#------------------------------------------------------------------------------
#$Date: 2016-02-05 02:06:34 +0200 (Fri, 05 Feb 2016) $
#$Revision: 176079 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/53/7035368.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7035368
loop_
_publ_author_name
'Alvarez, Belén'
'Alvarez, M. Angeles'
'García, M Esther'
'Ruiz, Miguel A.'
_publ_section_title
;
 P-S bond cleavage in reactions of thiophosphinidene-bridged dimolybdenum
 complexes with [Co2(CO)8] to give phosphinidene-bridged heterometallic
 derivatives.
;
_journal_issue                   5
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1937
_journal_page_last               1952
_journal_paper_doi               10.1039/c5dt01450f
_journal_volume                  45
_journal_year                    2016
_chemical_compound_source        'synthesis as described'
_chemical_formula_moiety         'C32 H34 Co3 Mo O9 P'
_chemical_formula_sum            'C32 H34 Co3 Mo O9 P'
_chemical_formula_weight         866.29
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_conform_dict_location     ftp://ftp.iucr.org/pub/cif_core.dic
_audit_conform_dict_name         cif_core.dic
_audit_conform_dict_version      2.4
_audit_creation_method           'WinGX routine CIF_UPDATE'
_audit_update_record
;
2015-04-06 deposited with the CCDC.
2015-05-18 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 95.980(2)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   9.9372(2)
_cell_length_b                   15.6891(3)
_cell_length_c                   10.8895(2)
_cell_measurement_reflns_used    4278
_cell_measurement_temperature    100.0
_cell_measurement_theta_max      74.5566
_cell_measurement_theta_min      4.0785
_cell_measurement_wavelength     1.54184
_cell_volume                     1688.50(6)
_computing_cell_refinement
;
CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.31.7 (release 18-10-2006 CrysAlis171 .NET)
(compiled Oct 18 2006,16:28:17)
;
_computing_data_collection
;
CrysAlis CCD, Oxford Diffraction Ltd.,
Version 1.171.31.7 (release 18-10-2006 CrysAlis171 .NET)
(compiled Oct 18 2006,16:28:17)
;
_computing_data_reduction
;
CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.31.7 (release 18-10-2006 CrysAlis171 .NET)
(compiled Oct 18 2006,16:28:17)
;
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.942
_diffrn_measured_fraction_theta_max 0.942
_diffrn_measurement_device_type  'Xcalibur, Onyx, Nova'
_diffrn_measurement_method       CCD
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'Nova (Cu) X-ray Source'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.5418
_diffrn_reflns_av_R_equivalents  0.0865
_diffrn_reflns_av_unetI/netI     0.0823
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            5841
_diffrn_reflns_theta_full        74.72
_diffrn_reflns_theta_max         74.72
_diffrn_reflns_theta_min         4.08
_exptl_absorpt_coefficient_mu    15.199
_exptl_absorpt_correction_T_max  0.281
_exptl_absorpt_correction_T_min  0.109
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.36 (release 02-08-2010 CrysAlis171 .NET)
(compiled Aug  2 2010,13:00:58)
Analytical numeric absorption correction using a multifaceted crystal
            model based on expressions derived by R.C. Clark & J.S. Reid.
(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
;
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    1.704
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             872
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.12
_refine_diff_density_max         4.071
_refine_diff_density_min         -3.388
_refine_diff_density_rms         0.297
_refine_ls_extinction_coef       0.0018(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.034
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     214
_refine_ls_number_reflns         3397
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.034
_refine_ls_R_factor_all          0.0949
_refine_ls_R_factor_gt           0.0921
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1998P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2325
_refine_ls_wR_factor_ref         0.2395
_reflns_number_gt                3143
_reflns_number_total             3397
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            c5dt01450f1.cif
_cod_data_source_block           compound6
_cod_depositor_comments
'Adding full bibliography for 7035367--7035372.cif.'
_cod_database_code               7035368
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
'-x, -y, -z'
'x, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Mo1 Mo 0.54987(6) 0.25 0.36186(5) 0.0120(3) Uani 1 2 d S
Co1 Co 0.72149(13) 0.25 0.18949(11) 0.0134(4) Uani 1 2 d S
Co2 Co 0.80336(9) 0.33088(5) 0.37819(8) 0.0129(3) Uani 1 1 d .
P1 P 0.73177(19) 0.25 0.52132(17) 0.0115(4) Uani 1 2 d S
O1 O 0.5329(5) 0.0964(3) 0.1786(4) 0.0234(10) Uani 1 1 d .
O2 O 0.6185(7) 0.25 -0.0705(6) 0.0268(14) Uani 1 2 d S
O3 O 0.9254(6) 0.1251(4) 0.1460(4) 0.0365(13) Uani 1 1 d .
O4 O 0.7239(6) 0.5113(3) 0.3721(4) 0.0307(11) Uani 1 1 d .
O5 O 1.0788(5) 0.3504(3) 0.4988(4) 0.0269(10) Uani 1 1 d .
C1 C 0.5649(6) 0.1557(4) 0.2354(5) 0.0186(11) Uani 1 1 d .
C2 C 0.6595(9) 0.25 0.0300(7) 0.0166(16) Uani 1 2 d S
C3 C 0.8499(7) 0.1649(4) 0.1940(5) 0.0201(12) Uani 1 1 d .
C4 C 0.7554(6) 0.4405(4) 0.3762(5) 0.0199(12) Uani 1 1 d .
C5 C 0.9739(6) 0.3423(3) 0.4479(5) 0.0158(11) Uani 1 1 d .
C11 C 0.3239(6) 0.2049(4) 0.3331(6) 0.0229(12) Uani 1 1 d .
H11 H 0.2912 0.1703 0.2673 0.027 Uiso 1 1 calc R
C12 C 0.3816(6) 0.1762(4) 0.4494(6) 0.0241(13) Uani 1 1 d .
H12 H 0.3943 0.1198 0.4742 0.029 Uiso 1 1 calc R
C13 C 0.4169(9) 0.25 0.5220(8) 0.0250(19) Uani 1 2 d S
H13 H 0.4564 0.25 0.6032 0.03 Uiso 1 2 calc SR
C20 C 0.7947(7) 0.25 0.6861(7) 0.0117(14) Uiso 1 2 d S
C21 C 0.8447(6) 0.1725(3) 0.7410(5) 0.0158(11) Uani 1 1 d .
C22 C 0.9686(7) 0.1748(3) 0.8164(6) 0.0184(12) Uani 1 1 d .
H22 H 1.0059 0.1239 0.8477 0.022 Uiso 1 1 calc R
C23 C 1.0365(9) 0.25 0.8455(9) 0.0224(17) Uani 1 2 d S
C30 C 0.7754(7) 0.0839(3) 0.7329(5) 0.0188(12) Uani 1 1 d .
C31 C 0.6307(7) 0.0864(4) 0.6659(6) 0.0230(12) Uani 1 1 d .
H31A H 0.59 0.0311 0.6693 0.034 Uiso 1 1 calc R
H31B H 0.6344 0.1024 0.5812 0.034 Uiso 1 1 calc R
H31C H 0.5777 0.1273 0.7054 0.034 Uiso 1 1 calc R
C32 C 0.8612(7) 0.0182(4) 0.6721(6) 0.0225(13) Uani 1 1 d .
H32A H 0.8097 -0.0331 0.6559 0.034 Uiso 1 1 calc R
H32B H 0.9411 0.0057 0.7264 0.034 Uiso 1 1 calc R
H32C H 0.8865 0.0409 0.5959 0.034 Uiso 1 1 calc R
C33 C 0.7593(8) 0.0531(4) 0.8648(6) 0.0272(14) Uani 1 1 d .
H33A H 0.7064 0.0937 0.9051 0.041 Uiso 1 1 calc R
H33B H 0.8469 0.0476 0.9103 0.041 Uiso 1 1 calc R
H33C H 0.7145 -0.0012 0.8612 0.041 Uiso 1 1 calc R
C40 C 1.1840(9) 0.25 0.9031(9) 0.0251(18) Uiso 1 2 d S
C41 C 1.2698(17) 0.25 0.7981(15) 0.063(4) Uiso 1 2 d S
H41A H 1.3636 0.25 0.8299 0.095 Uiso 0.5 2 calc SPR
H41B H 1.2504 0.3 0.7485 0.095 Uiso 0.25 1 calc PR
H41C H 1.2504 0.2 0.7485 0.095 Uiso 0.25 1 calc PR
H41D H 1.2127 0.25 0.7214 0.095 Uiso 0.5 2 calc SPR
H41E H 1.3259 0.2 0.8028 0.095 Uiso 0.25 1 calc PR
H41F H 1.3259 0.3 0.8028 0.095 Uiso 0.25 1 calc PR
C42 C 1.2188(16) 0.1711(10) 0.9836(14) 0.083(4) Uiso 1 1 d .
H42A H 1.2203 0.1216 0.9319 0.125 Uiso 1 1 calc R
H42B H 1.1518 0.1638 1.0402 0.125 Uiso 1 1 calc R
H42C H 1.3061 0.1786 1.0291 0.125 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co -2.3653 3.6143 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -0.0483 2.7339 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Mo1 C1 93.2(3) . 4_565
C1 Mo1 C13 127.0(2) . .
C1 Mo1 C13 127.0(2) 4_565 .
C1 Mo1 C12 91.2(3) . .
C1 Mo1 C12 138.4(2) 4_565 .
C13 Mo1 C12 36.0(2) . .
C1 Mo1 C12 138.4(2) . 4_565
C1 Mo1 C12 91.2(3) 4_565 4_565
C13 Mo1 C12 36.0(2) . 4_565
C12 Mo1 C12 59.9(4) . 4_565
C1 Mo1 C11 80.0(2) . .
C1 Mo1 C11 105.4(2) 4_565 .
C13 Mo1 C11 58.8(3) . .
C12 Mo1 C11 35.2(2) . .
C12 Mo1 C11 58.9(2) 4_565 .
C1 Mo1 C11 105.4(2) . 4_565
C1 Mo1 C11 80.0(2) 4_565 4_565
C13 Mo1 C11 58.8(3) . 4_565
C12 Mo1 C11 58.9(2) . 4_565
C12 Mo1 C11 35.2(2) 4_565 4_565
C11 Mo1 C11 35.1(3) . 4_565
C1 Mo1 P1 113.01(17) . .
C1 Mo1 P1 113.01(17) 4_565 .
C13 Mo1 P1 84.2(2) . .
C12 Mo1 P1 103.06(17) . .
C12 Mo1 P1 103.06(17) 4_565 .
C11 Mo1 P1 138.06(16) . .
C11 Mo1 P1 138.06(16) 4_565 .
C1 Mo1 Co1 55.02(18) . .
C1 Mo1 Co1 55.02(18) 4_565 .
C13 Mo1 Co1 175.4(2) . .
C12 Mo1 Co1 146.26(18) . .
C12 Mo1 Co1 146.26(18) 4_565 .
C11 Mo1 Co1 125.49(15) . .
C11 Mo1 Co1 125.49(15) 4_565 .
P1 Mo1 Co1 91.19(6) . .
C1 Mo1 Co2 104.04(18) . .
C1 Mo1 Co2 65.58(17) 4_565 .
C13 Mo1 Co2 122.37(19) . .
C12 Mo1 Co2 151.58(17) . .
C12 Mo1 Co2 115.37(17) 4_565 .
C11 Mo1 Co2 170.03(16) . .
C11 Mo1 Co2 135.41(17) 4_565 .
P1 Mo1 Co2 49.00(4) . .
Co1 Mo1 Co2 53.78(3) . .
C1 Mo1 Co2 65.58(17) . 4_565
C1 Mo1 Co2 104.04(18) 4_565 4_565
C13 Mo1 Co2 122.37(19) . 4_565
C12 Mo1 Co2 115.37(17) . 4_565
C12 Mo1 Co2 151.58(17) 4_565 4_565
C11 Mo1 Co2 135.41(16) . 4_565
C11 Mo1 Co2 170.03(16) 4_565 4_565
P1 Mo1 Co2 49.00(4) . 4_565
Co1 Mo1 Co2 53.78(3) . 4_565
Co2 Mo1 Co2 53.70(4) . 4_565
C2 Co1 C3 101.2(3) . .
C2 Co1 C3 101.2(3) . 4_565
C3 Co1 C3 92.8(4) . 4_565
C2 Co1 C1 92.3(3) . .
C3 Co1 C1 90.6(3) . .
C3 Co1 C1 165.2(3) 4_565 .
C2 Co1 C1 92.3(3) . 4_565
C3 Co1 C1 165.2(3) . 4_565
C3 Co1 C1 90.6(3) 4_565 4_565
C1 Co1 C1 82.6(3) . 4_565
C2 Co1 Co2 149.14(3) . .
C3 Co1 Co2 100.50(19) . .
C3 Co1 Co2 56.01(19) 4_565 .
C1 Co1 Co2 109.17(16) . .
C1 Co1 Co2 69.68(15) 4_565 .
C2 Co1 Co2 149.14(3) . 4_565
C3 Co1 Co2 56.01(19) . 4_565
C3 Co1 Co2 100.50(19) 4_565 4_565
C1 Co1 Co2 69.68(15) . 4_565
C1 Co1 Co2 109.17(16) 4_565 4_565
Co2 Co1 Co2 61.57(5) . 4_565
C2 Co1 Mo1 120.4(3) . .
C3 Co1 Mo1 118.3(2) . .
C3 Co1 Mo1 118.3(2) 4_565 .
C1 Co1 Mo1 48.12(15) . .
C1 Co1 Mo1 48.12(15) 4_565 .
Co2 Co1 Mo1 66.11(4) . .
Co2 Co1 Mo1 66.11(4) 4_565 .
C4 Co2 C5 98.5(3) . .
C4 Co2 C3 92.5(3) . 4_565
C5 Co2 C3 96.2(3) . 4_565
C4 Co2 P1 117.5(2) . .
C5 Co2 P1 96.89(19) . .
C3 Co2 P1 144.83(17) 4_565 .
C4 Co2 Co1 114.78(19) . .
C5 Co2 Co1 128.06(19) . .
C3 Co2 Co1 46.54(17) 4_565 .
P1 Co2 Co1 101.00(5) . .
C4 Co2 Co2 164.6(2) . 4_565
C5 Co2 Co2 95.76(17) . 4_565
C3 Co2 Co2 91.79(17) 4_565 4_565
P1 Co2 Co2 54.51(4) . 4_565
Co1 Co2 Co2 59.21(2) . 4_565
C4 Co2 Mo1 101.4(2) . .
C5 Co2 Mo1 150.94(18) . .
C3 Co2 Mo1 103.78(17) 4_565 .
P1 Co2 Mo1 55.01(5) . .
Co1 Co2 Mo1 60.12(4) . .
Co2 Co2 Mo1 63.152(18) 4_565 .
C20 P1 Co2 126.41(17) . 4_565
C20 P1 Co2 126.41(17) . .
Co2 P1 Co2 70.98(7) 4_565 .
C20 P1 Mo1 150.5(2) . .
Co2 P1 Mo1 75.99(6) 4_565 .
Co2 P1 Mo1 75.99(6) . .
O1 C1 Mo1 157.0(6) . .
O1 C1 Co1 125.2(5) . .
Mo1 C1 Co1 76.9(2) . .
O2 C2 Co1 179.0(8) . .
O3 C3 Co1 150.3(5) . .
O3 C3 Co2 132.2(5) . 4_565
Co1 C3 Co2 77.4(2) . 4_565
O4 C4 Co2 178.5(5) . .
O5 C5 Co2 175.8(5) . .
C12 C11 C11 108.6(4) . 4_565
C12 C11 Mo1 71.4(4) . .
C11 C11 Mo1 72.43(17) 4_565 .
C12 C11 H11 125.7 . .
C11 C11 H11 125.7 4_565 .
Mo1 C11 H11 122.1 . .
C11 C12 C13 107.0(6) . .
C11 C12 Mo1 73.4(4) . .
C13 C12 Mo1 71.1(4) . .
C11 C12 H12 126.5 . .
C13 C12 H12 126.5 . .
Mo1 C12 H12 120.8 . .
C12 C13 C12 108.7(8) . 4_565
C12 C13 Mo1 72.9(4) . .
C12 C13 Mo1 72.9(4) 4_565 .
C12 C13 H13 125.6 . .
C12 C13 H13 125.6 4_565 .
Mo1 C13 H13 120.2 . .
C21 C20 C21 117.7(7) 4_565 .
C21 C20 P1 118.6(4) 4_565 .
C21 C20 P1 118.6(4) . .
C22 C21 C20 118.0(5) . .
C22 C21 C30 114.4(5) . .
C20 C21 C30 127.6(5) . .
C23 C22 C21 122.2(5) . .
C23 C22 H22 118.9 . .
C21 C22 H22 118.9 . .
C22 C23 C22 117.6(8) . 4_565
C22 C23 C40 121.2(4) . .
C22 C23 C40 121.2(4) 4_565 .
C32 C30 C33 108.0(5) . .
C32 C30 C31 110.3(5) . .
C33 C30 C31 105.5(5) . .
C32 C30 C21 111.3(5) . .
C33 C30 C21 108.5(5) . .
C31 C30 C21 113.0(5) . .
C30 C31 H31A 109.5 . .
C30 C31 H31B 109.5 . .
H31A C31 H31B 109.5 . .
C30 C31 H31C 109.5 . .
H31A C31 H31C 109.5 . .
H31B C31 H31C 109.5 . .
C30 C32 H32A 109.5 . .
C30 C32 H32B 109.5 . .
H32A C32 H32B 109.5 . .
C30 C32 H32C 109.5 . .
H32A C32 H32C 109.5 . .
H32B C32 H32C 109.5 . .
C30 C33 H33A 109.5 . .
C30 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
C30 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
C41 C40 C23 106.5(9) . .
C41 C40 C42 108.9(8) . 4_565
C23 C40 C42 112.5(8) . 4_565
C41 C40 C42 108.9(8) . .
C23 C40 C42 112.5(8) . .
C42 C40 C42 107.5(13) 4_565 .
C40 C41 H41A 109.5 . .
C40 C41 H41B 109.5 . .
H41A C41 H41B 109.5 . .
C40 C41 H41C 109.5 . .
H41A C41 H41C 109.5 . .
H41B C41 H41C 109.5 . .
C40 C41 H41D 109.5 . .
H41A C41 H41D 141.1 . .
H41B C41 H41D 56.3 . .
H41C C41 H41D 56.3 . .
C40 C41 H41E 109.5 . .
H41A C41 H41E 56.3 . .
H41B C41 H41E 141.1 . .
H41C C41 H41E 56.3 . .
H41D C41 H41E 109.5 . .
C40 C41 H41F 109.5 . .
H41A C41 H41F 56.3 . .
H41B C41 H41F 56.3 . .
H41C C41 H41F 141.1 . .
H41D C41 H41F 109.5 . .
H41E C41 H41F 109.5 . .
C40 C42 H42A 109.5 . .
C40 C42 H42B 109.5 . .
H42A C42 H42B 109.5 . .
C40 C42 H42C 109.5 . .
H42A C42 H42C 109.5 . .
H42B C42 H42C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Mo1 C1 2.037(6) .
Mo1 C1 2.037(6) 4_565
Mo1 C13 2.295(9) .
Mo1 C12 2.319(6) .
Mo1 C12 2.319(6) 4_565
Mo1 C11 2.344(6) .
Mo1 C11 2.344(6) 4_565
Mo1 P1 2.3725(19) .
Mo1 Co1 2.6644(14) .
Mo1 Co2 2.8096(10) .
Mo1 Co2 2.8096(10) 4_565
Co1 C2 1.782(8) .
Co1 C3 1.843(6) .
Co1 C3 1.843(6) 4_565
Co1 C1 2.242(6) .
Co1 C1 2.242(6) 4_565
Co1 Co2 2.4791(13) .
Co1 Co2 2.4791(13) 4_565
Co2 C4 1.784(6) .
Co2 C5 1.792(6) .
Co2 C3 2.106(6) 4_565
Co2 P1 2.1855(17) .
Co2 Co2 2.5378(17) 4_565
P1 C20 1.838(8) .
P1 Co2 2.1855(17) 4_565
O1 C1 1.143(8) .
O2 C2 1.127(11) .
O3 C3 1.144(8) .
O4 C4 1.153(9) .
O5 C5 1.135(8) .
C3 Co2 2.106(6) 4_565
C11 C12 1.409(9) .
C11 C11 1.415(13) 4_565
C11 H11 0.93 .
C12 C13 1.425(9) .
C12 H12 0.93 .
C13 C12 1.425(9) 4_565
C13 H13 0.93 .
C20 C21 1.422(6) 4_565
C20 C21 1.422(6) .
C21 C22 1.408(9) .
C21 C30 1.550(7) .
C22 C23 1.380(7) .
C22 H22 0.93 .
C23 C22 1.380(7) 4_565
C23 C40 1.533(13) .
C30 C32 1.531(8) .
C30 C33 1.540(8) .
C30 C31 1.544(9) .
C31 H31A 0.96 .
C31 H31B 0.96 .
C31 H31C 0.96 .
C32 H32A 0.96 .
C32 H32B 0.96 .
C32 H32C 0.96 .
C33 H33A 0.96 .
C33 H33B 0.96 .
C33 H33C 0.96 .
C40 C41 1.495(18) .
C40 C42 1.535(16) 4_565
C40 C42 1.535(16) .
C41 H41A 0.96 .
C41 H41B 0.96 .
C41 H41C 0.96 .
C41 H41D 0.96 .
C41 H41E 0.96 .
C41 H41F 0.96 .
C42 H42A 0.96 .
C42 H42B 0.96 .
C42 H42C 0.96 .
