . .
N1 Cu1 N2 C9 -39.1(9) . .
N1 Cu1 O1 C18 -37.3(7) . .
N1 Cu1 O1 Dy1 176.4(3) . .
N1 Cu1 O2 C7 -64.6(16) . .
N1 Cu1 O2 Dy1 73.6(14) . .
N1 Cu1 O26 C64 -121.3(8) . .
N2 C9 C10 C11 -64.3(15) . .
N2 Cu1 N1 C11 41.5(9) . .
N2 Cu1 N1 C12 -132.7(10) . .
N2 Cu1 O1 C18 55.6(14) . .
N2 Cu1 O1 Dy1 -90.6(11) . .
N2 Cu1 O2 C7 38.5(8) . .
N2 Cu1 O2 Dy1 176.7(4) . .
N2 Cu1 O26 C64 145.4(8) . .
N3 C34 C35 C36 -51.3(14) . .
N3 Cu2 N4 C36 -19.1(8) . .
N3 Cu2 N4 C37 159.4(9) . .
N3 Cu2 O17 C43 -104(2) . .
N3 Cu2 O17 Dy2 50(2) . .
N3 Cu2 O18 C32 -34.8(7) . .
N3 Cu2 O18 Dy2 169.2(3) . .
N3 Cu2 O27 C66 -134.2(8) . .
N4 C37 C38 C39 -177.2(11) . .
N4 C37 C38 C43 6.8(17) . .
N4 Cu2 N3 C33 -126.9(10) . .
N4 Cu2 N3 C34 48.0(9) . .
N4 Cu2 O17 C43 17.7(8) . .
N4 Cu2 O17 Dy2 171.6(3) . .
N4 Cu2 O18 C32 63.9(11) . .
N4 Cu2 O18 Dy2 -92.2(8) . .
N4 Cu2 O27 C66 130.7(7) . .
N5 C53 C54 C55 -66.8(19) . .
N5 Cu3 N6 C55 39.1(10) . .
N5 Cu3 N6 C56 -141.0(11) . .
N5 Cu3 O21 C62 71.2(18) . .
N5 Cu3 O21 Dy3 -73.5(16) . .
N5 Cu3 O22 C51 30.3(8) . .
N5 Cu3 O22 Dy3 -174.8(4) . .
N5 Cu3 O29 C68 130.2(10) . .
N6 C56 C57 C58 173.3(13) . .
N6 C56 C57 C62 -10(2) . .
N6 Cu3 N5 C52 138.4(11) . .
N6 Cu3 N5 C53 -38.9(9) . .
N6 Cu3 O21 C62 -33.1(9) . .
N6 Cu3 O21 Dy3 -177.8(4) . .
N6 Cu3 O22 C51 -68.2(14) . .
N6 Cu3 O22 Dy3 86.7(11) . .
N6 Cu3 O29 C68 -134.6(10) . .
O1 Cu1 N1 C11 -156.6(8) . .
O1 Cu1 N1 C12 29.2(10) . .
O1 Cu1 N2 C8 44.3(16) . .
O1 Cu1 N2 C9 -131.6(11) . .
O1 Cu1 O2 C7 -123.9(8) . .
O1 Cu1 O2 Dy1 14.3(3) . .
O1 Cu1 O26 C64 -32.1(8) . .
O1 Dy1 O2 C7 126.4(8) . .
O1 Dy1 O2 Cu1 -12.9(3) . .
O1 Dy1 O3 C17 -21.4(6) . .
O1 Dy1 O3 C19 163.1(7) . .
O1 Dy1 O4 C1 154.9(8) . .
O1 Dy1 O4 C2 -3.8(7) . .
O1 Dy1 O5 C20 139.1(7) . .
O1 Dy1 O6 C21 -38.8(8) . .
O1 Dy1 O9 C23 -96.0(8) . .
O1 Dy1 O10 C22 161.6(7) . .
O1 Dy1 O25 C64 23.2(11) . .
O2 Cu1 N1 C11 144.6(13) . .
O2 Cu1 N1 C12 -30(2) . .
O2 Cu1 N2 C8 -30.7(9) . .
O2 Cu1 N2 C9 153.4(9) . .
O2 Cu1 O1 C18 131.7(7) . .
O2 Cu1 O1 Dy1 -14.6(3) . .
O2 Cu1 O26 C64 52.4(8) . .
O2 Dy1 O1 C18 -132.5(7) . .
O2 Dy1 O1 Cu1 12.9(2) . .
O2 Dy1 O3 C17 7.7(7) . .
O2 Dy1 O3 C19 -167.8(7) . .
O2 Dy1 O4 C1 -174.9(9) . .
O2 Dy1 O4 C2 26.4(6) . .
O2 Dy1 O5 C20 -150.1(7) . .
O2 Dy1 O6 C21 55.1(8) . .
O2 Dy1 O9 C23 -164.6(7) . .
O2 Dy1 O10 C22 86.6(8) . .
O2 Dy1 O25 C64 -47.5(11) . .
O3 C17 C18 C13 173.3(8) . .
O3 C17 C18 O1 -2.6(12) . .
O3 Dy1 O1 C18 21.9(6) . .
O3 Dy1 O1 Cu1 167.3(4) . .
O3 Dy1 O2 C7 98.8(7) . .
O3 Dy1 O2 Cu1 -40.5(4) . .
O3 Dy1 O4 C1 72.2(9) . .
O3 Dy1 O4 C2 -86.5(7) . .
O3 Dy1 O5 C20 73.6(7) . .
O3 Dy1 O6 C21 -66.1(7) . .
O3 Dy1 O9 C23 14.9(8) . .
O3 Dy1 O10 C22 -148.0(7) . .
O3 Dy1 O25 C64 75.1(11) . .
O4 C2 C3 C4 179.0(11) . .
O4 C2 C7 C6 -176.0(9) . .
O4 C2 C7 O2 1.3(15) . .
O4 Dy1 O1 C18 -103.9(7) . .
O4 Dy1 O1 Cu1 41.5(4) . .
O4 Dy1 O2 C7 -27.1(7) . .
O4 Dy1 O2 Cu1 -166.5(4) . .
O4 Dy1 O3 C17 91.0(6) . .
O4 Dy1 O3 C19 -84.5(7) . .
O4 Dy1 O5 C20 -84.6(7) . .
O4 Dy1 O6 C21 82.2(7) . .
O4 Dy1 O9 C23 143.6(8) . .
O4 Dy1 O10 C22 -18.1(8) . .
O4 Dy1 O25 C64 -97.6(11) . .
O5 C20 C21 O6 3.5(12) . .
O5 C20 C21 O8 -174.7(8) . .
O5 C20 O7 Dy2 169.3(7) . .
O5 Dy1 O1 C18 -52.0(6) . .
O5 Dy1 O1 Cu1 93.4(3) . .
O5 Dy1 O2 C7 47.1(7) . .
O5 Dy1 O2 Cu1 -92.2(3) . .
O5 Dy1 O3 C17 62.3(6) . .
O5 Dy1 O3 C19 -113.3(7) . .
O5 Dy1 O4 C1 100.8(9) . .
O5 Dy1 O4 C2 -57.9(6) . .
O5 Dy1 O6 C21 7.7(6) . .
O5 Dy1 O9 C23 112.8(7) . .
O5 Dy1 O10 C22 -114.0(7) . .
O5 Dy1 O25 C64 -5.6(13) . .
O6 C21 O8 Dy2 -174.0(7) . .
O6 Dy1 O1 C18 -7.7(8) . .
O6 Dy1 O1 Cu1 137.7(3) . .
O6 Dy1 O2 C7 2.3(9) . .
O6 Dy1 O2 Cu1 -137.0(3) . .
O6 Dy1 O3 C17 135.1(6) . .
O6 Dy1 O3 C19 -40.5(7) . .
O6 Dy1 O4 C1 28.2(8) . .
O6 Dy1 O4 C2 -130.5(7) . .
O6 Dy1 O5 C20 -5.5(6) . .
O6 Dy1 O9 C23 66.7(7) . .
O6 Dy1 O10 C22 -71.0(7) . .
O6 Dy1 O25 C64 162.8(10) . .
O7 C20 C21 O6 -179.3(8) . .
O7 C20 C21 O8 2.5(12) . .
O7 C20 O5 Dy1 -173.6(7) . .
O7 Dy2 O8 C21 -5.5(6) . .
O7 Dy2 O13 C24 -157.6(8) . .
O7 Dy2 O14 C25 64.2(8) . .
O7 Dy2 O17 C43 -153.2(7) . .
O7 Dy2 O17 Cu2 51.7(6) . .
O7 Dy2 O18 C32 67.3(8) . .
O7 Dy2 O18 Cu2 -137.9(3) . .
O7 Dy2 O19 C42 171.0(6) . .
O7 Dy2 O19 C44 -17.7(9) . .
O7 Dy2 O20 C26 55.8(7) . .
O7 Dy2 O20 C27 -123.0(7) . .
O7 Dy2 O28 C66 148.1(12) . .
O8 C21 O6 Dy1 169.2(7) . .
O8 Dy2 O7 C20 7.1(6) . .
O8 Dy2 O13 C24 131.6(8) . .
O8 Dy2 O14 C25 -30.3(8) . .
O8 Dy2 O17 C43 -72.3(7) . .
O8 Dy2 O17 Cu2 132.6(3) . .
O8 Dy2 O18 C32 129.9(8) . .
O8 Dy2 O18 Cu2 -75.2(5) . .
O8 Dy2 O19 C42 150.6(7) . .
O8 Dy2 O19 C44 -38.1(7) . .
O8 Dy2 O20 C26 25.2(8) . .
O8 Dy2 O20 C27 -153.6(6) . .
O8 Dy2 O28 C66 -140.4(12) . .
O9 C23 O11 Dy3 176.3(8) . .
O9 Dy1 O1 C18 150.3(6) . .
O9 Dy1 O1 Cu1 -64.3(5) . .
O9 Dy1 O2 C7 -81.7(8) . .
O9 Dy1 O2 Cu1 138.9(3) . .
O9 Dy1 O3 C17 -171.6(5) . .
O9 Dy1 O3 C19 12.9(8) . .
O9 Dy1 O4 C1 -54.6(8) . .
O9 Dy1 O4 C2 146.7(7) . .
O9 Dy1 O5 C20 -54.5(7) . .
O9 Dy1 O6 C21 151.6(7) . .
O9 Dy1 O10 C22 10.8(7) . .
O9 Dy1 O25 C64 -154.1(11) . .
O10 C22 C23 O9 -1.9(13) . .
O10 C22 C23 O11 177.1(9) . .
O10 C22 O12 Dy3 -172.4(8) . .
O10 Dy1 O1 C18 76.4(7) . .
O10 Dy1 O1 Cu1 -138.2(3) . .
O10 Dy1 O2 C7 -148.8(7) . .
O10 Dy1 O2 Cu1 71.8(6) . .
O10 Dy1 O3 C17 -144.8(6) . .
O10 Dy1 O3 C19 39.6(7) . .
O10 Dy1 O4 C1 -25.5(9) . .
O10 Dy1 O4 C2 175.9(6) . .
O10 Dy1 O5 C20 39.6(8) . .
O10 Dy1 O6 C21 -138.4(7) . .
O10 Dy1 O9 C23 -12.2(7) . .
O10 Dy1 O25 C64 136.1(11) . .
O11 C23 O9 Dy1 -166.5(8) . .
O11 Dy3 O12 C22 -7.5(7) . .
O11 Dy3 O15 C25 -122.4(7) . 2_776
O11 Dy3 O16 C24 120.2(7) . 2_776
O11 Dy3 O21 C62 -49.4(7) . .
O11 Dy3 O21 Cu3 96.1(3) . .
O11 Dy3 O22 C51 62.0(7) . .
O11 Dy3 O22 Cu3 -92.7(3) . .
O11 Dy3 O23 C61 59.1(7) . .
O11 Dy3 O23 C63 -101.0(9) . .
O11 Dy3 O24 C45 112.7(8) . .
O11 Dy3 O24 C46 -74.1(7) . .
O11 Dy3 O30 C68 11.9(17) . .
O12 C22 C23 O9 177.0(9) . .
O12 C22 C23 O11 -4.0(13) . .
O12 C22 O10 Dy1 172.2(8) . .
O12 Dy3 O11 C23 4.9(7) . .
O12 Dy3 O15 C25 -80.2(7) . 2_776
O12 Dy3 O16 C24 72.4(7) . 2_776
O12 Dy3 O21 C62 -7.7(9) . .
O12 Dy3 O21 Cu3 137.8(3) . .
O12 Dy3 O22 C51 15.5(9) . .
O12 Dy3 O22 Cu3 -139.2(3) . .
O12 Dy3 O23 C61 131.1(7) . .
O12 Dy3 O23 C63 -29.0(9) . .
O12 Dy3 O24 C45 39.8(8) . .
O12 Dy3 O24 C46 -147.0(7) . .
O12 Dy3 O30 C68 -173.9(13) . .
O13 C24 C25 O14 3.0(14) . .
O13 C24 C25 O15 -175.6(9) . 2_776
O13 Dy2 O7 C20 -70.2(7) . .
O13 Dy2 O8 C21 78.3(6) . .
O13 Dy2 O14 C25 14.6(7) . .
O13 Dy2 O17 C43 13.5(8) . .
O13 Dy2 O17 Cu2 -141.6(3) . .
O13 Dy2 O18 C32 -15.4(9) . .
O13 Dy2 O18 Cu2 139.5(3) . .
O13 Dy2 O19 C42 -131.0(7) . .
O13 Dy2 O19 C44 40.3(7) . .
O13 Dy2 O20 C26 -28.6(7) . .
O13 Dy2 O20 C27 152.6(7) . .
O13 Dy2 O28 C66 -163.6(10) . .
O14 Dy2 O7 C20 -116.0(7) . .
O14 Dy2 O8 C21 120.8(6) . .
O14 Dy2 O13 C24 -13.4(7) . .
O14 Dy2 O17 C43 53.7(7) . .
O14 Dy2 O17 Cu2 -101.4(3) . .
O14 Dy2 O18 C32 -63.3(8) . .
O14 Dy2 O18 Cu2 91.5(3) . .
O14 Dy2 O19 C42 -60.3(6) . .
O14 Dy2 O19 C44 111.0(7) . .
O14 Dy2 O20 C26 -99.5(7) . .
O14 Dy2 O20 C27 81.7(6) . .
O14 Dy2 O28 C66 -4.5(14) . .
O15 C25 O14 Dy2 163.7(8) 2_776 .
O15 Dy3 O11 C23 49.4(8) . .
O15 Dy3 O12 C22 -154.5(8) . .
O15 Dy3 O16 C24 -6.0(7) . 2_776
O15 Dy3 O21 C62 79.4(8) . .
O15 Dy3 O21 Cu3 -135.1(3) . .
O15 Dy3 O22 C51 -129.6(7) . .
O15 Dy3 O22 Cu3 75.7(5) . .
O15 Dy3 O23 C61 -149.2(8) . .
O15 Dy3 O23 C63 50.7(9) . .
O15 Dy3 O24 C45 -13.9(9) . .
O15 Dy3 O24 C46 159.4(6) . .
O15 Dy3 O30 C68 156.5(15) . .
O16 C24 C25 O14 -177.3(9) 2_776 .
O16 C24 C25 O15 4.1(14) 2_776 2_776
O16 C24 O13 Dy2 -168.6(7) 2_776 .
O16 Dy3 O11 C23 -46.6(8) . .
O16 Dy3 O12 C22 135.5(7) . .
O16 Dy3 O15 C25 3.7(7) . 2_776
O16 Dy3 O21 C62 158.9(7) . .
O16 Dy3 O21 Cu3 -55.6(6) . .
O16 Dy3 O22 C51 -68.2(8) . .
O16 Dy3 O22 Cu3 137.1(3) . .
O16 Dy3 O23 C61 -172.6(7) . .
O16 Dy3 O23 C63 27.4(10) . .
O16 Dy3 O24 C45 -45.8(7) . .
O16 Dy3 O24 C46 127.4(7) . .
O16 Dy3 O30 C68 -132.6(15) . .
O17 Cu2 N3 C33 -6(3) . .
O17 Cu2 N3 C34 169.2(18) . .
O17 Cu2 N4 C36 168.7(8) . .
O17 Cu2 N4 C37 -12.7(9) . .
O17 Cu2 O18 C32 140.1(7) . .
O17 Cu2 O18 Dy2 -15.9(3) . .
O17 Cu2 O27 C66 39.0(7) . .
O17 Dy2 O7 C20 99.6(7) . .
O17 Dy2 O8 C21 -153.0(6) . .
O17 Dy2 O13 C24 29.2(9) . .
O17 Dy2 O14 C25 -133.6(7) . .
O17 Dy2 O18 C32 -140.7(8) . .
O17 Dy2 O18 Cu2 14.1(2) . .
O17 Dy2 O19 C42 22.8(6) . .
O17 Dy2 O19 C44 -165.9(8) . .
O17 Dy2 O20 C26 -157.6(7) . .
O17 Dy2 O20 C27 23.6(7) . .
O17 Dy2 O28 C66 -23.3(11) . .
O18 Cu2 N3 C33 28.4(10) . .
O18 Cu2 N3 C34 -156.6(9) . .
O18 Cu2 N4 C36 -117.0(9) . .
O18 Cu2 N4 C37 61.6(13) . .
O18 Cu2 O17 C43 -138.2(8) . .
O18 Cu2 O17 Dy2 15.8(3) . .
O18 Cu2 O27 C66 -43.5(8) . .
O18 Dy2 O7 C20 157.7(7) . .
O18 Dy2 O8 C21 -76.0(8) . .
O18 Dy2 O13 C24 -66.1(8) . .
O18 Dy2 O14 C25 158.4(7) . .
O18 Dy2 O17 C43 140.7(8) . .
O18 Dy2 O17 Cu2 -14.4(2) . .
O18 Dy2 O19 C42 2.2(7) . .
O18 Dy2 O19 C44 173.4(7) . .
O18 Dy2 O20 C26 170.4(8) . .
O18 Dy2 O20 C27 -8.4(6) . .
O18 Dy2 O28 C66 45.8(11) . .
O19 C42 C43 C38 -173.9(9) . .
O19 C42 C43 O17 5.5(13) . .
O19 Dy2 O7 C20 -13.3(8) . .
O19 Dy2 O8 C21 158.9(7) . .
O19 Dy2 O13 C24 60.7(7) . .
O19 Dy2 O14 C25 -67.8(7) . .
O19 Dy2 O17 C43 -21.2(7) . .
O19 Dy2 O17 Cu2 -176.3(4) . .
O19 Dy2 O18 C32 -120.8(8) . .
O19 Dy2 O18 Cu2 34.1(4) . .
O19 Dy2 O20 C26 -74.9(8) . .
O19 Dy2 O20 C27 106.3(7) . .
O19 Dy2 O28 C66 -79.0(12) . .
O20 C27 C28 C29 -177.3(11) . .
O20 C27 C32 C31 176.5(9) . .
O20 C27 C32 O18 0.4(14) . .
O20 Dy2 O7 C20 -147.8(7) . .
O20 Dy2 O8 C21 24.5(7) . .
O20 Dy2 O13 C24 -89.2(8) . .
O20 Dy2 O14 C25 94.8(7) . .
O20 Dy2 O17 C43 110.0(7) . .
O20 Dy2 O17 Cu2 -45.1(3) . .
O20 Dy2 O18 C32 9.8(7) . .
O20 Dy2 O18 Cu2 164.6(3) . .
O20 Dy2 O19 C42 -85.1(7) . .
O20 Dy2 O19 C44 86.2(8) . .
O20 Dy2 O28 C66 94.4(11) . .
O21 Cu3 N5 C52 34(2) . .
O21 Cu3 N5 C53 -142.9(14) . .
O21 Cu3 N6 C55 -153.2(10) . .
O21 Cu3 N6 C56 26.8(10) . .
O21 Cu3 O22 C51 -139.0(8) . .
O21 Cu3 O22 Dy3 15.9(3) . .
O21 Cu3 O29 C68 -43.7(10) . .
O21 Dy3 O11 C23 151.9(8) . .
O21 Dy3 O12 C22 -51.3(8) . .
O21 Dy3 O15 C25 151.4(7) . 2_776
O21 Dy3 O16 C24 -97.2(8) . 2_776
O21 Dy3 O22 C51 140.5(8) . .
O21 Dy3 O22 Cu3 -14.2(3) . .
O21 Dy3 O23 C61 -23.5(7) . .
O21 Dy3 O23 C63 176.4(9) . .
O21 Dy3 O24 C45 167.0(7) . .
O21 Dy3 O24 C46 -19.8(8) . .
O21 Dy3 O30 C68 41.3(14) . .
O22 Cu3 N5 C52 -22.6(10) . .
O22 Cu3 N5 C53 160.1(9) . .
O22 Cu3 N6 C55 137.0(12) . .
O22 Cu3 N6 C56 -43.0(18) . .
O22 Cu3 O21 C62 128.7(8) . .
O22 Cu3 O21 Dy3 -15.9(3) . .
O22 Cu3 O29 C68 40.0(10) . .
O22 Dy3 O11 C23 -137.9(8) . .
O22 Dy3 O12 C22 42.0(8) . .
O22 Dy3 O15 C25 72.6(9) . 2_776
O22 Dy3 O16 C24 -159.0(7) . 2_776
O22 Dy3 O21 C62 -131.2(8) . .
O22 Dy3 O21 Cu3 14.3(3) . .
O22 Dy3 O23 C61 3.4(8) . .
O22 Dy3 O23 C63 -156.7(8) . .
O22 Dy3 O24 C45 -161.6(8) . .
O22 Dy3 O24 C46 11.6(6) . .
O22 Dy3 O30 C68 -28.7(14) . .
O23 C61 C62 C57 174.4(10) . .
O23 C61 C62 O21 -0.4(15) . .
O23 Dy3 O11 C23 85.7(7) . .
O23 Dy3 O12 C22 -81.5(7) . .
O23 Dy3 O15 C25 -158.6(8) . 2_776
O23 Dy3 O16 C24 17.7(8) . 2_776
O23 Dy3 O21 C62 25.3(7) . .
O23 Dy3 O21 Cu3 170.8(4) . .
O23 Dy3 O22 C51 114.7(7) . .
O23 Dy3 O22 Cu3 -40.0(4) . .
O23 Dy3 O24 C45 84.7(8) . .
O23 Dy3 O24 C46 -102.1(7) . .
O23 Dy3 O30 C68 94.7(15) . .
O24 C46 C47 C48 177.3(10) . .
O24 C46 C51 C50 -177.7(9) . .
O24 C46 C51 O22 2.9(14) . .
O24 Dy3 O11 C23 -73.2(7) . .
O24 Dy3 O12 C22 66.6(7) . .
O24 Dy3 O15 C25 -27.9(8) . 2_776
O24 Dy3 O16 C24 147.2(7) . 2_776
O24 Dy3 O21 C62 -101.3(8) . .
O24 Dy3 O21 Cu3 44.2(4) . .
O24 Dy3 O22 C51 -11.2(7) . .
O24 Dy3 O22 Cu3 -165.9(4) . .
O24 Dy3 O23 C61 86.9(8) . .
O24 Dy3 O23 C63 -73.2(9) . .
O24 Dy3 O30 C68 -78.4(15) . .
O25 C64 O26 Cu1 -21.2(15) . .
O25 Dy1 O1 C18 144.7(7) . .
O25 Dy1 O1 Cu1 -69.8(3) . .
O25 Dy1 O2 C7 -156.4(8) . .
O25 Dy1 O2 Cu1 64.2(3) . .
O25 Dy1 O3 C17 -80.0(6) . .
O25 Dy1 O3 C19 104.5(7) . .
O25 Dy1 O4 C1 -117.3(9) . .
O25 Dy1 O4 C2 84.0(7) . .
O25 Dy1 O5 C20 167.7(6) . .
O25 Dy1 O6 C21 -165.0(6) . .
O25 Dy1 O9 C23 -90.6(7) . .
O25 Dy1 O10 C22 94.2(7) . .
O26 C64 O25 Dy1 26.7(18) . .
O26 Cu1 N1 C11 -64.9(8) . .
O26 Cu1 N1 C12 120.8(10) . .
O26 Cu1 N2 C8 -127.5(9) . .
O26 Cu1 N2 C9 56.6(9) . .
O26 Cu1 O1 C18 -132.3(7) . .
O26 Cu1 O1 Dy1 81.5(3) . .
O26 Cu1 O2 C7 144.9(7) . .
O26 Cu1 O2 Dy1 -76.9(3) . .
O27 C66 O28 Dy2 -18.7(18) . .
O27 Cu2 N3 C33 126.1(10) . .
O27 Cu2 N3 C34 -59.0(9) . .
O27 Cu2 N4 C36 76.9(8) . .
O27 Cu2 N4 C37 -104.6(9) . .
O27 Cu2 O17 C43 124.3(8) . .
O27 Cu2 O17 Dy2 -81.8(3) . .
O27 Cu2 O18 C32 -129.5(7) . .
O27 Cu2 O18 Dy2 74.5(3) . .
O28 C66 O27 Cu2 11.0(13) . .
O28 Dy2 O7 C20 83.1(7) . .
O28 Dy2 O8 C21 -87.7(6) . .
O28 Dy2 O13 C24 154.6(7) . .
O28 Dy2 O14 C25 -152.3(7) . .
O28 Dy2 O17 C43 -136.6(7) . .
O28 Dy2 O17 Cu2 68.3(3) . .
O28 Dy2 O18 C32 141.4(8) . .
O28 Dy2 O18 Cu2 -63.8(3) . .
O28 Dy2 O19 C42 86.3(7) . .
O28 Dy2 O19 C44 -102.4(7) . .
O28 Dy2 O20 C26 114.6(7) . .
O28 Dy2 O20 C27 -64.2(7) . .
O29 C68 O30 Dy3 -10(3) . .
O29 Cu3 N5 C52 -116.7(10) . .
O29 Cu3 N5 C53 66.0(9) . .
O29 Cu3 N6 C55 -59.5(10) . .
O29 Cu3 N6 C56 120.5(10) . .
O29 Cu3 O21 C62 -137.5(8) . .
O29 Cu3 O21 Dy3 77.8(3) . .
O29 Cu3 O22 C51 127.8(8) . .
O29 Cu3 O22 Dy3 -77.3(3) . .
O30 C68 O29 Cu3 6(2) . .
O30 Dy3 O11 C23 -178.5(7) . .
O30 Dy3 O12 C22 176.0(7) . .
O30 Dy3 O15 C25 83.2(7) . 2_776
O30 Dy3 O16 C24 -85.4(7) . 2_776
O30 Dy3 O21 C62 147.2(8) . .
O30 Dy3 O21 Cu3 -67.3(3) . .
O30 Dy3 O22 C51 -140.0(8) . .
O30 Dy3 O22 Cu3 65.3(3) . .
O30 Dy3 O23 C61 -84.5(7) . .
O30 Dy3 O23 C63 115.4(9) . .
O30 Dy3 O24 C45 -104.2(8) . .
O30 Dy3 O24 C46 69.0(7) . .
C69X C68 O29 Cu3 167.1(14) . .
C69X C68 O30 Dy3 -172.0(14) . .
C69 C68 O29 Cu3 -161.6(14) . .
C69 C68 O30 Dy3 157.4(14) . .
#BEGIN Loops that were not found in dictionaries:
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
1 -0.051 0.280 0.098 9.3 0.0
2 0.500 0.500 -0.742 1159.1 409.3
3 0.051 0.720 0.902 9.3 0.0
#END Loops that were not found in dictionaries
