#------------------------------------------------------------------------------
#$Date: 2015-07-11 00:39:46 +0300 (Sat, 11 Jul 2015) $
#$Revision: 143578 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/53/7035312.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7035312
loop_
_publ_author_name
'Ma, Pengtao'
'Wan, Rong'
'Si, Yanan'
'Hu, Feng'
'Wang, Yueyan'
'Niu, Jingyang'
'Wang, Jingping'
_publ_section_title
;
 Double-malate bridging tri-lanthanoid cluster encapsulated
 arsenotungstates: syntheses, structures, luminescence and magnetic
 properties.
;
_journal_issue                   25
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              11514
_journal_page_last               11523
_journal_paper_doi               10.1039/c5dt01323b
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         '0.5(C16 H12 As8 Eu12 K40 Li4 O360 W76), O'
_chemical_formula_sum            'C8 H74 As4 Eu6 K20 Li2 O181 W38'
_chemical_formula_weight         12060.29
_chemical_name_systematic
;
 ? 
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   difmap
_audit_creation_date             2015-05-01
_audit_creation_method
;
Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
;
_audit_update_record
;
2015-05-05 deposited with the CCDC.
2015-06-02 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 112.625(9)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   21.063(11)
_cell_length_b                   25.446(14)
_cell_length_c                   22.740(12)
_cell_measurement_reflns_used    9455
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.08
_cell_measurement_theta_min      2.24
_cell_volume                     11250(10)
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'ShelXD-1997 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296.15
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0621
_diffrn_reflns_av_unetI/netI     0.0741
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -30
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            57476
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.86
_diffrn_source                   'fine-focus sealed tube'
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    22.029
_exptl_absorpt_correction_T_max  0.7457
_exptl_absorpt_correction_T_min  0.4331
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.1241 before and 0.0577 after correction.
The Ratio of minimum to maximum transmission is 0.5808.
The λ/2 correction factor is 0.0015.
;
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    3.560
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             10556
_exptl_crystal_preparation       'Magnetic properties, Luminescent'
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.12
_refine_diff_density_max         2.988
_refine_diff_density_min         -1.556
_refine_diff_density_rms         0.368
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.007
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1108
_refine_ls_number_reflns         19740
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.007
_refine_ls_R_factor_all          0.0729
_refine_ls_R_factor_gt           0.0429
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0542P)²+82.4822P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1037
_refine_ls_wR_factor_ref         0.1181
_reflns_number_gt                14124
_reflns_number_total             19740
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5dt01323b2.cif
_cod_data_source_block           1043922
_cod_depositor_comments
'Adding full bibliography for 7035309--7035313.cif.'
_cod_original_cell_volume        11250(11)
_cod_database_code               7035312
_audit_block_doi                 10.5517/cc1418xc
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2. Others
 Fixed Sof: K3(0.5) K4(0.5) K5(0.5) K6(0.5) K7(0.5) K8(0.5) K9(0.5) K10(0.5)
 K11(0.5) K12(0.5) K13(0.5) K14(0.5) K15(0.5) K16(0.25) K17(0.25) K18(0.25)
 K19(0.25) K20(0.25) K21(0.25) O10W(0.5) O11W(0.5) O12W(0.5) O13W(0.5)
 O14W(0.5) O15W(0.5) O16W(0.5) O17W(0.5) O18W(0.5) O19W(0.5) O20W(0.5)
 O21W(0.5) O22W(0.5) O23W(0.5) O24W(0.5)
 Fixed Uiso: K15(0.15015) O9W(0.10229) O20W(0.10311) O23W(0.11879) O24W(0.11649)
3.a Ternary CH refined with riding coordinates:
 C2(H2)
3.b Secondary CH2 refined with riding coordinates:
 C3(H3A,H3B)
;
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 'x, y, z'
2 '-x+1/2, y+1/2, -z+1/2'
3 '-x, -y, -z'
4 'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags_posn
W1 W 0.66625(3) 0.11255(3) 0.85165(3) 0.02455(15) Uani 1 d .
W2 W 0.58620(3) 0.01351(3) 0.75414(3) 0.02637(16) Uani 1 d .
W3 W 0.66421(3) 0.11003(3) 0.70149(3) 0.03053(17) Uani 1 d .
W4 W 0.42676(4) 0.03380(3) 0.61177(3) 0.02753(16) Uani 1 d .
W5 W 0.50115(4) 0.13065(3) 0.55785(3) 0.03335(18) Uani 1 d .
W6 W 0.35337(3) 0.15299(3) 0.58276(3) 0.02878(17) Uani 1 d .
W7 W 0.58170(4) 0.24178(3) 0.66583(3) 0.03058(17) Uani 1 d .
W8 W 0.43541(3) 0.26093(3) 0.69436(3) 0.02760(16) Uani 1 d .
W9 W 0.58880(3) 0.24533(3) 0.81612(3) 0.02557(16) Uani 1 d .
W10 W 0.53557(3) 0.15873(2) 0.91809(3) 0.02173(15) Uani 1 d .
W11 W 0.18820(3) -0.00357(3) 0.76509(3) 0.02528(16) Uani 1 d .
W12 W 0.12380(3) 0.08958(3) 0.64598(3) 0.02783(16) Uani 1 d .
W13 W 0.02057(4) 0.03518(3) 0.71265(4) 0.03581(19) Uani 1 d .
W14 W 0.08293(3) 0.22227(3) 0.68697(3) 0.03108(17) Uani 1 d .
W15 W -0.02369(4) 0.16852(3) 0.75097(4) 0.0387(2) Uani 1 d .
W16 W 0.10779(4) 0.25121(3) 0.83806(4) 0.03422(18) Uani 1 d .
W17 W 0.04622(4) 0.06713(3) 0.87949(4) 0.0403(2) Uani 1 d .
W18 W 0.17620(4) 0.15225(3) 0.96326(4) 0.03581(19) Uani 1 d .
W19 W 0.21505(4) 0.03119(3) 0.93076(3) 0.02904(17) Uani 1 d .
Eu1 Eu 0.29789(4) 0.05424(3) 0.69980(4) 0.02284(18) Uani 1 d .
Eu2 Eu 0.36776(4) 0.06722(3) 0.87522(4) 0.02063(18) Uani 1 d .
Eu3 Eu 0.27947(4) 0.19552(3) 0.71358(4) 0.02475(19) Uani 1 d .
As1 As 0.49718(8) 0.13267(6) 0.72762(7) 0.0199(3) Uani 1 d .
As2 As 0.16704(8) 0.12850(6) 0.80776(8) 0.0225(4) Uani 1 d .
K1 K 0.7605(3) 0.2333(2) 0.9493(3) 0.0685(15) Uani 1 d .
K2 K 0.5117(4) -0.1052(3) 0.6354(3) 0.104(2) Uani 1 d .
K3 K 0.0749(5) -0.0763(4) 0.8350(4) 0.049(2) Uiso 0.50 d .
K4 K 0.4261(5) 0.2872(4) 0.8583(5) 0.058(3) Uiso 0.50 d .
K5 K 0.1580(6) -0.1133(4) 0.9452(5) 0.070(3) Uiso 0.50 d .
K6 K 0.5862(6) 0.2359(4) 0.4997(5) 0.069(3) Uiso 0.50 d .
K7 K 0.1900(7) 0.3451(5) 0.7539(6) 0.089(4) Uiso 0.50 d .
K8 K 0.5769(7) 0.0047(5) 0.9322(6) 0.090(4) Uiso 0.50 d .
K9 K 0.4463(7) 0.1716(5) 0.0470(7) 0.096(4) Uiso 0.50 d .
K10 K 0.2306(7) 0.0249(5) 0.1046(7) 0.098(4) Uiso 0.50 d .
K11 K 0.7654(9) 0.2289(7) 0.6610(9) 0.134(6) Uiso 0.50 d .
K12 K 0.6207(9) 0.8641(7) 0.8215(8) 0.125(5) Uiso 0.50 d .
K13 K 0.9019(11) 0.2136(8) 1.0124(10) 0.156(7) Uiso 0.50 d .
K14 K 0.6740(9) 0.0747(7) 0.5424(8) 0.132(6) Uiso 0.50 d .
K15 K 0.5855(10) -0.0198(8) 0.5759(9) 0.150 Uiso 0.50 d .
K16 K 0.3583(15) 0.0926(12) 0.0747(14) 0.105(9) Uiso 0.25 d .
K17 K -0.0720(16) 0.1295(12) 0.5639(15) 0.112(9) Uiso 0.25 d .
K18 K 0.0892(15) 0.1980(12) 0.5032(14) 0.106(9) Uiso 0.25 d .
K19 K 0.1220(17) -0.0573(13) 0.5863(16) 0.122(11) Uiso 0.25 d .
K20 K 0.463(2) 0.3836(16) 0.8219(19) 0.150(13) Uiso 0.25 d .
K21 K 0.783(2) 0.2277(16) 0.8159(19) 0.149(13) Uiso 0.25 d .
O1 O 0.7406(6) 0.1158(5) 0.9212(6) 0.040(3) Uani 1 d .
O2 O 0.6600(5) 0.0390(4) 0.8318(5) 0.028(3) Uani 1 d .
O3 O 0.7137(5) 0.1195(4) 0.7901(5) 0.028(3) Uani 1 d .
O4 O 0.6504(5) 0.1876(4) 0.8350(5) 0.028(3) Uani 1 d .
O5 O 0.5976(5) 0.1125(4) 0.8805(5) 0.028(3) Uani 1 d .
O6 O 0.5812(5) 0.1031(4) 0.7475(5) 0.025(2) Uani 1 d .
O7 O 0.6112(6) -0.0517(5) 0.7580(6) 0.043(3) Uani 1 d .
O8 O 0.5245(5) 0.0154(4) 0.7883(5) 0.031(3) Uani 1 d .
O9 O 0.6527(5) 0.0384(4) 0.7129(5) 0.032(3) Uani 1 d .
O10 O 0.5166(6) 0.0150(4) 0.6679(5) 0.032(3) Uani 1 d .
O11 O 0.7329(6) 0.1094(5) 0.6778(6) 0.041(3) Uani 1 d .
O12 O 0.5880(6) 0.1086(5) 0.6208(5) 0.037(3) Uani 1 d .
O13 O 0.6445(6) 0.1861(4) 0.6983(5) 0.034(3) Uani 1 d .
O14 O 0.3986(6) -0.0250(5) 0.5718(5) 0.042(3) Uani 1 d .
O15 O 0.3917(6) 0.0349(4) 0.6713(5) 0.033(3) Uani 1 d .
O16 O 0.4708(6) 0.0610(4) 0.5513(5) 0.036(3) Uani 1 d .
O17 O 0.3509(5) 0.0798(4) 0.5582(5) 0.027(3) Uani 1 d .
O18 O 0.4613(6) 0.1195(5) 0.6433(5) 0.033(3) Uani 1 d .
O19 O 0.5193(6) 0.1357(5) 0.4891(5) 0.046(3) Uani 1 d .
O20 O 0.4121(6) 0.1589(4) 0.5293(5) 0.034(3) Uani 1 d .
O21 O 0.5323(6) 0.2009(4) 0.5954(5) 0.033(3) Uani 1 d .
O22 O 0.2783(6) 0.1747(5) 0.5214(5) 0.041(3) Uani 1 d .
O23 O 0.3270(5) 0.1377(4) 0.6487(5) 0.029(3) Uani 1 d .
O24 O 0.3950(6) 0.2182(4) 0.6178(5) 0.033(3) Uani 1 d .
O25 O 0.6257(6) 0.2835(5) 0.6350(6) 0.043(3) Uani 1 d .
O26 O 0.5036(6) 0.2826(4) 0.6547(5) 0.037(3) Uani 1 d .
O27 O 0.6216(5) 0.2693(4) 0.7542(5) 0.031(3) Uani 1 d .
O28 O 0.5222(5) 0.1995(4) 0.7217(5) 0.024(2) Uani 1 d .
O29 O 0.3867(6) 0.3180(4) 0.6743(6) 0.044(3) Uani 1 d .
O30 O 0.3928(5) 0.2227(4) 0.7339(5) 0.030(3) Uani 1 d .
O31 O 0.5055(5) 0.2846(4) 0.7746(5) 0.023(2) Uani 1 d .
O32 O 0.6333(7) 0.2869(5) 0.8786(5) 0.042(3) Uani 1 d .
O33 O 0.5355(5) 0.2045(4) 0.8532(5) 0.025(2) Uani 1 d .
O34 O 0.4970(6) 0.2029(5) 0.9524(5) 0.038(3) Uani 1 d .
O35 O 0.4672(5) 0.1137(4) 0.8811(5) 0.029(3) Uani 1 d .
O36 O 0.6375(6) 0.1903(4) 0.9705(5) 0.033(3) Uani 1 d .
O37 O 0.5760(6) 0.1120(4) 0.9905(5) 0.031(3) Uani 1 d .
O38 O 0.7358(7) 0.1797(5) 1.0520(6) 0.050(4) Uani 1 d .
O39 O 0.6223(6) 0.0240(5) 1.0954(5) 0.039(3) Uani 1 d .
O40 O 0.6111(7) 0.0743(5) 1.1707(7) 0.051(4) Uani 1 d .
O41 O 0.2161(6) -0.0661(4) 0.7590(5) 0.035(3) Uani 1 d .
O42 O 0.2696(5) 0.0343(4) 0.7905(5) 0.024(2) Uani 1 d .
O43 O 0.1743(5) 0.0227(4) 0.6783(5) 0.027(3) Uani 1 d .
O44 O 0.0893(5) -0.0193(4) 0.7293(5) 0.031(3) Uani 1 d .
O45 O 0.1878(5) -0.0034(4) 0.8485(5) 0.028(3) Uani 1 d .
O46 O 0.1293(5) 0.0785(4) 0.7510(5) 0.027(3) Uani 1 d .
O47 O 0.1114(6) 0.0852(5) 0.5658(6) 0.045(3) Uani 1 d .
O48 O 0.2109(5) 0.1196(4) 0.6827(5) 0.029(3) Uani 1 d .
O49 O 0.0412(5) 0.0508(5) 0.6389(5) 0.037(3) Uani 1 d .
O50 O 0.0795(5) 0.1526(4) 0.6475(5) 0.029(3) Uani 1 d .
O51 O -0.0531(6) -0.0020(5) 0.6761(7) 0.057(4) Uani 1 d .
O52 O -0.0165(6) 0.1029(5) 0.7088(6) 0.044(3) Uani 1 d .
O53 O 0.0323(6) 0.0317(4) 0.7993(6) 0.041(3) Uani 1 d .
O54 O 0.0583(7) 0.2615(5) 0.6198(6) 0.051(4) Uani 1 d .
O55 O -0.0129(6) 0.2025(5) 0.6807(6) 0.042(3) Uani 1 d .
O56 O 0.1744(5) 0.2204(4) 0.7157(5) 0.030(3) Uani 1 d .
O57 O 0.0809(6) 0.2741(4) 0.7480(5) 0.033(3) Uani 1 d .
O58 O 0.0966(5) 0.1752(4) 0.7797(5) 0.030(3) Uani 1 d .
O59 O -0.1126(6) 0.1710(6) 0.7265(7) 0.058(4) Uani 1 d .
O60 O 0.0048(6) 0.2277(5) 0.8031(6) 0.040(3) Uani 1 d .
O61 O -0.0008(6) 0.1233(5) 0.8234(6) 0.044(3) Uani 1 d .
O62 O 0.0925(7) 0.3098(5) 0.8709(7) 0.049(4) Uani 1 d .
O63 O 0.1954(6) 0.2532(5) 0.8513(6) 0.043(3) Uani 1 d .
O64 O 0.1176(6) 0.2048(4) 0.9073(5) 0.033(3) Uani 1 d .
O65 O -0.0196(7) 0.0412(6) 0.8966(8) 0.068(5) Uani 1 d .
O66 O 0.0823(6) 0.1136(5) 0.9461(6) 0.045(3) Uani 1 d .
O67 O 0.1160(6) 0.0167(4) 0.9176(6) 0.042(3) Uani 1 d .
O68 O 0.1490(5) 0.1021(4) 0.8723(5) 0.030(3) Uani 1 d .
O69 O 0.1832(7) 0.1782(5) 1.0357(6) 0.052(4) Uani 1 d .
O70 O 0.2522(6) 0.1719(5) 0.9544(6) 0.038(3) Uani 1 d .
O71 O 0.2135(6) 0.0810(4) 0.9928(6) 0.037(3) Uani 1 d .
O72 O 0.2514(7) -0.0212(5) 0.9823(6) 0.046(3) Uani 1 d .
O73 O 0.2864(6) 0.0605(5) 0.9193(5) 0.035(3) Uani 1 d .
O74 O 0.3424(6) 0.1231(4) 0.7780(5) 0.029(3) Uani 1 d .
C1 C 0.6751(9) 0.1655(7) 1.0190(8) 0.034(4) Uani 1 d .
C2 C 0.6436(9) 0.1170(9) 1.0329(9) 0.053(6) Uani 1 d .
H2 H 0.6690 0.0870 1.0259 0.063 Uiso 1 calc R
C3 C 0.6513(12) 0.1154(8) 1.0990(9) 0.053(6) Uani 1 d .
H3A H 0.6278 0.1459 1.1066 0.064 Uiso 1 calc R
H3B H 0.6998 0.1196 1.1250 0.064 Uiso 1 calc R
C4 C 0.6266(8) 0.0687(6) 1.1233(9) 0.028(4) Uani 1 d .
O1W O 0.2979(6) -0.0426(5) 0.6872(6) 0.039(3) Uiso 1 d .
O2W O 0.2419(6) 0.0403(5) 0.5830(5) 0.037(3) Uiso 1 d .
O3W O 0.4020(5) 0.0206(4) 0.7968(5) 0.024(2) Uiso 1 d .
O4W O 0.4546(6) 0.0616(5) 0.9870(6) 0.040(3) Uiso 1 d .
O5W O 0.3577(6) 0.1532(5) 0.9196(5) 0.037(3) Uiso 1 d .
O6W O 0.2789(7) 0.2943(5) 0.7106(6) 0.050(3) Uiso 1 d .
O7W O 0.3048(6) 0.2270(5) 0.8224(5) 0.037(3) Uiso 1 d .
O8W O 0.2188(7) 0.2227(5) 0.6038(6) 0.056(4) Uiso 1 d .
O9W O 0.4316(10) -0.0839(8) 0.7064(9) 0.102 Uiso 1 d .
O10W O 0.3089(15) 0.3501(12) 0.8726(14) 0.066(8) Uiso 0.50 d .
O11W O 0.9955(14) 0.3594(12) 0.6865(13) 0.056(8) Uiso 0.50 d .
O12W O 0.5847(17) -0.1835(13) 0.7255(16) 0.077(10) Uiso 0.50 d .
O13W O 0.8720(17) 0.2685(13) 0.6110(16) 0.078(10) Uiso 0.50 d .
O14W O 0.2913(15) 0.2835(11) 0.9788(14) 0.061(8) Uiso 0.50 d .
O15W O 0.639(2) 0.3703(15) 0.9626(18) 0.097(12) Uiso 0.50 d .
O16W O 0.302(2) -0.1069(18) 0.575(2) 0.124(15) Uiso 0.50 d .
O17W O 0.8553(19) 0.1109(15) 0.8270(17) 0.093(11) Uiso 0.50 d .
O18W O 0.835(2) 0.0734(15) 0.6502(18) 0.102(12) Uiso 0.50 d .
O19W O 0.744(2) 0.8655(18) 0.839(2) 0.126(15) Uiso 0.50 d .
O20W O 0.714(2) -0.0483(16) 0.6848(19) 0.103 Uiso 0.50 d .
O21W O 0.344(2) 0.1911(16) 0.4056(19) 0.108(13) Uiso 0.50 d .
O22W O 0.105(2) -0.0460(17) 1.020(2) 0.113(14) Uiso 0.50 d .
O23W O 0.968(2) 0.4026(18) 0.663(2) 0.119 Uiso 0.50 d .
O24W O -0.010(2) 0.1932(17) 0.495(2) 0.116 Uiso 0.50 d .
Li1 Li 0.789(4) 0.855(3) 0.727(3) 0.14(2) Uiso 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
K1 W1 K8 119.6(2) . .
K1 W1 K10 116.1(2) . 3_656
K1 W1 K21 48.0(6) . .
K10 W1 K8 67.0(3) 3_656 .
K10 W1 K21 111.2(6) 3_656 .
K21 W1 K8 166.4(6) . .
O1 W1 K1 50.1(4) . .
O1 W1 K8 91.9(4) . .
O1 W1 K10 66.9(5) . 3_656
O1 W1 K21 75.4(7) . .
O1 W1 O2 102.5(5) . .
O1 W1 O3 96.5(5) . .
O1 W1 O4 99.0(5) . .
O1 W1 O5 103.7(5) . .
O1 W1 O6 168.3(5) . .
O2 W1 K1 152.3(3) . .
O2 W1 K8 57.0(4) . .
O2 W1 K10 36.3(4) . 3_656
O2 W1 K21 130.0(7) . .
O2 W1 O3 85.9(4) . .
O2 W1 O4 156.7(4) . .
O2 W1 O6 73.0(4) . .
O3 W1 K1 92.7(3) . .
O3 W1 K8 142.9(4) . .
O3 W1 K10 83.3(4) . 3_656
O3 W1 K21 46.0(6) . .
O3 W1 O6 72.6(4) . .
O4 W1 K1 49.0(3) . .
O4 W1 K8 131.5(4) . .
O4 W1 K10 158.8(4) . 3_656
O4 W1 K21 48.2(7) . .
O4 W1 O3 82.7(4) . .
O4 W1 O6 84.2(4) . .
O5 W1 K1 95.6(4) . .
O5 W1 K8 43.3(4) . .
O5 W1 K10 109.9(4) . 3_656
O5 W1 K21 134.3(7) . .
O5 W1 O2 95.4(5) . .
O5 W1 O3 159.0(5) . .
O5 W1 O4 88.3(5) . .
O5 W1 O6 87.7(4) . .
O6 W1 K1 132.8(3) . .
O6 W1 K8 94.4(3) . .
O6 W1 K10 106.6(3) . 3_656
O6 W1 K21 98.9(6) . .
K2 W2 K8 118.2(2) . .
K2 W2 K10 111.2(2) . 3_656
K2 W2 K12 60.6(3) . 1_545
K2 W2 K15 47.4(3) . .
K8 W2 K15 164.8(3) . .
K10 W2 K8 66.6(3) 3_656 .
K10 W2 K15 111.6(3) 3_656 .
K12 W2 K8 69.4(3) 1_545 .
K12 W2 K10 60.0(3) 1_545 3_656
K12 W2 K15 96.4(4) 1_545 .
O2 W2 K2 146.9(3) . .
O2 W2 K8 57.0(4) . .
O2 W2 K10 35.7(4) . 3_656
O2 W2 K12 90.3(4) . 1_545
O2 W2 K15 130.8(4) . .
O2 W2 O6 74.3(4) . .
O2 W2 O9 82.3(4) . .
O6 W2 K2 136.2(3) . .
O6 W2 K8 95.8(3) . .
O6 W2 K10 107.3(3) . 3_656
O6 W2 K12 163.1(3) . 1_545
O6 W2 K15 99.0(4) . .
O7 W2 K2 48.4(4) . .
O7 W2 K8 91.5(5) . .
O7 W2 K10 63.5(5) . 3_656
O7 W2 K12 22.7(5) . 1_545
O7 W2 K15 74.9(5) . .
O7 W2 O2 98.7(5) . .
O7 W2 O6 164.6(5) . .
O7 W2 O8 105.4(6) . .
O7 W2 O9 94.0(5) . .
O7 W2 O10 99.5(5) . .
O8 W2 K2 99.0(4) . .
O8 W2 K8 40.9(4) . .
O8 W2 K10 107.2(4) . 3_656
O8 W2 K12 85.0(4) . 1_545
O8 W2 K15 135.8(5) . .
O8 W2 O2 93.3(5) . .
O8 W2 O6 88.8(4) . .
O8 W2 O9 160.5(5) . .
O8 W2 O10 92.7(5) . .
O9 W2 K2 94.8(3) . .
O9 W2 K8 139.3(4) . .
O9 W2 K10 80.2(4) . 3_656
O9 W2 K12 113.9(4) . 1_545
O9 W2 K15 50.5(4) . .
O9 W2 O6 71.7(4) . .
O10 W2 K2 51.6(3) . .
O10 W2 K8 133.4(4) . .
O10 W2 K10 156.4(4) . 3_656
O10 W2 K12 110.8(4) . 1_545
O10 W2 K15 45.4(4) . .
O10 W2 O2 158.5(5) . .
O10 W2 O6 85.2(4) . .
O10 W2 O9 85.1(5) . .
K11 W3 K21 49.4(6) . .
K14 W3 K11 74.5(4) . .
K14 W3 K21 122.0(6) . .
O3 W3 K11 91.4(4) . .
O3 W3 K14 146.2(4) . .
O3 W3 K21 44.3(6) . .
O3 W3 O6 74.7(4) . .
O3 W3 O12 159.3(5) . .
O3 W3 O13 86.4(5) . .
O6 W3 K11 135.0(4) . .
O6 W3 K14 136.2(4) . .
O6 W3 K21 98.5(6) . .
O9 W3 K11 151.2(4) . .
O9 W3 K14 87.6(4) . .
O9 W3 K21 134.4(7) . .
O9 W3 O3 91.4(5) . .
O9 W3 O6 73.1(4) . .
O9 W3 O12 90.5(5) . .
O9 W3 O13 157.5(4) . .
O11 W3 K11 49.6(5) . .
O11 W3 K14 49.0(5) . .
O11 W3 K21 80.0(7) . .
O11 W3 O3 98.6(5) . .
O11 W3 O6 171.1(5) . .
O11 W3 O9 101.7(5) . .
O11 W3 O12 101.2(5) . .
O11 W3 O13 100.8(5) . .
O12 W3 K11 96.8(4) . .
O12 W3 K14 54.4(4) . .
O12 W3 K21 134.4(7) . .
O12 W3 O6 86.1(4) . .
O12 W3 O13 84.1(5) . .
O13 W3 K11 51.3(4) . .
O13 W3 K14 106.5(4) . .
O13 W3 K21 51.6(6) . .
O13 W3 O6 84.8(4) . .
K2 W4 K15 48.8(3) . .
O10 W4 K2 52.5(4) . .
O10 W4 K15 49.4(4) . .
O10 W4 O16 86.8(5) . .
O10 W4 O17 157.9(5) . .
O10 W4 O18 85.2(4) . .
O14 W4 K2 48.4(4) . .
O14 W4 K15 75.0(5) . .
O14 W4 O10 100.7(5) . .
O14 W4 O15 104.8(5) . .
O14 W4 O16 95.2(5) . .
O14 W4 O17 99.0(5) . .
O14 W4 O18 167.4(5) . .
O15 W4 K2 102.3(4) . .
O15 W4 K15 142.4(4) . .
O15 W4 O10 95.3(5) . .
O15 W4 O16 159.0(5) . .
O15 W4 O17 89.2(5) . .
O15 W4 O18 85.5(4) . .
O16 W4 K2 95.5(3) . .
O16 W4 K15 49.1(4) . .
O16 W4 O18 73.8(4) . .
O17 W4 K2 147.1(3) . .
O17 W4 K15 128.4(4) . .
O17 W4 O16 81.6(5) . .
O17 W4 O18 73.6(4) . .
O18 W4 K2 137.3(3) . .
O18 W4 K15 101.3(4) . .
K6 W5 K14 69.6(3) . .
K6 W5 K15 111.9(3) . 3_656
K15 W5 K14 81.3(4) 3_656 .
O12 W5 K6 91.4(4) . .
O12 W5 K14 48.1(4) . .
O12 W5 K15 112.4(5) . 3_656
O12 W5 O18 83.8(4) . .
O12 W5 O21 83.1(5) . .
O16 W5 K6 147.9(4) . .
O16 W5 K14 87.2(4) . .
O16 W5 K15 40.1(4) . 3_656
O16 W5 O12 88.9(5) . .
O16 W5 O18 74.8(4) . .
O16 W5 O20 94.0(5) . .
O16 W5 O21 159.4(4) . .
O18 W5 K6 137.1(3) . .
O18 W5 K14 129.2(4) . .
O18 W5 K15 109.2(4) . 3_656
O19 W5 K6 48.1(5) . .
O19 W5 K14 55.6(5) . .
O19 W5 K15 64.5(5) . 3_656
O19 W5 O12 102.4(5) . .
O19 W5 O16 100.6(5) . .
O19 W5 O18 172.4(5) . .
O19 W5 O20 101.3(5) . .
O19 W5 O21 99.7(5) . .
O20 W5 K6 98.9(4) . .
O20 W5 K14 156.5(4) . .
O20 W5 K15 84.5(4) . 3_656
O20 W5 O12 155.2(5) . .
O20 W5 O18 73.3(4) . .
O20 W5 O21 85.7(5) . .
O21 W5 K6 51.8(4) . .
O21 W5 K14 101.2(4) . .
O21 W5 K15 159.2(4) . 3_656
O21 W5 O18 85.4(4) . .
K13 W6 K1 40.3(3) 4_565 4_565
O17 W6 K1 120.8(3) . 4_565
O17 W6 K13 132.4(4) . 4_565
O17 W6 O18 74.3(4) . .
O17 W6 O20 81.6(4) . .
O18 W6 K1 141.0(3) . 4_565
O18 W6 K13 101.8(4) . 4_565
O20 W6 K1 74.6(3) . 4_565
O20 W6 K13 53.3(4) . 4_565
O20 W6 O18 72.6(4) . .
O22 W6 K1 32.8(4) . 4_565
O22 W6 K13 73.1(5) . 4_565
O22 W6 O17 99.1(5) . .
O22 W6 O18 165.7(5) . .
O22 W6 O20 94.1(5) . .
O22 W6 O23 104.7(5) . .
O22 W6 O24 100.9(5) . .
O23 W6 K1 123.2(3) . 4_565
O23 W6 K13 134.8(4) . 4_565
O23 W6 O17 92.8(5) . .
O23 W6 O18 88.5(4) . .
O23 W6 O20 161.0(5) . .
O23 W6 O24 94.5(5) . .
O24 W6 K1 72.9(3) . 4_565
O24 W6 K13 44.6(4) . 4_565
O24 W6 O17 156.3(4) . .
O24 W6 O18 83.3(4) . .
O24 W6 O20 84.2(5) . .
K6 W7 K11 64.5(3) . .
O13 W7 K6 94.4(4) . .
O13 W7 K11 52.9(4) . .
O13 W7 O27 84.8(5) . .
O13 W7 O28 83.4(4) . .
O21 W7 K6 48.9(4) . .
O21 W7 K11 99.2(4) . .
O21 W7 O13 89.6(5) . .
O21 W7 O26 91.3(5) . .
O21 W7 O27 161.8(4) . .
O21 W7 O28 88.4(4) . .
O25 W7 K6 53.1(4) . .
O25 W7 K11 49.5(5) . .
O25 W7 O13 102.4(5) . .
O25 W7 O21 101.7(5) . .
O25 W7 O26 100.7(5) . .
O25 W7 O27 96.3(5) . .
O25 W7 O28 168.2(5) . .
O26 W7 K6 104.0(4) . .
O26 W7 K11 149.8(4) . .
O26 W7 O13 156.2(5) . .
O26 W7 O27 87.1(5) . .
O26 W7 O28 72.8(4) . .
O27 W7 K6 148.7(3) . .
O27 W7 K11 91.2(4) . .
O27 W7 O28 73.8(4) . .
O28 W7 K6 137.3(3) . .
O28 W7 K11 135.3(4) . .
Eu3 W8 K4 66.66(15) . .
Eu3 W8 K13 111.8(3) . 4_565
K4 W8 K13 157.1(3) . 4_565
O24 W8 Eu3 76.2(3) . .
O24 W8 K4 142.3(4) . .
O24 W8 K13 47.1(4) . 4_565
O24 W8 O26 84.0(5) . .
O24 W8 O28 83.8(4) . .
O24 W8 O31 157.2(4) . .
O26 W8 Eu3 160.2(3) . .
O26 W8 K4 133.1(4) . .
O26 W8 K13 51.0(4) . 4_565
O26 W8 O28 71.4(4) . .
O28 W8 Eu3 107.4(2) . .
O28 W8 K4 100.7(3) . .
O28 W8 K13 101.3(4) . 4_565
O29 W8 Eu3 87.0(4) . .
O29 W8 K4 82.2(5) . .
O29 W8 K13 74.9(5) . 4_565
O29 W8 O24 102.8(5) . .
O29 W8 O26 95.9(5) . .
O29 W8 O28 165.3(5) . .
O29 W8 O30 103.2(5) . .
O29 W8 O31 98.4(5) . .
O30 W8 Eu3 24.7(3) . .
O30 W8 K4 52.1(4) . .
O30 W8 K13 133.8(5) . 4_565
O30 W8 O24 90.9(5) . .
O30 W8 O26 160.9(5) . .
O30 W8 O28 89.7(4) . .
O30 W8 O31 92.5(5) . .
O31 W8 Eu3 113.5(3) . .
O31 W8 K4 49.1(3) . .
O31 W8 K13 133.8(4) . 4_565
O31 W8 O26 85.5(4) . .
O31 W8 O28 73.7(4) . .
K1 W9 K4 118.32(17) . .
K1 W9 K21 48.6(6) . .
K4 W9 K21 164.3(6) . .
O4 W9 K1 52.2(3) . .
O4 W9 K4 136.0(4) . .
O4 W9 K21 47.3(6) . .
O4 W9 O28 86.5(4) . .
O4 W9 O31 158.4(4) . .
O4 W9 O33 87.0(4) . .
O27 W9 K1 96.5(3) . .
O27 W9 K4 132.6(4) . .
O27 W9 K21 52.2(6) . .
O27 W9 O4 90.3(5) . .
O27 W9 O28 75.1(4) . .
O27 W9 O31 89.6(5) . .
O27 W9 O33 158.8(4) . .
O28 W9 K1 138.3(3) . .
O28 W9 K4 94.8(3) . .
O28 W9 K21 100.8(6) . .
O31 W9 K1 149.1(3) . .
O31 W9 K4 44.1(3) . .
O31 W9 K21 140.9(6) . .
O31 W9 O28 72.5(4) . .
O31 W9 O33 85.4(4) . .
O32 W9 K1 48.2(4) . .
O32 W9 K4 83.4(5) . .
O32 W9 K21 81.0(7) . .
O32 W9 O4 100.4(5) . .
O32 W9 O27 100.1(5) . .
O32 W9 O28 171.7(5) . .
O32 W9 O31 100.9(5) . .
O32 W9 O33 101.0(5) . .
O33 W9 K1 98.3(3) . .
O33 W9 K4 49.8(3) . .
O33 W9 K21 133.0(6) . .
O33 W9 O28 83.7(4) . .
K4 W10 K8 157.4(2) . .
K4 W10 K9 79.0(2) . 1_556
K4 W10 K18 55.9(4) . 4_666
K8 W10 K9 99.7(3) . 1_556
K8 W10 K18 145.7(5) . 4_666
K9 W10 K18 72.9(5) 1_556 4_666
O5 W10 K4 132.7(3) . .
O5 W10 K8 49.7(3) . .
O5 W10 K9 147.9(3) . 1_556
O5 W10 K18 125.0(5) . 4_666
O5 W10 O36 78.3(4) . .
O33 W10 K4 52.4(4) . .
O33 W10 K8 127.2(4) . .
O33 W10 K9 131.0(4) . 1_556
O33 W10 K18 74.6(5) . 4_666
O33 W10 O5 81.1(4) . .
O33 W10 O36 84.5(4) . .
O33 W10 O37 155.9(5) . .
O34 W10 K4 45.9(4) . .
O34 W10 K8 136.3(4) . .
O34 W10 K9 36.6(4) . 1_556
O34 W10 K18 45.6(6) . 4_666
O34 W10 O5 170.6(5) . .
O34 W10 O33 95.3(5) . .
O34 W10 O35 101.3(5) . .
O34 W10 O36 92.8(5) . .
O34 W10 O37 98.2(5) . .
O35 W10 K4 96.4(4) . .
O35 W10 K8 61.2(4) . .
O35 W10 K9 83.0(4) . 1_556
O35 W10 K18 145.8(6) . 4_666
O35 W10 O5 88.0(5) . .
O35 W10 O33 105.8(4) . .
O35 W10 O36 161.5(5) . .
O35 W10 O37 91.0(5) . .
O36 W10 K4 101.9(3) . .
O36 W10 K8 100.3(4) . .
O36 W10 K9 102.1(4) . 1_556
O36 W10 K18 51.2(5) . 4_666
O37 W10 K4 144.1(4) . .
O37 W10 K8 47.3(4) . .
O37 W10 K9 67.1(4) . 1_556
O37 W10 K18 101.2(5) . 4_666
O37 W10 O5 82.4(4) . .
O37 W10 O36 75.1(4) . .
Eu1 W11 K3 175.72(14) . .
Eu1 W11 K19 75.1(5) . .
K3 W11 K19 103.2(5) . .
O41 W11 Eu1 93.0(4) . .
O41 W11 K3 82.7(4) . .
O41 W11 K19 66.3(6) . .
O41 W11 O42 101.6(5) . .
O41 W11 O43 98.9(5) . .
O41 W11 O44 96.9(5) . .
O41 W11 O45 102.5(5) . .
O41 W11 O46 167.0(5) . .
O42 W11 Eu1 40.1(3) . .
O42 W11 K3 140.6(3) . .
O42 W11 K19 114.4(6) . .
O42 W11 O43 84.3(4) . .
O42 W11 O44 160.2(4) . .
O42 W11 O45 92.7(4) . .
O42 W11 O46 87.6(4) . .
O43 W11 Eu1 46.5(3) . .
O43 W11 K3 134.2(3) . .
O43 W11 K19 41.2(6) . .
O43 W11 O46 72.7(4) . .
O44 W11 Eu1 132.4(3) . .
O44 W11 K3 48.7(4) . .
O44 W11 K19 67.0(6) . .
O44 W11 O43 86.0(4) . .
O44 W11 O46 73.1(4) . .
O45 W11 Eu1 132.6(3) . .
O45 W11 K3 48.8(3) . .
O45 W11 K19 151.9(6) . .
O45 W11 O43 158.6(4) . .
O45 W11 O44 90.2(5) . .
O45 W11 O46 86.0(4) . .
O46 W11 Eu1 88.2(3) . .
O46 W11 K3 96.0(3) . .
O46 W11 K19 101.7(5) . .
Eu1 W12 K17 172.9(5) . .
Eu1 W12 K18 107.0(4) . .
Eu1 W12 K19 75.5(5) . .
K17 W12 K18 67.6(6) . .
K17 W12 K19 102.1(7) . .
K19 W12 K18 112.7(6) . .
O43 W12 Eu1 46.7(3) . .
O43 W12 K17 135.0(6) . .
O43 W12 K18 140.6(5) . .
O43 W12 K19 41.9(6) . .
O43 W12 O46 73.3(4) . .
O46 W12 Eu1 88.8(2) . .
O46 W12 K17 98.3(5) . .
O46 W12 K18 143.5(5) . .
O46 W12 K19 102.9(6) . .
O47 W12 Eu1 93.7(4) . .
O47 W12 K17 79.2(6) . .
O47 W12 K18 46.1(6) . .
O47 W12 K19 66.7(6) . .
O47 W12 O43 100.1(5) . .
O47 W12 O46 168.2(5) . .
O47 W12 O48 102.7(5) . .
O47 W12 O49 96.4(5) . .
O47 W12 O50 101.5(5) . .
O48 W12 Eu1 39.8(3) . .
O48 W12 K17 140.8(6) . .
O48 W12 K18 85.6(5) . .
O48 W12 K19 114.7(6) . .
O48 W12 O43 83.8(4) . .
O48 W12 O46 86.5(4) . .
O48 W12 O49 159.6(5) . .
O48 W12 O50 93.0(5) . .
O49 W12 Eu1 132.7(3) . .
O49 W12 K17 49.9(6) . .
O49 W12 K18 113.1(5) . .
O49 W12 K19 66.7(6) . .
O49 W12 O43 86.1(5) . .
O49 W12 O46 73.7(4) . .
O50 W12 Eu1 132.7(3) . .
O50 W12 K17 49.3(6) . .
O50 W12 K18 59.9(5) . .
O50 W12 K19 151.4(6) . .
O50 W12 O43 158.3(4) . .
O50 W12 O46 85.1(4) . .
O50 W12 O49 90.0(5) . .
K3 W13 K17 166.9(5) . .
K3 W13 K20 53.2(6) . 2_546
K20 W13 K17 117.8(7) 2_546 .
O44 W13 K3 48.3(4) . .
O44 W13 K17 133.0(6) . .
O44 W13 K20 39.6(7) . 2_546
O44 W13 O46 73.6(4) . .
O46 W13 K3 95.8(3) . .
O46 W13 K17 96.9(5) . .
O46 W13 K20 112.2(6) . 2_546
O49 W13 K3 132.9(4) . .
O49 W13 K17 48.6(6) . .
O49 W13 K20 87.9(7) . 2_546
O49 W13 O44 85.2(5) . .
O49 W13 O46 73.5(4) . .
O51 W13 K3 84.6(5) . .
O51 W13 K17 82.3(7) . .
O51 W13 K20 60.3(7) . 2_546
O51 W13 O44 99.6(6) . .
O51 W13 O46 170.0(6) . .
O51 W13 O49 98.9(6) . .
O51 W13 O52 101.5(6) . .
O51 W13 O53 102.0(6) . .
O52 W13 K3 135.7(4) . .
O52 W13 K17 49.5(6) . .
O52 W13 K20 161.0(7) . 2_546
O52 W13 O44 158.8(5) . .
O52 W13 O46 85.2(4) . .
O52 W13 O49 90.0(5) . .
O52 W13 O53 88.6(5) . .
O53 W13 K3 47.6(4) . .
O53 W13 K17 137.4(6) . .
O53 W13 K20 100.0(7) . 2_546
O53 W13 O44 88.6(5) . .
O53 W13 O46 85.3(4) . .
O53 W13 O49 158.8(5) . .
K7 W14 K17 158.7(5) . .
O50 W14 K7 146.1(4) . .
O50 W14 K17 45.4(5) . .
O50 W14 O55 83.3(5) . .
O50 W14 O58 85.5(4) . .
O54 W14 K7 79.1(5) . .
O54 W14 K17 80.8(6) . .
O54 W14 O50 99.8(6) . .
O54 W14 O55 97.4(6) . .
O54 W14 O56 104.7(6) . .
O54 W14 O57 99.2(6) . .
O54 W14 O58 168.8(5) . .
O55 W14 K7 130.6(4) . .
O55 W14 K17 46.0(6) . .
O55 W14 O58 73.3(4) . .
O56 W14 K7 59.0(4) . .
O56 W14 K17 134.1(6) . .
O56 W14 O50 89.3(5) . .
O56 W14 O55 157.6(5) . .
O56 W14 O57 94.3(5) . .
O56 W14 O58 85.2(4) . .
O57 W14 K7 47.5(4) . .
O57 W14 K17 130.5(6) . .
O57 W14 O50 159.1(5) . .
O57 W14 O55 85.6(5) . .
O57 W14 O58 74.4(4) . .
O58 W14 K7 102.1(3) . .
O58 W14 K17 96.3(5) . .
O52 W15 K17 47.2(6) . .
O52 W15 O58 85.4(4) . .
O55 W15 K17 45.7(6) . .
O55 W15 O52 85.4(5) . .
O55 W15 O58 74.8(4) . .
O55 W15 O61 157.4(5) . .
O58 W15 K17 96.7(5) . .
O59 W15 K17 82.5(7) . .
O59 W15 O52 98.7(6) . .
O59 W15 O55 100.1(6) . .
O59 W15 O58 173.3(5) . .
O59 W15 O60 102.6(6) . .
O59 W15 O61 100.5(6) . .
O60 W15 K17 138.2(6) . .
O60 W15 O52 158.6(5) . .
O60 W15 O55 93.1(5) . .
O60 W15 O58 73.6(4) . .
O60 W15 O61 91.5(5) . .
O61 W15 K17 128.9(6) . .
O61 W15 O52 82.3(6) . .
O61 W15 O58 85.3(4) . .
K7 W16 K6 130.8(3) . 4_566
O57 W16 K6 149.1(4) . 4_566
O57 W16 K7 46.7(4) . .
O57 W16 O58 74.2(4) . .
O57 W16 O60 81.3(5) . .
O58 W16 K6 126.3(3) . 4_566
O58 W16 K7 101.5(3) . .
O60 W16 K6 84.4(4) . 4_566
O60 W16 K7 125.9(4) . .
O60 W16 O58 71.3(4) . .
O62 W16 K6 54.4(5) . 4_566
O62 W16 K7 82.9(5) . .
O62 W16 O57 99.4(5) . .
O62 W16 O58 164.6(5) . .
O62 W16 O60 94.1(6) . .
O62 W16 O63 104.9(6) . .
O62 W16 O64 98.8(5) . .
O63 W16 K6 109.5(4) . 4_566
O63 W16 K7 54.8(4) . .
O63 W16 O57 91.8(5) . .
O63 W16 O58 89.5(5) . .
O63 W16 O60 160.7(5) . .
O63 W16 O64 95.9(5) . .
O64 W16 K6 44.7(3) . 4_566
O64 W16 K7 149.5(4) . .
O64 W16 O57 157.6(5) . .
O64 W16 O58 84.9(4) . .
O64 W16 O60 84.5(5) . .
O53 W17 K3 46.2(4) . .
O53 W17 O68 85.6(4) . .
O61 W17 K3 128.1(4) . .
O61 W17 O53 82.4(5) . .
O61 W17 O68 85.8(4) . .
O65 W17 K3 85.3(5) . .
O65 W17 O53 101.1(7) . .
O65 W17 O61 100.5(6) . .
O65 W17 O66 100.1(7) . .
O65 W17 O67 100.9(6) . .
O65 W17 O68 171.3(6) . .
O66 W17 K3 139.5(4) . .
O66 W17 O53 158.6(5) . .
O66 W17 O61 90.7(6) . .
O66 W17 O67 93.3(5) . .
O66 W17 O68 73.7(4) . .
O67 W17 K3 46.6(4) . .
O67 W17 O53 85.7(5) . .
O67 W17 O61 157.2(5) . .
O67 W17 O68 73.8(4) . .
O68 W17 K3 95.5(3) . .
K6 W18 K16 127.0(5) 4_566 1_556
O64 W18 K6 50.2(4) . 4_566
O64 W18 K16 153.6(6) . 1_556
O64 W18 O66 83.4(5) . .
O64 W18 O68 85.2(4) . .
O64 W18 O71 157.6(5) . .
O66 W18 K6 82.8(4) . 4_566
O66 W18 K16 123.0(5) . 1_556
O66 W18 O68 71.6(4) . .
O68 W18 K6 131.0(3) . 4_566
O68 W18 K16 101.9(5) . 1_556
O69 W18 K6 49.7(5) . 4_566
O69 W18 K16 80.3(6) . 1_556
O69 W18 O64 99.3(5) . .
O69 W18 O66 94.8(6) . .
O69 W18 O68 165.2(6) . .
O69 W18 O70 104.7(6) . .
O69 W18 O71 98.6(5) . .
O70 W18 K6 112.1(4) . 4_566
O70 W18 K16 59.1(6) . 1_556
O70 W18 O64 96.1(5) . .
O70 W18 O66 160.3(5) . .
O70 W18 O68 88.7(5) . .
O70 W18 O71 92.2(5) . .
O71 W18 K6 143.1(4) . 4_566
O71 W18 K16 44.0(6) . 1_556
O71 W18 O66 81.8(5) . .
O71 W18 O68 74.2(4) . .
K5 W19 K3 38.6(2) . .
K10 W19 K3 106.5(3) 1_556 .
K10 W19 K5 77.4(3) 1_556 .
K16 W19 K3 156.7(5) 1_556 .
K16 W19 K5 118.5(5) 1_556 .
K16 W19 K10 53.8(5) 1_556 1_556
O45 W19 K3 44.2(3) . .
O45 W19 K5 70.7(3) . .
O45 W19 K10 148.0(4) . 1_556
O45 W19 K16 148.4(5) . 1_556
O45 W19 O67 82.4(5) . .
O45 W19 O68 84.9(4) . .
O67 W19 K3 44.9(4) . .
O67 W19 K5 60.6(4) . .
O67 W19 K10 79.6(4) . 1_556
O67 W19 K16 129.0(6) . 1_556
O67 W19 O68 72.8(4) . .
O68 W19 K3 93.7(3) . .
O68 W19 K5 129.3(3) . .
O68 W19 K10 114.3(3) . 1_556
O68 W19 K16 105.7(5) . 1_556
O71 W19 K3 129.7(4) . .
O71 W19 K5 117.9(4) . .
O71 W19 K10 44.4(4) . 1_556
O71 W19 K16 47.8(6) . 1_556
O71 W19 O45 158.5(5) . .
O71 W19 O67 85.5(5) . .
O71 W19 O68 74.5(4) . .
O72 W19 K3 83.4(5) . .
O72 W19 K5 45.3(5) . .
O72 W19 K10 55.7(4) . 1_556
O72 W19 K16 74.9(6) . 1_556
O72 W19 O45 101.0(5) . .
O72 W19 O67 97.0(5) . .
O72 W19 O68 167.5(5) . .
O72 W19 O71 98.0(5) . .
O72 W19 O73 103.9(6) . .
O73 W19 K3 133.9(4) . .
O73 W19 K5 135.0(4) . .
O73 W19 K10 115.1(4) . 1_556
O73 W19 K16 61.5(6) . 1_556
O73 W19 O45 90.2(5) . .
O73 W19 O67 158.9(5) . .
O73 W19 O68 86.9(5) . .
O73 W19 O71 94.9(5) . .
W11 Eu1 Eu3 105.53(3) . .
W12 Eu1 W11 59.04(4) . .
W12 Eu1 Eu3 69.22(2) . .
O15 Eu1 W11 141.8(3) . .
O15 Eu1 W12 146.4(3) . .
O15 Eu1 Eu3 111.0(3) . .
O15 Eu1 O23 71.4(4) . .
O15 Eu1 O42 134.5(4) . .
O15 Eu1 O43 140.7(4) . .
O15 Eu1 O48 140.4(4) . .
O15 Eu1 O74 103.0(4) . .
O15 Eu1 O1W 74.0(4) . .
O15 Eu1 O2W 77.2(4) . .
O15 Eu1 O3W 68.9(4) . .
O23 Eu1 W11 146.7(2) . .
O23 Eu1 W12 91.7(2) . .
O23 Eu1 Eu3 44.3(2) . .
O42 Eu1 W11 29.7(2) . .
O42 Eu1 W12 77.5(2) . .
O42 Eu1 Eu3 93.7(2) . .
O42 Eu1 O23 137.0(3) . .
O42 Eu1 O43 62.2(3) . .
O42 Eu1 O74 71.1(3) . .
O42 Eu1 O1W 84.3(4) . .
O42 Eu1 O2W 135.5(4) . .
O42 Eu1 O3W 66.9(3) . .
O43 Eu1 W11 34.1(2) . .
O43 Eu1 W12 34.1(2) . .
O43 Eu1 Eu3 101.0(2) . .
O43 Eu1 O23 124.2(3) . .
O43 Eu1 O3W 121.4(3) . .
O48 Eu1 W11 76.9(2) . .
O48 Eu1 W12 29.9(3) . .
O48 Eu1 Eu3 39.4(3) . .
O48 Eu1 O23 70.0(3) . .
O48 Eu1 O42 81.9(3) . .
O48 Eu1 O43 62.2(3) . .
O48 Eu1 O74 70.8(4) . .
O48 Eu1 O1W 134.9(4) . .
O48 Eu1 O2W 84.6(4) . .
O48 Eu1 O3W 135.6(3) . .
O74 Eu1 W11 97.2(2) . .
O74 Eu1 W12 97.4(3) . .
O74 Eu1 Eu3 40.9(2) . .
O74 Eu1 O23 69.2(3) . .
O74 Eu1 O43 116.2(3) . .
O74 Eu1 O1W 142.0(4) . .
O74 Eu1 O2W 141.4(4) . .
O74 Eu1 O3W 69.5(3) . .
O1W Eu1 W11 70.2(3) . .
O1W Eu1 W12 105.1(3) . .
O1W Eu1 Eu3 174.3(3) . .
O1W Eu1 O23 138.4(4) . .
O1W Eu1 O43 73.4(4) . .
O1W Eu1 O2W 75.9(4) . .
O1W Eu1 O3W 74.4(4) . .
O2W Eu1 W11 105.9(3) . .
O2W Eu1 W12 70.2(3) . .
O2W Eu1 Eu3 102.1(3) . .
O2W Eu1 O23 74.7(4) . .
O2W Eu1 O43 74.0(4) . .
O2W Eu1 O3W 139.8(4) . .
O3W Eu1 W11 88.9(2) . .
O3W Eu1 W12 144.3(2) . .
O3W Eu1 Eu3 109.7(2) . .
O3W Eu1 O23 112.5(3) . .
Eu1 Eu2 K8 102.94(18) . .
Eu1 Eu2 K8 150.04(17) . 3_657
Eu1 Eu2 K9 148.63(18) . 1_556
K8 Eu2 K8 73.0(3) . 3_657
K8 Eu2 K9 88.0(2) . 1_556
K8 Eu2 K9 61.2(2) 3_657 1_556
O35 Eu2 Eu1 94.7(3) . .
O35 Eu2 K8 52.9(3) . .
O35 Eu2 K8 105.0(3) . 3_657
O35 Eu2 K9 68.4(3) . 1_556
O35 Eu2 O39 119.1(4) . 3_657
O35 Eu2 O42 134.4(4) . .
O35 Eu2 O74 69.5(4) . .
O35 Eu2 O3W 77.4(4) . .
O35 Eu2 O4W 71.7(4) . .
O35 Eu2 O5W 75.3(4) . .
O39 Eu2 Eu1 99.8(3) 3_657 .
O39 Eu2 K8 50.9(3) 3_657 3_657
O39 Eu2 K8 66.2(3) 3_657 .
O39 Eu2 K9 111.5(3) 3_657 1_556
O39 Eu2 O74 139.4(4) 3_657 .
O39 Eu2 O3W 73.7(4) 3_657 .
O39 Eu2 O4W 73.1(4) 3_657 .
O39 Eu2 O5W 139.4(4) 3_657 .
O42 Eu2 Eu1 39.8(2) . .
O42 Eu2 K8 117.9(3) . 3_657
O42 Eu2 K8 125.1(3) . .
O42 Eu2 K9 146.3(3) . 1_556
O42 Eu2 O39 80.8(4) . 3_657
O42 Eu2 O74 70.2(4) . .
O42 Eu2 O3W 69.5(3) . .
O42 Eu2 O4W 150.9(4) . .
O42 Eu2 O5W 117.6(4) . .
O73 Eu2 Eu1 114.2(3) . .
O73 Eu2 K8 59.9(3) . 3_657
O73 Eu2 K8 132.6(3) . .
O73 Eu2 K9 75.6(3) . 1_556
O73 Eu2 O35 143.6(4) . .
O73 Eu2 O39 78.8(4) . 3_657
O73 Eu2 O42 76.4(4) . .
O73 Eu2 O74 119.0(4) . .
O73 Eu2 O3W 138.8(4) . .
O73 Eu2 O4W 85.9(4) . .
O73 Eu2 O5W 72.0(4) . .
O74 Eu2 Eu1 40.3(3) . .
O74 Eu2 K8 108.4(3) . .
O74 Eu2 K8 169.6(3) . 3_657
O74 Eu2 K9 108.4(3) . 1_556
O3W Eu2 Eu1 44.2(2) . .
O3W Eu2 K8 118.2(3) . 3_657
O3W Eu2 K8 60.0(3) . .
O3W Eu2 K9 143.3(3) . 1_556
O3W Eu2 O74 70.0(3) . .
O3W Eu2 O4W 113.9(4) . .
O4W Eu2 Eu1 157.5(3) . .
O4W Eu2 K8 33.6(3) . 3_657
O4W Eu2 K8 54.6(3) . .
O4W Eu2 K9 42.9(3) . 1_556
O4W Eu2 O74 138.9(4) . .
O5W Eu2 Eu1 117.5(3) . .
O5W Eu2 K8 89.6(3) . 3_657
O5W Eu2 K8 116.0(3) . .
O5W Eu2 K9 34.3(3) . 1_556
O5W Eu2 O74 80.5(4) . .
O5W Eu2 O3W 145.2(4) . .
O5W Eu2 O4W 77.2(4) . .
W8 Eu3 K4 56.79(14) . .
W8 Eu3 K7 95.74(17) . .
Eu1 Eu3 W8 107.03(3) . .
Eu1 Eu3 K4 122.66(14) . .
Eu1 Eu3 K7 156.94(17) . .
K4 Eu3 K7 67.3(2) . .
O23 Eu3 W8 69.0(2) . .
O23 Eu3 Eu1 45.6(2) . .
O23 Eu3 K4 115.9(3) . .
O23 Eu3 K7 153.8(3) . .
O30 Eu3 W8 18.4(2) . .
O30 Eu3 Eu1 100.0(3) . .
O30 Eu3 K4 46.0(3) . .
O30 Eu3 K7 100.6(3) . .
O30 Eu3 O23 71.9(4) . .
O30 Eu3 O74 80.0(4) . .
O30 Eu3 O6W 72.9(4) . .
O30 Eu3 O7W 84.0(4) . .
O30 Eu3 O8W 102.2(4) . .
O48 Eu3 W8 140.6(3) . .
O48 Eu3 Eu1 40.3(3) . .
O48 Eu3 K4 149.7(3) . .
O48 Eu3 K7 119.9(3) . .
O48 Eu3 O23 71.7(4) . .
O48 Eu3 O30 139.5(4) . .
O48 Eu3 O74 71.6(4) . .
O48 Eu3 O6W 144.8(4) . .
O48 Eu3 O7W 116.1(4) . .
O48 Eu3 O8W 84.7(4) . .
O56 Eu3 W8 138.2(3) . .
O56 Eu3 Eu1 113.9(3) . .
O56 Eu3 K4 104.5(3) . .
O56 Eu3 K7 44.5(3) . .
O56 Eu3 O23 139.5(4) . .
O56 Eu3 O30 145.0(4) . .
O56 Eu3 O48 75.5(4) . .
O56 Eu3 O74 120.2(4) . .
O56 Eu3 O6W 74.5(4) . .
O56 Eu3 O7W 74.3(4) . .
O56 Eu3 O8W 79.3(4) . .
O74 Eu3 W8 96.1(3) . .
O74 Eu3 Eu1 41.0(3) . .
O74 Eu3 K4 83.3(3) . .
O74 Eu3 K7 134.4(3) . .
O74 Eu3 O23 70.3(3) . .
O74 Eu3 O6W 141.0(4) . .
O74 Eu3 O7W 77.4(4) . .
O74 Eu3 O8W 142.4(4) . .
O6W Eu3 W8 64.0(3) . .
O6W Eu3 Eu1 169.7(3) . .
O6W Eu3 K4 57.7(3) . .
O6W Eu3 K7 33.0(3) . .
O6W Eu3 O23 124.2(4) . .
O7W Eu3 W8 96.3(3) . .
O7W Eu3 Eu1 114.8(3) . .
O7W Eu3 K4 39.5(3) . .
O7W Eu3 K7 57.6(3) . .
O7W Eu3 O23 142.3(4) . .
O7W Eu3 O6W 72.4(4) . .
O8W Eu3 W8 84.0(3) . .
O8W Eu3 Eu1 103.0(3) . .
O8W Eu3 K4 125.4(4) . .
O8W Eu3 K7 82.6(4) . .
O8W Eu3 O23 74.8(4) . .
O8W Eu3 O6W 72.1(4) . .
O8W Eu3 O7W 140.1(4) . .
O18 As1 O6 99.0(5) . .
O28 As1 O6 97.2(5) . .
O28 As1 O18 96.4(5) . .
O46 As2 O58 97.9(5) . .
O46 As2 O68 98.7(5) . .
O68 As2 O58 97.6(5) . .
W9 K1 K5 129.1(2) . 3_657
K13 K1 W9 159.3(5) . .
K13 K1 K5 53.8(5) . 3_657
K13 K1 K21 87.8(8) . .
K13 K1 O1 88.0(5) . .
K13 K1 O4 133.9(5) . .
K13 K1 O32 160.9(5) . .
K13 K1 O36 131.3(5) . .
K13 K1 O38 89.3(5) . .
K13 K1 C1 109.1(6) . .
K13 K1 O21W 69.2(9) . 4_666
K21 K1 W9 71.9(7) . .
K21 K1 K5 110.8(7) . 3_657
K21 K1 C1 136.6(8) . .
O1 K1 W9 84.1(2) . .
O1 K1 K5 49.2(3) . 3_657
O1 K1 K21 79.5(8) . .
O1 K1 C1 62.2(4) . .
O4 K1 W9 30.3(2) . .
O4 K1 K5 104.2(3) . 3_657
O4 K1 K21 60.7(7) . .
O4 K1 O1 55.7(3) . .
O4 K1 O36 64.5(3) . .
O4 K1 C1 80.2(4) . .
O4 K1 O21W 108.5(8) . 4_666
O22 K1 W9 106.1(3) 4_666 .
O22 K1 K5 111.8(3) 4_666 3_657
O22 K1 K13 88.5(5) 4_666 .
O22 K1 K21 123.3(8) 4_666 .
O22 K1 O1 156.7(4) 4_666 .
O22 K1 O4 136.3(4) 4_666 .
O22 K1 O32 79.5(4) 4_666 .
O22 K1 O36 98.0(4) 4_666 .
O22 K1 O38 87.0(4) 4_666 .
O22 K1 C1 97.5(4) 4_666 .
O22 K1 O21W 72.4(8) 4_666 4_666
O32 K1 W9 26.6(2) . .
O32 K1 K5 144.9(3) . 3_657
O32 K1 K21 86.4(8) . .
O32 K1 O1 108.9(4) . .
O32 K1 O4 56.8(3) . .
O32 K1 O36 65.8(3) . .
O32 K1 O38 104.7(4) . .
O32 K1 C1 87.4(4) . .
O32 K1 O21W 92.8(8) . 4_666
O36 K1 W9 62.3(2) . .
O36 K1 K5 79.5(3) . 3_657
O36 K1 K21 125.1(8) . .
O36 K1 O1 67.7(3) . .
O36 K1 C1 22.3(3) . .
O36 K1 O21W 158.2(8) . 4_666
O38 K1 W9 105.8(3) . .
O38 K1 K5 46.1(3) . 3_657
O38 K1 K21 149.4(8) . .
O38 K1 O1 70.0(4) . .
O38 K1 O4 101.4(4) . .
O38 K1 O36 43.5(3) . .
O38 K1 C1 22.3(4) . .
O38 K1 O21W 150.1(8) . 4_666
C1 K1 W9 84.0(3) . .
C1 K1 K5 58.8(4) . 3_657
O21W K1 W9 100.7(8) 4_666 .
O21W K1 K5 122.1(8) 4_666 3_657
O21W K1 K21 53.7(11) 4_666 .
O21W K1 O1 127.2(8) 4_666 .
O21W K1 C1 169.7(9) 4_666 .
W2 K2 K6 176.2(3) . 3_656
W2 K2 K12 61.0(3) . 1_545
W4 K2 W2 56.11(10) . .
W4 K2 K6 121.0(2) . 3_656
W4 K2 K12 111.4(3) . 1_545
K12 K2 K6 120.2(3) 1_545 3_656
K15 K2 W2 69.3(4) . .
K15 K2 W4 66.7(4) . .
K15 K2 K6 112.3(4) . 3_656
K15 K2 K12 113.3(5) . 1_545
O7 K2 W2 24.8(2) . .
O7 K2 W4 80.9(3) . .
O7 K2 K6 157.6(3) . 3_656
O7 K2 K12 39.1(3) . 1_545
O7 K2 K15 79.3(5) . .
O7 K2 O10 53.7(3) . .
O10 K2 W2 29.1(2) . .
O10 K2 W4 28.6(2) . .
O10 K2 K6 148.6(3) . 3_656
O10 K2 K12 89.3(3) . 1_545
O10 K2 K15 57.9(4) . .
O14 K2 W2 81.1(3) . .
O14 K2 W4 25.2(2) . .
O14 K2 K6 95.9(3) . 3_656
O14 K2 K12 130.7(4) . 1_545
O14 K2 K15 76.5(4) . .
O14 K2 O7 105.6(4) . .
O14 K2 O10 53.7(3) . .
O14 K2 O62 92.1(4) . 2_546
O19 K2 W2 142.3(4) 3_656 .
O19 K2 W4 101.4(3) 3_656 .
O19 K2 K6 38.7(3) 3_656 3_656
O19 K2 K12 146.6(4) 3_656 1_545
O19 K2 K15 74.0(5) 3_656 .
O19 K2 O7 149.5(5) 3_656 .
O19 K2 O10 119.3(4) 3_656 .
O19 K2 O14 82.4(4) 3_656 .
O19 K2 O62 82.5(4) 3_656 2_546
O19 K2 O9W 133.5(6) 3_656 .
O19 K2 O12W 113.0(8) 3_656 .
O62 K2 W2 131.6(3) 2_546 .
O62 K2 W4 110.7(3) 2_546 .
O62 K2 K6 45.9(3) 2_546 3_656
O62 K2 K12 91.2(4) 2_546 1_545
O62 K2 K15 154.9(5) 2_546 .
O62 K2 O7 125.6(4) 2_546 .
O62 K2 O10 131.4(4) 2_546 .
O9W K2 W2 68.1(4) . .
O9W K2 W4 63.8(4) . .
O9W K2 K6 108.6(5) . 3_656
O9W K2 K12 70.1(5) . 1_545
O9W K2 K15 126.9(6) . .
O9W K2 O7 75.2(5) . .
O9W K2 O10 69.4(5) . .
O9W K2 O14 67.0(5) . .
O9W K2 O62 65.2(5) . 2_546
O9W K2 O12W 89.9(8) . .
O12W K2 W2 94.6(7) . .
O12W K2 W4 145.5(7) . .
O12W K2 K6 87.3(7) . 3_656
O12W K2 K12 34.8(7) . 1_545
O12W K2 K15 123.7(8) . .
O12W K2 O7 70.6(7) . .
O12W K2 O10 123.5(7) . .
O12W K2 O14 156.5(8) . .
O12W K2 O62 73.5(7) . 2_546
W11 K3 W13 52.97(13) . .
W11 K3 W17 80.69(18) . .
W11 K3 W19 56.37(13) . .
W11 K3 K13 138.2(3) . 3_657
W13 K3 W17 57.44(13) . .
W13 K3 W19 80.83(18) . .
W13 K3 K13 168.8(4) . 3_657
W17 K3 W19 51.22(12) . .
W17 K3 K13 118.4(3) . 3_657
W19 K3 K13 104.8(3) . 3_657
K5 K3 W11 106.1(4) . .
K5 K3 W13 149.9(4) . .
K5 K3 W17 101.7(4) . .
K5 K3 W19 69.1(3) . .
K5 K3 K13 37.2(4) . 3_657
K5 K3 K20 132.7(8) . 2_546
K5 K3 O29 68.0(4) . 2_546
K5 K3 O44 136.3(5) . .
K5 K3 O45 84.9(4) . .
K5 K3 O53 128.9(5) . .
K5 K3 O67 75.8(4) . .
K20 K3 W11 69.6(7) 2_546 .
K20 K3 W13 65.6(7) 2_546 .
K20 K3 W17 122.8(7) 2_546 .
K20 K3 W19 126.0(7) 2_546 .
K20 K3 K13 116.3(7) 2_546 3_657
O29 K3 W11 100.7(4) 2_546 .
O29 K3 W13 131.4(4) 2_546 .
O29 K3 W17 169.6(4) 2_546 .
O29 K3 W19 121.1(4) 2_546 .
O29 K3 K13 54.1(4) 2_546 3_657
O29 K3 K20 66.9(7) 2_546 2_546
O29 K3 O44 106.6(5) 2_546 .
O29 K3 O45 111.3(4) 2_546 .
O29 K3 O53 160.1(5) 2_546 .
O29 K3 O67 142.0(5) 2_546 .
O44 K3 W11 30.3(2) . .
O44 K3 W13 29.6(2) . .
O44 K3 W17 79.9(3) . .
O44 K3 W19 79.6(3) . .
O44 K3 K13 159.9(4) . 3_657
O44 K3 K20 50.3(7) . 2_546
O44 K3 O45 55.7(3) . .
O44 K3 O67 91.6(4) . .
O45 K3 W11 29.2(2) . .
O45 K3 W13 67.1(3) . .
O45 K3 W17 65.2(3) . .
O45 K3 W19 27.5(2) . .
O45 K3 K13 121.9(4) . 3_657
O45 K3 K20 98.7(7) . 2_546
O53 K3 W11 66.4(3) . .
O53 K3 W13 28.7(3) . .
O53 K3 W17 29.0(3) . .
O53 K3 W19 65.8(3) . .
O53 K3 K13 145.3(5) . 3_657
O53 K3 K20 93.8(7) . 2_546
O53 K3 O44 54.5(4) . .
O53 K3 O45 65.3(4) . .
O53 K3 O67 53.2(4) . .
O67 K3 W11 78.4(3) . .
O67 K3 W13 78.5(3) . .
O67 K3 W17 27.9(2) . .
O67 K3 W19 29.1(2) . .
O67 K3 K13 101.6(4) . 3_657
O67 K3 K20 141.6(8) . 2_546
O67 K3 O45 52.9(3) . .
W8 K4 W9 50.47(13) . .
W8 K4 W10 87.1(2) . .
W10 K4 W9 54.88(13) . .
K18 K4 W8 119.7(5) 4_666 .
K18 K4 W9 70.2(5) 4_666 .
K18 K4 W10 64.1(5) 4_666 .
K20 K4 W8 75.1(8) . .
K20 K4 W9 78.5(9) . .
K20 K4 W10 129.7(9) . .
K20 K4 K18 84.6(10) . 4_666
K20 K4 O30 100.7(9) . .
K20 K4 O31 62.6(9) . .
K20 K4 O33 106.4(9) . .
K20 K4 O34 136.2(9) . .
K20 K4 O7W 135.8(9) . .
K20 K4 O10W 84.4(10) . .
K20 K4 O24W 95.7(12) . 4_666
O30 K4 W8 26.9(2) . .
O30 K4 W9 63.9(3) . .
O30 K4 W10 76.9(3) . .
O30 K4 K18 131.5(6) . 4_666
O30 K4 O33 61.8(3) . .
O31 K4 W8 29.6(2) . .
O31 K4 W9 26.7(2) . .
O31 K4 W10 78.7(3) . .
O31 K4 K18 90.8(6) . 4_666
O31 K4 O30 52.6(3) . .
O31 K4 O33 50.6(3) . .
O31 K4 O34 101.1(4) . .
O31 K4 O10W 138.9(7) . .
O33 K4 W8 62.7(3) . .
O33 K4 W9 28.09(19) . .
O33 K4 W10 28.1(2) . .
O33 K4 K18 70.4(5) . 4_666
O34 K4 W8 111.7(4) . .
O34 K4 W9 75.2(3) . .
O34 K4 W10 24.6(2) . .
O34 K4 K18 53.7(5) . 4_666
O34 K4 O30 98.5(4) . .
O34 K4 O33 51.5(3) . .
O34 K4 O10W 120.0(7) . .
O7W K4 W8 90.2(3) . .
O7W K4 W9 123.1(4) . .
O7W K4 W10 89.7(3) . .
O7W K4 K18 137.0(6) . 4_666
O7W K4 O30 65.6(4) . .
O7W K4 O31 118.2(5) . .
O7W K4 O33 102.8(4) . .
O7W K4 O34 88.0(4) . .
O7W K4 O10W 68.7(6) . .
O7W K4 O24W 113.2(10) . 4_666
O10W K4 W8 122.3(6) . .
O10W K4 W9 162.7(7) . .
O10W K4 W10 141.9(7) . .
O10W K4 K18 110.9(8) . 4_666
O10W K4 O30 117.6(7) . .
O10W K4 O33 169.2(7) . .
O24W K4 W8 152.3(9) 4_666 .
O24W K4 W9 102.5(9) 4_666 .
O24W K4 W10 78.8(9) 4_666 .
O24W K4 K18 32.6(10) 4_666 4_666
O24W K4 O30 155.7(10) 4_666 .
O24W K4 O31 123.1(10) 4_666 .
O24W K4 O33 96.4(9) 4_666 .
O24W K4 O34 57.5(9) 4_666 .
O24W K4 O10W 81.6(11) 4_666 .
W19 K5 K10 50.6(2) . 1_556
K1 K5 W19 135.9(3) 3_657 .
K1 K5 K10 99.9(3) 3_657 1_556
K3 K5 W19 72.3(3) . .
K3 K5 K1 148.7(4) . 3_657
K3 K5 K10 110.9(4) . 1_556
K3 K5 K13 112.6(6) . 3_657
K3 K5 O1 160.1(5) . 3_657
K3 K5 O29 59.4(4) . 2_546
K3 K5 O38 118.4(5) . 3_657
K3 K5 O67 56.3(4) . .
K3 K5 O72 96.5(5) . .
K3 K5 O22W 94.7(9) . .
K13 K5 W19 162.7(5) 3_657 .
K13 K5 K1 45.9(4) 3_657 3_657
K13 K5 K10 113.9(5) 3_657 1_556
K13 K5 O67 137.1(6) 3_657 .
O1 K5 W19 89.0(3) 3_657 .
O1 K5 K1 51.2(3) 3_657 3_657
O1 K5 K10 49.8(3) 3_657 1_556
O1 K5 K13 83.4(5) 3_657 3_657
O1 K5 O29 138.8(5) 3_657 2_546
O1 K5 O67 104.0(5) 3_657 .
O29 K5 W19 117.4(4) 2_546 .
O29 K5 K1 90.7(4) 2_546 3_657
O29 K5 K10 167.9(5) 2_546 1_556
O29 K5 K13 77.7(5) 2_546 3_657
O29 K5 O67 114.8(5) 2_546 .
O38 K5 W19 107.5(4) 3_657 .
O38 K5 K1 49.0(3) 3_657 3_657
O38 K5 K10 113.8(4) 3_657 1_556
O38 K5 K13 85.1(5) 3_657 3_657
O38 K5 O1 73.0(4) 3_657 3_657
O38 K5 O29 69.1(4) 3_657 2_546
O38 K5 O67 137.7(5) 3_657 .
O38 K5 O72 91.9(5) 3_657 .
O38 K5 O22W 145.6(10) 3_657 .
O67 K5 W19 31.1(2) . .
O67 K5 K1 154.5(4) . 3_657
O67 K5 K10 54.6(3) . 1_556
O72 K5 W19 24.7(3) . .
O72 K5 K1 111.2(4) . 3_657
O72 K5 K10 39.8(3) . 1_556
O72 K5 K13 148.4(6) . 3_657
O72 K5 O1 65.7(4) . 3_657
O72 K5 O29 130.3(5) . 2_546
O72 K5 O67 52.0(4) . .
O22W K5 W19 72.3(9) . .
O22W K5 K1 106.3(9) . 3_657
O22W K5 K10 38.8(9) . 1_556
O22W K5 K13 90.6(10) . 3_657
O22W K5 O1 72.6(9) . 3_657
O22W K5 O29 142.9(9) . 2_546
O22W K5 O67 53.9(9) . .
O22W K5 O72 74.4(9) . .
W5 K6 W7 58.66(17) . .
W5 K6 W16 129.9(3) . 4_665
W5 K6 K11 93.0(3) . .
W5 K6 K13 67.3(3) . 4_565
W7 K6 W16 171.4(3) . 4_665
W7 K6 K11 59.0(3) . .
W7 K6 K13 62.9(3) . 4_565
W16 K6 K11 116.3(4) 4_665 .
W16 K6 K13 119.1(4) 4_665 4_565
W18 K6 W5 172.4(3) 4_665 .
W18 K6 W7 113.7(3) 4_665 .
W18 K6 W16 57.65(17) 4_665 4_665
W18 K6 K11 81.9(3) 4_665 .
W18 K6 K13 110.3(4) 4_665 4_565
K11 K6 K13 120.3(5) . 4_565
O19 K6 W5 27.0(2) . .
O19 K6 W7 85.4(3) . .
O19 K6 W16 103.1(4) . 4_665
O19 K6 W18 160.5(4) . 4_665
O19 K6 K11 106.6(5) . .
O19 K6 K13 80.9(5) . 4_565
O19 K6 O21 58.7(4) . .
O19 K6 O25 111.4(5) . .
O19 K6 O62 78.1(4) . 4_665
O19 K6 O69 164.7(6) . 4_665
O21 K6 W5 31.8(2) . .
O21 K6 W7 28.3(2) . .
O21 K6 W16 160.1(4) . 4_665
O21 K6 W18 140.8(4) . 4_665
O21 K6 K11 79.1(4) . .
O21 K6 K13 54.2(4) . 4_565
O21 K6 O25 54.6(4) . .
O21 K6 O62 136.7(5) . 4_665
O25 K6 W5 84.9(3) . .
O25 K6 W7 26.4(2) . .
O25 K6 W16 145.0(4) . 4_665
O25 K6 W18 87.5(3) . 4_665
O25 K6 K11 48.1(4) . .
O25 K6 K13 73.5(4) . 4_565
O25 K6 O62 163.3(5) . 4_665
O62 K6 W5 105.0(4) 4_665 .
O62 K6 W7 161.0(4) 4_665 .
O62 K6 W16 26.4(2) 4_665 4_665
O62 K6 W18 82.5(3) 4_665 4_665
O62 K6 K11 116.8(5) 4_665 .
O62 K6 K13 122.6(5) 4_665 4_565
O64 K6 W5 156.3(4) 4_665 .
O64 K6 W7 143.7(4) 4_665 .
O64 K6 W16 28.0(2) 4_665 4_665
O64 K6 W18 31.2(3) 4_665 4_665
O64 K6 K11 106.5(5) 4_665 .
O64 K6 K13 111.7(5) 4_665 4_565
O64 K6 O19 130.5(5) 4_665 .
O64 K6 O21 164.3(5) 4_665 .
O64 K6 O25 118.1(5) 4_665 .
O64 K6 O62 54.3(4) 4_665 4_665
O64 K6 O69 58.1(4) 4_665 4_665
O69 K6 W5 145.6(4) 4_665 .
O69 K6 W7 88.5(4) 4_665 .
O69 K6 W16 82.9(4) 4_665 4_665
O69 K6 W18 27.2(3) 4_665 4_665
O69 K6 K11 58.4(4) 4_665 .
O69 K6 K13 108.7(5) 4_665 4_565
O69 K6 O21 116.7(5) 4_665 .
O69 K6 O25 62.1(4) 4_665 .
O69 K6 O62 105.1(5) 4_665 4_665
W14 K7 W16 51.81(17) . .
O40 K7 W14 102.7(5) 4_565 .
O40 K7 W16 121.0(5) 4_565 .
O40 K7 O41 69.0(5) 4_565 2_556
O40 K7 O56 123.2(5) 4_565 .
O40 K7 O57 99.7(5) 4_565 .
O40 K7 O63 147.5(6) 4_565 .
O40 K7 C3 42.5(4) 4_565 4_565
O40 K7 C4 19.2(4) 4_565 4_565
O40 K7 O1W 63.7(4) 4_565 2_556
O40 K7 O10W 131.5(8) 4_565 .
O41 K7 W14 149.7(5) 2_556 .
O41 K7 W16 157.6(5) 2_556 .
O41 K7 O56 133.3(5) 2_556 .
O41 K7 O63 138.4(5) 2_556 .
O41 K7 C3 66.3(5) 2_556 4_565
O41 K7 C4 60.8(4) 2_556 4_565
O41 K7 O1W 54.7(4) 2_556 2_556
O56 K7 W14 27.8(2) . .
O56 K7 W16 60.9(3) . .
O56 K7 C3 92.9(5) . 4_565
O56 K7 C4 114.4(5) . 4_565
O57 K7 W14 29.5(3) . .
O57 K7 W16 30.1(3) . .
O57 K7 O41 168.7(6) . 2_556
O57 K7 O56 52.0(4) . .
O57 K7 O63 52.3(4) . .
O57 K7 C3 105.3(6) . 4_565
O57 K7 C4 108.4(5) . 4_565
O57 K7 O1W 121.7(5) . 2_556
O57 K7 O10W 117.3(8) . .
O63 K7 W14 62.3(3) . .
O63 K7 W16 26.7(2) . .
O63 K7 O56 56.5(4) . .
O63 K7 C3 148.7(6) . 4_565
O63 K7 C4 160.7(6) . 4_565
C3 K7 W14 87.7(5) 4_565 .
C3 K7 W16 135.4(6) 4_565 .
C3 K7 C4 24.6(4) 4_565 4_565
C4 K7 W14 101.6(4) 4_565 .
C4 K7 W16 135.0(5) 4_565 .
O1W K7 W14 149.2(5) 2_556 .
O1W K7 W16 109.4(4) 2_556 .
O1W K7 O56 169.7(6) 2_556 .
O1W K7 O63 113.4(5) 2_556 .
O1W K7 C3 96.8(5) 2_556 4_565
O1W K7 C4 74.5(4) 2_556 4_565
O6W K7 W14 81.5(4) . .
O6W K7 W16 112.6(5) . .
O6W K7 O40 113.8(6) . 4_565
O6W K7 O41 76.2(5) . 2_556
O6W K7 O56 57.5(4) . .
O6W K7 O57 109.2(6) . .
O6W K7 O63 93.3(5) . .
O6W K7 C3 72.4(5) . 4_565
O6W K7 C4 94.6(5) . 4_565
O6W K7 O1W 128.9(6) . 2_556
O6W K7 O10W 83.7(8) . .
O10W K7 W14 125.1(7) . .
O10W K7 W16 87.6(7) . .
O10W K7 O41 72.6(7) . 2_556
O10W K7 O56 104.6(7) . .
O10W K7 O63 66.3(7) . .
O10W K7 C3 136.1(9) . 4_565
O10W K7 C4 132.2(8) . 4_565
O10W K7 O1W 70.2(7) . 2_556
W1 K8 W2 47.85(15) . .
W1 K8 Eu2 101.9(3) . .
W1 K8 Eu2 135.6(3) . 3_657
W2 K8 Eu2 96.4(3) . .
W2 K8 Eu2 152.8(3) . 3_657
W10 K8 W1 55.69(18) . .
W10 K8 W2 87.7(3) . .
W10 K8 Eu2 57.18(17) . .
W10 K8 Eu2 116.5(3) . 3_657
Eu2 K8 Eu2 107.0(3) . 3_657
K16 K8 W1 104.0(7) 3_656 .
K16 K8 W2 77.9(7) 3_656 .
K16 K8 W10 159.6(8) 3_656 .
K16 K8 Eu2 75.5(7) 3_656 3_657
K16 K8 Eu2 138.1(7) 3_656 .
K16 K8 O5 127.5(8) 3_656 .
K16 K8 O8 90.1(7) 3_656 .
K16 K8 O37 152.3(8) 3_656 .
K16 K8 O72 73.4(7) 3_656 3_657
K16 K8 O23W 45.8(10) 3_656 2_646
O5 K8 W1 23.7(2) . .
O5 K8 W2 60.7(3) . .
O5 K8 W10 32.4(2) . .
O5 K8 Eu2 80.7(3) . .
O5 K8 Eu2 135.8(4) . 3_657
O5 K8 O72 80.4(4) . 3_657
O5 K8 O23W 120.0(9) . 2_646
O8 K8 W1 60.1(3) . .
O8 K8 W2 22.2(2) . .
O8 K8 W10 81.3(4) . .
O8 K8 Eu2 160.5(5) . 3_657
O8 K8 Eu2 75.0(3) . .
O8 K8 O5 63.6(4) . .
O8 K8 O37 109.2(5) . .
O8 K8 O72 118.0(5) . 3_657
O8 K8 O23W 57.7(8) . 2_646
O37 K8 W1 71.2(3) . .
O37 K8 W2 112.9(4) . .
O37 K8 W10 28.0(2) . .
O37 K8 Eu2 89.0(4) . 3_657
O37 K8 Eu2 68.2(3) . .
O37 K8 O5 52.6(3) . .
O37 K8 O72 79.9(4) . 3_657
O37 K8 O23W 161.9(9) . 2_646
O72 K8 W1 66.9(3) 3_657 .
O72 K8 W2 96.5(4) 3_657 .
O72 K8 W10 94.3(4) 3_657 .
O72 K8 Eu2 148.1(4) 3_657 .
O72 K8 Eu2 70.8(3) 3_657 3_657
O4W K8 W1 165.7(5) 3_657 .
O4W K8 W2 143.1(5) 3_657 .
O4W K8 W10 123.5(5) 3_657 .
O4W K8 Eu2 87.0(4) 3_657 .
O4W K8 Eu2 30.1(3) 3_657 3_657
O4W K8 K16 75.5(7) 3_657 3_656
O4W K8 O5 154.8(6) 3_657 .
O4W K8 O8 133.8(6) 3_657 .
O4W K8 O37 102.4(5) 3_657 .
O4W K8 O72 99.8(5) 3_657 3_657
O4W K8 O23W 82.7(9) 3_657 2_646
O23W K8 W1 107.4(9) 2_646 .
O23W K8 W2 60.5(8) 2_646 .
O23W K8 W10 136.3(8) 2_646 .
O23W K8 Eu2 95.0(8) 2_646 .
O23W K8 Eu2 102.9(8) 2_646 3_657
O23W K8 O72 116.7(9) 2_646 3_657
W10 K9 Eu2 56.01(18) 1_554 1_554
W10 K9 K8 95.4(3) 1_554 3_656
Eu2 K9 K8 59.3(2) 1_554 3_656
K12 K9 W10 161.1(5) 3_666 1_554
K12 K9 Eu2 114.3(4) 3_666 1_554
K12 K9 K8 66.6(4) 3_666 3_656
K16 K9 W10 126.9(7) . 1_554
K16 K9 Eu2 74.5(6) . 1_554
K16 K9 K8 37.7(6) . 3_656
K16 K9 K12 39.9(7) . 3_666
K16 K9 O4W 68.4(7) . 1_554
K16 K9 O11W 65.9(8) . 4_565
K16 K9 O23W 46.7(10) . 4_565
O34 K9 W10 21.2(3) 1_554 1_554
O34 K9 Eu2 68.2(4) 1_554 1_554
O34 K9 K8 116.0(5) 1_554 3_656
O34 K9 K12 177.3(6) 1_554 3_666
O34 K9 K16 142.7(8) 1_554 .
O34 K9 O54 78.8(5) 1_554 4_665
O34 K9 O4W 79.8(5) 1_554 1_554
O34 K9 O11W 141.4(8) 1_554 4_565
O34 K9 O13W 130.7(8) 1_554 4_565
O34 K9 O23W 145.6(10) 1_554 4_565
O54 K9 W10 87.6(4) 4_665 1_554
O54 K9 Eu2 143.3(5) 4_665 1_554
O54 K9 K8 128.5(5) 4_665 3_656
O54 K9 K12 99.1(5) 4_665 3_666
O54 K9 K16 136.4(8) 4_665 .
O54 K9 O4W 127.5(6) 4_665 1_554
O54 K9 O11W 71.1(7) 4_665 4_565
O54 K9 O13W 83.3(8) 4_665 4_565
O54 K9 O23W 92.8(10) 4_665 4_565
O4W K9 W10 59.8(3) 1_554 1_554
O4W K9 Eu2 32.7(3) 1_554 1_554
O4W K9 K8 36.5(3) 1_554 3_656
O4W K9 K12 102.9(5) 1_554 3_666
O5W K9 W10 63.4(4) 1_554 1_554
O5W K9 Eu2 29.4(3) 1_554 1_554
O5W K9 K8 83.6(4) 1_554 3_656
O5W K9 K12 117.5(6) 1_554 3_666
O5W K9 K16 83.4(7) 1_554 .
O5W K9 O34 64.1(5) 1_554 1_554
O5W K9 O54 139.9(6) 1_554 4_665
O5W K9 O4W 62.1(4) 1_554 1_554
O5W K9 O11W 148.9(8) 1_554 4_565
O5W K9 O13W 109.1(8) 1_554 4_565
O5W K9 O23W 126.4(10) 1_554 4_565
O11W K9 W10 131.8(7) 4_565 1_554
O11W K9 Eu2 128.3(7) 4_565 1_554
O11W K9 K8 69.1(6) 4_565 3_656
O11W K9 K12 38.1(6) 4_565 3_666
O11W K9 O4W 99.7(7) 4_565 1_554
O11W K9 O23W 23.5(9) 4_565 4_565
O13W K9 W10 151.9(8) 4_565 1_554
O13W K9 Eu2 130.6(8) 4_565 1_554
O13W K9 K8 111.1(8) 4_565 3_656
O13W K9 K12 47.0(7) 4_565 3_666
O13W K9 K16 75.6(9) 4_565 .
O13W K9 O4W 143.6(9) 4_565 1_554
O13W K9 O11W 69.5(9) 4_565 4_565
O13W K9 O23W 80.2(11) 4_565 4_565
O23W K9 W10 126.9(9) 4_565 1_554
O23W K9 Eu2 105.3(9) 4_565 1_554
O23W K9 K8 46.1(9) 4_565 3_656
O23W K9 K12 35.7(9) 4_565 3_666
O23W K9 O4W 79.3(9) 4_565 1_554
W1 K10 W2 48.81(16) 3_656 3_656
W1 K10 K5 62.7(2) 3_656 1_554
W1 K10 K8 57.5(3) 3_656 3_656
W1 K10 K12 104.1(4) 3_656 3_666
W2 K10 K5 110.2(3) 3_656 1_554
W2 K10 K8 57.3(2) 3_656 3_656
W19 K10 W1 96.6(3) 1_554 3_656
W19 K10 W2 120.1(4) 1_554 3_656
W19 K10 K5 52.0(2) 1_554 1_554
W19 K10 K8 62.8(3) 1_554 3_656
W19 K10 K12 98.2(4) 1_554 3_666
K8 K10 K5 77.7(3) 3_656 1_554
K12 K10 W2 59.8(3) 3_666 3_656
K12 K10 K5 141.5(5) 3_666 1_554
K12 K10 K8 65.7(4) 3_666 3_656
K16 K10 W1 95.4(6) . 3_656
K16 K10 W2 72.8(5) . 3_656
K16 K10 W19 62.9(5) . 1_554
K16 K10 K5 105.0(6) . 1_554
K16 K10 K8 39.4(5) . 3_656
K16 K10 K12 37.4(6) . 3_666
O2 K10 W1 24.5(3) 3_656 3_656
O2 K10 W2 24.7(3) 3_656 3_656
O2 K10 W19 106.8(5) 3_656 1_554
O2 K10 K5 85.6(4) 3_656 1_554
O2 K10 K8 50.5(4) 3_656 3_656
O2 K10 K12 80.6(5) 3_656 3_666
O2 K10 K16 80.8(6) 3_656 .
O2 K10 O71 124.6(6) 3_656 1_554
O2 K10 O72 82.7(5) 3_656 1_554
O2 K10 O19W 110.5(10) 3_656 3_666
O2 K10 O22W 108.6(9) 3_656 1_554
O71 K10 W1 122.1(5) 1_554 3_656
O71 K10 W2 125.9(5) 1_554 3_656
O71 K10 W19 28.2(3) 1_554 1_554
O71 K10 K5 78.4(4) 1_554 1_554
O71 K10 K8 74.3(4) 1_554 3_656
O71 K10 K12 80.3(5) 1_554 3_666
O71 K10 K16 54.0(6) 1_554 .
O71 K10 O72 54.1(4) 1_554 1_554
O71 K10 O19W 81.7(10) 1_554 3_666
O71 K10 O22W 87.4(9) 1_554 1_554
O72 K10 W1 69.9(3) 1_554 3_656
O72 K10 W2 101.1(4) 1_554 3_656
O72 K10 W19 26.8(2) 1_554 1_554
O72 K10 K5 36.4(3) 1_554 1_554
O72 K10 K8 49.0(4) 1_554 3_656
O72 K10 K12 105.8(5) 1_554 3_666
O72 K10 K16 68.7(6) 1_554 .
O19W K10 W1 134.8(10) 3_666 3_656
O19W K10 W2 86.0(9) 3_666 3_656
O19W K10 W19 109.2(10) 3_666 1_554
O19W K10 K5 159.4(10) 3_666 1_554
O19W K10 K8 102.1(10) 3_666 3_656
O19W K10 K12 37.4(9) 3_666 3_666
O19W K10 K16 66.7(10) 3_666 .
O19W K10 O72 130.2(10) 3_666 1_554
O19W K10 O22W 138.6(13) 3_666 1_554
O22W K10 W1 84.3(8) 1_554 3_656
O22W K10 W2 131.1(9) 1_554 3_656
O22W K10 W19 71.3(8) 1_554 1_554
O22W K10 K5 35.4(8) 1_554 1_554
O22W K10 K8 113.1(9) 1_554 3_656
O22W K10 K12 167.5(9) 1_554 3_666
O22W K10 K16 133.8(10) 1_554 .
O22W K10 O72 68.0(9) 1_554 1_554
W3 K11 K6 81.5(4) . .
W3 K11 K12 161.6(6) . 2_646
W3 K11 K14 50.9(3) . .
W7 K11 W3 55.9(3) . .
W7 K11 K6 56.5(3) . .
W7 K11 K12 118.0(5) . 2_646
W7 K11 K14 84.1(4) . .
K6 K11 K14 59.8(4) . .
K12 K11 K6 110.3(5) 2_646 .
K12 K11 K14 147.2(6) 2_646 .
K21 K11 W3 67.1(7) . .
K21 K11 W7 71.8(7) . .
K21 K11 K6 128.2(8) . .
K21 K11 K12 94.6(8) . 2_646
K21 K11 K14 116.2(8) . .
O11 K11 W3 24.5(3) . .
O11 K11 W7 79.4(4) . .
O11 K11 K6 89.0(5) . .
O11 K11 K12 158.8(7) . 2_646
O11 K11 K14 38.2(4) . .
O11 K11 K21 79.0(8) . .
O13 K11 W3 29.1(3) . .
O13 K11 W7 28.3(3) . .
O13 K11 K6 72.5(4) . .
O13 K11 K12 139.3(6) . 2_646
O13 K11 K14 71.1(5) . .
O13 K11 K21 59.9(8) . .
O13 K11 O11 53.6(4) . .
O25 K11 W3 80.4(5) . .
O25 K11 W7 25.1(3) . .
O25 K11 K6 48.3(4) . .
O25 K11 K12 96.8(6) . 2_646
O25 K11 K14 96.6(5) . .
O25 K11 K21 85.3(8) . .
O25 K11 O11 102.7(6) . .
O25 K11 O13 53.4(4) . .
O59 K11 W3 86.7(5) 1_655 .
O59 K11 W7 137.1(7) 1_655 .
O59 K11 K6 145.3(7) 1_655 .
O59 K11 K12 90.4(6) 1_655 2_646
O59 K11 K14 87.5(6) 1_655 .
O59 K11 K21 74.7(8) 1_655 .
O59 K11 O11 68.5(5) 1_655 .
O59 K11 O13 109.9(7) 1_655 .
O59 K11 O25 159.3(8) 1_655 .
O59 K11 O13W 73.7(8) 1_655 .
O13W K11 W3 150.2(9) . .
O13W K11 W7 148.9(8) . .
O13W K11 K6 101.9(8) . .
O13W K11 K12 43.6(7) . 2_646
O13W K11 K14 104.9(8) . .
O13W K11 K21 126.0(11) . .
O13W K11 O11 125.8(9) . .
O13W K11 O13 174.2(9) . .
O13W K11 O25 124.1(9) . .
W2 K12 K10 60.2(3) 1_565 3_666
W2 K12 K11 146.2(5) 1_565 2_656
K2 K12 W2 58.4(3) 1_565 1_565
K2 K12 K10 109.6(5) 1_565 3_666
K2 K12 K11 109.7(5) 1_565 2_656
K9 K12 W2 116.5(5) 3_666 1_565
K9 K12 K2 128.7(5) 3_666 1_565
K9 K12 K10 107.2(5) 3_666 3_666
K9 K12 K11 95.8(5) 3_666 2_656
K10 K12 K11 102.3(5) 3_666 2_656
K16 K12 W2 83.4(8) 3_666 1_565
K16 K12 K2 137.0(9) 3_666 1_565
K16 K12 K9 49.9(8) 3_666 3_666
K16 K12 K10 58.2(8) 3_666 3_666
K16 K12 K11 113.2(9) 3_666 2_656
K16 K12 O7 96.5(10) 3_666 1_565
K16 K12 O13W 85.1(11) 3_666 2_656
O7 K12 W2 15.2(3) 1_565 1_565
O7 K12 K2 49.8(4) 1_565 1_565
O7 K12 K9 131.5(7) 1_565 3_666
O7 K12 K10 62.0(5) 1_565 3_666
O7 K12 K11 132.2(7) 1_565 2_656
O7 K12 O13W 178.1(11) 1_565 2_656
O11W K12 W2 89.4(9) 2_656 1_565
O11W K12 K2 77.1(8) 2_656 1_565
O11W K12 K9 51.7(8) 2_656 3_666
O11W K12 K10 132.1(10) 2_656 3_666
O11W K12 K11 120.4(10) 2_656 2_656
O11W K12 K16 84.1(11) 2_656 3_666
O11W K12 O7 98.4(10) 2_656 1_565
O11W K12 O13W 80.7(11) 2_656 2_656
O11W K12 O19W 175.0(15) 2_656 .
O12W K12 W2 100.7(10) 1_565 1_565
O12W K12 K2 43.7(9) 1_565 1_565
O12W K12 K9 120.8(10) 1_565 3_666
O12W K12 K10 131.5(11) 1_565 3_666
O12W K12 K11 68.1(9) 1_565 2_656
O12W K12 K16 170.2(14) 1_565 3_666
O12W K12 O7 88.8(10) 1_565 1_565
O12W K12 O11W 87.0(12) 1_565 2_656
O12W K12 O13W 89.5(12) 1_565 2_656
O12W K12 O19W 95.8(15) 1_565 .
O13W K12 W2 165.5(9) 2_656 1_565
O13W K12 K2 128.3(9) 2_656 1_565
O13W K12 K9 49.0(8) 2_656 3_666
O13W K12 K10 119.8(9) 2_656 3_666
O13W K12 K11 47.7(8) 2_656 2_656
O19W K12 W2 94.2(12) . 1_565
O19W K12 K2 107.7(12) . 1_565
O19W K12 K9 123.4(12) . 3_666
O19W K12 K10 47.9(11) . 3_666
O19W K12 K11 57.3(12) . 2_656
O19W K12 K16 92.8(14) . 3_666
O19W K12 O7 85.9(12) . 1_565
O19W K12 O13W 95.1(14) . 2_656
O23W K12 W2 67.3(12) 2_656 1_565
O23W K12 K2 84.6(12) 2_656 1_565
O23W K12 K9 54.0(12) 2_656 3_666
O23W K12 K10 100.9(13) 2_656 3_666
O23W K12 K11 146.4(14) 2_656 2_656
O23W K12 K16 61.2(14) 2_656 3_666
O23W K12 O7 80.5(13) 2_656 1_565
O23W K12 O11W 31.3(12) 2_656 2_656
O23W K12 O12W 112.0(15) 2_656 1_565
O23W K12 O13W 99.4(15) 2_656 2_656
O23W K12 O19W 148.6(18) 2_656 .
W6 K13 K3 107.2(5) 4_666 3_657
W6 K13 K6 98.7(5) 4_666 4_666
W6 K13 K21 102.1(7) 4_666 .
W8 K13 W6 54.7(3) 4_666 4_666
W8 K13 K3 56.0(3) 4_666 3_657
W8 K13 K6 102.9(5) 4_666 4_666
W8 K13 K21 152.3(8) 4_666 .
K1 K13 W6 70.9(4) . 4_666
K1 K13 W8 103.4(6) . 4_666
K1 K13 K3 107.0(6) . 3_657
K1 K13 K5 80.3(6) . 3_657
K1 K13 K6 137.3(7) . 4_666
K1 K13 K21 50.4(7) . .
K1 K13 O20 83.7(6) . 4_666
K1 K13 O24 86.4(6) . 4_666
K1 K13 O26 134.0(8) . 4_666
K1 K13 O21W 58.4(8) . 4_666
K5 K13 W6 111.5(6) 3_657 4_666
K5 K13 W8 75.3(5) 3_657 4_666
K5 K13 K3 30.2(3) 3_657 3_657
K5 K13 K6 139.1(7) 3_657 4_666
K5 K13 K21 104.4(8) 3_657 .
K5 K13 O20 141.6(8) 3_657 4_666
K5 K13 O21W 137.5(10) 3_657 4_666
K6 K13 K3 115.5(5) 4_666 3_657
K6 K13 K21 95.1(7) 4_666 .
K21 K13 K3 132.9(7) . 3_657
O20 K13 W6 30.2(3) 4_666 4_666
O20 K13 W8 74.8(4) 4_666 4_666
O20 K13 K3 130.8(6) 4_666 3_657
O20 K13 K6 71.5(5) 4_666 4_666
O20 K13 K21 91.4(7) 4_666 .
O20 K13 O21W 49.3(8) 4_666 4_666
O24 K13 W6 26.4(3) 4_666 4_666
O24 K13 W8 28.3(3) 4_666 4_666
O24 K13 K3 82.4(5) 4_666 3_657
O24 K13 K5 94.4(7) 4_666 3_657
O24 K13 K6 102.0(6) 4_666 4_666
O24 K13 K21 127.2(8) 4_666 .
O24 K13 O20 49.8(4) 4_666 4_666
O24 K13 O26 51.7(4) 4_666 4_666
O24 K13 O21W 92.6(9) 4_666 4_666
O26 K13 W6 75.0(5) 4_666 4_666
O26 K13 W8 30.6(3) 4_666 4_666
O26 K13 K3 55.7(4) 4_666 3_657
O26 K13 K5 84.5(6) 4_666 3_657
O26 K13 K6 77.2(5) 4_666 4_666
O26 K13 K21 171.1(9) 4_666 .
O26 K13 O20 81.9(6) 4_666 4_666
O26 K13 O21W 130.5(10) 4_666 4_666
O21W K13 W6 66.3(8) 4_666 4_666
O21W K13 W8 120.8(9) 4_666 4_666
O21W K13 K3 165.0(9) 4_666 3_657
O21W K13 K6 79.3(8) 4_666 4_666
O21W K13 K21 42.2(9) 4_666 .
W3 K14 W5 57.0(3) . .
W3 K14 K2 117.9(4) . 3_656
W3 K14 K6 79.6(4) . .
W3 K14 K11 54.6(3) . .
W5 K14 K2 61.0(3) . 3_656
W5 K14 K6 51.9(3) . .
W5 K14 K11 80.8(4) . .
K2 K14 K11 113.1(4) 3_656 .
K6 K14 K2 59.9(3) . 3_656
K6 K14 K11 53.4(3) . .
K15 K14 W3 73.2(5) . .
K15 K14 W5 68.3(5) . .
K15 K14 K2 87.7(5) . 3_656
K15 K14 K6 119.7(6) . .
K15 K14 K11 127.8(6) . .
K15 K14 O19 82.3(6) . .
K15 K14 O18W 109.2(9) . .
O11 K14 W3 26.0(3) . .
O11 K14 W5 80.6(5) . .
O11 K14 K2 138.9(6) . 3_656
O11 K14 K6 85.7(5) . .
O11 K14 K11 41.2(4) . .
O11 K14 K15 91.4(6) . .
O11 K14 O12 55.1(4) . .
O11 K14 O19 101.2(6) . .
O11 K14 O16W 133.6(11) . 3_656
O11 K14 O18W 48.9(8) . .
O12 K14 W3 30.1(3) . .
O12 K14 W5 27.4(3) . .
O12 K14 K2 88.3(5) . 3_656
O12 K14 K6 65.5(4) . .
O12 K14 K11 69.0(4) . .
O12 K14 K15 64.2(5) . .
O12 K14 O19 52.1(4) . .
O12 K14 O18W 103.6(9) . .
O14 K14 W3 142.0(7) 3_656 .
O14 K14 W5 92.9(5) 3_656 .
O14 K14 K2 41.9(4) 3_656 3_656
O14 K14 K6 100.5(6) 3_656 .
O14 K14 K11 150.7(7) 3_656 .
O14 K14 K15 74.1(6) 3_656 .
O14 K14 O11 165.5(8) 3_656 .
O14 K14 O12 115.5(7) 3_656 .
O14 K14 O19 76.3(5) 3_656 .
O14 K14 O16W 60.9(10) 3_656 3_656
O14 K14 O18W 136.5(10) 3_656 .
O19 K14 W3 80.5(4) . .
O19 K14 W5 25.3(2) . .
O19 K14 K2 37.9(3) . 3_656
O19 K14 K6 40.3(3) . .
O19 K14 K11 87.0(5) . .
O16W K14 W3 149.9(10) 3_656 .
O16W K14 W5 116.3(10) 3_656 .
O16W K14 K2 62.6(9) 3_656 3_656
O16W K14 K6 75.7(9) 3_656 .
O16W K14 K11 96.3(10) 3_656 .
O16W K14 K15 134.7(11) 3_656 .
O16W K14 O12 139.8(11) 3_656 .
O16W K14 O19 91.3(10) 3_656 .
O16W K14 O18W 100.5(12) 3_656 .
O18W K14 W3 73.6(8) . .
O18W K14 W5 129.4(8) . .
O18W K14 K2 162.3(9) . 3_656
O18W K14 K6 112.9(8) . .
O18W K14 K11 60.9(8) . .
O18W K14 O19 146.6(9) . .
W4 K15 W2 54.2(3) . .
W4 K15 W5 102.9(4) . 3_656
W4 K15 K15 63.0(5) . 3_656
W5 K15 W2 135.4(5) 3_656 .
W5 K15 K15 62.2(5) 3_656 3_656
K2 K15 W2 63.4(4) . .
K2 K15 W4 64.5(4) . .
K2 K15 W5 72.3(4) . 3_656
K2 K15 K14 169.6(8) . .
K2 K15 K15 96.3(7) . 3_656
K2 K15 O12 118.0(6) . .
K14 K15 W2 106.7(6) . .
K14 K15 W4 113.1(6) . .
K14 K15 W5 117.8(6) . 3_656
K14 K15 K15 91.1(7) . 3_656
K14 K15 O12 55.2(5) . .
K15 K15 W2 116.9(8) 3_656 .
O9 K15 W2 29.4(3) . .
O9 K15 W4 74.8(4) . .
O9 K15 W5 161.4(7) . 3_656
O9 K15 K2 90.4(6) . .
O9 K15 K14 79.2(6) . .
O9 K15 K15 128.6(9) . 3_656
O9 K15 O12 47.6(4) . .
O10 K15 W2 26.6(3) . .
O10 K15 W4 27.7(3) . .
O10 K15 W5 121.0(6) . 3_656
O10 K15 K2 59.2(4) . .
O10 K15 K14 113.6(7) . .
O10 K15 K15 90.6(7) . 3_656
O10 K15 O9 50.6(4) . .
O10 K15 O12 58.8(4) . .
O12 K15 W2 61.1(4) . .
O12 K15 W4 61.8(4) . .
O12 K15 W5 147.6(6) . 3_656
O12 K15 K15 85.6(7) . 3_656
O16 K15 W2 75.3(5) . .
O16 K15 W2 155.1(7) 3_656 .
O16 K15 W4 106.2(6) 3_656 .
O16 K15 W4 30.5(3) . .
O16 K15 W5 24.9(3) 3_656 3_656
O16 K15 W5 103.6(6) . 3_656
O16 K15 K2 93.2(6) . .
O16 K15 K2 95.6(6) 3_656 .
O16 K15 K14 94.8(7) 3_656 .
O16 K15 K14 86.9(6) . .
O16 K15 K15 45.1(5) . 3_656
O16 K15 K15 49.0(5) 3_656 3_656
O16 K15 O9 83.8(6) . .
O16 K15 O9 173.7(8) 3_656 .
O16 K15 O10 52.3(4) . .
O16 K15 O10 131.8(8) 3_656 .
O16 K15 O12 48.1(4) . .
O16 K15 O12 127.1(7) 3_656 .
O16 K15 O16 94.0(6) 3_656 .
O16 K15 O20W 129.8(11) 3_656 .
O20W K15 W2 64.9(9) . .
O20W K15 W4 118.9(10) . .
O20W K15 W5 117.4(10) . 3_656
O20W K15 K2 85.4(9) . .
O20W K15 K14 87.4(10) . .
O20W K15 K15 177.9(13) . 3_656
O20W K15 O9 52.4(9) . .
O20W K15 O10 91.3(10) . .
O20W K15 O12 94.6(10) . .
O20W K15 O16 136.1(11) . .
W18 K16 Eu2 79.9(5) 1_554 1_554
W19 K16 W18 50.5(4) 1_554 1_554
W19 K16 Eu2 55.0(4) 1_554 1_554
K8 K16 W18 131.0(10) 3_656 1_554
K8 K16 W19 80.5(7) 3_656 1_554
K8 K16 Eu2 68.1(6) 3_656 1_554
K8 K16 K9 103.0(10) 3_656 .
K8 K16 K10 90.2(9) 3_656 .
K8 K16 O71 106.3(10) 3_656 1_554
K8 K16 O73 76.3(8) 3_656 1_554
K8 K16 O11W 93.9(10) 3_656 4_565
K9 K16 W18 97.7(8) . 1_554
K9 K16 W19 116.5(9) . 1_554
K9 K16 Eu2 67.8(6) . 1_554
K9 K16 K10 166.7(11) . .
K9 K16 O73 90.4(8) . 1_554
K9 K16 O11W 58.2(8) . 4_565
K10 K16 W18 71.7(6) . 1_554
K10 K16 W19 63.3(5) . 1_554
K10 K16 Eu2 116.6(8) . 1_554
K12 K16 W18 102.2(10) 3_666 1_554
K12 K16 W19 141.9(12) 3_666 1_554
K12 K16 Eu2 158.0(11) 3_666 1_554
K12 K16 K8 121.4(12) 3_666 3_656
K12 K16 K9 90.2(10) 3_666 .
K12 K16 K10 84.4(9) 3_666 .
K12 K16 O71 114.4(12) 3_666 1_554
K12 K16 O73 161.5(13) 3_666 1_554
K12 K16 O11W 46.7(8) 3_666 4_565
O71 K16 W18 28.3(4) 1_554 1_554
O71 K16 W19 29.0(4) 1_554 1_554
O71 K16 Eu2 77.8(6) 1_554 1_554
O71 K16 K9 121.3(11) 1_554 .
O71 K16 K10 51.4(6) 1_554 .
O71 K16 O73 50.7(5) 1_554 1_554
O71 K16 O11W 158.7(12) 1_554 4_565
O73 K16 W18 59.5(5) 1_554 1_554
O73 K16 W19 27.8(3) 1_554 1_554
O73 K16 Eu2 27.8(3) 1_554 1_554
O73 K16 K10 90.9(8) 1_554 .
O11W K16 W18 134.3(10) 4_565 1_554
O11W K16 W19 171.4(11) 4_565 1_554
O11W K16 Eu2 116.9(9) 4_565 1_554
O11W K16 K10 123.6(10) 4_565 .
O11W K16 O73 144.5(11) 4_565 1_554
O23W K16 W18 152.6(16) 4_565 1_554
O23W K16 W19 156.9(16) 4_565 1_554
O23W K16 Eu2 115.5(14) 4_565 1_554
O23W K16 K8 76.4(14) 4_565 3_656
O23W K16 K9 70.4(13) 4_565 .
O23W K16 K10 115.4(15) 4_565 .
O23W K16 K12 54.8(13) 4_565 3_666
O23W K16 O71 165.9(17) 4_565 1_554
O23W K16 O73 141.8(16) 4_565 1_554
O23W K16 O11W 19.1(12) 4_565 4_565
W12 K17 W13 50.5(4) . .
W12 K17 W14 54.3(4) . .
W12 K17 W15 77.0(5) . .
W12 K17 K18 57.9(6) . .
W13 K17 W14 76.6(5) . .
W13 K17 W15 54.6(4) . .
W13 K17 K18 108.3(8) . .
W14 K17 K18 59.4(6) . .
W15 K17 W14 48.8(4) . .
W15 K17 K18 108.1(8) . .
K19 K17 W12 100.6(9) 3_556 .
K19 K17 W13 111.1(9) 3_556 .
K19 K17 W14 142.1(10) 3_556 .
K19 K17 W15 163.4(11) 3_556 .
K19 K17 K18 83.5(9) 3_556 .
O49 K17 W12 29.0(4) . .
O49 K17 W13 28.1(4) . .
O49 K17 W14 75.8(7) . .
O49 K17 W15 75.7(7) . .
O49 K17 K18 84.6(8) . .
O49 K17 K19 94.2(10) . 3_556
O49 K17 O50 52.0(6) . .
O49 K17 O52 51.5(6) . .
O49 K17 O55 86.8(8) . .
O50 K17 W12 27.3(3) . .
O50 K17 W13 62.6(6) . .
O50 K17 W14 27.2(3) . .
O50 K17 W15 61.9(6) . .
O50 K17 K18 52.2(6) . .
O50 K17 K19 122.0(11) . 3_556
O50 K17 O52 60.7(6) . .
O50 K17 O55 51.2(6) . .
O52 K17 W12 63.0(6) . .
O52 K17 W13 27.3(3) . .
O52 K17 W14 62.0(6) . .
O52 K17 W15 27.5(4) . .
O52 K17 K18 112.9(9) . .
O52 K17 K19 137.2(12) . 3_556
O55 K17 W12 75.3(7) . .
O55 K17 W13 74.3(7) . .
O55 K17 W14 28.3(4) . .
O55 K17 W15 26.3(3) . .
O55 K17 K18 85.9(8) . .
O55 K17 K19 169.2(12) . 3_556
O55 K17 O52 50.0(6) . .
O24W K17 W12 78.2(11) . .
O24W K17 W13 128.5(13) . .
O24W K17 W14 69.1(10) . .
O24W K17 W15 116.3(12) . .
O24W K17 K18 20.3(10) . .
O24W K17 K19 78.6(12) . 3_556
O24W K17 O49 104.6(13) . .
O24W K17 O50 69.6(11) . .
O24W K17 O52 129.2(14) . .
O24W K17 O55 90.7(12) . .
W10 K18 W12 155.3(8) 4_565 .
W10 K18 K20 91.1(8) 4_565 4_565
W12 K18 K20 106.3(8) . 4_565
K4 K18 W10 60.0(5) 4_565 4_565
K4 K18 W12 125.9(8) 4_565 .
K4 K18 K20 38.6(6) 4_565 4_565
O32 K18 W10 67.0(6) 4_565 4_565
O32 K18 W12 136.8(9) 4_565 .
O32 K18 K4 72.6(6) 4_565 4_565
O32 K18 K20 61.8(7) 4_565 4_565
O32 K18 O54 144.6(10) 4_565 .
O34 K18 W10 23.4(3) 4_565 4_565
O34 K18 W12 137.0(9) 4_565 .
O34 K18 K4 50.6(5) 4_565 4_565
O34 K18 K20 88.3(9) 4_565 4_565
O34 K18 O32 85.9(8) 4_565 4_565
O34 K18 O36 53.4(6) 4_565 4_565
O34 K18 O47 149.9(11) 4_565 .
O34 K18 O54 67.9(7) 4_565 .
O36 K18 W10 31.9(3) 4_565 4_565
O36 K18 W12 143.6(9) 4_565 .
O36 K18 K4 88.4(7) 4_565 4_565
O36 K18 K20 109.1(9) 4_565 4_565
O36 K18 O32 58.8(6) 4_565 4_565
O36 K18 O54 86.1(8) 4_565 .
O47 K18 W10 173.0(10) . 4_565
O47 K18 W12 23.4(3) . .
O47 K18 K4 114.5(9) . 4_565
O47 K18 K20 85.8(9) . 4_565
O47 K18 O32 116.6(10) . 4_565
O47 K18 O36 155.0(11) . 4_565
O47 K18 O54 97.0(9) . .
O54 K18 W10 80.9(6) . 4_565
O54 K18 W12 74.3(6) . .
O54 K18 K4 104.7(8) . 4_565
O54 K18 K20 136.3(10) . 4_565
O8W K18 W10 100.7(8) . 4_565
O8W K18 W12 72.1(7) . .
O8W K18 K4 160.7(11) . 4_565
O8W K18 K20 151.8(11) . 4_565
O8W K18 O32 99.3(9) . 4_565
O8W K18 O34 112.4(10) . 4_565
O8W K18 O36 72.6(7) . 4_565
O8W K18 O47 84.8(8) . .
O8W K18 O54 71.4(7) . .
O15W K18 W10 123.3(14) 4_565 4_565
O15W K18 W12 81.1(12) 4_565 .
O15W K18 K4 97.0(13) 4_565 4_565
O15W K18 K20 59.8(12) 4_565 4_565
O15W K18 O32 56.5(11) 4_565 4_565
O15W K18 O34 138.3(15) 4_565 4_565
O15W K18 O36 109.3(14) 4_565 4_565
O15W K18 O47 60.1(12) 4_565 .
O15W K18 O54 153.8(15) 4_565 .
O15W K18 O8W 92.6(13) 4_565 .
O24W K18 W10 85.6(15) . 4_565
O24W K18 W12 84.0(15) . .
O24W K18 K4 50.5(14) . 4_565
O24W K18 K20 70.3(16) . 4_565
O24W K18 O32 123.0(17) . 4_565
O24W K18 O34 62.8(15) . 4_565
O24W K18 O36 116.1(17) . 4_565
O24W K18 O47 87.4(16) . .
O24W K18 O54 66.2(15) . .
O24W K18 O8W 135.6(19) . .
O24W K18 O15W 121(2) . 4_565
W11 K19 Eu1 47.7(4) . .
W11 K19 K4 92.6(7) . 2_546
W11 K19 K7 63.4(5) . 2_546
W12 K19 W11 51.5(4) . .
W12 K19 Eu1 47.7(4) . .
W12 K19 K4 136.4(9) . 2_546
W12 K19 K7 109.0(7) . 2_546
Eu1 K19 K7 69.5(5) . 2_546
K4 K19 Eu1 128.4(8) 2_546 .
K4 K19 K7 62.6(5) 2_546 2_546
K17 K19 W11 169.7(11) 3_556 .
K17 K19 W12 138.9(11) 3_556 .
K17 K19 Eu1 135.6(10) 3_556 .
K17 K19 K4 78.5(8) 3_556 2_546
K17 K19 K7 107.3(9) 3_556 2_546
K20 K19 W11 66.9(9) 2_546 .
K20 K19 W12 97.9(10) 2_546 .
K20 K19 Eu1 114.3(10) 2_546 .
K20 K19 K4 39.5(7) 2_546 2_546
K20 K19 K7 78.3(9) 2_546 2_546
K20 K19 K17 107.8(12) 2_546 3_556
O43 K19 W11 27.8(4) . .
O43 K19 W12 28.1(4) . .
O43 K19 Eu1 30.3(4) . .
O43 K19 K4 120.3(10) . 2_546
O43 K19 K7 80.9(8) . 2_546
O43 K19 K17 160.8(13) . 3_556
O43 K19 K20 90.7(11) . 2_546
O10W K19 W11 90.9(10) 2_546 .
O10W K19 W12 139.4(13) 2_546 .
O10W K19 Eu1 97.6(11) 2_546 .
O10W K19 K4 43.7(8) 2_546 2_546
O10W K19 K7 30.5(8) 2_546 2_546
O10W K19 K17 79.1(11) 2_546 3_556
O10W K19 K20 76.0(12) 2_546 2_546
O10W K19 O43 111.3(13) 2_546 .
W13 K20 K18 124.6(10) 2_556 4_666
K3 K20 W13 61.2(6) 2_556 2_556
K3 K20 K18 154.3(12) 2_556 4_666
K3 K20 K19 120.2(12) 2_556 2_556
K4 K20 W13 164.7(14) . 2_556
K4 K20 K3 125.3(13) . 2_556
K4 K20 K18 56.9(8) . 4_666
K4 K20 K19 86.3(12) . 2_556
K4 K20 O31 61.7(9) . .
K19 K20 W13 78.9(9) 2_556 2_556
K19 K20 K18 84.8(10) 2_556 4_666
O31 K20 W13 133.1(13) . 2_556
O31 K20 K3 82.1(10) . 2_556
O31 K20 K18 77.8(9) . 4_666
O31 K20 K19 148.0(15) . 2_556
O44 K20 W13 26.3(5) 2_556 2_556
O44 K20 K3 54.1(7) 2_556 2_556
O44 K20 K4 142.5(16) 2_556 .
O44 K20 K18 143.2(14) 2_556 4_666
O44 K20 K19 70.1(10) 2_556 2_556
O44 K20 O31 136.2(15) 2_556 .
W1 K21 W3 48.8(5) . .
W1 K21 W9 53.6(5) . .
W9 K21 W3 73.6(7) . .
K1 K21 W1 62.2(7) . .
K1 K21 W3 110.6(11) . .
K1 K21 W9 59.5(7) . .
K1 K21 K11 166.2(14) . .
K1 K21 O13 111.9(12) . .
K1 K21 O27 83.5(10) . .
K1 K21 O17W 101.4(13) . .
K1 K21 Li1 90.8(15) . 2_646
K11 K21 W1 112.2(11) . .
K11 K21 W3 63.5(7) . .
K11 K21 W9 106.8(10) . .
K11 K21 Li1 81.1(15) . 2_646
O3 K21 W1 28.2(4) . .
O3 K21 W3 25.6(4) . .
O3 K21 W9 72.5(8) . .
O3 K21 K1 89.4(11) . .
O3 K21 K11 87.4(10) . .
O3 K21 O4 49.8(7) . .
O3 K21 O13 49.2(7) . .
O3 K21 O27 82.6(10) . .
O3 K21 O17W 51.6(9) . .
O3 K21 Li1 130.3(17) . 2_646
O4 K21 W1 27.5(4) . .
O4 K21 W3 59.9(7) . .
O4 K21 W9 26.2(4) . .
O4 K21 K1 55.4(7) . .
O4 K21 K11 113.4(12) . .
O4 K21 O13 56.8(7) . .
O4 K21 O27 49.0(7) . .
O4 K21 O17W 96.1(13) . .
O4 K21 Li1 91.4(16) . 2_646
O13 K21 W1 61.3(7) . .
O13 K21 W3 28.1(4) . .
O13 K21 W9 57.6(7) . .
O13 K21 K11 56.6(7) . .
O13 K21 O27 46.6(6) . .
O13 K21 O17W 90.7(12) . .
O13 K21 Li1 85.4(15) . 2_646
O27 K21 W1 73.6(8) . .
O27 K21 W3 72.0(8) . .
O27 K21 W9 26.8(4) . .
O27 K21 K11 82.7(9) . .
O27 K21 Li1 48.1(13) . 2_646
O17W K21 W1 68.7(10) . .
O17W K21 W3 62.9(9) . .
O17W K21 W9 121.9(13) . .
O17W K21 K11 87.1(12) . .
O17W K21 O27 133.5(14) . .
O17W K21 Li1 167.8(19) . 2_646
O21W K21 W1 121.2(15) 4_666 .
O21W K21 W3 168.4(16) 4_666 .
O21W K21 W9 95.5(14) 4_666 .
O21W K21 K1 59.1(11) 4_666 .
O21W K21 K11 125.2(16) 4_666 .
O21W K21 O3 147.4(17) 4_666 .
O21W K21 O4 108.5(16) 4_666 .
O21W K21 O13 146.6(17) 4_666 .
O21W K21 O27 100.3(14) 4_666 .
O21W K21 O17W 122.1(17) 4_666 .
O21W K21 Li1 63.8(16) 4_666 2_646
Li1 K21 W1 118.7(16) 2_646 .
Li1 K21 W3 113.6(15) 2_646 .
Li1 K21 W9 65.2(13) 2_646 .
W1 O1 K1 103.8(5) . .
W1 O1 K5 165.2(7) . 3_657
K5 O1 K1 79.6(4) 3_657 .
W1 O2 W2 119.6(5) . .
W1 O2 K10 119.2(5) . 3_656
W2 O2 K10 119.6(5) . 3_656
W1 O3 K21 105.8(9) . .
W3 O3 W1 120.7(5) . .
W3 O3 K21 110.2(9) . .
W1 O4 K1 101.3(4) . .
W1 O4 K21 104.4(8) . .
W9 O4 W1 148.6(6) . .
W9 O4 K1 97.5(4) . .
W9 O4 K21 106.5(8) . .
K1 O4 K21 63.9(8) . .
W1 O5 W10 146.6(6) . .
W1 O5 K8 113.0(5) . .
W10 O5 K8 97.9(4) . .
W2 O6 W1 92.1(4) . .
W2 O6 W3 94.6(4) . .
W3 O6 W1 91.8(4) . .
As1 O6 W1 119.8(5) . .
As1 O6 W2 116.6(5) . .
As1 O6 W3 132.5(5) . .
W2 O7 K2 106.8(5) . .
W2 O7 K12 142.1(8) . 1_545
K12 O7 K2 91.1(6) 1_545 .
W2 O8 K8 116.8(6) . .
W2 O9 K15 100.1(5) . .
W3 O9 W2 120.6(5) . .
W3 O9 K15 110.1(6) . .
W2 O10 K2 99.4(4) . .
W2 O10 K15 108.0(6) . .
W4 O10 W2 148.7(6) . .
W4 O10 K2 98.9(4) . .
W4 O10 K15 102.9(6) . .
K15 O10 K2 62.9(4) . .
W3 O11 K11 105.9(6) . .
W3 O11 K14 105.1(6) . .
K14 O11 K11 100.6(6) . .
W3 O12 W5 155.9(7) . .
W3 O12 K14 95.5(5) . .
W3 O12 K15 102.5(5) . .
W5 O12 K14 104.5(5) . .
W5 O12 K15 99.0(5) . .
K14 O12 K15 60.6(5) . .
W3 O13 K11 99.6(5) . .
W3 O13 K21 100.2(8) . .
W7 O13 W3 149.0(6) . .
W7 O13 K11 98.8(5) . .
W7 O13 K21 110.3(8) . .
K11 O13 K21 63.5(8) . .
W4 O14 K2 106.4(5) . .
W4 O14 K14 147.4(8) . 3_656
K14 O14 K2 100.9(5) 3_656 .
W4 O15 Eu1 148.5(6) . .
W4 O16 K15 100.3(6) . .
W4 O16 K15 115.8(6) . 3_656
W5 O16 W4 119.6(5) . .
W5 O16 K15 113.6(6) . .
W5 O16 K15 115.0(6) . 3_656
K15 O16 K15 86.0(6) 3_656 .
W6 O17 W4 117.8(5) . .
W4 O18 W5 91.6(4) . .
W6 O18 W4 92.5(4) . .
W6 O18 W5 92.5(4) . .
As1 O18 W4 117.2(5) . .
As1 O18 W5 134.6(6) . .
As1 O18 W6 118.5(6) . .
W5 O19 K2 148.0(7) . 3_656
W5 O19 K6 105.0(6) . .
W5 O19 K14 99.1(6) . .
K2 O19 K6 104.5(5) 3_656 .
K2 O19 K14 93.1(5) 3_656 .
K6 O19 K14 90.2(5) . .
W5 O20 W6 121.2(5) . .
W5 O20 K13 115.7(6) . 4_565
W6 O20 K13 96.6(6) . 4_565
W5 O21 K6 96.4(5) . .
W7 O21 W5 149.3(6) . .
W7 O21 K6 102.8(5) . .
W6 O22 K1 127.4(6) . 4_565
W6 O23 Eu1 137.4(5) . .
W6 O23 Eu3 131.5(5) . .
Eu3 O23 Eu1 90.0(3) . .
W6 O24 W8 146.4(6) . .
W6 O24 K13 109.0(6) . 4_565
W8 O24 K13 104.6(6) . 4_565
W7 O25 K6 100.5(6) . .
W7 O25 K11 105.4(6) . .
K11 O25 K6 83.6(5) . .
W7 O26 W8 121.3(5) . .
W7 O26 K13 111.9(6) . 4_565
W8 O26 K13 98.5(6) . 4_565
W7 O27 K21 106.4(8) . .
W9 O27 W7 120.4(5) . .
W9 O27 K21 100.9(8) . .
W7 O28 W9 90.7(3) . .
W8 O28 W7 94.4(3) . .
W8 O28 W9 92.5(4) . .
As1 O28 W7 134.6(5) . .
As1 O28 W8 115.9(5) . .
As1 O28 W9 119.0(5) . .
W8 O29 K3 131.0(6) . 2_556
W8 O29 K5 131.3(7) . 2_556
K3 O29 K5 52.6(3) 2_556 2_556
W8 O30 Eu3 136.9(5) . .
W8 O30 K4 100.9(5) . .
Eu3 O30 K4 101.0(4) . .
W8 O31 K4 101.3(4) . .
W8 O31 K20 111.9(8) . .
W9 O31 W8 121.3(5) . .
W9 O31 K4 109.2(5) . .
W9 O31 K20 126.8(9) . .
K4 O31 K20 55.7(8) . .
W9 O32 K1 105.2(6) . .
W9 O32 K18 122.0(8) . 4_666
K1 O32 K18 94.8(6) . 4_666
W9 O33 K4 102.2(4) . .
W10 O33 W9 147.7(6) . .
W10 O33 K4 99.5(4) . .
W10 O34 K4 109.5(5) . .
W10 O34 K9 122.2(6) . 1_556
W10 O34 K18 110.9(8) . 4_666
K4 O34 K18 75.7(6) . 4_666
K9 O34 K4 120.6(5) 1_556 .
K9 O34 K18 107.8(7) 1_556 4_666
W10 O35 Eu2 152.6(6) . .
W10 O36 K1 140.9(5) . .
W10 O36 K18 96.9(7) . 4_666
K1 O36 K18 94.8(6) . 4_666
C1 O36 W10 117.0(10) . .
C1 O36 K1 91.9(10) . .
C1 O36 K18 113.1(12) . 4_666
W10 O37 K8 104.7(5) . .
C2 O37 W10 122.1(10) . .
C2 O37 K8 102.1(12) . .
K5 O38 K1 85.0(5) 3_657 .
C1 O38 K1 96.4(10) . .
C1 O38 K5 117.4(12) . 3_657
C4 O39 Eu2 137.2(11) . 3_657
C4 O40 K7 112.1(11) . 4_666
W11 O41 K7 159.3(6) . 2_546
W11 O42 Eu1 110.2(5) . .
W11 O42 Eu2 148.1(5) . .
Eu2 O42 Eu1 101.3(4) . .
W11 O43 Eu1 99.4(4) . .
W11 O43 K19 111.0(8) . .
W12 O43 W11 120.4(5) . .
W12 O43 Eu1 99.2(4) . .
W12 O43 K19 110.0(8) . .
Eu1 O43 K19 116.2(8) . .
W11 O44 K3 100.9(5) . .
W11 O44 K20 123.0(9) . 2_546
W13 O44 W11 122.0(6) . .
W13 O44 K3 102.1(4) . .
W13 O44 K20 114.1(9) . 2_546
K20 O44 K3 75.6(9) 2_546 .
W11 O45 W19 148.1(6) . .
W11 O45 K3 102.0(5) . .
W19 O45 K3 108.3(4) . .
W12 O46 W11 93.5(4) . .
W12 O46 W13 91.1(4) . .
W13 O46 W11 91.2(4) . .
As2 O46 W11 117.9(5) . .
As2 O46 W12 119.0(5) . .
As2 O46 W13 134.3(5) . .
W12 O47 K18 110.5(8) . .
W12 O48 Eu1 110.3(5) . .
W12 O48 Eu3 149.0(6) . .
Eu3 O48 Eu1 100.3(4) . .
W12 O49 K17 101.1(7) . .
W13 O49 W12 121.6(6) . .
W13 O49 K17 103.3(7) . .
W12 O50 W14 148.2(6) . .
W12 O50 K17 103.4(7) . .
W14 O50 K17 107.4(7) . .
W13 O52 W15 150.1(7) . .
W13 O52 K17 103.2(8) . .
W15 O52 K17 105.3(7) . .
W13 O53 W17 149.8(6) . .
W13 O53 K3 103.7(5) . .
W17 O53 K3 104.8(5) . .
W14 O54 K9 138.9(7) . 4_566
W14 O54 K18 109.6(7) . .
K9 O54 K18 101.3(7) 4_566 .
W14 O55 K17 105.7(8) . .
W15 O55 W14 119.3(6) . .
W15 O55 K17 108.1(8) . .
W14 O56 Eu3 154.9(6) . .
W14 O56 K7 93.2(5) . .
Eu3 O56 K7 105.8(4) . .
W14 O57 W16 117.7(5) . .
W14 O57 K7 102.9(5) . .
W16 O57 K7 103.2(5) . .
W14 O58 W15 92.3(4) . .
W16 O58 W14 92.3(4) . .
W16 O58 W15 94.6(4) . .
As2 O58 W14 116.9(5) . .
As2 O58 W15 133.9(6) . .
As2 O58 W16 117.3(5) . .
W15 O59 K11 146.6(8) . 1_455
W15 O60 W16 120.4(6) . .
W15 O61 W17 156.3(7) . .
W16 O62 K2 146.3(7) . 2_556
W16 O62 K6 99.2(5) . 4_566
K2 O62 K6 91.0(4) 2_556 4_566
W16 O63 K7 98.5(5) . .
W16 O64 W18 144.1(6) . .
W16 O64 K6 107.2(5) . 4_566
W18 O64 K6 98.7(5) . 4_566
W17 O66 W18 120.9(6) . .
W17 O67 W19 121.2(6) . .
W17 O67 K3 105.5(6) . .
W17 O67 K5 147.3(6) . .
W19 O67 K3 106.0(5) . .
W19 O67 K5 88.3(4) . .
K3 O67 K5 47.9(3) . .
W18 O68 W17 93.7(4) . .
W18 O68 W19 91.6(4) . .
W19 O68 W17 91.7(4) . .
As2 O68 W17 132.7(5) . .
As2 O68 W18 118.1(6) . .
As2 O68 W19 119.1(5) . .
W18 O69 K6 103.2(6) . 4_566
W18 O71 K10 131.6(6) . 1_556
W18 O71 K16 107.7(8) . 1_556
W19 O71 W18 118.3(6) . .
W19 O71 K10 107.4(5) . 1_556
W19 O71 K16 103.3(8) . 1_556
K10 O71 K16 74.6(7) 1_556 1_556
W19 O72 K5 110.0(6) . .
W19 O72 K8 112.6(6) . 3_657
W19 O72 K10 97.6(5) . 1_556
K5 O72 K8 134.5(5) . 3_657
K5 O72 K10 103.8(5) . 1_556
K10 O72 K8 85.9(5) 1_556 3_657
W19 O73 Eu2 154.8(6) . .
W19 O73 K16 90.7(7) . 1_556
Eu2 O73 K16 109.3(7) . 1_556
Eu1 O74 Eu2 97.4(4) . .
Eu3 O74 Eu1 98.1(4) . .
Eu3 O74 Eu2 148.3(5) . .
O36 C1 K1 65.9(9) . .
O36 C1 O38 122.1(15) . .
O36 C1 C2 114.9(14) . .
O38 C1 K1 61.4(9) . .
O38 C1 C2 122.9(15) . .
C2 C1 K1 154.5(14) . .
O37 C2 C1 110.5(15) . .
O37 C2 H2 107.2 . .
O37 C2 C3 113.2(17) . .
C1 C2 H2 107.2 . .
C3 C2 C1 111.3(17) . .
C3 C2 H2 107.2 . .
K7 C3 H3A 61.4 4_666 .
K7 C3 H3B 64.2 4_666 .
C2 C3 K7 160.0(13) . 4_666
C2 C3 H3A 107.4 . .
C2 C3 H3B 107.4 . .
C2 C3 C4 119.5(17) . .
H3A C3 H3B 107.0 . .
C4 C3 K7 80.4(11) . 4_666
C4 C3 H3A 107.4 . .
C4 C3 H3B 107.4 . .
O39 C4 K7 154.0(11) . 4_666
O39 C4 C3 119.5(17) . .
O40 C4 K7 48.7(9) . 4_666
O40 C4 O39 122.3(15) . .
O40 C4 C3 118.2(17) . .
C3 C4 K7 75.0(11) . 4_666
Eu1 O1W K7 149.6(5) . 2_546
Eu2 O3W Eu1 94.0(3) . .
Eu2 O4W K8 116.3(5) . 3_657
Eu2 O4W K9 104.4(5) . 1_556
K8 O4W K9 100.8(5) 3_657 1_556
Eu2 O5W K9 116.3(5) . 1_556
Eu3 O6W K7 117.2(6) . .
Eu3 O7W K4 106.9(5) . .
Eu3 O8W K18 135.9(8) . .
K7 O10W K4 108.8(10) . .
K19 O10W K4 98.1(12) 2_556 .
K19 O10W K7 120.8(13) 2_556 .
K9 O11W K16 55.9(8) 4_666 4_666
K12 O11W K9 90.3(10) 2_646 4_666
K12 O11W K16 49.2(9) 2_646 4_666
O23W O11W K9 83(2) . 4_666
O23W O11W K12 69(3) . 2_646
O23W O11W K16 39(2) . 4_666
K12 O12W K2 101.5(12) 1_545 .
K9 O13W K11 164.5(13) 4_666 .
K12 O13W K9 84.0(10) 2_646 4_666
K12 O13W K11 88.7(10) 2_646 .
K12 O19W K10 94.7(15) . 3_666
K1 O21W K13 52.4(8) 4_565 4_565
K21 O21W K1 67.2(12) 4_565 4_565
K21 O21W K13 86.1(14) 4_565 4_565
K5 O22W K10 105.8(13) . 1_556
K9 O23W K8 90.4(12) 4_666 2_656
K12 O23W K8 113.3(17) 2_646 2_656
K12 O23W K9 90.3(15) 2_646 4_666
K12 O23W K16 64.0(14) 2_646 4_666
K16 O23W K8 57.9(12) 4_666 2_656
K16 O23W K9 62.9(12) 4_666 4_666
O11W O23W K8 160(3) . 2_656
O11W O23W K9 74(2) . 4_666
O11W O23W K12 80(3) . 2_646
O11W O23W K16 122(3) . 4_666
K17 O24W K4 123.9(16) . 4_565
K18 O24W K4 96.9(18) . 4_565
K18 O24W K17 130(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 K1 3.864(5) .
W1 K8 4.132(14) .
W1 K10 4.035(14) 3_656
W1 K21 4.10(4) .
W1 O1 1.748(11) .
W1 O2 1.917(11) .
W1 O3 2.016(11) .
W1 O4 1.952(11) .
W1 O5 1.802(10) .
W1 O6 2.369(10) .
W2 K2 3.952(7) .
W2 K8 4.134(14) .
W2 K10 4.077(14) 3_656
W2 K12 4.058(17) 1_545
W2 K15 4.14(2) .
W2 O2 1.961(10) .
W2 O6 2.284(10) .
W2 O7 1.734(11) .
W2 O8 1.753(10) .
W2 O9 2.063(11) .
W2 O10 1.946(11) .
W3 K11 4.005(19) .
W3 K14 3.811(18) .
W3 K21 4.12(4) .
W3 O3 1.894(10) .
W3 O6 2.365(10) .
W3 O9 1.870(11) .
W3 O11 1.728(11) .
W3 O12 1.918(11) .
W3 O13 1.975(12) .
W4 K2 3.906(7) .
W4 K15 3.97(2) .
W4 O10 1.893(11) .
W4 O14 1.733(11) .
W4 O15 1.774(11) .
W4 O16 2.052(11) .
W4 O17 1.978(10) .
W4 O18 2.323(12) .
W5 K6 3.735(11) .
W5 K14 4.050(18) .
W5 K15 4.03(2) 3_656
W5 O12 1.922(11) .
W5 O16 1.871(11) .
W5 O18 2.411(10) .
W5 O19 1.753(11) .
W5 O20 1.876(12) .
W5 O21 1.981(11) .
W6 K1 4.103(5) 4_565
W6 K13 4.05(2) 4_565
W6 O17 1.938(11) .
W6 O18 2.320(11) .
W6 O20 2.047(11) .
W6 O22 1.747(11) .
W6 O23 1.831(11) .
W6 O24 1.903(12) .
W7 K6 3.819(11) .
W7 K11 3.927(19) .
W7 O13 1.885(11) .
W7 O21 1.857(11) .
W7 O25 1.726(11) .
W7 O26 1.878(12) .
W7 O27 1.984(11) .
W7 O28 2.359(10) .
W8 Eu3 3.854(2) .
W8 K4 3.865(10) .
W8 K13 3.97(2) 4_565
W8 O24 1.948(11) .
W8 O26 2.044(11) .
W8 O28 2.301(10) .
W8 O29 1.735(11) .
W8 O30 1.784(11) .
W8 O31 1.949(10) .
W9 K1 3.731(6) .
W9 K4 4.040(10) .
W9 K21 4.12(4) .
W9 O4 1.896(11) .
W9 O27 1.892(10) .
W9 O28 2.371(10) .
W9 O31 1.922(10) .
W9 O32 1.730(11) .
W9 O33 1.945(10) .
W10 K4 3.929(10) .
W10 K8 4.000(13) .
W10 K9 4.059(14) 1_556
W10 K18 4.08(3) 4_666
W10 O5 2.164(10) .
W10 O33 1.878(10) .
W10 O34 1.737(12) .
W10 O35 1.778(10) .
W10 O36 2.169(11) .
W10 O37 1.942(10) .
W11 Eu1 3.5136(16) .
W11 K3 3.817(9) .
W11 K19 4.00(3) .
W11 O41 1.720(11) .
W11 O42 1.855(10) .
W11 O43 1.995(10) .
W11 O44 1.964(11) .
W11 O45 1.901(11) .
W11 O46 2.386(10) .
W12 Eu1 3.507(2) .
W12 K17 3.95(3) .
W12 K18 4.11(3) .
W12 K19 3.97(3) .
W12 O43 1.992(10) .
W12 O46 2.362(11) .
W12 O47 1.744(12) .
W12 O48 1.863(11) .
W12 O49 1.952(11) .
W12 O50 1.863(11) .
W13 K3 3.827(9) .
W13 K17 3.99(3) .
W13 K20 3.98(4) 2_546
W13 O44 1.933(11) .
W13 O46 2.384(10) .
W13 O49 1.929(12) .
W13 O51 1.733(12) .
W13 O52 1.880(12) .
W13 O53 1.891(13) .
W14 K7 3.811(13) .
W14 K17 4.13(3) .
W14 O50 1.975(11) .
W14 O54 1.730(13) .
W14 O55 2.031(11) .
W14 O56 1.782(11) .
W14 O57 1.927(12) .
W14 O58 2.344(11) .
W15 K17 4.10(3) .
W15 O52 1.960(12) .
W15 O55 1.907(12) .
W15 O58 2.367(11) .
W15 O59 1.738(12) .
W15 O60 1.868(13) .
W15 O61 1.913(12) .
W16 K6 3.887(11) 4_566
W16 K7 3.861(13) .
W16 O57 1.990(11) .
W16 O58 2.305(11) .
W16 O60 2.089(11) .
W16 O62 1.751(12) .
W16 O63 1.753(12) .
W16 O64 1.913(11) .
W17 K3 3.895(9) .
W17 O53 1.953(13) .
W17 O61 1.918(11) .
W17 O65 1.710(13) .
W17 O66 1.840(14) .
W17 O67 1.891(11) .
W17 O68 2.403(11) .
W18 K6 3.687(11) 4_566
W18 K16 3.99(3) 1_556
W18 O64 1.930(11) .
W18 O66 2.105(13) .
W18 O68 2.307(11) .
W18 O69 1.728(12) .
W18 O70 1.760(12) .
W18 O71 1.988(10) .
W19 K3 3.999(9) .
W19 K5 3.922(11) .
W19 K10 3.843(14) 1_556
W19 K16 3.83(3) 1_556
W19 O45 1.942(11) .
W19 O67 2.025(12) .
W19 O68 2.353(10) .
W19 O71 1.905(11) .
W19 O72 1.746(12) .
W19 O73 1.784(11) .
Eu1 Eu3 3.642(2) .
Eu1 O15 2.356(11) .
Eu1 O23 2.604(11) .
Eu1 O42 2.411(10) .
Eu1 O43 2.585(11) .
Eu1 O48 2.394(11) .
Eu1 O74 2.414(11) .
Eu1 O1W 2.482(12) .
Eu1 O2W 2.482(12) .
Eu1 O3W 2.585(10) .
Eu2 K8 4.385(13) .
Eu2 K8 4.468(13) 3_657
Eu2 K9 4.480(14) 1_556
Eu2 O35 2.364(10) .
Eu2 O39 2.402(12) 3_657
Eu2 O42 2.371(10) .
Eu2 O73 2.301(11) .
Eu2 O74 2.506(10) .
Eu2 O3W 2.470(10) .
Eu2 O4W 2.500(12) .
Eu2 O5W 2.453(12) .
Eu3 K4 4.242(10) .
Eu3 K7 4.495(13) .
Eu3 O23 2.545(11) .
Eu3 O30 2.354(11) .
Eu3 O48 2.351(11) .
Eu3 O56 2.320(11) .
Eu3 O74 2.411(10) .
Eu3 O6W 2.515(13) .
Eu3 O7W 2.456(12) .
Eu3 O8W 2.427(14) .
As1 O6 1.813(10) .
As1 O18 1.802(10) .
As1 O28 1.802(10) .
As2 O46 1.769(11) .
As2 O58 1.815(10) .
As2 O68 1.783(10) .
K1 K5 3.854(12) 3_657
K1 K13 2.81(2) .
K1 K21 3.25(4) .
K1 O1 3.053(13) .
K1 O4 2.975(11) .
K1 O22 2.800(13) 4_666
K1 O32 2.883(14) .
K1 O36 3.017(12) .
K1 O38 2.918(14) .
K1 C1 3.305(18) .
K1 O21W 3.02(4) 4_666
K2 K6 4.457(13) 3_656
K2 K12 4.041(18) 1_545
K2 K15 3.25(2) .
K2 O7 3.086(15) .
K2 O10 3.138(13) .
K2 O14 3.045(15) .
K2 O19 2.759(13) 3_656
K2 O62 3.046(14) 2_546
K2 O9W 2.80(2) .
K2 O12W 2.85(3) .
K3 K5 2.619(14) .
K3 K13 4.81(2) 3_657
K3 K20 3.50(4) 2_546
K3 O29 2.841(14) 2_546
K3 O44 2.923(14) .
K3 O45 2.937(14) .
K3 O53 2.908(15) .
K3 O67 2.936(16) .
K4 K18 3.75(3) 4_666
K4 K20 2.79(4) .
K4 O30 3.107(15) .
K4 O31 2.977(14) .
K4 O33 3.154(15) .
K4 O34 2.992(15) .
K4 O7W 2.818(15) .
K4 O10W 3.06(3) .
K4 O24W 2.92(4) 4_666
K5 K1 3.854(12) 3_657
K5 K10 4.857(18) 1_556
K5 K13 3.16(2) 3_657
K5 O1 2.967(16) 3_657
K5 O29 3.059(16) 2_546
K5 O38 2.785(19) 3_657
K5 O67 3.420(16) .
K5 O72 2.967(18) .
K5 O22W 2.92(4) .
K6 W16 3.887(11) 4_665
K6 W18 3.687(11) 4_665
K6 K11 4.13(2) .
K6 K13 4.20(2) 4_565
K6 O19 2.877(17) .
K6 O21 2.952(15) .
K6 O25 3.108(16) .
K6 O62 3.200(17) 4_665
K6 O64 2.864(15) 4_665
K6 O69 2.887(17) 4_665
K7 O40 2.852(18) 4_565
K7 O41 3.091(18) 2_556
K7 O56 3.272(17) .
K7 O57 2.885(17) .
K7 O63 3.190(18) .
K7 C3 3.45(2) 4_565
K7 C4 3.52(2) 4_565
K7 O1W 3.124(18) 2_556
K7 O6W 2.749(19) .
K7 O10W 2.89(3) .
K8 Eu2 4.468(13) 3_657
K8 K16 2.86(3) 3_656
K8 O5 3.080(17) .
K8 O8 3.035(17) .
K8 O37 3.038(18) .
K8 O72 3.409(19) 3_657
K8 O4W 2.757(18) 3_657
K8 O23W 3.28(5) 2_646
K9 W10 4.059(14) 1_554
K9 Eu2 4.480(14) 1_554
K9 K8 4.557(19) 3_656
K9 K12 3.87(2) 3_666
K9 K16 2.96(3) .
K9 O34 2.859(18) 1_554
K9 O54 2.864(19) 4_665
K9 O4W 3.148(18) 1_554
K9 O5W 2.816(18) 1_554
K9 O11W 3.04(3) 4_565
K9 O13W 2.94(4) 4_565
K9 O23W 3.13(5) 4_565
K10 W1 4.035(14) 3_656
K10 W2 4.077(14) 3_656
K10 W19 3.843(14) 1_554
K10 K5 4.857(18) 1_554
K10 K8 4.51(2) 3_656
K10 K12 4.07(2) 3_666
K10 K16 3.47(3) .
K10 O2 2.736(18) 3_656
K10 O71 2.816(18) 1_554
K10 O72 3.201(19) 1_554
K10 O19W 3.03(5) 3_666
K10 O22W 3.16(4) 1_554
K11 K12 4.13(3) 2_646
K11 K14 4.73(3) .
K11 K21 3.40(4) .
K11 O11 3.17(2) .
K11 O13 3.17(2) .
K11 O25 3.10(2) .
K11 O59 2.84(2) 1_655
K11 O13W 3.05(4) .
K12 W2 4.058(17) 1_565
K12 K2 4.041(18) 1_565
K12 K9 3.87(2) 3_666
K12 K10 4.07(2) 3_666
K12 K11 4.13(3) 2_656
K12 K16 2.48(3) 3_666
K12 O7 2.55(2) 1_565
K12 O11W 2.39(3) 2_656
K12 O12W 2.35(4) 1_565
K12 O13W 2.85(4) 2_656
K12 O19W 2.48(5) .
K12 O23W 2.26(5) 2_656
K13 W6 4.05(2) 4_666
K13 W8 3.97(2) 4_666
K13 K3 4.81(2) 3_657
K13 K5 3.16(2) 3_657
K13 K6 4.20(2) 4_666
K13 K21 4.21(4) .
K13 O20 3.27(2) 4_666
K13 O24 3.01(2) 4_666
K13 O26 3.12(2) 4_666
K13 O21W 3.31(5) 4_666
K14 K2 4.481(19) 3_656
K14 K15 3.31(3) .
K14 O11 2.98(2) .
K14 O12 3.11(2) .
K14 O14 2.76(2) 3_656
K14 O19 3.39(2) .
K14 O16W 3.00(5) 3_656
K14 O18W 3.34(4) .
K15 W5 4.03(2) 3_656
K15 K15 4.04(4) 3_656
K15 O9 3.24(2) .
K15 O10 3.10(2) .
K15 O12 3.42(2) .
K15 O16 3.05(2) .
K15 O16 2.87(2) 3_656
K15 O20W 2.98(4) .
K16 W18 3.99(3) 1_554
K16 W19 3.83(3) 1_554
K16 Eu2 4.66(3) 1_554
K16 K8 2.86(3) 3_656
K16 K12 2.48(3) 3_666
K16 O71 2.91(3) 1_554
K16 O73 3.37(3) 1_554
K16 O11W 3.26(4) 4_565
K16 O23W 2.42(5) 4_565
K17 K18 4.48(4) .
K17 K19 3.66(5) 3_556
K17 O49 3.08(3) .
K17 O50 3.08(3) .
K17 O52 3.12(3) .
K17 O55 3.08(3) .
K17 O24W 2.88(5) .
K18 W10 4.08(3) 4_565
K18 K4 3.75(3) 4_565
K18 K20 4.46(5) 4_565
K18 O32 3.33(3) 4_565
K18 O34 3.12(3) 4_565
K18 O36 3.20(3) 4_565
K18 O47 3.16(3) .
K18 O54 3.37(3) .
K18 O8W 2.88(3) .
K18 O15W 2.39(5) 4_565
K18 O24W 2.04(5) .
K19 K4 4.39(4) 2_546
K19 K7 4.90(4) 2_546
K19 K17 3.66(5) 3_556
K19 K20 3.57(5) 2_546
K19 O43 2.82(4) .
K19 O10W 2.74(4) 2_546
K20 W13 3.98(4) 2_556
K20 K3 3.50(4) 2_556
K20 K18 4.46(5) 4_666
K20 K19 3.57(5) 2_556
K20 O31 3.00(4) .
K20 O44 2.78(4) 2_556
K21 O3 3.06(4) .
K21 O4 3.15(4) .
K21 O13 3.28(4) .
K21 O27 3.31(4) .
K21 O17W 3.31(5) .
K21 O21W 2.84(6) 4_666
K21 Li1 3.55(8) 2_646
O1 K5 2.967(16) 3_657
O2 K10 2.736(18) 3_656
O7 K12 2.55(2) 1_545
O14 K14 2.76(2) 3_656
O16 K15 2.87(2) 3_656
O19 K2 2.759(13) 3_656
O20 K13 3.27(2) 4_565
O22 K1 2.800(13) 4_565
O24 K13 3.01(2) 4_565
O26 K13 3.12(2) 4_565
O29 K3 2.841(14) 2_556
O29 K5 3.059(16) 2_556
O32 K18 3.33(3) 4_666
O34 K9 2.859(18) 1_556
O34 K18 3.12(3) 4_666
O36 K18 3.20(3) 4_666
O36 C1 1.253(19) .
O37 C2 1.39(2) .
O38 K5 2.785(19) 3_657
O38 C1 1.261(19) .
O39 Eu2 2.402(12) 3_657
O39 C4 1.29(2) .
O40 K7 2.852(18) 4_666
O40 C4 1.25(2) .
O41 K7 3.091(18) 2_546
O44 K20 2.78(4) 2_546
O54 K9 2.864(19) 4_566
O59 K11 2.84(2) 1_455
O62 K2 3.046(14) 2_556
O62 K6 3.200(17) 4_566
O64 K6 2.864(15) 4_566
O69 K6 2.887(17) 4_566
O71 K10 2.816(18) 1_556
O71 K16 2.91(3) 1_556
O72 K8 3.409(19) 3_657
O72 K10 3.201(19) 1_556
O73 K16 3.37(3) 1_556
C1 C2 1.49(2) .
C2 H2 0.9800 .
C2 C3 1.45(3) .
C3 K7 3.45(2) 4_666
C3 H3A 0.9700 .
C3 H3B 0.9700 .
C3 C4 1.49(2) .
C4 K7 3.52(2) 4_666
O1W K7 3.124(18) 2_546
O4W K8 2.757(18) 3_657
O4W K9 3.148(18) 1_556
O5W K9 2.816(18) 1_556
O10W K19 2.74(4) 2_556
O11W K9 3.04(3) 4_666
O11W K12 2.39(3) 2_646
O11W K16 3.26(4) 4_666
O11W O23W 1.26(5) .
O12W K12 2.35(4) 1_545
O13W K9 2.94(4) 4_666
O13W K12 2.85(4) 2_646
O15W K18 2.39(5) 4_666
O16W K14 3.00(5) 3_656
O19W K10 3.03(5) 3_666
O21W K1 3.02(4) 4_565
O21W K13 3.31(5) 4_565
O21W K21 2.84(6) 4_565
O22W K10 3.16(4) 1_556
O23W K8 3.28(5) 2_656
O23W K9 3.13(5) 4_666
O23W K12 2.26(5) 2_646
O23W K16 2.42(5) 4_666
O24W K4 2.92(4) 4_565
Li1 K21 3.55(8) 2_656
