#------------------------------------------------------------------------------
#$Date: 2015-12-09 15:43:08 +0200 (Wed, 09 Dec 2015) $
#$Revision: 171134 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/70/7037050.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7037050
loop_
_publ_author_name
'Duval, Sylvain'
'Sobanska, Sophie'
'Roussel, Pascal'
'Loiseau, Thierry'
_publ_section_title
;
 B-α-[AsW9O33](9-) polyoxometalates incorporating hexanuclear uranium
 {U6O8}-like clusters bearing the U(IV) form or unprecedented mixed
 valence U(IV)/U(VI) involving direct U(VI)[double bond, length as
 m-dash]O-U(IV) bonding.
;
_journal_issue                   46
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              19772
_journal_page_last               19776
_journal_paper_doi               10.1039/c5dt02932e
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         '0.5(As6 Na30 O325.5 U12 W54), 6.25(O)'
_chemical_formula_sum            'As3 Na15 O169 U6 W27'
_chemical_formula_weight         9665.74
_space_group_crystal_system      monoclinic
_space_group_IT_number           11
_space_group_name_Hall           '-P 2yb'
_space_group_name_H-M_alt        'P 1 21/m 1'
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_atom_sites_solution_primary     iterative
_audit_creation_date             2015-09-11
_audit_creation_method
;
Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
;
_audit_update_record
;
2015-10-09 deposited with the CCDC.
2015-10-21 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 91.543(3)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   13.7846(8)
_cell_length_b                   31.0033(14)
_cell_length_c                   17.7568(8)
_cell_measurement_reflns_used    9713
_cell_measurement_temperature    100
_cell_measurement_theta_max      29.09
_cell_measurement_theta_min      2.27
_cell_volume                     7585.9(7)
_computing_data_collection       'Bruker APEX2'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'olex2.solve (Bourhis et al., 2015)'
_diffrn_ambient_temperature      100.03
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0625
_diffrn_reflns_av_unetI/netI     0.0395
_diffrn_reflns_laue_measured_fraction_full 1.000
_diffrn_reflns_laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       42
_diffrn_reflns_limit_k_min       -42
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            254548
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         29.179
_diffrn_reflns_theta_min         1.314
_exptl_absorpt_coefficient_mu    27.575
_exptl_absorpt_correction_T_max  0.3363
_exptl_absorpt_correction_T_min  0.1243
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'SADABS 'numercal''
_exptl_crystal_colour            'clear dark brown'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   dark
_exptl_crystal_colour_primary    brown
_exptl_crystal_density_diffrn    4.232
_exptl_crystal_description       block
_exptl_crystal_F_000             8332
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.494
_refine_diff_density_min         -2.468
_refine_diff_density_rms         0.365
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.066
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     996
_refine_ls_number_reflns         20819
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.066
_refine_ls_R_factor_all          0.0696
_refine_ls_R_factor_gt           0.0380
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0298P)²+173.2665P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0798
_refine_ls_wR_factor_ref         0.0934
_reflns_Friedel_coverage         0.000
_reflns_number_gt                15162
_reflns_number_total             20819
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c5dt02932e2.cif
_cod_data_source_block           sd162
_cod_depositor_comments
'Adding full bibliography for 7037049--7037051.cif.'
_cod_database_code               7037050
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_olex2_refinement_description
;
1. Uiso/Uaniso restraints and constraints
Uanis(Na6B) \\sim Ueq: with sigma of 0.1 and sigma for terminal atoms of 0.2
2. Others
 Sof(Na0A)=Sof(OW10)=Sof(O1A)=Sof(O1C)=1-FVAR(1)
 Sof(O1B)=0.5*(1-FVAR(2))
 Sof(OW61)=0.5*FVAR(2)
 Sof(Na1)=Sof(OW64)=Sof(OW62)=Sof(OW63)=FVAR(1)
 Fixed Sof: OW89(0.75) OW94(0.5) OW95(0.75) Na2(0.5) Na6B(0.5) OW78(0.375)
 OW82(0.5) OW97(0.25) OW69(0.7) NaW7(0.5) Na9(0.5) OW79(0.25) OW71(0.25)
 OW73(0.125) OW91(0.5) OW68(0.5) OW80(0.5) OW92(0.25) OW76(0.125) O4AA(0.5)
 O1D(0.3) O1E(0.25) O1F(0.25) O8AA(0.5) O6AA(0.25) O7AA(0.25) O1G(0.25)
 O0BA(0.125) O1H(0.25) O9AA(0.25) O1BA(0.25) O3BA(0.25) O2BA(0.25) O4BA(0.125)
 O1I(0.125) O6BA(0.25) O5BA(0.25)
;
_shelx_shelxl_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z'
'-x, -y, -z'
'x, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
U1 U 0.23747(4) 0.2500 0.72304(3) 0.01735(11) Uani 1 2 d S T P . .
U2 U 0.19773(3) 0.31441(2) 0.91541(2) 0.01862(8) Uani 1 1 d . . . . .
U3 U 0.44462(3) 0.31138(2) 0.82205(2) 0.02028(8) Uani 1 1 d . . . . .
U4 U 0.40817(4) 0.2500 1.00453(3) 0.02155(12) Uani 1 2 d S T P . .
W13 W 0.35364(4) 0.19066(2) 1.20060(2) 0.02399(10) Uani 1 1 d . . . . .
W5 W 0.46880(4) 0.38261(2) 0.63360(2) 0.02518(10) Uani 1 1 d . . . . .
W10 W 0.13866(4) 0.18995(2) 1.29017(2) 0.02330(10) Uani 1 1 d . . . . .
W4 W 0.28248(3) 0.33097(2) 0.54917(2) 0.02211(10) Uani 1 1 d . . . . .
W7 W 0.21154(3) 0.44344(2) 0.88348(2) 0.02162(9) Uani 1 1 d . . . . .
W12 W -0.04116(4) 0.30395(2) 1.04141(2) 0.02622(10) Uani 1 1 d . . . . .
W11 W -0.07015(5) 0.2500 1.20525(3) 0.02601(14) Uani 1 2 d S T P . .
W2 W 0.25200(4) 0.50055(2) 0.72524(2) 0.02665(11) Uani 1 1 d . . . . .
W14 W 0.16414(4) 0.36239(2) 1.12441(2) 0.02515(10) Uani 1 1 d . . . . .
W6 W 0.43224(4) 0.44153(2) 0.80974(3) 0.02569(10) Uani 1 1 d . . . . .
W9 W 0.04239(3) 0.33386(2) 0.63147(2) 0.02284(9) Uani 1 1 d . . . . .
W8 W 0.00794(3) 0.38740(2) 0.79210(2) 0.02222(9) Uani 1 1 d . . . . .
W1 W 0.28996(4) 0.44083(2) 0.54749(2) 0.02770(11) Uani 1 1 d . . . . .
W3 W 0.04509(4) 0.44331(2) 0.63083(2) 0.02657(10) Uani 1 1 d . . . . .
As2 As 0.16829(11) 0.2500 1.10787(8) 0.0169(3) Uani 1 2 d S T P . .
As1 As 0.24546(8) 0.37902(3) 0.72536(5) 0.0163(2) Uani 1 1 d . . . . .
O51 O 0.0353(6) 0.3425(2) 1.1017(4) 0.0281(18) Uani 1 1 d . . . . .
O48 O 0.2766(6) 0.1825(2) 1.2935(4) 0.0282(18) Uani 1 1 d . . . . .
O31 O 0.1457(6) 0.3385(2) 0.5616(4) 0.0266(17) Uani 1 1 d . . . . .
O29 O 0.0881(6) 0.4315(2) 0.8373(4) 0.0241(16) Uani 1 1 d . . . . .
O35 O 0.3000(6) 0.3872(2) 0.6359(4) 0.0244(17) Uani 1 1 d . . . . .
O12 O 0.2970(6) 0.4797(2) 0.6298(4) 0.0318(19) Uani 1 1 d . . . . .
O18 O -0.0003(6) 0.3912(2) 0.5876(4) 0.0287(18) Uani 1 1 d . . . . .
O24 O -0.0397(7) 0.3022(3) 0.5827(5) 0.036(2) Uani 1 1 d . . . . .
O30 O -0.0401(6) 0.3491(2) 0.7144(4) 0.0272(17) Uani 1 1 d . . . . .
O15 O 0.3828(6) 0.4965(2) 0.7637(4) 0.0277(17) Uani 1 1 d . . . . .
O58 O 0.2050(6) 0.3412(2) 1.0362(4) 0.0275(18) Uani 1 1 d . . . . .
O41 O 0.4601(5) 0.3414(2) 0.7055(4) 0.0230(16) Uani 1 1 d . . . . .
O9 O 0.2966(7) 0.4757(2) 0.4707(4) 0.042(2) Uani 1 1 d . . . . .
O17 O -0.0282(6) 0.4345(2) 0.7175(4) 0.0314(19) Uani 1 1 d . . . . .
O32 O 0.4211(6) 0.3431(2) 0.5567(4) 0.0285(18) Uani 1 1 d . . . . .
O59 O 0.0389(8) 0.2500 1.1105(6) 0.024(2) Uani 1 2 d S T P . .
O7 O 0.2988(5) 0.3005(2) 0.8125(4) 0.0209(15) Uani 1 1 d . . . . .
O19 O 0.2731(6) 0.3877(2) 0.4939(4) 0.0301(19) Uani 1 1 d . . . . .
O13 O 0.1275(6) 0.4814(2) 0.6875(4) 0.0273(17) Uani 1 1 d . . . . .
O47 O -0.1137(6) 0.2929(2) 1.1367(4) 0.0287(18) Uani 1 1 d . . . . .
O45 O 0.0146(6) 0.2084(2) 1.2534(4) 0.0266(17) Uani 1 1 d . . . . .
O27 O 0.4669(6) 0.4268(2) 0.7085(4) 0.0269(17) Uani 1 1 d . . . . .
O25 O 0.2852(6) 0.2970(2) 0.4724(4) 0.0303(19) Uani 1 1 d . . . . .
O26 O 0.5893(7) 0.3829(3) 0.6109(5) 0.039(2) Uani 1 1 d . . . . .
O20 O 0.4249(6) 0.4289(2) 0.5614(4) 0.0301(18) Uani 1 1 d . . . . .
O14 O 0.1532(6) 0.4395(2) 0.5633(4) 0.0312(19) Uani 1 1 d . . . . .
O21 O 0.5418(6) 0.4606(3) 0.8459(5) 0.037(2) Uani 1 1 d . . . . .
O6 O 0.3821(6) 0.3198(2) 0.9466(4) 0.0231(16) Uani 1 1 d . . . . .
O56 O 0.0548(6) 0.2991(2) 0.9747(4) 0.0268(17) Uani 1 1 d . . . . .
O16 O 0.2067(6) 0.4993(2) 0.8248(4) 0.0274(18) Uani 1 1 d . . . . .
O52 O 0.2957(6) 0.1369(2) 1.1675(4) 0.0294(18) Uani 1 1 d . . . . .
O44 O 0.1257(6) 0.1386(2) 1.2333(4) 0.0275(18) Uani 1 1 d . . . . .
O11 O -0.0294(7) 0.4797(3) 0.5837(4) 0.037(2) Uani 1 1 d . . . . .
O57 O 0.1515(7) 0.4170(2) 1.1103(4) 0.037(2) Uani 1 1 d . . . . .
O39 O 0.1138(5) 0.2967(2) 0.6897(4) 0.0225(16) Uani 1 1 d . . . . .
O38 O 0.0825(6) 0.3462(2) 0.8363(4) 0.0221(16) Uani 1 1 d . . . . .
O28 O 0.3508(6) 0.4561(2) 0.8931(4) 0.0279(18) Uani 1 1 d . . . . .
O10 O 0.2453(7) 0.5548(2) 0.7069(4) 0.040(2) Uani 1 1 d . . . . .
O55 O 0.3772(6) 0.2064(2) 1.1045(4) 0.0260(17) Uani 1 1 d . . . . .
O40 O 0.2887(5) 0.2958(2) 0.6308(4) 0.0200(15) Uani 1 1 d . . . . .
O36 O 0.4320(6) 0.3851(2) 0.8355(4) 0.0248(16) Uani 1 1 d . . . . .
O37 O 0.2328(5) 0.3870(2) 0.9012(4) 0.0204(15) Uani 1 1 d . . . . .
O34 O 0.1223(5) 0.3890(2) 0.6971(4) 0.0214(15) Uani 1 1 d . . . . .
O22 O 0.1782(6) 0.4647(2) 0.9683(4) 0.0309(19) Uani 1 1 d . . . . .
O33 O 0.2726(5) 0.43069(19) 0.7659(4) 0.0207(16) Uani 1 1 d . . . . .
O42 O 0.1110(6) 0.1696(2) 1.3768(4) 0.0298(18) Uani 1 1 d . . . . .
O5 O 0.2683(7) 0.2500 0.9622(5) 0.019(2) Uani 1 2 d S T P . .
O4 O 0.4234(8) 0.2500 0.7393(5) 0.022(2) Uani 1 2 d S T P . .
O60 O 0.1913(6) 0.2937(2) 1.1721(4) 0.0221(16) Uani 1 1 d . . . . .
O49 O -0.1224(7) 0.3387(3) 0.9995(5) 0.040(2) Uani 1 1 d . . . . .
O3 O 0.4581(8) 0.2500 0.8868(6) 0.025(2) Uani 1 2 d S T P . .
O23 O -0.0932(6) 0.3907(2) 0.8473(4) 0.0297(18) Uani 1 1 d . . . . .
O8 O 0.1438(8) 0.2500 0.8418(5) 0.021(2) Uani 1 2 d S T P . .
O54 O 0.4632(6) 0.1710(3) 1.2354(5) 0.0344(19) Uani 1 1 d . . . . .
O46 O 0.1624(8) 0.2500 1.3131(5) 0.022(2) Uani 1 2 d S T P . .
O50 O -0.0998(8) 0.2500 1.0100(6) 0.032(3) Uani 1 2 d S T P . .
O53 O 0.3604(8) 0.2500 1.2316(6) 0.026(2) Uani 1 2 d S T P . .
O2 O 0.5776(7) 0.3178(3) 0.8388(6) 0.046(2) Uani 1 1 d . . . . .
O1 O 0.5391(10) 0.2500 1.0361(8) 0.055(4) Uani 1 2 d S T P . .
Na3 Na 0.3234(5) 0.2500 0.3728(3) 0.0242(13) Uani 1 2 d S T P . .
Na10 Na 0.0945(4) 0.11100(16) 1.4595(3) 0.0461(14) Uani 1 1 d . . . . .
Na8 Na -0.4093(5) 0.4073(2) 1.0555(4) 0.0650(18) Uani 1 1 d . . . . .
Na7 Na -0.1764(5) 0.4098(2) 0.9647(4) 0.0669(18) Uani 1 1 d . . . . .
OW87 O -0.5844(8) 0.3958(3) 1.0254(6) 0.054(3) Uiso 1 1 d . . . . .
OW85 O -0.2355(8) 0.4244(3) 1.0886(6) 0.056(3) Uiso 1 1 d . . . . .
OW86 O -0.4097(8) 0.4791(4) 1.0112(6) 0.063(3) Uiso 1 1 d . . . . .
OW90 O -0.2003(10) 0.3637(5) 1.1982(8) 0.088(4) Uiso 1 1 d . . . . .
OW70 O 0.4927(12) 0.2500 0.3766(9) 0.062(4) Uiso 1 2 d S T P . .
OW89 O -0.4544(13) 0.4255(6) 1.1827(10) 0.078(5) Uiso 0.75 1 d . . . . .
OW94 O 0.1241(13) 0.0554(5) 1.3687(10) 0.037(4) Uiso 0.5 1 d . . . . .
OW81 O -0.0377(11) 0.4496(5) 0.9972(8) 0.095(4) Uiso 1 1 d . . . . .
Na4 Na -0.0829(8) 0.2500 0.4906(5) 0.072(3) Uani 1 2 d S T P . .
OW75 O -0.1202(11) 0.1928(5) 0.3994(8) 0.091(4) Uiso 1 1 d . . . . .
OW74 O 0.0834(11) 0.2500 0.4738(8) 0.051(4) Uiso 1 2 d S T P . .
Na1 Na 0.2912(14) 0.4674(4) 0.3285(8) 0.048(4) Uani 0.56(2) 1 d . . . A 1
OW43 O -0.1641(9) 0.2500 1.2677(6) 0.035(3) Uani 1 2 d S T P . .
OW95 O -0.0685(11) 0.1101(5) 1.4034(9) 0.064(4) Uiso 0.75 1 d . . . . .
OW83 O -0.2331(15) 0.4768(7) 0.8997(11) 0.144(7) Uiso 1 1 d . . . . .
OW88 O -0.3987(16) 0.3368(7) 1.1031(12) 0.156(8) Uiso 1 1 d . . . . .
OW64 O 0.3374(13) 0.3944(4) 0.3531(8) 0.026(4) Uiso 0.56(2) 1 d . . . A 1
OW62 O 0.3276(19) 0.4548(7) 0.1969(13) 0.064(6) Uiso 0.56(2) 1 d . . . A 1
OW63 O 0.4384(17) 0.5010(6) 0.3575(11) 0.059(6) Uiso 0.56(2) 1 d . . . A 1
OW61 O 0.228(2) 0.5397(9) 0.3185(16) 0.034(7) Uiso 0.281(11) 1 d . . . A 1
OW84 O -0.3375(15) 0.3799(6) 0.9414(11) 0.139(7) Uiso 1 1 d . . . . .
OW72 O 0.8145(12) 0.1972(5) 0.8475(9) 0.109(5) Uiso 1 1 d . . . . .
Na2 Na 0.6979(11) 0.4430(5) 0.5557(9) 0.082(5) Uani 0.5 1 d . . . . .
Na6B Na 0.0998(13) 0.4855(3) 1.0754(8) 0.094(6) Uani 0.5 1 d . U . . .
OW96 O 0.0378(10) 0.5908(4) 0.7440(7) 0.078(4) Uiso 1 1 d . . . . .
Na5 Na 0.6872(11) 0.2500 0.8461(10) 0.122(5) Uani 1 2 d S T P . .
OW93 O -0.4707(13) 0.3832(5) 1.3368(10) 0.113(5) Uiso 1 1 d . . . . .
OW78 O -0.0468(15) 0.2500 0.7753(11) 0.053(5) Uiso 0.75 2 d S T P . .
OW82 O 0.009(2) 0.4838(11) 1.1685(18) 0.078(10) Uiso 0.5 1 d . . . . .
OW97 O 0.499(5) 0.2500 0.597(4) 0.11(3) Uiso 0.5 2 d S T P . .
OW67 O 0.8335(14) 0.4534(6) 0.4727(10) 0.126(6) Uiso 1 1 d . . . . .
OW69 O -0.4604(12) 0.3279(5) 0.4370(9) 0.065(4) Uiso 0.7 1 d . . . . .
NaW7 Na -0.2873(12) 0.3249(6) 0.4395(15) 0.126(8) Uani 0.5 1 d . . . . .
OW66 O 0.5606(15) 0.4464(7) 0.4588(12) 0.147(7) Uiso 1 1 d . . . . .
Na9 Na -0.3710(11) 0.3564(6) 1.2281(12) 0.104(6) Uani 0.5 1 d . . . . .
OW79 O -0.230(3) 0.3344(14) 0.698(2) 0.060(11) Uiso 0.25 1 d . . . . .
OW71 O 0.682(3) 0.2500 0.7090(19) 0.071(9) Uiso 0.5 2 d S T P . .
OW73 O 0.698(10) 0.2500 0.963(8) 0.16(5) Uiso 0.25 2 d S T P . .
OW91 O -0.375(3) 0.2682(14) 1.254(2) 0.178(19) Uiso 0.5 1 d . . . . .
OW68 O 0.791(2) 0.3794(11) 0.5727(19) 0.109(10) Uiso 0.5 1 d . . . . .
OW80 O -0.307(2) 0.4032(9) 0.7804(16) 0.089(8) Uiso 0.5 1 d . . . . .
OW92 O -0.311(3) 0.3637(12) 1.331(2) 0.040(8) Uiso 0.25 1 d . . . . .
OW76 O -0.257(6) 0.2500 0.521(5) 0.07(2) Uiso 0.25 2 d S T P . .
Na0A Na 0.347(2) 0.4587(8) 0.3413(13) 0.075(7) Uani 0.44(2) 1 d . . . A 2
OW10 O 0.5056(18) 0.4927(7) 0.3628(12) 0.042(6) Uiso 0.44(2) 1 d . . . A 2
O1A O 0.3845(18) 0.3869(6) 0.3652(11) 0.031(5) Uiso 0.44(2) 1 d . . . A 2
O1B O 0.306(5) 0.5371(18) 0.317(3) 0.072(16) Uiso 0.219(11) 1 d . . . A 2
O1C O 0.369(2) 0.4465(9) 0.2126(16) 0.061(8) Uiso 0.44(2) 1 d . . . A 2
O4AA O 0.148(3) 0.5044(12) 0.235(2) 0.126(12) Uiso 0.5 1 d . . . . .
O1D O -0.444(2) 0.2960(11) 0.4916(19) 0.051(8) Uiso 0.3 1 d . . . . .
O1E O -0.278(3) 0.4015(15) 0.422(2) 0.062(12) Uiso 0.25 1 d . . . . .
O1F O -0.030(3) 0.0715(11) 1.4129(19) 0.036(8) Uiso 0.25 1 d . . . . .
O8AA O 0.856(3) 0.3884(11) 0.503(2) 0.118(11) Uiso 0.5 1 d . . . . .
O6AA O 0.703(3) 0.2802(14) 0.975(2) 0.053(10) Uiso 0.25 1 d . . . . .
O7AA O -0.468(3) 0.4214(12) 1.231(2) 0.042(9) Uiso 0.25 1 d . . . . .
O1G O 0.182(2) 0.0671(9) 1.3417(17) 0.026(6) Uiso 0.25 1 d . . . . .
O0BA O -0.219(10) 0.2500 0.547(8) 0.15(5) Uiso 0.25 2 d S T P . .
O1H O 0.145(5) 0.057(2) 1.299(4) 0.100(19) Uiso 0.25 1 d . . . . .
O9AA O -0.027(3) 0.4683(13) 1.144(2) 0.047(10) Uiso 0.25 1 d . . . . .
O1BA O 0.004(3) 0.4892(12) 1.195(2) 0.027(8) Uiso 0.25 1 d . . . . .
O3BA O -0.280(4) 0.3524(17) 0.739(3) 0.078(14) Uiso 0.25 1 d . . . . .
O2BA O 0.525(4) 0.2500 0.608(3) 0.080(18) Uiso 0.5 2 d S T P . .
O4BA O -0.044(5) 0.2500 0.836(4) 0.059(16) Uiso 0.25 2 d S T P . .
O1I O -0.154(5) 0.2500 0.698(4) 0.065(17) Uiso 0.25 2 d S T P . .
O6BA O -0.328(5) 0.332(2) 1.298(3) 0.097(18) Uiso 0.25 1 d . . . . .
O5BA O -0.252(6) 0.338(3) 0.549(4) 0.13(2) Uiso 0.25 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
U2 U1 U2 59.779(12) 4_565 .
U3 U1 U2 58.474(10) . .
U3 U1 U2 88.484(14) . 4_565
U3 U1 U2 88.485(14) 4_565 .
U3 U1 U2 58.474(10) 4_565 4_565
U3 U1 U3 59.749(14) 4_565 .
O7 U1 U2 32.20(17) . .
O7 U1 U2 32.21(17) 4_565 4_565
O7 U1 U2 79.17(16) . 4_565
O7 U1 U2 79.17(16) 4_565 .
O7 U1 U3 76.81(17) . 4_565
O7 U1 U3 76.80(17) 4_565 .
O7 U1 U3 27.60(17) . .
O7 U1 U3 27.60(17) 4_565 4_565
O7 U1 O7 82.7(3) 4_565 .
O7 U1 O4 65.7(2) 4_565 .
O7 U1 O4 65.7(2) . .
O7 U1 O8 67.5(2) 4_565 .
O7 U1 O8 67.5(2) . .
O39 U1 U2 114.55(17) . 4_565
O39 U1 U2 77.77(17) 4_565 4_565
O39 U1 U2 77.77(17) . .
O39 U1 U2 114.55(17) 4_565 .
O39 U1 U3 110.11(17) 4_565 4_565
O39 U1 U3 166.11(17) . 4_565
O39 U1 U3 166.11(17) 4_565 .
O39 U1 U3 110.11(18) . .
O39 U1 O7 90.3(2) . .
O39 U1 O7 90.3(2) 4_565 4_565
O39 U1 O7 146.7(2) . 4_565
O39 U1 O7 146.7(2) 4_565 .
O39 U1 O39 78.0(4) 4_565 .
O39 U1 O4 139.25(18) . .
O39 U1 O4 139.25(18) 4_565 .
O39 U1 O8 79.7(3) . .
O39 U1 O8 79.7(3) 4_565 .
O40 U1 U2 110.65(16) 4_565 4_565
O40 U1 U2 165.75(18) . 4_565
O40 U1 U2 110.65(16) . .
O40 U1 U2 165.75(18) 4_565 .
O40 U1 U3 113.35(19) . 4_565
O40 U1 U3 77.29(18) . .
O40 U1 U3 113.35(19) 4_565 .
O40 U1 U3 77.29(18) 4_565 4_565
O40 U1 O7 87.7(2) 4_565 4_565
O40 U1 O7 140.9(3) . 4_565
O40 U1 O7 140.9(3) 4_565 .
O40 U1 O7 87.7(2) . .
O40 U1 O39 70.5(2) . .
O40 U1 O39 70.6(3) 4_565 4_565
O40 U1 O39 116.5(2) 4_565 .
O40 U1 O39 116.5(2) . 4_565
O40 U1 O40 76.4(3) . 4_565
O40 U1 O4 75.8(2) . .
O40 U1 O4 75.8(2) 4_565 .
O40 U1 O8 141.08(17) . .
O40 U1 O8 141.08(17) 4_565 .
O4 U1 U2 93.63(18) . .
O4 U1 U2 93.62(18) . 4_565
O4 U1 U3 38.56(13) . .
O4 U1 U3 38.56(13) . 4_565
O8 U1 U2 36.50(14) . .
O8 U1 U2 36.49(14) . 4_565
O8 U1 U3 90.5(2) . 4_565
O8 U1 U3 90.5(2) . .
O8 U1 O4 116.2(3) . .
U2 U2 U1 60.110(6) 4_565 .
U3 U2 U1 58.324(11) . .
U3 U2 U2 88.594(7) . 4_565
U3 U2 U4 59.570(12) . .
U4 U2 U1 88.453(13) . .
U4 U2 U2 58.564(8) . 4_565
O58 U2 U1 166.3(2) . .
O58 U2 U2 111.15(17) . 4_565
O58 U2 U3 113.3(2) . .
O58 U2 U4 77.81(19) . .
O58 U2 O7 140.7(3) . .
O58 U2 O6 76.1(3) . .
O58 U2 O56 70.4(3) . .
O58 U2 O38 115.2(3) . .
O58 U2 O37 75.3(2) . .
O58 U2 O5 88.3(3) . .
O58 U2 O8 141.7(3) . .
O7 U2 U1 32.25(18) . .
O7 U2 U2 79.49(16) . 4_565
O7 U2 U3 27.42(18) . .
O7 U2 U4 76.63(17) . .
O7 U2 O6 65.3(2) . .
O7 U2 O8 67.8(3) . .
O6 U2 U1 93.35(15) . .
O6 U2 U2 93.67(14) . 4_565
O6 U2 U3 38.36(15) . .
O6 U2 U4 38.50(14) . .
O56 U2 U1 115.14(18) . .
O56 U2 U2 78.16(17) . 4_565
O56 U2 U3 166.59(18) . .
O56 U2 U4 110.54(19) . .
O56 U2 O7 147.4(3) . .
O56 U2 O6 139.4(2) . .
O56 U2 O38 77.5(3) . .
O56 U2 O37 115.6(2) . .
O56 U2 O5 90.8(3) . .
O56 U2 O8 80.1(3) . .
O38 U2 U1 78.56(16) . .
O38 U2 U2 115.20(16) . 4_565
O38 U2 U3 110.60(17) . .
O38 U2 U4 166.83(17) . .
O38 U2 O7 91.0(2) . .
O38 U2 O6 139.1(2) . .
O38 U2 O37 70.3(2) . .
O38 U2 O5 147.5(3) . .
O38 U2 O8 80.3(3) . .
O37 U2 U1 110.95(16) . .
O37 U2 U2 166.25(17) . 4_565
O37 U2 U3 77.66(17) . .
O37 U2 U4 113.19(18) . .
O37 U2 O7 88.0(2) . .
O37 U2 O6 75.8(2) . .
O37 U2 O5 140.7(3) . .
O37 U2 O8 141.5(3) . .
O5 U2 U1 79.3(2) . .
O5 U2 U2 32.3(2) . 4_565
O5 U2 U3 76.6(2) . .
O5 U2 U4 27.6(2) . .
O5 U2 O7 82.6(3) . .
O5 U2 O6 65.6(3) . .
O5 U2 O8 67.7(3) . .
O8 U2 U1 36.7(2) . .
O8 U2 U2 36.7(2) . 4_565
O8 U2 U3 90.5(2) . .
O8 U2 U4 90.6(2) . .
O8 U2 O6 116.2(3) . .
U1 U3 U2 63.202(12) . .
U1 U3 Na5 116.09(13) . .
U2 U3 Na5 137.9(2) . .
U3 U3 U1 60.125(7) 4_565 .
U3 U3 U2 91.406(7) 4_565 .
U3 U3 Na5 60.48(11) 4_565 .
U4 U3 U1 91.640(13) . .
U4 U3 U2 60.244(12) . .
U4 U3 U3 59.972(7) . 4_565
U4 U3 Na5 78.1(2) . .
O41 U3 U1 82.72(19) . .
O41 U3 U2 119.22(19) . .
O41 U3 U3 114.08(16) . 4_565
O41 U3 U4 173.51(17) . .
O41 U3 O6 146.3(2) . .
O41 U3 O36 72.4(2) . .
O41 U3 O4 77.5(2) . .
O41 U3 Na5 101.5(3) . .
O7 U3 U1 32.55(18) . .
O7 U3 U2 32.28(18) . .
O7 U3 U3 80.47(18) . 4_565
O7 U3 U4 80.53(18) . .
O7 U3 O41 96.2(3) . .
O7 U3 O6 73.6(3) . .
O7 U3 O36 95.5(3) . .
O7 U3 O4 73.5(3) . .
O7 U3 O3 88.3(3) . .
O7 U3 Na5 140.9(2) . .
O6 U3 U1 101.24(18) . .
O6 U3 U2 41.89(19) . .
O6 U3 U3 96.19(15) . 4_565
O6 U3 U4 38.09(16) . .
O6 U3 O4 127.1(3) . .
O6 U3 Na5 106.4(3) . .
O36 U3 U1 118.9(2) . .
O36 U3 U2 81.98(18) . .
O36 U3 U3 172.55(17) . 4_565
O36 U3 U4 113.33(18) . .
O36 U3 O6 76.6(2) . .
O36 U3 O4 146.6(3) . .
O36 U3 Na5 123.0(2) . .
O4 U3 U1 41.5(3) . .
O4 U3 U2 100.9(2) . .
O4 U3 U3 38.08(19) . 4_565
O4 U3 U4 96.18(18) . .
O4 U3 Na5 76.7(3) . .
O3 U3 U1 82.1(3) . .
O3 U3 U2 82.0(3) . .
O3 U3 U3 31.4(2) . 4_565
O3 U3 U4 31.1(2) . .
O3 U3 O41 143.8(3) . .
O3 U3 O6 69.2(3) . .
O3 U3 O36 143.0(3) . .
O3 U3 O4 69.4(3) . .
O3 U3 Na5 57.5(3) . .
O2 U3 U1 148.1(3) . .
O2 U3 U2 144.3(3) . .
O2 U3 U3 96.2(3) . 4_565
O2 U3 U4 94.0(3) . .
O2 U3 O41 89.2(3) . .
O2 U3 O7 174.5(3) . .
O2 U3 O6 102.5(4) . .
O2 U3 O36 87.3(3) . .
O2 U3 O4 106.5(4) . .
O2 U3 O3 86.6(4) . .
O2 U3 Na5 35.8(3) . .
U2 U4 U2 62.870(15) 4_565 .
U3 U4 U2 60.186(11) . .
U3 U4 U2 91.420(15) . 4_565
U3 U4 U2 91.420(15) 4_565 .
U3 U4 U2 60.187(11) 4_565 4_565
U3 U4 U3 60.055(14) 4_565 .
O6 U4 U2 100.87(18) 4_565 .
O6 U4 U2 41.87(18) . .
O6 U4 U2 41.88(18) 4_565 4_565
O6 U4 U2 100.87(18) . 4_565
O6 U4 U3 96.14(16) . 4_565
O6 U4 U3 37.95(16) . .
O6 U4 U3 37.95(16) 4_565 4_565
O6 U4 U3 96.14(16) 4_565 .
O6 U4 O6 126.9(3) . 4_565
O55 U4 U2 81.8(2) . 4_565
O55 U4 U2 118.4(2) . .
O55 U4 U2 118.4(2) 4_565 4_565
O55 U4 U2 81.78(19) 4_565 .
O55 U4 U3 172.58(18) 4_565 4_565
O55 U4 U3 113.48(17) . 4_565
O55 U4 U3 113.48(17) 4_565 .
O55 U4 U3 172.57(18) . .
O55 U4 O6 76.8(2) . 4_565
O55 U4 O6 76.8(2) 4_565 .
O55 U4 O6 146.4(2) . .
O55 U4 O6 146.4(2) 4_565 4_565
O55 U4 O55 72.7(3) 4_565 .
O5 U4 U2 32.22(5) . 4_565
O5 U4 U2 32.22(5) . .
O5 U4 U3 80.3(2) . .
O5 U4 U3 80.3(2) . 4_565
O5 U4 O6 73.5(2) . 4_565
O5 U4 O6 73.5(2) . .
O5 U4 O55 95.2(3) . .
O5 U4 O55 95.2(3) . 4_565
O5 U4 O3 88.1(4) . .
O3 U4 U2 82.0(2) . .
O3 U4 U2 82.0(2) . 4_565
O3 U4 U3 31.31(8) . 4_565
O3 U4 U3 31.31(8) . .
O3 U4 O6 69.24(18) . 4_565
O3 U4 O6 69.24(18) . .
O3 U4 O55 143.40(18) . .
O3 U4 O55 143.40(18) . 4_565
O1 U4 U2 146.71(13) . .
O1 U4 U2 146.71(13) . 4_565
O1 U4 U3 96.1(4) . 4_565
O1 U4 U3 96.1(4) . .
O1 U4 O6 104.9(2) . .
O1 U4 O6 104.9(2) . 4_565
O1 U4 O55 88.1(4) . .
O1 U4 O55 88.1(4) . 4_565
O1 U4 O5 175.9(5) . .
O1 U4 O3 87.8(5) . .
O48 W13 O60 71.2(3) . 4_565
O48 W13 Na3 44.7(2) . 1_556
O52 W13 O48 85.3(3) . .
O52 W13 O60 74.1(3) . 4_565
O52 W13 Na3 130.0(2) . 1_556
O55 W13 O48 157.3(3) . .
O55 W13 O52 91.6(3) . .
O55 W13 O60 86.3(3) . 4_565
O55 W13 O53 90.2(3) . .
O55 W13 Na3 133.6(2) . 1_556
O60 W13 Na3 86.91(19) 4_565 1_556
O54 W13 O48 98.0(4) . .
O54 W13 O52 98.9(4) . .
O54 W13 O55 104.8(4) . .
O54 W13 O60 167.3(3) . 4_565
O54 W13 O53 101.5(4) . .
O54 W13 Na3 89.8(3) . 1_556
O53 W13 O48 84.7(3) . .
O53 W13 O52 158.3(4) . .
O53 W13 O60 84.4(4) . 4_565
O53 W13 Na3 43.4(3) . 1_556
O41 W5 O35 86.9(3) . .
O41 W5 O32 91.3(3) . .
O41 W5 O27 90.7(3) . .
O41 W5 O20 158.3(3) . .
O32 W5 O35 74.4(3) . .
O32 W5 O20 84.9(3) . .
O27 W5 O35 84.9(3) . .
O27 W5 O32 159.1(3) . .
O27 W5 O20 85.5(3) . .
O26 W5 O35 166.9(3) . .
O26 W5 O41 104.6(4) . .
O26 W5 O32 98.6(4) . .
O26 W5 O27 101.0(4) . .
O26 W5 O20 97.1(4) . .
O20 W5 O35 71.6(3) . .
O48 W10 O60 73.5(3) . 4_565
O48 W10 O46 87.0(4) . .
O48 W10 Na3 48.0(2) . 1_556
O45 W10 O48 158.4(3) . .
O45 W10 O60 85.6(3) . 4_565
O45 W10 O46 85.9(4) . .
O45 W10 Na3 129.1(2) . 1_556
O44 W10 O48 89.7(3) . .
O44 W10 O45 89.9(3) . .
O44 W10 O60 74.0(3) . 4_565
O44 W10 O46 159.5(3) . .
O44 W10 Na3 137.7(3) . 1_556
O42 W10 O48 99.9(4) . .
O42 W10 O45 101.5(4) . .
O42 W10 O44 98.6(3) . .
O42 W10 O60 169.9(3) . 4_565
O42 W10 O46 101.9(4) . .
O42 W10 Na3 89.8(3) . 1_556
O60 W10 Na3 91.2(2) 4_565 1_556
O46 W10 O60 85.7(3) . 4_565
O46 W10 Na3 43.2(3) . 1_556
O31 W4 O35 85.3(3) . .
O31 W4 O32 159.0(3) . .
O31 W4 O19 84.2(3) . .
O31 W4 Na10 43.3(2) . 4_564
O35 W4 Na10 88.8(2) . 4_564
O32 W4 O35 74.2(3) . .
O32 W4 O19 85.1(3) . .
O32 W4 Na10 130.1(2) . 4_564
O19 W4 O35 70.9(3) . .
O19 W4 Na10 45.1(3) . 4_564
O25 W4 O31 102.0(4) . .
O25 W4 O35 166.9(3) . .
O25 W4 O32 97.5(4) . .
O25 W4 O19 98.6(3) . .
O25 W4 O40 105.2(3) . .
O25 W4 Na10 89.2(3) . 4_564
O40 W4 O31 90.4(3) . .
O40 W4 O35 85.5(3) . .
O40 W4 O32 92.1(3) . .
O40 W4 O19 156.1(3) . .
O40 W4 Na10 133.7(3) . 4_564
O29 W7 O16 85.9(3) . .
O29 W7 O28 159.5(3) . .
O29 W7 O33 85.5(3) . .
O16 W7 O33 71.8(2) . .
O28 W7 O16 83.8(3) . .
O28 W7 O33 74.5(3) . .
O37 W7 O29 91.5(3) . .
O37 W7 O16 157.8(3) . .
O37 W7 O28 91.4(3) . .
O37 W7 O33 86.0(3) . .
O22 W7 O29 101.2(4) . .
O22 W7 O16 96.8(3) . .
O22 W7 O28 97.6(4) . .
O22 W7 O37 105.4(3) . .
O22 W7 O33 166.5(3) . .
O51 W12 O59 84.7(3) . .
O51 W12 O47 85.1(3) . .
O51 W12 O50 157.8(4) . .
O47 W12 O59 71.1(3) . .
O56 W12 O51 90.9(3) . .
O56 W12 O59 86.6(3) . .
O56 W12 O47 157.6(3) . .
O56 W12 O50 92.7(4) . .
O49 W12 O51 101.3(4) . .
O49 W12 O59 167.2(4) . .
O49 W12 O47 97.9(4) . .
O49 W12 O56 104.5(4) . .
O49 W12 O50 99.0(5) . .
O50 W12 O59 73.7(4) . .
O50 W12 O47 83.2(4) . .
O47 W11 O59 74.3(3) 4_565 .
O47 W11 O59 74.3(3) . .
O47 W11 O47 89.4(5) . 4_565
O47 W11 O45 89.6(3) 4_565 .
O47 W11 O45 89.6(3) . 4_565
O47 W11 O45 159.4(3) . .
O47 W11 O45 159.4(3) 4_565 4_565
O45 W11 O59 85.6(3) 4_565 .
O45 W11 O59 85.6(3) . .
O45 W11 O45 84.1(4) . 4_565
OW43 W11 O59 172.6(5) . .
OW43 W11 O47 100.5(4) . .
OW43 W11 O47 100.5(4) . 4_565
OW43 W11 O45 99.9(4) . .
OW43 W11 O45 99.9(4) . 4_565
O12 W2 O33 85.5(3) . .
O15 W2 O12 88.2(3) . .
O15 W2 O13 158.2(3) . .
O15 W2 O33 73.7(3) . .
O13 W2 O12 84.0(3) . .
O13 W2 O33 85.4(3) . .
O16 W2 O12 159.3(3) . .
O16 W2 O15 89.8(3) . .
O16 W2 O13 90.3(3) . .
O16 W2 O33 74.2(3) . .
O10 W2 O12 100.2(3) . .
O10 W2 O15 100.2(4) . .
O10 W2 O13 101.2(4) . .
O10 W2 O16 100.4(3) . .
O10 W2 O33 171.6(4) . .
O51 W14 O52 159.2(3) . 4_565
O51 W14 O44 86.0(3) . 4_565
O51 W14 O60 85.4(3) . .
O58 W14 O51 90.5(3) . .
O58 W14 O52 92.0(3) . 4_565
O58 W14 O44 157.3(3) . 4_565
O58 W14 O60 86.0(3) . .
O52 W14 O44 83.7(3) 4_565 4_565
O52 W14 O60 74.2(3) 4_565 .
O44 W14 O60 71.3(2) 4_565 .
O57 W14 O51 101.4(4) . .
O57 W14 O58 105.4(3) . .
O57 W14 O52 97.8(4) . 4_565
O57 W14 O44 97.3(3) . 4_565
O57 W14 O60 166.5(3) . .
O15 W6 O33 71.3(3) . .
O27 W6 O15 84.9(3) . .
O27 W6 O28 158.8(3) . .
O27 W6 O33 84.8(3) . .
O21 W6 O15 98.3(4) . .
O21 W6 O27 101.0(4) . .
O21 W6 O28 99.0(4) . .
O21 W6 O36 104.1(4) . .
O21 W6 O33 167.8(3) . .
O28 W6 O15 85.2(3) . .
O28 W6 O33 74.2(3) . .
O36 W6 O15 157.5(3) . .
O36 W6 O27 90.5(3) . .
O36 W6 O28 91.6(3) . .
O36 W6 O33 86.4(3) . .
O31 W9 O18 84.2(3) . .
O31 W9 O30 158.7(3) . .
O31 W9 O34 85.4(3) . .
O31 W9 Na10 41.0(2) . 4_564
O18 W9 O34 71.1(3) . .
O18 W9 Na10 46.9(2) . 4_564
O24 W9 O31 102.0(4) . .
O24 W9 O18 97.4(4) . .
O24 W9 O30 97.5(4) . .
O24 W9 O39 105.3(4) . .
O24 W9 O34 165.9(3) . .
O24 W9 Na10 89.3(3) . 4_564
O30 W9 O18 84.7(3) . .
O30 W9 O34 73.8(3) . .
O30 W9 Na10 131.6(2) . 4_564
O39 W9 O31 90.9(3) . .
O39 W9 O18 157.3(3) . .
O39 W9 O30 92.4(3) . .
O39 W9 O34 86.4(3) . .
O39 W9 Na10 131.9(2) . 4_564
O34 W9 Na10 88.50(19) . 4_564
O29 W8 O30 157.3(3) . .
O29 W8 O17 83.6(3) . .
O29 W8 O34 84.0(3) . .
O30 W8 O17 84.4(3) . .
O30 W8 O34 73.8(3) . .
O17 W8 O34 70.9(3) . .
O38 W8 O29 90.5(3) . .
O38 W8 O30 93.1(3) . .
O38 W8 O17 157.2(3) . .
O38 W8 O34 86.6(3) . .
O23 W8 O29 100.6(3) . .
O23 W8 O30 100.1(3) . .
O23 W8 O17 98.1(3) . .
O23 W8 O38 104.6(3) . .
O23 W8 O34 167.7(3) . .
O35 W1 Na10 90.3(2) . 4_564
O12 W1 O35 86.1(3) . .
O12 W1 O19 159.1(3) . .
O12 W1 O20 89.6(4) . .
O12 W1 O14 86.0(3) . .
O12 W1 Na10 131.6(3) . 4_564
O9 W1 O35 169.4(3) . .
O9 W1 O12 101.9(3) . .
O9 W1 O19 98.8(3) . .
O9 W1 O20 98.6(4) . .
O9 W1 O14 101.6(4) . .
O9 W1 Na10 89.5(3) . 4_564
O19 W1 O35 73.8(3) . .
O19 W1 O14 87.0(3) . .
O19 W1 Na10 45.2(3) . 4_564
O20 W1 O35 74.3(3) . .
O20 W1 O19 90.1(3) . .
O20 W1 O14 159.8(3) . .
O20 W1 Na10 135.3(2) . 4_564
O14 W1 O35 85.7(3) . .
O14 W1 Na10 45.6(2) . 4_564
O18 W3 O13 158.5(3) . .
O18 W3 O14 87.1(3) . .
O18 W3 O34 74.0(3) . .
O18 W3 Na10 46.9(3) . 4_564
O17 W3 O18 91.7(3) . .
O17 W3 O13 89.1(3) . .
O17 W3 O14 159.0(3) . .
O17 W3 O34 74.1(3) . .
O17 W3 Na10 138.5(3) . 4_564
O13 W3 O14 84.6(3) . .
O13 W3 O34 85.5(3) . .
O13 W3 Na10 128.2(2) . 4_564
O14 W3 O34 85.4(3) . .
O14 W3 Na10 43.6(3) . 4_564
O11 W3 O18 100.1(4) . .
O11 W3 O17 99.5(4) . .
O11 W3 O13 100.9(4) . .
O11 W3 O14 101.3(4) . .
O11 W3 O34 171.0(4) . .
O11 W3 Na10 91.2(3) . 4_564
O34 W3 Na10 89.67(18) . 4_564
O59 As2 O60 98.2(3) . .
O59 As2 O60 98.2(3) . 4_565
O60 As2 O60 98.1(4) . 4_565
O34 As1 O35 98.4(3) . .
O34 As1 O33 98.4(3) . .
O33 As1 O35 98.1(3) . .
W12 O51 W14 144.9(4) . .
W13 O48 Na3 102.4(3) . 1_556
W10 O48 W13 120.5(4) . .
W10 O48 Na3 98.7(3) . 1_556
W4 O31 W9 144.5(4) . .
W4 O31 Na10 104.7(3) . 4_564
W9 O31 Na10 108.6(4) . 4_564
W7 O29 W8 144.6(4) . .
W5 O35 W4 91.6(2) . .
W1 O35 W5 94.2(3) . .
W1 O35 W4 94.9(2) . .
As1 O35 W5 116.7(4) . .
As1 O35 W4 116.1(3) . .
As1 O35 W1 133.8(4) . .
W1 O12 W2 151.4(5) . .
W9 O18 Na10 99.3(3) . 4_564
W3 O18 W9 120.4(4) . .
W3 O18 Na10 101.8(3) . 4_564
W9 O24 Na4 153.0(6) . .
W8 O30 W9 119.7(4) . .
W2 O15 W6 120.5(4) . .
W14 O58 U2 159.2(5) . .
W5 O41 U3 159.3(4) . .
W1 O9 Na1 135.6(5) . .
W1 O9 Na2 138.9(6) . 3_666
W1 O9 Na0A 128.0(7) . .
Na1 O9 Na2 85.3(5) . 3_666
Na0A O9 Na2 91.7(7) . 3_666
W3 O17 W8 120.8(4) . .
W5 O32 W4 119.0(4) . .
W12 O59 W12 91.5(4) 4_565 .
W11 O59 W12 94.3(3) . .
W11 O59 W12 94.3(3) . 4_565
As2 O59 W12 116.4(3) . .
As2 O59 W12 116.4(3) . 4_565
As2 O59 W11 134.2(6) . .
U2 O7 U1 115.5(3) . .
U3 O7 U1 119.8(3) . .
U3 O7 U2 120.3(3) . .
W4 O19 Na10 100.4(3) . 4_564
W1 O19 W4 120.3(4) . .
W1 O19 Na10 102.2(3) . 4_564
W3 O13 W2 152.9(4) . .
W11 O47 W12 120.2(4) . .
W10 O45 W11 152.1(4) . .
W5 O27 W6 145.9(4) . .
W4 O25 Na3 168.3(5) . .
W5 O26 Na2 131.5(6) . .
W1 O20 W5 119.9(4) . .
W1 O14 W3 149.9(4) . .
W1 O14 Na10 101.7(3) . 4_564
W3 O14 Na10 104.6(4) . 4_564
U3 O6 U2 99.8(3) . .
U3 O6 U4 104.0(2) . .
U4 O6 U2 99.6(2) . .
W12 O56 U2 158.8(4) . .
W2 O16 W7 119.4(3) . .
W13 O52 W14 118.8(4) . 4_565
W10 O44 W14 120.1(3) . 4_565
W14 O57 Na6B 165.8(8) . .
W9 O39 U1 158.4(4) . .
W8 O38 U2 159.8(4) . .
W6 O28 W7 118.3(4) . .
W13 O55 U4 159.1(4) . .
W4 O40 U1 159.1(4) . .
W6 O36 U3 158.9(4) . .
W7 O37 U2 158.4(4) . .
W9 O34 W8 91.6(3) . .
W3 O34 W9 94.3(3) . .
W3 O34 W8 94.2(3) . .
As1 O34 W9 116.6(3) . .
As1 O34 W8 116.7(3) . .
As1 O34 W3 133.9(4) . .
W7 O22 Na6B 166.7(7) . .
W7 O33 W6 92.1(2) . .
W2 O33 W7 94.5(2) . .
W2 O33 W6 94.4(2) . .
As1 O33 W7 116.1(3) . .
As1 O33 W2 133.9(4) . .
As1 O33 W6 116.5(3) . .
W10 O42 Na10 150.7(4) . .
U2 O5 U2 115.4(4) 4_565 .
U4 O5 U2 120.2(2) . 4_565
U4 O5 U2 120.2(2) . .
U3 O4 U1 99.9(3) 4_565 .
U3 O4 U1 99.9(3) . .
U3 O4 U3 103.8(4) 4_565 .
W10 O60 W13 94.7(3) 4_565 4_565
W10 O60 W14 94.5(2) 4_565 .
W14 O60 W13 91.9(2) . 4_565
As2 O60 W13 116.6(3) . 4_565
As2 O60 W10 133.9(4) . 4_565
As2 O60 W14 116.0(3) . .
W12 O49 Na7 152.3(6) . .
U3 O3 U3 117.3(5) 4_565 .
U4 O3 U3 117.5(2) . .
U4 O3 U3 117.5(2) . 4_565
W8 O23 Na7 152.9(5) . .
U2 O8 U1 106.8(3) . .
U2 O8 U1 106.8(3) 4_565 .
U2 O8 U2 106.7(4) 4_565 .
W13 O54 Na9 155.9(7) . 4_665
W10 O46 W10 149.0(6) . 4_565
W10 O46 Na3 103.8(3) . 1_556
W10 O46 Na3 103.8(3) 4_565 1_556
W12 O50 W12 119.8(6) 4_565 .
W13 O53 W13 146.4(6) . 4_565
W13 O53 Na3 105.7(3) 4_565 1_556
W13 O53 Na3 105.7(3) . 1_556
U3 O2 Na5 119.5(5) . .
W13 Na3 W13 61.43(9) 1_554 4_564
W10 Na3 W13 90.89(14) 4_564 1_554
W10 Na3 W13 57.61(8) 1_554 1_554
W10 Na3 W13 90.89(14) 1_554 4_564
W10 Na3 W13 57.61(8) 4_564 4_564
W10 Na3 W10 65.31(12) 1_554 4_564
O48 Na3 W13 32.87(17) 1_554 1_554
O48 Na3 W13 89.1(2) 1_554 4_564
O48 Na3 W13 32.87(17) 4_564 4_564
O48 Na3 W13 89.1(2) 4_564 1_554
O48 Na3 W10 92.0(3) 1_554 4_564
O48 Na3 W10 33.26(19) 1_554 1_554
O48 Na3 W10 92.0(3) 4_564 1_554
O48 Na3 W10 33.26(19) 4_564 4_564
O48 Na3 O48 107.6(4) 1_554 4_564
O25 Na3 W13 110.70(18) . 4_564
O25 Na3 W13 169.7(3) 4_565 4_564
O25 Na3 W13 169.7(3) . 1_554
O25 Na3 W13 110.70(18) 4_565 1_554
O25 Na3 W10 118.3(3) . 1_554
O25 Na3 W10 78.9(2) 4_565 1_554
O25 Na3 W10 118.3(3) 4_565 4_564
O25 Na3 W10 78.9(2) . 4_564
O25 Na3 O48 147.9(4) . 1_554
O25 Na3 O48 81.4(2) . 4_564
O25 Na3 O48 147.9(4) 4_565 4_564
O25 Na3 O48 81.4(2) 4_565 1_554
O25 Na3 O25 76.2(4) 4_565 .
O25 Na3 O46 96.1(3) . 1_554
O25 Na3 O46 96.1(3) 4_565 1_554
O25 Na3 O53 141.61(19) 4_565 1_554
O25 Na3 O53 141.62(19) . 1_554
O46 Na3 W13 75.9(2) 1_554 1_554
O46 Na3 W13 75.9(2) 1_554 4_564
O46 Na3 W10 32.94(6) 1_554 4_564
O46 Na3 W10 32.94(6) 1_554 1_554
O46 Na3 O48 63.5(2) 1_554 4_564
O46 Na3 O48 63.5(2) 1_554 1_554
O46 Na3 O53 77.2(4) 1_554 1_554
O53 Na3 W13 30.91(5) 1_554 1_554
O53 Na3 W13 30.91(5) 1_554 4_564
O53 Na3 W10 75.5(3) 1_554 1_554
O53 Na3 W10 75.5(3) 1_554 4_564
O53 Na3 O48 61.6(2) 1_554 1_554
O53 Na3 O48 61.6(2) 1_554 4_564
OW70 Na3 W13 83.5(4) . 4_564
OW70 Na3 W13 83.5(4) . 1_554
OW70 Na3 W10 137.6(3) . 4_564
OW70 Na3 W10 137.6(3) . 1_554
OW70 Na3 O48 104.5(3) . 4_564
OW70 Na3 O48 104.5(3) . 1_554
OW70 Na3 O25 102.8(4) . .
OW70 Na3 O25 102.8(4) . 4_565
OW70 Na3 O46 155.9(5) . 1_554
OW70 Na3 O53 78.7(5) . 1_554
W4 Na10 W3 90.63(11) 4_566 4_566
W1 Na10 W4 58.51(9) 4_566 4_566
W1 Na10 W3 63.94(8) 4_566 4_566
O31 Na10 W4 32.0(2) 4_566 4_566
O31 Na10 W1 76.2(2) 4_566 4_566
O31 Na10 W3 74.4(2) 4_566 4_566
O31 Na10 O18 61.8(3) 4_566 4_566
O31 Na10 O19 63.7(3) 4_566 4_566
O31 Na10 O14 77.3(3) 4_566 4_566
O31 Na10 O1G 137.2(7) 4_566 .
O18 Na10 W4 90.0(2) 4_566 4_566
O18 Na10 W1 89.8(2) 4_566 4_566
O18 Na10 W3 31.26(17) 4_566 4_566
O18 Na10 O1G 149.4(7) 4_566 .
O19 Na10 W4 34.50(17) 4_566 4_566
O19 Na10 W1 32.58(17) 4_566 4_566
O19 Na10 W3 90.5(2) 4_566 4_566
O19 Na10 O18 107.0(3) 4_566 4_566
O19 Na10 O14 62.8(3) 4_566 4_566
O19 Na10 O1G 75.7(7) 4_566 .
O14 Na10 W4 76.7(2) 4_566 4_566
O14 Na10 W1 32.7(2) 4_566 4_566
O14 Na10 W3 31.9(2) 4_566 4_566
O14 Na10 O18 61.0(3) 4_566 4_566
O14 Na10 O1G 96.2(7) 4_566 .
O42 Na10 W4 78.7(2) . 4_566
O42 Na10 W1 123.5(3) . 4_566
O42 Na10 W3 157.5(3) . 4_566
O42 Na10 O31 86.5(3) . 4_566
O42 Na10 O18 127.8(3) . 4_566
O42 Na10 O19 91.7(3) . 4_566
O42 Na10 O14 153.9(4) . 4_566
O42 Na10 OW94 96.5(5) . .
O42 Na10 OW95 81.8(4) . .
O42 Na10 O1G 81.8(7) . .
OW94 Na10 W4 122.5(5) . 4_566
OW94 Na10 W1 80.0(5) . 4_566
OW94 Na10 W3 105.9(4) . 4_566
OW94 Na10 O31 153.2(6) . 4_566
OW94 Na10 O18 130.7(5) . 4_566
OW94 Na10 O19 89.5(5) . 4_566
OW94 Na10 O14 89.3(5) . 4_566
OW94 Na10 OW95 83.6(6) . .
OW94 Na10 O1G 20.6(7) . .
OW95 Na10 W4 148.9(4) . 4_566
OW95 Na10 W1 151.1(4) . 4_566
OW95 Na10 W3 98.5(4) . 4_566
OW95 Na10 O31 123.2(5) . 4_566
OW95 Na10 O18 83.1(4) . 4_566
OW95 Na10 O19 169.9(5) . 4_566
OW95 Na10 O14 124.3(5) . 4_566
OW95 Na10 O1G 95.7(8) . .
O1F Na10 W4 174.6(9) . 4_566
O1F Na10 W1 119.3(9) . 4_566
O1F Na10 W3 84.0(9) . 4_566
O1F Na10 O31 144.2(9) . 4_566
O1F Na10 O18 85.0(9) . 4_566
O1F Na10 O19 146.0(9) . 4_566
O1F Na10 O14 99.0(9) . 4_566
O1F Na10 O42 106.0(9) . .
O1F Na10 OW94 60.3(10) . .
O1F Na10 OW95 32.3(9) . .
O1F Na10 O1G 78.4(11) . .
O1G Na10 W4 105.2(7) . 4_566
O1G Na10 W1 76.6(7) . 4_566
O1G Na10 W3 120.4(6) . 4_566
OW87 Na8 Na7 140.7(4) . .
OW87 Na8 OW85 175.8(5) . .
OW87 Na8 Na9 104.4(4) . .
OW85 Na8 Na7 41.4(3) . .
OW85 Na8 Na9 76.5(4) . .
OW86 Na8 Na7 80.0(3) . .
OW86 Na8 OW87 94.0(4) . .
OW86 Na8 OW85 82.7(4) . .
OW86 Na8 OW89 95.3(5) . .
OW86 Na8 OW84 92.8(6) . .
OW86 Na8 Na9 136.1(5) . .
OW89 Na8 Na7 131.3(5) . .
OW89 Na8 OW87 87.8(5) . .
OW89 Na8 OW85 90.0(5) . .
OW89 Na8 OW84 167.8(7) . .
OW89 Na8 Na9 47.2(5) . .
OW88 Na8 Na7 97.7(6) . .
OW88 Na8 OW87 89.7(6) . .
OW88 Na8 OW85 93.6(6) . .
OW88 Na8 OW86 176.2(7) . .
OW88 Na8 OW89 84.0(7) . .
OW88 Na8 OW84 87.3(7) . .
OW88 Na8 Na9 41.7(6) . .
OW84 Na8 Na7 41.7(5) . .
OW84 Na8 OW87 100.7(6) . .
OW84 Na8 OW85 82.0(6) . .
OW84 Na8 Na9 121.4(6) . .
Na9 Na8 Na7 106.6(3) . .
O49 Na7 O23 81.3(3) . .
O49 Na7 Na8 97.9(3) . .
O49 Na7 OW85 92.6(4) . .
O49 Na7 OW83 167.3(6) . .
O49 Na7 OW84 88.2(6) . .
O49 Na7 Na6B 144.3(5) . 3_567
O23 Na7 Na8 143.4(3) . .
O23 Na7 OW83 87.6(5) . .
O23 Na7 Na6B 84.4(3) . 3_567
OW85 Na7 O23 171.2(5) . .
OW85 Na7 Na8 43.5(3) . .
OW85 Na7 OW83 99.1(6) . .
OW85 Na7 OW84 84.1(6) . .
OW85 Na7 Na6B 97.1(4) . 3_567
OW81 Na7 O49 100.1(5) . .
OW81 Na7 O23 86.6(5) . .
OW81 Na7 Na8 129.0(4) . .
OW81 Na7 OW85 88.3(5) . .
OW81 Na7 OW83 85.3(6) . .
OW81 Na7 OW84 169.0(7) . .
OW81 Na7 Na6B 46.3(5) . 3_567
OW83 Na7 Na8 87.3(5) . .
OW83 Na7 Na6B 39.1(6) . 3_567
OW84 Na7 O23 102.0(6) . .
OW84 Na7 Na8 41.7(5) . .
OW84 Na7 OW83 88.0(7) . .
OW84 Na7 Na6B 126.9(6) . 3_567
Na6B Na7 Na8 112.8(3) 3_567 .
Na7 OW85 Na8 95.2(4) . .
Na8 OW89 Na9 88.6(8) . .
O7AA OW89 Na8 158(3) . .
O7AA OW89 Na9 71(3) . .
Na10 OW94 Na1 124.2(8) . 4_566
O1G OW94 Na10 102(2) . .
O1G OW94 Na1 39.7(19) . 4_566
O1G OW94 O1H 47(3) . .
O1H OW94 Na10 132(3) . .
O1H OW94 Na1 60(3) . 4_566
Na7 OW81 Na6B 91.8(7) . 3_567
Na7 OW81 Na6B 161.5(7) . .
Na6B OW81 Na6B 99.6(7) 3_567 .
O24 Na4 O24 86.3(5) . 4_565
O24 Na4 OW75 90.4(4) 4_565 .
O24 Na4 OW75 176.3(6) . .
O24 Na4 OW75 90.4(4) . 4_565
O24 Na4 OW75 176.3(6) 4_565 4_565
O24 Na4 NaW7 85.2(5) 4_565 4_565
O24 Na4 NaW7 140.0(6) 4_565 .
O24 Na4 NaW7 85.3(5) . .
O24 Na4 NaW7 140.0(6) . 4_565
O24 Na4 OW76 94.5(15) . .
O24 Na4 OW76 94.5(15) 4_565 .
OW75 Na4 OW75 92.9(7) . 4_565
OW75 Na4 NaW7 98.4(6) 4_565 4_565
OW75 Na4 NaW7 41.1(5) 4_565 .
OW75 Na4 NaW7 98.4(6) . .
OW75 Na4 NaW7 41.1(5) . 4_565
OW75 Na4 OW76 87.4(14) 4_565 .
OW75 Na4 OW76 87.4(14) . .
OW74 Na4 O24 81.8(5) . .
OW74 Na4 O24 81.8(5) . 4_565
OW74 Na4 OW75 96.1(5) . .
OW74 Na4 OW75 96.1(5) . 4_565
OW74 Na4 NaW7 135.1(4) . .
OW74 Na4 NaW7 135.1(4) . 4_565
OW74 Na4 OW76 175(2) . .
NaW7 Na4 NaW7 76.7(6) 4_565 .
OW76 Na4 NaW7 47.5(11) . 4_565
OW76 Na4 NaW7 47.5(11) . .
O0BA Na4 O24 83(3) . .
O0BA Na4 O24 83(3) . 4_565
O0BA Na4 OW75 98(3) . 4_565
O0BA Na4 OW75 98(3) . .
O0BA Na4 OW74 160(4) . .
O0BA Na4 NaW7 57(3) . .
O0BA Na4 NaW7 57(3) . 4_565
O0BA Na4 OW76 15(4) . .
Na4 OW75 NaW7 98.6(8) . 4_565
O9 Na1 Na2 47.7(4) . 3_666
O9 Na1 O4AA 123.4(10) . .
OW94 Na1 O9 75.5(6) 4_564 .
OW94 Na1 Na2 94.7(6) 4_564 3_666
OW94 Na1 O4AA 69.3(10) 4_564 .
OW64 Na1 O9 85.1(6) . .
OW64 Na1 OW94 85.7(7) . 4_564
OW64 Na1 OW62 87.9(8) . .
OW64 Na1 OW61 171.7(10) . .
OW64 Na1 Na2 130.2(7) . 3_666
OW64 Na1 O4AA 132.8(10) . .
OW62 Na1 O9 165.9(10) . .
OW62 Na1 OW94 116.1(9) . 4_564
OW62 Na1 Na2 133.8(7) . 3_666
OW62 Na1 O4AA 70.0(10) . .
OW63 Na1 O9 74.5(7) . .
OW63 Na1 OW94 149.1(9) . 4_564
OW63 Na1 OW64 99.0(8) . .
OW63 Na1 OW62 94.7(9) . .
OW63 Na1 OW61 84.8(10) . .
OW63 Na1 Na2 59.0(7) . 3_666
OW63 Na1 O4AA 123.2(10) . .
OW61 Na1 O9 88.9(8) . .
OW61 Na1 OW94 87.3(10) . 4_564
OW61 Na1 OW62 99.2(10) . .
OW61 Na1 Na2 46.0(8) . 3_666
OW61 Na1 O4AA 47.6(11) . .
O4AA Na1 Na2 92.3(9) . 3_666
O1G Na1 O9 86.3(11) 4_564 .
O1G Na1 OW94 20.1(10) 4_564 4_564
O1G Na1 OW64 69.3(11) 4_564 .
O1G Na1 OW62 102.6(12) 4_564 .
O1G Na1 OW63 158.5(13) 4_564 .
O1G Na1 OW61 104.6(14) 4_564 .
O1G Na1 Na2 114.1(11) 4_564 3_666
O1G Na1 O4AA 75.4(14) 4_564 .
O1G Na1 O1H 25.6(17) 4_564 4_564
O1H Na1 O9 106.0(18) 4_564 .
O1H Na1 OW94 30.5(17) 4_564 4_564
O1H Na1 OW64 87.6(18) 4_564 .
O1H Na1 OW62 85.8(18) 4_564 .
O1H Na1 OW63 173.4(19) 4_564 .
O1H Na1 OW61 88.6(19) 4_564 .
O1H Na1 Na2 116.3(18) 4_564 3_666
O1H Na1 O4AA 50.9(19) 4_564 .
O1F OW95 Na10 66.0(17) . .
Na6B OW83 Na7 95.7(8) 3_567 .
Na9 OW88 Na8 96.2(9) . .
Na1 OW63 Na2 79.6(7) . 3_666
Na1 OW61 Na2 89.9(11) . 3_666
Na8 OW84 Na7 96.7(7) . .
O9 Na2 O26 142.5(8) 3_666 .
O9 Na2 Na1 47.0(4) 3_666 3_666
O9 Na2 OW63 63.2(6) 3_666 3_666
O9 Na2 Na0A 43.2(5) 3_666 3_666
O9 Na2 O1E 107.4(11) 3_666 1_655
O9 Na2 O8AA 118.9(9) 3_666 .
O26 Na2 Na1 111.6(6) . 3_666
O26 Na2 OW63 81.2(6) . 3_666
O26 Na2 Na0A 107.8(7) . 3_666
O26 Na2 O1E 94.3(11) . 1_655
O26 Na2 O8AA 98.4(9) . .
OW63 Na2 Na1 41.4(5) 3_666 3_666
OW61 Na2 O9 86.5(8) 3_666 3_666
OW61 Na2 O26 92.4(9) 3_666 .
OW61 Na2 Na1 44.1(8) 3_666 3_666
OW61 Na2 OW63 70.2(9) 3_666 3_666
OW61 Na2 OW66 152.0(12) 3_666 .
OW61 Na2 O1E 145.9(14) 3_666 1_655
OW61 Na2 O8AA 96.9(11) 3_666 .
OW67 Na2 O9 74.4(6) . 3_666
OW67 Na2 O26 141.6(9) . .
OW67 Na2 Na1 103.4(7) . 3_666
OW67 Na2 OW63 137.1(8) . 3_666
OW67 Na2 OW61 102.3(10) . 3_666
OW67 Na2 OW66 99.0(8) . .
OW67 Na2 Na0A 109.8(7) . 3_666
OW67 Na2 O1E 54.8(11) . 1_655
OW67 Na2 O8AA 45.1(9) . .
OW66 Na2 O9 81.9(7) . 3_666
OW66 Na2 O26 81.9(7) . .
OW66 Na2 Na1 113.0(8) . 3_666
OW66 Na2 OW63 81.8(8) . 3_666
OW66 Na2 Na0A 100.0(8) . 3_666
OW66 Na2 O1E 62.1(11) . 1_655
OW66 Na2 O8AA 111.1(10) . .
OW68 Na2 O9 145.5(11) . 3_666
OW68 Na2 O26 70.7(9) . .
OW68 Na2 Na1 125.4(10) . 3_666
OW68 Na2 OW63 139.3(11) . 3_666
OW68 Na2 OW61 81.9(12) . 3_666
OW68 Na2 OW67 76.5(11) . .
OW68 Na2 OW66 121.0(12) . .
OW68 Na2 Na0A 137.5(11) . 3_666
OW68 Na2 O1E 69.0(13) . 1_655
OW68 Na2 O8AA 32.3(10) . .
O1B Na2 O9 85.4(15) 3_666 3_666
O1B Na2 O26 78.3(15) 3_666 .
O1B Na2 OW67 125.9(17) 3_666 .
O1B Na2 OW66 127.6(17) 3_666 .
O1B Na2 OW68 97.0(17) 3_666 .
O1B Na2 Na0A 44.2(15) 3_666 3_666
O1B Na2 O1E 165.8(18) 3_666 1_655
O1B Na2 O8AA 119.5(17) 3_666 .
O1E Na2 Na1 153.1(11) 1_655 3_666
O1E Na2 OW63 143.9(12) 1_655 3_666
O1E Na2 Na0A 149.7(11) 1_655 3_666
O1E Na2 O8AA 49.0(12) 1_655 .
O8AA Na2 Na1 129.1(9) . 3_666
O8AA Na2 OW63 167.0(10) . 3_666
O8AA Na2 Na0A 141.8(10) . 3_666
O57 Na6B Na7 144.3(8) . 3_567
O57 Na6B OW81 164.3(9) . 3_567
O57 Na6B OW81 88.0(6) . .
O57 Na6B Na6B 127.0(9) . 3_567
O57 Na6B O4AA 82.3(9) . 1_556
O57 Na6B O1BA 88.9(9) . .
O22 Na6B O57 79.4(4) . .
O22 Na6B Na7 86.6(4) . 3_567
O22 Na6B OW81 77.8(6) . .
O22 Na6B OW81 87.8(5) . 3_567
O22 Na6B Na6B 80.5(6) . 3_567
O22 Na6B O4AA 138.6(11) . 1_556
O22 Na6B O1BA 166.1(10) . .
Na7 Na6B Na6B 81.8(3) 3_567 3_567
OW81 Na6B Na7 120.9(6) . 3_567
OW81 Na6B Na7 41.9(4) 3_567 3_567
OW81 Na6B OW81 80.4(7) 3_567 .
OW81 Na6B Na6B 40.6(4) 3_567 3_567
OW81 Na6B Na6B 39.8(5) . 3_567
OW81 Na6B O4AA 113.3(9) 3_567 1_556
OW81 Na6B O4AA 138.3(9) . 1_556
OW81 Na6B O1BA 102.4(10) 3_567 .
OW83 Na6B O57 100.5(9) 3_567 .
OW83 Na6B O22 84.7(7) 3_567 .
OW83 Na6B Na7 45.2(6) 3_567 3_567
OW83 Na6B OW81 87.1(7) 3_567 3_567
OW83 Na6B OW81 158.7(8) 3_567 .
OW83 Na6B Na6B 125.6(7) 3_567 3_567
OW83 Na6B O4AA 62.7(10) 3_567 1_556
OW83 Na6B O9AA 132.9(15) 3_567 .
OW83 Na6B O1BA 105.0(12) 3_567 .
OW82 Na6B O57 87.3(10) . .
OW82 Na6B O22 161.0(12) . .
OW82 Na6B Na7 111.9(10) . 3_567
OW82 Na6B OW81 102.8(10) . 3_567
OW82 Na6B OW81 88.3(12) . .
OW82 Na6B OW83 111.3(14) . 3_567
OW82 Na6B Na6B 97.2(12) . 3_567
OW82 Na6B O4AA 50.9(13) . 1_556
OW82 Na6B O9AA 21.6(12) . .
OW82 Na6B O1BA 6.3(16) . .
O4AA Na6B Na7 87.1(8) 1_556 3_567
O4AA Na6B Na6B 138.6(9) 1_556 3_567
O9AA Na6B O57 82.8(11) . .
O9AA Na6B O22 141.0(14) . .
O9AA Na6B Na7 125.6(11) . 3_567
O9AA Na6B OW81 102.1(12) . 3_567
O9AA Na6B OW81 67.1(13) . .
O9AA Na6B Na6B 83.1(13) . 3_567
O9AA Na6B O4AA 71.4(14) . 1_556
O9AA Na6B O1BA 27.9(15) . .
O1BA Na6B Na7 107.3(9) . 3_567
O1BA Na6B OW81 94.5(11) . .
O1BA Na6B Na6B 101.0(10) . 3_567
O1BA Na6B O4AA 45.1(12) . 1_556
U3 Na5 U3 59.0(2) 4_565 .
O2 Na5 U3 24.8(2) 4_565 4_565
O2 Na5 U3 24.8(2) . .
O2 Na5 U3 83.8(4) 4_565 .
O2 Na5 U3 83.8(4) . 4_565
O2 Na5 O2 108.5(6) . 4_565
OW72 Na5 U3 107.2(4) 4_565 .
OW72 Na5 U3 107.2(4) . 4_565
OW72 Na5 U3 165.5(5) . .
OW72 Na5 U3 165.5(5) 4_565 4_565
OW72 Na5 O2 168.4(7) 4_565 4_565
OW72 Na5 O2 82.7(4) 4_565 .
OW72 Na5 O2 82.7(4) . 4_565
OW72 Na5 O2 168.4(7) . .
OW72 Na5 OW72 86.0(9) 4_565 .
OW72 Na5 OW71 90.6(9) 4_565 .
OW72 Na5 OW71 90.6(9) . .
OW72 Na5 O6AA 101.6(12) 4_565 4_565
OW72 Na5 O6AA 101.6(12) . .
OW72 Na5 O6AA 71.6(11) . 4_565
OW72 Na5 O6AA 71.6(11) 4_565 .
OW71 Na5 U3 83.6(8) . .
OW71 Na5 U3 83.6(8) . 4_565
OW71 Na5 O2 87.1(7) . .
OW71 Na5 O2 87.1(7) . 4_565
OW71 Na5 O6AA 157.4(10) . 4_565
OW71 Na5 O6AA 157.4(10) . .
OW73 Na5 U3 99(3) . 4_565
OW73 Na5 U3 99(3) . .
OW73 Na5 O2 94(2) . 4_565
OW73 Na5 O2 94(2) . .
OW73 Na5 OW72 87(3) . .
OW73 Na5 OW72 87(3) . 4_565
OW73 Na5 OW71 177(4) . .
OW73 Na5 O6AA 22.3(10) . .
OW73 Na5 O6AA 22.3(10) . 4_565
O6AA Na5 U3 88.4(11) . .
O6AA Na5 U3 88.4(11) 4_565 4_565
O6AA Na5 U3 110.1(12) . 4_565
O6AA Na5 U3 110.1(12) 4_565 .
O6AA Na5 O2 77.1(11) 4_565 4_565
O6AA Na5 O2 77.1(11) . .
O6AA Na5 O2 113.0(12) . 4_565
O6AA Na5 O2 113.0(12) 4_565 .
O6AA Na5 O6AA 44(2) 4_565 .
O9AA OW82 Na6B 88(4) . .
O1BA OW82 Na6B 146(8) . .
O1BA OW82 O9AA 126(10) . .
O1D OW69 NaW7 79.5(17) . .
Na4 NaW7 Na2 117.8(6) . 1_455
Na4 NaW7 Na9 124.9(7) . 1_554
OW75 NaW7 Na4 40.2(5) 4_565 .
OW75 NaW7 Na2 112.9(7) 4_565 1_455
OW75 NaW7 Na9 91.7(8) 4_565 1_554
OW75 NaW7 OW76 80.5(18) 4_565 .
OW75 NaW7 O1D 146.0(12) 4_565 .
OW75 NaW7 O8AA 69.3(9) 4_565 1_455
OW75 NaW7 O6BA 85.2(16) 4_565 1_554
OW69 NaW7 Na4 140.7(8) . .
OW69 NaW7 OW75 159.2(13) . 4_565
OW69 NaW7 Na2 85.0(7) . 1_455
OW69 NaW7 Na9 73.2(7) . 1_554
OW69 NaW7 OW76 100.4(19) . .
OW69 NaW7 O1D 32.8(8) . .
OW69 NaW7 O1E 90.8(13) . .
OW69 NaW7 O8AA 129.2(11) . 1_455
OW69 NaW7 O6BA 77.8(16) . 1_554
Na9 NaW7 Na2 103.3(5) 1_554 1_455
OW92 NaW7 Na4 128.3(12) 1_554 .
OW92 NaW7 OW75 89.3(12) 1_554 4_565
OW92 NaW7 Na2 87.0(11) 1_554 1_455
OW92 NaW7 OW69 81.0(12) 1_554 .
OW92 NaW7 Na9 19.0(10) 1_554 1_554
OW92 NaW7 OW76 154(2) 1_554 .
OW92 NaW7 O1D 112.9(14) 1_554 .
OW92 NaW7 O1E 51.4(15) 1_554 .
OW92 NaW7 O8AA 93.0(13) 1_554 1_455
OW92 NaW7 O6BA 26.8(15) 1_554 1_554
OW76 NaW7 Na4 41.3(18) . .
OW76 NaW7 Na2 119.0(17) . 1_455
OW76 NaW7 Na9 136.7(17) . 1_554
OW76 NaW7 O8AA 105.4(19) . 1_455
O1D NaW7 Na4 109.6(10) . .
O1D NaW7 Na2 94.4(10) . 1_455
O1D NaW7 Na9 101.6(10) . 1_554
O1D NaW7 OW76 68(2) . .
O1D NaW7 O8AA 130.9(14) . 1_455
O1D NaW7 O6BA 103.0(17) . 1_554
O1E NaW7 Na4 127.2(13) . .
O1E NaW7 OW75 97.4(13) . 4_565
O1E NaW7 Na2 37.6(11) . 1_455
O1E NaW7 Na9 69.6(12) . 1_554
O1E NaW7 OW76 153(2) . .
O1E NaW7 O1D 116.5(15) . .
O1E NaW7 O8AA 50.4(13) . 1_455
O1E NaW7 O6BA 78.1(19) . 1_554
O8AA NaW7 Na4 80.2(8) 1_455 .
O8AA NaW7 Na2 44.2(8) 1_455 1_455
O8AA NaW7 Na9 111.4(9) 1_455 1_554
O6BA NaW7 Na4 115.7(16) 1_554 .
O6BA NaW7 Na2 113.0(16) 1_554 1_455
O6BA NaW7 Na9 10.1(15) 1_554 1_554
O6BA NaW7 OW76 128(2) 1_554 .
O6BA NaW7 O8AA 115.9(17) 1_554 1_455
O5BA NaW7 Na4 75(2) . .
O5BA NaW7 OW75 97(2) . 4_565
O5BA NaW7 Na2 51(2) . 1_455
O5BA NaW7 OW69 103(2) . .
O5BA NaW7 Na9 154(2) . 1_554
O5BA NaW7 OW92 136(3) . 1_554
O5BA NaW7 OW76 69(3) . .
O5BA NaW7 O1D 85(2) . .
O5BA NaW7 O1E 85(3) . .
O5BA NaW7 O8AA 51(2) . 1_455
O5BA NaW7 O6BA 163(3) . 1_554
O54 Na9 Na8 94.8(6) 4_465 .
O54 Na9 OW89 83.9(7) 4_465 .
O54 Na9 OW93 63.1(6) 4_465 .
O54 Na9 NaW7 96.4(6) 4_465 1_556
O54 Na9 OW91 68.0(10) 4_465 .
Na8 Na9 NaW7 165.3(6) . 1_556
OW90 Na9 O54 162.5(10) . 4_465
OW90 Na9 Na8 83.7(6) . .
OW90 Na9 OW89 106.4(8) . .
OW90 Na9 OW93 132.9(10) . .
OW90 Na9 NaW7 88.4(7) . 1_556
OW90 Na9 OW91 98.8(11) . .
OW89 Na9 Na8 44.2(5) . .
OW89 Na9 NaW7 127.9(9) . 1_556
OW89 Na9 OW91 150.3(12) . .
OW88 Na9 O54 80.2(8) . 4_465
OW88 Na9 Na8 42.2(7) . .
OW88 Na9 OW90 87.2(9) . .
OW88 Na9 OW89 81.7(9) . .
OW88 Na9 OW93 137.2(10) . .
OW88 Na9 NaW7 149.9(9) . 1_556
OW88 Na9 OW91 83.9(12) . .
OW88 Na9 O7AA 99.3(13) . .
OW93 Na9 Na8 116.7(7) . .
OW93 Na9 OW89 73.5(7) . .
OW93 Na9 NaW7 61.1(6) . 1_556
OW93 Na9 OW91 100.7(11) . .
OW91 Na9 Na8 126.0(12) . .
OW91 Na9 NaW7 67.4(10) . 1_556
OW92 Na9 O54 110.8(13) . 4_465
OW92 Na9 Na8 143.5(13) . .
OW92 Na9 OW90 79.1(12) . .
OW92 Na9 OW89 111.4(14) . .
OW92 Na9 OW88 163.2(15) . .
OW92 Na9 OW93 59.1(12) . .
OW92 Na9 NaW7 21.9(11) . 1_556
OW92 Na9 OW91 88.5(15) . .
OW92 Na9 O7AA 95.7(16) . .
O7AA Na9 O54 76.7(10) . 4_465
O7AA Na9 Na8 64.5(10) . .
O7AA Na9 OW90 117.6(12) . .
O7AA Na9 OW89 20.5(9) . .
O7AA Na9 OW93 53.1(11) . .
O7AA Na9 NaW7 109.1(12) . 1_556
O7AA Na9 OW91 143.5(14) . .
O6BA Na9 O54 97(2) . 4_465
O6BA Na9 Na8 166(2) . .
O6BA Na9 OW90 82(2) . .
O6BA Na9 OW89 145(3) . .
O6BA Na9 OW88 133(3) . .
O6BA Na9 OW93 76(2) . .
O6BA Na9 NaW7 17(2) . 1_556
O6BA Na9 OW91 53(3) . .
O6BA Na9 OW92 35(2) . .
O6BA Na9 O7AA 126(3) . .
O6AA OW73 Na5 102(9) . .
O6AA OW73 Na5 102(9) 4_565 .
O6AA OW73 O6AA 154(10) . 4_565
OW91 OW91 Na9 170.5(10) 4_565 .
O8AA OW68 Na2 94(2) . .
O5BA OW68 Na2 118(4) 1_655 .
O5BA OW68 O8AA 100(4) 1_655 .
Na9 OW92 NaW7 139(2) . 1_556
O6BA OW92 NaW7 90(4) . 1_556
O6BA OW92 Na9 51(3) . .
Na4 OW76 NaW7 91(2) . 4_565
Na4 OW76 NaW7 91(2) . .
NaW7 OW76 NaW7 115(3) 4_565 .
O0BA OW76 Na4 55(10) . .
O0BA OW76 NaW7 117(6) . .
O0BA OW76 NaW7 117(6) . 4_565
O9 Na0A Na2 45.2(5) . 3_666
O9 Na0A O1B 83.5(15) . .
O9 Na0A O1H 89.1(15) . 4_564
OW10 Na0A O9 92.0(10) . .
OW10 Na0A Na2 73.8(8) . 3_666
OW10 Na0A O1B 78.9(16) . .
OW10 Na0A O1H 163.3(18) . 4_564
O1A Na0A O9 95.8(10) . .
O1A Na0A Na2 139.1(10) . 3_666
O1A Na0A OW10 101.1(12) . .
O1A Na0A O1B 179.3(17) . .
O1A Na0A O1C 89.5(12) . .
O1A Na0A O1G 83.5(12) . 4_564
O1A Na0A O1H 95.4(16) . 4_564
O1B Na0A Na2 40.3(13) . 3_666
O1B Na0A O1H 85(2) . 4_564
O1C Na0A O9 170.5(15) . .
O1C Na0A Na2 131.1(11) . 3_666
O1C Na0A OW10 94.8(12) . .
O1C Na0A O1B 91.2(16) . .
O1C Na0A O1G 95.6(13) . 4_564
O1C Na0A O1H 82.5(16) . 4_564
O1G Na0A O9 77.2(10) 4_564 .
O1G Na0A Na2 95.9(11) 4_564 3_666
O1G Na0A OW10 168.7(14) 4_564 .
O1G Na0A O1B 96.4(18) 4_564 .
O1G Na0A O1H 17.9(14) 4_564 4_564
O1H Na0A Na2 95.5(15) 4_564 3_666
Na2 O1B Na0A 96(2) 3_666 .
Na1 O4AA Na6B 128.6(14) . 1_554
OW69 O1D NaW7 67.7(15) . .
NaW7 O1E Na2 110.1(18) . 1_455
OW95 O1F Na10 81.7(18) . .
Na2 O8AA NaW7 90.5(11) . 1_655
OW68 O8AA Na2 53.5(17) . .
OW68 O8AA NaW7 78.0(19) . 1_655
OW73 O6AA Na5 55(9) . .
OW89 O7AA Na9 88(3) . .
OW94 O1G Na10 57.2(18) . .
OW94 O1G Na1 120(3) . 4_566
OW94 O1G Na0A 130(3) . 4_566
Na1 O1G Na10 137.5(16) 4_566 .
Na0A O1G Na10 126.1(14) 4_566 .
O1H O1G Na10 122(5) . .
O1H O1G OW94 82(5) . .
O1H O1G Na1 97(5) . 4_566
O1H O1G Na0A 111(5) . 4_566
OW76 O0BA Na4 109(10) . .
OW94 O1H Na1 89(4) . 4_566
OW94 O1H Na0A 89(3) . 4_566
O1G O1H OW94 51(4) . .
O1G O1H Na1 58(4) . 4_566
O1G O1H Na0A 51(4) . 4_566
OW82 O9AA Na6B 71(4) . .
OW82 O9AA O1BA 20(4) . .
O1BA O9AA Na6B 91(3) . .
OW82 O1BA Na6B 28(7) . .
OW82 O1BA O9AA 34(6) . .
O9AA O1BA Na6B 61(3) . .
OW79 O3BA OW80 145(5) . .
Na9 O6BA NaW7 153(4) . 1_556
OW92 O6BA NaW7 63(3) . 1_556
OW92 O6BA Na9 94(5) . .
OW68 O5BA NaW7 123(5) 1_455 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
U1 U2 4.0071(6) .
U1 U2 4.0071(6) 4_565
U1 U3 3.8204(7) .
U1 U3 3.8204(7) 4_565
U1 O7 2.370(7) 4_565
U1 O7 2.370(7) .
U1 O39 2.303(7) .
U1 O39 2.302(7) 4_565
U1 O40 2.293(6) 4_565
U1 O40 2.293(6) .
U1 O4 2.572(11) .
U1 O8 2.502(9) .
U2 U2 3.9937(7) 4_565
U2 U3 3.8266(6) .
U2 U4 3.8288(7) .
U2 O58 2.300(7) .
U2 O7 2.367(6) .
U2 O6 2.592(8) .
U2 O56 2.308(8) .
U2 O38 2.312(7) .
U2 O37 2.317(6) .
U2 O5 2.362(5) .
U2 O8 2.489(6) .
U3 U3 3.8059(7) 4_565
U3 U4 3.8028(6) .
U3 O41 2.284(7) .
U3 O7 2.041(8) .
U3 O6 2.410(7) .
U3 O36 2.304(7) .
U3 O4 2.418(6) .
U3 O3 2.229(5) .
U3 O2 1.860(9) .
U3 Na5 3.862(13) .
U4 U2 3.8288(7) 4_565
U4 U3 3.8027(6) 4_565
U4 O6 2.418(7) 4_565
U4 O6 2.417(7) .
U4 O55 2.282(7) 4_565
U4 O55 2.282(7) .
U4 O5 2.050(10) .
U4 O3 2.219(10) .
U4 O1 1.876(14) .
W13 O48 2.002(7) .
W13 O52 1.932(7) .
W13 O55 1.811(7) .
W13 O60 2.332(8) 4_565
W13 O54 1.727(9) .
W13 O53 1.922(3) .
W13 Na3 3.602(5) 1_556
W5 O35 2.333(8) .
W5 O41 1.812(7) .
W5 O32 1.937(7) .
W5 O27 1.909(7) .
W5 O26 1.720(9) .
W5 O20 2.007(8) .
W10 O48 1.915(8) .
W10 O45 1.902(8) .
W10 O44 1.890(7) .
W10 O42 1.716(7) .
W10 O60 2.293(6) 4_565
W10 O46 1.932(3) .
W10 Na3 3.450(6) 1_556
W4 O31 1.919(8) .
W4 O35 2.335(7) .
W4 O32 1.948(8) .
W4 O19 2.016(7) .
W4 O25 1.723(7) .
W4 O40 1.814(6) .
W4 Na10 3.501(5) 4_564
W7 O29 1.905(8) .
W7 O16 2.022(7) .
W7 O28 1.962(8) .
W7 O37 1.801(6) .
W7 O22 1.718(7) .
W7 O33 2.306(6) .
W12 O51 1.903(8) .
W12 O59 2.334(8) .
W12 O47 2.018(7) .
W12 O56 1.805(7) .
W12 O49 1.710(8) .
W12 O50 1.933(6) .
W11 O59 2.286(10) .
W11 O47 1.890(8) 4_565
W11 O47 1.890(8) .
W11 O45 1.925(8) .
W11 O45 1.925(8) 4_565
W11 OW43 1.727(11) .
W2 O12 1.932(7) .
W2 O15 1.914(8) .
W2 O13 1.920(8) .
W2 O16 1.891(7) .
W2 O10 1.716(7) .
W2 O33 2.298(6) .
W14 O51 1.913(8) .
W14 O58 1.803(7) .
W14 O52 1.950(9) 4_565
W14 O44 2.018(7) 4_565
W14 O57 1.719(7) .
W14 O60 2.318(6) .
W6 O15 2.003(7) .
W6 O27 1.928(7) .
W6 O21 1.729(9) .
W6 O28 1.935(7) .
W6 O36 1.809(7) .
W6 O33 2.339(8) .
W9 O31 1.919(8) .
W9 O18 2.023(7) .
W9 O24 1.715(9) .
W9 O30 1.942(7) .
W9 O39 1.819(7) .
W9 O34 2.328(7) .
W9 Na10 3.588(5) 4_564
W8 O29 1.921(7) .
W8 O30 1.925(7) .
W8 O17 2.025(7) .
W8 O38 1.807(7) .
W8 O34 2.339(7) .
W8 O23 1.728(8) .
W1 O35 2.288(7) .
W1 O12 1.895(7) .
W1 O9 1.744(7) .
W1 O19 1.913(7) .
W1 O20 1.906(8) .
W1 O14 1.914(9) .
W1 Na10 3.471(6) 4_564
W3 O18 1.887(7) .
W3 O17 1.883(7) .
W3 O13 1.906(8) .
W3 O14 1.941(8) .
W3 O11 1.727(8) .
W3 O34 2.300(7) .
W3 Na10 3.558(5) 4_564
As2 O59 1.785(11) .
As2 O60 1.794(6) .
As2 O60 1.794(6) 4_565
As1 O35 1.793(7) .
As1 O34 1.784(7) .
As1 O33 1.792(6) .
O48 Na3 2.594(8) 1_556
O31 Na10 2.482(9) 4_564
O18 Na10 2.655(9) 4_564
O24 Na4 2.365(11) .
O9 Na1 2.537(16) .
O9 Na2 2.566(15) 3_666
O9 Na0A 2.48(2) .
O59 W12 2.334(8) 4_565
O19 Na10 2.520(11) 4_564
O25 Na3 2.364(8) .
O26 Na2 2.597(15) .
O14 Na10 2.535(9) 4_564
O52 W14 1.950(9) 4_565
O44 W14 2.018(7) 4_565
O57 Na6B 2.319(12) .
O22 Na6B 2.305(13) .
O42 Na10 2.351(8) .
O5 U2 2.362(5) 4_565
O4 U3 2.418(6) 4_565
O60 W13 2.332(8) 4_565
O60 W10 2.293(6) 4_565
O49 Na7 2.404(11) .
O3 U3 2.229(5) 4_565
O23 Na7 2.478(10) .
O8 U2 2.489(6) 4_565
O54 Na9 2.445(17) 4_665
O46 W10 1.932(3) 4_565
O46 Na3 2.434(13) 1_556
O50 W12 1.933(6) 4_565
O53 W13 1.922(3) 4_565
O53 Na3 2.571(11) 1_556
O2 Na5 2.591(13) .
Na3 W13 3.602(5) 4_564
Na3 W13 3.602(5) 1_554
Na3 W10 3.450(5) 4_564
Na3 W10 3.450(5) 1_554
Na3 O48 2.594(8) 4_564
Na3 O48 2.594(8) 1_554
Na3 O25 2.364(8) 4_565
Na3 O46 2.434(13) 1_554
Na3 O53 2.571(11) 1_554
Na3 OW70 2.332(18) .
Na10 W4 3.501(5) 4_566
Na10 W1 3.471(6) 4_566
Na10 W3 3.558(5) 4_566
Na10 O31 2.482(9) 4_566
Na10 O18 2.654(9) 4_566
Na10 O19 2.520(11) 4_566
Na10 O14 2.535(9) 4_566
Na10 OW94 2.402(18) .
Na10 OW95 2.434(17) .
Na10 O1F 2.25(4) .
Na10 O1G 2.79(3) .
Na8 Na7 3.632(10) .
Na8 OW87 2.484(13) .
Na8 OW85 2.508(13) .
Na8 OW86 2.362(13) .
Na8 OW89 2.42(2) .
Na8 OW88 2.35(2) .
Na8 OW84 2.43(2) .
Na8 Na9 3.48(2) .
Na7 OW85 2.410(12) .
Na7 OW81 2.335(17) .
Na7 OW83 2.49(2) .
Na7 OW84 2.43(2) .
Na7 Na6B 3.492(14) 3_567
OW90 Na9 2.44(2) .
OW89 Na9 2.55(3) .
OW89 O7AA 0.89(4) .
OW94 Na1 2.53(2) 4_566
OW94 O1G 1.01(3) .
OW94 O1H 1.28(6) .
OW81 Na6B 2.57(3) .
OW81 Na6B 2.526(19) 3_567
Na4 O24 2.365(11) 4_565
Na4 OW75 2.447(16) 4_565
Na4 OW75 2.447(16) .
Na4 OW74 2.320(18) .
Na4 NaW7 3.74(2) .
Na4 NaW7 3.74(2) 4_565
Na4 OW76 2.47(9) .
Na4 O0BA 2.15(14) .
OW75 NaW7 2.49(2) 4_565
Na1 OW94 2.53(2) 4_564
Na1 OW64 2.388(19) .
Na1 OW62 2.44(3) .
Na1 OW63 2.33(3) .
Na1 OW61 2.41(3) .
Na1 Na2 3.46(2) 3_666
Na1 O4AA 2.79(4) .
Na1 O1G 1.87(3) 4_564
Na1 O1H 2.20(7) 4_564
OW95 O1F 1.32(4) .
OW83 Na6B 2.21(3) 3_567
OW88 Na9 2.32(3) .
OW63 Na2 3.01(3) 3_666
OW61 Na2 2.49(3) 3_666
OW72 Na5 2.40(2) .
Na2 O9 2.566(15) 3_666
Na2 Na1 3.46(2) 3_666
Na2 OW63 3.01(3) 3_666
Na2 OW61 2.49(3) 3_666
Na2 OW67 2.43(2) .
Na2 OW66 2.52(3) .
Na2 OW68 2.37(4) .
Na2 Na0A 3.62(3) 3_666
Na2 O1B 2.35(6) 3_666
Na2 O1E 2.73(5) 1_655
Na2 O8AA 2.93(4) .
Na6B Na7 3.492(14) 3_567
Na6B OW81 2.526(19) 3_567
Na6B OW83 2.21(3) 3_567
Na6B Na6B 3.89(4) 3_567
Na6B OW82 2.10(3) .
Na6B O4AA 2.95(4) 1_556
Na6B O9AA 2.22(4) .
Na6B O1BA 2.53(4) .
Na5 U3 3.862(13) 4_565
Na5 O2 2.591(13) 4_565
Na5 OW72 2.40(2) 4_565
Na5 OW71 2.43(4) .
Na5 OW73 2.09(14) .
Na5 O6AA 2.48(5) 4_565
Na5 O6AA 2.48(5) .
OW93 Na9 2.54(3) .
OW78 O4BA 1.08(6) .
OW82 O9AA 0.82(4) .
OW82 O1BA 0.50(5) .
OW69 NaW7 2.39(2) .
OW69 O1D 1.40(4) .
NaW7 OW75 2.49(2) 4_565
NaW7 Na2 4.21(3) 1_455
NaW7 Na9 4.02(3) 1_554
NaW7 OW92 2.29(4) 1_554
NaW7 OW76 2.76(5) .
NaW7 O1D 2.54(4) .
NaW7 O1E 2.40(5) .
NaW7 O8AA 2.99(4) 1_455
NaW7 O6BA 2.57(7) 1_554
NaW7 O5BA 2.03(8) .
Na9 O54 2.445(17) 4_465
Na9 NaW7 4.02(3) 1_556
Na9 OW91 2.77(5) .
Na9 OW92 2.00(4) .
Na9 O7AA 2.42(4) .
Na9 O6BA 1.55(6) .
OW79 O3BA 1.17(6) .
OW73 O6AA 0.96(5) 4_565
OW73 O6AA 0.96(5) .
OW91 OW91 1.13(9) 4_565
OW68 O8AA 1.57(4) .
OW68 O5BA 1.46(8) 1_655
OW80 O3BA 1.78(6) .
OW92 NaW7 2.29(4) 1_556
OW92 O6BA 1.16(6) .
OW76 NaW7 2.76(5) 4_565
OW76 O0BA 0.69(15) .
Na0A Na2 3.62(3) 3_666
Na0A OW10 2.45(3) .
Na0A O1A 2.32(3) .
Na0A O1B 2.53(6) .
Na0A O1C 2.34(4) .
Na0A O1G 2.42(4) 4_564
Na0A O1H 2.90(7) 4_564
O1B Na2 2.35(6) 3_666
O4AA Na6B 2.95(4) 1_554
O1E Na2 2.73(5) 1_455
O8AA NaW7 2.99(4) 1_655
O1G Na1 1.87(3) 4_566
O1G Na0A 2.42(4) 4_566
O1G O1H 0.96(6) .
O1H Na1 2.20(7) 4_566
O1H Na0A 2.90(7) 4_566
O9AA O1BA 1.18(6) .
O6BA NaW7 2.57(7) 1_556
O5BA OW68 1.46(8) 1_455
