#------------------------------------------------------------------------------
#$Date: 2016-02-13 14:50:18 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176428 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/64/7036481.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7036481
loop_
_publ_author_name
'Chen, Zhao'
'Liang, Jinhua'
'Nie, Yuting'
'Xu, Xuqingfeng'
'Yu, Guang-Ao'
'Yin, Jun'
'Liu, Sheng Hua'
_publ_section_title
;
 A novel carbazole-based gold(i) complex with interesting solid-state,
 multistimuli-responsive characteristics.
;
_journal_issue                   40
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              17473
_journal_page_last               17477
_journal_paper_doi               10.1039/c5dt02035b
_journal_volume                  44
_journal_year                    2015
_chemical_formula_sum            'C32 H26 Au Cl2 F5 N2 O'
_chemical_formula_weight         817.41
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-08-27 deposited with the CCDC.
2015-09-10 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 114.175(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   18.712(4)
_cell_length_b                   8.2180(16)
_cell_length_c                   21.103(4)
_cell_measurement_reflns_used    9891
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      31.92
_cell_measurement_theta_min      2.39
_cell_volume                     2960.5(10)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0335
_diffrn_reflns_av_sigmaI/netI    0.0314
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            28688
_diffrn_reflns_theta_full        30.00
_diffrn_reflns_theta_max         30.00
_diffrn_reflns_theta_min         1.19
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    5.211
_exptl_absorpt_correction_T_max  0.6238
_exptl_absorpt_correction_T_min  0.5736
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.834
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             1592
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_refine_diff_density_max         2.061
_refine_diff_density_min         -1.887
_refine_diff_density_rms         0.121
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.097
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     388
_refine_ls_number_reflns         8617
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.097
_refine_ls_R_factor_all          0.0323
_refine_ls_R_factor_gt           0.0260
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0387P)²+1.5484P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0681
_refine_ls_wR_factor_ref         0.0710
_reflns_number_gt                7662
_reflns_number_total             8617
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5dt02035b2.cif
_cod_data_source_block           e131103h_work_mo_131103h_0m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 7036480--7036481.cif.
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7036481
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Au1 Au 0.518196(6) -0.300400(12) 0.544130(5) 0.01877(4) Uani 1 1 d .
C1 C 1.14154(14) 0.6242(3) 0.26677(12) 0.0151(4) Uani 1 1 d .
C2 C 1.21414(15) 0.5993(3) 0.32182(13) 0.0198(5) Uani 1 1 d .
H2 H 1.2250 0.6395 0.3671 0.024 Uiso 1 1 calc R
C3 C 1.27004(16) 0.5134(4) 0.30783(14) 0.0234(5) Uani 1 1 d .
H3 H 1.3201 0.4945 0.3443 0.028 Uiso 1 1 calc R
C4 C 1.25441(17) 0.4540(3) 0.24131(15) 0.0241(5) Uani 1 1 d .
H4 H 1.2940 0.3967 0.2333 0.029 Uiso 1 1 calc R
C5 C 1.18206(17) 0.4777(3) 0.18710(13) 0.0216(5) Uani 1 1 d .
H5 H 1.1715 0.4364 0.1421 0.026 Uiso 1 1 calc R
C6 C 1.12470(15) 0.5636(3) 0.19981(12) 0.0173(5) Uani 1 1 d .
C7 C 1.04512(15) 0.6119(3) 0.15754(13) 0.0184(5) Uani 1 1 d .
C8 C 0.99488(18) 0.5866(4) 0.08790(13) 0.0271(6) Uani 1 1 d .
H8 H 1.0121 0.5280 0.0579 0.033 Uiso 1 1 calc R
C9 C 0.91935(19) 0.6488(4) 0.06336(15) 0.0322(7) Uani 1 1 d .
H9 H 0.8848 0.6332 0.0160 0.039 Uiso 1 1 calc R
C10 C 0.89354(18) 0.7337(4) 0.10717(16) 0.0288(6) Uani 1 1 d .
H10 H 0.8413 0.7735 0.0892 0.035 Uiso 1 1 calc R
C11 C 0.94203(16) 0.7616(3) 0.17628(15) 0.0221(5) Uani 1 1 d .
H11 H 0.9242 0.8205 0.2058 0.027 Uiso 1 1 calc R
C12 C 1.01807(15) 0.6997(3) 0.20083(13) 0.0171(5) Uani 1 1 d .
C13 C 1.07568(16) 0.7961(3) 0.32599(13) 0.0173(5) Uani 1 1 d .
H13A H 1.0377 0.8866 0.3085 0.021 Uiso 1 1 calc R
H13B H 1.1280 0.8444 0.3525 0.021 Uiso 1 1 calc R
C14 C 1.05364(15) 0.6925(3) 0.37496(13) 0.0174(5) Uani 1 1 d .
H14A H 1.0619 0.7569 0.4170 0.021 Uiso 1 1 calc R
H14B H 1.0889 0.5970 0.3896 0.021 Uiso 1 1 calc R
C15 C 0.96899(14) 0.6334(3) 0.34248(13) 0.0166(4) Uani 1 1 d .
H15A H 0.9617 0.5627 0.3023 0.020 Uiso 1 1 calc R
H15B H 0.9339 0.7285 0.3249 0.020 Uiso 1 1 calc R
C16 C 0.94536(15) 0.5393(3) 0.39321(13) 0.0176(5) Uani 1 1 d .
H16A H 0.9810 0.4454 0.4118 0.021 Uiso 1 1 calc R
H16B H 0.9508 0.6107 0.4327 0.021 Uiso 1 1 calc R
C17 C 0.86115(14) 0.4784(3) 0.35819(13) 0.0180(5) Uani 1 1 d .
H17A H 0.8254 0.5730 0.3424 0.022 Uiso 1 1 calc R
H17B H 0.8550 0.4137 0.3167 0.022 Uiso 1 1 calc R
C18 C 0.83799(14) 0.3756(3) 0.40557(13) 0.0188(5) Uani 1 1 d .
H18A H 0.8734 0.2808 0.4223 0.023 Uiso 1 1 calc R
H18B H 0.8411 0.4399 0.4463 0.023 Uiso 1 1 calc R
C19 C 0.72589(15) 0.2192(3) 0.39698(13) 0.0158(5) Uani 1 1 d .
C20 C 0.76136(16) 0.1741(4) 0.46675(14) 0.0224(5) Uani 1 1 d .
H20 H 0.8123 0.2127 0.4953 0.027 Uiso 1 1 calc R
C21 C 0.72212(16) 0.0727(4) 0.49433(13) 0.0233(5) Uani 1 1 d .
H21 H 0.7458 0.0419 0.5419 0.028 Uiso 1 1 calc R
C22 C 0.64819(15) 0.0170(3) 0.45197(13) 0.0182(5) Uani 1 1 d .
C23 C 0.61287(15) 0.0579(3) 0.38173(13) 0.0190(5) Uani 1 1 d .
H23 H 0.5624 0.0169 0.3531 0.023 Uiso 1 1 calc R
C24 C 0.65193(15) 0.1584(3) 0.35450(13) 0.0181(5) Uani 1 1 d .
H24 H 0.6286 0.1866 0.3067 0.022 Uiso 1 1 calc R
C25 C 0.57644(17) -0.1628(4) 0.50527(15) 0.0225(5) Uani 1 1 d .
C26 C 0.45371(14) -0.4360(3) 0.58138(12) 0.0153(4) Uani 1 1 d .
C27 C 0.37683(15) -0.4760(3) 0.53949(12) 0.0184(5) Uani 1 1 d .
C28 C 0.32954(15) -0.5663(4) 0.56166(14) 0.0222(5) Uani 1 1 d .
C29 C 0.35832(16) -0.6204(3) 0.62903(15) 0.0217(5) Uani 1 1 d .
C30 C 0.43423(16) -0.5840(4) 0.67308(13) 0.0223(5) Uani 1 1 d .
C31 C 0.47970(14) -0.4944(3) 0.64882(12) 0.0190(5) Uani 1 1 d .
C32 C 0.6756(3) 0.0231(9) 0.7028(2) 0.0767(19) Uani 1 1 d .
H32A H 0.6545 -0.0674 0.7210 0.092 Uiso 1 1 calc R
H32B H 0.7046 0.0967 0.7421 0.092 Uiso 1 1 calc R
Cl1 Cl 0.59784(6) 0.12925(12) 0.64181(5) 0.0493(2) Uani 1 1 d .
Cl2 Cl 0.74135(5) -0.05680(10) 0.67090(4) 0.03611(17) Uani 1 1 d .
F1 F 0.34563(10) -0.4258(2) 0.47278(8) 0.0297(4) Uani 1 1 d .
F2 F 0.25538(10) -0.6016(3) 0.51817(10) 0.0361(4) Uani 1 1 d .
F3 F 0.31227(12) -0.7059(2) 0.65169(11) 0.0353(4) Uani 1 1 d .
F4 F 0.46199(12) -0.6371(3) 0.73896(9) 0.0388(5) Uani 1 1 d .
F5 F 0.55358(9) -0.4622(2) 0.69483(8) 0.0313(4) Uani 1 1 d .
N1 N 1.07741(13) 0.7073(2) 0.26692(11) 0.0152(4) Uani 1 1 d .
N2 N 0.60837(13) -0.0827(3) 0.48069(11) 0.0202(4) Uani 1 1 d .
O1 O 0.75867(11) 0.3220(2) 0.36604(10) 0.0189(4) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
C25 Au1 C26 177.32(11)
N1 C1 C2 128.4(2)
N1 C1 C6 109.9(2)
C2 C1 C6 121.7(2)
C3 C2 C1 117.3(2)
C3 C2 H2 121.4
C1 C2 H2 121.4
C2 C3 C4 121.6(2)
C2 C3 H3 119.2
C4 C3 H3 119.2
C5 C4 C3 120.8(2)
C5 C4 H4 119.6
C3 C4 H4 119.6
C4 C5 C6 118.7(2)
C4 C5 H5 120.6
C6 C5 H5 120.6
C5 C6 C1 119.8(2)
C5 C6 C7 134.3(2)
C1 C6 C7 105.9(2)
C8 C7 C12 119.5(3)
C8 C7 C6 133.5(3)
C12 C7 C6 107.1(2)
C9 C8 C7 118.7(3)
C9 C8 H8 120.6
C7 C8 H8 120.6
C8 C9 C10 120.9(3)
C8 C9 H9 119.6
C10 C9 H9 119.5
C11 C10 C9 121.7(3)
C11 C10 H10 119.1
C9 C10 H10 119.1
C10 C11 C12 117.3(3)
C10 C11 H11 121.3
C12 C11 H11 121.3
N1 C12 C11 129.3(2)
N1 C12 C7 108.9(2)
C11 C12 C7 121.8(2)
N1 C13 C14 114.1(2)
N1 C13 H13A 108.7
C14 C13 H13A 108.7
N1 C13 H13B 108.7
C14 C13 H13B 108.7
H13A C13 H13B 107.6
C13 C14 C15 113.2(2)
C13 C14 H14A 108.9
C15 C14 H14A 108.9
C13 C14 H14B 108.9
C15 C14 H14B 108.9
H14A C14 H14B 107.8
C14 C15 C16 113.1(2)
C14 C15 H15A 109.0
C16 C15 H15A 109.0
C14 C15 H15B 109.0
C16 C15 H15B 109.0
H15A C15 H15B 107.8
C17 C16 C15 111.4(2)
C17 C16 H16A 109.3
C15 C16 H16A 109.3
C17 C16 H16B 109.3
C15 C16 H16B 109.3
H16A C16 H16B 108.0
C18 C17 C16 112.6(2)
C18 C17 H17A 109.1
C16 C17 H17A 109.1
C18 C17 H17B 109.1
C16 C17 H17B 109.1
H17A C17 H17B 107.8
O1 C18 C17 107.22(19)
O1 C18 H18A 110.3
C17 C18 H18A 110.3
O1 C18 H18B 110.3
C17 C18 H18B 110.3
H18A C18 H18B 108.5
O1 C19 C20 124.0(2)
O1 C19 C24 115.9(2)
C20 C19 C24 120.0(2)
C21 C20 C19 119.9(2)
C21 C20 H20 120.1
C19 C20 H20 120.1
C22 C21 C20 119.3(2)
C22 C21 H21 120.3
C20 C21 H21 120.3
C21 C22 C23 121.4(2)
C21 C22 N2 118.9(2)
C23 C22 N2 119.8(2)
C24 C23 C22 119.2(2)
C24 C23 H23 120.4
C22 C23 H23 120.4
C23 C24 C19 120.2(2)
C23 C24 H24 119.9
C19 C24 H24 119.9
N2 C25 Au1 177.9(3)
C27 C26 C31 114.1(2)
C27 C26 Au1 120.79(18)
C31 C26 Au1 125.08(18)
F1 C27 C28 117.1(2)
F1 C27 C26 119.1(2)
C28 C27 C26 123.8(2)
F2 C28 C29 119.6(3)
F2 C28 C27 120.8(2)
C29 C28 C27 119.6(2)
F3 C29 C28 120.1(3)
F3 C29 C30 120.6(3)
C28 C29 C30 119.2(2)
F4 C30 C31 121.6(3)
F4 C30 C29 119.0(2)
C31 C30 C29 119.4(2)
F5 C31 C30 116.4(2)
F5 C31 C26 119.7(2)
C30 C31 C26 123.9(2)
Cl1 C32 Cl2 114.3(2)
Cl1 C32 H32A 108.7
Cl2 C32 H32A 108.7
Cl1 C32 H32B 108.7
Cl2 C32 H32B 108.7
H32A C32 H32B 107.6
C1 N1 C12 108.3(2)
C1 N1 C13 125.0(2)
C12 N1 C13 126.6(2)
C25 N2 C22 178.8(3)
C19 O1 C18 118.20(19)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Au1 C25 1.967(3)
Au1 C26 2.023(2)
C1 N1 1.382(3)
C1 C2 1.394(3)
C1 C6 1.407(3)
C2 C3 1.390(4)
C2 H2 0.9500
C3 C4 1.399(4)
C3 H3 0.9500
C4 C5 1.382(4)
C4 H4 0.9500
C5 C6 1.399(4)
C5 H5 0.9500
C6 C7 1.443(4)
C7 C8 1.398(3)
C7 C12 1.411(4)
C8 C9 1.388(5)
C8 H8 0.9500
C9 C10 1.393(5)
C9 H9 0.9500
C10 C11 1.385(4)
C10 H10 0.9500
C11 C12 1.396(4)
C11 H11 0.9500
C12 N1 1.383(3)
C13 N1 1.456(3)
C13 C14 1.521(4)
C13 H13A 0.9900
C13 H13B 0.9900
C14 C15 1.525(4)
C14 H14A 0.9900
C14 H14B 0.9900
C15 C16 1.526(3)
C15 H15A 0.9900
C15 H15B 0.9900
C16 C17 1.525(3)
C16 H16A 0.9900
C16 H16B 0.9900
C17 C18 1.502(3)
C17 H17A 0.9900
C17 H17B 0.9900
C18 O1 1.442(3)
C18 H18A 0.9900
C18 H18B 0.9900
C19 O1 1.358(3)
C19 C20 1.395(4)
C19 C24 1.397(3)
C20 C21 1.386(4)
C20 H20 0.9500
C21 C22 1.382(4)
C21 H21 0.9500
C22 C23 1.395(3)
C22 N2 1.401(3)
C23 C24 1.375(4)
C23 H23 0.9500
C24 H24 0.9500
C25 N2 1.146(4)
C26 C27 1.385(3)
C26 C31 1.388(3)
C27 F1 1.349(3)
C27 C28 1.375(4)
C28 F2 1.345(3)
C28 C29 1.372(4)
C29 F3 1.343(3)
C29 C30 1.375(4)
C30 F4 1.342(3)
C30 C31 1.373(4)
C31 F5 1.351(3)
C32 Cl1 1.732(4)
C32 Cl2 1.754(5)
C32 H32A 0.9900
C32 H32B 0.9900
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
N1 C1 C2 C3 -178.7(3)
C6 C1 C2 C3 0.8(4)
C1 C2 C3 C4 0.0(4)
C2 C3 C4 C5 -0.6(4)
C3 C4 C5 C6 0.5(4)
C4 C5 C6 C1 0.2(4)
C4 C5 C6 C7 179.5(3)
N1 C1 C6 C5 178.7(2)
C2 C1 C6 C5 -0.9(4)
N1 C1 C6 C7 -0.7(3)
C2 C1 C6 C7 179.7(2)
C5 C6 C7 C8 2.0(5)
C1 C6 C7 C8 -178.7(3)
C5 C6 C7 C12 -179.0(3)
C1 C6 C7 C12 0.3(3)
C12 C7 C8 C9 -0.1(4)
C6 C7 C8 C9 178.7(3)
C7 C8 C9 C10 -0.5(4)
C8 C9 C10 C11 1.0(5)
C9 C10 C11 C12 -0.6(4)
C10 C11 C12 N1 -178.8(3)
C10 C11 C12 C7 -0.1(4)
C8 C7 C12 N1 179.4(2)
C6 C7 C12 N1 0.3(3)
C8 C7 C12 C11 0.4(4)
C6 C7 C12 C11 -178.7(2)
N1 C13 C14 C15 -67.4(3)
C13 C14 C15 C16 -176.1(2)
C14 C15 C16 C17 -178.4(2)
C15 C16 C17 C18 176.1(2)
C16 C17 C18 O1 -178.3(2)
O1 C19 C20 C21 177.7(3)
C24 C19 C20 C21 -1.9(4)
C19 C20 C21 C22 0.3(4)
C20 C21 C22 C23 1.3(4)
C20 C21 C22 N2 -178.7(3)
C21 C22 C23 C24 -1.3(4)
N2 C22 C23 C24 178.7(2)
C22 C23 C24 C19 -0.4(4)
O1 C19 C24 C23 -177.7(2)
C20 C19 C24 C23 1.9(4)
C26 Au1 C25 N2 -36(8)
C25 Au1 C26 C27 35(2)
C25 Au1 C26 C31 -144(2)
C31 C26 C27 F1 -179.8(2)
Au1 C26 C27 F1 1.2(3)
C31 C26 C27 C28 -0.3(4)
Au1 C26 C27 C28 -179.3(2)
F1 C27 C28 F2 -0.2(4)
C26 C27 C28 F2 -179.7(2)
F1 C27 C28 C29 -180.0(2)
C26 C27 C28 C29 0.6(4)
F2 C28 C29 F3 -1.1(4)
C27 C28 C29 F3 178.7(2)
F2 C28 C29 C30 179.9(3)
C27 C28 C29 C30 -0.3(4)
F3 C29 C30 F4 0.9(4)
C28 C29 C30 F4 179.9(3)
F3 C29 C30 C31 -179.1(2)
C28 C29 C30 C31 -0.1(4)
F4 C30 C31 F5 -0.3(4)
C29 C30 C31 F5 179.7(2)
F4 C30 C31 C26 -179.7(3)
C29 C30 C31 C26 0.3(4)
C27 C26 C31 F5 -179.5(2)
Au1 C26 C31 F5 -0.5(4)
C27 C26 C31 C30 -0.1(4)
Au1 C26 C31 C30 178.9(2)
C2 C1 N1 C12 -179.5(2)
C6 C1 N1 C12 0.9(3)
C2 C1 N1 C13 4.2(4)
C6 C1 N1 C13 -175.4(2)
C11 C12 N1 C1 178.1(3)
C7 C12 N1 C1 -0.7(3)
C11 C12 N1 C13 -5.7(4)
C7 C12 N1 C13 175.5(2)
C14 C13 N1 C1 -87.5(3)
C14 C13 N1 C12 96.8(3)
Au1 C25 N2 C22 146(11)
C21 C22 N2 C25 30(14)
C23 C22 N2 C25 -150(14)
C20 C19 O1 C18 6.4(4)
C24 C19 O1 C18 -174.0(2)
C17 C18 O1 C19 176.5(2)
