#------------------------------------------------------------------------------
#$Date: 2015-07-11 00:39:46 +0300 (Sat, 11 Jul 2015) $
#$Revision: 143578 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/53/7035313.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7035313
loop_
_publ_author_name
'Ma, Pengtao'
'Wan, Rong'
'Si, Yanan'
'Hu, Feng'
'Wang, Yueyan'
'Niu, Jingyang'
'Wang, Jingping'
_publ_section_title
;
 Double-malate bridging tri-lanthanoid cluster encapsulated
 arsenotungstates: syntheses, structures, luminescence and magnetic
 properties.
;
_journal_issue                   25
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              11514
_journal_page_last               11523
_journal_paper_doi               10.1039/c5dt01323b
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         '0.5(C16 H12 As8 K40 Li4 O360 Sm12 W76), O'
_chemical_formula_sum            'C8 H74 As4 K20 Li2 O181 Sm6 W38'
_chemical_formula_weight         12050.63
_chemical_name_systematic
;
 ? 
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2015-05-01
_audit_creation_method
;
Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
;
_audit_update_record
;
2015-05-05 deposited with the CCDC.
2015-06-02 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 112.774(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   21.047(3)
_cell_length_b                   25.429(3)
_cell_length_c                   22.733(3)
_cell_measurement_reflns_used    9162
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      25.78
_cell_measurement_theta_min      2.32
_cell_volume                     11218(3)
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'ShelXS-1997 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296.15
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0648
_diffrn_reflns_av_unetI/netI     0.0822
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            56793
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.87
_diffrn_source                   'fine-focus sealed tube'
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    21.984
_exptl_absorpt_correction_T_max  0.7457
_exptl_absorpt_correction_T_min  0.4939
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.0993 before and 0.0510 after correction.
The Ratio of minimum to maximum transmission is 0.6623.
The λ/2 correction factor is 0.0015.
;
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    3.568
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             10544
_exptl_crystal_preparation       'Magnetic properties, Luminescent'
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.19
_refine_diff_density_max         2.868
_refine_diff_density_min         -1.486
_refine_diff_density_rms         0.335
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.006
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1109
_refine_ls_number_reflns         19695
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.006
_refine_ls_R_factor_all          0.0890
_refine_ls_R_factor_gt           0.0464
_refine_ls_shift/su_max          0.005
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0571P)²+22.7062P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1041
_refine_ls_wR_factor_ref         0.1217
_reflns_number_gt                13030
_reflns_number_total             19695
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5dt01323b2.cif
_cod_data_source_block           1043923
_cod_depositor_comments
'Adding full bibliography for 7035309--7035313.cif.'
_cod_database_code               7035313
_audit_block_doi                 10.5517/cc1418yd
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2. Others
 Fixed Sof: K3(0.5) K4(0.5) K5(0.5) K6(0.5) K7(0.5) K8(0.5) K9(0.5) K10(0.5)
 K11(0.5) K12(0.5) K13(0.5) K14(0.5) K15(0.5) K16(0.25) K17(0.25) K18(0.25)
 K19(0.25) K20(0.25) K21(0.25) O10W(0.5) O11W(0.5) O12W(0.5) O13W(0.5)
 O14W(0.5) O15W(0.5) O16W(0.5) O17W(0.5) O18W(0.5) O19W(0.5) O20W(0.5)
 O21W(0.5) O22W(0.5) O23W(0.5) O24W(0.5)
 Fixed Uiso: O9W(0.10958) O20W(0.10311) O23W(0.11879) O24W(0.11649)
3.a Ternary CH refined with riding coordinates:
 C2(H2)
3.b Secondary CH2 refined with riding coordinates:
 C3(H3A,H3B)
;
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 'x, y, z'
2 '-x+1/2, y+1/2, -z+1/2'
3 '-x, -y, -z'
4 'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags_posn
W1 W 0.66619(4) 0.11237(3) 0.85159(4) 0.02746(18) Uani 1 d .
W2 W 0.58629(4) 0.01323(3) 0.75400(4) 0.02875(18) Uani 1 d .
W3 W 0.66428(4) 0.10985(3) 0.70158(4) 0.0334(2) Uani 1 d .
W4 W 0.42717(4) 0.03348(3) 0.61149(4) 0.03001(19) Uani 1 d .
W5 W 0.50150(4) 0.13061(4) 0.55791(4) 0.0359(2) Uani 1 d .
W6 W 0.35386(4) 0.15280(3) 0.58273(4) 0.03126(19) Uani 1 d .
W7 W 0.58205(4) 0.24168(3) 0.66588(4) 0.0340(2) Uani 1 d .
W8 W 0.43595(4) 0.26081(3) 0.69441(4) 0.03075(19) Uani 1 d .
W9 W 0.58921(4) 0.24524(3) 0.81609(4) 0.02845(18) Uani 1 d .
W10 W 0.53605(4) 0.15888(3) 0.91815(3) 0.02454(17) Uani 1 d .
W11 W 0.18808(4) -0.00384(3) 0.76480(4) 0.02740(18) Uani 1 d .
W12 W 0.12373(4) 0.08945(3) 0.64583(4) 0.03020(19) Uani 1 d .
W13 W 0.02056(4) 0.03483(3) 0.71227(4) 0.0376(2) Uani 1 d .
W14 W 0.08259(4) 0.22208(3) 0.68676(4) 0.0335(2) Uani 1 d .
W15 W -0.02391(4) 0.16810(3) 0.75054(4) 0.0403(2) Uani 1 d .
W16 W 0.10726(4) 0.25083(3) 0.83773(4) 0.0361(2) Uani 1 d .
W17 W 0.04579(4) 0.06657(3) 0.87891(4) 0.0411(2) Uani 1 d .
W18 W 0.17544(4) 0.15173(3) 0.96288(4) 0.0370(2) Uani 1 d .
W19 W 0.21446(4) 0.03075(3) 0.93033(4) 0.03048(19) Uani 1 d .
Sm1 Sm 0.29800(5) 0.05385(4) 0.69930(4) 0.0256(2) Uani 1 d .
Sm2 Sm 0.36797(4) 0.06701(4) 0.87560(4) 0.0234(2) Uani 1 d .
Sm3 Sm 0.27950(5) 0.19575(4) 0.71351(5) 0.0278(2) Uani 1 d .
As1 As 0.49749(9) 0.13262(7) 0.72769(8) 0.0227(4) Uani 1 d .
As2 As 0.16639(9) 0.12815(7) 0.80752(9) 0.0252(4) Uani 1 d .
K1 K 0.7608(3) 0.2331(2) 0.9496(3) 0.0697(16) Uani 1 d .
K2 K 0.5123(4) -0.1056(3) 0.6351(3) 0.114(3) Uani 1 d .
K3 K 0.0742(5) -0.0757(4) 0.8341(5) 0.055(3) Uiso 0.50 d .
K4 K 0.4273(6) 0.2873(5) 0.8587(5) 0.065(3) Uiso 0.50 d .
K5 K 0.1568(6) -0.1127(5) 0.9466(6) 0.073(3) Uiso 0.50 d .
K6 K 0.5848(6) 0.2369(5) 0.4994(6) 0.069(3) Uiso 0.50 d .
K7 K 0.1897(7) 0.3452(5) 0.7532(7) 0.088(4) Uiso 0.50 d .
K8 K 0.5759(7) 0.0056(6) 0.9295(7) 0.094(4) Uiso 0.50 d .
K9 K 0.4464(6) 0.1725(5) 0.0469(6) 0.078(4) Uiso 0.50 d .
K10 K 0.2300(7) 0.0246(5) 0.1038(6) 0.087(4) Uiso 0.50 d .
K11 K 0.7653(9) 0.2282(8) 0.6604(9) 0.136(6) Uiso 0.50 d .
K12 K 0.6226(8) 0.8650(7) 0.8223(8) 0.119(5) Uiso 0.50 d .
K13 K 0.9015(10) 0.2130(9) 1.0144(10) 0.157(7) Uiso 0.50 d .
K14 K 0.6762(10) 0.0758(8) 0.5445(9) 0.143(7) Uiso 0.50 d .
K15 K 0.5836(10) -0.0210(9) 0.5748(10) 0.157(7) Uiso 0.50 d .
K16 K 0.3579(12) 0.0935(10) 0.0755(12) 0.078(7) Uiso 0.25 d .
K17 K -0.0747(14) 0.1311(12) 0.5605(14) 0.098(9) Uiso 0.25 d .
K18 K 0.0939(16) 0.1966(14) 0.5025(16) 0.119(11) Uiso 0.25 d .
K19 K 0.119(2) -0.0607(16) 0.587(2) 0.149(14) Uiso 0.25 d .
K20 K 0.4630(19) 0.3825(16) 0.8230(19) 0.143(13) Uiso 0.25 d .
K21 K 0.7829(18) 0.2227(15) 0.8174(18) 0.130(12) Uiso 0.25 d .
O1 O 0.7404(6) 0.1159(5) 0.9219(6) 0.037(3) Uani 1 d .
O2 O 0.6598(6) 0.0387(5) 0.8326(6) 0.030(3) Uani 1 d .
O3 O 0.7133(6) 0.1197(5) 0.7906(5) 0.030(3) Uani 1 d .
O4 O 0.6515(5) 0.1884(5) 0.8359(5) 0.027(3) Uani 1 d .
O5 O 0.5980(6) 0.1122(5) 0.8806(5) 0.029(3) Uani 1 d .
O6 O 0.5800(5) 0.1029(5) 0.7470(5) 0.027(3) Uani 1 d .
O7 O 0.6104(6) -0.0525(5) 0.7588(6) 0.042(3) Uani 1 d .
O8 O 0.5235(6) 0.0152(5) 0.7873(6) 0.036(3) Uani 1 d .
O9 O 0.6538(6) 0.0389(5) 0.7135(6) 0.036(3) Uani 1 d .
O10 O 0.5178(6) 0.0149(5) 0.6672(5) 0.033(3) Uani 1 d .
O11 O 0.7319(7) 0.1088(6) 0.6785(7) 0.048(4) Uani 1 d .
O12 O 0.5886(6) 0.1089(5) 0.6212(6) 0.039(3) Uani 1 d .
O13 O 0.6456(6) 0.1859(5) 0.6984(6) 0.040(3) Uani 1 d .
O14 O 0.3987(7) -0.0247(5) 0.5710(6) 0.050(4) Uani 1 d .
O15 O 0.3916(6) 0.0338(5) 0.6713(6) 0.033(3) Uani 1 d .
O16 O 0.4710(6) 0.0619(5) 0.5509(5) 0.036(3) Uani 1 d .
O17 O 0.3519(6) 0.0797(5) 0.5591(5) 0.031(3) Uani 1 d .
O18 O 0.4620(5) 0.1194(4) 0.6437(5) 0.024(3) Uani 1 d .
O19 O 0.5195(7) 0.1362(6) 0.4904(6) 0.047(4) Uani 1 d .
O20 O 0.4136(6) 0.1582(5) 0.5296(5) 0.034(3) Uani 1 d .
O21 O 0.5336(6) 0.2008(5) 0.5952(6) 0.040(3) Uani 1 d .
O22 O 0.2796(6) 0.1740(6) 0.5213(6) 0.044(4) Uani 1 d .
O23 O 0.3277(6) 0.1376(5) 0.6475(6) 0.031(3) Uani 1 d .
O24 O 0.3940(6) 0.2181(5) 0.6181(6) 0.040(3) Uani 1 d .
O25 O 0.6265(7) 0.2821(6) 0.6348(6) 0.048(4) Uani 1 d .
O26 O 0.5046(6) 0.2817(5) 0.6551(6) 0.033(3) Uani 1 d .
O27 O 0.6221(6) 0.2691(5) 0.7549(6) 0.037(3) Uani 1 d .
O28 O 0.5226(6) 0.1993(4) 0.7221(6) 0.027(3) Uani 1 d .
O29 O 0.3873(6) 0.3188(5) 0.6730(7) 0.049(4) Uani 1 d .
O30 O 0.3934(6) 0.2229(5) 0.7339(6) 0.036(3) Uani 1 d .
O31 O 0.5067(6) 0.2855(5) 0.7750(5) 0.030(3) Uani 1 d .
O32 O 0.6334(6) 0.2868(5) 0.8778(6) 0.040(3) Uani 1 d .
O33 O 0.5354(5) 0.2045(4) 0.8525(5) 0.027(3) Uani 1 d .
O34 O 0.4992(7) 0.2025(5) 0.9540(7) 0.047(4) Uani 1 d .
O35 O 0.4680(6) 0.1152(5) 0.8822(5) 0.030(3) Uani 1 d .
O36 O 0.6373(6) 0.1910(5) 0.9695(5) 0.030(3) Uani 1 d .
O37 O 0.5759(6) 0.1115(5) 0.9910(6) 0.033(3) Uani 1 d .
O38 O 0.7376(6) 0.1802(6) 1.0524(7) 0.051(4) Uani 1 d .
O39 O 0.6224(7) 0.0250(5) 1.0953(6) 0.039(3) Uani 1 d .
O40 O 0.6109(7) 0.0751(5) 1.1711(7) 0.048(4) Uani 1 d .
O41 O 0.2152(6) -0.0664(5) 0.7592(6) 0.036(3) Uani 1 d .
O42 O 0.2694(5) 0.0348(4) 0.7896(6) 0.027(3) Uani 1 d .
O43 O 0.1740(5) 0.0219(5) 0.6781(5) 0.029(3) Uani 1 d .
O44 O 0.0897(6) -0.0190(5) 0.7291(6) 0.035(3) Uani 1 d .
O45 O 0.1872(6) -0.0030(5) 0.8466(6) 0.032(3) Uani 1 d .
O46 O 0.1294(6) 0.0776(5) 0.7506(6) 0.034(3) Uani 1 d .
O47 O 0.1124(6) 0.0850(5) 0.5656(6) 0.043(4) Uani 1 d .
O48 O 0.2101(6) 0.1201(5) 0.6817(5) 0.031(3) Uani 1 d .
O49 O 0.0416(6) 0.0502(5) 0.6389(6) 0.037(3) Uani 1 d .
O50 O 0.0802(6) 0.1531(5) 0.6477(6) 0.033(3) Uani 1 d .
O51 O -0.0529(6) -0.0028(5) 0.6766(7) 0.052(4) Uani 1 d .
O52 O -0.0175(6) 0.1027(5) 0.7084(6) 0.041(3) Uani 1 d .
O53 O 0.0314(6) 0.0324(5) 0.7980(7) 0.047(4) Uani 1 d .
O54 O 0.0571(7) 0.2618(6) 0.6198(7) 0.054(4) Uani 1 d .
O55 O -0.0125(6) 0.2022(5) 0.6813(6) 0.044(4) Uani 1 d .
O56 O 0.1733(6) 0.2204(5) 0.7157(6) 0.033(3) Uani 1 d .
O57 O 0.0804(6) 0.2728(5) 0.7484(6) 0.035(3) Uani 1 d .
O58 O 0.0963(6) 0.1739(5) 0.7791(6) 0.032(3) Uani 1 d .
O59 O -0.1134(7) 0.1708(6) 0.7266(8) 0.062(5) Uani 1 d .
O60 O 0.0046(6) 0.2273(5) 0.8018(7) 0.046(4) Uani 1 d .
O61 O -0.0005(6) 0.1226(5) 0.8236(6) 0.041(3) Uani 1 d .
O62 O 0.0917(7) 0.3087(5) 0.8700(7) 0.050(4) Uani 1 d .
O63 O 0.1950(7) 0.2529(5) 0.8517(6) 0.039(3) Uani 1 d .
O64 O 0.1169(6) 0.2040(5) 0.9067(6) 0.039(3) Uani 1 d .
O65 O -0.0206(7) 0.0398(6) 0.8949(8) 0.061(5) Uani 1 d .
O66 O 0.0826(7) 0.1123(5) 0.9465(7) 0.048(4) Uani 1 d .
O67 O 0.1152(6) 0.0169(5) 0.9165(6) 0.040(3) Uani 1 d .
O68 O 0.1489(5) 0.1013(5) 0.8728(6) 0.031(3) Uani 1 d .
O69 O 0.1833(8) 0.1776(6) 1.0363(6) 0.054(4) Uani 1 d .
O70 O 0.2519(6) 0.1713(5) 0.9548(6) 0.041(3) Uani 1 d .
O71 O 0.2122(6) 0.0804(5) 0.9921(6) 0.034(3) Uani 1 d .
O72 O 0.2495(7) -0.0215(6) 0.9820(6) 0.048(4) Uani 1 d .
O73 O 0.2860(6) 0.0605(5) 0.9201(5) 0.029(3) Uani 1 d .
O74 O 0.3439(5) 0.1227(4) 0.7786(5) 0.024(3) Uani 1 d .
C1 C 0.6764(10) 0.1661(8) 1.0198(9) 0.037(5) Uani 1 d .
C2 C 0.6449(10) 0.1153(9) 1.0352(10) 0.055(7) Uani 1 d .
H2 H 0.6705 0.0850 1.0291 0.066 Uiso 1 calc R
C3 C 0.6511(10) 0.1158(8) 1.0998(9) 0.042(5) Uani 1 d .
H3A H 0.6267 0.1464 1.1058 0.050 Uiso 1 calc R
H3B H 0.6994 0.1205 1.1268 0.050 Uiso 1 calc R
C4 C 0.6255(9) 0.0691(8) 1.1228(10) 0.034(5) Uani 1 d .
O1W O 0.2973(6) -0.0437(5) 0.6866(6) 0.043(3) Uiso 1 d .
O2W O 0.2420(6) 0.0399(5) 0.5810(6) 0.041(3) Uiso 1 d .
O3W O 0.4015(5) 0.0194(4) 0.7963(5) 0.023(3) Uiso 1 d .
O4W O 0.4569(6) 0.0607(5) 0.9870(6) 0.039(3) Uiso 1 d .
O5W O 0.3566(6) 0.1540(5) 0.9198(6) 0.043(4) Uiso 1 d .
O6W O 0.2794(7) 0.2945(6) 0.7109(7) 0.053(4) Uiso 1 d .
O7W O 0.3051(6) 0.2277(5) 0.8234(6) 0.040(3) Uiso 1 d .
O8W O 0.2180(8) 0.2238(6) 0.6035(7) 0.063(4) Uiso 1 d .
O9W O 0.4332(11) -0.0846(9) 0.7071(10) 0.110 Uiso 1 d .
O10W O 0.3083(15) 0.3484(13) 0.8741(15) 0.066(9) Uiso 0.50 d .
O11W O 0.9982(13) 0.3581(11) 0.6874(13) 0.048(7) Uiso 0.50 d .
O12W O 0.5883(16) -0.1851(13) 0.7265(15) 0.066(9) Uiso 0.50 d .
O13W O 0.8718(16) 0.2719(13) 0.6163(16) 0.070(10) Uiso 0.50 d .
O14W O 0.2933(17) 0.2800(14) 0.9790(17) 0.079(11) Uiso 0.50 d .
O15W O 0.6428(17) 0.3703(14) 0.9639(17) 0.080(11) Uiso 0.50 d .
O16W O 0.301(2) -0.104(2) 0.580(2) 0.133(17) Uiso 0.50 d .
O17W O 0.854(2) 0.1040(18) 0.825(2) 0.113(14) Uiso 0.50 d .
O18W O 0.830(2) 0.0783(18) 0.636(2) 0.114(15) Uiso 0.50 d .
O19W O 0.7379(19) 0.8634(16) 0.8373(19) 0.097(13) Uiso 0.50 d .
O20W O 0.711(2) -0.0511(17) 0.683(2) 0.103 Uiso 0.50 d .
O21W O 0.348(2) 0.1875(19) 0.404(2) 0.127(16) Uiso 0.50 d .
O22W O 0.107(2) -0.0438(19) 1.021(2) 0.124(16) Uiso 0.50 d .
O23W O 0.972(2) 0.4031(19) 0.663(2) 0.119 Uiso 0.50 d .
O24W O -0.017(2) 0.1954(18) 0.493(2) 0.116 Uiso 0.50 d .
Li1 Li 0.778(3) 0.850(3) 0.725(3) 0.13(2) Uiso 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sm Sm -0.1638 3.4418 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
K1 W1 K8 120.0(2) . .
K1 W1 K10 115.7(2) . 3_656
K1 W1 K21 48.4(5) . .
K10 W1 K8 67.3(3) 3_656 .
K21 W1 K8 166.8(6) . .
K21 W1 K10 110.0(6) . 3_656
O1 W1 K1 49.8(4) . .
O1 W1 K8 92.2(5) . .
O1 W1 K10 67.0(5) . 3_656
O1 W1 K21 75.2(7) . .
O1 W1 O2 102.4(5) . .
O1 W1 O3 97.0(5) . .
O1 W1 O4 97.9(5) . .
O1 W1 O5 102.8(5) . .
O1 W1 O6 169.2(5) . .
O2 W1 K1 152.0(4) . .
O2 W1 K8 56.3(4) . .
O2 W1 K10 36.4(4) . 3_656
O2 W1 K21 129.6(6) . .
O2 W1 O3 86.8(5) . .
O2 W1 O4 158.0(5) . .
O2 W1 O6 73.5(4) . .
O3 W1 K1 92.5(4) . .
O3 W1 K8 143.1(4) . .
O3 W1 K10 83.6(4) . 3_656
O3 W1 K21 45.1(6) . .
O3 W1 O6 73.0(4) . .
O4 W1 K1 48.2(3) . .
O4 W1 K8 131.6(4) . .
O4 W1 K10 158.0(4) . 3_656
O4 W1 K21 48.8(6) . .
O4 W1 O3 82.4(5) . .
O4 W1 O6 85.0(4) . .
O5 W1 K1 95.5(4) . .
O5 W1 K8 43.0(4) . .
O5 W1 K10 109.8(4) . 3_656
O5 W1 K21 135.3(7) . .
O5 W1 O2 94.9(5) . .
O5 W1 O3 159.3(5) . .
O5 W1 O4 88.7(5) . .
O5 W1 O6 87.6(4) . .
O6 W1 K1 132.9(3) . .
O6 W1 K8 93.6(3) . .
O6 W1 K10 107.1(3) . 3_656
O6 W1 K21 99.5(6) . .
K2 W2 K8 118.4(2) . .
K2 W2 K10 111.3(2) . 3_656
K2 W2 K12 60.9(3) . 1_545
K10 W2 K8 66.9(3) 3_656 .
K12 W2 K8 69.7(3) 1_545 .
K12 W2 K10 59.6(3) 1_545 3_656
O2 W2 K2 146.8(4) . .
O2 W2 K8 56.6(4) . .
O2 W2 K10 35.6(4) . 3_656
O2 W2 K12 89.6(4) . 1_545
O2 W2 O6 74.9(4) . .
O2 W2 O9 82.3(5) . .
O6 W2 K2 135.9(3) . .
O6 W2 K8 95.3(3) . .
O6 W2 K10 107.6(3) . 3_656
O6 W2 K12 162.9(4) . 1_545
O7 W2 K2 48.3(4) . .
O7 W2 K8 91.0(5) . .
O7 W2 K10 63.9(5) . 3_656
O7 W2 K12 21.6(5) . 1_545
O7 W2 O2 98.8(5) . .
O7 W2 O6 166.2(5) . .
O7 W2 O8 104.5(6) . .
O7 W2 O9 95.5(6) . .
O7 W2 O10 99.7(6) . .
O8 W2 K2 98.8(4) . .
O8 W2 K8 41.2(4) . .
O8 W2 K10 107.7(4) . 3_656
O8 W2 K12 85.6(5) . 1_545
O8 W2 O2 93.3(5) . .
O8 W2 O6 88.2(5) . .
O8 W2 O9 160.0(5) . .
O8 W2 O10 92.9(5) . .
O9 W2 K2 95.3(4) . .
O9 W2 K8 138.9(4) . .
O9 W2 K10 79.9(4) . 3_656
O9 W2 K12 113.8(4) . 1_545
O9 W2 O6 71.8(4) . .
O10 W2 K2 51.7(4) . .
O10 W2 K8 134.0(4) . .
O10 W2 K10 156.0(4) . 3_656
O10 W2 K12 111.5(4) . 1_545
O10 W2 O2 158.4(5) . .
O10 W2 O6 84.7(5) . .
O10 W2 O9 84.8(5) . .
K11 W3 K21 50.8(6) . .
K14 W3 K11 73.4(4) . .
K14 W3 K21 121.9(6) . .
O3 W3 K11 91.8(5) . .
O3 W3 K14 146.2(4) . .
O3 W3 K21 43.0(6) . .
O3 W3 O6 74.7(4) . .
O3 W3 O12 158.7(5) . .
O3 W3 O13 85.9(5) . .
O6 W3 K11 135.3(4) . .
O6 W3 K14 136.6(4) . .
O6 W3 K21 98.4(6) . .
O9 W3 K11 150.7(5) . .
O9 W3 K14 88.3(5) . .
O9 W3 K21 132.6(7) . .
O9 W3 O3 91.1(5) . .
O9 W3 O6 73.3(5) . .
O9 W3 O12 91.4(6) . .
O9 W3 O13 158.4(5) . .
O11 W3 K11 49.8(6) . .
O11 W3 K14 48.2(6) . .
O11 W3 K21 80.3(7) . .
O11 W3 O3 99.1(6) . .
O11 W3 O6 171.2(5) . .
O11 W3 O9 101.0(6) . .
O11 W3 O12 101.2(6) . .
O11 W3 O13 100.6(6) . .
O12 W3 K11 96.2(5) . .
O12 W3 K14 55.0(5) . .
O12 W3 K21 135.3(7) . .
O12 W3 O6 85.9(4) . .
O12 W3 O13 84.0(6) . .
O13 W3 K11 50.9(4) . .
O13 W3 K14 106.0(5) . .
O13 W3 K21 52.4(6) . .
O13 W3 O6 85.2(4) . .
K2 W4 K15 48.4(3) . .
O10 W4 K2 52.6(4) . .
O10 W4 K15 49.3(5) . .
O10 W4 O16 86.6(5) . .
O10 W4 O17 157.2(5) . .
O10 W4 O18 84.9(5) . .
O14 W4 K2 48.8(5) . .
O14 W4 K15 74.4(6) . .
O14 W4 O10 101.2(6) . .
O14 W4 O15 104.4(6) . .
O14 W4 O16 95.6(6) . .
O14 W4 O17 99.1(6) . .
O14 W4 O18 167.2(5) . .
O15 W4 K2 101.8(4) . .
O15 W4 K15 142.4(5) . .
O15 W4 O10 95.9(5) . .
O15 W4 O16 158.9(5) . .
O15 W4 O17 88.9(5) . .
O15 W4 O18 86.0(5) . .
O16 W4 K2 96.3(4) . .
O16 W4 K15 50.0(5) . .
O16 W4 O18 73.4(4) . .
O17 W4 K2 147.7(4) . .
O17 W4 K15 128.7(4) . .
O17 W4 O16 81.3(5) . .
O17 W4 O18 73.2(4) . .
O18 W4 K2 137.2(3) . .
O18 W4 K15 102.1(4) . .
K6 W5 K14 70.0(3) . .
K6 W5 K15 111.8(4) . 3_656
K15 W5 K14 81.8(4) 3_656 .
O12 W5 K6 91.8(4) . .
O12 W5 K14 47.7(5) . .
O12 W5 K15 112.6(5) . 3_656
O12 W5 O18 83.6(4) . .
O12 W5 O21 82.5(5) . .
O16 W5 K6 148.1(4) . .
O16 W5 K14 87.9(5) . .
O16 W5 K15 40.0(5) . 3_656
O16 W5 O12 89.6(5) . .
O16 W5 O18 75.0(5) . .
O16 W5 O20 93.5(5) . .
O16 W5 O21 160.1(5) . .
O18 W5 K6 136.8(3) . .
O18 W5 K14 128.8(4) . .
O18 W5 K15 109.5(4) . 3_656
O19 W5 K6 47.8(5) . .
O19 W5 K14 56.1(5) . .
O19 W5 K15 64.7(6) . 3_656
O19 W5 O12 102.5(6) . .
O19 W5 O16 100.9(6) . .
O19 W5 O18 172.8(5) . .
O19 W5 O20 101.2(6) . .
O19 W5 O21 98.7(6) . .
O20 W5 K6 98.4(4) . .
O20 W5 K14 157.0(4) . .
O20 W5 K15 84.6(5) . 3_656
O20 W5 O12 155.1(5) . .
O20 W5 O18 73.4(4) . .
O20 W5 O21 86.4(5) . .
O21 W5 K6 50.9(4) . .
O21 W5 K14 99.9(5) . .
O21 W5 K15 159.0(5) . 3_656
O21 W5 O18 85.9(5) . .
K13 W6 K1 40.2(3) 4_565 4_565
O17 W6 K1 121.5(3) . 4_565
O17 W6 K13 133.6(5) . 4_565
O17 W6 O18 74.0(4) . .
O17 W6 O20 81.6(5) . .
O18 W6 K1 141.1(3) . 4_565
O18 W6 K13 102.0(4) . 4_565
O20 W6 K1 75.3(3) . 4_565
O20 W6 K13 54.4(5) . 4_565
O20 W6 O18 72.2(4) . .
O22 W6 K1 32.8(5) . 4_565
O22 W6 K13 72.9(5) . 4_565
O22 W6 O17 99.2(6) . .
O22 W6 O18 165.3(5) . .
O22 W6 O20 94.1(5) . .
O22 W6 O23 105.1(6) . .
O22 W6 O24 100.6(6) . .
O23 W6 K1 123.0(4) . 4_565
O23 W6 K13 134.1(5) . 4_565
O23 W6 O17 92.3(5) . .
O23 W6 O18 88.4(5) . .
O23 W6 O20 160.6(5) . .
O23 W6 O24 93.9(5) . .
O24 W6 K1 72.6(4) . 4_565
O24 W6 K13 44.4(5) . 4_565
O24 W6 O17 156.9(5) . .
O24 W6 O18 83.9(4) . .
O24 W6 O20 85.3(5) . .
K6 W7 K11 64.7(3) . .
O13 W7 K6 94.9(4) . .
O13 W7 K11 52.6(5) . .
O13 W7 O27 84.8(5) . .
O13 W7 O28 83.6(4) . .
O21 W7 K6 48.3(4) . .
O21 W7 K11 98.1(5) . .
O21 W7 O13 89.3(6) . .
O21 W7 O26 91.9(6) . .
O21 W7 O27 162.1(5) . .
O21 W7 O28 89.1(5) . .
O25 W7 K6 52.4(5) . .
O25 W7 K11 48.6(5) . .
O25 W7 O13 101.2(6) . .
O25 W7 O21 100.6(6) . .
O25 W7 O26 102.0(6) . .
O25 W7 O27 97.2(6) . .
O25 W7 O28 169.2(6) . .
O26 W7 K6 103.7(4) . .
O26 W7 K11 150.3(5) . .
O26 W7 O13 156.0(5) . .
O26 W7 O27 86.9(5) . .
O26 W7 O28 72.5(4) . .
O27 W7 K6 149.0(4) . .
O27 W7 K11 91.6(5) . .
O27 W7 O28 73.4(4) . .
O28 W7 K6 137.5(3) . .
O28 W7 K11 135.2(4) . .
K4 W8 K13 156.7(4) . 4_565
O24 W8 K4 141.6(4) . .
O24 W8 K13 47.8(5) . 4_565
O24 W8 O26 84.8(5) . .
O24 W8 O28 84.4(5) . .
O24 W8 O31 158.3(5) . .
O26 W8 K4 133.1(4) . .
O26 W8 K13 51.4(4) . 4_565
O26 W8 O28 71.1(4) . .
O28 W8 K4 100.5(3) . .
O28 W8 K13 102.0(4) . 4_565
O29 W8 K4 83.2(5) . .
O29 W8 K13 73.4(6) . 4_565
O29 W8 O24 101.9(6) . .
O29 W8 O26 95.5(6) . .
O29 W8 O28 164.8(5) . .
O29 W8 O30 104.0(6) . .
O29 W8 O31 98.1(6) . .
O30 W8 K4 52.1(4) . .
O30 W8 K13 133.8(5) . 4_565
O30 W8 O24 90.2(6) . .
O30 W8 O26 160.5(5) . .
O30 W8 O28 89.6(5) . .
O30 W8 O31 92.9(5) . .
O31 W8 K4 49.2(4) . .
O31 W8 K13 133.3(5) . 4_565
O31 W8 O26 85.1(5) . .
O31 W8 O28 74.2(4) . .
K1 W9 K4 117.99(19) . .
K1 W9 K21 48.4(5) . .
K4 W9 K21 164.7(5) . .
O4 W9 K1 51.4(3) . .
O4 W9 K4 136.1(4) . .
O4 W9 K21 45.1(6) . .
O4 W9 O28 87.2(4) . .
O4 W9 O31 160.1(5) . .
O4 W9 O33 87.4(5) . .
O27 W9 K1 96.4(4) . .
O27 W9 K4 132.9(4) . .
O27 W9 K21 53.2(6) . .
O27 W9 O4 90.2(5) . .
O27 W9 O28 75.5(5) . .
O27 W9 O31 89.4(5) . .
O27 W9 O33 158.7(5) . .
O28 W9 K1 138.2(3) . .
O28 W9 K4 95.0(3) . .
O28 W9 K21 100.2(6) . .
O31 W9 K1 148.3(4) . .
O31 W9 K4 44.4(4) . .
O31 W9 K21 141.9(6) . .
O31 W9 O28 73.5(4) . .
O31 W9 O33 85.7(5) . .
O32 W9 K1 48.4(4) . .
O32 W9 K4 83.2(5) . .
O32 W9 K21 81.8(7) . .
O32 W9 O4 99.8(5) . .
O32 W9 O27 99.6(6) . .
O32 W9 O28 171.6(5) . .
O32 W9 O31 99.9(6) . .
O32 W9 O33 101.6(5) . .
O33 W9 K1 98.6(3) . .
O33 W9 K4 49.6(4) . .
O33 W9 K21 131.6(6) . .
O33 W9 O28 83.2(4) . .
K4 W10 K8 157.0(3) . .
K4 W10 K9 78.8(2) . 1_556
K4 W10 K18 56.1(5) . 4_666
K8 W10 K9 100.5(3) . 1_556
K8 W10 K18 146.1(5) . 4_666
K9 W10 K18 73.9(5) 1_556 4_666
O5 W10 K4 132.9(3) . .
O5 W10 K8 49.0(4) . .
O5 W10 K9 148.0(4) . 1_556
O5 W10 K18 124.0(6) . 4_666
O33 W10 K4 52.4(4) . .
O33 W10 K8 126.3(4) . .
O33 W10 K9 130.8(4) . 1_556
O33 W10 K18 74.3(6) . 4_666
O33 W10 O5 81.2(5) . .
O33 W10 O36 84.2(4) . .
O33 W10 O37 156.7(5) . .
O34 W10 K4 47.0(5) . .
O34 W10 K8 136.1(5) . .
O34 W10 K9 35.6(5) . 1_556
O34 W10 K18 46.5(7) . 4_666
O34 W10 O5 170.2(5) . .
O34 W10 O33 96.4(6) . .
O34 W10 O35 101.1(6) . .
O34 W10 O36 91.8(6) . .
O34 W10 O37 96.9(6) . .
O35 W10 K4 96.1(4) . .
O35 W10 K8 61.3(4) . .
O35 W10 K9 82.3(4) . 1_556
O35 W10 K18 146.1(6) . 4_666
O35 W10 O5 88.6(5) . .
O35 W10 O33 105.5(5) . .
O35 W10 O36 162.7(5) . .
O35 W10 O37 90.6(5) . .
O36 W10 K4 101.2(4) . .
O36 W10 K8 101.4(4) . .
O36 W10 K9 102.4(4) . 1_556
O36 W10 K18 49.8(6) . 4_666
O36 W10 O5 78.6(4) . .
O37 W10 K4 143.9(4) . .
O37 W10 K8 48.0(4) . .
O37 W10 K9 67.0(4) . 1_556
O37 W10 K18 101.7(6) . 4_666
O37 W10 O5 82.5(5) . .
O37 W10 O36 76.4(4) . .
Sm1 W11 K3 175.93(16) . .
Sm1 W11 K19 76.5(6) . .
K3 W11 K19 101.7(6) . .
O41 W11 Sm1 93.6(4) . .
O41 W11 K3 82.3(4) . .
O41 W11 K19 65.8(7) . .
O41 W11 O42 102.6(5) . .
O41 W11 O43 99.1(5) . .
O41 W11 O44 96.7(5) . .
O41 W11 O45 102.5(6) . .
O41 W11 O46 166.9(5) . .
O42 W11 Sm1 39.6(4) . .
O42 W11 K3 141.3(4) . .
O42 W11 K19 115.4(7) . .
O42 W11 O43 83.9(5) . .
O42 W11 O44 159.3(5) . .
O42 W11 O45 93.1(5) . .
O42 W11 O46 87.1(4) . .
O43 W11 Sm1 46.6(3) . .
O43 W11 K3 133.8(4) . .
O43 W11 K19 42.4(7) . .
O43 W11 O46 73.0(5) . .
O44 W11 Sm1 132.3(4) . .
O44 W11 K3 48.7(4) . .
O44 W11 K19 66.0(7) . .
O44 W11 O43 85.7(5) . .
O44 W11 O46 72.7(4) . .
O45 W11 Sm1 132.7(4) . .
O45 W11 K3 48.9(4) . .
O45 W11 K19 150.5(7) . .
O45 W11 O43 158.3(5) . .
O45 W11 O44 90.0(5) . .
O45 W11 O46 85.4(5) . .
O46 W11 Sm1 88.3(3) . .
O46 W11 K3 95.6(3) . .
O46 W11 K19 102.3(7) . .
Sm1 W12 K17 172.0(4) . .
Sm1 W12 K18 105.3(5) . .
Sm1 W12 K19 76.1(6) . .
K17 W12 K18 68.3(6) . .
K17 W12 K19 101.7(7) . .
K19 W12 K18 113.0(8) . .
O43 W12 Sm1 47.0(3) . .
O43 W12 K17 135.1(5) . .
O43 W12 K18 139.2(6) . .
O43 W12 K19 41.4(7) . .
O43 W12 O46 73.0(4) . .
O46 W12 Sm1 88.8(3) . .
O46 W12 K17 99.2(5) . .
O46 W12 K18 145.0(6) . .
O46 W12 K19 101.3(7) . .
O47 W12 Sm1 92.7(4) . .
O47 W12 K17 79.4(6) . .
O47 W12 K18 45.5(7) . .
O47 W12 K19 67.6(7) . .
O47 W12 O43 99.5(5) . .
O47 W12 O46 168.0(5) . .
O47 W12 O48 101.6(6) . .
O47 W12 O49 97.1(6) . .
O47 W12 O50 102.1(6) . .
O48 W12 Sm1 40.5(4) . .
O48 W12 K17 139.8(6) . .
O48 W12 K18 83.9(6) . .
O48 W12 K19 116.0(7) . .
O48 W12 O43 84.9(5) . .
O48 W12 O46 87.2(5) . .
O48 W12 O49 160.0(5) . .
O48 W12 O50 91.9(5) . .
O49 W12 Sm1 132.2(4) . .
O49 W12 K17 51.0(6) . .
O49 W12 K18 114.7(6) . .
O49 W12 K19 65.2(7) . .
O49 W12 O43 85.2(5) . .
O49 W12 O46 73.3(5) . .
O50 W12 Sm1 132.2(4) . .
O50 W12 K17 49.7(6) . .
O50 W12 K18 61.1(6) . .
O50 W12 K19 151.4(7) . .
O50 W12 O43 158.3(5) . .
O50 W12 O46 85.5(5) . .
O50 W12 O49 91.0(5) . .
K3 W13 K17 166.7(4) . .
K3 W13 K20 53.5(6) . 2_546
K20 W13 K17 117.7(7) 2_546 .
O44 W13 K3 48.8(4) . .
O44 W13 K17 133.0(6) . .
O44 W13 K20 39.9(6) . 2_546
O44 W13 O46 72.9(4) . .
O46 W13 K3 95.7(3) . .
O46 W13 K17 97.1(5) . .
O46 W13 K20 111.8(6) . 2_546
O49 W13 K3 132.8(4) . .
O49 W13 K17 49.2(5) . .
O49 W13 K20 87.5(7) . 2_546
O49 W13 O44 84.6(5) . .
O49 W13 O46 73.2(5) . .
O51 W13 K3 83.8(5) . .
O51 W13 K17 83.0(6) . .
O51 W13 K20 60.1(7) . 2_546
O51 W13 O44 99.8(6) . .
O51 W13 O46 170.0(6) . .
O51 W13 O49 99.8(6) . .
O51 W13 O52 101.4(6) . .
O51 W13 O53 101.3(6) . .
O52 W13 K3 135.3(4) . .
O52 W13 K17 49.5(6) . .
O52 W13 K20 160.6(6) . 2_546
O52 W13 O44 158.8(5) . .
O52 W13 O46 86.0(5) . .
O52 W13 O49 90.6(6) . .
O53 W13 K3 48.3(4) . .
O53 W13 K17 136.4(6) . .
O53 W13 K20 101.0(7) . 2_546
O53 W13 O44 89.5(6) . .
O53 W13 O46 85.6(5) . .
O53 W13 O49 158.8(5) . .
O53 W13 O52 87.6(6) . .
O50 W14 K7 145.4(4) . .
O50 W14 O55 84.1(5) . .
O50 W14 O58 84.9(5) . .
O54 W14 K7 78.7(5) . .
O54 W14 O50 100.4(6) . .
O54 W14 O55 97.4(6) . .
O54 W14 O56 105.4(6) . .
O54 W14 O57 99.4(6) . .
O54 W14 O58 168.3(6) . .
O55 W14 K7 130.5(4) . .
O55 W14 O58 72.6(4) . .
O56 W14 K7 58.9(4) . .
O56 W14 O50 88.9(5) . .
O56 W14 O55 157.0(5) . .
O56 W14 O57 94.2(5) . .
O56 W14 O58 85.0(5) . .
O57 W14 K7 48.4(4) . .
O57 W14 O50 158.4(5) . .
O57 W14 O55 84.8(5) . .
O57 W14 O58 74.2(5) . .
O58 W14 K7 103.0(4) . .
O52 W15 K17 48.1(6) . .
O52 W15 O58 85.3(5) . .
O55 W15 K17 45.6(6) . .
O55 W15 O52 85.8(6) . .
O55 W15 O58 74.5(5) . .
O55 W15 O61 157.0(5) . .
O58 W15 K17 96.8(5) . .
O59 W15 K17 82.6(7) . .
O59 W15 O52 98.7(6) . .
O59 W15 O55 101.0(6) . .
O59 W15 O58 173.9(6) . .
O59 W15 O60 102.2(7) . .
O59 W15 O61 100.2(6) . .
O60 W15 K17 136.9(6) . .
O60 W15 O52 159.0(5) . .
O60 W15 O55 92.1(6) . .
O60 W15 O58 74.1(5) . .
O60 W15 O61 91.9(6) . .
O61 W15 K17 129.8(6) . .
O61 W15 O52 82.4(6) . .
O61 W15 O58 84.9(5) . .
K7 W16 K6 131.2(3) . 4_566
O57 W16 K6 149.4(4) . 4_566
O57 W16 K7 47.0(4) . .
O57 W16 O58 73.9(5) . .
O57 W16 O60 80.6(5) . .
O58 W16 K6 125.9(4) . 4_566
O58 W16 K7 101.6(4) . .
O60 W16 K6 84.6(4) . 4_566
O60 W16 K7 125.4(4) . .
O60 W16 O58 71.1(5) . .
O62 W16 K6 54.6(5) . 4_566
O62 W16 K7 83.0(5) . .
O62 W16 O57 99.8(6) . .
O62 W16 O58 164.6(5) . .
O62 W16 O60 94.2(6) . .
O62 W16 O63 104.9(6) . .
O62 W16 O64 99.2(6) . .
O63 W16 K6 109.4(5) . 4_566
O63 W16 K7 55.1(4) . .
O63 W16 O57 92.3(6) . .
O63 W16 O58 89.6(5) . .
O63 W16 O60 160.6(6) . .
O63 W16 O64 95.7(5) . .
O64 W16 K6 44.8(4) . 4_566
O64 W16 K7 149.8(4) . .
O64 W16 O57 156.7(5) . .
O64 W16 O58 84.3(5) . .
O64 W16 O60 84.7(5) . .
O53 W17 K3 46.9(4) . .
O53 W17 O68 85.6(5) . .
O61 W17 K3 128.2(4) . .
O61 W17 O53 81.8(6) . .
O61 W17 O68 85.9(5) . .
O65 W17 K3 84.6(5) . .
O65 W17 O53 100.4(7) . .
O65 W17 O61 100.8(6) . .
O65 W17 O66 100.8(7) . .
O65 W17 O67 101.0(6) . .
O65 W17 O68 171.5(6) . .
O66 W17 K3 138.8(4) . .
O66 W17 O53 158.5(5) . .
O66 W17 O61 91.2(6) . .
O66 W17 O67 92.5(6) . .
O66 W17 O68 73.6(5) . .
O67 W17 K3 46.8(4) . .
O67 W17 O53 86.5(6) . .
O67 W17 O61 156.8(5) . .
O67 W17 O68 73.2(5) . .
O68 W17 K3 95.4(3) . .
K6 W18 K16 126.5(4) 4_566 1_556
O64 W18 K6 50.5(4) . 4_566
O64 W18 K16 153.3(5) . 1_556
O64 W18 O66 84.2(5) . .
O64 W18 O68 85.5(5) . .
O64 W18 O71 157.1(5) . .
O66 W18 K6 83.0(4) . 4_566
O66 W18 K16 122.4(5) . 1_556
O66 W18 O68 71.7(5) . .
O68 W18 K6 131.5(3) . 4_566
O68 W18 K16 101.9(5) . 1_556
O69 W18 K6 50.1(5) . 4_566
O69 W18 K16 79.3(6) . 1_556
O69 W18 O64 100.0(6) . .
O69 W18 O66 95.0(6) . .
O69 W18 O68 165.2(6) . .
O69 W18 O70 104.0(7) . .
O69 W18 O71 98.3(6) . .
O70 W18 K6 112.3(5) . 4_566
O70 W18 K16 58.6(6) . 1_556
O70 W18 O64 96.4(6) . .
O70 W18 O66 160.6(6) . .
O70 W18 O68 88.9(5) . .
O70 W18 O71 92.3(6) . .
O71 W18 K6 142.8(4) . 4_566
O71 W18 K16 44.8(5) . 1_556
O71 W18 O66 80.7(5) . .
O71 W18 O68 73.5(5) . .
K5 W19 K3 39.2(2) . .
K10 W19 K3 106.7(3) 1_556 .
K10 W19 K5 76.7(3) 1_556 .
K10 W19 K16 53.8(4) 1_556 1_556
K16 W19 K3 157.2(4) 1_556 .
K16 W19 K5 118.3(4) 1_556 .
O45 W19 K3 45.0(4) . .
O45 W19 K5 72.5(4) . .
O45 W19 K10 149.1(4) . 1_556
O45 W19 K16 148.3(5) . 1_556
O45 W19 O67 83.0(5) . .
O45 W19 O68 84.5(5) . .
O67 W19 K3 45.1(4) . .
O67 W19 K5 60.8(4) . .
O67 W19 K10 79.8(4) . 1_556
O67 W19 K16 128.7(5) . 1_556
O67 W19 O68 72.2(5) . .
O68 W19 K3 93.6(3) . .
O68 W19 K5 129.3(3) . .
O68 W19 K10 113.9(4) . 1_556
O68 W19 K16 105.0(5) . 1_556
O71 W19 K3 129.2(4) . .
O71 W19 K5 116.9(4) . .
O71 W19 K10 44.3(4) . 1_556
O71 W19 K16 47.8(5) . 1_556
O71 W19 O45 157.7(5) . .
O71 W19 O67 84.8(5) . .
O71 W19 O68 74.0(5) . .
O72 W19 K3 83.2(5) . .
O72 W19 K5 44.6(5) . .
O72 W19 K10 55.1(5) . 1_556
O72 W19 K16 75.6(6) . 1_556
O72 W19 O45 102.1(6) . .
O72 W19 O67 96.6(6) . .
O72 W19 O68 166.4(5) . .
O72 W19 O71 97.7(6) . .
O72 W19 O73 104.7(6) . .
O73 W19 K3 134.6(4) . .
O73 W19 K5 135.9(4) . .
O73 W19 K10 114.4(4) . 1_556
O73 W19 K16 60.9(5) . 1_556
O73 W19 O45 90.1(5) . .
O73 W19 O67 158.6(5) . .
O73 W19 O68 87.0(4) . .
O73 W19 O71 94.5(5) . .
W11 Sm1 Sm3 105.31(3) . .
W12 Sm1 W11 58.92(2) . .
W12 Sm1 Sm3 69.09(3) . .
O15 Sm1 W11 141.4(3) . .
O15 Sm1 W12 146.7(3) . .
O15 Sm1 Sm3 111.5(3) . .
O15 Sm1 O23 71.6(4) . .
O15 Sm1 O42 134.6(4) . .
O15 Sm1 O43 140.4(4) . .
O15 Sm1 O48 140.8(4) . .
O15 Sm1 O74 102.9(4) . .
O15 Sm1 O1W 73.8(4) . .
O15 Sm1 O2W 76.9(4) . .
O15 Sm1 O3W 68.8(4) . .
O23 Sm1 W11 146.9(3) . .
O23 Sm1 W12 91.9(3) . .
O23 Sm1 Sm3 44.8(3) . .
O42 Sm1 W11 29.7(2) . .
O42 Sm1 W12 76.9(3) . .
O42 Sm1 Sm3 93.1(3) . .
O42 Sm1 O23 136.8(4) . .
O42 Sm1 O43 61.9(4) . .
O42 Sm1 O48 81.5(4) . .
O42 Sm1 O74 70.7(4) . .
O42 Sm1 O1W 84.6(4) . .
O42 Sm1 O2W 135.9(4) . .
O42 Sm1 O3W 67.0(4) . .
O43 Sm1 W11 33.8(3) . .
O43 Sm1 W12 34.4(3) . .
O43 Sm1 Sm3 101.1(3) . .
O43 Sm1 O23 124.6(4) . .
O48 Sm1 W11 76.9(3) . .
O48 Sm1 W12 29.8(3) . .
O48 Sm1 Sm3 39.4(3) . .
O48 Sm1 O23 70.2(4) . .
O48 Sm1 O43 62.4(4) . .
O48 Sm1 O74 71.3(4) . .
O48 Sm1 O1W 134.6(4) . .
O48 Sm1 O2W 84.8(4) . .
O48 Sm1 O3W 135.8(4) . .
O74 Sm1 W11 97.1(3) . .
O74 Sm1 W12 97.6(2) . .
O74 Sm1 Sm3 41.3(2) . .
O74 Sm1 O23 69.7(4) . .
O74 Sm1 O43 116.5(4) . .
O74 Sm1 O1W 141.7(4) . .
O74 Sm1 O2W 141.7(4) . .
O74 Sm1 O3W 69.4(3) . .
O1W Sm1 W11 70.1(3) . .
O1W Sm1 W12 104.9(3) . .
O1W Sm1 Sm3 174.0(3) . .
O1W Sm1 O23 138.3(4) . .
O1W Sm1 O43 72.9(4) . .
O1W Sm1 O2W 75.9(4) . .
O1W Sm1 O3W 74.1(4) . .
O2W Sm1 W11 106.4(3) . .
O2W Sm1 W12 70.8(3) . .
O2W Sm1 Sm3 102.2(3) . .
O2W Sm1 O23 74.2(4) . .
O2W Sm1 O43 74.6(4) . .
O2W Sm1 O3W 139.4(4) . .
O3W Sm1 W11 88.4(2) . .
O3W Sm1 W12 143.9(2) . .
O3W Sm1 Sm3 110.1(2) . .
O3W Sm1 O23 113.0(4) . .
O3W Sm1 O43 120.6(4) . .
Sm1 Sm2 K8 150.07(19) . 3_657
Sm1 Sm2 K8 101.94(19) . .
Sm1 Sm2 K9 148.25(17) . 1_556
K8 Sm2 K8 74.0(3) . 3_657
K8 Sm2 K9 88.7(2) . 1_556
K9 Sm2 K8 61.6(2) 1_556 3_657
O35 Sm2 Sm1 94.9(3) . .
O35 Sm2 K8 105.0(3) . 3_657
O35 Sm2 K8 53.2(3) . .
O35 Sm2 K9 67.6(3) . 1_556
O35 Sm2 O39 120.0(4) . 3_657
O35 Sm2 O74 68.8(4) . .
O35 Sm2 O3W 78.7(4) . .
O35 Sm2 O4W 71.0(4) . .
O35 Sm2 O5W 74.9(4) . .
O39 Sm2 Sm1 99.5(3) 3_657 .
O39 Sm2 K8 51.2(4) 3_657 3_657
O39 Sm2 K8 66.9(4) 3_657 .
O39 Sm2 K9 112.2(3) 3_657 1_556
O39 Sm2 O74 139.1(4) 3_657 .
O39 Sm2 O3W 73.2(4) 3_657 .
O39 Sm2 O4W 73.2(4) 3_657 .
O39 Sm2 O5W 139.7(4) 3_657 .
O42 Sm2 Sm1 39.3(3) . .
O42 Sm2 K8 118.7(3) . 3_657
O42 Sm2 K8 124.7(3) . .
O42 Sm2 K9 146.2(3) . 1_556
O42 Sm2 O35 134.0(4) . .
O42 Sm2 O39 81.1(4) . 3_657
O42 Sm2 O74 69.8(4) . .
O42 Sm2 O3W 68.8(4) . .
O42 Sm2 O4W 151.9(4) . .
O42 Sm2 O5W 116.8(4) . .
O73 Sm2 Sm1 114.4(3) . .
O73 Sm2 K8 59.9(3) . 3_657
O73 Sm2 K8 133.5(3) . .
O73 Sm2 K9 75.5(3) . 1_556
O73 Sm2 O35 142.7(4) . .
O73 Sm2 O39 79.0(4) . 3_657
O73 Sm2 O42 77.0(4) . .
O73 Sm2 O74 119.6(4) . .
O73 Sm2 O3W 138.4(4) . .
O73 Sm2 O4W 86.8(4) . .
O73 Sm2 O5W 71.5(4) . .
O74 Sm2 Sm1 40.4(3) . .
O74 Sm2 K8 169.5(3) . 3_657
O74 Sm2 K8 106.9(3) . .
O74 Sm2 K9 107.9(3) . 1_556
O74 Sm2 O4W 138.2(4) . .
O3W Sm2 Sm1 43.9(2) . .
O3W Sm2 K8 59.6(3) . .
O3W Sm2 K8 118.2(3) . 3_657
O3W Sm2 K9 143.8(3) . 1_556
O3W Sm2 O74 69.8(4) . .
O3W Sm2 O4W 113.0(4) . .
O4W Sm2 Sm1 156.2(3) . .
O4W Sm2 K8 54.3(3) . .
O4W Sm2 K8 34.1(3) . 3_657
O4W Sm2 K9 44.0(3) . 1_556
O5W Sm2 Sm1 117.3(3) . .
O5W Sm2 K8 89.8(4) . 3_657
O5W Sm2 K8 116.8(4) . .
O5W Sm2 K9 34.4(3) . 1_556
O5W Sm2 O74 80.5(4) . .
O5W Sm2 O3W 145.7(4) . .
O5W Sm2 O4W 78.4(4) . .
Sm1 Sm3 K4 122.57(16) . .
Sm1 Sm3 K7 157.01(18) . .
K4 Sm3 K7 67.6(2) . .
O23 Sm3 Sm1 45.9(3) . .
O23 Sm3 K4 115.6(3) . .
O23 Sm3 K7 153.3(3) . .
O30 Sm3 Sm1 99.8(3) . .
O30 Sm3 K4 46.0(3) . .
O30 Sm3 K7 100.8(4) . .
O30 Sm3 O23 71.5(4) . .
O30 Sm3 O74 79.7(4) . .
O30 Sm3 O6W 72.8(4) . .
O30 Sm3 O7W 84.2(4) . .
O30 Sm3 O8W 102.2(5) . .
O48 Sm3 Sm1 40.6(3) . .
O48 Sm3 K4 150.1(3) . .
O48 Sm3 K7 119.6(3) . .
O48 Sm3 O23 71.9(4) . .
O48 Sm3 O30 139.6(4) . .
O48 Sm3 O74 72.3(4) . .
O48 Sm3 O6W 144.6(4) . .
O48 Sm3 O7W 116.3(4) . .
O48 Sm3 O8W 84.5(5) . .
O56 Sm3 Sm1 113.6(3) . .
O56 Sm3 K4 104.8(3) . .
O56 Sm3 K7 44.7(3) . .
O56 Sm3 O23 139.5(4) . .
O56 Sm3 O30 145.4(4) . .
O56 Sm3 O48 75.0(4) . .
O56 Sm3 O74 120.2(4) . .
O56 Sm3 O6W 75.0(4) . .
O56 Sm3 O7W 74.2(4) . .
O56 Sm3 O8W 79.1(5) . .
O74 Sm3 Sm1 41.2(3) . .
O74 Sm3 K4 83.0(3) . .
O74 Sm3 K7 134.6(3) . .
O74 Sm3 O23 70.4(4) . .
O74 Sm3 O6W 140.6(4) . .
O74 Sm3 O7W 77.6(4) . .
O74 Sm3 O8W 142.8(5) . .
O6W Sm3 Sm1 169.6(3) . .
O6W Sm3 K4 57.6(3) . .
O6W Sm3 K7 33.0(4) . .
O6W Sm3 O23 123.8(4) . .
O7W Sm3 Sm1 115.0(3) . .
O7W Sm3 K4 39.6(3) . .
O7W Sm3 K7 57.6(3) . .
O7W Sm3 O23 142.5(4) . .
O7W Sm3 O6W 72.2(4) . .
O8W Sm3 Sm1 103.3(4) . .
O8W Sm3 K4 125.2(4) . .
O8W Sm3 K7 82.0(4) . .
O8W Sm3 O23 75.1(5) . .
O8W Sm3 O6W 71.8(5) . .
O8W Sm3 O7W 139.5(5) . .
O6 As1 O18 98.5(5) . .
O6 As1 O28 97.6(5) . .
O18 As1 O28 96.6(5) . .
O46 As2 O58 98.1(5) . .
O46 As2 O68 98.9(6) . .
O58 As2 O68 98.1(5) . .
W9 K1 K5 129.1(2) . 3_657
K13 K1 W9 160.0(5) . .
K13 K1 K5 52.9(5) . 3_657
K13 K1 K21 88.3(8) . .
K13 K1 O1 88.1(5) . .
K13 K1 O4 134.5(6) . .
K13 K1 O22 88.0(5) . 4_666
K13 K1 O32 161.2(6) . .
K13 K1 O36 131.1(6) . .
K13 K1 O38 88.0(5) . .
K13 K1 C1 108.1(6) . .
K13 K1 O21W 70.0(10) . 4_666
K21 K1 W9 72.0(6) . .
K21 K1 K5 108.3(7) . 3_657
K21 K1 C1 135.3(7) . .
O1 K1 W9 84.1(2) . .
O1 K1 K5 48.8(3) . 3_657
O1 K1 K21 77.6(7) . .
O1 K1 C1 62.2(4) . .
O1 K1 O21W 127.7(9) . 4_666
O4 K1 W9 30.1(2) . .
O4 K1 K5 104.2(3) . 3_657
O4 K1 K21 59.7(7) . .
O4 K1 O1 55.9(3) . .
O4 K1 O36 64.3(3) . .
O4 K1 C1 80.8(4) . .
O4 K1 O21W 108.4(9) . 4_666
O22 K1 W9 106.1(3) 4_666 .
O22 K1 K5 112.6(4) 4_666 3_657
O22 K1 K21 124.8(8) 4_666 .
O22 K1 O1 157.1(4) 4_666 .
O22 K1 O4 136.2(4) 4_666 .
O22 K1 O32 79.7(4) 4_666 .
O22 K1 O36 98.5(4) 4_666 .
O22 K1 O38 87.3(4) 4_666 .
O22 K1 C1 97.8(5) 4_666 .
O22 K1 O21W 71.5(9) 4_666 4_666
O32 K1 W9 26.4(3) . .
O32 K1 K5 145.5(4) . 3_657
O32 K1 K21 87.1(7) . .
O32 K1 O1 108.7(4) . .
O32 K1 O4 56.4(4) . .
O32 K1 O36 65.5(4) . .
O32 K1 O38 105.5(4) . .
O32 K1 C1 87.8(5) . .
O32 K1 O21W 92.4(9) . 4_666
O36 K1 W9 61.9(2) . .
O36 K1 K5 80.5(3) . 3_657
O36 K1 K21 123.8(7) . .
O36 K1 O1 67.8(3) . .
O36 K1 C1 23.1(4) . .
O36 K1 O21W 157.4(9) . 4_666
O38 K1 W9 106.5(3) . .
O38 K1 K5 46.5(4) . 3_657
O38 K1 K21 147.6(8) . .
O38 K1 O1 70.0(4) . .
O38 K1 O4 102.2(4) . .
O38 K1 O36 44.5(3) . .
O38 K1 C1 22.5(4) . .
O38 K1 O21W 149.5(9) . 4_666
C1 K1 W9 84.4(4) . .
C1 K1 K5 59.3(4) . 3_657
O21W K1 W9 100.5(9) 4_666 .
O21W K1 K5 121.9(9) 4_666 3_657
O21W K1 K21 55.7(11) 4_666 .
O21W K1 C1 169.0(10) 4_666 .
W2 K2 K6 176.2(3) . 3_656
W2 K2 K12 60.6(3) . 1_545
W4 K2 W2 55.93(11) . .
W4 K2 K6 121.3(2) . 3_656
W4 K2 K12 110.9(3) . 1_545
K12 K2 K6 120.5(4) 1_545 3_656
K15 K2 W2 69.8(4) . .
K15 K2 W4 66.5(4) . .
K15 K2 K6 112.0(5) . 3_656
K15 K2 K12 113.5(5) . 1_545
O7 K2 W2 24.9(2) . .
O7 K2 W4 80.7(3) . .
O7 K2 K6 157.3(4) . 3_656
O7 K2 K12 38.1(4) . 1_545
O7 K2 K15 80.7(5) . .
O7 K2 O10 53.8(3) . .
O10 K2 W2 29.0(2) . .
O10 K2 W4 28.7(2) . .
O10 K2 K6 148.9(3) . 3_656
O10 K2 K12 88.9(4) . 1_545
O10 K2 K15 57.7(5) . .
O14 K2 W2 80.8(3) . .
O14 K2 W4 25.1(2) . .
O14 K2 K6 96.3(3) . 3_656
O14 K2 K12 130.4(4) . 1_545
O14 K2 K15 75.8(5) . .
O14 K2 O7 105.3(4) . .
O14 K2 O10 53.6(3) . .
O19 K2 W2 142.3(4) 3_656 .
O19 K2 W4 101.3(4) 3_656 .
O19 K2 K6 38.8(3) 3_656 3_656
O19 K2 K12 147.1(5) 3_656 1_545
O19 K2 K15 73.5(5) 3_656 .
O19 K2 O7 150.4(5) 3_656 .
O19 K2 O10 118.9(5) 3_656 .
O19 K2 O14 82.3(4) 3_656 .
O19 K2 O62 83.0(4) 3_656 2_546
O19 K2 O9W 133.8(6) 3_656 .
O19 K2 O12W 112.8(8) 3_656 .
O62 K2 W2 131.1(4) 2_546 .
O62 K2 W4 110.9(4) 2_546 .
O62 K2 K6 46.3(3) 2_546 3_656
O62 K2 K12 91.1(4) 2_546 1_545
O62 K2 K15 154.8(5) 2_546 .
O62 K2 O7 124.3(5) 2_546 .
O62 K2 O10 131.7(5) 2_546 .
O62 K2 O14 92.6(4) 2_546 .
O9W K2 W2 67.7(5) . .
O9W K2 W4 64.1(5) . .
O9W K2 K6 109.0(5) . 3_656
O9W K2 K12 69.5(5) . 1_545
O9W K2 K15 127.0(7) . .
O9W K2 O7 73.9(5) . .
O9W K2 O10 69.8(5) . .
O9W K2 O14 67.6(5) . .
O9W K2 O62 65.2(6) . 2_546
O9W K2 O12W 90.2(8) . .
O12W K2 W2 94.7(7) . .
O12W K2 W4 145.8(7) . .
O12W K2 K6 87.0(7) . 3_656
O12W K2 K12 35.4(7) . 1_545
O12W K2 K15 123.6(8) . .
O12W K2 O7 70.3(7) . .
O12W K2 O10 123.6(7) . .
O12W K2 O14 157.4(8) . .
O12W K2 O62 73.7(7) . 2_546
W11 K3 W17 81.2(2) . .
W11 K3 W19 56.55(14) . .
W11 K3 K13 137.6(4) . 3_657
W13 K3 W11 53.12(14) . .
W13 K3 W17 57.80(15) . .
W13 K3 W19 81.1(2) . .
W13 K3 K13 169.3(4) . 3_657
W17 K3 W19 51.40(13) . .
W17 K3 K13 118.5(4) . 3_657
W19 K3 K13 104.5(3) . 3_657
K5 K3 W11 106.7(4) . .
K5 K3 W13 150.0(5) . .
K5 K3 W17 100.9(4) . .
K5 K3 W19 68.9(3) . .
K5 K3 K13 36.8(4) . 3_657
K5 K3 K20 132.8(8) . 2_546
K5 K3 O29 67.8(5) . 2_546
K5 K3 O44 136.7(5) . .
K5 K3 O45 85.7(4) . .
K5 K3 O53 128.6(6) . .
K5 K3 O67 75.3(4) . .
K20 K3 W11 69.7(7) 2_546 .
K20 K3 W13 66.2(7) 2_546 .
K20 K3 W17 123.7(7) 2_546 .
K20 K3 W19 126.2(7) 2_546 .
K20 K3 K13 115.5(8) 2_546 3_657
O29 K3 W11 101.1(4) 2_546 .
O29 K3 W13 132.2(5) 2_546 .
O29 K3 W17 168.6(5) 2_546 .
O29 K3 W19 120.6(4) 2_546 .
O29 K3 K13 52.8(4) 2_546 3_657
O29 K3 K20 67.1(8) 2_546 2_546
O29 K3 O44 107.3(5) 2_546 .
O29 K3 O45 111.3(5) 2_546 .
O29 K3 O53 161.0(6) 2_546 .
O29 K3 O67 141.4(5) 2_546 .
O44 K3 W11 30.1(2) . .
O44 K3 W13 29.8(3) . .
O44 K3 W17 80.3(3) . .
O44 K3 W19 79.6(3) . .
O44 K3 K13 159.2(5) . 3_657
O44 K3 K20 50.8(7) . 2_546
O44 K3 O45 54.9(4) . .
O44 K3 O67 91.6(4) . .
O45 K3 W11 28.6(2) . .
O45 K3 W13 66.8(3) . .
O45 K3 W17 65.7(3) . .
O45 K3 W19 28.1(2) . .
O45 K3 K13 122.1(4) . 3_657
O45 K3 K20 98.2(7) . 2_546
O53 K3 W11 66.8(3) . .
O53 K3 W13 28.7(3) . .
O53 K3 W17 29.3(3) . .
O53 K3 W19 66.1(3) . .
O53 K3 K13 145.7(5) . 3_657
O53 K3 K20 94.4(8) . 2_546
O53 K3 O44 54.7(4) . .
O53 K3 O45 65.4(4) . .
O53 K3 O67 53.3(4) . .
O67 K3 W11 78.6(3) . .
O67 K3 W13 78.6(3) . .
O67 K3 W17 27.8(3) . .
O67 K3 W19 29.3(3) . .
O67 K3 K13 101.8(4) . 3_657
O67 K3 K20 142.2(8) . 2_546
O67 K3 O45 53.4(4) . .
W8 K4 W9 50.33(14) . .
W8 K4 W10 87.0(2) . .
W10 K4 W9 54.99(15) . .
K18 K4 W8 118.7(6) 4_666 .
K18 K4 W9 69.5(6) 4_666 .
K18 K4 W10 64.5(6) 4_666 .
K20 K4 W8 75.4(9) . .
K20 K4 W9 79.0(9) . .
K20 K4 W10 130.3(9) . .
K20 K4 K18 83.8(10) . 4_666
K20 K4 O30 100.8(9) . .
K20 K4 O31 62.6(9) . .
K20 K4 O33 106.9(9) . .
K20 K4 O34 136.4(9) . .
K20 K4 O7W 135.4(9) . .
K20 K4 O10W 85.2(11) . .
K20 K4 O24W 97.7(13) . 4_666
O30 K4 W8 26.8(2) . .
O30 K4 W9 63.8(3) . .
O30 K4 W10 76.9(3) . .
O30 K4 K18 130.9(7) . 4_666
O30 K4 O33 61.4(4) . .
O31 K4 W8 29.9(3) . .
O31 K4 W9 26.8(2) . .
O31 K4 W10 79.1(3) . .
O31 K4 K18 89.5(6) . 4_666
O31 K4 O30 52.9(4) . .
O31 K4 O33 50.7(4) . .
O31 K4 O34 101.4(5) . .
O31 K4 O10W 139.6(8) . .
O33 K4 W8 62.3(3) . .
O33 K4 W9 28.1(2) . .
O33 K4 W10 28.4(2) . .
O33 K4 K18 70.5(6) . 4_666
O34 K4 W8 111.8(4) . .
O34 K4 W9 75.4(3) . .
O34 K4 W10 24.8(3) . .
O34 K4 K18 54.3(6) . 4_666
O34 K4 O30 98.8(5) . .
O34 K4 O33 51.9(4) . .
O34 K4 O10W 118.9(8) . .
O7W K4 W8 90.6(4) . .
O7W K4 W9 123.5(4) . .
O7W K4 W10 89.8(4) . .
O7W K4 K18 138.0(7) . 4_666
O7W K4 O30 66.1(4) . .
O7W K4 O31 119.0(5) . .
O7W K4 O33 102.9(5) . .
O7W K4 O34 88.2(5) . .
O7W K4 O10W 67.1(7) . .
O7W K4 O24W 109.9(10) . 4_666
O10W K4 W8 122.8(7) . .
O10W K4 W9 164.0(7) . .
O10W K4 W10 140.7(7) . .
O10W K4 K18 111.7(9) . 4_666
O10W K4 O30 117.3(7) . .
O10W K4 O33 167.9(8) . .
O24W K4 W8 155.2(10) 4_666 .
O24W K4 W9 105.2(9) 4_666 .
O24W K4 W10 79.4(9) 4_666 .
O24W K4 K18 36.6(10) 4_666 4_666
O24W K4 O30 155.9(10) 4_666 .
O24W K4 O31 125.9(10) 4_666 .
O24W K4 O33 98.4(10) 4_666 .
O24W K4 O34 57.1(10) 4_666 .
O24W K4 O10W 79.4(11) 4_666 .
W19 K5 K10 50.9(2) . 1_556
K1 K5 W19 136.0(3) 3_657 .
K1 K5 K10 100.6(3) 3_657 1_556
K3 K5 W19 71.8(4) . .
K3 K5 K1 148.0(5) . 3_657
K3 K5 K10 111.2(4) . 1_556
K3 K5 K13 112.5(6) . 3_657
K3 K5 O1 160.6(6) . 3_657
K3 K5 O29 58.9(4) . 2_546
K3 K5 O38 116.6(6) . 3_657
K3 K5 O67 56.0(4) . .
K3 K5 O72 95.9(5) . .
K3 K5 O22W 95.6(10) . .
K13 K5 W19 164.9(6) 3_657 .
K13 K5 K1 46.0(4) 3_657 3_657
K13 K5 K10 115.7(5) 3_657 1_556
K13 K5 O67 138.7(6) 3_657 .
O1 K5 W19 89.3(4) 3_657 .
O1 K5 K1 51.2(3) 3_657 3_657
O1 K5 K10 50.5(3) 3_657 1_556
O1 K5 K13 84.5(6) 3_657 3_657
O1 K5 O29 137.8(6) 3_657 2_546
O1 K5 O67 105.1(5) 3_657 .
O29 K5 W19 116.5(5) 2_546 .
O29 K5 K1 90.1(4) 2_546 3_657
O29 K5 K10 167.4(5) 2_546 1_556
O29 K5 K13 76.6(6) 2_546 3_657
O29 K5 O67 114.0(5) 2_546 .
O38 K5 W19 107.4(4) 3_657 .
O38 K5 K1 48.6(3) 3_657 3_657
O38 K5 K10 114.5(4) 3_657 1_556
O38 K5 K13 83.9(6) 3_657 3_657
O38 K5 O1 72.9(5) 3_657 3_657
O38 K5 O29 68.0(5) 3_657 2_546
O38 K5 O67 137.3(5) 3_657 .
O38 K5 O72 92.4(5) 3_657 .
O38 K5 O22W 146.2(11) 3_657 .
O67 K5 W19 31.1(2) . .
O67 K5 K1 155.8(4) . 3_657
O67 K5 K10 55.3(3) . 1_556
O72 K5 W19 24.5(3) . .
O72 K5 K1 111.5(4) . 3_657
O72 K5 K10 40.0(3) . 1_556
O72 K5 K13 149.9(6) . 3_657
O72 K5 O1 66.0(4) . 3_657
O72 K5 O29 129.5(6) . 2_546
O72 K5 O67 51.9(4) . .
O22W K5 W19 71.8(10) . .
O22W K5 K1 107.6(10) . 3_657
O22W K5 K10 37.9(9) . 1_556
O22W K5 K13 93.3(11) . 3_657
O22W K5 O1 73.3(10) . 3_657
O22W K5 O29 144.0(10) . 2_546
O22W K5 O67 53.9(10) . .
O22W K5 O72 73.5(10) . .
W5 K6 W7 58.64(18) . .
W5 K6 W16 129.7(3) . 4_665
W5 K6 K11 92.5(4) . .
W5 K6 K13 67.5(4) . 4_565
W7 K6 W16 171.5(3) . 4_665
W7 K6 K11 59.0(3) . .
W7 K6 K13 62.7(3) . 4_565
W16 K6 K11 115.7(4) 4_665 .
W16 K6 K13 120.2(4) 4_665 4_565
W18 K6 W5 172.6(4) 4_665 .
W18 K6 W7 114.1(3) 4_665 .
W18 K6 W16 57.54(18) 4_665 4_665
W18 K6 K11 82.1(3) 4_665 .
W18 K6 K13 111.0(4) 4_665 4_565
K11 K6 K13 120.2(5) . 4_565
O19 K6 W5 26.3(3) . .
O19 K6 W7 84.7(4) . .
O19 K6 W16 103.5(4) . 4_665
O19 K6 W18 160.6(5) . 4_665
O19 K6 K11 105.4(5) . .
O19 K6 K13 81.2(5) . 4_565
O19 K6 O21 58.0(4) . .
O19 K6 O25 110.3(5) . .
O19 K6 O62 78.7(4) . 4_665
O19 K6 O69 163.3(6) . 4_665
O21 K6 W5 31.7(3) . .
O21 K6 W7 28.2(3) . .
O21 K6 W16 160.3(5) . 4_665
O21 K6 W18 141.3(5) . 4_665
O21 K6 K11 78.6(4) . .
O21 K6 K13 54.6(4) . 4_565
O21 K6 O25 54.4(4) . .
O21 K6 O62 136.7(5) . 4_665
O25 K6 W5 84.6(4) . .
O25 K6 W7 26.2(3) . .
O25 K6 W16 145.3(4) . 4_665
O25 K6 W18 88.1(4) . 4_665
O25 K6 K11 47.7(4) . .
O25 K6 K13 73.8(4) . 4_565
O25 K6 O62 162.3(5) . 4_665
O62 K6 W5 105.0(4) 4_665 .
O62 K6 W7 160.6(5) 4_665 .
O62 K6 W16 26.0(2) 4_665 4_665
O62 K6 W18 82.0(3) 4_665 4_665
O62 K6 K11 116.0(5) 4_665 .
O62 K6 K13 123.5(5) 4_665 4_565
O64 K6 W5 156.3(5) 4_665 .
O64 K6 W7 144.1(5) 4_665 .
O64 K6 W16 28.0(3) 4_665 4_665
O64 K6 W18 31.1(3) 4_665 4_665
O64 K6 K11 106.3(5) 4_665 .
O64 K6 K13 112.7(5) 4_665 4_565
O64 K6 O19 130.9(6) 4_665 .
O64 K6 O21 165.6(6) 4_665 .
O64 K6 O25 118.8(5) 4_665 .
O64 K6 O62 53.9(4) 4_665 4_665
O64 K6 O69 58.3(4) 4_665 4_665
O69 K6 W5 145.3(5) 4_665 .
O69 K6 W7 88.4(4) 4_665 .
O69 K6 W16 83.0(4) 4_665 4_665
O69 K6 W18 27.5(3) 4_665 4_665
O69 K6 K11 58.3(4) 4_665 .
O69 K6 K13 109.1(5) 4_665 4_565
O69 K6 O21 116.6(5) 4_665 .
O69 K6 O25 62.3(4) 4_665 .
O69 K6 O62 104.8(5) 4_665 4_665
W14 K7 W16 51.59(18) . .
O40 K7 W14 102.8(5) 4_565 .
O40 K7 W16 120.8(5) 4_565 .
O40 K7 O41 69.7(5) 4_565 2_556
O40 K7 O56 123.3(6) 4_565 .
O40 K7 O57 100.2(6) 4_565 .
O40 K7 O63 147.1(6) 4_565 .
O40 K7 C3 42.9(5) 4_565 4_565
O40 K7 C4 19.4(4) 4_565 4_565
O40 K7 O1W 64.3(5) 4_565 2_556
O40 K7 O10W 132.5(9) 4_565 .
O41 K7 W14 149.8(5) 2_556 .
O41 K7 W16 157.5(5) 2_556 .
O41 K7 O56 133.4(6) 2_556 .
O41 K7 O63 138.1(6) 2_556 .
O41 K7 C3 66.5(5) 2_556 4_565
O41 K7 C4 61.4(5) 2_556 4_565
O41 K7 O1W 55.2(4) 2_556 2_556
O56 K7 W14 27.5(2) . .
O56 K7 W16 60.4(3) . .
O56 K7 C3 93.2(5) . 4_565
O56 K7 C4 114.5(5) . 4_565
O57 K7 W14 29.4(3) . .
O57 K7 W16 29.5(3) . .
O57 K7 O41 169.8(6) . 2_556
O57 K7 O56 51.3(4) . .
O57 K7 O63 51.6(4) . .
O57 K7 C3 105.8(6) . 4_565
O57 K7 C4 108.7(5) . 4_565
O57 K7 O1W 121.8(6) . 2_556
O63 K7 W14 62.1(3) . .
O63 K7 W16 26.5(3) . .
O63 K7 O56 56.3(4) . .
O63 K7 C3 148.7(6) . 4_565
O63 K7 C4 160.4(6) . 4_565
C3 K7 W14 87.9(5) 4_565 .
C3 K7 W16 135.4(5) 4_565 .
C3 K7 C4 24.7(4) 4_565 4_565
C4 K7 W14 101.5(4) 4_565 .
C4 K7 W16 134.8(5) 4_565 .
O1W K7 W14 149.4(5) 2_556 .
O1W K7 W16 109.0(5) 2_556 .
O1W K7 O56 168.8(6) 2_556 .
O1W K7 O63 112.6(5) 2_556 .
O1W K7 C3 97.6(6) 2_556 4_565
O1W K7 C4 75.3(5) 2_556 4_565
O6W K7 W14 81.8(5) . .
O6W K7 W16 112.5(5) . .
O6W K7 O40 114.4(7) . 4_565
O6W K7 O41 75.7(5) . 2_556
O6W K7 O56 58.0(5) . .
O6W K7 O57 109.2(6) . .
O6W K7 O63 93.3(5) . .
O6W K7 C3 72.6(5) . 4_565
O6W K7 C4 95.0(6) . 4_565
O6W K7 O1W 128.7(6) . 2_556
O6W K7 O10W 83.6(8) . .
O10W K7 W14 123.8(8) . .
O10W K7 W16 86.2(7) . .
O10W K7 O41 73.6(7) . 2_556
O10W K7 O56 103.8(8) . .
O10W K7 O57 115.4(8) . .
O10W K7 O63 65.0(7) . .
O10W K7 C3 137.3(9) . 4_565
O10W K7 C4 133.7(8) . 4_565
O10W K7 O1W 70.2(7) . 2_556
W1 K8 Sm2 103.0(3) . .
W1 K8 K10 55.7(3) . 3_656
W2 K8 W1 48.39(17) . .
W2 K8 Sm2 97.8(3) . .
W2 K8 K10 56.5(3) . 3_656
W10 K8 W1 56.1(2) . .
W10 K8 W2 88.8(3) . .
W10 K8 Sm2 57.70(19) . .
W10 K8 K10 109.8(4) . 3_656
Sm2 K8 K10 153.3(4) . 3_656
K16 K8 W1 104.4(6) 3_656 .
K16 K8 W2 78.2(6) 3_656 .
K16 K8 W10 160.3(7) 3_656 .
K16 K8 Sm2 138.3(7) 3_656 .
K16 K8 K10 50.6(6) 3_656 3_656
K16 K8 O2 79.3(7) 3_656 .
K16 K8 O5 128.2(8) 3_656 .
K16 K8 O8 90.6(7) 3_656 .
K16 K8 O37 150.9(7) 3_656 .
K16 K8 O23W 46.5(9) 3_656 2_646
O2 K8 W1 27.8(2) . .
O2 K8 W2 28.7(2) . .
O2 K8 W10 82.3(4) . .
O2 K8 Sm2 116.4(4) . .
O2 K8 K10 37.3(3) . 3_656
O5 K8 W1 23.8(2) . .
O5 K8 W2 61.7(3) . .
O5 K8 W10 32.7(3) . .
O5 K8 Sm2 81.7(4) . .
O5 K8 K10 79.2(4) . 3_656
O5 K8 O2 49.7(4) . .
O5 K8 O37 53.3(4) . .
O5 K8 O23W 122.2(10) . 2_646
O8 K8 W1 61.1(3) . .
O8 K8 W2 22.8(2) . .
O8 K8 W10 82.5(4) . .
O8 K8 Sm2 75.9(4) . .
O8 K8 K10 79.1(4) . 3_656
O8 K8 O2 49.5(4) . .
O8 K8 O5 65.0(4) . .
O8 K8 O37 111.1(6) . .
O8 K8 O23W 58.4(9) . 2_646
O37 K8 W1 72.1(4) . .
O37 K8 W2 114.7(5) . .
O37 K8 W10 28.6(3) . .
O37 K8 Sm2 68.4(3) . .
O37 K8 K10 113.0(5) . 3_656
O37 K8 O2 99.8(5) . .
O37 K8 O23W 162.5(9) . 2_646
O4W K8 W1 164.9(5) 3_657 .
O4W K8 W2 143.7(5) 3_657 .
O4W K8 W10 122.0(5) 3_657 .
O4W K8 Sm2 85.5(4) 3_657 .
O4W K8 K10 119.1(5) 3_657 3_656
O4W K8 K16 75.7(7) 3_657 3_656
O4W K8 O2 154.7(6) 3_657 .
O4W K8 O5 153.4(7) 3_657 .
O4W K8 O8 133.8(6) 3_657 .
O4W K8 O37 100.2(6) 3_657 .
O4W K8 O23W 81.9(9) 3_657 2_646
O23W K8 W1 109.4(9) 2_646 .
O23W K8 W2 61.8(9) 2_646 .
O23W K8 W10 137.7(9) 2_646 .
O23W K8 Sm2 94.6(8) 2_646 .
O23W K8 K10 80.1(9) 2_646 3_656
O23W K8 O2 83.7(9) 2_646 .
W10 K9 Sm2 56.04(17) 1_554 1_554
W10 K9 K8 95.6(3) 1_554 3_656
Sm2 K9 K8 59.5(2) 1_554 3_656
K12 K9 W10 160.4(4) 3_666 1_554
K12 K9 Sm2 113.2(4) 3_666 1_554
K12 K9 K8 65.5(4) 3_666 3_656
K16 K9 W10 127.1(6) . 1_554
K16 K9 Sm2 74.6(6) . 1_554
K16 K9 K8 37.8(5) . 3_656
K16 K9 K12 38.7(6) . 3_666
K16 K9 O4W 69.2(6) . 1_554
K16 K9 O11W 66.4(8) . 4_565
K16 K9 O23W 47.2(10) . 4_565
O34 K9 W10 20.7(3) 1_554 1_554
O34 K9 Sm2 68.5(4) 1_554 1_554
O34 K9 K8 115.9(5) 1_554 3_656
O34 K9 K12 178.2(6) 1_554 3_666
O34 K9 K16 143.1(7) 1_554 .
O34 K9 O4W 79.1(5) 1_554 1_554
O34 K9 O11W 139.7(7) 1_554 4_565
O34 K9 O13W 134.8(8) 1_554 4_565
O34 K9 O23W 143.1(10) 1_554 4_565
O54 K9 W10 88.1(4) 4_665 1_554
O54 K9 Sm2 143.8(5) 4_665 1_554
O54 K9 K8 127.7(5) 4_665 3_656
O54 K9 K12 99.4(5) 4_665 3_666
O54 K9 K16 135.6(7) 4_665 .
O54 K9 O34 78.9(5) 4_665 1_554
O54 K9 O4W 126.8(6) 4_665 1_554
O54 K9 O11W 69.9(7) 4_665 4_565
O54 K9 O13W 83.8(8) 4_665 4_565
O54 K9 O23W 92.1(10) 4_665 4_565
O4W K9 W10 59.3(3) 1_554 1_554
O4W K9 Sm2 33.0(3) 1_554 1_554
O4W K9 K8 37.1(3) 1_554 3_656
O4W K9 K12 102.3(5) 1_554 3_666
O5W K9 W10 64.0(4) 1_554 1_554
O5W K9 Sm2 29.9(3) 1_554 1_554
O5W K9 K8 84.1(4) 1_554 3_656
O5W K9 K12 116.1(5) 1_554 3_666
O5W K9 K16 83.2(6) 1_554 .
O5W K9 O34 65.4(5) 1_554 1_554
O5W K9 O54 140.9(6) 1_554 4_665
O5W K9 O4W 62.9(4) 1_554 1_554
O5W K9 O11W 149.1(8) 1_554 4_565
O5W K9 O13W 109.9(8) 1_554 4_565
O5W K9 O23W 126.0(10) 1_554 4_565
O11W K9 W10 130.9(6) 4_565 1_554
O11W K9 Sm2 128.2(7) 4_565 1_554
O11W K9 K8 68.8(6) 4_565 3_656
O11W K9 K12 39.3(6) 4_565 3_666
O11W K9 O4W 99.4(7) 4_565 1_554
O11W K9 O23W 24.2(9) 4_565 4_565
O13W K9 W10 155.4(8) 4_565 1_554
O13W K9 Sm2 130.6(7) 4_565 1_554
O13W K9 K8 107.8(8) 4_565 3_656
O13W K9 K12 44.2(7) 4_565 3_666
O13W K9 K16 72.6(9) 4_565 .
O13W K9 O4W 141.7(8) 4_565 1_554
O13W K9 O11W 67.3(9) 4_565 4_565
O13W K9 O23W 78.4(11) 4_565 4_565
O23W K9 W10 125.2(9) 4_565 1_554
O23W K9 Sm2 104.3(9) 4_565 1_554
O23W K9 K8 44.8(9) 4_565 3_656
O23W K9 K12 37.0(9) 4_565 3_666
O23W K9 O4W 78.1(10) 4_565 1_554
W1 K10 W2 48.80(16) 3_656 3_656
W1 K10 K5 62.9(2) 3_656 1_554
W1 K10 K8 57.0(3) 3_656 3_656
W1 K10 K12 104.0(4) 3_656 3_666
W2 K10 K5 110.5(3) 3_656 1_554
W2 K10 K8 56.6(2) 3_656 3_656
W19 K10 W1 96.7(3) 1_554 3_656
W19 K10 W2 120.2(3) 1_554 3_656
W19 K10 K5 52.4(2) 1_554 1_554
W19 K10 K8 63.6(3) 1_554 3_656
W19 K10 K12 98.4(4) 1_554 3_666
K8 K10 K5 78.6(3) 3_656 1_554
K12 K10 W2 59.6(3) 3_666 3_656
K12 K10 K5 142.1(4) 3_666 1_554
K12 K10 K8 65.6(4) 3_666 3_656
K16 K10 W1 95.7(5) . 3_656
K16 K10 W2 72.6(5) . 3_656
K16 K10 W19 63.4(5) . 1_554
K16 K10 K5 106.1(6) . 1_554
K16 K10 K8 40.2(5) . 3_656
K16 K10 K12 36.9(5) . 3_666
O2 K10 W1 24.6(3) 3_656 3_656
O2 K10 W2 24.8(3) 3_656 3_656
O2 K10 W19 106.6(5) 3_656 1_554
O2 K10 K5 85.8(4) 3_656 1_554
O2 K10 K8 49.4(4) 3_656 3_656
O2 K10 K12 80.3(5) 3_656 3_666
O2 K10 K16 80.6(6) 3_656 .
O2 K10 O71 124.5(6) 3_656 1_554
O2 K10 O72 82.8(5) 3_656 1_554
O2 K10 O19W 108.3(9) 3_656 3_666
O2 K10 O22W 109.4(10) 3_656 1_554
O71 K10 W1 122.4(5) 1_554 3_656
O71 K10 W2 126.2(5) 1_554 3_656
O71 K10 W19 28.3(3) 1_554 1_554
O71 K10 K5 78.6(4) 1_554 1_554
O71 K10 K8 75.3(4) 1_554 3_656
O71 K10 K12 80.6(5) 1_554 3_666
O71 K10 K16 54.5(5) 1_554 .
O71 K10 O72 54.2(4) 1_554 1_554
O71 K10 O19W 81.8(9) 1_554 3_666
O71 K10 O22W 87.0(10) 1_554 1_554
O72 K10 W1 70.1(4) 1_554 3_656
O72 K10 W2 101.6(4) 1_554 3_656
O72 K10 W19 26.7(3) 1_554 1_554
O72 K10 K5 36.4(3) 1_554 1_554
O72 K10 K8 50.1(4) 1_554 3_656
O72 K10 K12 106.4(5) 1_554 3_666
O72 K10 K16 69.8(6) 1_554 .
O19W K10 W1 132.7(8) 3_666 3_656
O19W K10 W2 83.9(8) 3_666 3_656
O19W K10 W19 108.9(8) 3_666 1_554
O19W K10 K5 160.1(9) 3_666 1_554
O19W K10 K8 99.7(8) 3_666 3_656
O19W K10 K12 34.9(8) 3_666 3_666
O19W K10 K16 64.1(9) 3_666 .
O19W K10 O72 129.4(9) 3_666 1_554
O22W K10 W1 85.0(9) 1_554 3_656
O22W K10 W2 131.7(10) 1_554 3_656
O22W K10 W19 71.3(9) 1_554 1_554
O22W K10 K5 35.4(9) 1_554 1_554
O22W K10 K8 113.9(10) 1_554 3_656
O22W K10 K12 167.3(10) 1_554 3_666
O22W K10 K16 134.5(11) 1_554 .
O22W K10 O72 67.8(10) 1_554 1_554
O22W K10 O19W 140.4(12) 1_554 3_666
W3 K11 K6 81.8(4) . .
W3 K11 K12 161.1(6) . 2_646
W3 K11 K14 51.1(3) . .
W7 K11 W3 55.9(3) . .
W7 K11 K6 56.3(3) . .
W7 K11 K12 117.1(5) . 2_646
W7 K11 K14 84.5(4) . .
K6 K11 K14 60.8(4) . .
K12 K11 K6 109.5(5) 2_646 .
K12 K11 K14 147.6(6) 2_646 .
K21 K11 W3 65.2(7) . .
K21 K11 W7 71.5(7) . .
K21 K11 K6 127.7(8) . .
K21 K11 K12 96.1(8) . 2_646
K21 K11 K14 114.2(8) . .
O11 K11 W3 24.1(3) . .
O11 K11 W7 79.0(5) . .
O11 K11 K6 89.6(5) . .
O11 K11 K12 159.7(7) . 2_646
O11 K11 K14 38.5(4) . .
O11 K11 K21 76.5(8) . .
O13 K11 W3 29.0(3) . .
O13 K11 W7 28.5(3) . .
O13 K11 K6 72.7(5) . .
O13 K11 K12 138.4(7) . 2_646
O13 K11 K14 71.4(5) . .
O13 K11 K21 58.6(7) . .
O13 K11 O11 53.0(5) . .
O25 K11 W3 80.0(5) . .
O25 K11 W7 24.8(3) . .
O25 K11 K6 47.8(4) . .
O25 K11 K12 96.2(6) . 2_646
O25 K11 K14 96.8(6) . .
O25 K11 K21 85.8(8) . .
O25 K11 O11 102.1(6) . .
O25 K11 O13 53.2(5) . .
O59 K11 W3 86.5(6) 1_655 .
O59 K11 W7 136.6(7) 1_655 .
O59 K11 K6 146.3(7) 1_655 .
O59 K11 K12 91.1(6) 1_655 2_646
O59 K11 K14 87.4(6) 1_655 .
O59 K11 K21 73.4(8) 1_655 .
O59 K11 O11 68.6(6) 1_655 .
O59 K11 O13 109.4(7) 1_655 .
O59 K11 O25 158.6(9) 1_655 .
O59 K11 O13W 74.4(8) 1_655 .
O13W K11 W3 152.9(9) . .
O13W K11 W7 148.1(9) . .
O13W K11 K6 103.5(8) . .
O13W K11 K12 41.2(7) . 2_646
O13W K11 K14 108.0(8) . .
O13W K11 K21 124.5(10) . .
O13W K11 O11 128.9(9) . .
O13W K11 O13 176.1(10) . .
O13W K11 O25 123.4(9) . .
W2 K12 K2 58.5(3) 1_565 1_565
W2 K12 K10 60.7(3) 1_565 3_666
W2 K12 K11 147.0(5) 1_565 2_656
K2 K12 K11 109.2(5) 1_565 2_656
K9 K12 W2 116.8(5) 3_666 1_565
K9 K12 K2 127.9(5) 3_666 1_565
K9 K12 K10 107.8(5) 3_666 3_666
K9 K12 K11 95.1(5) 3_666 2_656
K10 K12 K2 110.2(5) 3_666 1_565
K10 K12 K11 103.2(5) 3_666 2_656
K16 K12 W2 84.2(8) 3_666 1_565
K16 K12 K2 137.6(9) 3_666 1_565
K16 K12 K9 49.8(7) 3_666 3_666
K16 K12 K10 58.9(7) 3_666 3_666
K16 K12 K11 113.2(8) 3_666 2_656
K16 K12 O7 97.4(9) 3_666 1_565
K16 K12 O11W 84.5(10) 3_666 2_656
K16 K12 O13W 86.0(11) 3_666 2_656
O7 K12 W2 14.8(4) 1_565 1_565
O7 K12 K2 49.5(4) 1_565 1_565
O7 K12 K9 131.3(7) 1_565 3_666
O7 K12 K10 63.1(5) 1_565 3_666
O7 K12 K11 133.4(7) 1_565 2_656
O7 K12 O13W 175.7(10) 1_565 2_656
O11W K12 W2 89.8(8) 2_656 1_565
O11W K12 K2 76.6(8) 2_656 1_565
O11W K12 K9 51.4(7) 2_656 3_666
O11W K12 K10 133.2(9) 2_656 3_666
O11W K12 K11 118.5(9) 2_656 2_656
O11W K12 O7 97.8(9) 2_656 1_565
O11W K12 O13W 79.8(11) 2_656 2_656
O12W K12 W2 101.7(9) 1_565 1_565
O12W K12 K2 44.8(8) 1_565 1_565
O12W K12 K9 119.7(10) 1_565 3_666
O12W K12 K10 131.7(10) 1_565 3_666
O12W K12 K11 66.2(9) 1_565 2_656
O12W K12 K16 169.4(13) 1_565 3_666
O12W K12 O7 89.6(10) 1_565 1_565
O12W K12 O11W 86.7(11) 1_565 2_656
O12W K12 O13W 86.7(12) 1_565 2_656
O13W K12 W2 166.4(9) 2_656 1_565
O13W K12 K2 126.2(9) 2_656 1_565
O13W K12 K9 49.6(8) 2_656 3_666
O13W K12 K10 121.1(9) 2_656 3_666
O13W K12 K11 46.4(8) 2_656 2_656
O19W K12 W2 96.0(11) . 1_565
O19W K12 K2 107.4(11) . 1_565
O19W K12 K9 124.2(12) . 3_666
O19W K12 K10 50.1(11) . 3_666
O19W K12 K11 56.3(11) . 2_656
O19W K12 K16 95.0(13) . 3_666
O19W K12 O7 88.2(12) . 1_565
O19W K12 O11W 174.1(15) . 2_656
O19W K12 O12W 93.1(14) . 1_565
O19W K12 O13W 94.2(13) . 2_656
O19W K12 O23W 151.9(18) . 2_656
O23W K12 W2 68.0(12) 2_656 1_565
O23W K12 K2 84.5(12) 2_656 1_565
O23W K12 K9 53.5(12) 2_656 3_666
O23W K12 K10 102.1(13) 2_656 3_666
O23W K12 K11 144.7(14) 2_656 2_656
O23W K12 K16 61.5(13) 2_656 3_666
O23W K12 O7 80.5(13) 2_656 1_565
O23W K12 O11W 31.2(12) 2_656 2_656
O23W K12 O12W 112.3(15) 2_656 1_565
O23W K12 O13W 98.9(15) 2_656 2_656
W6 K13 K3 108.3(5) 4_666 3_657
W6 K13 K6 98.5(5) 4_666 4_666
W6 K13 K21 103.1(7) 4_666 .
W8 K13 W6 55.2(3) 4_666 4_666
W8 K13 K3 56.6(3) 4_666 3_657
W8 K13 K6 103.2(5) 4_666 4_666
W8 K13 K21 153.4(8) 4_666 .
K1 K13 W6 71.2(5) . 4_666
K1 K13 W8 104.4(6) . 4_666
K1 K13 K3 108.0(6) . 3_657
K1 K13 K5 81.1(6) . 3_657
K1 K13 K6 136.1(7) . 4_666
K1 K13 K21 50.0(6) . .
K1 K13 O20 84.1(6) . 4_666
K1 K13 O24 86.6(6) . 4_666
K1 K13 O26 135.4(8) . 4_666
K5 K13 W6 113.6(6) 3_657 4_666
K5 K13 W8 77.0(5) 3_657 4_666
K5 K13 K3 30.7(3) 3_657 3_657
K5 K13 K6 138.5(7) 3_657 4_666
K5 K13 K21 102.4(8) 3_657 .
K5 K13 O20 144.1(8) 3_657 4_666
K6 K13 K3 115.7(5) 4_666 3_657
K6 K13 K21 94.6(7) 4_666 .
K21 K13 K3 131.5(7) . 3_657
O20 K13 W6 30.6(3) 4_666 4_666
O20 K13 W8 75.3(5) 4_666 4_666
O20 K13 K3 131.9(6) 4_666 3_657
O20 K13 K6 70.8(5) 4_666 4_666
O20 K13 K21 92.5(7) 4_666 .
O24 K13 W6 26.3(3) 4_666 4_666
O24 K13 W8 28.8(3) 4_666 4_666
O24 K13 K3 83.4(6) 4_666 3_657
O24 K13 K5 96.3(7) 4_666 3_657
O24 K13 K6 102.5(6) 4_666 4_666
O24 K13 K21 127.9(8) 4_666 .
O24 K13 O20 50.2(5) 4_666 4_666
O24 K13 O26 52.4(5) 4_666 4_666
O26 K13 W6 75.2(5) 4_666 4_666
O26 K13 W8 31.0(3) 4_666 4_666
O26 K13 K3 56.8(4) 4_666 3_657
O26 K13 K5 86.4(6) 4_666 3_657
O26 K13 K6 76.9(5) 4_666 4_666
O26 K13 K21 170.8(9) 4_666 .
O26 K13 O20 81.6(6) 4_666 4_666
W3 K14 W5 57.0(3) . .
W3 K14 K2 117.3(5) . 3_656
W3 K14 K6 80.0(4) . .
W3 K14 K11 55.5(4) . .
W5 K14 K2 60.4(3) . 3_656
W5 K14 K6 51.7(3) . .
W5 K14 K11 81.4(4) . .
K2 K14 K11 113.1(5) 3_656 .
K6 K14 K2 59.4(3) . 3_656
K6 K14 K11 53.9(4) . .
K15 K14 W3 73.7(5) . .
K15 K14 W5 67.8(5) . .
K15 K14 K2 86.1(5) . 3_656
K15 K14 K6 118.9(6) . .
K15 K14 K11 129.1(7) . .
K15 K14 O19 81.2(6) . .
O11 K14 W3 25.6(3) . .
O11 K14 W5 80.4(5) . .
O11 K14 K2 138.5(7) . 3_656
O11 K14 K6 86.6(6) . .
O11 K14 K11 42.5(5) . .
O11 K14 K15 91.5(7) . .
O11 K14 O12 54.9(5) . .
O11 K14 O19 100.9(7) . .
O11 K14 O16W 137.4(12) . 3_656
O11 K14 O18W 53.5(9) . .
O12 K14 W3 30.2(3) . .
O12 K14 W5 27.3(3) . .
O12 K14 K2 87.6(5) . 3_656
O12 K14 K6 65.4(5) . .
O12 K14 K11 69.7(5) . .
O12 K14 K15 64.4(6) . .
O12 K14 O19 51.5(4) . .
O12 K14 O16W 141.0(11) . 3_656
O12 K14 O18W 108.4(11) . .
O14 K14 W3 140.6(7) 3_656 .
O14 K14 W5 91.8(6) 3_656 .
O14 K14 K2 41.7(4) 3_656 3_656
O14 K14 K6 100.0(6) 3_656 .
O14 K14 K11 150.8(7) 3_656 .
O14 K14 K15 72.1(6) 3_656 .
O14 K14 O11 163.6(9) 3_656 .
O14 K14 O12 114.2(7) 3_656 .
O14 K14 O19 75.9(6) 3_656 .
O14 K14 O16W 59.0(10) 3_656 3_656
O14 K14 O18W 134.3(11) 3_656 .
O19 K14 W3 80.1(5) . .
O19 K14 W5 24.8(3) . .
O19 K14 K2 37.8(3) . 3_656
O19 K14 K6 40.0(3) . .
O19 K14 K11 87.2(5) . .
O16W K14 W3 153.2(11) 3_656 .
O16W K14 W5 116.7(10) 3_656 .
O16W K14 K2 62.0(9) 3_656 3_656
O16W K14 K6 77.7(10) 3_656 .
O16W K14 K11 98.9(11) 3_656 .
O16W K14 K15 130.7(12) 3_656 .
O16W K14 O19 92.0(10) 3_656 .
O18W K14 W3 78.4(9) . .
O18W K14 W5 133.5(10) . .
O18W K14 K2 157.7(10) . 3_656
O18W K14 K6 112.4(10) . .
O18W K14 K11 61.1(9) . .
O18W K14 K15 114.6(11) . .
O18W K14 O19 148.0(11) . .
O18W K14 O16W 96.6(13) . 3_656
W4 K15 W5 103.8(5) . 3_656
W4 K15 K15 63.4(5) . 3_656
K2 K15 W4 65.2(4) . .
K2 K15 W5 73.0(4) . 3_656
K2 K15 K14 167.6(8) . .
K2 K15 K15 98.0(8) . 3_656
K2 K15 O9 90.6(6) . .
K14 K15 W4 112.5(7) . .
K14 K15 W5 118.8(7) . 3_656
K14 K15 K15 91.1(8) . 3_656
K15 K15 W5 63.3(6) 3_656 3_656
O9 K15 W4 74.8(5) . .
O9 K15 W5 162.1(7) . 3_656
O9 K15 K14 77.1(6) . .
O9 K15 K15 128.0(9) . 3_656
O10 K15 W4 27.9(3) . .
O10 K15 W5 122.4(6) . 3_656
O10 K15 K2 59.9(5) . .
O10 K15 K14 111.9(8) . .
O10 K15 K15 91.2(8) . 3_656
O10 K15 O9 50.3(4) . .
O16 K15 W4 31.1(3) . .
O16 K15 W4 107.3(6) 3_656 .
O16 K15 W5 104.9(6) . 3_656
O16 K15 W5 24.8(3) 3_656 3_656
O16 K15 K2 96.3(7) 3_656 .
O16 K15 K2 94.6(6) . .
O16 K15 K14 95.9(7) 3_656 .
O16 K15 K14 86.0(7) . .
O16 K15 K15 45.2(5) . 3_656
O16 K15 K15 50.0(5) 3_656 3_656
O16 K15 O9 172.9(9) 3_656 .
O16 K15 O9 83.2(6) . .
O16 K15 O10 133.3(8) 3_656 .
O16 K15 O10 52.6(5) . .
O16 K15 O16 95.2(7) 3_656 .
O16 K15 O20W 129.0(12) 3_656 .
O20W K15 W4 118.4(10) . .
O20W K15 W5 116.6(10) . 3_656
O20W K15 K2 83.8(10) . .
O20W K15 K14 87.2(10) . .
O20W K15 K15 177.9(13) . 3_656
O20W K15 O9 52.7(9) . .
O20W K15 O10 90.5(10) . .
O20W K15 O16 135.8(12) . .
W19 K16 W18 50.4(3) 1_554 1_554
K8 K16 W18 131.0(8) 3_656 1_554
K8 K16 W19 80.6(6) 3_656 1_554
K8 K16 K9 103.1(9) 3_656 .
K8 K16 K10 89.3(8) 3_656 .
K8 K16 O70 130.2(9) 3_656 1_554
K8 K16 O71 105.9(9) 3_656 1_554
K8 K16 O73 76.7(7) 3_656 1_554
K8 K16 O11W 93.1(9) 3_656 4_565
K9 K16 W18 97.9(7) . 1_554
K9 K16 W19 116.2(8) . 1_554
K9 K16 K10 167.4(10) . .
K9 K16 O70 72.7(6) . 1_554
K9 K16 O73 90.2(7) . 1_554
K9 K16 O11W 57.9(7) . 4_565
K10 K16 W18 71.6(5) . 1_554
K10 K16 W19 62.8(5) . 1_554
K12 K16 W18 102.5(8) 3_666 1_554
K12 K16 W19 141.5(10) 3_666 1_554
K12 K16 K8 120.4(11) 3_666 3_656
K12 K16 K9 91.6(9) 3_666 .
K12 K16 K10 84.2(8) 3_666 .
K12 K16 O70 109.3(10) 3_666 1_554
K12 K16 O71 114.4(10) 3_666 1_554
K12 K16 O73 161.7(11) 3_666 1_554
K12 K16 O11W 48.2(8) 3_666 4_565
K12 K16 O23W 57.5(13) 3_666 4_565
O70 K16 W18 26.1(3) 1_554 1_554
O70 K16 W19 60.0(4) 1_554 1_554
O70 K16 K10 97.4(7) 1_554 .
O71 K16 W18 28.4(3) 1_554 1_554
O71 K16 W19 28.7(3) 1_554 1_554
O71 K16 K9 121.4(9) 1_554 .
O71 K16 K10 51.1(5) 1_554 .
O71 K16 O70 49.6(5) 1_554 1_554
O71 K16 O73 50.3(5) 1_554 1_554
O71 K16 O11W 160.0(11) 1_554 4_565
O73 K16 W18 59.3(4) 1_554 1_554
O73 K16 W19 27.5(3) 1_554 1_554
O73 K16 K10 90.2(7) 1_554 .
O73 K16 O70 54.1(5) 1_554 1_554
O11W K16 W18 135.1(9) 4_565 1_554
O11W K16 W19 170.3(10) 4_565 1_554
O11W K16 K10 124.8(9) 4_565 .
O11W K16 O70 120.9(9) 4_565 1_554
O11W K16 O73 143.7(10) 4_565 1_554
O23W K16 W18 154.7(15) 4_565 1_554
O23W K16 W19 154.8(15) 4_565 1_554
O23W K16 K8 74.2(13) 4_565 3_656
O23W K16 K9 69.8(13) 4_565 .
O23W K16 K10 116.9(14) 4_565 .
O23W K16 O70 139.4(15) 4_565 1_554
O23W K16 O71 167.7(16) 4_565 1_554
O23W K16 O73 139.4(15) 4_565 1_554
O23W K16 O11W 20.0(12) 4_565 4_565
W12 K17 W13 49.6(3) . .
W12 K17 W15 75.8(5) . .
W12 K17 K9 101.1(6) . 4_566
W12 K17 K18 56.9(6) . .
W13 K17 W15 53.7(4) . .
W13 K17 K9 128.5(7) . 4_566
W13 K17 K18 106.4(7) . .
W15 K17 K9 81.1(5) . 4_566
W15 K17 K18 107.7(8) . .
K18 K17 K9 61.4(6) . 4_566
K19 K17 W12 99.5(9) 3_556 .
K19 K17 W13 110.9(10) 3_556 .
K19 K17 W15 163.2(11) 3_556 .
K19 K17 K9 115.7(10) 3_556 4_566
K19 K17 K18 82.0(10) 3_556 .
O49 K17 W12 28.6(3) . .
O49 K17 W13 27.4(4) . .
O49 K17 W15 74.3(6) . .
O49 K17 K9 127.7(8) . 4_566
O49 K17 K18 83.2(8) . .
O49 K17 K19 93.8(10) . 3_556
O49 K17 O52 50.5(6) . .
O49 K17 O18W 86.4(11) . 1_455
O50 K17 W12 27.0(3) . .
O50 K17 W13 61.4(5) . .
O50 K17 W15 61.0(5) . .
O50 K17 K9 76.6(6) . 4_566
O50 K17 K18 51.9(6) . .
O50 K17 K19 120.5(11) . 3_556
O50 K17 O49 51.2(5) . .
O50 K17 O52 59.9(6) . .
O50 K17 O18W 115.1(12) . 1_455
O52 K17 W12 62.0(5) . .
O52 K17 W13 26.8(3) . .
O52 K17 W15 27.1(3) . .
O52 K17 K9 106.5(8) . 4_566
O52 K17 K18 111.7(9) . .
O52 K17 K19 136.8(12) . 3_556
O52 K17 O18W 55.3(9) . 1_455
O55 K17 W12 73.9(6) . .
O55 K17 W13 72.6(6) . .
O55 K17 W15 25.7(4) . .
O55 K17 K9 57.5(5) . 4_566
O55 K17 K18 86.2(8) . .
O55 K17 K19 168.2(12) . 3_556
O55 K17 O49 84.9(8) . .
O55 K17 O50 50.4(6) . .
O55 K17 O52 49.0(6) . .
O55 K17 O18W 85.1(11) . 1_455
O18W K17 W12 111.1(11) 1_455 .
O18W K17 W13 61.6(9) 1_455 .
O18W K17 W15 61.7(9) 1_455 .
O18W K17 K9 120.7(11) 1_455 4_566
O18W K17 K18 166.9(12) 1_455 .
O18W K17 K19 106.6(13) 1_455 3_556
O24W K17 W12 80.1(11) . .
O24W K17 W13 129.4(13) . .
O24W K17 W15 116.4(13) . .
O24W K17 K9 47.5(11) . 4_566
O24W K17 K18 23.3(10) . .
O24W K17 K19 77.9(13) . 3_556
O24W K17 O49 106.3(13) . .
O24W K17 O50 71.3(11) . .
O24W K17 O52 129.8(13) . .
O24W K17 O55 91.2(13) . .
O24W K17 O18W 166.5(16) . 1_455
W10 K18 W12 153.1(9) 4_565 .
W10 K18 K1 68.9(5) 4_565 4_565
W10 K18 K20 90.6(8) 4_565 4_565
W12 K18 K1 125.5(8) . 4_565
W12 K18 K20 106.2(9) . 4_565
K4 K18 W10 59.4(5) 4_565 4_565
K4 K18 W12 124.3(9) 4_565 .
K4 K18 K1 106.5(8) 4_565 4_565
K4 K18 K20 38.1(6) 4_565 4_565
K20 K18 K1 101.9(9) 4_565 4_565
O32 K18 W10 67.0(7) 4_565 4_565
O32 K18 W12 139.5(10) 4_565 .
O32 K18 K1 39.8(4) 4_565 4_565
O32 K18 K4 72.5(7) 4_565 4_565
O32 K18 K20 62.4(8) 4_565 4_565
O34 K18 W10 23.2(4) 4_565 4_565
O34 K18 W12 134.1(11) 4_565 .
O34 K18 K1 92.1(8) 4_565 4_565
O34 K18 K4 50.5(6) 4_565 4_565
O34 K18 K20 87.9(9) 4_565 4_565
O34 K18 O32 86.0(9) 4_565 4_565
O34 K18 O36 52.4(6) 4_565 4_565
O36 K18 W10 31.2(4) 4_565 4_565
O36 K18 W12 144.6(10) 4_565 .
O36 K18 K1 41.8(5) 4_565 4_565
O36 K18 K4 87.3(8) 4_565 4_565
O36 K18 K20 108.9(10) 4_565 4_565
O36 K18 O32 59.2(7) 4_565 4_565
O47 K18 W10 170.3(11) . 4_565
O47 K18 W12 23.4(4) . .
O47 K18 K1 120.7(9) . 4_565
O47 K18 K4 113.8(10) . 4_565
O47 K18 K20 86.1(9) . 4_565
O47 K18 O32 118.9(11) . 4_565
O47 K18 O34 147.2(12) . 4_565
O47 K18 O36 157.9(12) . 4_565
O8W K18 W10 100.1(10) . 4_565
O8W K18 W12 73.0(8) . .
O8W K18 K1 63.0(7) . 4_565
O8W K18 K4 159.4(13) . 4_565
O8W K18 K20 156.0(13) . 4_565
O8W K18 O32 102.0(11) . 4_565
O8W K18 O34 110.2(12) . 4_565
O8W K18 O36 73.2(9) . 4_565
O8W K18 O47 86.4(10) . .
O15W K18 W10 124.9(15) 4_565 4_565
O15W K18 W12 82.0(13) 4_565 .
O15W K18 K1 71.6(12) 4_565 4_565
O15W K18 K4 98.6(13) 4_565 4_565
O15W K18 K20 61.9(12) 4_565 4_565
O15W K18 O32 58.0(12) 4_565 4_565
O15W K18 O34 140.3(17) 4_565 4_565
O15W K18 O36 111.0(15) 4_565 4_565
O15W K18 O47 61.1(12) 4_565 .
O15W K18 O8W 94.6(14) 4_565 .
O24W K18 W10 81.9(15) . 4_565
O24W K18 W12 84.4(15) . .
O24W K18 K1 149.8(17) . 4_565
O24W K18 K4 48.7(13) . 4_565
O24W K18 K20 69.7(15) . 4_565
O24W K18 O32 121.1(17) . 4_565
O24W K18 O34 59.4(14) . 4_565
O24W K18 O36 111.7(17) . 4_565
O24W K18 O47 88.4(16) . .
O24W K18 O8W 132.8(19) . .
O24W K18 O15W 123(2) . 4_565
W11 K19 W12 51.0(5) . .
W11 K19 K4 94.2(9) . 2_546
W11 K19 K7 63.5(6) . 2_546
W12 K19 K4 137.8(11) . 2_546
W12 K19 K7 108.2(9) . 2_546
K4 K19 K7 63.8(6) 2_546 2_546
K17 K19 W11 170.2(13) 3_556 .
K17 K19 W12 138.0(13) 3_556 .
K17 K19 K4 79.2(9) 3_556 2_546
K17 K19 K7 106.9(10) 3_556 2_546
K20 K19 W11 68.0(10) 2_546 .
K20 K19 W12 99.0(12) 2_546 .
K20 K19 K4 39.9(8) 2_546 2_546
K20 K19 K7 79.3(10) 2_546 2_546
K20 K19 K17 109.6(14) 2_546 3_556
O43 K19 W11 28.0(5) . .
O43 K19 W12 27.6(5) . .
O43 K19 K4 122.1(13) . 2_546
O43 K19 K7 80.6(9) . 2_546
O43 K19 K17 157.8(16) . 3_556
O43 K19 K20 92.1(13) . 2_546
O10W K19 W11 92.5(12) 2_546 .
O10W K19 W12 139.4(15) 2_546 .
O10W K19 K4 45.9(9) 2_546 2_546
O10W K19 K7 31.2(8) 2_546 2_546
O10W K19 K17 77.8(13) 2_546 3_556
O10W K19 K20 78.6(14) 2_546 2_546
O10W K19 O43 111.8(15) 2_546 .
W13 K20 K18 123.6(10) 2_556 4_666
K3 K20 W13 60.4(6) 2_556 2_556
K3 K20 K18 152.8(12) 2_556 4_666
K4 K20 W13 165.3(14) . 2_556
K4 K20 K3 126.0(13) . 2_556
K4 K20 K18 58.1(9) . 4_666
K4 K20 K19 86.5(13) . 2_556
K4 K20 O31 62.5(9) . .
K4 K20 O44 143.3(15) . 2_556
K19 K20 W13 79.4(11) 2_556 2_556
K19 K20 K3 120.5(13) 2_556 2_556
K19 K20 K18 85.5(11) 2_556 4_666
O31 K20 W13 131.6(12) . 2_556
O31 K20 K3 81.8(10) . 2_556
O31 K20 K18 78.0(10) . 4_666
O31 K20 K19 149.0(16) . 2_556
O44 K20 W13 26.1(5) 2_556 2_556
O44 K20 K3 53.5(7) 2_556 2_556
O44 K20 K18 142.9(14) 2_556 4_666
O44 K20 K19 70.7(11) 2_556 2_556
O44 K20 O31 135.3(15) 2_556 .
W1 K21 W3 50.0(4) . .
W1 K21 W9 54.3(5) . .
W3 K21 W9 74.5(6) . .
K1 K21 W1 63.6(6) . .
K1 K21 W3 113.0(10) . .
K1 K21 W9 59.6(6) . .
K1 K21 K11 164.9(12) . .
K1 K21 O13 113.4(11) . .
K1 K21 O27 83.1(9) . .
K1 K21 O17W 104.2(13) . .
K1 K21 Li1 90.5(15) . 2_646
K11 K21 W1 113.7(10) . .
K11 K21 W3 64.0(7) . .
K11 K21 W9 106.2(9) . .
K11 K21 Li1 78.3(14) . 2_646
O3 K21 W1 28.7(4) . .
O3 K21 W3 26.0(4) . .
O3 K21 W9 73.1(8) . .
O3 K21 K1 91.5(10) . .
O3 K21 K11 88.7(10) . .
O3 K21 O4 51.3(7) . .
O3 K21 O13 50.1(6) . .
O3 K21 O27 83.4(9) . .
O3 K21 O17W 51.9(10) . .
O3 K21 O21W 151.8(17) . 4_666
O3 K21 Li1 132.3(16) . 2_646
O4 K21 W1 28.7(4) . .
O4 K21 W3 61.7(7) . .
O4 K21 W9 25.7(4) . .
O4 K21 K1 55.6(7) . .
O4 K21 K11 114.3(11) . .
O4 K21 O13 58.3(7) . .
O4 K21 O27 48.9(6) . .
O4 K21 O17W 98.1(13) . .
O4 K21 Li1 92.9(15) . 2_646
O13 K21 W1 62.8(6) . .
O13 K21 W3 28.8(4) . .
O13 K21 W9 58.1(6) . .
O13 K21 K11 56.2(7) . .
O13 K21 O27 46.9(6) . .
O13 K21 O17W 91.1(12) . .
O13 K21 Li1 85.9(14) . 2_646
O27 K21 W1 74.5(7) . .
O27 K21 W3 72.8(7) . .
O27 K21 W9 26.8(3) . .
O27 K21 K11 82.0(9) . .
O27 K21 Li1 49.6(12) . 2_646
O17W K21 W1 69.5(10) . .
O17W K21 W3 62.8(10) . .
O17W K21 W9 123.2(12) . .
O17W K21 K11 87.7(12) . .
O17W K21 O27 134.4(14) . .
O17W K21 Li1 164.9(19) . 2_646
O21W K21 W1 124.6(15) 4_666 .
O21W K21 W3 170.1(15) 4_666 .
O21W K21 W9 95.6(13) 4_666 .
O21W K21 K1 61.0(12) 4_666 .
O21W K21 K11 119.5(15) 4_666 .
O21W K21 O4 109.4(15) 4_666 .
O21W K21 O13 143.7(16) 4_666 .
O21W K21 O27 98.1(14) 4_666 .
O21W K21 O17W 125.2(16) 4_666 .
O21W K21 Li1 59.5(16) 4_666 2_646
Li1 K21 W1 121.4(15) 2_646 .
Li1 K21 W3 114.6(14) 2_646 .
Li1 K21 W9 67.1(13) 2_646 .
W1 O1 K1 104.1(5) . .
W1 O1 K5 166.6(7) . 3_657
K5 O1 K1 80.0(4) 3_657 .
W1 O2 W2 119.3(6) . .
W1 O2 K8 96.0(5) . .
W1 O2 K10 119.1(6) . 3_656
W2 O2 K8 94.8(5) . .
W2 O2 K10 119.7(6) . 3_656
K10 O2 K8 93.3(5) 3_656 .
W1 O3 K21 106.2(9) . .
W3 O3 W1 121.1(6) . .
W3 O3 K21 111.0(9) . .
W1 O4 K1 101.9(4) . .
W1 O4 K21 102.5(8) . .
W9 O4 W1 147.4(6) . .
W9 O4 K1 98.5(5) . .
W9 O4 K21 109.1(8) . .
K1 O4 K21 64.7(7) . .
W1 O5 W10 146.2(7) . .
W1 O5 K8 113.2(6) . .
W10 O5 K8 98.3(5) . .
W2 O6 W1 91.7(4) . .
W2 O6 W3 94.1(4) . .
W3 O6 W1 91.0(4) . .
As1 O6 W1 119.7(6) . .
As1 O6 W2 117.6(5) . .
As1 O6 W3 132.8(6) . .
W2 O7 K2 106.8(5) . .
W2 O7 K12 143.5(8) . 1_545
K12 O7 K2 92.4(6) 1_545 .
W2 O8 K8 116.0(6) . .
W2 O9 K15 98.6(6) . .
W3 O9 W2 120.8(6) . .
W3 O9 K15 110.2(6) . .
W2 O10 K2 99.2(5) . .
W2 O10 K15 109.6(6) . .
W4 O10 W2 147.5(7) . .
W4 O10 K2 98.7(5) . .
W4 O10 K15 102.7(6) . .
K15 O10 K2 62.4(5) . .
W3 O11 K11 106.2(7) . .
W3 O11 K14 106.2(7) . .
K14 O11 K11 99.1(7) . .
W3 O12 W5 156.4(7) . .
W3 O12 K14 94.8(6) . .
W5 O12 K14 105.0(6) . .
W3 O13 K11 100.1(6) . .
W3 O13 K21 98.8(8) . .
W7 O13 W3 148.4(7) . .
W7 O13 K11 98.9(6) . .
W7 O13 K21 112.1(9) . .
K11 O13 K21 65.2(8) . .
W4 O14 K2 106.1(6) . .
W4 O14 K14 148.3(9) . 3_656
K14 O14 K2 100.8(6) 3_656 .
W4 O15 Sm1 148.2(6) . .
W4 O16 K15 115.7(7) . 3_656
W4 O16 K15 98.9(6) . .
W5 O16 W4 120.3(6) . .
W5 O16 K15 114.6(6) . .
W5 O16 K15 115.3(7) . 3_656
K15 O16 K15 84.8(7) 3_656 .
W6 O17 W4 118.8(6) . .
W4 O18 W5 91.2(4) . .
W6 O18 W4 92.3(4) . .
W6 O18 W5 92.2(4) . .
As1 O18 W4 117.5(5) . .
As1 O18 W5 134.9(6) . .
As1 O18 W6 118.5(5) . .
W5 O19 K2 147.5(7) . 3_656
W5 O19 K6 105.9(6) . .
W5 O19 K14 99.1(6) . .
K2 O19 K6 103.9(5) 3_656 .
K2 O19 K14 93.4(5) 3_656 .
K6 O19 K14 90.4(5) . .
W5 O20 W6 121.8(6) . .
W5 O20 K13 116.2(6) . 4_565
W6 O20 K13 95.0(6) . 4_565
W5 O21 K6 97.3(6) . .
W7 O21 W5 149.2(7) . .
W7 O21 K6 103.4(5) . .
W6 O22 K1 127.7(6) . 4_565
W6 O23 Sm1 137.9(6) . .
W6 O23 Sm3 131.8(6) . .
Sm3 O23 Sm1 89.3(4) . .
W6 O24 W8 147.3(7) . .
W6 O24 K13 109.3(7) . 4_565
W8 O24 K13 103.4(7) . 4_565
W7 O25 K6 101.4(6) . .
W7 O25 K11 106.6(7) . .
K11 O25 K6 84.5(5) . .
W7 O26 W8 122.3(6) . .
W7 O26 K13 112.8(7) . 4_565
W8 O26 K13 97.6(6) . 4_565
W7 O27 K21 105.6(8) . .
W9 O27 W7 120.5(6) . .
W9 O27 K21 100.0(8) . .
W8 O28 W7 94.1(4) . .
W8 O28 W9 92.4(4) . .
W9 O28 W7 90.6(4) . .
As1 O28 W7 134.4(6) . .
As1 O28 W8 116.0(5) . .
As1 O28 W9 119.5(6) . .
W8 O29 K3 131.7(7) . 2_556
W8 O29 K5 132.1(8) . 2_556
K3 O29 K5 53.3(4) 2_556 2_556
W8 O30 Sm3 137.0(6) . .
W8 O30 K4 101.1(6) . .
Sm3 O30 K4 100.9(5) . .
W8 O31 K4 100.9(5) . .
W8 O31 K20 112.0(9) . .
W9 O31 W8 120.0(6) . .
W9 O31 K4 108.8(5) . .
W9 O31 K20 127.8(9) . .
K4 O31 K20 54.9(8) . .
W9 O32 K1 105.2(6) . .
W9 O32 K18 123.2(8) . 4_666
K1 O32 K18 93.6(7) . 4_666
W9 O33 K4 102.4(5) . .
W10 O33 W9 147.1(6) . .
W10 O33 K4 99.2(5) . .
W10 O34 K4 108.2(6) . .
W10 O34 K9 123.6(7) . 1_556
W10 O34 K18 110.3(8) . 4_666
K4 O34 K18 75.2(7) . 4_666
K9 O34 K4 119.6(6) 1_556 .
K9 O34 K18 109.3(8) 1_556 4_666
W10 O35 Sm2 153.9(6) . .
W10 O36 K1 141.7(5) . .
W10 O36 K18 98.9(7) . 4_666
K1 O36 K18 93.4(7) . 4_666
C1 O36 W10 116.9(11) . .
C1 O36 K1 90.9(10) . .
C1 O36 K18 112.1(13) . 4_666
W10 O37 K8 103.4(5) . .
C2 O37 W10 123.1(11) . .
C2 O37 K8 101.8(13) . .
K5 O38 K1 84.8(5) 3_657 .
C1 O38 K1 96.3(11) . .
C1 O38 K5 117.1(13) . 3_657
C4 O39 Sm2 137.4(12) . 3_657
C4 O40 K7 112.7(13) . 4_666
W11 O41 K7 158.1(6) . 2_546
W11 O42 Sm1 110.7(5) . .
W11 O42 Sm2 146.9(6) . .
Sm2 O42 Sm1 101.9(4) . .
W11 O43 W12 120.1(6) . .
W11 O43 Sm1 99.5(4) . .
W11 O43 K19 109.7(10) . .
W12 O43 Sm1 98.6(5) . .
W12 O43 K19 111.0(9) . .
Sm1 O43 K19 117.5(9) . .
W11 O44 K3 101.2(5) . .
W11 O44 K20 122.4(9) . 2_546
W13 O44 W11 122.8(6) . .
W13 O44 K3 101.4(5) . .
W13 O44 K20 113.9(9) . 2_546
K20 O44 K3 75.7(9) 2_546 .
W11 O45 W19 149.4(7) . .
W11 O45 K3 102.5(5) . .
W19 O45 K3 106.9(5) . .
W11 O46 W13 91.6(4) . .
W12 O46 W11 94.0(4) . .
W12 O46 W13 91.3(4) . .
As2 O46 W11 118.4(6) . .
As2 O46 W12 118.7(6) . .
As2 O46 W13 133.4(6) . .
W12 O47 K18 111.1(9) . .
W12 O48 Sm1 109.8(5) . .
W12 O48 Sm3 150.0(6) . .
Sm3 O48 Sm1 100.0(4) . .
W12 O49 K17 100.4(7) . .
W13 O49 W12 121.9(6) . .
W13 O49 K17 103.5(7) . .
W12 O50 W14 149.3(6) . .
W12 O50 K17 103.3(7) . .
W14 O50 K17 106.5(7) . .
W13 O52 W15 149.9(7) . .
W13 O52 K17 103.7(8) . .
W15 O52 K17 104.7(7) . .
W13 O53 W17 151.4(7) . .
W13 O53 K3 103.0(6) . .
W17 O53 K3 103.7(6) . .
W14 O54 K9 140.1(8) . 4_566
W14 O55 K17 105.5(8) . .
W15 O55 W14 120.4(6) . .
W15 O55 K17 108.8(8) . .
W14 O56 Sm3 154.7(7) . .
W14 O56 K7 93.6(5) . .
Sm3 O56 K7 105.1(5) . .
W14 O57 W16 119.1(6) . .
W14 O57 K7 102.2(6) . .
W16 O57 K7 103.5(5) . .
W14 O58 W15 92.2(4) . .
W16 O58 W14 91.4(4) . .
W16 O58 W15 93.9(4) . .
As2 O58 W14 117.4(6) . .
As2 O58 W15 134.8(6) . .
As2 O58 W16 117.0(6) . .
W15 O59 K11 146.2(9) . 1_455
W15 O60 W16 120.9(6) . .
W17 O61 W15 156.3(7) . .
W16 O62 K2 147.1(7) . 2_556
W16 O62 K6 99.5(6) . 4_566
K2 O62 K6 90.4(4) 2_556 4_566
W16 O63 K7 98.3(5) . .
W16 O64 W18 144.2(7) . .
W16 O64 K6 107.1(6) . 4_566
W18 O64 K6 98.4(5) . 4_566
W17 O66 W18 120.8(6) . .
W17 O67 W19 122.1(6) . .
W17 O67 K3 105.5(6) . .
W17 O67 K5 147.1(6) . .
W19 O67 K3 105.7(5) . .
W19 O67 K5 88.1(5) . .
K3 O67 K5 48.6(3) . .
W18 O68 W17 93.8(4) . .
W18 O68 W19 92.4(4) . .
W19 O68 W17 92.1(4) . .
As2 O68 W17 131.9(6) . .
As2 O68 W18 117.9(6) . .
As2 O68 W19 119.4(5) . .
W18 O69 K6 102.4(6) . 4_566
W18 O70 K16 95.3(7) . 1_556
W18 O71 K10 131.6(6) . 1_556
W18 O71 K16 106.7(7) . 1_556
W19 O71 W18 118.6(6) . .
W19 O71 K10 107.4(6) . 1_556
W19 O71 K16 103.5(7) . 1_556
K10 O71 K16 74.5(6) 1_556 1_556
W19 O72 K5 110.9(7) . .
W19 O72 K10 98.2(6) . 1_556
K5 O72 K10 103.6(5) . 1_556
W19 O73 Sm2 153.9(7) . .
W19 O73 K16 91.6(6) . 1_556
Sm2 O73 K16 109.4(6) . 1_556
Sm1 O74 Sm2 97.7(4) . .
Sm1 O74 Sm3 97.5(4) . .
Sm3 O74 Sm2 147.5(5) . .
O36 C1 K1 66.0(9) . .
O36 C1 C2 115.3(15) . .
O38 C1 K1 61.2(10) . .
O38 C1 O36 122.5(17) . .
O38 C1 C2 122.1(18) . .
C2 C1 K1 154.0(15) . .
O37 C2 C1 107.9(16) . .
O37 C2 H2 108.5 . .
O37 C2 C3 113.1(18) . .
C1 C2 H2 108.5 . .
C3 C2 C1 110.3(18) . .
C3 C2 H2 108.5 . .
K7 C3 H3A 63.5 4_666 .
K7 C3 H3B 62.7 4_666 .
C2 C3 K7 161.7(13) . 4_666
C2 C3 H3A 108.0 . .
C2 C3 H3B 108.0 . .
C2 C3 C4 117.0(18) . .
H3A C3 H3B 107.3 . .
C4 C3 K7 81.2(12) . 4_666
C4 C3 H3A 108.0 . .
C4 C3 H3B 108.0 . .
O39 C4 K7 153.3(12) . 4_666
O39 C4 C3 119(2) . .
O40 C4 K7 47.9(10) . 4_666
O40 C4 O39 123.4(17) . .
O40 C4 C3 117(2) . .
C3 C4 K7 74.1(12) . 4_666
Sm1 O1W K7 149.1(6) . 2_546
Sm2 O3W Sm1 94.1(4) . .
Sm2 O4W K8 115.9(5) . 3_657
Sm2 O4W K9 103.1(5) . 1_556
K8 O4W K9 99.8(5) 3_657 1_556
Sm2 O5W K9 115.7(5) . 1_556
Sm3 O6W K7 117.1(6) . .
Sm3 O7W K4 106.3(5) . .
Sm3 O8W K18 136.2(10) . .
K7 O10W K4 108.5(11) . .
K19 O10W K4 94.8(12) 2_556 .
K19 O10W K7 119.8(14) 2_556 .
K9 O11W K16 55.8(7) 4_666 4_666
K12 O11W K9 89.2(9) 2_646 4_666
K12 O11W K16 47.3(8) 2_646 4_666
O23W O11W K9 82(2) . 4_666
O23W O11W K12 69(2) . 2_646
O23W O11W K16 40(2) . 4_666
K12 O12W K2 99.8(12) 1_545 .
K9 O13W K11 165.5(13) 4_666 .
K12 O13W K9 86.1(10) 2_646 4_666
K12 O13W K11 92.3(11) 2_646 .
K14 O18W K17 110.0(14) . 1_655
K12 O19W K10 95.0(14) . 3_666
K21 O21W K1 63.4(12) 4_565 4_565
K5 O22W K10 106.7(15) . 1_556
K9 O23W K8 92.3(13) 4_666 2_656
K12 O23W K8 110.9(16) 2_646 2_656
K12 O23W K9 89.4(15) 2_646 4_666
K12 O23W K16 61.0(13) 2_646 4_666
K16 O23W K8 59.2(12) 4_666 2_656
K16 O23W K9 63.1(12) 4_666 4_666
O11W O23W K8 163(3) . 2_656
O11W O23W K9 74(2) . 4_666
O11W O23W K12 80(3) . 2_646
O11W O23W K16 120(3) . 4_666
K17 O24W K4 126.0(17) . 4_565
K18 O24W K4 94.7(18) . 4_565
K18 O24W K17 127(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 K1 3.862(6) .
W1 K8 4.089(15) .
W1 K10 4.026(14) 3_656
W1 K21 4.00(4) .
W1 O1 1.751(12) .
W1 O2 1.915(12) .
W1 O3 2.000(11) .
W1 O4 1.968(12) .
W1 O5 1.796(11) .
W1 O6 2.380(11) .
W2 K2 3.950(8) .
W2 K8 4.083(15) .
W2 K10 4.080(13) 3_656
W2 K12 4.035(17) 1_545
W2 O2 1.967(11) .
W2 O6 2.286(12) .
W2 O7 1.737(13) .
W2 O8 1.759(12) .
W2 O9 2.075(12) .
W2 O10 1.942(11) .
W3 K11 4.00(2) .
W3 K14 3.78(2) .
W3 K21 4.04(4) .
W3 O3 1.899(11) .
W3 O6 2.379(11) .
W3 O9 1.851(13) .
W3 O11 1.698(12) .
W3 O12 1.904(12) .
W3 O13 1.969(13) .
W4 K2 3.907(8) .
W4 K15 3.95(2) .
W4 O10 1.896(11) .
W4 O14 1.723(13) .
W4 O15 1.788(12) .
W4 O16 2.063(12) .
W4 O17 1.962(12) .
W4 O18 2.331(11) .
W5 K6 3.736(12) .
W5 K14 4.05(2) .
W5 K15 3.99(2) 3_656
W5 O12 1.921(12) .
W5 O16 1.846(13) .
W5 O18 2.415(11) .
W5 O19 1.722(13) .
W5 O20 1.846(12) .
W5 O21 1.980(13) .
W6 K1 4.102(6) 4_565
W6 K13 4.03(2) 4_565
W6 O17 1.931(12) .
W6 O18 2.319(11) .
W6 O20 2.058(12) .
W6 O22 1.730(12) .
W6 O23 1.802(12) .
W6 O24 1.895(13) .
W7 K6 3.809(12) .
W7 K11 3.923(19) .
W7 O13 1.893(13) .
W7 O21 1.853(13) .
W7 O25 1.715(13) .
W7 O26 1.856(12) .
W7 O27 1.993(12) .
W7 O28 2.367(11) .
W8 K4 3.868(12) .
W8 K13 3.93(2) 4_565
W8 O24 1.945(13) .
W8 O26 2.041(12) .
W8 O28 2.298(11) .
W8 O29 1.752(12) .
W8 O30 1.778(12) .
W8 O31 1.964(12) .
W9 K1 3.723(6) .
W9 K4 4.031(11) .
W9 K21 4.11(4) .
W9 O4 1.886(12) .
W9 O27 1.878(12) .
W9 O28 2.361(12) .
W9 O31 1.918(11) .
W9 O32 1.715(12) .
W9 O33 1.941(11) .
W10 K4 3.915(11) .
W10 K8 3.975(15) .
W10 K9 4.063(13) 1_556
W10 K18 4.11(3) 4_666
W10 O5 2.168(11) .
W10 O33 1.886(11) .
W10 O34 1.727(14) .
W10 O35 1.746(11) .
W10 O36 2.155(11) .
W10 O37 1.955(11) .
W11 Sm1 3.5197(12) .
W11 K3 3.807(11) .
W11 K19 3.99(4) .
W11 O41 1.710(13) .
W11 O42 1.862(10) .
W11 O43 1.987(12) .
W11 O44 1.947(11) .
W11 O45 1.867(11) .
W11 O46 2.368(11) .
W12 Sm1 3.5069(12) .
W12 K17 4.01(3) .
W12 K18 4.10(3) .
W12 K19 4.03(4) .
W12 O43 2.002(11) .
W12 O46 2.357(13) .
W12 O47 1.749(13) .
W12 O48 1.851(11) .
W12 O49 1.948(12) .
W12 O50 1.868(12) .
W13 K3 3.798(10) .
W13 K17 4.07(3) .
W13 K20 4.00(4) 2_546
W13 O44 1.926(12) .
W13 O46 2.377(11) .
W13 O49 1.925(13) .
W13 O51 1.730(12) .
W13 O52 1.889(13) .
W13 O53 1.874(15) .
W14 K7 3.812(14) .
W14 O50 1.958(13) .
W14 O54 1.730(13) .
W14 O55 2.020(13) .
W14 O56 1.763(11) .
W14 O57 1.917(12) .
W14 O58 2.350(12) .
W15 K17 4.14(3) .
W15 O52 1.951(13) .
W15 O55 1.892(14) .
W15 O58 2.361(11) .
W15 O59 1.747(13) .
W15 O60 1.856(14) .
W15 O61 1.925(12) .
W16 K6 3.895(12) 4_566
W16 K7 3.878(14) .
W16 O57 1.966(12) .
W16 O58 2.328(12) .
W16 O60 2.081(13) .
W16 O62 1.730(13) .
W16 O63 1.750(13) .
W16 O64 1.916(12) .
W17 K3 3.867(10) .
W17 O53 1.949(15) .
W17 O61 1.901(12) .
W17 O65 1.716(13) .
W17 O66 1.842(15) .
W17 O67 1.868(13) .
W17 O68 2.397(11) .
W18 K6 3.684(12) 4_566
W18 K16 3.99(2) 1_556
W18 O64 1.922(12) .
W18 O66 2.097(13) .
W18 O68 2.295(12) .
W18 O69 1.743(13) .
W18 O70 1.760(13) .
W18 O71 1.981(12) .
W19 K3 3.979(10) .
W19 K5 3.907(12) .
W19 K10 3.832(14) 1_556
W19 K16 3.85(2) 1_556
W19 O45 1.960(12) .
W19 O67 2.020(12) .
W19 O68 2.331(11) .
W19 O71 1.903(13) .
W19 O72 1.737(13) .
W19 O73 1.780(11) .
Sm1 Sm3 3.6569(14) .
Sm1 O15 2.348(12) .
Sm1 O23 2.624(12) .
Sm1 O42 2.400(12) .
Sm1 O43 2.595(11) .
Sm1 O48 2.418(12) .
Sm1 O74 2.428(11) .
Sm1 O1W 2.496(13) .
Sm1 O2W 2.509(13) .
Sm1 O3W 2.580(10) .
Sm2 K8 4.353(14) .
Sm2 K8 4.515(15) 3_657
Sm2 K9 4.484(13) 1_556
Sm2 O35 2.390(11) .
Sm2 O39 2.418(12) 3_657
Sm2 O42 2.379(11) .
Sm2 O73 2.318(12) .
Sm2 O74 2.501(11) .
Sm2 O3W 2.491(11) .
Sm2 O4W 2.505(12) .
Sm2 O5W 2.480(13) .
Sm3 K4 4.247(11) .
Sm3 K7 4.491(14) .
Sm3 O23 2.578(12) .
Sm3 O30 2.361(12) .
Sm3 O48 2.355(11) .
Sm3 O56 2.340(12) .
Sm3 O74 2.435(11) .
Sm3 O6W 2.513(15) .
Sm3 O7W 2.479(13) .
Sm3 O8W 2.436(15) .
As1 O6 1.786(11) .
As1 O18 1.792(10) .
As1 O28 1.794(11) .
As2 O46 1.776(12) .
As2 O58 1.791(11) .
As2 O68 1.796(12) .
K1 K5 3.843(13) 3_657
K1 K13 2.80(2) .
K1 K21 3.23(4) .
K1 O1 3.043(14) .
K1 O4 2.943(12) .
K1 O22 2.809(15) 4_666
K1 O32 2.887(14) .
K1 O36 3.003(13) .
K1 O38 2.897(15) .
K1 C1 3.286(19) .
K1 O21W 3.16(5) 4_666
K2 K6 4.454(14) 3_656
K2 K12 4.050(18) 1_545
K2 K15 3.22(2) .
K2 O7 3.081(15) .
K2 O10 3.142(15) .
K2 O14 3.061(17) .
K2 O19 2.779(15) 3_656
K2 O62 3.060(15) 2_546
K2 O9W 2.80(2) .
K2 O12W 2.89(3) .
K3 K5 2.647(16) .
K3 K13 4.79(2) 3_657
K3 K20 3.51(4) 2_546
K3 O29 2.826(17) 2_546
K3 O44 2.914(16) .
K3 O45 2.940(15) .
K3 O53 2.909(17) .
K3 O67 2.925(17) .
K4 K18 3.78(3) 4_666
K4 K20 2.75(4) .
K4 O30 3.111(17) .
K4 O31 2.981(16) .
K4 O33 3.142(16) .
K4 O34 3.015(18) .
K4 O7W 2.822(17) .
K4 O10W 3.08(3) .
K4 O24W 2.85(5) 4_666
K5 K1 3.843(13) 3_657
K5 K10 4.803(18) 1_556
K5 K13 3.10(2) 3_657
K5 O1 2.936(17) 3_657
K5 O29 3.055(18) 2_546
K5 O38 2.800(19) 3_657
K5 O67 3.412(18) .
K5 O72 2.935(19) .
K5 O22W 2.90(5) .
K6 W16 3.895(12) 4_665
K6 W18 3.684(12) 4_665
K6 K11 4.14(2) .
K6 K13 4.20(2) 4_565
K6 O19 2.877(18) .
K6 O21 2.925(18) .
K6 O25 3.078(18) .
K6 O62 3.218(19) 4_665
K6 O64 2.874(17) 4_665
K6 O69 2.894(18) 4_665
K7 O40 2.817(19) 4_565
K7 O41 3.095(19) 2_556
K7 O56 3.272(19) .
K7 O57 2.915(19) .
K7 O63 3.216(19) .
K7 C3 3.41(2) 4_565
K7 C4 3.50(3) 4_565
K7 O1W 3.104(19) 2_556
K7 O6W 2.75(2) .
K7 O10W 2.91(3) .
K8 K10 4.50(2) 3_656
K8 K16 2.90(3) 3_656
K8 O2 3.419(19) .
K8 O5 3.033(19) .
K8 O8 2.994(19) .
K8 O37 3.036(19) .
K8 O4W 2.82(2) 3_657
K8 O23W 3.25(5) 2_646
K9 W10 4.063(13) 1_554
K9 Sm2 4.484(13) 1_554
K9 K8 4.607(19) 3_656
K9 K12 3.90(2) 3_666
K9 K16 2.98(3) .
K9 O34 2.843(19) 1_554
K9 O54 2.823(18) 4_665
K9 O4W 3.196(18) 1_554
K9 O5W 2.812(18) 1_554
K9 O11W 3.05(3) 4_565
K9 O13W 2.98(4) 4_565
K9 O23W 3.14(5) 4_565
K10 W1 4.026(14) 3_656
K10 W2 4.080(13) 3_656
K10 W19 3.832(14) 1_554
K10 K5 4.803(18) 1_554
K10 K8 4.50(2) 3_656
K10 K12 4.04(2) 3_666
K10 K16 3.47(3) .
K10 O2 2.731(18) 3_656
K10 O71 2.806(18) 1_554
K10 O72 3.18(2) 1_554
K10 O19W 3.11(4) 3_666
K10 O22W 3.08(5) 1_554
K11 K12 4.14(3) 2_646
K11 K14 4.65(3) .
K11 K21 3.45(4) .
K11 O11 3.18(2) .
K11 O13 3.15(2) .
K11 O25 3.07(2) .
K11 O59 2.82(2) 1_655
K11 O13W 3.00(4) .
K12 W2 4.035(17) 1_565
K12 K2 4.050(18) 1_565
K12 K9 3.90(2) 3_666
K12 K10 4.04(2) 3_666
K12 K11 4.14(3) 2_656
K12 K16 2.44(3) 3_666
K12 O7 2.50(2) 1_565
K12 O11W 2.47(3) 2_656
K12 O12W 2.38(4) 1_565
K12 O13W 2.73(4) 2_656
K12 O19W 2.32(4) .
K12 O23W 2.35(5) 2_656
K13 W6 4.03(2) 4_666
K13 W8 3.93(2) 4_666
K13 K3 4.79(2) 3_657
K13 K5 3.10(2) 3_657
K13 K6 4.20(2) 4_666
K13 K21 4.21(4) .
K13 O20 3.29(2) 4_666
K13 O24 2.99(3) 4_666
K13 O26 3.10(2) 4_666
K14 K2 4.52(2) 3_656
K14 K15 3.37(3) .
K14 O11 2.93(2) .
K14 O12 3.11(2) .
K14 O14 2.80(2) 3_656
K14 O19 3.41(2) .
K14 O16W 3.13(5) 3_656
K14 O18W 3.10(5) .
K15 W5 3.99(2) 3_656
K15 K15 3.98(4) 3_656
K15 O9 3.29(2) .
K15 O10 3.07(2) .
K15 O16 2.83(2) 3_656
K15 O16 3.06(2) .
K15 O20W 2.96(4) .
K16 W18 3.99(2) 1_554
K16 W19 3.85(2) 1_554
K16 K8 2.90(3) 3_656
K16 K12 2.44(3) 3_666
K16 O70 3.42(3) 1_554
K16 O71 2.93(3) 1_554
K16 O73 3.37(3) 1_554
K16 O11W 3.30(4) 4_565
K16 O23W 2.45(5) 4_565
K17 K9 5.03(3) 4_566
K17 K18 4.55(5) .
K17 K19 3.60(5) 3_556
K17 O49 3.17(3) .
K17 O50 3.14(3) .
K17 O52 3.19(3) .
K17 O55 3.12(3) .
K17 O18W 3.37(5) 1_455
K17 O24W 2.82(6) .
K18 W10 4.11(3) 4_565
K18 K1 4.50(3) 4_565
K18 K4 3.78(3) 4_565
K18 K20 4.43(5) 4_565
K18 O32 3.28(4) 4_565
K18 O34 3.17(4) 4_565
K18 O36 3.18(4) 4_565
K18 O47 3.14(4) .
K18 O8W 2.81(4) .
K18 O15W 2.33(5) 4_565
K18 O24W 2.26(6) .
K19 K4 4.28(4) 2_546
K19 K7 4.87(4) 2_546
K19 K17 3.60(5) 3_556
K19 K20 3.45(6) 2_546
K19 O43 2.86(4) .
K19 O10W 2.72(5) 2_546
K20 W13 4.00(4) 2_556
K20 K3 3.51(4) 2_556
K20 K18 4.43(5) 4_666
K20 K19 3.45(6) 2_556
K20 O31 2.98(4) .
K20 O44 2.81(4) 2_556
K21 O3 2.95(4) .
K21 O4 3.08(4) .
K21 O13 3.24(4) .
K21 O27 3.34(4) .
K21 O17W 3.34(6) .
K21 O21W 2.98(6) 4_666
K21 Li1 3.49(8) 2_646
O1 K5 2.936(17) 3_657
O2 K10 2.731(18) 3_656
O7 K12 2.50(2) 1_545
O14 K14 2.80(2) 3_656
O16 K15 2.83(2) 3_656
O19 K2 2.779(15) 3_656
O20 K13 3.29(2) 4_565
O22 K1 2.809(15) 4_565
O24 K13 2.99(3) 4_565
O26 K13 3.10(2) 4_565
O29 K3 2.826(17) 2_556
O29 K5 3.055(18) 2_556
O32 K18 3.28(4) 4_666
O34 K9 2.843(19) 1_556
O34 K18 3.17(4) 4_666
O36 K18 3.18(4) 4_666
O36 C1 1.29(2) .
O37 C2 1.41(2) .
O38 K5 2.80(2) 3_657
O38 C1 1.26(2) .
O39 Sm2 2.418(12) 3_657
O39 C4 1.27(2) .
O40 K7 2.817(19) 4_666
O40 C4 1.26(2) .
O41 K7 3.095(19) 2_546
O44 K20 2.81(4) 2_546
O54 K9 2.823(18) 4_566
O59 K11 2.82(2) 1_455
O62 K2 3.060(15) 2_556
O62 K6 3.218(19) 4_566
O64 K6 2.874(17) 4_566
O69 K6 2.894(18) 4_566
O70 K16 3.42(3) 1_556
O71 K10 2.806(18) 1_556
O71 K16 2.93(3) 1_556
O72 K10 3.18(2) 1_556
O73 K16 3.37(3) 1_556
C1 C2 1.55(3) .
C2 H2 0.9800 .
C2 C3 1.42(3) .
C3 K7 3.41(2) 4_666
C3 H3A 0.9700 .
C3 H3B 0.9700 .
C3 C4 1.48(2) .
C4 K7 3.50(3) 4_666
O1W K7 3.104(19) 2_546
O4W K8 2.82(2) 3_657
O4W K9 3.196(18) 1_556
O5W K9 2.812(18) 1_556
O10W K19 2.72(5) 2_556
O11W K9 3.05(3) 4_666
O11W K12 2.47(3) 2_646
O11W K16 3.30(4) 4_666
O11W O23W 1.30(5) .
O12W K12 2.38(4) 1_545
O13W K9 2.98(4) 4_666
O13W K12 2.73(4) 2_646
O15W K18 2.33(5) 4_666
O16W K14 3.13(5) 3_656
O18W K17 3.37(5) 1_655
O19W K10 3.11(4) 3_666
O21W K1 3.16(5) 4_565
O21W K21 2.98(6) 4_565
O22W K10 3.08(5) 1_556
O23W K8 3.25(5) 2_656
O23W K9 3.14(5) 4_666
O23W K12 2.35(5) 2_646
O23W K16 2.45(5) 4_666
O24W K4 2.85(5) 4_565
Li1 K21 3.49(8) 2_656
