#------------------------------------------------------------------------------
#$Date: 2016-02-13 21:28:24 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176429 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/70/7037093.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7037093
loop_
_publ_author_name
'Yang, Jin-Xia'
'Zhai, Ji-Quan'
'Zhang, Xin'
'Qin, Ye-Yan'
'Yao, Yuan-Gen'
_publ_section_title
;
 Tuning different kinds of entangled metal-organic frameworks by modifying
 the spacer group of aliphatic dicarboxylate ligands and the reactant
 ratio.
;
_journal_issue                   2
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              711
_journal_page_last               723
_journal_paper_doi               10.1039/c5dt03731j
_journal_volume                  45
_journal_year                    2015
_chemical_formula_moiety         '2(C30 H32 Cd N4 O4), 3(O)'
_chemical_formula_sum            'C60 H64 Cd2 N8 O11'
_chemical_formula_weight         1298.01
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-04-28 deposited with the CCDC.
2015-11-04 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 97.612(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   21.9308(10)
_cell_length_b                   11.2167(4)
_cell_length_c                   24.9201(11)
_cell_measurement_reflns_used    4182
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      26.9090
_cell_measurement_theta_min      2.6760
_cell_volume                     6076.1(4)
_computing_cell_refinement       'Bruker FRAMBO'
_computing_data_collection       'Bruker FRAMBO'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'multiwire proportional'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0231
_diffrn_reflns_av_sigmaI/netI    0.0354
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            12696
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.55
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  none
_diffrn_standards_number         none
_exptl_absorpt_coefficient_mu    0.764
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.83264
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   crystalclear
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.419
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2656.0
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.2
_refine_diff_density_max         1.605
_refine_diff_density_min         -1.592
_refine_diff_density_rms         0.146
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.046
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     366
_refine_ls_number_reflns         5354
_refine_ls_number_restraints     144
_refine_ls_restrained_S_all      1.119
_refine_ls_R_factor_all          0.0904
_refine_ls_R_factor_gt           0.0740
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1426P)²+49.6938P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2194
_refine_ls_wR_factor_ref         0.2390
_reflns_number_gt                4269
_reflns_number_total             5354
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5dt03731j2.cif
_cod_data_source_block           Compound-4
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 7037090--7037095.cif.
;
_cod_original_sg_symbol_H-M      C2/c
_cod_original_formula_sum        'C60 H64 Cd2 N8 O11 '
_cod_database_code               7037093
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cd1 Cd 0.17047(2) 0.95610(5) -0.30781(2) 0.0436(3) Uani 1 1 d .
C1 C 0.2549(4) 0.7994(7) -0.3424(3) 0.0460(18) Uani 1 1 d .
C2 C 0.3003(4) 0.7169(9) -0.3635(3) 0.060(2) Uani 1 1 d .
H2A H 0.2795 0.6431 -0.3749 0.072 Uiso 1 1 calc R
H2B H 0.3141 0.7530 -0.3952 0.072 Uiso 1 1 calc R
C3 C 0.3558(4) 0.6880(9) -0.3234(4) 0.059(2) Uani 1 1 d .
H3A H 0.3738 0.7621 -0.3089 0.071 Uiso 1 1 calc R
H3B H 0.3860 0.6488 -0.3425 0.071 Uiso 1 1 calc R
C4 C 0.3433(4) 0.6096(7) -0.2769(3) 0.0468(18) Uani 1 1 d .
C5 C 0.0358(5) 1.0356(9) -0.3746(4) 0.069(3) Uani 1 1 d .
H5A H 0.0441 1.1029 -0.3531 0.083 Uiso 1 1 calc R
C6 C -0.0188(5) 1.0325(9) -0.4090(4) 0.068(3) Uani 1 1 d .
H6A H -0.0459 1.0965 -0.4101 0.082 Uiso 1 1 calc R
C7 C -0.0334(4) 0.9363(9) -0.4415(4) 0.059(2) Uani 1 1 d .
C8 C 0.0090(5) 0.8469(10) -0.4369(4) 0.072(3) Uani 1 1 d .
H8A H 0.0013 0.7792 -0.4582 0.086 Uiso 1 1 calc R
C9 C 0.0634(4) 0.8536(8) -0.4013(4) 0.059(2) Uani 1 1 d .
H9A H 0.0909 0.7901 -0.3992 0.070 Uiso 1 1 calc R
C10 C -0.2806(4) 0.7254(8) -0.3349(4) 0.056(2) Uani 1 1 d .
H10A H -0.3000 0.7462 -0.3052 0.067 Uiso 1 1 calc R
C11 C -0.2454(5) 0.8104(8) -0.3567(4) 0.066(2) Uani 1 1 d .
H11A H -0.2416 0.8862 -0.3415 0.079 Uiso 1 1 calc R
C12 C -0.2158(5) 0.7835(8) -0.4010(4) 0.066(2) Uani 1 1 d .
C13 C -0.2267(5) 0.6695(9) -0.4225(4) 0.072(3) Uani 1 1 d .
H13A H -0.2096 0.6472 -0.4532 0.086 Uiso 1 1 calc R
C14 C -0.2620(5) 0.5910(9) -0.3990(4) 0.063(2) Uani 1 1 d .
H14A H -0.2684 0.5161 -0.4147 0.075 Uiso 1 1 calc R
C15 C -0.0919(5) 0.9260(12) -0.4791(5) 0.092(4) Uani 1 1 d .
H15A H -0.0819 0.9082 -0.5151 0.110 Uiso 1 1 calc R
H15B H -0.1124 1.0027 -0.4809 0.110 Uiso 1 1 calc R
C16 C -0.1366(5) 0.8325(11) -0.4644(5) 0.084(3) Uani 1 1 d .
H16A H -0.1645 0.8112 -0.4965 0.101 Uiso 1 1 calc R
H16B H -0.1140 0.7614 -0.4517 0.101 Uiso 1 1 calc R
C17 C -0.1722(7) 0.8739(10) -0.4226(5) 0.090(4) Uani 1 1 d .
H17A H -0.1965 0.9419 -0.4369 0.108 Uiso 1 1 calc R
H17B H -0.1436 0.9022 -0.3923 0.108 Uiso 1 1 calc R
C18 C 0.1551(4) 0.6890(9) -0.2536(4) 0.0660(11) Uani 1 1 d U
H18A H 0.1866 0.6703 -0.2738 0.079 Uiso 1 1 calc R
C19 C 0.1360(5) 0.6032(10) -0.2209(4) 0.0711(12) Uani 1 1 d U
H19A H 0.1548 0.5288 -0.2189 0.085 Uiso 1 1 calc R
C20 C 0.0890(5) 0.6256(10) -0.1908(5) 0.0768(11) Uani 1 1 d U
C21 C 0.0647(5) 0.7389(9) -0.1957(4) 0.0708(12) Uani 1 1 d U
H21A H 0.0335 0.7599 -0.1756 0.085 Uiso 1 1 calc R
C22 C 0.0854(4) 0.8206(9) -0.2293(4) 0.0655(11) Uani 1 1 d U
H22A H 0.0668 0.8953 -0.2322 0.079 Uiso 1 1 calc R
C23 C -0.1374(6) 0.5280(10) -0.0977(6) 0.1319(18) Uani 1 1 d DU
H23A H -0.1699 0.5774 -0.1112 0.158 Uiso 1 1 calc R
C24 C -0.1010(6) 0.4807(11) -0.1333(5) 0.1287(17) Uani 1 1 d DU
H24A H -0.1096 0.4986 -0.1700 0.154 Uiso 1 1 calc R
C25 C -0.0521(6) 0.4074(11) -0.1156(5) 0.1233(16) Uani 1 1 d DU
C26 C -0.0418(6) 0.3842(11) -0.0616(6) 0.1292(17) Uani 1 1 d DU
H26A H -0.0096 0.3344 -0.0480 0.155 Uiso 1 1 calc R
C27 C -0.0791(6) 0.4342(12) -0.0261(5) 0.1327(18) Uani 1 1 d DU
H27A H -0.0703 0.4182 0.0107 0.159 Uiso 1 1 calc R
C28 C 0.0651(6) 0.5310(10) -0.1549(6) 0.0901(13) Uani 1 1 d U
H28A H 0.0995 0.4830 -0.1385 0.108 Uiso 1 1 calc R
H28B H 0.0472 0.5700 -0.1260 0.108 Uiso 1 1 calc R
C29 C 0.0219(7) 0.4575(11) -0.1830(6) 0.1036(14) Uani 1 1 d U
H29A H 0.0416 0.4145 -0.2097 0.124 Uiso 1 1 calc R
H29B H -0.0097 0.5075 -0.2025 0.124 Uiso 1 1 calc R
C30 C -0.0101(7) 0.3660(13) -0.1506(7) 0.1137(15) Uani 1 1 d U
H30A H -0.0322 0.3111 -0.1763 0.136 Uiso 1 1 calc R
H30B H 0.0217 0.3204 -0.1288 0.136 Uiso 1 1 calc R
N1 N 0.0771(3) 0.9491(6) -0.3703(3) 0.0503(16) Uani 1 1 d .
N2 N -0.2881(3) 0.6141(6) -0.3547(3) 0.0530(17) Uani 1 1 d .
N3 N 0.1308(4) 0.7994(7) -0.2582(3) 0.0625(11) Uani 1 1 d U
N4 N -0.1278(5) 0.5054(10) -0.0437(5) 0.1338(18) Uani 1 1 d DU
O1 O 0.2028(3) 0.8126(6) -0.3710(2) 0.0598(15) Uani 1 1 d .
O1W O 0.5000 0.2961(13) 0.2500 0.186(10) Uani 1 2 d S
O2 O 0.2684(3) 0.8542(5) -0.2993(2) 0.0559(14) Uani 1 1 d .
O2W O 0.3125(7) 0.3113(17) -0.0157(4) 0.185(7) Uani 1 1 d .
O3 O 0.2937(3) 0.5571(5) -0.2774(2) 0.0547(14) Uani 1 1 d .
O4 O 0.3868(3) 0.5962(6) -0.2385(3) 0.0626(16) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cd Cd -0.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Cd1 N3 178.2(3) 3 .
N2 Cd1 O4 90.4(3) 3 4_554
N3 Cd1 O4 89.1(3) . 4_554
N2 Cd1 N1 93.2(2) 3 .
N3 Cd1 N1 88.5(3) . .
O4 Cd1 N1 83.0(2) 4_554 .
N2 Cd1 O2 90.1(2) 3 .
N3 Cd1 O2 89.2(2) . .
O4 Cd1 O2 141.5(2) 4_554 .
N1 Cd1 O2 135.4(2) . .
N2 Cd1 O1 90.7(2) 3 .
N3 Cd1 O1 90.3(3) . .
O4 Cd1 O1 164.6(2) 4_554 .
N1 Cd1 O1 81.7(2) . .
O2 Cd1 O1 53.9(2) . .
N2 Cd1 O3 88.9(2) 3 4_554
N3 Cd1 O3 89.4(2) . 4_554
O4 Cd1 O3 53.6(2) 4_554 4_554
N1 Cd1 O3 136.6(2) . 4_554
O2 Cd1 O3 87.89(19) . 4_554
O1 Cd1 O3 141.75(19) . 4_554
O2 C1 O1 121.4(7) . .
O2 C1 C2 121.0(8) . .
O1 C1 C2 117.6(8) . .
C3 C2 C1 114.6(8) . .
C3 C2 H2A 108.6 . .
C1 C2 H2A 108.6 . .
C3 C2 H2B 108.6 . .
C1 C2 H2B 108.6 . .
H2A C2 H2B 107.6 . .
C2 C3 C4 115.1(7) . .
C2 C3 H3A 108.5 . .
C4 C3 H3A 108.5 . .
C2 C3 H3B 108.5 . .
C4 C3 H3B 108.5 . .
H3A C3 H3B 107.5 . .
O3 C4 O4 121.5(7) . .
O3 C4 C3 121.3(7) . .
O4 C4 C3 117.1(8) . .
N1 C5 C6 124.2(9) . .
N1 C5 H5A 117.9 . .
C6 C5 H5A 117.9 . .
C7 C6 C5 120.4(9) . .
C7 C6 H6A 119.8 . .
C5 C6 H6A 119.8 . .
C6 C7 C8 115.5(9) . .
C6 C7 C15 123.4(10) . .
C8 C7 C15 121.1(11) . .
C7 C8 C9 122.1(9) . .
C7 C8 H8A 118.9 . .
C9 C8 H8A 118.9 . .
N1 C9 C8 121.4(9) . .
N1 C9 H9A 119.3 . .
C8 C9 H9A 119.3 . .
N2 C10 C11 122.8(9) . .
N2 C10 H10A 118.6 . .
C11 C10 H10A 118.6 . .
C10 C11 C12 120.6(9) . .
C10 C11 H11A 119.7 . .
C12 C11 H11A 119.7 . .
C11 C12 C13 115.4(9) . .
C11 C12 C17 120.9(9) . .
C13 C12 C17 123.6(9) . .
C14 C13 C12 120.7(9) . .
C14 C13 H13A 119.7 . .
C12 C13 H13A 119.7 . .
N2 C14 C13 124.3(9) . .
N2 C14 H14A 117.9 . .
C13 C14 H14A 117.9 . .
C7 C15 C16 115.6(9) . .
C7 C15 H15A 108.4 . .
C16 C15 H15A 108.4 . .
C7 C15 H15B 108.4 . .
C16 C15 H15B 108.4 . .
H15A C15 H15B 107.4 . .
C17 C16 C15 112.2(11) . .
C17 C16 H16A 109.2 . .
C15 C16 H16A 109.2 . .
C17 C16 H16B 109.2 . .
C15 C16 H16B 109.2 . .
H16A C16 H16B 107.9 . .
C16 C17 C12 117.1(10) . .
C16 C17 H17A 108.0 . .
C12 C17 H17A 108.0 . .
C16 C17 H17B 108.0 . .
C12 C17 H17B 108.0 . .
H17A C17 H17B 107.3 . .
N3 C18 C19 123.4(9) . .
N3 C18 H18A 118.3 . .
C19 C18 H18A 118.3 . .
C18 C19 C20 120.6(10) . .
C18 C19 H19A 119.7 . .
C20 C19 H19A 119.7 . .
C19 C20 C21 115.4(10) . .
C19 C20 C28 122.2(10) . .
C21 C20 C28 122.4(10) . .
C22 C21 C20 121.3(10) . .
C22 C21 H21A 119.3 . .
C20 C21 H21A 119.3 . .
N3 C22 C21 123.3(9) . .
N3 C22 H22A 118.3 . .
C21 C22 H22A 118.3 . .
N4 C23 C24 122.7(9) . .
N4 C23 H23A 118.6 . .
C24 C23 H23A 118.6 . .
C23 C24 C25 121.1(9) . .
C23 C24 H24A 119.4 . .
C25 C24 H24A 119.4 . .
C26 C25 C24 116.8(10) . .
C26 C25 C30 120.5(13) . .
C24 C25 C30 122.5(13) . .
C25 C26 C27 121.0(9) . .
C25 C26 H26A 119.5 . .
C27 C26 H26A 119.5 . .
N4 C27 C26 122.1(9) . .
N4 C27 H27A 119.0 . .
C26 C27 H27A 119.0 . .
C29 C28 C20 112.7(12) . .
C29 C28 H28A 109.0 . .
C20 C28 H28A 109.0 . .
C29 C28 H28B 109.0 . .
C20 C28 H28B 109.0 . .
H28A C28 H28B 107.8 . .
C28 C29 C30 117.9(14) . .
C28 C29 H29A 107.8 . .
C30 C29 H29A 107.8 . .
C28 C29 H29B 107.8 . .
C30 C29 H29B 107.8 . .
H29A C29 H29B 107.2 . .
C25 C30 C29 118.7(12) . .
C25 C30 H30A 107.6 . .
C29 C30 H30A 107.6 . .
C25 C30 H30B 107.6 . .
C29 C30 H30B 107.6 . .
H30A C30 H30B 107.1 . .
C5 N1 C9 116.3(8) . .
C5 N1 Cd1 123.0(6) . .
C9 N1 Cd1 120.6(5) . .
C14 N2 C10 116.1(8) . .
C14 N2 Cd1 119.8(6) . 3_445
C10 N2 Cd1 123.3(6) . 3_445
C22 N3 C18 115.9(8) . .
C22 N3 Cd1 120.1(7) . .
C18 N3 Cd1 123.8(6) . .
C27 N4 C23 116.2(10) . .
C1 O1 Cd1 91.8(5) . .
C1 O2 Cd1 92.9(5) . .
C4 O3 Cd1 91.9(5) . 4_544
C4 O4 Cd1 93.0(5) . 4_544
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cd1 N2 2.369(7) 3
Cd1 N3 2.379(8) .
Cd1 O4 2.400(6) 4_554
Cd1 N1 2.404(7) .
Cd1 O2 2.417(6) .
Cd1 O1 2.424(6) .
Cd1 O3 2.442(6) 4_554
C1 O2 1.241(10) .
C1 O1 1.273(10) .
C1 C2 1.504(11) .
C2 C3 1.503(13) .
C2 H2A 0.9700 .
C2 H2B 0.9700 .
C3 C4 1.508(11) .
C3 H3A 0.9700 .
C3 H3B 0.9700 .
C4 O3 1.236(10) .
C4 O4 1.267(10) .
C5 N1 1.322(11) .
C5 C6 1.378(15) .
C5 H5A 0.9300 .
C6 C7 1.360(14) .
C6 H6A 0.9300 .
C7 C8 1.361(14) .
C7 C15 1.491(14) .
C8 C9 1.392(13) .
C8 H8A 0.9300 .
C9 N1 1.332(10) .
C9 H9A 0.9300 .
C10 N2 1.345(11) .
C10 C11 1.383(12) .
C10 H10A 0.9300 .
C11 C12 1.388(14) .
C11 H11A 0.9300 .
C12 C13 1.394(13) .
C12 C17 1.539(14) .
C13 C14 1.355(13) .
C13 H13A 0.9300 .
C14 N2 1.334(12) .
C14 H14A 0.9300 .
C15 C16 1.513(15) .
C15 H15A 0.9700 .
C15 H15B 0.9700 .
C16 C17 1.458(16) .
C16 H16A 0.9700 .
C16 H16B 0.9700 .
C17 H17A 0.9700 .
C17 H17B 0.9700 .
C18 N3 1.347(12) .
C18 C19 1.363(14) .
C18 H18A 0.9300 .
C19 C20 1.375(14) .
C19 H19A 0.9300 .
C20 C21 1.377(15) .
C20 C28 1.524(15) .
C21 C22 1.360(13) .
C21 H21A 0.9300 .
C22 N3 1.325(12) .
C22 H22A 0.9300 .
C23 N4 1.359(9) .
C23 C24 1.375(9) .
C23 H23A 0.9300 .
C24 C25 1.377(10) .
C24 H24A 0.9300 .
C25 C26 1.362(9) .
C25 C30 1.427(18) .
C26 C27 1.398(9) .
C26 H26A 0.9300 .
C27 N4 1.358(9) .
C27 H27A 0.9300 .
C28 C29 1.375(18) .
C28 H28A 0.9700 .
C28 H28B 0.9700 .
C29 C30 1.531(18) .
C29 H29A 0.9700 .
C29 H29B 0.9700 .
C30 H30A 0.9700 .
C30 H30B 0.9700 .
N2 Cd1 2.369(7) 3_445
O3 Cd1 2.442(6) 4_544
O4 Cd1 2.400(6) 4_544
