#------------------------------------------------------------------------------
#$Date: 2016-02-13 14:50:18 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176428 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/69/7036943.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7036943
loop_
_publ_author_name
'Gao, Feng'
'Yang, Feng-Lei'
'Zhu, Guang-Zhou'
'Zhao, Yue'
_publ_section_title
;
 Syntheses, structures, and magnetic properties of homodinuclear
 lanthanide complexes based on dinucleating Schiff base ligands.
;
_journal_issue                   46
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              20232
_journal_page_last               20241
_journal_paper_doi               10.1039/c5dt03580e
_journal_volume                  44
_journal_year                    2015
_chemical_formula_sum            'C68 H92 Co2 Dy2 N4 O22 P6'
_chemical_formula_weight         1946.14
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-05-26 deposited with the CCDC.
2015-10-28 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 103.965(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   16.545(2)
_cell_length_b                   15.0376(19)
_cell_length_c                   18.105(2)
_cell_measurement_reflns_used    9916
_cell_measurement_temperature    123(2)
_cell_measurement_theta_max      27.42
_cell_measurement_theta_min      2.32
_cell_volume                     4371.3(9)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      123(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker APEX II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0402
_diffrn_reflns_av_sigmaI/netI    0.0327
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            31435
_diffrn_reflns_theta_full        25.01
_diffrn_reflns_theta_max         25.01
_diffrn_reflns_theta_min         1.27
_exptl_absorpt_coefficient_mu    2.238
_exptl_absorpt_correction_T_max  0.6631
_exptl_absorpt_correction_T_min  0.5938
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS; Bruker, 2000'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.479
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1960
_exptl_crystal_size_max          0.26
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.20
_platon_squeeze_details
;
;
_refine_diff_density_max         1.085
_refine_diff_density_min         -1.093
_refine_diff_density_rms         0.101
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.124
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     481
_refine_ls_number_reflns         7676
_refine_ls_number_restraints     66
_refine_ls_restrained_S_all      1.121
_refine_ls_R_factor_all          0.0393
_refine_ls_R_factor_gt           0.0315
_refine_ls_shift/su_max          0.008
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0000P)²+14.0643P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0637
_refine_ls_wR_factor_ref         0.0660
_reflns_number_gt                6484
_reflns_number_total             7676
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5dt03580e2.cif
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 7036943--7036951.cif.
;
_cod_original_cell_volume        4371.4(10)
_cod_original_sg_symbol_H-M      'P2(1)/c  '
_cod_database_code               7036943
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.0161(3) 0.3799(4) 0.4369(3) 0.0235(19) Uani 0.647(12) 1 d PGU A 1
H1 H 0.0020 0.4282 0.4632 0.028 Uiso 0.647(12) 1 calc PR A 1
C2 C 0.0771(3) 0.3143(4) 0.4670(3) 0.0222(18) Uani 0.647(12) 1 d PGU A 1
H2 H 0.1099 0.3123 0.5165 0.027 Uiso 0.647(12) 1 calc PR A 1
C3 C 0.0791(3) 0.2524(4) 0.4081(4) 0.028(2) Uani 0.647(12) 1 d PGU A 1
H3 H 0.1135 0.2028 0.4124 0.034 Uiso 0.647(12) 1 calc PR A 1
C4 C 0.0194(4) 0.2798(4) 0.3416(3) 0.0289(18) Uani 0.647(12) 1 d PGU A 1
H4 H 0.0079 0.2511 0.2946 0.035 Uiso 0.647(12) 1 calc PR A 1
C5 C -0.0195(3) 0.3585(4) 0.3593(3) 0.026(2) Uani 0.647(12) 1 d PGU A 1
H5 H -0.0610 0.3904 0.3261 0.032 Uiso 0.647(12) 1 calc PR A 1
C6 C 0.3175(4) 0.2083(4) 0.3479(4) 0.0684(19) Uani 1 1 d . A .
H6A H 0.3543 0.2021 0.3983 0.082 Uiso 1 1 calc R . .
H6B H 0.3432 0.2494 0.3192 0.082 Uiso 1 1 calc R . .
C7 C 0.3076(5) 0.1228(4) 0.3105(5) 0.080(2) Uani 1 1 d . . .
H7A H 0.2824 0.0819 0.3390 0.120 Uiso 1 1 calc R . .
H7B H 0.3612 0.1006 0.3076 0.120 Uiso 1 1 calc R . .
H7C H 0.2727 0.1290 0.2601 0.120 Uiso 1 1 calc R . .
C8 C 0.3491(4) 0.3451(5) 0.5246(3) 0.0669(19) Uani 1 1 d . A .
H8A H 0.3451 0.4090 0.5301 0.080 Uiso 1 1 calc R . .
H8B H 0.3908 0.3345 0.4961 0.080 Uiso 1 1 calc R . .
C9 C 0.3800(4) 0.3095(5) 0.5982(4) 0.087 Uani 1 1 d . . .
H9A H 0.3365 0.3091 0.6249 0.130 Uiso 1 1 calc R . .
H9B H 0.4255 0.3454 0.6255 0.130 Uiso 1 1 calc R . .
H9C H 0.3991 0.2499 0.5941 0.130 Uiso 1 1 calc R . .
C10 C 0.1612(4) 0.3146(4) 0.1668(4) 0.0668(18) Uani 1 1 d . . .
H10A H 0.2145 0.3194 0.2035 0.080 Uiso 1 1 calc R . .
H10B H 0.1528 0.2520 0.1543 0.080 Uiso 1 1 calc R . .
C11 C 0.1696(4) 0.3572(4) 0.1016(4) 0.065 Uani 1 1 d . . .
H11A H 0.1200 0.3486 0.0619 0.098 Uiso 1 1 calc R . .
H11B H 0.2165 0.3329 0.0858 0.098 Uiso 1 1 calc R . .
H11C H 0.1782 0.4196 0.1116 0.098 Uiso 1 1 calc R . .
C12 C -0.0082(3) 0.5301(4) 0.1735(3) 0.046 Uani 1 1 d . . .
H12A H 0.0391 0.5701 0.1818 0.055 Uiso 1 1 calc R . .
H12B H -0.0548 0.5630 0.1835 0.055 Uiso 1 1 calc R . .
C13 C -0.0291(4) 0.5028(4) 0.0942(3) 0.0540(15) Uani 1 1 d . . .
H13A H 0.0186 0.4757 0.0821 0.081 Uiso 1 1 calc R . .
H13B H -0.0457 0.5539 0.0623 0.081 Uiso 1 1 calc R . .
H13C H -0.0741 0.4608 0.0858 0.081 Uiso 1 1 calc R . .
C14 C 0.2111(3) 0.5671(4) 0.5570(3) 0.0397(12) Uani 1 1 d . A .
H14A H 0.1751 0.6180 0.5571 0.048 Uiso 1 1 calc R . .
H14B H 0.2584 0.5863 0.5383 0.048 Uiso 1 1 calc R . .
C15 C 0.2400(4) 0.5316(4) 0.6352(3) 0.0631(17) Uani 1 1 d . . .
H15A H 0.1931 0.5098 0.6523 0.095 Uiso 1 1 calc R . .
H15B H 0.2669 0.5781 0.6685 0.095 Uiso 1 1 calc R . .
H15C H 0.2786 0.4840 0.6353 0.095 Uiso 1 1 calc R . .
C16 C 0.0514(3) 0.6494(4) 0.3581(3) 0.0473(14) Uani 1 1 d . A .
H16A H -0.0065 0.6548 0.3307 0.057 Uiso 1 1 calc R . .
H16B H 0.0848 0.6445 0.3210 0.057 Uiso 1 1 calc R . .
C17 C 0.0768(3) 0.7292(3) 0.4056(3) 0.0404(12) Uani 1 1 d . . .
H17A H 0.0478 0.7306 0.4455 0.061 Uiso 1 1 calc R . .
H17B H 0.0633 0.7816 0.3747 0.061 Uiso 1 1 calc R . .
H17C H 0.1357 0.7274 0.4274 0.061 Uiso 1 1 calc R . .
C18 C 0.3706(2) 0.6976(3) 0.4403(2) 0.0187(8) Uani 1 1 d . . .
H18 H 0.4037 0.7147 0.4872 0.022 Uiso 1 1 calc R . .
C19 C 0.3104(2) 0.7613(3) 0.4001(2) 0.0187(8) Uani 1 1 d . . .
C20 C 0.3006(2) 0.8398(3) 0.4395(2) 0.0238(9) Uani 1 1 d . . .
H20 H 0.3302 0.8461 0.4898 0.029 Uiso 1 1 calc R . .
C21 C 0.2488(3) 0.9074(3) 0.4059(3) 0.0289(10) Uani 1 1 d . . .
H21 H 0.2425 0.9583 0.4331 0.035 Uiso 1 1 calc R . .
C22 C 0.2056(3) 0.8976(3) 0.3298(3) 0.0308(10) Uani 1 1 d . . .
H22 H 0.1705 0.9429 0.3060 0.037 Uiso 1 1 calc R . .
C23 C 0.2142(3) 0.8224(3) 0.2899(2) 0.0260(10) Uani 1 1 d . . .
H23 H 0.1856 0.8184 0.2391 0.031 Uiso 1 1 calc R . .
C24 C 0.2650(2) 0.7511(3) 0.3232(2) 0.0202(9) Uani 1 1 d . A .
C25 C 0.4891(2) 0.4674(3) 0.2969(2) 0.0218(9) Uani 1 1 d . . .
H25 H 0.5431 0.4501 0.3209 0.026 Uiso 1 1 calc R . .
C26 C 0.4655(2) 0.4603(3) 0.2153(2) 0.0211(8) Uani 1 1 d . . .
C27 C 0.5252(3) 0.4296(3) 0.1780(3) 0.0326(11) Uani 1 1 d . . .
H27 H 0.5773 0.4126 0.2070 0.039 Uiso 1 1 calc R . .
C28 C 0.5095(3) 0.4237(4) 0.1006(3) 0.0404(12) Uani 1 1 d . . .
H28 H 0.5502 0.4033 0.0772 0.048 Uiso 1 1 calc R . .
C29 C 0.4313(3) 0.4488(3) 0.0571(2) 0.0361(11) Uani 1 1 d . . .
H29 H 0.4201 0.4456 0.0043 0.043 Uiso 1 1 calc R . .
C30 C 0.3708(3) 0.4782(3) 0.0913(2) 0.0282(10) Uani 1 1 d . . .
H30 H 0.3190 0.4943 0.0611 0.034 Uiso 1 1 calc R . .
C31 C 0.3852(2) 0.4846(3) 0.1709(2) 0.0206(9) Uani 1 1 d . A .
C32 C 0.4747(2) 0.4961(3) 0.4204(2) 0.0176(8) Uani 1 1 d . . .
C33 C 0.4421(2) 0.5611(3) 0.4612(2) 0.0171(8) Uani 1 1 d . . .
C34 C 0.4677(2) 0.5649(3) 0.5400(2) 0.0178(8) Uani 1 1 d . . .
H34 H 0.4462 0.6083 0.5664 0.021 Uiso 1 1 calc R . .
Co1 Co 0.10819(3) 0.37734(4) 0.37438(3) 0.02112(13) Uani 1 1 d . . .
Dy1 Dy 0.293075(10) 0.536287(12) 0.310006(10) 0.01559(6) Uani 1 1 d . A .
N1 N 0.38191(18) 0.6192(2) 0.41631(18) 0.0169(7) Uani 1 1 d . . .
N2 N 0.44259(19) 0.4956(2) 0.34042(17) 0.0171(7) Uani 1 1 d . . .
O1 O 0.2407(2) 0.2433(2) 0.3546(3) 0.0562(11) Uani 1 1 d . . .
O2 O 0.27498(19) 0.3168(3) 0.4808(2) 0.0579(12) Uani 1 1 d . . .
O3 O 0.29740(16) 0.39944(19) 0.36675(17) 0.0271(7) Uani 1 1 d . . .
O4 O 0.1008(3) 0.3389(3) 0.2040(2) 0.0784(16) Uani 1 1 d . . .
O5 O 0.0111(2) 0.4594(3) 0.2259(2) 0.071 Uani 1 1 d . . .
O6 O 0.16504(16) 0.4871(2) 0.24412(15) 0.0280(7) Uani 1 1 d . . .
O7 O 0.1669(3) 0.4997(3) 0.50910(19) 0.0606(12) Uani 1 1 d . . .
O8 O 0.0623(2) 0.5701(2) 0.4054(3) 0.0628(13) Uani 1 1 d . . .
O9 O 0.21010(17) 0.56003(19) 0.39441(16) 0.0250(7) Uani 1 1 d . . .
O10 O 0.27056(16) 0.68013(18) 0.28233(15) 0.0205(6) Uani 1 1 d . . .
O11 O 0.32604(16) 0.51380(19) 0.20124(15) 0.0234(6) Uani 1 1 d . . .
P1 P 0.23764(7) 0.33918(8) 0.39345(7) 0.0288(3) Uani 1 1 d . A .
P2 P 0.10289(7) 0.42035(9) 0.25907(6) 0.0293(3) Uani 1 1 d . A .
P3 P 0.14221(7) 0.50928(8) 0.41812(7) 0.0264(3) Uani 1 1 d . A .
C4' C 0.0549(7) 0.2495(6) 0.3614(7) 0.025(3) Uani 0.353(12) 1 d PGU A 2
H4' H 0.0727 0.2019 0.3366 0.030 Uiso 0.353(12) 1 calc PR A 2
C5' C -0.0056(6) 0.3118(8) 0.3283(6) 0.024(3) Uani 0.353(12) 1 d PGU A 2
H5' H -0.0352 0.3130 0.2776 0.029 Uiso 0.353(12) 1 calc PR A 2
C3' C -0.0139(7) 0.3721(7) 0.3847(7) 0.030(4) Uani 0.353(12) 1 d PGU A 2
H3' H -0.0500 0.4204 0.3782 0.036 Uiso 0.353(12) 1 calc PR A 2
C2' C 0.0415(7) 0.3470(8) 0.4527(6) 0.030(3) Uani 0.353(12) 1 d PGU A 2
H2' H 0.0487 0.3757 0.4993 0.037 Uiso 0.353(12) 1 calc PR A 2
C1' C 0.0840(6) 0.2712(8) 0.4382(7) 0.033(4) Uani 0.353(12) 1 d PGU A 2
H1' H 0.1246 0.2406 0.4736 0.039 Uiso 0.353(12) 1 calc PR A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C5 C1 C2 108.0 . .
C5 C1 Co1 69.33(18) . .
C2 C1 Co1 69.83(19) . .
C5 C1 H1 126.0 . .
C2 C1 H1 126.0 . .
Co1 C1 H1 126.4 . .
C3 C2 C1 108.0 . .
C3 C2 Co1 68.95(18) . .
C1 C2 Co1 70.60(19) . .
C3 C2 H2 126.0 . .
C1 C2 H2 126.0 . .
Co1 C2 H2 126.0 . .
C2 C3 C4 108.0 . .
C2 C3 Co1 71.11(18) . .
C4 C3 Co1 69.57(19) . .
C2 C3 H3 126.0 . .
C4 C3 H3 126.0 . .
Co1 C3 H3 124.9 . .
C5 C4 C3 108.0 . .
C5 C4 Co1 70.84(19) . .
C3 C4 Co1 70.13(19) . .
C5 C4 H4 126.0 . .
C3 C4 H4 126.0 . .
Co1 C4 H4 124.6 . .
C1 C5 C4 108.0 . .
C1 C5 Co1 71.00(18) . .
C4 C5 Co1 69.02(19) . .
C1 C5 H5 126.0 . .
C4 C5 H5 126.0 . .
Co1 C5 H5 125.6 . .
O1 C6 C7 111.8(5) . .
O1 C6 H6A 109.3 . .
C7 C6 H6A 109.3 . .
O1 C6 H6B 109.3 . .
C7 C6 H6B 109.3 . .
H6A C6 H6B 107.9 . .
C6 C7 H7A 109.5 . .
C6 C7 H7B 109.5 . .
H7A C7 H7B 109.5 . .
C6 C7 H7C 109.5 . .
H7A C7 H7C 109.5 . .
H7B C7 H7C 109.5 . .
O2 C8 C9 120.2(5) . .
O2 C8 H8A 107.3 . .
C9 C8 H8A 107.3 . .
O2 C8 H8B 107.3 . .
C9 C8 H8B 107.3 . .
H8A C8 H8B 106.9 . .
C8 C9 H9A 109.5 . .
C8 C9 H9B 109.5 . .
H9A C9 H9B 109.5 . .
C8 C9 H9C 109.5 . .
H9A C9 H9C 109.5 . .
H9B C9 H9C 109.5 . .
C11 C10 O4 121.9(6) . .
C11 C10 H10A 106.9 . .
O4 C10 H10A 106.9 . .
C11 C10 H10B 106.9 . .
O4 C10 H10B 106.9 . .
H10A C10 H10B 106.7 . .
C10 C11 H11A 109.5 . .
C10 C11 H11B 109.5 . .
H11A C11 H11B 109.5 . .
C10 C11 H11C 109.5 . .
H11A C11 H11C 109.5 . .
H11B C11 H11C 109.5 . .
O5 C12 C13 114.4(5) . .
O5 C12 H12A 108.7 . .
C13 C12 H12A 108.7 . .
O5 C12 H12B 108.7 . .
C13 C12 H12B 108.7 . .
H12A C12 H12B 107.6 . .
C12 C13 H13A 109.5 . .
C12 C13 H13B 109.5 . .
H13A C13 H13B 109.5 . .
C12 C13 H13C 109.5 . .
H13A C13 H13C 109.5 . .
H13B C13 H13C 109.5 . .
O7 C14 C15 109.1(5) . .
O7 C14 H14A 109.9 . .
C15 C14 H14A 109.9 . .
O7 C14 H14B 109.9 . .
C15 C14 H14B 109.9 . .
H14A C14 H14B 108.3 . .
C14 C15 H15A 109.5 . .
C14 C15 H15B 109.5 . .
H15A C15 H15B 109.5 . .
C14 C15 H15C 109.5 . .
H15A C15 H15C 109.5 . .
H15B C15 H15C 109.5 . .
O8 C16 C17 110.2(4) . .
O8 C16 H16A 109.6 . .
C17 C16 H16A 109.6 . .
O8 C16 H16B 109.6 . .
C17 C16 H16B 109.6 . .
H16A C16 H16B 108.1 . .
C16 C17 H17A 109.5 . .
C16 C17 H17B 109.5 . .
H17A C17 H17B 109.5 . .
C16 C17 H17C 109.5 . .
H17A C17 H17C 109.5 . .
H17B C17 H17C 109.5 . .
N1 C18 C19 125.2(4) . .
N1 C18 H18 117.4 . .
C19 C18 H18 117.4 . .
C20 C19 C24 119.2(4) . .
C20 C19 C18 116.7(3) . .
C24 C19 C18 124.0(4) . .
C21 C20 C19 122.1(4) . .
C21 C20 H20 118.9 . .
C19 C20 H20 118.9 . .
C20 C21 C22 118.3(4) . .
C20 C21 H21 120.8 . .
C22 C21 H21 120.8 . .
C23 C22 C21 120.9(4) . .
C23 C22 H22 119.5 . .
C21 C22 H22 119.5 . .
C22 C23 C24 122.2(4) . .
C22 C23 H23 118.9 . .
C24 C23 H23 118.9 . .
O10 C24 C23 119.7(4) . .
O10 C24 C19 123.1(4) . .
C23 C24 C19 117.2(4) . .
N2 C25 C26 126.4(3) . .
N2 C25 H25 116.8 . .
C26 C25 H25 116.8 . .
C27 C26 C31 118.8(4) . .
C27 C26 C25 118.1(4) . .
C31 C26 C25 123.1(3) . .
C28 C27 C26 122.3(4) . .
C28 C27 H27 118.9 . .
C26 C27 H27 118.9 . .
C27 C28 C29 118.9(4) . .
C27 C28 H28 120.6 . .
C29 C28 H28 120.6 . .
C30 C29 C28 120.8(4) . .
C30 C29 H29 119.6 . .
C28 C29 H29 119.6 . .
C29 C30 C31 121.5(4) . .
C29 C30 H30 119.2 . .
C31 C30 H30 119.2 . .
O11 C31 C30 119.7(4) . .
O11 C31 C26 122.7(3) . .
C30 C31 C26 117.7(4) . .
C34 C32 C33 119.3(3) 3_666 .
C34 C32 N2 124.4(3) 3_666 .
C33 C32 N2 116.3(3) . .
C34 C33 C32 120.4(3) . .
C34 C33 N1 124.0(3) . .
C32 C33 N1 115.5(3) . .
C33 C34 C32 120.3(4) . 3_666
C33 C34 H34 119.9 . .
C32 C34 H34 119.9 3_666 .
C2' Co1 C4 64.8(3) . .
C2' Co1 C1' 39.7(2) . .
C4 Co1 C1' 52.4(3) . .
C2' Co1 C3 52.4(3) . .
C4 Co1 C3 40.31(13) . .
C1' Co1 C3 16.8(3) . .
C2' Co1 C3' 39.6(2) . .
C4 Co1 C3' 50.0(3) . .
C1' Co1 C3' 66.2(4) . .
C3 Co1 C3' 68.8(3) . .
C2' Co1 C5 50.3(3) . .
C4 Co1 C5 40.13(12) . .
C1' Co1 C5 69.0(3) . .
C3 Co1 C5 67.3(2) . .
C3' Co1 C5 13.6(3) . .
C2' Co1 C2 21.2(3) . .
C4 Co1 C2 67.2(2) . .
C1' Co1 C2 23.7(3) . .
C3 Co1 C2 39.94(12) . .
C3' Co1 C2 58.5(3) . .
C5 Co1 C2 66.8(2) . .
C2' Co1 C4' 66.0(4) . .
C4 Co1 C4' 21.0(2) . .
C1' Co1 C4' 39.1(2) . .
C3 Co1 C4' 23.4(2) . .
C3' Co1 C4' 65.5(4) . .
C5 Co1 C4' 58.5(2) . .
C2 Co1 C4' 60.0(3) . .
C2' Co1 C1 18.4(3) . .
C4 Co1 C1 67.0(2) . .
C1' Co1 C1 56.7(3) . .
C3 Co1 C1 66.9(2) . .
C3' Co1 C1 26.6(3) . .
C5 Co1 C1 39.67(12) . .
C2 Co1 C1 39.56(12) . .
C4' Co1 C1 74.9(3) . .
C2' Co1 C5' 65.8(4) . .
C4 Co1 C5' 17.7(2) . .
C1' Co1 C5' 65.5(4) . .
C3 Co1 C5' 56.2(2) . .
C3' Co1 C5' 39.0(2) . .
C5 Co1 C5' 26.5(2) . .
C2 Co1 C5' 74.8(3) . .
C4' Co1 C5' 38.7(2) . .
C1 Co1 C5' 61.9(3) . .
C2' Co1 P3 95.0(3) . .
C4 Co1 P3 149.87(18) . .
C1' Co1 P3 125.0(4) . .
C3 Co1 P3 141.7(2) . .
C3' Co1 P3 100.1(3) . .
C5 Co1 P3 109.83(18) . .
C2 Co1 P3 102.40(17) . .
C4' Co1 P3 161.0(3) . .
C1 Co1 P3 86.84(15) . .
C5' Co1 P3 134.6(3) . .
C2' Co1 P1 120.6(4) . .
C4 Co1 P1 117.81(19) . .
C1' Co1 P1 91.4(3) . .
C3 Co1 P1 90.21(15) . .
C3' Co1 P1 157.5(3) . .
C5 Co1 P1 156.73(16) . .
C2 Co1 P1 100.21(16) . .
C4' Co1 P1 98.5(3) . .
C1 Co1 P1 137.39(18) . .
C5' Co1 P1 133.9(3) . .
P3 Co1 P1 91.42(5) . .
O11 Dy1 O10 90.69(10) . .
O11 Dy1 O6 83.20(10) . .
O10 Dy1 O6 96.47(10) . .
O11 Dy1 O3 106.04(11) . .
O10 Dy1 O3 162.92(10) . .
O6 Dy1 O3 82.45(10) . .
O11 Dy1 O9 158.78(10) . .
O10 Dy1 O9 84.56(10) . .
O6 Dy1 O9 76.82(10) . .
O3 Dy1 O9 78.58(10) . .
O11 Dy1 N1 123.33(10) . .
O10 Dy1 N1 73.75(10) . .
O6 Dy1 N1 150.98(10) . .
O3 Dy1 N1 98.99(11) . .
O9 Dy1 N1 75.11(10) . .
O11 Dy1 N2 73.15(10) . .
O10 Dy1 N2 113.15(10) . .
O6 Dy1 N2 141.71(11) . .
O3 Dy1 N2 75.94(10) . .
O9 Dy1 N2 127.64(10) . .
N1 Dy1 N2 64.88(10) . .
C18 N1 C33 120.7(3) . .
C18 N1 Dy1 128.3(3) . .
C33 N1 Dy1 109.8(2) . .
C25 N2 C32 119.4(3) . .
C25 N2 Dy1 130.7(3) . .
C32 N2 Dy1 109.5(2) . .
C6 O1 P1 119.8(4) . .
C8 O2 P1 126.5(3) . .
P1 O3 Dy1 137.10(16) . .
C10 O4 P2 127.3(4) . .
C12 O5 P2 124.7(3) . .
P2 O6 Dy1 135.00(17) . .
C14 O7 P3 122.0(3) . .
C16 O8 P3 122.8(3) . .
P3 O9 Dy1 135.48(16) . .
C24 O10 Dy1 133.7(2) . .
C31 O11 Dy1 143.3(2) . .
O3 P1 O2 108.65(18) . .
O3 P1 O1 107.86(18) . .
O2 P1 O1 101.5(2) . .
O3 P1 Co1 119.42(12) . .
O2 P1 Co1 110.32(15) . .
O1 P1 Co1 107.57(14) . .
O6 P2 O4 108.44(19) . .
O6 P2 O5 108.33(19) . .
O4 P2 O5 100.0(3) . .
O6 P2 Co1 120.06(12) . .
O4 P2 Co1 111.55(18) . .
O5 P2 Co1 106.52(14) . .
O9 P3 O8 108.75(19) . .
O9 P3 O7 108.44(18) . .
O8 P3 O7 101.5(2) . .
O9 P3 Co1 120.54(12) . .
O8 P3 Co1 110.10(15) . .
O7 P3 Co1 105.83(15) . .
C5' C4' C1' 108.0 . .
C5' C4' Co1 70.9(4) . .
C1' C4' Co1 68.9(3) . .
C5' C4' H4' 126.0 . .
C1' C4' H4' 126.0 . .
Co1 C4' H4' 125.8 . .
C4' C5' C3' 108.0 . .
C4' C5' Co1 70.4(4) . .
C3' C5' Co1 69.2(4) . .
C4' C5' H5' 126.0 . .
C3' C5' H5' 126.0 . .
Co1 C5' H5' 126.0 . .
C2' C3' C5' 108.0 . .
C2' C3' Co1 69.1(4) . .
C5' C3' Co1 71.9(4) . .
C2' C3' H3' 126.0 . .
C5' C3' H3' 126.0 . .
Co1 C3' H3' 124.6 . .
C1' C2' C3' 108.0 . .
C1' C2' Co1 70.8(4) . .
C3' C2' Co1 71.3(4) . .
C1' C2' H2' 126.0 . .
C3' C2' H2' 126.0 . .
Co1 C2' H2' 123.5 . .
C2' C1' C4' 108.0 . .
C2' C1' Co1 69.4(4) . .
C4' C1' Co1 71.9(4) . .
C2' C1' H1' 126.0 . .
C4' C1' H1' 126.0 . .
Co1 C1' H1' 124.2 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 C5 1.422(5) .
C1 C2 1.422(5) .
C1 Co1 2.106(5) .
C1 H1 0.9300 .
C2 C3 1.422(5) .
C2 Co1 2.095(5) .
C2 H2 0.9300 .
C3 C4 1.422(5) .
C3 Co1 2.067(5) .
C3 H3 0.9300 .
C4 C5 1.422(5) .
C4 Co1 2.060(5) .
C4 H4 0.9300 .
C5 Co1 2.084(5) .
C5 H5 0.9300 .
C6 O1 1.408(6) .
C6 C7 1.444(8) .
C6 H6A 0.9700 .
C6 H6B 0.9700 .
C7 H7A 0.9600 .
C7 H7B 0.9600 .
C7 H7C 0.9600 .
C8 O2 1.358(6) .
C8 C9 1.411(8) .
C8 H8A 0.9700 .
C8 H8B 0.9700 .
C9 H9A 0.9600 .
C9 H9B 0.9600 .
C9 H9C 0.9600 .
C10 C11 1.379(8) .
C10 O4 1.383(7) .
C10 H10A 0.9700 .
C10 H10B 0.9700 .
C11 H11A 0.9600 .
C11 H11B 0.9600 .
C11 H11C 0.9600 .
C12 O5 1.410(6) .
C12 C13 1.452(7) .
C12 H12A 0.9700 .
C12 H12B 0.9700 .
C13 H13A 0.9600 .
C13 H13B 0.9600 .
C13 H13C 0.9600 .
C14 O7 1.418(6) .
C14 C15 1.479(7) .
C14 H14A 0.9700 .
C14 H14B 0.9700 .
C15 H15A 0.9600 .
C15 H15B 0.9600 .
C15 H15C 0.9600 .
C16 O8 1.454(7) .
C16 C17 1.478(7) .
C16 H16A 0.9700 .
C16 H16B 0.9700 .
C17 H17A 0.9600 .
C17 H17B 0.9600 .
C17 H17C 0.9600 .
C18 N1 1.286(5) .
C18 C19 1.445(5) .
C18 H18 0.9300 .
C19 C20 1.409(6) .
C19 C24 1.422(5) .
C20 C21 1.373(6) .
C20 H20 0.9300 .
C21 C22 1.397(6) .
C21 H21 0.9300 .
C22 C23 1.367(6) .
C22 H22 0.9300 .
C23 C24 1.405(6) .
C23 H23 0.9300 .
C24 O10 1.315(5) .
C25 N2 1.299(5) .
C25 C26 1.437(5) .
C25 H25 0.9300 .
C26 C27 1.403(6) .
C26 C31 1.426(5) .
C27 C28 1.365(6) .
C27 H27 0.9300 .
C28 C29 1.394(7) .
C28 H28 0.9300 .
C29 C30 1.371(6) .
C29 H29 0.9300 .
C30 C31 1.407(6) .
C30 H30 0.9300 .
C31 O11 1.308(5) .
C32 C34 1.390(5) 3_666
C32 C33 1.408(5) .
C32 N2 1.417(5) .
C33 C34 1.388(5) .
C33 N1 1.423(5) .
C34 C32 1.390(5) 3_666
C34 H34 0.9300 .
Co1 C2' 2.047(10) .
Co1 C1' 2.065(10) .
Co1 C3' 2.075(10) .
Co1 C4' 2.104(10) .
Co1 C5' 2.110(10) .
Co1 P3 2.1600(13) .
Co1 P1 2.1631(12) .
Dy1 O11 2.193(3) .
Dy1 O10 2.231(3) .
Dy1 O6 2.288(3) .
Dy1 O3 2.293(3) .
Dy1 O9 2.315(3) .
Dy1 N1 2.461(3) .
Dy1 N2 2.478(3) .
O1 P1 1.610(4) .
O2 P1 1.589(4) .
O3 P1 1.504(3) .
O4 P2 1.574(4) .
O5 P2 1.603(4) .
O6 P2 1.508(3) .
O7 P3 1.605(4) .
O8 P3 1.578(4) .
O9 P3 1.504(3) .
C4' C5' 1.397(9) .
C4' C1' 1.397(9) .
C4' H4' 0.9300 .
C5' C3' 1.397(9) .
C5' H5' 0.9300 .
C3' C2' 1.397(9) .
C3' H3' 0.9300 .
C2' C1' 1.397(9) .
C2' H2' 0.9300 .
C1' H1' 0.9300 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C5 C1 C2 C3 0.0 . .
Co1 C1 C2 C3 -59.02(19) . .
C5 C1 C2 Co1 59.02(19) . .
C1 C2 C3 C4 0.0 . .
Co1 C2 C3 C4 -60.1(2) . .
C1 C2 C3 Co1 60.1(2) . .
C2 C3 C4 C5 0.0 . .
Co1 C3 C4 C5 -61.0(2) . .
C2 C3 C4 Co1 61.0(2) . .
C2 C1 C5 C4 0.0 . .
Co1 C1 C5 C4 59.3(2) . .
C2 C1 C5 Co1 -59.3(2) . .
C3 C4 C5 C1 0.0 . .
Co1 C4 C5 C1 -60.6(2) . .
C3 C4 C5 Co1 60.6(2) . .
N1 C18 C19 C20 172.9(4) . .
N1 C18 C19 C24 -10.5(6) . .
C24 C19 C20 C21 -0.4(6) . .
C18 C19 C20 C21 176.4(4) . .
C19 C20 C21 C22 -0.9(6) . .
C20 C21 C22 C23 0.5(7) . .
C21 C22 C23 C24 1.3(7) . .
C22 C23 C24 O10 179.5(4) . .
C22 C23 C24 C19 -2.5(6) . .
C20 C19 C24 O10 179.9(4) . .
C18 C19 C24 O10 3.4(6) . .
C20 C19 C24 C23 2.1(5) . .
C18 C19 C24 C23 -174.5(4) . .
N2 C25 C26 C27 179.0(4) . .
N2 C25 C26 C31 0.2(7) . .
C31 C26 C27 C28 1.3(7) . .
C25 C26 C27 C28 -177.6(5) . .
C26 C27 C28 C29 -0.2(8) . .
C27 C28 C29 C30 -0.6(8) . .
C28 C29 C30 C31 0.4(7) . .
C29 C30 C31 O11 179.3(4) . .
C29 C30 C31 C26 0.7(6) . .
C27 C26 C31 O11 180.0(4) . .
C25 C26 C31 O11 -1.2(6) . .
C27 C26 C31 C30 -1.5(6) . .
C25 C26 C31 C30 177.3(4) . .
C34 C32 C33 C34 0.6(6) 3_666 .
N2 C32 C33 C34 177.8(3) . .
C34 C32 C33 N1 -178.4(3) 3_666 .
N2 C32 C33 N1 -1.2(5) . .
C32 C33 C34 C32 -0.6(6) . 3_666
N1 C33 C34 C32 178.3(3) . 3_666
C5 C4 Co1 C2' 57.4(3) . .
C3 C4 Co1 C2' -60.8(3) . .
C5 C4 Co1 C1' 102.1(4) . .
C3 C4 Co1 C1' -16.1(4) . .
C5 C4 Co1 C3 118.26(11) . .
C5 C4 Co1 C3' 13.3(4) . .
C3 C4 Co1 C3' -105.0(4) . .
C3 C4 Co1 C5 -118.26(11) . .
C5 C4 Co1 C2 80.50(13) . .
C3 C4 Co1 C2 -37.75(8) . .
C5 C4 Co1 C4' 145.6(9) . .
C3 C4 Co1 C4' 27.3(9) . .
C5 C4 Co1 C1 37.41(8) . .
C3 C4 Co1 C1 -80.85(13) . .
C5 C4 Co1 C5' -31.7(11) . .
C3 C4 Co1 C5' -149.9(11) . .
C5 C4 Co1 P3 5.5(5) . .
C3 C4 Co1 P3 -112.7(5) . .
C5 C4 Co1 P1 170.3(2) . .
C3 C4 Co1 P1 52.0(2) . .
C2 C3 Co1 C2' -24.0(4) . .
C4 C3 Co1 C2' 94.5(4) . .
C2 C3 Co1 C4 -118.43(12) . .
C2 C3 Co1 C1' 11.8(12) . .
C4 C3 Co1 C1' 130.2(11) . .
C2 C3 Co1 C3' -65.9(3) . .
C4 C3 Co1 C3' 52.5(3) . .
C2 C3 Co1 C5 -80.45(13) . .
C4 C3 Co1 C5 37.98(8) . .
C4 C3 Co1 C2 118.43(12) . .
C2 C3 Co1 C4' -143.0(8) . .
C4 C3 Co1 C4' -24.5(8) . .
C2 C3 Co1 C1 -37.22(8) . .
C4 C3 Co1 C1 81.20(13) . .
C2 C3 Co1 C5' -107.9(3) . .
C4 C3 Co1 C5' 10.6(4) . .
C2 C3 Co1 P3 13.2(3) . .
C4 C3 Co1 P3 131.6(4) . .
C2 C3 Co1 P1 105.8(2) . .
C4 C3 Co1 P1 -135.8(3) . .
C1 C5 Co1 C2' 21.5(4) . .
C4 C5 Co1 C2' -97.4(4) . .
C1 C5 Co1 C4 118.82(11) . .
C1 C5 Co1 C1' 62.7(3) . .
C4 C5 Co1 C1' -56.1(3) . .
C1 C5 Co1 C3 80.68(13) . .
C4 C5 Co1 C3 -38.14(8) . .
C1 C5 Co1 C3' -12.7(15) . .
C4 C5 Co1 C3' -131.5(15) . .
C1 C5 Co1 C2 37.15(8) . .
C4 C5 Co1 C2 -81.67(13) . .
C1 C5 Co1 C4' 105.1(3) . .
C4 C5 Co1 C4' -13.8(3) . .
C4 C5 Co1 C1 -118.82(12) . .
C1 C5 Co1 C5' 139.8(7) . .
C4 C5 Co1 C5' 21.0(7) . .
C1 C5 Co1 P3 -58.2(2) . .
C4 C5 Co1 P3 -177.1(3) . .
C1 C5 Co1 P1 96.6(6) . .
C4 C5 Co1 P1 -22.2(6) . .
C3 C2 Co1 C2' 117.0(9) . .
C1 C2 Co1 C2' -2.1(9) . .
C3 C2 Co1 C4 38.10(8) . .
C1 C2 Co1 C4 -81.02(13) . .
C3 C2 Co1 C1' -8.4(8) . .
C1 C2 Co1 C1' -127.5(8) . .
C1 C2 Co1 C3 -119.11(12) . .
C3 C2 Co1 C3' 94.0(3) . .
C1 C2 Co1 C3' -25.1(4) . .
C3 C2 Co1 C5 81.86(13) . .
C1 C2 Co1 C5 -37.25(8) . .
C3 C2 Co1 C4' 16.0(3) . .
C1 C2 Co1 C4' -103.1(3) . .
C3 C2 Co1 C1 119.11(12) . .
C3 C2 Co1 C5' 55.1(3) . .
C1 C2 Co1 C5' -64.1(3) . .
C3 C2 Co1 P3 -171.7(2) . .
C1 C2 Co1 P3 69.2(2) . .
C3 C2 Co1 P1 -77.9(2) . .
C1 C2 Co1 P1 163.0(2) . .
C5 C1 Co1 C2' -116.9(10) . .
C2 C1 Co1 C2' 2.4(11) . .
C5 C1 Co1 C4 -37.83(8) . .
C2 C1 Co1 C4 81.54(14) . .
C5 C1 Co1 C1' -96.9(3) . .
C2 C1 Co1 C1' 22.5(4) . .
C5 C1 Co1 C3 -81.80(13) . .
C2 C1 Co1 C3 37.57(8) . .
C5 C1 Co1 C3' 6.6(8) . .
C2 C1 Co1 C3' 126.0(8) . .
C2 C1 Co1 C5 119.37(12) . .
C5 C1 Co1 C2 -119.37(12) . .
C5 C1 Co1 C4' -58.5(3) . .
C2 C1 Co1 C4' 60.9(3) . .
C5 C1 Co1 C5' -19.0(3) . .
C2 C1 Co1 C5' 100.3(3) . .
C5 C1 Co1 P3 126.8(3) . .
C2 C1 Co1 P3 -113.9(3) . .
C5 C1 Co1 P1 -144.6(3) . .
C2 C1 Co1 P1 -25.2(3) . .
C19 C18 N1 C33 -178.9(3) . .
C19 C18 N1 Dy1 -12.8(6) . .
C34 C33 N1 C18 26.8(5) . .
C32 C33 N1 C18 -154.2(4) . .
C34 C33 N1 Dy1 -141.7(3) . .
C32 C33 N1 Dy1 37.3(4) . .
O11 Dy1 N1 C18 107.0(3) . .
O10 Dy1 N1 C18 27.2(3) . .
O6 Dy1 N1 C18 -46.3(4) . .
O3 Dy1 N1 C18 -137.0(3) . .
O9 Dy1 N1 C18 -61.4(3) . .
N2 Dy1 N1 C18 153.3(3) . .
O11 Dy1 N1 C33 -85.7(2) . .
O10 Dy1 N1 C33 -165.5(2) . .
O6 Dy1 N1 C33 121.0(3) . .
O3 Dy1 N1 C33 30.4(2) . .
O9 Dy1 N1 C33 105.9(2) . .
N2 Dy1 N1 C33 -39.4(2) . .
C26 C25 N2 C32 178.2(4) . .
C26 C25 N2 Dy1 6.3(6) . .
C34 C32 N2 C25 -31.6(6) 3_666 .
C33 C32 N2 C25 151.3(4) . .
C34 C32 N2 Dy1 141.9(3) 3_666 .
C33 C32 N2 Dy1 -35.1(4) . .
O11 Dy1 N2 C25 -7.9(3) . .
O10 Dy1 N2 C25 -91.2(4) . .
O6 Dy1 N2 C25 46.5(4) . .
O3 Dy1 N2 C25 104.1(4) . .
O9 Dy1 N2 C25 167.3(3) . .
N1 Dy1 N2 C25 -148.8(4) . .
O11 Dy1 N2 C32 179.6(3) . .
O10 Dy1 N2 C32 96.2(2) . .
O6 Dy1 N2 C32 -126.1(2) . .
O3 Dy1 N2 C32 -68.5(2) . .
O9 Dy1 N2 C32 -5.3(3) . .
N1 Dy1 N2 C32 38.7(2) . .
C7 C6 O1 P1 -178.9(5) . .
C9 C8 O2 P1 -170.6(6) . .
O11 Dy1 O3 P1 -119.1(3) . .
O10 Dy1 O3 P1 49.0(5) . .
O6 Dy1 O3 P1 -38.5(3) . .
O9 Dy1 O3 P1 39.5(3) . .
N1 Dy1 O3 P1 112.2(3) . .
N2 Dy1 O3 P1 173.4(3) . .
C11 C10 O4 P2 -78.8(9) . .
C13 C12 O5 P2 90.7(5) . .
O11 Dy1 O6 P2 132.1(3) . .
O10 Dy1 O6 P2 -138.0(3) . .
O3 Dy1 O6 P2 24.8(3) . .
O9 Dy1 O6 P2 -55.2(3) . .
N1 Dy1 O6 P2 -70.1(4) . .
N2 Dy1 O6 P2 80.5(3) . .
C15 C14 O7 P3 -168.0(4) . .
C17 C16 O8 P3 -96.4(5) . .
O11 Dy1 O9 P3 61.3(4) . .
O10 Dy1 O9 P3 139.1(3) . .
O6 Dy1 O9 P3 41.2(2) . .
O3 Dy1 O9 P3 -43.6(2) . .
N1 Dy1 O9 P3 -146.3(3) . .
N2 Dy1 O9 P3 -105.7(3) . .
C23 C24 O10 Dy1 -150.1(3) . .
C19 C24 O10 Dy1 32.1(5) . .
O11 Dy1 O10 C24 -162.5(3) . .
O6 Dy1 O10 C24 114.3(3) . .
O3 Dy1 O10 C24 29.0(5) . .
O9 Dy1 O10 C24 38.3(3) . .
N1 Dy1 O10 C24 -37.8(3) . .
N2 Dy1 O10 C24 -90.5(3) . .
C30 C31 O11 Dy1 175.1(3) . .
C26 C31 O11 Dy1 -6.4(7) . .
O10 Dy1 O11 C31 122.7(4) . .
O6 Dy1 O11 C31 -140.8(4) . .
O3 Dy1 O11 C31 -60.7(4) . .
O9 Dy1 O11 C31 -160.6(4) . .
N1 Dy1 O11 C31 51.8(5) . .
N2 Dy1 O11 C31 8.7(4) . .
Dy1 O3 P1 O2 -124.4(3) . .
Dy1 O3 P1 O1 126.3(3) . .
Dy1 O3 P1 Co1 3.3(3) . .
C8 O2 P1 O3 -1.3(6) . .
C8 O2 P1 O1 112.3(6) . .
C8 O2 P1 Co1 -133.9(5) . .
C6 O1 P1 O3 40.2(5) . .
C6 O1 P1 O2 -73.9(5) . .
C6 O1 P1 Co1 170.2(4) . .
C2' Co1 P1 O3 -144.8(4) . .
C4 Co1 P1 O3 139.5(2) . .
C1' Co1 P1 O3 -173.2(4) . .
C3 Co1 P1 O3 170.1(2) . .
C3' Co1 P1 O3 -169.3(9) . .
C5 Co1 P1 O3 155.5(5) . .
C2 Co1 P1 O3 -151.0(2) . .
C4' Co1 P1 O3 148.2(4) . .
C1 Co1 P1 O3 -135.0(3) . .
C5' Co1 P1 O3 130.4(4) . .
P3 Co1 P1 O3 -48.14(16) . .
C2' Co1 P1 O2 -17.9(4) . .
C4 Co1 P1 O2 -93.7(2) . .
C1' Co1 P1 O2 -46.3(4) . .
C3 Co1 P1 O2 -63.0(3) . .
C3' Co1 P1 O2 -42.4(9) . .
C5 Co1 P1 O2 -77.6(5) . .
C2 Co1 P1 O2 -24.1(2) . .
C4' Co1 P1 O2 -84.9(4) . .
C1 Co1 P1 O2 -8.1(3) . .
C5' Co1 P1 O2 -102.7(4) . .
P3 Co1 P1 O2 78.75(18) . .
C2' Co1 P1 O1 92.0(4) . .
C4 Co1 P1 O1 16.2(2) . .
C1' Co1 P1 O1 63.6(4) . .
C3 Co1 P1 O1 46.9(3) . .
C3' Co1 P1 O1 67.5(9) . .
C5 Co1 P1 O1 32.2(5) . .
C2 Co1 P1 O1 85.8(2) . .
C4' Co1 P1 O1 24.9(4) . .
C1 Co1 P1 O1 101.8(3) . .
C5' Co1 P1 O1 7.1(4) . .
P3 Co1 P1 O1 -171.37(17) . .
Dy1 O6 P2 O4 -110.4(3) . .
Dy1 O6 P2 O5 142.0(3) . .
Dy1 O6 P2 Co1 19.4(3) . .
C10 O4 P2 O6 20.3(6) . .
C10 O4 P2 O5 133.6(6) . .
C10 O4 P2 Co1 -114.1(5) . .
C12 O5 P2 O6 16.6(5) . .
C12 O5 P2 O4 -96.7(5) . .
C12 O5 P2 Co1 147.1(4) . .
C2' Co1 P2 O6 138.6(6) . .
C4 Co1 P2 O6 -172.2(2) . .
C1' Co1 P2 O6 -149.5(5) . .
C3 Co1 P2 O6 -146.1(2) . .
C3' Co1 P2 O6 138.4(3) . .
C5 Co1 P2 O6 147.5(2) . .
C2 Co1 P2 O6 174.4(6) . .
C4' Co1 P2 O6 -153.4(3) . .
C1 Co1 P2 O6 124.5(2) . .
C5' Co1 P2 O6 172.0(4) . .
P3 Co1 P2 O6 37.39(16) . .
P1 Co1 P2 O6 -54.09(16) . .
C2' Co1 P2 O4 -93.0(6) . .
C4 Co1 P2 O4 -43.8(3) . .
C1' Co1 P2 O4 -21.1(5) . .
C3 Co1 P2 O4 -17.7(3) . .
C3' Co1 P2 O4 -93.2(4) . .
C5 Co1 P2 O4 -84.0(3) . .
C2 Co1 P2 O4 -57.2(6) . .
C4' Co1 P2 O4 -25.0(3) . .
C1 Co1 P2 O4 -107.1(3) . .
C5' Co1 P2 O4 -59.6(4) . .
P3 Co1 P2 O4 165.8(2) . .
P1 Co1 P2 O4 74.3(2) . .
C2' Co1 P2 O5 15.2(6) . .
C4 Co1 P2 O5 64.4(3) . .
C1' Co1 P2 O5 87.1(5) . .
C3 Co1 P2 O5 90.5(3) . .
C3' Co1 P2 O5 14.9(4) . .
C5 Co1 P2 O5 24.1(3) . .
C2 Co1 P2 O5 51.0(6) . .
C4' Co1 P2 O5 83.1(3) . .
C1 Co1 P2 O5 1.1(3) . .
C5' Co1 P2 O5 48.6(4) . .
P3 Co1 P2 O5 -86.02(19) . .
P1 Co1 P2 O5 -177.50(19) . .
Dy1 O9 P3 O8 -124.2(3) . .
Dy1 O9 P3 O7 126.3(3) . .
Dy1 O9 P3 Co1 4.2(3) . .
C16 O8 P3 O9 16.4(5) . .
C16 O8 P3 O7 130.6(4) . .
C16 O8 P3 Co1 -117.7(4) . .
C14 O7 P3 O9 34.1(5) . .
C14 O7 P3 O8 -80.3(4) . .
C14 O7 P3 Co1 164.7(4) . .
C2' Co1 P3 O9 165.6(4) . .
C4 Co1 P3 O9 -148.7(4) . .
C1' Co1 P3 O9 137.4(4) . .
C3 Co1 P3 O9 136.9(3) . .
C3' Co1 P3 O9 -154.7(4) . .
C5 Co1 P3 O9 -144.9(2) . .
C2 Co1 P3 O9 145.5(2) . .
C4' Co1 P3 O9 166.3(10) . .
C1 Co1 P3 O9 -177.9(2) . .
C5' Co1 P3 O9 -133.7(4) . .
P1 Co1 P3 O9 44.75(16) . .
C2' Co1 P3 O8 -66.5(4) . .
C4 Co1 P3 O8 -20.9(4) . .
C1' Co1 P3 O8 -94.8(4) . .
C3 Co1 P3 O8 -95.3(3) . .
C3' Co1 P3 O8 -26.9(4) . .
C5 Co1 P3 O8 -17.1(3) . .
C2 Co1 P3 O8 -86.6(2) . .
C4' Co1 P3 O8 -65.9(10) . .
C1 Co1 P3 O8 -50.0(3) . .
C5' Co1 P3 O8 -5.9(4) . .
P1 Co1 P3 O8 172.58(19) . .
C2' Co1 P3 O7 42.3(4) . .
C4 Co1 P3 O7 88.0(4) . .
C1' Co1 P3 O7 14.1(4) . .
C3 Co1 P3 O7 13.6(3) . .
C3' Co1 P3 O7 82.0(4) . .
C5 Co1 P3 O7 91.8(2) . .
C2 Co1 P3 O7 22.2(2) . .
C4' Co1 P3 O7 43.0(10) . .
C1 Co1 P3 O7 58.8(2) . .
C5' Co1 P3 O7 103.0(4) . .
P1 Co1 P3 O7 -78.54(17) . .
C2' Co1 C4' C5' 80.8(3) . .
C4 Co1 C4' C5' -1.3(9) . .
C1' Co1 C4' C5' 119.0(2) . .
C3 Co1 C4' C5' 130.2(8) . .
C3' Co1 C4' C5' 37.17(16) . .
C5 Co1 C4' C5' 24.0(4) . .
C2 Co1 C4' C5' 103.7(3) . .
C1 Co1 C4' C5' 63.7(3) . .
P3 Co1 C4' C5' 80.1(13) . .
P1 Co1 C4' C5' -159.4(4) . .
C2' Co1 C4' C1' -38.15(16) . .
C4 Co1 C4' C1' -120.3(8) . .
C3 Co1 C4' C1' 11.2(9) . .
C3' Co1 C4' C1' -81.8(2) . .
C5 Co1 C4' C1' -95.0(3) . .
C2 Co1 C4' C1' -15.3(4) . .
C1 Co1 C4' C1' -55.3(3) . .
C5' Co1 C4' C1' -119.0(2) . .
P3 Co1 C4' C1' -38.9(13) . .
P1 Co1 C4' C1' 81.7(5) . .
C1' C4' C5' C3' 0.0 . .
Co1 C4' C5' C3' -59.2(4) . .
C1' C4' C5' Co1 59.2(4) . .
C2' Co1 C5' C4' -81.1(3) . .
C4 Co1 C5' C4' 1.6(11) . .
C1' Co1 C5' C4' -37.35(16) . .
C3 Co1 C5' C4' -21.4(4) . .
C3' Co1 C5' C4' -119.1(2) . .
C5 Co1 C5' C4' -129.0(7) . .
C2 Co1 C5' C4' -60.7(3) . .
C1 Co1 C5' C4' -101.2(3) . .
P3 Co1 C5' C4' -153.2(5) . .
P1 Co1 C5' C4' 28.9(5) . .
C2' Co1 C5' C3' 37.99(16) . .
C4 Co1 C5' C3' 120.7(10) . .
C1' Co1 C5' C3' 81.8(2) . .
C3 Co1 C5' C3' 97.7(3) . .
C5 Co1 C5' C3' -9.9(8) . .
C2 Co1 C5' C3' 58.4(3) . .
C4' Co1 C5' C3' 119.1(2) . .
C1 Co1 C5' C3' 17.9(4) . .
P3 Co1 C5' C3' -34.1(5) . .
P1 Co1 C5' C3' 148.0(6) . .
C4' C5' C3' C2' 0.0 . .
Co1 C5' C3' C2' -59.9(4) . .
C4' C5' C3' Co1 59.9(4) . .
C4 Co1 C3' C2' 98.3(4) . .
C1' Co1 C3' C2' 38.25(15) . .
C3 Co1 C3' C2' 56.2(3) . .
C5 Co1 C3' C2' 137.3(14) . .
C2 Co1 C3' C2' 12.8(4) . .
C4' Co1 C3' C2' 81.3(2) . .
C1 Co1 C3' C2' -24.4(8) . .
C5' Co1 C3' C2' 118.2(2) . .
P3 Co1 C3' C2' -85.7(5) . .
P1 Co1 C3' C2' 34.0(12) . .
C2' Co1 C3' C5' -118.2(2) . .
C4 Co1 C3' C5' -20.0(4) . .
C1' Co1 C3' C5' -80.0(2) . .
C3 Co1 C3' C5' -62.1(3) . .
C5 Co1 C3' C5' 19.1(15) . .
C2 Co1 C3' C5' -105.4(3) . .
C4' Co1 C3' C5' -36.91(15) . .
C1 Co1 C3' C5' -142.6(8) . .
P3 Co1 C3' C5' 156.1(4) . .
P1 Co1 C3' C5' -84.3(12) . .
C5' C3' C2' C1' 0.0 . .
Co1 C3' C2' C1' -61.7(4) . .
C5' C3' C2' Co1 61.7(4) . .
C4 Co1 C2' C1' 60.7(3) . .
C3 Co1 C2' C1' 15.3(4) . .
C3' Co1 C2' C1' 117.6(2) . .
C5 Co1 C2' C1' 105.7(4) . .
C2 Co1 C2' C1' -30.9(10) . .
C4' Co1 C2' C1' 37.60(16) . .
C1 Co1 C2' C1' 153.4(11) . .
C5' Co1 C2' C1' 80.2(2) . .
P3 Co1 C2' C1' -142.6(5) . .
P1 Co1 C2' C1' -48.0(5) . .
C4 Co1 C2' C3' -56.9(3) . .
C1' Co1 C2' C3' -117.6(2) . .
C3 Co1 C2' C3' -102.3(3) . .
C5 Co1 C2' C3' -11.9(4) . .
C2 Co1 C2' C3' -148.5(9) . .
C4' Co1 C2' C3' -80.0(2) . .
C1 Co1 C2' C3' 35.8(11) . .
C5' Co1 C2' C3' -37.40(15) . .
P3 Co1 C2' C3' 99.8(5) . .
P1 Co1 C2' C3' -165.6(5) . .
C3' C2' C1' C4' 0.0 . .
Co1 C2' C1' C4' -62.0(4) . .
C3' C2' C1' Co1 62.0(4) . .
C5' C4' C1' C2' 0.0 . .
Co1 C4' C1' C2' 60.4(4) . .
C5' C4' C1' Co1 -60.4(4) . .
C4 Co1 C1' C2' -95.0(3) . .
C3 Co1 C1' C2' -133.6(11) . .
C3' Co1 C1' C2' -38.15(15) . .
C5 Co1 C1' C2' -52.5(3) . .
C2 Co1 C1' C2' 27.5(9) . .
C4' Co1 C1' C2' -118.0(2) . .
C1 Co1 C1' C2' -9.7(4) . .
C5' Co1 C1' C2' -81.0(3) . .
P3 Co1 C1' C2' 47.5(5) . .
P1 Co1 C1' C2' 140.2(5) . .
C2' Co1 C1' C4' 118.0(2) . .
C4 Co1 C1' C4' 23.0(4) . .
C3 Co1 C1' C4' -15.6(11) . .
C3' Co1 C1' C4' 79.8(2) . .
C5 Co1 C1' C4' 65.5(3) . .
C2 Co1 C1' C4' 145.5(8) . .
C1 Co1 C1' C4' 108.3(3) . .
C5' Co1 C1' C4' 36.96(15) . .
P3 Co1 C1' C4' 165.5(5) . .
P1 Co1 C1' C4' -101.8(5) . .
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.668 0.195 0.364 148 39 ' '
2 0.669 0.305 0.864 148 39 ' '
3 0.331 0.695 0.136 148 39 ' '
4 0.331 0.805 0.636 148 39 ' '
