#------------------------------------------------------------------------------
#$Date: 2015-08-08 05:21:28 +0300 (Sat, 08 Aug 2015) $
#$Revision: 153189 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/54/7035408.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7035408
loop_
_publ_author_name
'Das, Ankita'
'Mobin, Shaikh M.'
'Lahiri, Goutam Kumar'
_publ_section_title
;
 Recognition of fractional non-innocent feature of osmium coordinated
 2,2'-biimidazole or 2,2'-bis(4,5-dimethylimidazole) and their
 interactions with anions.
;
_journal_issue                   29
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              13204
_journal_page_last               13219
_journal_paper_doi               10.1039/c5dt01763g
_journal_volume                  44
_journal_year                    2015
_chemical_formula_sum            'C26 H22 Cl2 N8 O8 Os'
_chemical_formula_weight         835.61
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2015-06-04 deposited with the CCDC.
2015-06-15 downloaded from the CCDC.
;
_cell_angle_alpha                81.375(10)
_cell_angle_beta                 70.669(11)
_cell_angle_gamma                85.884(11)
_cell_formula_units_Z            2
_cell_length_a                   11.9969(17)
_cell_length_b                   13.3981(19)
_cell_length_c                   13.9695(14)
_cell_measurement_reflns_used    2906
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      71.6502
_cell_measurement_theta_min      3.3805
_cell_volume                     2094.3(5)
_computing_cell_refinement       'CrysAlis RED, Oxford Diffraction Ltd.,'
_computing_data_collection       'CrysAlis CCD, Oxford Diffraction Ltd.,'
_computing_data_reduction        'CrysAlis RED, Oxford Diffraction Ltd.,'
_computing_molecular_graphics    Ortep3
_computing_publication_material  Shelx97
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 15.9948
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.957
_diffrn_measurement_device_type  'OXFORD DIFFRACTION SUPER NOVA'
_diffrn_measurement_method       ω/q-scan
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Micro-Focus (Cu) X-ray Source'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0499
_diffrn_reflns_av_unetI/netI     0.0670
_diffrn_reflns_laue_measured_fraction_full 0.990
_diffrn_reflns_laue_measured_fraction_max 0.957
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            12873
_diffrn_reflns_point_group_measured_fraction_full 0.990
_diffrn_reflns_point_group_measured_fraction_max 0.957
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         71.794
_diffrn_reflns_theta_min         3.383
_exptl_absorpt_coefficient_mu    7.320
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.537
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.20 (release 27-06-2012 CrysAlis171 .NET)
(compiled Jul 11 2012,15:38:31)
Analytical numeric absorption correction using a multifaceted crystal
            model based on expressions derived by R.C. Clark & J.S. Reid.
(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
;
_exptl_crystal_colour            BLACK
_exptl_crystal_density_diffrn    1.325
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       BLOCK
_exptl_crystal_F_000             816
_platon_squeeze_details
;
;
_refine_diff_density_max         1.482
_refine_diff_density_min         -2.413
_refine_diff_density_rms         0.156
_refine_ls_extinction_coef       0.0015(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
_refine_ls_goodness_of_fit_ref   1.017
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     377
_refine_ls_number_reflns         7856
_refine_ls_number_restraints     3
_refine_ls_restrained_S_all      1.017
_refine_ls_R_factor_all          0.1096
_refine_ls_R_factor_gt           0.0880
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1669P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2363
_refine_ls_wR_factor_ref         0.2633
_reflns_Friedel_coverage         0.000
_reflns_number_gt                5224
_reflns_number_total             7856
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c5dt01763g2.cif
_cod_data_source_block           '[1](ClO4)2'
_cod_depositor_comments
'Adding full bibliography for 7035408--7035410.cif.'
_cod_database_code               7035408
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.284
_shelx_estimated_absorpt_t_max   0.450
_shelx_hkl_file_presqueezed
;
   0   0  -1 191498. 1372.93   3
   0   0  -2 99246.5 1408.27   3
   0   0  -3 258196. 2779.04   3
   0   0  -4 7279.52 548.403   2
   0   0   4 8116.18 510.978   6
   0   0  -4 8674.39 595.951   3
   0   0   5 50852.0 1463.16   6
   0   0  -5 49655.5 1588.35   3
   0   0   5 54057.0 1602.39   8
   0   0   6 15861.2 973.578   8
   0   0   6 15580.9 921.657   6
   0   0   7 38686.0 1640.31   8
   0   0   7 38483.9 1616.15   6
   0   0   8 52633.8 2082.41   8
   0   0   9 419.332 458.435   8
   0   0  10 38757.4 2040.09   8
   0   0  11 6378.43 959.961  13
   0   0  11 6089.62 883.141   8
   0   0  11 6830.11 1070.02  21
   0   0  12 149.790 415.113  21
   0   0  12-711.323 444.327  13
   0   0  13 6689.50 1070.79  21
   0   0  13 6512.46 952.238  14
   0   0  13 6225.91 952.509  13
   0   0  14 930.265 474.010  21
   0   0  14 732.311 357.125  13
   0   0  14 603.332 350.184  14
   0   0  15 760.087 302.940  14
   0  -1  15 845.390 319.105  21
   0  -1  15 663.258 257.857  14
   0  -1  14 2915.08 695.801  21
   0  -1  14 2412.75 544.123  13
   0  -1  14 2594.62 527.079  14
   0  -1  13-81.0974 267.849  13
   0  -1  13 1.12769 317.305  21
   0  -1  13-65.1183 244.307  14
   0  -1  12 6921.14 958.245  14
   0  -1  12 8417.80 1190.56  21
   0  -1  12 8037.93 1060.59  13
   0  -1  11 2052.11 616.265  21
   0  -1  11 2960.43 616.522   8
   0  -1  11 2570.54 607.355  13
   0  -1  10 3460.35 639.952   8
   0  -1   9 55320.0 2303.37   8
   0  -1   8 4354.62 654.261   8
   0  -1   7 58142.1 2085.33   8
   0  -1   6 76314.0 2143.41   8
   0   1  -5 585.843 194.084   2
   0   1  -5 216.796 128.108   3
   0  -1   5 489.737 205.600   9
   0   1  -4 20329.2 908.733   2
   0  -1   4 22177.3 914.588   9
   0   1  -4 23695.2 907.579   3
   0  -1   4 21525.7 869.227   8
   0   1  -3 8165.57 473.223   3
   0   1  -2 7180.54 322.291   3
   0  -1   2 7884.19 340.308   3
   0   1  -1 167181. 981.100   3
   0  -1  -2 345550. 2948.90   3
   0  -1  -3 8863.58 565.600   3
   0   1   4 77605.5 1527.81   6
   0  -1  -4 84219.0 1936.63   3
   0   1   5 60047.0 1636.78   8
   0  -1  -5 55140.5 1731.08   3
   0   1   5 56827.0 1479.11   6
   0  -1  -5 57235.4 1748.95   2
   0   1   6 10786.1 738.726   6
   0   1   6 11344.9 799.019   8
   0   1   7 95315.0 2564.05   8
   0   1   7 89202.4 2345.68   6
   0   1   8 6382.40 869.440   8
   0   1   8 4733.66 712.862   6
   0   1   9 34935.4 1841.33   8
   0   1  10 27843.4 1843.95   8
   0   1  11 4464.01 874.778  21
   0   1  11 4348.44 809.236  13
   0   1  11 4974.50 866.554   8
   0   1  12 7821.86 1089.96  13
   0   1  12 8101.71 1182.59  21
   0   1  13 4334.63 824.960  13
   0   1  13 4358.68 786.533  14
   0   1  13 4631.01 928.504  21
   0   1  14 2751.89 649.060  13
   0   1  14 2496.14 585.004  14
   0   1  14 2108.58 595.375  21
   0   1  15 2150.66 468.748  14
   0  -2  15 1962.03 441.887  21
   0  -2  14 615.933 405.056  21
   0  -2  13 8613.02 1151.96  21
   0  -2  13 6349.87 873.502  13
   0  -2  12 2786.27 651.178  13
   0  -2  12 1963.62 520.879  14
   0  -2  12 2918.64 730.183  21
   0  -2  11 5651.68 827.547  14
   0  -2  11 6038.62 907.323  13
   0  -2  11 7776.56 1129.09  21
   0  -2  11 5667.81 819.061   8
   0  -2  10 18748.5 1662.55  21
   0  -2  10 17693.6 1425.80  13
   0  -2  10 22231.7 1531.71   8
   0  -2   9 1653.52 453.157   8
   0  -2   8 58598.3 2302.81   8
   0  -2   7 37543.8 1660.59   8
   0  -2   6 6976.28 683.023   8
   0  -2   5 104927. 2351.97   9
   0  -2   5 106778. 2276.32   8
   0  -2   4 36589.2 1226.98   9
   0   2  -4 35931.8 1209.35   2
   0  -2   4 38877.5 1225.94   8
   0   2  -4 39966.8 1077.65   3
   0  -2   3 34629.1 1025.84   9
   0   2  -3 36526.4 1050.16   2
   0   2  -2 9015.23 326.196   3
   0   2  -2 8266.11 415.003   2
   0  -2   2 9344.96 342.966   3
   0   2  -1 10597.0 316.744   2
   0  -2   1 11107.2 247.603   3
   0  -2   0 257512. 1780.39   1
   0  -2  -2 98800.3 1662.39   3
   0  -2  -3 3272.63 380.457   3
   0  -2  -4 13988.5 823.178   3
   0  -2  -4 15343.9 806.110   2
   0   2   4 12412.5 602.167   6
   0   2   5 45009.7 1327.42   6
   0   2   5 45690.4 1447.32   8
   0  -2  -5 45621.2 1577.86   2
   0   2   6 60869.7 1739.92   6
   0   2   6 64984.4 1931.16   8
   0   2   7 1399.46 379.338   6
   0   2   7 1765.67 428.051   8
   0   2   8 62151.8 2287.54   8
   0   2   8 49274.8 1900.67   6
   0   2   9 43593.2 1956.08   6
   0   2   9 48272.9 2198.02   8
   0   2  10 6747.11 981.928   8
   0   2  11 9317.08 1256.69  21
   0   2  11 8461.18 1095.57  13
   0   2  11 8592.00 1034.92   8
   0   2  12-84.6955 334.595  21
   0   2  12-98.0372 275.847  13
   0   2  13 661.814 408.813  13
   0   2  13 1670.70 587.286  21
   0   2  14 1769.28 505.757  13
   0   2  14 3514.92 702.798  14
   0   2  15-211.936 252.259  14
   0   2  16 866.946 257.711  14
   0  -3  15-737.983 272.506  21
   0  -3  14 1772.88 463.187  21
   0  -3  13 830.711 343.592  13
   0  -3  13 623.363 338.686  21
   0  -3  12 2397.97 659.475  21
   0  -3  12 1500.98 462.696  13
   0  -3  11 4582.34 861.018  21
   0  -3  11 4117.41 711.995  13
   0  -3  11 3800.23 679.339   8
   0  -3  10 108.622 246.670   8
   0  -3  10-228.742 324.887  21
   0  -3   9 17778.0 1361.70   8
   0  -3   8 13037.5 1107.39   8
   0  -3   7 14792.2 1120.79   8
   0  -3   6 25612.7 1289.19   8
   0  -3   5 5297.63 547.248   8
   0  -3   5 4735.60 517.946   9
   0   3  -4 19271.6 683.342   3
   0   3  -4 19632.5 826.222   4
   0   3  -4 17869.9 836.555   2
   0  -3   4 19258.5 928.923   9
   0   3  -3 40860.9 1144.60   4
   0  -3   3 45421.6 1324.65   8
   0   3  -3 44101.6 850.328   3
   0   3  -3 40702.4 1084.85   2
   0  -3   3 39589.2 1163.04   9
   0   3  -2 17410.9 577.869   1
   0   3  -2 16396.0 550.438   2
   0   3  -2 15474.2 662.340   4
   0  -3   2 16859.3 404.451   3
   0   3  -1 74302.0 822.350   2
   0  -3   1 76499.4 720.843   3
   0   3  -1 75323.6 1148.13   1
   0  -3   0 65669.9 1090.91   1
   0  -3  -1 4365.99 206.271   2
   0  -3  -1 4567.74 346.205   1
   0  -3  -2 53342.0 1324.26   3
   0  -3  -2 62839.6 1159.77   2
   0  -3  -3 31855.0 1185.01   3
   0  -3  -3 35054.7 1075.18   2
   0  -3  -4 62297.3 1483.07   5
   0  -3  -4 63898.4 1847.43   3
   0   3   5 23719.6 981.112   6
   0  -3  -5 24796.0 1176.25   2
   0  -3  -5 25206.2 1038.99   5
   0   3   5 25721.1 1122.84   8
   0   3   6 3321.55 481.734   8
   0   3   6 2757.83 381.485   6
   0  -3  -6 2816.36 390.502   5
   0  -3  -7 67352.3 2033.06   5
   0   3   7 70632.7 2084.44   6
   0   3   8 17172.4 1131.45   6
   0   3   8 17652.3 1247.69   8
   0   3   9 18595.2 1269.76   6
   0   3   9 21260.7 1428.62   8
   0   3  10 46974.4 2200.29   6
   0   3  11-174.263 320.549  13
   0   3  11 1010.66 469.986  21
   0   3  12 4619.96 920.176  21
   0   3  12 4913.18 857.786  13
   0   3  13 3782.12 751.418  13
   0   3  14 856.461 491.378  14
   0   3  14-182.559 278.652  13
   0   3  15 2622.28 551.249  14
   0   3  16-43.1965 156.585  14
   0  -4  14 203.875 234.275  21
   0  -4  13 2901.05 654.399  21
   0  -4  12 5714.19 956.175  21
   0  -4  11-446.920 410.038  21
   0  -4  10 6590.69 1020.11  21
   0  -4  10 6097.23 841.333   8
   0  -4   9 1918.59 554.289  21
   0  -4   9 2398.09 542.101   8
   0  -4   8 12756.5 1131.50   8
   0  -4   7 33475.0 1665.83   8
   0  -4   6 3140.04 467.030   8
   0  -4   5 59566.3 1862.60   9
   0  -4   5 68756.9 2049.18   8
   0  -4   4 54559.6 1729.32   8
   0  -4   4 46287.5 1487.73   9
   0   4  -3 14608.9 824.286   4
   0  -4   3 13012.5 702.854   9
   0   4  -3 13438.1 619.029   2
   0   4  -2 144129. 1626.79   2
   0  -4   2 143111. 2351.12   5
   0   4  -1 18444.2 832.413   4
   0  -4   1 20069.9 835.272   5
   0  -4   0 11988.6 570.599   1
   0  -4  -1 120581. 1933.90   1
   0  -4  -2 6830.52 503.315   5
   0  -4  -2 6890.47 514.067   3
   0  -4  -2 7505.64 534.096   1
   0  -4  -2 7374.72 383.196   2
   0  -4  -3 46747.4 1504.82   3
   0  -4  -3 44503.7 1280.47   5
   0  -4  -4 13693.0 751.289   5
   0  -4  -4 14743.9 782.695   2
   0  -4  -4 12751.6 862.012   3
   0  -4  -5 3163.21 429.233   5
   0   4   6 13682.1 862.297   6
   0  -4  -6 13279.2 876.767   5
   0  -4  -7 377.196 252.939   5
   0   4   7 172.694 206.647   6
   0   4   8 18970.4 1198.36   6
   0  -4  -8 15720.3 1116.49   5
   0   4   9 28924.8 1584.99   6
   0   4  10 128.884 342.237   6
   0   4  10 204.654 295.967  21
   0   4  11 7702.24 922.796   6
   0   4  11 10118.1 1195.86  13
   0   4  12 2431.64 620.521  13
   0   4  13-218.061 331.872  13
   0   4  14 4012.51 737.976  14
   0   4  14 3053.75 615.580  13
   0   4  15-1001.24 398.116  14
   0   4  16 568.016 223.595  14
   0  -5  14 523.970 246.705  21
   0  -5  13 683.251 340.737  21
   0  -5  12-141.810 325.723  21
   0  -5  11 5730.84 951.880  21
   0  -5  10 1622.99 421.852   8
   0  -5  10 2269.57 598.276  21
   0  -5   9 2142.35 576.378  21
   0  -5   9 2629.13 586.802   8
   0  -5   8 19447.6 1416.57   8
   0  -5   7 3443.59 577.482   8
   0  -5   6 10396.6 920.793   8
   0  -5   5 60908.4 2099.12   8
   0  -5   4 644.625 292.806   8
   0  -5   4 458.482 215.516   9
   0  -5   3 34929.9 1484.05   8
   0  -5   3 24563.3 1000.73   9
   0  -5   2 4598.18 481.492   5
   0  -5   1 76346.1 1870.34   5
   0  -5   0 73316.8 1777.92   5
   0  -5   0 72928.0 1485.26   1
   0  -5  -1 213.621 159.927   5
   0  -5  -1 167.286 112.663   1
   0  -5  -2 99504.5 2083.12   1
   0  -5  -2 100752. 2098.40   5
   0  -5  -3 51139.6 1187.32   2
   0  -5  -3 44296.9 1495.87   3
   0  -5  -4 3918.42 411.230   2
   0  -5  -4 5824.01 569.152   5
   0  -5  -5 76466.1 2107.99   5
   0  -5  -6-151.241 249.583   5
   0  -5  -7 19271.5 1185.47   5
   0   5   7 19296.1 1164.99   6
   0  -5  -8 12549.0 1026.17   5
   0   5   8 15851.9 1144.47   6
   0   5   9 4441.80 630.490   6
   0   5  10 19468.6 1373.69   6
   0   5  10 18860.5 1574.02  18
   0   5  10 18928.6 1510.37  13
   0   5  11 1682.05 494.610  18
   0   5  11 1378.56 446.196  13
   0   5  12 3213.82 652.915  16
   0   5  12 2672.91 640.258  13
   0   5  13 5470.91 826.202  13
   0   5  14 45.6246 258.282  14
   0   5  14 436.687 273.308  13
   0   5  15 1877.04 440.274  14
   0  -6  14 238.534 183.949  21
   0  -6  13 309.476 244.905  21
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   1   3   5 20007.5 822.527   6
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   1   3   6 10823.4 688.387   6
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   1   3   7 48778.3 1832.81   8
   1   3   8 2447.45 396.388   6
   1   3   8 2852.89 492.589   8
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   1   3  10 4855.76 777.708   8
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   1   3  11 20675.2 1878.58  21
   1   3  12 8388.12 1117.31  13
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   1   3  13-506.957 386.096  13
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   1   4   6 35116.8 1245.81   6
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   1   4   7 166.266 148.122   6
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   1   4   8 27222.9 1325.80   6
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   1   4   9 17551.7 1143.09   6
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   1   4  11 20785.8 1678.51  13
   1   4  12-564.832 412.786  13
   1   4  13 3143.52 699.209  13
   1   4  14 5575.16 857.375  13
   1   4  15-144.258 205.726  13
   1   4  15 323.057 309.631  14
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   1   5  -4 28231.5 1335.79   4
   1   5  -3 41761.3 1573.99   4
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   2  -3   6 76216.2 2231.85   8
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   2  -3   9 5026.63 744.675   8
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   2  -1  -4 12913.0 780.873   1
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   2  -1   4 18363.6 817.794   8
   2  -1   5 184418. 2884.43   8
   2  -1   5 189967. 2812.01   3
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   2  -1   6 151183. 2987.61   8
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   2   0  -3 35140.0 1285.84   2
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   2   0  -1 425626. 3011.48   1
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   2   0   5 73142.9 1805.09   8
   2   0   6 24952.8 1189.61   8
   2   0   7 55883.1 2001.91   8
   2   0   8 6054.21 730.704   8
   2   0   9 10514.6 1028.21   8
   2   0  10 16499.0 1358.30   8
   2   0  11-267.149 381.440  21
   2   0  11-19.1681 389.850   8
   2   0  12 10236.3 1362.59  21
   2   0  12 11581.9 1341.61  13
   2   0  12 6871.53 971.113   8
   2   0  13 3877.26 865.825  21
   2   0  13 3665.99 777.788  13
   2   0  14 613.906 498.204  21
   2   0  14 591.954 351.612  13
   2   0  14-454.578 400.332  14
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   2   1  -4 38686.1 1079.96   1
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   2   1  -4 39393.0 1375.53   3
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   2   1  -3 1408.76 271.583   2
   2   1  -3 1146.16 177.344   1
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   2   1  -2 24184.0 940.240   2
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   2   1   1 182948. 1741.04   3
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   2   1   4 115137. 1888.04   8
   2   1   5 9038.77 644.948   3
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   2   1   5 9625.14 641.708   8
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   2   1   5 9718.51 556.358   6
   2   1   6 125459. 2590.46   8
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   2   1   7 6870.96 720.822   8
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   2   1   8 18789.1 1255.64   8
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   2   1   9 19755.2 1382.31   8
   2   1  10 5545.82 867.319   8
   2   1  11 13133.9 1291.41   8
   2   1  11 12762.0 1471.75  21
   2   1  12 1564.07 663.438  21
   2   1  12 1033.30 490.528   8
   2   1  12 1196.83 502.327  13
   2   1  13 7419.35 1228.09  21
   2   1  13 6936.12 1060.65  13
   2   1  14 6420.99 1005.11  13
   2   1  14 6053.62 1072.75  21
   2   1  15 147.645 256.499  14
   2   1  15-774.096 426.526  13
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   2   2   0 38558.5 686.495   3
   2   2   1 988.229 103.369   3
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   2   2   2 46631.2 1015.40   3
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   2   2   4 8113.49 509.575   8
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   2   2   5 39233.2 1410.57   3
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   2   2   5 38623.3 1018.23   6
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   2   2   6 1843.49 270.113   6
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   2   2   6 2287.79 388.436   8
   2   2   7 39876.5 1385.73   6
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   2   2   8 54514.9 2116.10   8
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   2   2  10 20145.0 1500.38   8
   2   2  11 1145.03 623.467   8
   2   2  11 1323.79 551.481  21
   2   2  12 4863.70 916.192  13
   2   2  12 2997.64 682.767   8
   2   2  12 5483.86 1053.65  21
   2   2  13 10610.7 1287.36  13
   2   2  13 11131.3 1472.05  21
   2   2  14-195.153 311.836  13
   2   2  15 4792.09 762.651  14
   2   2  15 4247.52 733.568  13
   2   2  16 559.529 264.614  14
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   2   3  -4 25144.3 1051.60   4
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   2   3  -3 3912.30 430.468   2
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   2   3   0 13216.5 340.571   3
   2   3   1 448610. 2705.00   3
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   2   3   2 1978.52 212.572   3
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   2   3   3 76617.4 1301.20   4
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   2   3   3 89691.6 1767.08   3
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   2   3   4 46291.7 1461.14   3
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   2   3   5 12485.8 584.661   6
   2   3   5 13383.9 783.302   8
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   2   3   6 28955.3 1016.10   6
   2   3   7 8965.59 805.301   8
   2   3   8 17671.4 1211.96   8
   2   3   9 31405.6 1751.55   8
   2   3  10 569.746 398.255   8
   2   3  11 12858.0 1540.32  21
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   2   3  12 3931.51 914.581  21
   2   3  12 3219.07 731.795  13
   2   3  13-502.667 421.811  13
   2   3  14 4455.18 840.299  13
   2   3  15 673.803 383.407  13
   2   3  16-85.4772 234.120  14
   2   3  16 358.304 235.085  13
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   2   4   1 76550.5 1711.11   4
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   2   4   2 192495. 2570.44   4
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   3  -4   0 102523. 2191.37   5
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   3  -4   1 92875.2 2060.10   3
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   3  -4   3 57714.4 1588.43   3
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   3  -4   5 27341.5 1340.41   8
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   3  -4   8 14134.1 1180.34   8
   3  -4   9 8834.55 1003.87   8
   3  -4  10 1464.29 477.923  21
   3  -4  10 1465.51 506.610  24
   3  -4  10 1682.91 504.266   8
   3  -4  11 10800.4 1371.83  17
   3  -4  11 7705.70 1014.27   8
   3  -4  11 7386.18 1029.62  21
   3  -4  11 8820.04 1159.35  24
   3  -4  12 2753.10 672.027  17
   3  -4  12 2664.72 650.578  21
   3  -4  13 1367.68 459.472  21
   3  -4  13 947.269 373.933  17
   3  -4  14 2531.10 546.317  17
   3  -4  14 981.913 339.111  21
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  -3   3  11 8863.32 1076.99  14
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  -3   3   9 4588.25 743.716  16
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  -3   3   6 22249.1 1374.91   6
  -3   3   5 5111.78 622.390   6
  -3   3   5 4667.80 533.565  11
  -3   3   4 52073.8 1678.95  11
  -3   3   3 98114.5 1837.11   7
  -3   3   3 104319. 2259.96  11
   3  -3  -2 3810.22 357.932   5
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   3  -3  -1 67085.7 1879.63   1
   3  -3  -1 63291.6 1469.33   5
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   3  -3   0 51500.1 1376.97   5
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   3  -3   1 601.242 186.834   3
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   3  -3   2 113676. 2109.86   3
   3  -3   3 49753.2 1485.46   8
   3  -3   3 51580.3 1433.54   3
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   3  -3   4 63806.5 1642.80   3
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   3  -3   4 67619.6 1839.03   8
   3  -3   5 202712. 3406.91   8
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   3  -3   6 4013.47 535.310   8
   3  -3   7 52566.1 2005.75   8
   3  -3   8 39875.5 1917.19   8
   3  -3   9 4371.78 721.219   8
   3  -3  10 19715.0 1566.34   8
   3  -3  10 16814.5 1541.14  24
   3  -3  11 567.408 380.614  17
   3  -3  11 952.835 401.521  21
   3  -3  11 440.191 289.663   8
   3  -3  12 4975.72 832.829  13
   3  -3  12 4629.84 861.102  21
   3  -3  12 5370.13 934.612  17
   3  -3  13 5480.92 889.895  17
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   3  -3  13 5193.53 807.266  13
   3  -3  14-600.154 326.008  17
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   3  -3  15 835.461 354.380  21
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  -3   2   4 89972.2 2093.11  11
  -3   2   3 25995.9 1107.57  11
   3  -2  -2 162596. 2878.80   1
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   3  -2  -1 89834.2 2030.30   1
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  -3   2   0 19622.9 777.699   7
  -3   2  -1 219318. 2880.19   1
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   3  -2   2 4079.72 392.107   3
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  -3   2  -2 3747.64 366.768  11
   3  -2   3 117939. 2021.11   8
  -3   2  -3 119630. 1949.55  11
  -3   2  -3 113087. 2071.36   7
   3  -2   4 53765.8 1506.53   8
   3  -2   4 58063.3 1533.17   3
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   3  -2   5 18880.7 973.657   8
  -3   2  -5 17728.9 894.741   7
   3  -2   6 153977. 3035.49   8
   3  -2   7 27266.2 1428.94   8
   3  -2   8 3432.68 560.139   8
   3  -2   9 15706.2 1267.84   8
   3  -2  10 395.263 311.683   8
   3  -2  11 4605.90 866.511  17
   3  -2  11 3847.13 713.229   8
   3  -2  11 3764.54 777.593  21
   3  -2  12 3349.62 736.778  21
   3  -2  12 2936.30 686.405  17
   3  -2  12 2009.98 510.747   8
   3  -2  13 56.0967 243.213  17
   3  -2  13 276.701 304.168  13
   3  -2  13-83.2349 306.943  21
   3  -2  14 2811.83 647.574  21
   3  -2  14 4031.45 763.659  13
   3  -2  15 263.911 257.301  21
   3  -2  15 675.705 320.879  13
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  -3   1   8 32980.2 1652.57   8
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  -3   1   7 4048.41 781.503   6
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  -3   1   6 43650.2 1820.67   9
  -3   1   6 41336.3 1625.53   8
  -3   1   5 112389. 2422.89   8
  -3   1   5 116907. 2799.12   9
  -3   1   5 118240. 2753.47   6
  -3   1   4 876.468 270.423   6
  -3   1   4 991.263 252.317   8
  -3   1   4 991.000 258.603  11
   3  -1  -3 179266. 3013.38   1
  -3   1   3 183153. 2383.46   8
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   3  -1  -2 39331.5 1314.91   1
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   3  -1  -1 1056.65 226.441   1
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   3  -1   3 9156.78 561.008   3
  -3   1  -3 8821.16 566.006   3
   3  -1   4 135694. 2209.94   8
  -3   1  -4 141311. 2366.32   3
   3  -1   5 276747. 3564.70   3
   3  -1   5 276514. 3527.95   8
  -3   1  -5 268508. 3126.47   7
   3  -1   6 39864.2 1534.50   8
   3  -1   7 61729.1 2122.10   8
   3  -1   8 25837.8 1519.62   8
   3  -1   9 966.708 326.306   8
  -3   1 -10 17414.5 1454.46  10
   3  -1  10 18749.8 1436.76   8
   3  -1  11 3898.32 796.741  17
   3  -1  11 4891.05 787.816   8
   3  -1  11 4661.92 868.707  21
   3  -1  12 1448.52 484.542  17
   3  -1  12 1379.55 525.613  21
   3  -1  12 1745.63 518.625   8
   3  -1  13 4201.92 754.903  17
   3  -1  13 5156.47 920.186  21
   3  -1  13 5985.42 994.658  13
   3  -1  14-338.571 384.728  21
   3  -1  14-458.865 380.093  13
   3  -1  15 3510.30 651.596  13
   3  -1  16 940.294 321.875  13
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  -3   0   8 380.777 502.214   8
  -3   0   7 49068.4 2110.34   6
  -3   0   7 51419.4 2154.09   9
  -3   0   7 46958.3 1866.22   8
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  -3   0   6 12532.8 1021.05   9
  -3   0   6 11417.8 866.000   8
  -3   0   5 10538.2 861.760   6
  -3   0   5 9883.06 851.176   9
  -3   0   5 9525.59 723.555   8
  -3   0   4 123210. 2239.52   8
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   3   0  -3 20262.9 900.118   1
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   3   0  -2 31893.5 1080.44   1
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  -3   0   1 22115.3 914.594   2
  -3   0   1 20547.2 688.157   6
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  -3   0   0 33424.0 950.470   1
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   3   0   4 9775.67 559.838   8
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   3   0   4 10719.8 652.566   3
   3   0   5 8646.46 645.520   3
   3   0   5 8743.09 629.216   8
   3   0   6 70045.9 1966.41   8
   3   0   7 85189.7 2457.70   8
   3   0   8 1145.85 386.301   8
  -3   0  -9 16454.6 1287.83  10
   3   0   9 17330.4 1283.76   8
  -3   0 -10 13662.5 1226.37  10
   3   0  10 15763.0 1333.80   8
   3   0  11 649.405 383.043  17
   3   0  11 884.772 432.768  21
   3   0  11 641.893 388.998   8
   3   0  12 10309.4 1210.05  17
   3   0  12 12126.9 1458.75  21
   3   0  12 9472.59 1109.45   8
   3   0  13-432.091 411.446  21
   3   0  13 128.243 310.674  13
   3   0  14 3910.41 834.607  21
   3   0  14 5148.34 902.314  13
   3   0  15 3478.97 694.706  13
   3   0  16-124.492 220.195  13
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  -3  -1   5 49976.0 1844.30   6
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  -3  -1   4 551.798 168.463  11
  -3  -1   4 681.550 248.935   6
  -3  -1   4 591.214 149.909   8
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  -3  -1   2 67417.7 1691.50   2
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  -3  -1   1 54245.7 1067.95   1
  -3  -1   1 50297.9 1297.65  11
  -3  -1   0 248477. 2298.74   1
   3   1   1 6083.94 424.259   3
  -3  -1  -2 750.416 176.421   3
   3   1   2 785.079 173.006   3
   3   1   3 70070.3 1497.13   3
  -3  -1  -3 71231.2 1494.73   3
  -3  -1  -4 375.266 179.666  10
   3   1   4 242.688 101.839   8
   3   1   4 65.8484 90.4924   3
  -3  -1  -4 133.398 114.779   3
   3   1   5 52118.7 1451.80   8
   3   1   5 51019.2 1557.84   3
  -3  -1  -5 54523.1 1592.71  10
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   3   1   6 74476.6 1972.75   8
  -3  -1  -7 10250.1 848.084  10
   3   1   7 10491.5 851.300   8
  -3  -1  -8 16820.5 1158.79  10
   3   1   8 17640.2 1201.20   8
  -3  -1  -9 488.916 315.991  10
   3   1   9 866.345 422.026   8
   3   1  10 13837.8 1278.48   8
   3   1  11 9071.51 1081.29   8
   3   1  11 8371.61 1189.66  21
   3   1  12-91.2319 318.895  21
   3   1  12 496.386 609.779   8
   3   1  13 6030.43 1074.24  21
   3   1  13 6838.37 1101.16  13
   3   1  14 575.995 422.173  13
   3   1  15 68.1768 313.028  13
   3   1  16 1800.69 392.367  14
   3   1  16 3159.00 570.065  13
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  -3  -2   6 31825.6 1692.99   9
  -3  -2   6 23837.9 1240.03   8
  -3  -2   5 124.151 169.850   8
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  -3  -2   4 29254.8 1095.44  11
  -3  -2   3 32865.1 1144.07  11
  -3  -2   3 32045.9 1051.03   8
  -3  -2   2 7925.72 561.347  11
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  -3  -2   2 7417.86 552.281   2
  -3  -2   1 156727. 2407.92   2
  -3  -2   1 150189. 2308.97  11
  -3  -2   0 63390.7 1369.19  10
   3   2   0 69701.5 1279.31   3
   3   2   1 56659.7 1143.84   3
  -3  -2  -2 139481. 2054.80  11
   3   2   2 139361. 1912.23   3
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   3   2   3 54779.1 1339.70   3
   3   2   4 75627.2 1756.26   3
   3   2   4 73327.4 1463.81   8
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   3   2   5 57308.0 1505.64   8
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   3   2   6 8116.89 653.679   8
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   3   2   7 78797.1 2235.70   8
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   3   2   8 930.129 337.502   8
   3   2   9 18049.8 1325.21   8
   3   2  10 20438.4 1531.76   8
   3   2  11 3412.70 749.986   8
   3   2  11 2984.94 748.705  21
   3   2  12 10609.8 1179.94   8
   3   2  12 15614.8 1722.32  21
   3   2  13 4143.37 948.399  21
   3   2  13 4008.00 837.423  13
   3   2  14 4231.78 835.452  13
   3   2  15 4343.70 797.241  13
   3   2  16-485.869 288.385  13
   3   2  16-182.511 262.067  14
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  -3  -3   7 31125.3 1787.39   9
  -3  -3   6 179.672 261.393   9
  -3  -3   6 621.761 289.921   8
  -3  -3   5 40399.1 1793.32   9
  -3  -3   5 36514.9 1460.59   8
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  -3  -3   1 3925.00 369.360   2
  -3  -3   1 4220.72 427.097  11
   3   3  -1 3755.30 265.722   3
  -3  -3   0 43853.9 1160.61   2
   3   3   0 45159.5 884.295   3
  -3  -3   0 47212.7 1366.79  11
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   3   3   1 32071.9 822.206   3
  -3  -3  -1 31936.3 1101.68  11
  -3  -3  -2 36072.3 1104.55  10
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   3   3   2 36568.9 993.900   3
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  -3  -3  -2 34859.6 933.518   5
  -3  -3  -3 122456. 1937.18   3
  -3  -3  -3 121442. 2132.96  10
   3   3   3 121732. 2055.64   3
   3   3   4 12030.0 723.145   3
  -3  -3  -4 12842.2 732.083  10
  -3  -3  -4 12140.5 686.234   3
  -3  -3  -5 61515.6 1662.35  10
  -3  -3  -6 74599.6 1977.62  10
   3   3   6 76676.3 1999.54   8
  -3  -3  -7 605.364 249.607  10
   3   3   7 676.751 290.494   8
  -3  -3  -8 22591.8 1242.02  10
   3   3   8 25193.5 1426.54   8
   3   3   9 12208.6 1097.29   8
   3   3  10 662.368 362.187   8
   3   3  11 6384.54 942.281  18
   3   3  11 7899.61 1183.70  21
   3   3  12 293.038 264.243  18
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   3   3  13 2074.43 612.479  13
   3   3  14 7202.25 1070.32  13
   3   3  15-201.535 346.576  13
   3   3  16 1963.24 460.059  13
   3   3  16 2772.48 544.505  14
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  -3  -4   6 29317.0 1674.79   9
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   3   4  -4 8903.68 751.194   4
   3   4  -3 40238.6 1512.17   4
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  -3  -4   2 3621.58 377.776   8
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  -3  -4   0 35533.5 1043.38   2
  -3  -4   0 39415.5 1038.98   5
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   3   4   1 5877.65 341.512   3
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   3   4   2 182936. 2298.72   3
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  -3  -4  -2 183630. 2401.63   5
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   3   4   3 5007.42 444.911   3
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   3   4   3 5883.77 479.887   4
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   3   4   4 27369.3 1156.49   3
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   3   4   4 29101.8 975.841   4
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   3   4  11 863.958 401.905  18
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   3   4  12 5534.93 933.338  18
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   3   4  13 4880.17 895.228  13
   3   4  13 3246.76 704.609  18
   3   4  14-219.042 338.423  13
   3   4  15 4651.21 749.144  13
   3   4  16 849.243 325.834  13
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  -3  -5   7 14370.9 1393.22  21
  -3  -5   6 319.836 238.860   9
  -3  -5   5 26071.1 1521.77   9
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   3   5  -4 16152.9 1088.97   4
   3   5  -3 2247.13 434.076   4
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   3   5  -2 56046.7 1926.50   4
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   3   5  -1 25310.4 1272.94   4
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   3   5   0 5040.40 558.877   4
   3   5   1 147439. 2838.49   4
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   3   5   2 9889.82 716.933   4
  -3  -5  -3 105622. 2308.30  10
  -3  -5  -3 112359. 2237.29   5
   3   5   3 108851. 2227.55   4
   3   5   4 32624.7 1165.16   4
  -3  -5  -4 33221.3 1278.11  10
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   3   5  11 10881.1 1281.07  18
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   3   5  12 8044.27 1144.49  18
   3   5  13 232.682 250.440  18
   3   5  13 206.395 284.484  13
   3   5  14 4767.98 804.050  13
   3   5  14 3784.43 721.141  18
   3   5  15 592.673 278.241  13
   3   5  16 520.636 248.399  13
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   3   6  -4 2736.00 530.021   4
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   3   6  -3 32428.2 1624.68   4
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   3   6  -2 3208.99 517.253   4
   3   6  -1 31569.1 1548.62   4
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   3   6   0 52521.0 1928.65   4
   3   6   1 8339.69 795.502   4
  -3  -6  -1 8412.61 652.468   5
  -3  -6  -2 157318. 2822.37   5
   3   6   2 160293. 3156.11   4
   3   6   3 65503.6 1941.34   4
  -3  -6  -3 70792.7 2005.26   5
   3   6   4 5143.98 555.636   4
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   3   6  10 16449.6 1584.49  18
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   3   6  13 3487.57 746.773  18
   3   6  14-56.5116 240.972  13
   3   6  14 158.480 216.140  18
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   3   7  -4 8002.60 912.350   4
   3   7  -3 606.844 358.685   4
   3   7  -2 8555.56 915.172   4
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   3   7  -1 13394.5 1114.28   4
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   3   7   0 167.870 405.696   4
   3   7   1 35545.5 1706.96   4
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   3   7   2 40247.7 1751.71   4
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   3   7   3 26615.8 1383.23   4
   3   7   4 32214.6 1465.46   4
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   3   7  10 4582.42 891.637  18
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   3   7  11 3738.25 802.178  18
   3   7  12 12854.0 1447.93  18
   3   7  13 44.7499 232.447  18
   3   7  14 748.094 323.725  18
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   3   8  -3 10421.7 1094.65   4
   3   8  -2 11037.5 1132.36   4
   3   8  -1 2159.80 557.542   4
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   3   8   0 22144.0 1518.11   4
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   3   8   1 8295.53 939.948   4
   3   8   2 18907.3 1359.07   4
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   3   8   3 36297.5 1769.35   4
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   3   8   9 700.921 411.261  18
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   3   8  10 1608.15 591.907  18
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   3   8  11 4223.35 867.384  18
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   3   8  13 1125.68 449.185  18
   3   8  14 299.505 240.126  18
   3   8  15-207.141 189.127  18
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   3   9  -1 18744.4 1514.84   4
   3   9   0 4308.86 755.486   4
   3   9   1 9311.52 1068.08   4
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   3   9   9 3280.39 754.293  18
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   3   9  11 169.021 264.001  18
   3   9  12 4266.97 842.805  18
   3   9  13 313.290 307.616  18
   3   9  14-85.9007 181.581  18
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   3  10   7-120.569 292.836  18
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   3  10   8 403.495 286.892  18
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   3  11   8 554.759 339.458  18
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   3  11  11-174.529 312.839  18
   3  11  12 444.305 318.921  18
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   3  12   8 138.079 254.909  18
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   3  12   9 725.320 388.147  18
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   3  12  10-497.010 336.292  18
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   3  13   9 74.9132 223.788  18
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   3  13  11 77.0513 156.832  18
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   4 -10   5 2676.84 1115.10  20
   4 -10   5 942.745 484.607  19
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   4  -9   8 4920.51 1019.20  24
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   4  -8   4 20067.2 1485.94   8
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   4  -8   7 5780.99 1520.53  20
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   4  -7   7 2706.71 562.738   8
   4  -7   7 3757.94 1213.36  20
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   4  -7   8 4800.97 777.980   8
   4  -7   8 6395.16 1517.55  20
   4  -7   9 10573.4 1404.98  24
   4  -7  10 381.290 381.412  24
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   4  -7  11 2257.36 644.213  24
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   4  -6   9 5369.26 1016.69  24
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   4  -5   4 72496.3 2294.12   8
   4  -5   5 12677.7 991.155   8
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   4  -5   6 25457.2 1456.41   8
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   4  -5   7 29792.3 1673.05   8
   4  -5   8 1343.15 442.763   8
   4  -5   9 14425.9 1581.32  24
   4  -5   9 12589.0 1218.91   8
   4  -5  10 2415.05 663.118  24
   4  -5  10 2200.38 555.517   8
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   4  -5  12 6871.95 1061.18  17
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  -4   4   9-235.594 311.740  14
  -4   4   8 10960.5 1159.82  16
  -4   4   8 12196.4 1226.27   6
  -4   4   8 9415.13 1041.39  14
  -4   4   7 688.110 270.368   6
  -4   4   6 21125.7 1489.00   6
  -4   4   5 16748.5 1238.50   6
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   4  -4   3 67883.2 1946.58   8
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  -4   4  -4 172.916 192.431   7
   4  -4   4 200.106 194.335   8
   4  -4   5 31531.3 1449.00   8
  -4   4  -5 34494.3 1569.78   7
   4  -4   6 30555.1 1520.48   8
  -4   4  -6 31276.8 1533.50   7
   4  -4   7 2035.31 466.419   8
   4  -4   8 26123.7 1604.50   8
   4  -4   9 8853.39 1013.65   8
   4  -4  10 250.076 286.553   8
   4  -4  10 795.811 414.993  24
   4  -4  11 4807.13 937.468  17
   4  -4  11 2913.81 622.063   8
   4  -4  12-631.844 471.232  17
   4  -4  13 3403.51 720.353  17
   4  -4  14 251.302 253.066  17
   4  -4  15-115.630 180.285  17
  -4   3  13 98.5959 220.317  16
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  -4   3  12 3881.64 639.101  16
  -4   3  12 3703.16 632.709  14
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  -4   3   4 115144. 2759.21  11
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   4  -3   3 972.121 232.583   8
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   4  -3   4 115822. 2401.30   8
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   4  -3   5 18691.1 1028.71   8
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   4  -3   6 50128.2 1838.10   8
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   4  -3   7 90082.5 2674.01   8
   4  -3   8 2564.35 527.312   8
   4  -3   9 25241.7 1637.26   8
   4  -3  10 12084.1 1431.16  17
   4  -3  10 12094.0 1215.40   8
   4  -3  10 12005.7 1368.02  24
   4  -3  11 241.357 330.424  17
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   4  -3  11 7.41301 269.642   8
   4  -3  12 3712.85 822.830  17
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   4  -3  13 861.406 441.133  17
   4  -3  13 623.479 323.906  21
   4  -3  13 469.697 348.143  13
   4  -3  14 1924.19 509.501  17
   4  -3  14 1020.86 369.027  21
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   4  -2   1 19381.8 990.371   3
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   4  -2   2 1084.27 231.778   3
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   4  -2   3 53097.0 1352.98   8
   4  -2   3 56190.7 1648.02   3
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   4  -2   4 802.007 214.115   8
   4  -2   5 70999.6 1890.08   8
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   4  -2   6 48088.3 1697.71   8
   4  -2   7 494.073 265.493   8
   4  -2   8 48556.0 2098.05   8
   4  -2   9 28426.7 1716.84   8
   4  -2  10 1564.87 471.775   8
   4  -2  11 7709.76 981.515   8
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   4  -2  11 7345.08 1046.17  21
   4  -2  11 10278.4 1306.12  17
   4  -2  12 2085.41 639.509  17
   4  -2  12 1340.63 505.561  21
   4  -2  13 2064.87 582.342  17
   4  -2  13 2051.23 602.776  21
   4  -2  14 4561.94 776.643  17
   4  -2  14 3350.99 682.603  21
   4  -2  14 5560.80 897.160  13
   4  -2  15-299.292 221.877  13
   4  -2  15-500.601 305.312  17
   4  -2  16 514.558 263.869  13
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  -4   1   6 38697.3 1844.70   6
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  -4   1   0 62605.0 1686.40  11
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   4  -1   1 33605.1 1260.89   3
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   4  -1   3 15960.4 839.390   3
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   4  -1   4 63612.6 1489.78   8
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   4  -1   5 59109.9 1627.51   8
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   4  -1   6 9225.30 738.748   8
   4  -1   7 42773.7 1755.03   8
   4  -1   8 5612.14 705.800   8
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   4  -1   9 11338.1 1059.18   8
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   4  -1  10 13338.0 1215.85   8
   4  -1  11-451.263 349.994  17
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   4  -1  11-532.188 453.410  21
   4  -1  11-320.169 280.332   8
   4  -1  12 5233.29 946.285  17
   4  -1  12 3671.52 689.421   8
   4  -1  12 4203.63 833.348  21
   4  -1  13 3132.36 712.099  17
   4  -1  13 2759.11 700.279  21
   4  -1  14 304.030 324.797  21
   4  -1  14-29.5883 322.638  13
   4  -1  15 3273.98 674.447  13
   4  -1  16 0.02742 177.725  13
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  -4   0   4 46918.4 1546.68  11
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  -4   0   1 78962.9 1577.91   6
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   4   0   1 180792. 2743.04   3
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   4   0   2 33507.9 1166.31   3
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   4   0   3 16992.1 832.689   3
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   4   0   4 47224.3 1465.13   3
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   4   0   5 56.1375 116.210   8
  -4   0  -6 100272. 2574.23  10
   4   0   6 93422.7 2276.25   8
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   4   0   7 35632.9 1551.09   8
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   4   0   8 4768.36 659.195   8
  -4   0  -9 29987.1 1790.08  10
   4   0   9 27056.5 1600.97   8
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   4   0  10 205.635 256.519   8
   4   0  11 13359.0 1449.84  17
   4   0  11 11474.0 1325.14  21
   4   0  11 12188.5 1204.41   8
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   4   0  12 5053.82 914.033  17
   4   0  12 3769.69 732.767   8
   4   0  12 5428.15 992.051  21
   4   0  13 2222.81 604.728  17
   4   0  13 2026.43 659.164  21
   4   0  14 6114.05 906.181  17
   4   0  14 8886.11 1209.69  13
   4   0  15-667.415 429.008  13
   4   0  16 1412.91 422.754  13
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   4   1   0 19957.1 916.203   3
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   4   1   1 12381.5 685.242   3
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   4   1   2 93600.2 1891.38   3
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   4   1   3 24677.7 1005.88   3
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   4   1   4 13458.7 771.914   3
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   4   1   5 56930.9 1448.69   8
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   4   1   6 13045.9 812.915   8
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   4   1   7 53973.7 1857.79   8
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   4   1   8 20900.4 1280.62   8
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   4   1   9 854.100 501.978   8
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   4   1  10 7165.13 901.545   8
   4   1  11 3766.70 806.657  17
   4   1  11 3064.93 678.637   8
   4   1  11 2965.29 713.806  21
   4   1  12 852.052 435.942  17
   4   1  12 1130.45 566.277  21
   4   1  12 1183.68 578.650   8
   4   1  13 3417.70 727.095  17
   4   1  13 4116.30 949.869  21
   4   1  14-492.380 449.113  13
   4   1  15 4810.91 883.777  13
   4   1  16 2234.81 503.935  13
   4   1  17-466.489 246.693  13
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  -4  -2   8 80.8579 296.419   9
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   4   2   0 2687.16 310.814   3
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   4   2   1 79059.0 1660.66   3
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   4   2   2 10960.6 626.300   3
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   4   2   3 11822.5 683.346   3
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   4   2   4 41986.7 1377.61   3
  -4  -2  -4 42856.7 1353.92   3
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   4   2   5 664.779 176.464   8
  -4  -2  -6 60093.8 1884.40  10
   4   2   6 56436.8 1655.08   8
  -4  -2  -7 87817.6 2466.38  10
   4   2   7 83558.2 2264.97   8
  -4  -2  -8 17556.7 1199.93  10
   4   2   8 17381.1 1171.29   8
  -4  -2  -9 42151.5 1973.60  10
   4   2   9 44900.3 2047.06   8
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   4   2  10 7235.40 936.697   8
   4   2  11 6322.20 973.719  17
   4   2  11 5460.33 911.782   8
   4   2  11 6067.60 1019.28  21
   4   2  12 8612.26 1168.85  17
   4   2  12 6468.47 939.271   8
   4   2  12 7789.30 1076.99  18
   4   2  13-188.136 239.834  17
   4   2  14 6728.32 1085.66  13
   4   2  15-339.058 472.355  13
   4   2  16-119.125 260.931  13
   4   2  17 1041.52 298.919  13
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  -4  -3  10 1762.46 480.075  16
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  -4  -3   9 892.504 413.208  16
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  -4  -3   8 8539.70 1054.67  21
  -4  -3   8 9093.74 1012.10  16
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  -4  -3   7 2383.46 561.974   9
  -4  -3   7 2281.06 519.088  14
  -4  -3   6 5785.71 784.882   9
  -4  -3   4 5090.06 530.033  11
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  -4  -3   2 59490.0 1771.36  11
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  -4  -3   0 17686.2 875.207   2
   4   3   0 18913.3 750.062   3
  -4  -3  -1 2063.59 333.127  10
   4   3   1 1554.03 228.092   3
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   4   3   2 19055.4 802.694   3
  -4  -3  -2 20110.5 725.658   5
   4   3   3 41818.5 1285.97   3
  -4  -3  -3 45100.6 1426.18  11
  -4  -3  -3 41498.6 1219.72   3
  -4  -3  -4 42.8087 92.3073   3
  -4  -3  -4 231.565 166.785  10
  -4  -3  -4 265.644 166.630  11
   4   3   4 132.024 119.825   3
  -4  -3  -5 25135.9 1162.15  10
  -4  -3  -6 22228.9 1178.18  10
   4   3   7 7338.97 680.017   8
  -4  -3  -7 8423.87 773.526  10
  -4  -3  -8 36441.3 1713.10  10
   4   3   8 35505.8 1629.77   8
  -4  -3  -9 3109.53 563.422  10
   4   3   9 3124.30 569.271   8
   4   3  10 5477.88 790.699   8
   4   3  11 18205.6 1634.87  17
   4   3  12 1221.26 432.847  18
   4   3  12 2079.38 602.756  17
   4   3  13 4809.55 857.881  18
   4   3  14 4471.06 892.944  13
   4   3  15 579.627 361.333  13
   4   3  16 3201.69 594.187  13
   4   3  17-38.1340 138.870  13
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  -4  -4   6 23147.9 1575.47   9
   4   4  -4 32221.6 1497.53   4
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   4   4   3 635.462 186.815   3
  -4  -4  -4 123210. 2531.99  10
  -4  -4  -4 121736. 2301.73   5
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   4   4  11 1270.87 503.713  17
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   4   4  12 5607.58 940.322  18
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   4   4  13 933.649 433.812  18
   4   4  14 1327.89 472.272  18
   4   4  14 2496.64 642.603  13
   4   4  15 3884.34 712.605  13
   4   4  16 75.0134 226.922  13
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  -4  -5   7 10130.9 1093.58   9
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   4   5  -4 5598.87 705.261   4
   4   5  -3 6307.85 726.951   4
   4   5  -2 35378.8 1612.46   4
   4   5  -1 1847.46 385.598   4
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   4   5   2 9594.24 759.637   4
  -4  -5  -3 132356. 2781.58  10
   4   5   3 130473. 2624.05   4
  -4  -5  -3 125363. 2391.19   5
  -4  -5  -4 46752.3 1668.14  10
   4   5   4 47200.6 1550.43   4
  -4  -5  -4 47335.4 1504.76   5
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   4   5   5 7916.30 611.039   4
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  -4  -5  -8 23878.5 1378.88  10
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   4   5  11 26140.4 2041.71  18
   4   5  12 1601.86 567.078  18
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   4   5  13 3103.59 733.562  18
   4   5  14 5820.28 882.274  13
   4   5  14 4183.58 772.442  18
   4   5  15 17.3224 237.038  13
   4   5  15-55.7403 210.652  18
   4   5  16 2123.20 436.730  13
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  -4  -6   7 4260.12 720.475  16
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   4   6  -4 20130.6 1349.27   4
   4   6  -3 23066.7 1458.11   4
   4   6  -2 1106.35 389.588   4
   4   6  -1 23674.1 1405.94   4
   4   6   0 2662.99 497.866   4
   4   6   1 2907.61 546.421   4
   4   6   2 55375.7 1976.78   4
  -4  -6  -2 50578.0 1611.63   5
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   4   6   3-99.3195 243.484   4
   4   6   4 40800.7 1577.69   4
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   4   6   5 16159.7 945.807   4
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   4   6  10 13506.7 1384.80  17
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   4   6  10 12580.8 1403.38  18
   4   6  11 2781.27 736.480  18
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   4   6  12 1848.91 600.103  18
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   4   6  13 1591.71 495.995  13
   4   6  14 625.819 373.955  18
   4   6  14 131.373 250.415  13
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   4   6  15 1439.89 420.061  18
   4   6  16 355.659 208.217  13
   4   6  16-78.8744 152.367  18
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  -4  -7   6 116.301 259.141  16
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   4   7  -4 15029.2 1252.97   4
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   4   7  -3 13.3781 293.377   4
   4   7  -2 18052.5 1345.80   4
   4   7  -1 9031.45 943.423   4
   4   7   0 3069.08 551.470   4
   4   7   1 29628.7 1644.14   4
   4   7   2 7065.37 833.587   4
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   4   7   3 42980.9 1819.60   4
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   4   7   4 12064.1 940.874   4
  -4  -7  -4 15531.7 1079.17   5
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   4   7   5 1051.27 295.369   4
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   4   7  10-560.216 387.459  18
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   4   7  14 1361.21 460.071  18
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   4   8  -4 2934.75 618.713   4
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   4   8  -3 15536.3 1356.05   4
   4   8  -2 2881.46 619.911   4
   4   8  -1 4619.17 749.134   4
   4   8   0 14025.5 1237.21   4
   4   8   1 274.359 374.215   4
   4   8   2 28138.4 1681.51   4
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   4   8   3 19445.3 1356.11   4
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   4   8   4 6487.67 769.247   4
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   4   8   9-177.497 316.812  18
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   4   9  -3 858.224 356.400   4
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   4   9  -2 5918.53 912.354   4
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   4   9  -1 15001.1 1402.72   4
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   4   9   0-1351.35 628.972   4
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   4   9   2 9064.36 1053.46   4
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   4   9   3 8627.46 1012.77   4
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   4   9   8 662.894 364.031  18
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   4  10   8 2524.98 662.429  18
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   4  10  11 1721.70 561.821  18
   4  10  12-229.502 281.414  18
   4  10  13 2003.19 525.190  18
   4  10  14 600.557 299.957  18
   4  10  15 140.116 154.919  18
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   4  11   9 474.406 348.203  18
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   4  11  11-148.965 245.950  18
   4  11  12 811.783 382.288  18
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   4  11  14-252.555 198.232  18
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   4  12   9 168.921 224.013  18
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   4  12  10-125.461 224.468  18
   4  12  11 860.563 369.265  18
   4  12  12-176.104 233.674  18
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  -4 -13   4 501.514 287.489  20
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   4  13  11-149.516 187.883  18
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   5 -14  -3 16.8745 238.469  19
   5 -14  -2 45.8231 225.370  19
   5 -14  -1-405.785 309.361  19
   5 -14   0-203.421 195.633  19
   5 -14   1 425.555 220.527  19
   5 -14   2 56.7521 222.296  19
   5 -14   3 621.637 288.051  19
   5 -14   4-30.8148 168.652  19
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   5  -3  10-36.9165 240.300   8
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   5   3  13 11702.6 1394.19  17
   5   3  13 9506.42 1239.86  18
   5   3  14-86.8985 301.179  18
   5   3  14 367.084 355.595  17
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   5   3  15 4445.71 828.665  13
   5   3  16 1789.89 461.374  13
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   5   5  -4-41.4597 315.297   4
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   5   5   4 644.433 259.773   4
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   5   5   5 27622.5 1249.54   4
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   5   5  10 23768.0 1932.29  17
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   5   5  11 20132.1 1819.72  17
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   5   5  11 18408.3 1754.04  18
   5   5  12 96.0377 259.075  18
   5   5  12-654.890 437.734  17
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   5   5  13 5050.07 883.658  17
   5   5  13 4568.46 899.831  18
   5   5  14 787.916 411.703  18
   5   5  14 1194.41 438.279  13
   5   5  15 629.790 299.376  18
   5   5  15 1103.75 397.299  13
   5   5  16 1432.74 386.670  13
   5   5  16 1168.55 331.999  18
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   6   0  15 1338.83 480.084  17
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   6   0  16 394.903 234.512  17
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   6   1  12 11590.5 1478.46  17
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   6   1  13 561.877 472.284  17
   6   1  14 1106.93 430.390  18
   6   1  14 3543.04 819.187  17
   6   1  15 4743.40 800.099  17
   6   1  16 56.3738 158.716  17
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   6   2  11 9132.19 1304.49  17
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   6   2  13 2159.57 680.276  17
   6   2  14 2765.95 653.978  18
   6   2  14 4326.97 898.825  17
   6   2  15 184.620 275.401  18
   6   2  15 162.726 355.059  17
   6   2  16 896.706 325.519  17
   6   2  16 1887.20 480.857  13
   6   2  17 264.730 202.316  13
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  -6  -3   6 5435.39 851.236  14
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   6   3  11-374.331 379.883  17
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   6   3  12 16933.2 1793.17  17
   6   3  13 6558.31 1129.01  17
   6   3  13 4484.65 874.575  18
   6   3  14 318.078 307.406  18
   6   3  14 1236.24 527.068  17
   6   3  15 4029.21 707.905  17
   6   3  15 2822.25 606.210  18
   6   3  16-30.0428 218.795  13
   6   3  17 307.058 188.669  13
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  -6  -4  -8 28813.0 1724.69  10
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   6   4  10 364.152 326.492  17
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   6   4  11 10096.6 1365.52  17
   6   4  12 5015.25 1006.25  17
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   6   4  13 1146.53 466.994  18
   6   4  13 2173.71 677.205  17
   6   4  14 6108.65 970.731  17
   6   4  14 5120.52 891.479  18
   6   4  15-15.7698 230.097  18
   6   4  15 461.867 325.083  17
   6   4  15-342.340 352.254  13
   6   4  16 665.162 284.181  18
   6   4  16 1311.05 388.257  13
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  -6  -5   4 2619.87 589.790  16
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   6   5  -4 1930.38 470.568   4
   6   5  -3 19612.6 1425.90   4
  -6  -5   1 48321.9 1976.88  11
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  -6  -5  -1 3521.72 552.908  11
  -6  -5  -2 44220.5 1897.25  11
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   6   5  10 13411.6 1538.30  17
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   6   5  11 1116.37 536.205  17
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   6   5  12 2262.82 679.299  18
   6   5  12 3255.11 841.728  17
   6   5  13 2499.77 673.817  18
   6   5  13 3330.20 791.818  17
   6   5  14-472.816 375.553  18
   6   5  14 680.658 426.285  17
   6   5  15 1402.01 462.021  18
   6   5  15 1763.29 473.171  13
   6   5  16 329.607 244.163  13
   6   5  16 32.0003 158.046  18
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  -6  -6   8 1124.24 428.088  16
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   6   6  -3-161.321 341.792   4
   6   6  -2 11334.3 1145.49   4
   6   6  -1 16869.4 1347.56   4
   6   6   0 278.775 339.854   4
   6   6   1 18060.7 1359.32   4
   6   6   2 5478.39 768.820   4
   6   6   3 5401.82 722.217   4
  -6  -6  -4 11962.9 1067.33  10
   6   6   4 12605.4 1040.97   4
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   6   6   5-24.3879 237.610   4
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   6   6   9 18502.4 1737.88  17
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   6   6  10 3031.22 756.351  18
   6   6  10 3623.56 834.261  17
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   6   6  11 307.995 320.560  18
   6   6  11 728.305 403.089  17
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   6   6  12 1241.05 524.317  18
   6   6  12 1819.85 620.949  17
   6   6  13-167.993 281.034  18
   6   6  13 230.558 273.956  17
   6   6  14 2747.12 687.642  18
   6   6  15 630.958 308.870  18
   6   6  15 478.846 266.373  13
   6   6  16 115.193 150.345  18
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  -6  -7   7 420.976 234.576  16
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  -6  -7   4 460.188 179.139   9
  -6  -7   4 609.014 259.485  23
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   6   7  -3 17735.0 1452.96   4
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   6   7  -2 10277.6 1134.89   4
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   6   7  -1 7460.05 967.662   4
   6   7   0 35832.0 2051.39   4
   6   7   1 3038.70 663.519   4
   6   7   2 15994.9 1326.63   4
   6   7   3 13723.3 1202.35   4
   6   7   4 1489.61 454.804   4
   6   7   5 12448.2 1068.49   4
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   6   7   9-57.5086 294.847  18
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  -6  -7 -10 3659.75 921.779  19
   6   7  10 3737.13 881.664  18
   6   7  11 1596.09 618.051  18
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   6   7  12-237.162 332.087  18
   6   7  13 795.184 396.709  18
   6   7  14-261.187 292.420  18
   6   7  15 504.736 285.855  18
   6   7  16 335.733 208.847  18
  -6  -8   9 348.843 192.691  21
  -6  -8   8 148.130 141.411  16
  -6  -8   8 265.350 152.670  21
  -6  -8   7 16.3845 174.573  16
  -6  -8   7 174.100 152.498  21
  -6  -8   6 1297.96 337.321  16
  -6  -8   6 872.370 250.467  21
  -6  -8   5-164.860 240.152  16
  -6  -8   5 88.8290 150.914  21
  -6  -8   4 2671.30 491.443  16
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   6   8  -3 789.426 438.853   4
  -6  -8   2 932.392 329.893  16
  -6  -8   2 1456.80 542.849  15
   6   8  -2 596.059 324.462   4
  -6  -8   1 4954.82 657.879  16
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  -6  -8   1 7014.89 1091.55  15
   6   8  -1 7517.39 1008.93   4
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  -6  -8   0 583.764 366.884  15
   6   8   0-399.157 432.801   4
   6   8   1 15836.4 1429.99   4
   6   8   2 20530.3 1590.38   4
   6   8   3-171.661 330.819   4
   6   8   4 14510.2 1248.86   4
   6   8   5 4051.03 670.883   4
  -6  -8  -6 5104.80 723.170   5
  -6  -8  -7 8185.46 1397.81  19
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   6   8   8 16.9142 269.512  18
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   6   8   9 8703.29 1217.86  18
   6   8  10 2722.59 747.191  18
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   6   8  11 662.611 451.401  18
  -6  -8 -11 465.400 417.386  19
   6   8  12 2944.14 735.416  18
   6   8  13 58.8305 233.171  18
   6   8  14 1057.69 421.120  18
   6   8  15 877.164 331.702  18
  -6  -9   8 598.871 220.713  16
  -6  -9   8 272.594 197.601  21
  -6  -9   7 840.346 236.922  16
  -6  -9   7 660.989 213.440  21
  -6  -9   6 78.7953 204.325  16
  -6  -9   6 27.9602 158.801  21
  -6  -9   5 1718.53 380.756  16
  -6  -9   5 1556.82 356.693  21
  -6  -9   4-358.018 250.031  16
  -6  -9   4-83.9854 233.570  20
  -6  -9   3 2489.63 490.540  16
  -6  -9   2 942.381 349.381  16
  -6  -9   2 508.193 248.394  15
  -6  -9   1 707.048 308.162  16
  -6  -9   1 337.883 210.938  15
   6   9  -1 961.375 477.332   4
  -6  -9   0 2859.18 535.752  16
   6   9   0 3955.19 795.735   4
  -6  -9   0 3259.52 801.213  15
  -6  -9  -1 735.457 434.836  16
  -6  -9  -1-56.0432 278.396  15
   6   9   1-66.4838 384.221   4
  -6  -9  -2 2121.27 618.114  16
  -6  -9  -2 1794.82 630.396  15
   6   9   2 2439.92 646.281   4
  -6  -9  -3 6374.37 1152.88  15
   6   9   3 8857.40 1112.98   4
  -6  -9  -3 8001.63 1224.95  19
  -6  -9  -4 650.707 483.455  15
   6   9   4 979.897 439.607   4
  -6  -9  -4-51.4442 337.244  19
   6   9   5 1120.12 442.347   4
  -6  -9  -5 513.455 403.842  15
  -6  -9  -5 2035.96 685.283  19
  -6  -9  -6 2371.11 480.080   5
  -6  -9  -6 1898.60 615.828  15
  -6  -9  -6 1850.97 720.457  19
  -6  -9  -7-409.671 349.798   5
  -6  -9  -7-164.572 203.804  19
  -6  -9  -8 1713.43 339.357   5
  -6  -9  -8 2970.19 910.524  19
   6   9   9 1344.58 530.114  18
  -6  -9  -9 1984.06 738.358  19
   6   9  10 360.843 329.278  18
  -6  -9 -10-180.001 277.511  19
   6   9  11 2458.21 701.953  18
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   6   9  12 580.339 396.366  18
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   7  -5   8 4573.46 844.571  17
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   7  -5  11 3902.38 820.826  17
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   7  -5  12 413.527 315.333  17
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   7  -4   8 80.1727 213.686  17
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   7  -2  10 7376.07 1050.52  12
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   7   3  13-15.4464 326.502  17
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   7   3  14 3291.26 794.516  17
   7   3  15 1814.39 506.378  18
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   7   4  11 11943.9 1517.62  17
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   7   4  14 4758.38 920.116  17
   7   4  15-36.1926 233.877  18
   7   4  15 51.9569 239.149  17
   7   4  16 1684.61 412.189  18
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   7   5  -3 6051.16 888.362   4
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   7   5   9 10733.0 1357.83  17
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   7   5  10 9531.35 1358.57  17
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  -7  -5 -10 8743.64 1063.98   5
   7   5  11 542.633 466.279  17
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   7   5  12 1731.88 642.337  18
   7   5  12 2970.28 797.609  17
   7   5  13 717.069 440.682  18
   7   5  13 514.112 408.258  17
   7   5  14-29.6070 299.276  18
   7   5  14-39.6340 289.721  17
   7   5  15 1219.20 426.633  18
   7   5  16 27.6699 172.727  18
   7   5  16-37.0779 157.192  13
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  -7  -6   3 983.238 465.371  16
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   7   6  -3 601.431 361.472   4
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   8 -12   6-349.794 191.875  12
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   8 -11   6 2442.46 535.258  12
   8 -11   7-109.407 231.246  12
   8 -11   8 208.554 205.028  12
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   8 -10   4 782.331 489.768  19
   8 -10   5 1129.11 390.278  25
   8 -10   5 863.166 483.871  19
   8 -10   7-468.068 361.206  12
   8 -10   8 1100.33 379.283  12
   8 -10   9 125.855 183.167  12
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   8  -8   4-625.105 496.632  19
   8  -8   5 6431.11 1255.38  19
   8  -8   6 4054.96 961.306  19
   8  -8   8 7771.70 1043.34  12
   8  -8   9 772.305 370.775  12
   8  -8  10 668.384 286.854  12
   8  -8  11 983.284 331.101  17
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   8  -7   2 4924.36 1100.46  19
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   8  -7   3-321.849 462.104  19
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   8  -7   5 2161.05 753.718  19
   8  -7   6 1699.91 474.509  25
   8  -7   6 898.687 471.650  19
   8  -7   8 490.426 358.162  12
   8  -7   9 5740.58 913.838  12
   8  -7  10 1987.89 508.946  17
   8  -7  10 4463.73 760.969  12
   8  -7  11-159.881 264.920  17
   8  -7  11-449.356 330.772  12
   8  -7  12 669.623 274.347  17
   8  -7  12 931.600 276.898  12
  -8   6   9 166.973 142.702  16
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  -8   6   1 568.212 326.805  11
  -8   6   1 745.375 432.100  22
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   8  -6   0 2990.09 794.055  19
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   8  -6   1 11986.0 1592.38  19
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  -8   6  -2-545.149 319.449  11
  -8   6  -2-153.214 270.487  22
   8  -6   2-518.996 432.281  19
  -8   6  -2-360.714 347.253   7
   8  -6   3 14803.4 1865.51  19
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   8  -6   5 3877.73 1006.52  19
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   8  -6   6 7165.94 954.930  25
   8  -6   6 8705.36 1415.94  19
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   8  -6   7 706.389 476.524  12
   8  -6   8 5841.76 990.932  12
   8  -6   9 4196.45 814.846  12
   8  -6  10 823.230 380.471  17
   8  -6  10 886.663 436.927  12
   8  -6  11 4633.11 789.111  17
   8  -6  11 6889.16 880.920  12
   8  -6  12 242.554 251.258  17
   8  -6  12-6.37107 215.667  12
   8  -6  13 775.397 296.947  17
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   8  -5   5 17667.0 2004.81  19
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   8  -5   9 321.403 369.239  12
   8  -5  10 2612.48 668.075  17
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   8  -5  11 19.8099 290.734  17
   8  -5  11-1147.27 464.695  12
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   8  -5  12 2202.84 496.289  12
   8  -5  13 941.848 383.031  17
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   8  -4   6 33484.3 2239.70  12
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   8  -4   9 7331.52 1087.76  12
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   8  -4  11 3472.26 767.141  17
   8  -4  11 4044.22 766.566  12
   8  -4  12 1093.42 476.751  17
   8  -4  12 887.897 365.083  12
   8  -4  13 717.976 391.896  17
   8  -4  14 1112.56 366.610  17
   8  -4  15-458.579 223.825  17
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   8  -3   9 2875.99 703.471  12
   8  -3  10 5165.41 954.524  17
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   8  -3  11 5281.54 975.901  17
   8  -3  11 5602.76 894.200  12
   8  -3  12 161.351 344.342  17
   8  -3  12 230.386 296.205  12
   8  -3  13 3518.11 759.526  17
   8  -3  14 597.222 302.175  17
   8  -3  15 545.981 276.564  17
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   8  -2  12 7393.41 1182.01  17
   8  -2  12 6151.26 889.862  12
   8  -2  13-344.618 392.053  17
   8  -2  14 1018.68 430.725  17
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   8  -1  10 8288.33 1133.76  12
   8  -1  11 13262.4 1560.30  17
   8  -1  11 12638.8 1372.12  12
   8  -1  12 317.614 353.350  17
   8  -1  12 690.459 372.352  12
   8  -1  13 10592.8 1373.53  17
   8  -1  14 3263.10 734.923  17
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   8   0   9 1945.58 580.157  17
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   8   0  10 10685.8 1378.13  17
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   8   0  10 13206.6 1444.82  12
   8   0  11-439.545 402.024  17
   8   0  11-784.208 330.515  12
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   8   0  13 2635.74 776.789  17
   8   0  14 2514.94 727.440  17
   8   0  15 1012.93 340.011  18
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   8   1  11 16259.8 1607.22  12
   8   1  12 855.370 596.624  17
   8   1  12 1106.92 618.172  12
   8   1  13 1969.77 724.872  17
   8   1  14 4123.22 871.127  17
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   8   1  15-4.93773 290.119  17
   8   1  16 639.774 277.236  17
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   8   2   9 5366.25 1008.91  12
   8   2  10 21342.5 1973.64  17
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   8   2  10 24303.3 1963.02  12
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   8   2  11 2382.78 867.491  12
   8   2  12 7513.28 1268.02  17
   8   2  13 6494.33 1140.81  17
   8   2  14 278.725 409.481  17
   8   2  15 1787.73 486.798  18
   8   2  15 2945.04 651.450  17
   8   2  16 571.565 244.396  18
   8   2  16 263.809 226.564  17
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   8   3   9 13061.1 1484.14  17
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   8   3   9 9886.20 1112.18  25
   8   3   9 14561.3 1516.69  12
   8   3  10 196.976 370.424  17
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   8   3  10 672.689 551.462  12
   8   3  11 11328.7 1517.90  17
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   8   3  12 5191.04 1051.15  17
   8   3  13 1243.93 631.876  17
   8   3  14 1958.02 579.834  18
   8   3  14 4094.82 881.044  17
   8   3  15 204.518 249.368  18
   8   3  15 1453.07 502.763  17
   8   3  16 165.933 192.602  18
   8   3  16 382.580 240.947  17
   8   3  16 95.4162 197.854  13
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  -8 -12  -6 7.25076 163.113  19
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   9 -12  -1 101.556 154.120  25
   9 -12   0-297.899 219.853  25
   9 -12   1 318.048 218.818  25
   9 -12   2-185.453 194.381  25
   9 -12   3-172.819 175.716  25
   9 -11  -2 353.646 215.911  25
   9 -11  -1-76.9443 218.598  25
   9 -11   2 81.4354 232.308  25
   9 -11   3 810.414 341.096  25
   9 -11   4-171.152 225.132  25
   9 -11   4-501.715 251.299  12
   9 -11   5 251.378 255.568  12
   9 -11   6 424.054 230.657  12
   9 -11   7 257.422 185.980  12
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   9 -10  -3 174.070 194.765  25
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   9 -10   0 665.533 385.882  19
   9 -10   1-237.740 312.387  19
   9 -10   2 285.076 283.268  19
   9 -10   3 321.223 349.662  19
   9 -10   4 147.004 238.400  25
   9 -10   4 200.926 268.500  12
   9 -10   5 535.809 281.762  25
   9 -10   5 767.257 338.855  12
   9 -10   6 80.4796 225.796  12
   9 -10   7 1521.66 435.521  12
   9 -10   8 602.318 267.047  12
   9 -10   9 268.270 178.418  12
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   9  -9  -3-238.387 198.649  25
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  -9   9   1 953.413 425.538  22
  -9   9   0 509.143 343.266  22
   9  -9   0 481.974 376.240  19
   9  -9   1 1868.27 640.308  19
   9  -9   2 77.3503 333.661  19
   9  -9   3 650.580 439.679  19
   9  -9   3 607.839 312.615  12
   9  -9   4 245.879 277.188  19
   9  -9   4 712.321 385.902  12
   9  -9   5 253.984 271.044  25
   9  -9   5 124.716 293.936  12
   9  -9   6 1872.43 449.969  25
   9  -9   6 3657.76 730.606  12
   9  -9   7 663.285 396.717  12
   9  -9   8 740.144 332.646  12
   9  -9   9 1976.27 453.360  12
   9  -9  10 143.872 190.707  12
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  -9   8   4 118.293 265.648  22
   9  -8  -3 930.075 359.351  25
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   9  -8   0 3112.79 805.060  19
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   9  -8   1-158.680 327.236  19
   9  -8   2 3185.58 892.001  19
   9  -8   3 1254.36 614.119  19
   9  -8   3 783.898 367.324  12
   9  -8   4 389.481 402.086  19
   9  -8   4-198.065 280.791  12
   9  -8   5 6571.69 933.672  25
   9  -8   5 5956.28 1194.60  19
   9  -8   5 6222.59 993.239  12
   9  -8   6 1472.52 417.924  25
   9  -8   6 730.019 460.258  12
   9  -8   7 3645.77 766.119  12
   9  -8   8 3240.82 655.852  12
   9  -8   9-150.890 286.199  12
   9  -8  10 1866.58 445.313  12
   9  -8  11 484.022 224.179  12
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  -9   7   5 87.8466 233.129  23
  -9   7   5 217.504 244.717  22
  -9   7   4 2193.27 549.008  22
  -9   7   3 101.334 277.188  22
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  -9   7   1 3400.05 779.280  22
  -9   7   0 62.1250 274.356  22
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   9  -7   1 2356.80 725.568  19
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   9  -7   2 1202.35 583.322  19
   9  -7   3 1022.87 553.330  19
   9  -7   4 3322.06 720.425  12
   9  -7   4 3638.94 958.084  19
   9  -7   5 747.598 409.476  25
   9  -7   5 750.151 542.247  19
   9  -7   5 627.008 401.350  12
   9  -7   6 3283.02 667.961  25
   9  -7   6 3903.60 841.339  12
   9  -7   7 5956.09 995.667  12
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   9   1  12 995.890 637.666  17
   9   1  12 3410.07 1015.61  12
   9   1  13 7247.71 1150.40  17
   9   1  14 736.040 470.973  17
   9   1  15 171.957 208.206  18
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   9   2   9 3795.22 835.835  17
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   9   2  12 11595.7 1491.53  17
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   9   2  13 1226.49 629.328  17
   9   2  14 3655.32 812.477  17
   9   2  15 1290.40 414.527  18
   9   2  15 2687.40 570.330  17
   9   2  16 172.276 167.860  18
   9   2  16 425.707 232.476  17
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   9   3   7 1621.62 520.934  17
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   9   3   7 2065.51 598.110  25
   9   3   7 2877.15 748.629  12
   9   3   8 6482.45 1025.82  17
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   9   3   8 7380.83 1090.55  25
   9   3   8 8153.85 1201.59  12
   9   3   9 7637.30 1169.14  17
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   9   3   9 6756.40 1036.94  25
   9   3   9 9333.31 1304.62  12
   9   3  10-200.608 363.466  17
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   9   3  10 140.772 434.021  12
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  12   5  12 65.9396 179.370  18
 -12  -5 -12-40.8068 233.270  19
  12   5  13 431.662 242.216  18
 -12  -5 -13 380.759 232.863  19
 -12  -6   0 42.7796 121.971  23
 -12  -6   0 470.717 297.487  15
 -12  -6  -1 1013.92 298.168  15
 -12  -6  -1 1450.82 305.106  23
 -12  -6  -2 315.510 194.579  23
 -12  -6  -2-89.5989 157.492  15
 -12  -6  -3 367.889 181.147  23
 -12  -6  -3 687.879 406.972  15
 -12  -6  -4 1258.33 385.558  15
 -12  -6  -5-23.4492 151.245  15
 -12  -6  -6 708.685 295.956  15
 -12  -6  -6 1451.32 378.111  19
 -12  -6  -7 471.093 277.695  15
 -12  -6  -7 592.638 285.736  19
 -12  -6  -8 458.856 236.194  15
 -12  -6  -8 667.139 297.553  19
 -12  -6  -9 1911.47 466.898  19
 -12  -6 -10-31.0330 181.687  19
 -12  -6 -11 478.883 337.540  19
 -12  -6 -12 874.416 378.624  19
 -12  -7   0 1337.93 378.016  15
 -12  -7  -1-229.532 229.929  15
 -12  -7  -2 1231.18 440.345  15
 -12  -7  -3 1257.28 504.543  15
 -12  -7  -4 166.631 169.363  15
 -12  -7  -5 936.274 317.319  15
 -12  -7  -6 66.2287 144.362  15
 -12  -7  -6-8.87190 145.002  19
 -12  -7  -7 358.385 224.538  15
 -12  -7  -7 514.846 250.427  19
 -12  -7  -8 642.638 243.909  15
 -12  -7  -8 941.105 322.834  19
 -12  -7  -9 399.310 348.684  19
 -12  -7 -10 1074.00 330.261  19
 -12  -7 -11-593.153 393.772  19
 -12  -7 -12-124.442 219.336  19
 -12  -8  -1 939.437 324.933  15
 -12  -8  -2 1121.75 373.022  15
 -12  -8  -3 289.303 271.568  15
 -12  -8  -4 1562.32 509.484  15
 -12  -8  -5-460.870 346.144  15
 -12  -8  -6 352.549 188.886  15
 -12  -8  -7 387.987 202.921  15
 -12  -8  -7 723.285 242.414  19
 -12  -8  -8-238.673 175.684  19
 -12  -8  -9 1143.75 461.266  19
 -12  -8 -10 387.649 289.471  19
 -12  -8 -11 408.971 301.264  19
 -12  -9  -2-62.5655 160.698  15
 -12  -9  -3 407.883 258.694  15
 -12  -9  -4-149.154 132.453  15
 -12  -9  -5 175.553 145.490  15
 -12  -9  -6 413.261 195.237  15
 -12  -9  -7-174.799 139.581  15
 -12  -9  -7-408.967 238.365  19
 -12  -9  -8 434.530 272.218  19
 -12  -9  -9-57.7462 196.349  19
 -12  -9 -10-41.6633 207.962  19
 -12 -10  -4 170.247 168.467  15
 -12 -10  -5 210.230 185.073  15
 -12 -10  -6 111.931 154.538  15
  13  -6   2 110.538 149.903  25
  13  -6   3 225.656 194.671  25
  13  -6   4-342.600 232.695  25
  13  -6   5-362.259 234.167  25
  13  -6   6 33.8770 165.491  25
  13  -5   1-204.330 163.257  25
  13  -5   2 651.516 263.988  25
  13  -5   3 420.247 244.683  25
  13  -5   4-159.434 270.397  25
  13  -5   5 2248.65 499.067  25
  13  -5   6 328.274 248.828  25
  13  -5   7 778.241 288.308  25
  13  -5   8 151.446 182.991  25
 -13   4   0-204.011 156.118  23
  13  -4   1 671.158 266.629  25
  13  -4   2 218.256 210.443  25
  13  -4   3 134.316 199.097  25
  13  -4   4 1667.27 459.024  25
  13  -4   5-1008.78 424.378  25
  13  -4   6 906.778 364.148  25
  13  -4   7 960.246 372.673  25
  13  -4   8-151.634 233.845  25
  13  -4   8-161.797 171.032  12
  13  -4   9 64.5424 163.732  25
  13  -4   9 833.739 297.842  12
 -13   3   1 197.918 153.496  23
 -13   3   0 590.582 213.634  23
  13  -3   1-190.049 221.149  25
 -13   3  -1-155.476 171.839  23
  13  -3   2 692.091 286.507  25
  13  -3   3 1556.99 434.764  25
  13  -3   4-360.876 349.574  25
  13  -3   5 418.125 276.569  25
  13  -3   6 1225.98 428.677  25
  13  -3   7 215.449 278.289  25
  13  -3   8 1767.95 449.713  25
  13  -3   8 1551.58 423.177  12
  13  -3   9 499.983 254.924  25
  13  -3   9 544.998 298.019  12
  13  -3  10 102.366 189.374  12
 -13   2   2-8.28342 111.403  23
 -13   2   1 1397.81 305.251  23
 -13   2   0 11.7390 168.817  23
 -13   2  -1 901.370 282.495  23
  13  -2   2 1040.05 347.646  25
  13  -2   3-410.716 355.720  25
  13  -2   4 2971.94 653.661  25
  13  -2   5 574.471 367.268  25
  13  -2   6 1173.65 476.817  25
  13  -2   7 3403.07 693.444  25
  13  -2   8 725.099 402.037  25
  13  -2   8-236.299 238.030  12
  13  -2   9 1114.26 358.525  25
  13  -2   9 967.111 346.914  12
  13  -2  10 596.833 275.389  25
 -13   2 -11-296.911 221.325  19
 -13   1   2 1297.37 286.168  23
 -13   1   1 760.154 272.178  23
 -13   1   0 1487.02 366.120  23
 -13   1  -1 1648.47 393.017  23
  13  -1   2-25.2885 230.771  25
 -13   1  -2 190.406 273.082  23
  13  -1   3 3096.95 617.212  25
  13  -1   4 1017.37 482.647  25
  13  -1   5-256.424 345.719  25
  13  -1   6 1034.52 436.480  25
  13  -1   7-325.486 369.411  25
  13  -1   8 4143.81 749.861  25
  13  -1   9 2538.97 569.005  25
  13  -1  10 384.717 293.097  25
 -13   1 -11 2655.05 586.166  19
 -13   0   2 591.080 223.172  23
 -13   0   1 1990.46 390.499  23
 -13   0   0 1231.37 359.559  23
 -13   0  -1 1274.50 398.117  23
  13   0   2 4337.26 670.781  25
 -13   0  -2 4888.59 665.370  23
  13   0   3 743.112 381.485  25
  13   0   4 2524.27 642.026  25
  13   0   5 3102.58 711.521  25
  13   0   6-190.882 361.916  25
  13   0   7 1952.55 625.930  25
  13   0   8 1021.39 477.407  25
  13   0   9 2074.64 581.400  25
 -13   0 -10 919.968 411.862  19
 -13   0 -11-85.6125 211.349  19
 -13  -1   2 502.949 204.820  23
 -13  -1   1 846.466 288.626  23
 -13  -1   0 710.526 312.386  23
 -13  -1   0 683.812 333.724  15
 -13  -1  -1 2777.74 513.690  23
 -13  -1  -2 1029.69 459.656  23
  13   1   3 2347.50 562.824  25
  13   1   4 4011.37 769.062  25
  13   1   5 586.882 473.807  25
  13   1   6 2649.11 666.807  25
  13   1   7 2006.01 673.527  25
  13   1   8 881.083 454.487  25
  13   1   9 3053.24 647.090  25
 -13  -1  -9 3154.71 771.833  19
 -13  -1 -10-321.985 304.939  19
 -13  -1 -11 1797.99 546.388  19
 -13  -1 -12 979.982 371.598  19
 -13  -2   2 194.796 168.023  23
 -13  -2   1 288.870 190.364  23
 -13  -2   0 1054.61 321.586  23
 -13  -2   0 1233.83 367.614  15
 -13  -2  -1-160.004 194.293  23
 -13  -2  -1 458.870 306.954  15
 -13  -2  -2 1033.63 351.610  23
  13   2   3 725.040 352.405  25
  13   2   4 357.079 368.911  25
  13   2   5 805.728 415.780  25
  13   2   6 619.061 512.739  25
 -13  -2  -6 662.991 406.634  19
  13   2   7 788.207 536.767  25
 -13  -2  -7 1174.07 509.689  19
  13   2   8 1951.36 599.685  25
 -13  -2  -8 1577.69 537.763  15
 -13  -2  -8 856.128 462.795  19
 -13  -2  -9 579.133 440.352  19
 -13  -2 -10 2791.95 711.860  19
 -13  -2 -11 1272.49 506.633  19
 -13  -2 -12 451.895 255.547  19
 -13  -3   1 1193.17 218.148  23
 -13  -3   0-180.846 132.772  23
 -13  -3   0 291.377 214.793  15
 -13  -3  -1 1163.88 247.495  23
 -13  -3  -1 1746.00 492.019  15
 -13  -3  -2-100.523 145.066  23
 -13  -3  -2 662.838 340.053  15
 -13  -3  -3 246.342 146.222  23
 -13  -3  -3 647.414 433.818  15
 -13  -3  -4 1691.61 562.159  15
 -13  -3  -5 555.443 392.888  15
 -13  -3  -6 2003.21 651.200  15
 -13  -3  -6 2053.32 561.875  19
 -13  -3  -7 887.635 445.750  15
 -13  -3  -7 1276.76 496.737  19
 -13  -3  -8 140.574 160.011  15
 -13  -3  -8 476.862 391.546  19
 -13  -3  -9 3110.74 742.941  19
 -13  -3 -10 569.584 385.322  19
 -13  -3 -11 698.446 370.328  19
 -13  -3 -12 881.998 342.701  19
 -13  -4   1-311.192 198.955  23
 -13  -4   0 1751.07 400.825  15
 -13  -4   0 1968.50 385.792  23
 -13  -4  -1 499.540 266.897  23
 -13  -4  -1 227.648 233.226  15
 -13  -4  -2 288.347 138.479  23
 -13  -4  -2 583.306 322.176  15
 -13  -4  -3 1941.90 440.535  23
 -13  -4  -3 2265.97 616.742  15
 -13  -4  -4-787.097 434.494  15
 -13  -4  -5 452.463 241.292  15
 -13  -4  -6 1079.73 353.364  15
 -13  -4  -6 1506.49 347.351  19
 -13  -4  -7-0.16257 269.854  15
 -13  -4  -7-160.492 183.693  19
 -13  -4  -8 1201.45 323.720  15
 -13  -4  -8 1228.37 347.896  19
 -13  -4  -9-56.4666 154.381  19
 -13  -4 -10 906.122 451.529  19
 -13  -4 -11 161.370 236.858  19
 -13  -4 -12 133.263 198.060  19
 -13  -5   0 33.3697 156.898  23
 -13  -5  -1 1291.31 332.194  23
 -13  -5  -1 1442.67 385.933  15
 -13  -5  -2 331.675 218.210  23
 -13  -5  -2 721.776 348.637  15
 -13  -5  -3 407.521 324.564  15
 -13  -5  -4 924.735 351.510  15
 -13  -5  -5 1724.44 527.613  15
 -13  -5  -6-12.4021 129.123  15
 -13  -5  -7 767.737 384.802  15
 -13  -5  -7 1014.60 291.416  19
 -13  -5  -8-133.723 222.100  15
 -13  -5  -8 207.170 165.332  19
 -13  -5  -9 710.760 380.151  19
 -13  -5 -10 374.424 302.269  19
 -13  -5 -11-131.898 244.396  19
 -13  -6  -1 512.233 231.173  15
 -13  -6  -2-263.804 239.006  15
 -13  -6  -3 1045.00 370.481  15
 -13  -6  -4-91.0345 261.495  15
 -13  -6  -5 161.722 203.965  15
 -13  -6  -6 2398.22 596.813  15
 -13  -6  -7 102.699 225.676  15
 -13  -6  -7-501.855 297.324  19
 -13  -6  -8 1634.89 443.689  15
 -13  -6  -8 1264.33 434.010  19
 -13  -6  -9 1424.54 475.187  19
 -13  -6 -10 149.051 224.306  19
 -13  -6 -11 1785.60 484.021  19
 -13  -7  -2 731.142 268.971  15
 -13  -7  -3-142.862 183.873  15
 -13  -7  -4-102.902 245.845  15
 -13  -7  -5 711.217 335.046  15
 -13  -7  -6-133.636 188.941  15
 -13  -7  -7 593.141 286.176  15
 -13  -7  -8 577.125 296.926  19
 -13  -7  -9 35.3615 202.276  19
 -13  -7 -10 1170.09 365.439  19
 -13  -8  -3 392.460 214.591  15
 -13  -8  -4-83.8839 174.377  15
 -13  -8  -5-149.262 188.851  15
 -13  -8  -6 643.186 278.221  15
  14  -4   5-226.124 198.242  25
  14  -4   6 1192.02 343.277  25
  14  -3   3-68.7474 190.516  25
  14  -3   4-225.845 214.686  25
  14  -3   5 183.116 202.040  25
  14  -3   6 44.0432 182.208  25
  14  -3   7 483.834 250.120  25
  14  -2   3 127.016 150.214  25
  14  -2   4 638.325 262.786  25
  14  -2   5-331.747 286.968  25
  14  -2   6-795.409 355.136  25
  14  -2   7 414.847 271.841  25
  14  -2   8 367.594 251.060  25
  14  -1   3 242.199 178.377  25
  14  -1   4-328.102 259.885  25
  14  -1   5 1060.45 370.885  25
  14  -1   6 447.735 252.818  25
 -14   1  -6 579.988 257.836  19
  14  -1   7 1143.24 408.348  25
 -14   1  -7 109.200 179.983  19
  14  -1   8 883.488 332.091  25
 -14   1  -8 1589.13 431.588  19
 -14   1  -9-254.461 245.646  19
 -14   0  -2 649.320 288.659  15
  14   0   3-400.541 253.667  25
  14   0   4 336.898 240.815  25
  14   0   5 186.320 265.997  25
  14   0   6 107.855 242.181  25
 -14   0  -6 158.978 199.556  19
  14   0   7 139.856 247.205  25
 -14   0  -7 596.240 298.860  19
  14   0   8 270.589 295.273  25
 -14   0  -8-238.632 231.338  19
 -14   0  -9 1591.13 431.615  19
 -14  -1  -2 217.614 221.318  15
 -14  -1  -3 1289.78 395.244  15
  14   1   4 99.8555 197.768  25
  14   1   5 394.524 287.233  25
  14   1   6 382.539 296.433  25
 -14  -1  -7 73.5768 190.754  15
 -14  -1  -7-47.9514 187.256  19
 -14  -1  -8 1254.84 422.160  19
 -14  -1  -9 673.955 338.668  19
 -14  -1 -10 457.061 258.993  19
 -14  -2  -2 783.257 286.702  15
 -14  -2  -3 80.1676 180.979  15
 -14  -2  -4 596.380 317.830  15
 -14  -2  -5 781.201 347.232  15
 -14  -2  -6 118.022 222.500  15
 -14  -2  -7 827.643 343.543  15
 -14  -2  -7 615.683 306.219  19
 -14  -2  -8 588.797 282.531  15
 -14  -2  -8 445.772 292.526  19
 -14  -2  -9-92.1953 219.909  19
 -14  -2 -10 924.824 336.979  19
 -14  -3  -2 74.0618 168.548  15
 -14  -3  -3 1203.68 371.779  15
 -14  -3  -4 784.895 336.388  15
 -14  -3  -5 89.0876 180.447  15
 -14  -3  -6 1453.86 426.375  15
 -14  -3  -7 461.300 293.975  15
 -14  -3  -7 8.10252 194.336  19
 -14  -3  -8-212.881 185.551  19
 -14  -3  -9 729.758 304.408  19
 -14  -3 -10-160.939 204.134  19
 -14  -4  -3 628.303 272.873  15
 -14  -4  -4 98.4390 175.218  15
 -14  -4  -5 1287.14 398.244  15
 -14  -4  -6 181.366 182.122  15
 -14  -4  -7 349.510 187.494  15
 -14  -4  -8 1414.97 375.610  19
 -14  -4  -9-116.301 195.016  19
 -14  -5  -4 479.360 262.577  15
 -14  -5  -5-317.981 241.555  15
 -14  -5  -6 729.922 308.115  15
   0   0   0    0.00    0.00   0
TITL GKL074 in P-1 
REM P-1 (#2 in standard setting)
CELL 1.54184  11.996863  13.398139  13.969543  81.3752  70.6688  85.8842
ZERR    2.00   0.001663   0.001873   0.001426   0.0099   0.0108   0.0113
LATT  1
SFAC C H N O Cl Ru
UNIT 84.00 72.00 12.00 16.00 2.00 2.00
TREF
HKLF 4
END
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
Os1 Os 0.58614(4) 0.21461(4) 0.18936(3) 0.0819(3) Uani 1 1 d . .
Cl1 Cl 0.2417(3) 0.1942(3) 0.7854(3) 0.1058(9) Uani 1 1 d . .
Cl2 Cl 0.1342(4) 0.4307(4) 0.1072(4) 0.1405(17) Uani 1 1 d . .
N7 N 0.9389(10) 0.2493(11) 0.0151(10) 0.118(4) Uani 1 1 d . .
H7 H 1.0004 0.2860 -0.0037 0.142 Uiso 1 1 calc R U
N4 N 0.5419(9) 0.2743(9) 0.0635(7) 0.091(3) Uani 1 1 d . .
O3 O 0.3577(11) 0.2284(14) 0.7360(10) 0.173(6) Uani 1 1 d . .
C26 C 0.9314(12) 0.1552(18) -0.0147(13) 0.145(7) Uani 1 1 d . .
H26 H 0.9919 0.1216 -0.0600 0.173 Uiso 1 1 calc R U
C18 C 0.4583(18) 0.3445(13) -0.1008(14) 0.119(5) Uani 1 1 d . .
H18 H 0.4296 0.3712 -0.1537 0.143 Uiso 1 1 calc R U
N3 N 0.5063(7) 0.0982(7) 0.1693(7) 0.083(2) Uani 1 1 d . .
C14 C 0.3693(11) 0.0484(11) 0.0845(11) 0.101(4) Uani 1 1 d . .
H14 H 0.3266 0.0651 0.0394 0.121 Uiso 1 1 calc R U
N6 N 0.7578(8) 0.1968(9) 0.0912(6) 0.093(3) Uani 1 1 d . .
C13 C 0.3647(13) -0.0436(14) 0.1395(12) 0.112(4) Uani 1 1 d . .
H13 H 0.3154 -0.0905 0.1326 0.135 Uiso 1 1 calc R U
N1 N 0.6166(7) 0.1489(8) 0.3199(7) 0.082(2) Uani 1 1 d . .
N5 N 0.6683(8) 0.3370(7) 0.1944(7) 0.082(2) Uani 1 1 d . .
N2 N 0.4345(10) 0.2495(11) 0.3004(9) 0.123(2) Uani 1 1 d . .
N8 N 0.8279(11) 0.4350(10) 0.1506(10) 0.113(3) Uani 1 1 d . .
H8 H 0.8989 0.4554 0.1200 0.135 Uiso 1 1 calc R U
O4 O 0.2345(13) 0.1316(14) 0.8767(12) 0.203(7) Uani 1 1 d . .
O8 O 0.2505(13) 0.4509(16) 0.0865(15) 0.203(7) Uani 1 1 d . .
C25 C 0.8236(11) 0.1231(11) 0.0330(9) 0.103(4) Uani 1 1 d . .
H25 H 0.7955 0.0616 0.0288 0.123 Uiso 1 1 calc R U
O6 O 0.0610(13) 0.5210(12) 0.0922(13) 0.187(6) Uani 1 1 d . .
C12 C 0.4290(13) -0.0732(11) 0.2064(11) 0.108(4) Uani 1 1 d . .
H12 H 0.4268 -0.1383 0.2411 0.129 Uiso 1 1 calc R U
C24 C 0.8328(10) 0.2704(11) 0.0777(9) 0.094(3) Uani 1 1 d . .
C10 C 0.3399(11) 0.3044(13) 0.2854(11) 0.123(2) Uani 1 1 d . .
H10 H 0.3406 0.3249 0.2186 0.147 Uiso 1 1 calc R U
C4 C 0.5536(14) 0.1246(14) 0.5024(11) 0.120(5) Uani 1 1 d . .
H4 H 0.4947 0.1320 0.5641 0.144 Uiso 1 1 calc R U
C15 C 0.4432(10) 0.1181(10) 0.0995(10) 0.094(3) Uani 1 1 d . .
C20 C 0.5739(14) 0.3647(11) 0.0038(10) 0.108(4) Uani 1 1 d . .
H20 H 0.6230 0.4062 0.0189 0.129 Uiso 1 1 calc R U
C17 C 0.4227(14) 0.2525(14) -0.0450(12) 0.118(5) Uani 1 1 d . .
H17 H 0.3725 0.2137 -0.0620 0.141 Uiso 1 1 calc R U
C19 C 0.5354(18) 0.3948(13) -0.0768(13) 0.124(5) Uani 1 1 d . .
H19 H 0.5645 0.4545 -0.1184 0.149 Uiso 1 1 calc R U
C21 C 0.6442(13) 0.4234(11) 0.2464(10) 0.101(4) Uani 1 1 d . .
H21 H 0.5718 0.4388 0.2933 0.121 Uiso 1 1 calc R U
C23 C 0.7847(10) 0.3482(10) 0.1371(9) 0.089(3) Uani 1 1 d . .
C11 C 0.4954(12) 0.0003(10) 0.2171(10) 0.100(4) Uani 1 1 d . .
H11 H 0.5382 -0.0180 0.2619 0.120 Uiso 1 1 calc R U
C22 C 0.7460(15) 0.4824(13) 0.2167(13) 0.116(5) Uani 1 1 d . .
H22 H 0.7532 0.5426 0.2394 0.139 Uiso 1 1 calc R U
C1 C 0.7163(10) 0.0946(11) 0.3251(9) 0.095(4) Uani 1 1 d . .
H1 H 0.7742 0.0836 0.2639 0.114 Uiso 1 1 calc R U
C16 C 0.4629(10) 0.2172(11) 0.0380(9) 0.095(3) Uani 1 1 d . .
C6 C 0.4294(11) 0.2193(11) 0.4009(11) 0.123(2) Uani 1 1 d . .
C3 C 0.6555(17) 0.0784(17) 0.5040(10) 0.141(8) Uani 1 1 d . .
H3 H 0.6720 0.0614 0.5650 0.169 Uiso 1 1 calc R U
C5 C 0.5335(12) 0.1608(13) 0.4143(8) 0.108(4) Uani 1 1 d . .
C2 C 0.7354(14) 0.0568(16) 0.4121(13) 0.135(6) Uani 1 1 d . .
H2 H 0.8018 0.0161 0.4111 0.162 Uiso 1 1 calc R U
O5 O 0.0795(19) 0.3865(19) 0.2062(13) 0.262(11) Uani 1 1 d . .
O7 O 0.115(2) 0.3700(19) 0.0405(17) 0.283(13) Uani 1 1 d . .
O1 O 0.1709(17) 0.2748(12) 0.816(2) 0.304(15) Uani 1 1 d . .
O2 O 0.196(3) 0.150(2) 0.7268(16) 0.306(15) Uani 1 1 d . .
C7 C 0.3358(11) 0.2439(12) 0.4797(11) 0.123(2) Uani 1 1 d . .
H7A H 0.3342 0.2229 0.5467 0.147 Uiso 1 1 calc R U
C9 C 0.2450(12) 0.3306(14) 0.3631(11) 0.123(2) Uani 1 1 d . .
H9 H 0.1839 0.3688 0.3475 0.147 Uiso 1 1 calc R U
C8 C 0.2363(12) 0.3041(13) 0.4596(11) 0.123(2) Uani 1 1 d . .
H8A H 0.1708 0.3223 0.5125 0.147 Uiso 1 1 calc R U
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Os Os -4.9801 6.2216 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
N3 Os1 N5 174.1(3)
N3 Os1 N4 79.4(4)
N5 Os1 N4 95.0(4)
N3 Os1 N1 96.7(4)
N5 Os1 N1 89.0(4)
N4 Os1 N1 175.0(3)
N3 Os1 N2 89.4(5)
N5 Os1 N2 93.5(5)
N4 Os1 N2 99.2(4)
N1 Os1 N2 77.6(4)
N3 Os1 N6 101.9(4)
N5 Os1 N6 75.7(4)
N4 Os1 N6 87.4(4)
N1 Os1 N6 96.5(3)
N2 Os1 N6 167.9(4)
O2 Cl1 O1 107.6(19)
O2 Cl1 O4 111.3(14)
O1 Cl1 O4 104.1(14)
O2 Cl1 O3 114.6(14)
O1 Cl1 O3 108.2(12)
O4 Cl1 O3 110.5(9)
O8 Cl2 O5 113.9(13)
O8 Cl2 O7 113.5(15)
O5 Cl2 O7 107.9(15)
O8 Cl2 O6 113.6(12)
O5 Cl2 O6 105.3(13)
O7 Cl2 O6 101.5(14)
C24 N7 C26 106.4(12)
C24 N7 H7 126.8
C26 N7 H7 126.8
C20 N4 C16 116.0(11)
C20 N4 Os1 128.0(10)
C16 N4 Os1 115.9(8)
C25 C26 N7 107.7(14)
C25 C26 H26 126.1
N7 C26 H26 126.1
C19 C18 C17 118.0(14)
C19 C18 H18 121.0
C17 C18 H18 121.0
C11 N3 C15 112.5(11)
C11 N3 Os1 130.9(9)
C15 N3 Os1 116.4(8)
C13 C14 C15 115.8(14)
C13 C14 H14 122.1
C15 C14 H14 122.1
C24 N6 C25 105.6(10)
C24 N6 Os1 117.3(9)
C25 N6 Os1 137.1(10)
C14 C13 C12 124.4(14)
C14 C13 H13 117.8
C12 C13 H13 117.8
C1 N1 C5 114.6(10)
C1 N1 Os1 125.8(7)
C5 N1 Os1 119.6(8)
C23 N5 C21 102.2(10)
C23 N5 Os1 118.9(9)
C21 N5 Os1 138.9(9)
C10 N2 C6 116.7(11)
C10 N2 Os1 126.3(10)
C6 N2 Os1 116.9(9)
C22 N8 C23 110.3(13)
C22 N8 H8 124.9
C23 N8 H8 124.9
C26 C25 N6 108.9(15)
C26 C25 H25 125.6
N6 C25 H25 125.6
C11 C12 C13 115.1(14)
C11 C12 H12 122.5
C13 C12 H12 122.5
N7 C24 N6 111.4(13)
N7 C24 C23 134.7(14)
N6 C24 C23 113.8(10)
C9 C10 N2 123.2(14)
C9 C10 H10 118.4
N2 C10 H10 118.4
C3 C4 C5 122.1(14)
C3 C4 H4 118.9
C5 C4 H4 118.9
N3 C15 C14 124.5(13)
N3 C15 C16 114.7(11)
C14 C15 C16 120.8(13)
C19 C20 N4 121.0(15)
C19 C20 H20 119.5
N4 C20 H20 119.5
C18 C17 C16 119.3(15)
C18 C17 H17 120.3
C16 C17 H17 120.3
C18 C19 C20 124.3(17)
C18 C19 H19 117.9
C20 C19 H19 117.9
C22 C21 N5 110.2(13)
C22 C21 H21 124.9
N5 C21 H21 124.9
N5 C23 N8 111.4(12)
N5 C23 C24 114.2(11)
N8 C23 C24 134.3(12)
C12 C11 N3 127.5(14)
C12 C11 H11 116.2
N3 C11 H11 116.2
N8 C22 C21 105.8(14)
N8 C22 H22 127.1
C21 C22 H22 127.1
C2 C1 N1 124.1(12)
C2 C1 H1 118.0
N1 C1 H1 118.0
C17 C16 N4 121.1(14)
C17 C16 C15 126.8(14)
N4 C16 C15 111.8(10)
C7 C6 N2 121.3(13)
C7 C6 C5 123.4(13)
N2 C6 C5 115.2(10)
C4 C3 C2 117.8(13)
C4 C3 H3 121.1
C2 C3 H3 121.1
C4 C5 N1 121.5(13)
C4 C5 C6 127.9(13)
N1 C5 C6 110.6(10)
C1 C2 C3 119.3(14)
C1 C2 H2 120.3
C3 C2 H2 120.3
C6 C7 C8 120.0(14)
C6 C7 H7A 120.0
C8 C7 H7A 120.0
C8 C9 C10 122.3(14)
C8 C9 H9 118.8
C10 C9 H9 118.8
C9 C8 C7 116.4(12)
C9 C8 H8A 121.8
C7 C8 H8A 121.8
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Os1 N3 1.988(10)
Os1 N5 1.995(10)
Os1 N4 2.037(10)
Os1 N1 2.037(9)
Os1 N2 2.040(10)
Os1 N6 2.082(8)
Cl1 O2 1.340(15)
Cl1 O1 1.355(16)
Cl1 O4 1.399(14)
Cl1 O3 1.408(12)
Cl2 O8 1.367(14)
Cl2 O5 1.381(15)
Cl2 O7 1.405(18)
Cl2 O6 1.474(14)
N7 C24 1.324(16)
N7 C26 1.40(2)
N7 H7 0.8600
N4 C20 1.365(16)
N4 C16 1.420(16)
C26 C25 1.313(19)
C26 H26 0.9300
C18 C19 1.34(2)
C18 C17 1.37(2)
C18 H18 0.9300
N3 C11 1.373(16)
N3 C15 1.406(16)
C14 C13 1.35(2)
C14 C15 1.415(17)
C14 H14 0.9300
N6 C24 1.333(17)
N6 C25 1.401(16)
C13 C12 1.40(2)
C13 H13 0.9300
N1 C1 1.372(14)
N1 C5 1.388(15)
N5 C23 1.366(15)
N5 C21 1.419(17)
N2 C10 1.366(17)
N2 C6 1.383(18)
N8 C22 1.31(2)
N8 C23 1.369(17)
N8 H8 0.8600
C25 H25 0.9300
C12 C11 1.364(19)
C12 H12 0.9300
C24 C23 1.401(18)
C10 C9 1.354(17)
C10 H10 0.9300
C4 C3 1.34(2)
C4 C5 1.345(18)
C4 H4 0.9300
C15 C16 1.458(19)
C20 C19 1.352(19)
C20 H20 0.9300
C17 C16 1.405(19)
C17 H17 0.9300
C19 H19 0.9300
C21 C22 1.41(2)
C21 H21 0.9300
C11 H11 0.9300
C22 H22 0.9300
C1 C2 1.331(18)
C1 H1 0.9300
C6 C7 1.349(17)
C6 C5 1.476(19)
C3 C2 1.38(2)
C3 H3 0.9300
C2 H2 0.9300
C7 C8 1.473(18)
C7 H7A 0.9300
C9 C8 1.31(2)
C9 H9 0.9300
C8 H8A 0.9300
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C24 N7 C26 C25 -2(2)
C15 C14 C13 C12 -2(2)
N7 C26 C25 N6 2(2)
C24 N6 C25 C26 -2.0(16)
Os1 N6 C25 C26 -179.7(11)
C14 C13 C12 C11 3(2)
C26 N7 C24 N6 0.5(17)
C26 N7 C24 C23 175.4(15)
C25 N6 C24 N7 0.8(14)
Os1 N6 C24 N7 179.1(9)
C25 N6 C24 C23 -175.2(11)
Os1 N6 C24 C23 3.0(14)
C6 N2 C10 C9 1(2)
Os1 N2 C10 C9 -175.4(13)
C11 N3 C15 C14 4.4(16)
Os1 N3 C15 C14 -171.9(9)
C11 N3 C15 C16 -173.1(10)
Os1 N3 C15 C16 10.6(12)
C13 C14 C15 N3 -2.5(19)
C13 C14 C15 C16 174.9(12)
C16 N4 C20 C19 -2(2)
Os1 N4 C20 C19 -178.8(12)
C19 C18 C17 C16 4(3)
C17 C18 C19 C20 -5(3)
N4 C20 C19 C18 5(3)
C23 N5 C21 C22 1.0(14)
Os1 N5 C21 C22 177.8(9)
C21 N5 C23 N8 -1.4(14)
Os1 N5 C23 N8 -179.0(8)
C21 N5 C23 C24 179.2(11)
Os1 N5 C23 C24 1.6(14)
C22 N8 C23 N5 1.3(17)
C22 N8 C23 C24 -179.4(15)
N7 C24 C23 N5 -177.8(14)
N6 C24 C23 N5 -2.9(16)
N7 C24 C23 N8 3(3)
N6 C24 C23 N8 177.8(14)
C13 C12 C11 N3 -1(2)
C15 N3 C11 C12 -2.8(18)
Os1 N3 C11 C12 172.8(10)
C23 N8 C22 C21 -0.6(17)
N5 C21 C22 N8 -0.3(17)
C5 N1 C1 C2 -1(2)
Os1 N1 C1 C2 176.7(14)
C18 C17 C16 N4 -2(2)
C18 C17 C16 C15 -174.0(14)
C20 N4 C16 C17 1.0(18)
Os1 N4 C16 C17 177.7(10)
C20 N4 C16 C15 174.5(11)
Os1 N4 C16 C15 -8.8(13)
N3 C15 C16 C17 172.1(12)
C14 C15 C16 C17 -5(2)
N3 C15 C16 N4 -1.0(14)
C14 C15 C16 N4 -178.6(11)
C10 N2 C6 C7 -0.5(11)
Os1 N2 C6 C7 176.1(10)
C10 N2 C6 C5 -179.5(15)
Os1 N2 C6 C5 -2.9(13)
C5 C4 C3 C2 -8(3)
C3 C4 C5 N1 2(3)
C3 C4 C5 C6 -175.3(19)
C1 N1 C5 C4 2(2)
Os1 N1 C5 C4 -175.4(13)
C1 N1 C5 C6 -179.6(12)
Os1 N1 C5 C6 2.6(16)
C7 C6 C5 C4 -1(2)
N2 C6 C5 C4 178.1(16)
C7 C6 C5 N1 -178.7(11)
N2 C6 C5 N1 0.3(17)
N1 C1 C2 C3 -5(3)
C4 C3 C2 C1 9(3)
N2 C6 C7 C8 0.0(11)
C5 C6 C7 C8 179.0(16)
N2 C10 C9 C8 -1(3)
C10 C9 C8 C7 0(3)
C6 C7 C8 C9 0.2(19)
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 -0.023 -0.022 0.500 834 189 ' '
