#------------------------------------------------------------------------------
#$Date: 2016-02-05 01:43:50 +0200 (Fri, 05 Feb 2016) $
#$Revision: 176056 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/76/7037625.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7037625
loop_
_publ_author_name
'Wang, Yongli'
'Guo, Wenzhen'
'Liu, Dongling'
'Yang, Ying'
'Zheng, Wenjun'
_publ_section_title
;
 1,2,4-Diazaphospholide complexes of yttrium(iii), dysprosium(iii),
 erbium(iii), and europium(ii,iii): synthesis, X-ray structural
 characterization, and EPR analysis.
;
_journal_issue                   3
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              899
_journal_page_last               903
_journal_paper_doi               10.1039/c5dt04285b
_journal_volume                  45
_journal_year                    2016
_chemical_absolute_configuration syn
_chemical_formula_moiety         'C70 H50 Eu K2 N10 P5, (C7 H8)'
_chemical_formula_sum            'C77 H58 Eu K2 N10 P5'
_chemical_formula_weight         1508.34
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           19
_space_group_name_Hall           'P 2ac 2ab'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-12-02 deposited with the CCDC.
2015-12-04 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.4510(8)
_cell_length_b                   21.6779(9)
_cell_length_c                   22.1731(7)
_cell_measurement_reflns_used    12960
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      26.4160
_cell_measurement_theta_min      3.0320
_cell_volume                     8388.1(6)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.33 (release 27-03-2014 CrysAlis171 .NET)
(compiled Mar 27 2014,17:12:48)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.33 (release 27-03-2014 CrysAlis171 .NET)
(compiled Mar 27 2014,17:12:48)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.33 (release 27-03-2014 CrysAlis171 .NET)
(compiled Mar 27 2014,17:12:48)
;
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 16.0251
_diffrn_detector_type            Eos
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'Xcalibur, Eos'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0785
_diffrn_reflns_av_unetI/netI     0.1321
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            46049
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         2.88
_diffrn_source                   'Enhance (Mo) X-ray Source'
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count 1
_diffrn_standards_interval_time  151.0800
_diffrn_standards_number         50699
_exptl_absorpt_coefficient_mu    0.986
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.40159
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.33 (release 27-03-2014 CrysAlis171 .NET)
(compiled Mar 27 2014,17:12:48)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.194
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             3064
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.381
_refine_diff_density_min         -0.707
_refine_diff_density_rms         0.089
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   -0.007(13)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.979
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     845
_refine_ls_number_reflns         17091
_refine_ls_number_restraints     114
_refine_ls_restrained_S_all      0.999
_refine_ls_R_factor_all          0.1198
_refine_ls_R_factor_gt           0.0724
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0747P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1539
_refine_ls_wR_factor_ref         0.1793
_reflns_number_gt                10225
_reflns_number_total             17091
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5dt04285b2.cif
_cod_data_source_block           compound8
_cod_depositor_comments
'Adding full bibliography for 7037620--7037625.cif.'
_cod_database_code               7037625
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C -0.0698(6) -0.0190(6) -0.0417(4) 0.081(3) Uani 1 1 d .
H1 H -0.0554 -0.0599 -0.0469 0.097 Uiso 1 1 calc R
C2 C -0.1145(8) 0.0085(8) -0.0848(5) 0.108(4) Uani 1 1 d .
H2 H -0.1308 -0.0142 -0.1180 0.129 Uiso 1 1 calc R
C3 C -0.1356(7) 0.0694(9) -0.0793(6) 0.118(5) Uani 1 1 d .
H3 H -0.1632 0.0889 -0.1096 0.141 Uiso 1 1 calc R
C4 C -0.1150(6) 0.1005(6) -0.0282(5) 0.101(4) Uani 1 1 d .
H4 H -0.1321 0.1407 -0.0220 0.121 Uiso 1 1 calc R
C5 C -0.0681(6) 0.0719(5) 0.0150(5) 0.075(3) Uani 1 1 d .
H5 H -0.0520 0.0941 0.0486 0.090 Uiso 1 1 calc R
C6 C -0.0459(5) 0.0119(5) 0.0085(4) 0.068(3) Uani 1 1 d .
C7 C 0.0018(5) -0.0212(4) 0.0532(3) 0.053(2) Uani 1 1 d .
C8 C 0.0708(5) -0.0843(5) 0.1249(3) 0.056(2) Uani 1 1 d .
C9 C 0.1085(5) -0.1276(4) 0.1665(3) 0.056(2) Uani 1 1 d .
C10 C 0.1660(6) -0.1106(5) 0.2090(4) 0.072(3) Uani 1 1 d .
H10 H 0.1831 -0.0700 0.2107 0.086 Uiso 1 1 calc R
C11 C 0.1966(7) -0.1542(6) 0.2477(5) 0.093(4) Uani 1 1 d .
H11 H 0.2281 -0.1416 0.2792 0.112 Uiso 1 1 calc R
C12 C 0.1807(8) -0.2164(6) 0.2400(6) 0.099(4) Uani 1 1 d .
H12 H 0.2062 -0.2458 0.2630 0.118 Uiso 1 1 calc R
C13 C 0.1231(8) -0.2352(6) 0.1952(7) 0.122(5) Uani 1 1 d .
H13 H 0.1294 -0.2757 0.1763 0.146 Uiso 1 1 calc R
C14 C 0.0918(7) -0.1912(5) 0.1626(5) 0.086(3) Uani 1 1 d .
H14 H 0.0714 -0.2047 0.1236 0.103 Uiso 1 1 calc R
C15 C -0.0628(7) -0.0747(6) 0.3545(5) 0.094(4) Uani 1 1 d .
H15 H -0.0407 -0.0672 0.3945 0.112 Uiso 1 1 calc R
C16 C -0.1337(8) -0.1036(6) 0.3501(7) 0.109(5) Uani 1 1 d .
H16 H -0.1615 -0.1133 0.3873 0.130 Uiso 1 1 calc R
C17 C -0.1700(8) -0.1082(8) 0.2987(7) 0.123(6) Uani 1 1 d .
H17 H -0.2240 -0.1206 0.2979 0.147 Uiso 1 1 calc R
C18 C -0.1332(7) -0.0887(6) 0.2453(6) 0.103(4) Uani 1 1 d .
H18 H -0.1618 -0.0888 0.2072 0.124 Uiso 1 1 calc R
C19 C -0.0621(7) -0.0605(5) 0.2478(5) 0.078(3) Uani 1 1 d .
H19 H -0.0397 -0.0440 0.2106 0.094 Uiso 1 1 calc R
C20 C -0.0244(7) -0.0510(4) 0.3024(4) 0.072(3) Uani 1 1 d .
C21 C 0.0504(6) -0.0227(4) 0.3050(4) 0.062(2) Uani 1 1 d .
C22 C 0.1781(6) 0.0140(4) 0.3220(4) 0.063(2) Uani 1 1 d .
C23 C 0.2565(6) 0.0339(5) 0.3366(3) 0.065(3) Uani 1 1 d .
C24 C 0.2983(7) 0.0023(5) 0.3810(4) 0.085(3) Uani 1 1 d .
H24 H 0.2994 -0.0422 0.3734 0.102 Uiso 1 1 calc R
C25 C 0.3698(7) 0.0247(6) 0.3960(5) 0.093(4) Uani 1 1 d .
H25 H 0.4073 -0.0089 0.3940 0.112 Uiso 1 1 calc R
C26 C 0.4024(8) 0.0798(8) 0.3694(6) 0.131(5) Uani 1 1 d .
H26 H 0.4498 0.0955 0.3810 0.158 Uiso 1 1 calc R
C27 C 0.3578(7) 0.1071(6) 0.3259(6) 0.106(4) Uani 1 1 d .
H27 H 0.3769 0.1414 0.3057 0.127 Uiso 1 1 calc R
C28 C 0.2886(6) 0.0864(5) 0.3113(4) 0.075(3) Uani 1 1 d .
H28 H 0.2604 0.1081 0.2827 0.091 Uiso 1 1 calc R
C29 C 0.4433(7) 0.0541(8) 0.1736(7) 0.136(3) Uani 1 1 d U
H29 H 0.4584 0.0876 0.1503 0.163 Uiso 1 1 calc R
C30 C 0.4965(9) 0.0255(9) 0.2153(6) 0.144(3) Uani 1 1 d U
H30 H 0.5462 0.0408 0.2180 0.173 Uiso 1 1 calc R
C31 C 0.4768(9) -0.0208(9) 0.2490(8) 0.141(3) Uani 1 1 d U
H31 H 0.5120 -0.0393 0.2748 0.170 Uiso 1 1 calc R
C32 C 0.4063(8) -0.0408(8) 0.2458(6) 0.135(3) Uani 1 1 d U
H32 H 0.3909 -0.0721 0.2717 0.162 Uiso 1 1 calc R
C33 C 0.3527(8) -0.0169(8) 0.2047(6) 0.125(3) Uani 1 1 d U
H33 H 0.3041 -0.0343 0.2020 0.150 Uiso 1 1 calc R
C34 C 0.3715(7) 0.0315(8) 0.1691(6) 0.122(3) Uani 1 1 d U
C35 C 0.3176(5) 0.0570(5) 0.1250(4) 0.070(3) Uani 1 1 d .
C36 C 0.2441(5) 0.1031(4) 0.0441(4) 0.063(3) Uani 1 1 d .
C37 C 0.2060(5) 0.1288(4) -0.0102(3) 0.057(2) Uani 1 1 d .
C38 C 0.1281(6) 0.1217(5) -0.0185(4) 0.073(3) Uani 1 1 d .
H38 H 0.0984 0.1009 0.0098 0.087 Uiso 1 1 calc R
C39 C 0.0951(7) 0.1467(6) -0.0705(4) 0.093(4) Uani 1 1 d .
H39 H 0.0422 0.1446 -0.0754 0.112 Uiso 1 1 calc R
C40 C 0.1357(10) 0.1726(7) -0.1119(6) 0.126(6) Uani 1 1 d .
H40 H 0.1133 0.1844 -0.1482 0.151 Uiso 1 1 calc R
C41 C 0.2136(9) 0.1826(6) -0.1017(5) 0.097(4) Uani 1 1 d .
H41 H 0.2416 0.2058 -0.1292 0.117 Uiso 1 1 calc R
C42 C 0.2487(6) 0.1598(5) -0.0535(4) 0.071(3) Uani 1 1 d .
H42 H 0.3013 0.1646 -0.0488 0.086 Uiso 1 1 calc R
C43 C -0.2307(8) 0.1306(8) 0.1588(6) 0.127(3) Uani 1 1 d U
H43 H -0.2390 0.1602 0.1293 0.152 Uiso 1 1 calc R
C44 C -0.2924(9) 0.0941(9) 0.1834(7) 0.161(3) Uani 1 1 d U
H44 H -0.3413 0.0956 0.1666 0.193 Uiso 1 1 calc R
C45 C -0.2762(9) 0.0554(8) 0.2343(6) 0.133(3) Uani 1 1 d U
H45 H -0.3145 0.0296 0.2489 0.159 Uiso 1 1 calc R
C46 C -0.2070(8) 0.0554(7) 0.2619(7) 0.127(3) Uani 1 1 d U
H46 H -0.1999 0.0343 0.2979 0.152 Uiso 1 1 calc R
C47 C -0.1466(7) 0.0873(8) 0.2356(6) 0.118(3) Uani 1 1 d U
H47 H -0.0990 0.0874 0.2543 0.141 Uiso 1 1 calc R
C48 C -0.1562(7) 0.1187(7) 0.1823(6) 0.111(3) Uani 1 1 d U
C49 C -0.0914(6) 0.1520(5) 0.1531(4) 0.070(3) Uani 1 1 d .
C50 C -0.0004(7) 0.2155(5) 0.0970(4) 0.074(3) Uani 1 1 d .
C51 C 0.0482(7) 0.2552(5) 0.0616(5) 0.083(3) Uani 1 1 d .
C52 C 0.0176(11) 0.2943(7) 0.0224(6) 0.127(6) Uani 1 1 d .
H52 H -0.0351 0.2959 0.0166 0.152 Uiso 1 1 calc R
C53 C 0.0698(17) 0.3350(10) -0.0119(9) 0.165(9) Uani 1 1 d .
H53 H 0.0495 0.3655 -0.0367 0.198 Uiso 1 1 calc R
C54 C 0.1430(14) 0.3287(9) -0.0076(8) 0.147(9) Uani 1 1 d .
H54 H 0.1746 0.3530 -0.0316 0.176 Uiso 1 1 calc R
C55 C 0.1731(10) 0.2904(6) 0.0283(6) 0.117(5) Uani 1 1 d .
H55 H 0.2261 0.2873 0.0309 0.140 Uiso 1 1 calc R
C56 C 0.1252(8) 0.2516(5) 0.0654(4) 0.089(4) Uani 1 1 d .
H56 H 0.1476 0.2239 0.0922 0.107 Uiso 1 1 calc R
C57 C 0.3329(6) 0.2874(4) 0.2387(4) 0.143(7) Uani 1 1 d G
H57 H 0.3202 0.3040 0.2761 0.171 Uiso 1 1 calc R
C58 C 0.3997(5) 0.3059(4) 0.2097(6) 0.161(8) Uani 1 1 d G
H58 H 0.4316 0.3349 0.2277 0.193 Uiso 1 1 calc R
C59 C 0.4187(5) 0.2810(5) 0.1539(6) 0.161(8) Uani 1 1 d G
H59 H 0.4634 0.2934 0.1345 0.193 Uiso 1 1 calc R
C60 C 0.3709(7) 0.2377(5) 0.1271(4) 0.137(6) Uani 1 1 d G
H60 H 0.3837 0.2211 0.0897 0.164 Uiso 1 1 calc R
C61 C 0.3041(6) 0.2192(4) 0.1560(4) 0.127(5) Uani 1 1 d G
H61 H 0.2722 0.1902 0.1381 0.152 Uiso 1 1 calc R
C62 C 0.2851(4) 0.2440(4) 0.2118(4) 0.094(4) Uani 1 1 d G
C63 C 0.2158(7) 0.2221(5) 0.2446(5) 0.082(3) Uani 1 1 d .
C64 C 0.1102(7) 0.1952(4) 0.3095(3) 0.071(3) Uani 1 1 d .
C65 C 0.0508(7) 0.1786(6) 0.3563(4) 0.080(4) Uani 1 1 d .
C66 C 0.0458(7) 0.2151(7) 0.4074(4) 0.099(4) Uani 1 1 d .
H66 H 0.0765 0.2496 0.4136 0.119 Uiso 1 1 calc R
C67 C -0.0096(11) 0.1956(10) 0.4490(5) 0.139(8) Uani 1 1 d .
H67 H -0.0115 0.2167 0.4856 0.167 Uiso 1 1 calc R
C68 C -0.0604(12) 0.1497(10) 0.4415(9) 0.152(9) Uani 1 1 d .
H68 H -0.0983 0.1408 0.4697 0.182 Uiso 1 1 calc R
C69 C -0.0524(9) 0.1180(7) 0.3910(6) 0.123(6) Uani 1 1 d .
H69 H -0.0861 0.0856 0.3837 0.148 Uiso 1 1 calc R
C70 C 0.0024(8) 0.1302(6) 0.3490(5) 0.099(4) Uani 1 1 d .
H70 H 0.0068 0.1052 0.3151 0.118 Uiso 1 1 calc R
C71 C 0.2324(10) 0.1726(8) 0.5654(8) 0.141(3) Uani 1 1 d U
H71 H 0.2572 0.1996 0.5950 0.170 Uiso 1 1 calc R
C72 C 0.1755(11) 0.1338(8) 0.5816(8) 0.142(3) Uani 1 1 d U
H72 H 0.1636 0.1323 0.6247 0.170 Uiso 1 1 calc R
C73 C 0.1324(10) 0.0988(8) 0.5465(7) 0.142(3) Uani 1 1 d U
H73 H 0.0872 0.0766 0.5611 0.171 Uiso 1 1 calc R
C74 C 0.1518(10) 0.1029(8) 0.4860(7) 0.139(3) Uani 1 1 d U
H74 H 0.1197 0.0799 0.4575 0.167 Uiso 1 1 calc R
C75 C 0.2127(10) 0.1392(8) 0.4611(8) 0.137(3) Uani 1 1 d U
H75 H 0.2192 0.1441 0.4175 0.164 Uiso 1 1 calc R
C76 C 0.2532(11) 0.1749(8) 0.5021(8) 0.144(3) Uani 1 1 d U
C77 C 0.3163(10) 0.2094(8) 0.4718(7) 0.157(4) Uani 1 1 d U
H77A H 0.3566 0.1814 0.4612 0.235 Uiso 1 1 calc R
H77B H 0.3358 0.2404 0.4986 0.235 Uiso 1 1 calc R
H77C H 0.2969 0.2288 0.4359 0.235 Uiso 1 1 calc R
Eu1 Eu 0.10732(2) 0.08339(2) 0.176207(16) 0.04759(13) Uani 1 1 d .
K1 K 0.30191(16) 0.03529(13) 0.53468(12) 0.0932(8) Uani 1 1 d .
K2 K 0.03102(18) 0.28572(13) 0.21527(12) 0.0995(9) Uani 1 1 d .
N1 N 0.2032(4) 0.0897(3) 0.0937(3) 0.0559(17) Uani 1 1 d .
N2 N 0.2417(4) 0.0647(4) 0.1402(3) 0.065(2) Uani 1 1 d .
N3 N -0.0197(4) 0.1342(4) 0.1610(3) 0.0551(18) Uani 1 1 d .
N4 N 0.0309(4) 0.1672(4) 0.1291(3) 0.0593(19) Uani 1 1 d .
N5 N 0.0445(4) 0.0122(4) 0.0929(3) 0.0562(19) Uani 1 1 d .
N6 N 0.0838(4) -0.0219(4) 0.1334(3) 0.0551(18) Uani 1 1 d .
N7 N 0.0727(4) 0.0146(3) 0.2625(3) 0.0523(19) Uani 1 1 d .
N8 N 0.1447(4) 0.0363(3) 0.2713(3) 0.0576(19) Uani 1 1 d .
N9 N 0.1706(5) 0.1807(3) 0.2193(3) 0.0579(19) Uani 1 1 d .
N10 N 0.1089(5) 0.1657(3) 0.2557(3) 0.0615(18) Uani 1 1 d .
P1 P 0.00878(16) -0.09994(12) 0.06641(11) 0.0694(7) Uani 1 1 d .
P2 P 0.34060(14) 0.08239(17) 0.05197(12) 0.0795(8) Uani 1 1 d .
P3 P 0.1183(2) -0.03572(14) 0.36321(10) 0.0798(9) Uani 1 1 d .
P4 P -0.0998(2) 0.21875(16) 0.10625(13) 0.0940(10) Uani 1 1 d .
P5 P 0.1870(2) 0.24713(14) 0.31742(13) 0.0888(9) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C6 C1 C2 122.0(12) . .
C6 C1 H1 119.0 . .
C2 C1 H1 119.0 . .
C1 C2 C3 120.5(12) . .
C1 C2 H2 119.7 . .
C3 C2 H2 119.7 . .
C4 C3 C2 118.6(12) . .
C4 C3 H3 120.7 . .
C2 C3 H3 120.7 . .
C3 C4 C5 120.0(13) . .
C3 C4 H4 120.0 . .
C5 C4 H4 120.0 . .
C6 C5 C4 120.9(11) . .
C6 C5 H5 119.5 . .
C4 C5 H5 119.5 . .
C1 C6 C5 117.9(10) . .
C1 C6 C7 118.8(10) . .
C5 C6 C7 123.3(9) . .
N5 C7 C6 119.0(8) . .
N5 C7 P1 112.1(6) . .
C6 C7 P1 128.9(7) . .
N5 C7 K1 65.3(4) . 2_554
C6 C7 K1 121.3(5) . 2_554
P1 C7 K1 82.2(3) . 2_554
N6 C8 C9 117.7(7) . .
N6 C8 P1 113.4(7) . .
C9 C8 P1 128.8(7) . .
N6 C8 K1 69.1(4) . 2_554
C9 C8 K1 107.2(5) . 2_554
P1 C8 K1 91.8(3) . 2_554
C14 C9 C10 116.0(9) . .
C14 C9 C8 119.5(9) . .
C10 C9 C8 124.3(8) . .
C11 C10 C9 120.3(10) . .
C11 C10 H10 119.8 . .
C9 C10 H10 119.8 . .
C10 C11 C12 120.8(10) . .
C10 C11 H11 119.6 . .
C12 C11 H11 119.6 . .
C11 C12 C13 119.2(11) . .
C11 C12 H12 120.4 . .
C13 C12 H12 120.4 . .
C14 C13 C12 117.0(14) . .
C14 C13 K2 83.9(8) . 3_545
C12 C13 K2 96.3(8) . 3_545
C14 C13 H13 117.5 . .
C12 C13 H13 117.5 . .
K2 C13 H13 117.5 3_545 .
C13 C14 C9 126.1(12) . .
C13 C14 K2 74.0(7) . 3_545
C9 C14 K2 102.6(6) . 3_545
C13 C14 H14 114.8 . .
C9 C14 H14 114.8 . .
K2 C14 H14 114.8 3_545 .
C16 C15 C20 121.3(11) . .
C16 C15 K2 73.5(8) . 3_545
C20 C15 K2 82.9(6) . 3_545
C16 C15 H15 119.2 . .
C20 C15 H15 119.2 . .
K2 C15 H15 119.2 3_545 .
C17 C16 C15 121.9(12) . .
C17 C16 K2 80.0(10) . 3_545
C15 C16 K2 82.9(8) . 3_545
C17 C16 H16 118.5 . .
C15 C16 H16 118.5 . .
K2 C16 H16 118.5 3_545 .
C16 C17 C18 119.2(13) . .
C16 C17 K2 77.5(10) . 3_545
C18 C17 K2 78.4(9) . 3_545
C16 C17 H17 120.2 . .
C18 C17 H17 120.2 . .
K2 C17 H17 120.2 3_545 .
C19 C18 C17 120.4(12) . .
C19 C18 K2 82.7(7) . 3_545
C17 C18 K2 77.4(9) . 3_545
C19 C18 H18 119.4 . .
C17 C18 H18 119.4 . .
K2 C18 H18 119.4 3_545 .
C18 C19 C20 121.6(11) . .
C18 C19 K2 74.1(7) . 3_545
C20 C19 K2 82.2(6) . 3_545
C18 C19 H19 119.1 . .
C20 C19 H19 119.1 . .
K2 C19 H19 119.1 3_545 .
C19 C20 C15 115.4(10) . .
C19 C20 C21 121.7(9) . .
C15 C20 C21 122.9(10) . .
N7 C21 C20 120.4(8) . .
N7 C21 P3 115.2(7) . .
C20 C21 P3 124.4(7) . .
N8 C22 C23 118.6(8) . .
N8 C22 P3 113.2(7) . .
C23 C22 P3 128.2(7) . .
C28 C23 C24 118.2(10) . .
C28 C23 C22 121.9(8) . .
C24 C23 C22 119.7(10) . .
C25 C24 C23 117.9(11) . .
C25 C24 K1 71.1(6) . .
C23 C24 K1 126.5(7) . .
C25 C24 H24 111.7 . .
C23 C24 H24 111.7 . .
K1 C24 H24 111.7 . .
C24 C25 C26 123.2(10) . .
C24 C25 K1 85.7(7) . .
C26 C25 K1 117.5(9) . .
C24 C25 H25 109.4 . .
C26 C25 H25 109.4 . .
K1 C25 H25 109.4 . .
C27 C26 C25 114.7(11) . .
C27 C26 H26 122.7 . .
C25 C26 H26 122.7 . .
C28 C27 C26 122.8(11) . .
C28 C27 H27 118.6 . .
C26 C27 H27 118.6 . .
C27 C28 C23 123.1(10) . .
C27 C28 H28 118.4 . .
C23 C28 H28 118.4 . .
C34 C29 C30 119.2(15) . .
C34 C29 H29 120.4 . .
C30 C29 H29 120.4 . .
C31 C30 C29 121.8(16) . .
C31 C30 H30 119.1 . .
C29 C30 H30 119.1 . .
C30 C31 C32 118.3(17) . .
C30 C31 H31 120.8 . .
C32 C31 H31 120.8 . .
C31 C32 C33 122.7(17) . .
C31 C32 H32 118.6 . .
C33 C32 H32 118.6 . .
C34 C33 C32 120.2(15) . .
C34 C33 H33 119.9 . .
C32 C33 H33 119.9 . .
C29 C34 C33 117.6(13) . .
C29 C34 C35 120.6(14) . .
C33 C34 C35 121.7(12) . .
N2 C35 C34 120.0(9) . .
N2 C35 P2 114.1(7) . .
C34 C35 P2 125.9(8) . .
N2 C35 K1 68.8(5) . 2_554
C34 C35 K1 123.1(8) . 2_554
P2 C35 K1 77.8(3) . 2_554
N1 C36 C37 120.4(7) . .
N1 C36 P2 112.0(7) . .
C37 C36 P2 127.5(6) . .
N1 C36 K1 73.1(5) . 2_554
C37 C36 K1 101.0(5) . 2_554
P2 C36 K1 90.4(4) . 2_554
C38 C37 C42 119.3(9) . .
C38 C37 C36 120.5(8) . .
C42 C37 C36 120.1(8) . .
C37 C38 C39 118.2(9) . .
C37 C38 H38 120.9 . .
C39 C38 H38 120.9 . .
C40 C39 C38 122.0(12) . .
C40 C39 H39 119.0 . .
C38 C39 H39 119.0 . .
C39 C40 C41 119.2(13) . .
C39 C40 H40 120.4 . .
C41 C40 H40 120.4 . .
C42 C41 C40 121.5(12) . .
C42 C41 H41 119.2 . .
C40 C41 H41 119.2 . .
C41 C42 C37 119.3(10) . .
C41 C42 H42 120.3 . .
C37 C42 H42 120.3 . .
C48 C43 C44 116.4(15) . .
C48 C43 H43 121.8 . .
C44 C43 H43 121.8 . .
C45 C44 C43 118.0(15) . .
C45 C44 H44 121.0 . .
C43 C44 H44 121.0 . .
C46 C45 C44 122.1(16) . .
C46 C45 H45 119.0 . .
C44 C45 H45 119.0 . .
C45 C46 C47 119.2(15) . .
C45 C46 H46 120.4 . .
C47 C46 H46 120.4 . .
C48 C47 C46 121.0(13) . .
C48 C47 H47 119.5 . .
C46 C47 H47 119.5 . .
C47 C48 C43 121.1(13) . .
C47 C48 C49 121.4(11) . .
C43 C48 C49 116.5(13) . .
N3 C49 C48 121.3(10) . .
N3 C49 P4 113.0(8) . .
C48 C49 P4 125.6(9) . .
N4 C50 C51 120.1(10) . .
N4 C50 P4 111.3(8) . .
C51 C50 P4 128.6(8) . .
N4 C50 K2 82.3(5) . .
C51 C50 K2 93.7(7) . .
P4 C50 K2 93.3(4) . .
C52 C51 C56 118.6(14) . .
C52 C51 C50 120.1(13) . .
C56 C51 C50 121.2(11) . .
C52 C51 K2 119.0(9) . .
C56 C51 K2 92.0(7) . .
C50 C51 K2 62.0(6) . .
C51 C52 C53 118.1(17) . .
C51 C52 H52 121.0 . .
C53 C52 H52 121.0 . .
C54 C53 C52 121(2) . .
C54 C53 H53 119.7 . .
C52 C53 H53 119.7 . .
C55 C54 C53 122(2) . .
C55 C54 H54 119.1 . .
C53 C54 H54 119.1 . .
C54 C55 C56 120.2(17) . .
C54 C55 H55 119.9 . .
C56 C55 H55 119.9 . .
C51 C56 C55 120.5(13) . .
C51 C56 H56 119.8 . .
C55 C56 H56 119.8 . .
C58 C57 C62 120.0 . .
C58 C57 H57 120.0 . .
C62 C57 H57 120.0 . .
C57 C58 C59 120.0 . .
C57 C58 H58 120.0 . .
C59 C58 H58 120.0 . .
C60 C59 C58 120.0 . .
C60 C59 H59 120.0 . .
C58 C59 H59 120.0 . .
C59 C60 C61 120.0 . .
C59 C60 H60 120.0 . .
C61 C60 H60 120.0 . .
C62 C61 C60 120.0 . .
C62 C61 H61 120.0 . .
C60 C61 H61 120.0 . .
C61 C62 C57 120.0 . .
C61 C62 C63 120.3(8) . .
C57 C62 C63 119.6(8) . .
N9 C63 C62 119.7(9) . .
N9 C63 P5 115.2(8) . .
C62 C63 P5 125.2(7) . .
N10 C64 C65 118.8(10) . .
N10 C64 P5 113.8(8) . .
C65 C64 P5 127.3(7) . .
N10 C64 K2 72.9(4) . .
C65 C64 K2 107.5(6) . .
P5 C64 K2 90.1(4) . .
C70 C65 C66 120.0(12) . .
C70 C65 C64 122.0(9) . .
C66 C65 C64 118.0(12) . .
C65 C66 C67 114.2(14) . .
C65 C66 H66 122.9 . .
C67 C66 H66 122.9 . .
C68 C67 C66 126.7(16) . .
C68 C67 H67 116.7 . .
C66 C67 H67 116.7 . .
C69 C68 C67 114.9(16) . .
C69 C68 H68 122.6 . .
C67 C68 H68 122.6 . .
C68 C69 C70 123.6(17) . .
C68 C69 H69 118.2 . .
C70 C69 H69 118.2 . .
C65 C70 C69 120.5(12) . .
C65 C70 H70 119.8 . .
C69 C70 H70 119.8 . .
C72 C71 C76 118(2) . .
C72 C71 K1 76.3(11) . .
C76 C71 K1 74.8(9) . .
C72 C71 H71 121.2 . .
C76 C71 H71 121.2 . .
K1 C71 H71 121.2 . .
C73 C72 C71 128(2) . .
C73 C72 K1 79.6(10) . .
C71 C72 K1 79.9(11) . .
C73 C72 H72 115.9 . .
C71 C72 H72 115.9 . .
K1 C72 H72 115.9 . .
C72 C73 C74 113(2) . .
C72 C73 K1 77.0(10) . .
C74 C73 K1 74.3(9) . .
C72 C73 H73 123.1 . .
C74 C73 H73 123.1 . .
K1 C73 H73 123.1 . .
C73 C74 C75 126.0(18) . .
C73 C74 K1 81.0(9) . .
C75 C74 K1 76.9(9) . .
C73 C74 H74 117.0 . .
C75 C74 H74 117.0 . .
K1 C74 H74 117.0 . .
C76 C75 C74 115.6(18) . .
C76 C75 K1 79.0(9) . .
C74 C75 K1 77.2(9) . .
C76 C75 H75 121.8 . .
C74 C75 H75 121.8 . .
K1 C75 H75 121.8 . .
C75 C76 C71 119(2) . .
C75 C76 C77 111.1(18) . .
C71 C76 C77 130(2) . .
C75 C76 K1 76.0(10) . .
C71 C76 K1 79.5(10) . .
C77 C76 K1 112.2(11) . .
C76 C77 H77A 109.5 . .
C76 C77 H77B 109.5 . .
H77A C77 H77B 109.5 . .
C76 C77 H77C 109.5 . .
H77A C77 H77C 109.5 . .
H77B C77 H77C 109.5 . .
N8 Eu1 N1 118.8(2) . .
N8 Eu1 N4 144.6(2) . .
N1 Eu1 N4 90.7(2) . .
N8 Eu1 N3 122.7(2) . .
N1 Eu1 N3 118.3(2) . .
N4 Eu1 N3 31.2(2) . .
N8 Eu1 N7 31.9(2) . .
N1 Eu1 N7 139.5(2) . .
N4 Eu1 N7 128.9(3) . .
N3 Eu1 N7 98.7(2) . .
N8 Eu1 N6 89.4(2) . .
N1 Eu1 N6 83.2(2) . .
N4 Eu1 N6 114.8(2) . .
N3 Eu1 N6 101.8(2) . .
N7 Eu1 N6 72.9(2) . .
N8 Eu1 N10 71.8(2) . .
N1 Eu1 N10 118.1(3) . .
N4 Eu1 N10 77.3(2) . .
N3 Eu1 N10 77.9(2) . .
N7 Eu1 N10 83.7(2) . .
N6 Eu1 N10 156.3(2) . .
N8 Eu1 N2 87.6(2) . .
N1 Eu1 N2 31.3(2) . .
N4 Eu1 N2 119.1(2) . .
N3 Eu1 N2 149.0(2) . .
N7 Eu1 N2 111.9(2) . .
N6 Eu1 N2 83.4(2) . .
N10 Eu1 N2 109.1(3) . .
N8 Eu1 N9 84.7(2) . .
N1 Eu1 N9 86.5(2) . .
N4 Eu1 N9 77.6(2) . .
N3 Eu1 N9 94.0(2) . .
N7 Eu1 N9 108.1(2) . .
N6 Eu1 N9 163.8(2) . .
N10 Eu1 N9 31.6(2) . .
N2 Eu1 N9 81.3(3) . .
N8 Eu1 N5 118.1(2) . .
N1 Eu1 N5 78.3(2) . .
N4 Eu1 N5 84.9(2) . .
N3 Eu1 N5 78.2(2) . .
N7 Eu1 N5 95.0(2) . .
N6 Eu1 N5 30.3(2) . .
N10 Eu1 N5 155.6(2) . .
N2 Eu1 N5 94.1(2) . .
N9 Eu1 N5 156.6(2) . .
N8 Eu1 K1 106.19(18) . 2_554
N1 Eu1 K1 42.00(17) . 2_554
N4 Eu1 K1 108.95(16) . 2_554
N3 Eu1 K1 119.06(15) . 2_554
N7 Eu1 K1 106.67(17) . 2_554
N6 Eu1 K1 41.30(15) . 2_554
N10 Eu1 K1 157.3(2) . 2_554
N2 Eu1 K1 48.40(17) . 2_554
N9 Eu1 K1 126.67(18) . 2_554
N5 Eu1 K1 45.81(14) . 2_554
N8 Eu1 K2 108.10(18) . .
N1 Eu1 K2 106.09(18) . .
N4 Eu1 K2 40.25(17) . .
N3 Eu1 K2 50.01(18) . .
N7 Eu1 K2 110.48(17) . .
N6 Eu1 K2 151.66(15) . .
N10 Eu1 K2 37.22(17) . .
N2 Eu1 K2 118.51(19) . .
N9 Eu1 K2 43.99(18) . .
N5 Eu1 K2 124.05(15) . .
K1 Eu1 K2 142.45(5) 2_554 .
N6 K1 N1 67.17(19) 2 2
N6 K1 C36 91.7(2) 2 2
N1 K1 C36 25.28(17) 2 2
N6 K1 N5 25.30(16) 2 2
N1 K1 N5 63.4(2) 2 2
C36 K1 N5 82.9(2) 2 2
N6 K1 C8 25.8(2) 2 2
N1 K1 C8 92.7(2) 2 2
C36 K1 C8 117.5(2) 2 2
N5 K1 C8 41.8(2) 2 2
N6 K1 C75 140.6(4) 2 .
N1 K1 C75 147.6(4) 2 .
C36 K1 C75 126.1(4) 2 .
N5 K1 C75 149.0(4) 2 .
C8 K1 C75 115.4(4) 2 .
N6 K1 C74 147.6(3) 2 .
N1 K1 C74 122.4(4) 2 .
C36 K1 C74 104.7(4) 2 .
N5 K1 C74 171.2(4) 2 .
C8 K1 C74 129.4(4) 2 .
C75 K1 C74 26.0(4) . .
N6 K1 C76 115.6(4) 2 .
N1 K1 C76 159.1(4) 2 .
C36 K1 C76 148.4(4) 2 .
N5 K1 C76 128.5(4) 2 .
C8 K1 C76 90.6(4) 2 .
C75 K1 C76 25.0(4) . .
C74 K1 C76 43.7(5) . .
N6 K1 C72 106.5(4) 2 .
N1 K1 C72 115.7(4) 2 .
C36 K1 C72 116.0(4) 2 .
N5 K1 C72 131.6(4) 2 .
C8 K1 C72 93.1(4) 2 .
C75 K1 C72 50.7(4) . .
C74 K1 C72 41.1(4) . .
C76 K1 C72 43.5(5) . .
N6 K1 C73 126.0(3) 2 .
N1 K1 C73 108.5(3) 2 .
C36 K1 C73 99.6(4) 2 .
N5 K1 C73 150.9(3) 2 .
C8 K1 C73 116.2(4) 2 .
C75 K1 C73 45.7(4) . .
C74 K1 C73 24.7(3) . .
C76 K1 C73 52.0(5) . .
C72 K1 C73 23.4(4) . .
N6 K1 N2 64.26(19) 2 2
N1 K1 N2 24.21(17) 2 2
C36 K1 N2 41.9(2) 2 2
N5 K1 N2 71.8(2) 2 2
C8 K1 N2 86.2(2) 2 2
C75 K1 N2 136.0(4) . 2
C74 K1 N2 110.8(4) . 2
C76 K1 N2 136.0(4) . 2
C72 K1 N2 92.8(4) . 2
C73 K1 N2 90.7(3) . 2
N6 K1 C71 100.6(3) 2 .
N1 K1 C71 135.6(4) 2 .
C36 K1 C71 139.8(4) 2 .
N5 K1 C71 121.7(4) 2 .
C8 K1 C71 79.9(4) 2 .
C75 K1 C71 44.4(4) . .
C74 K1 C71 49.5(5) . .
C76 K1 C71 25.7(4) . .
C72 K1 C71 23.9(4) . .
C73 K1 C71 43.0(4) . .
N2 K1 C71 111.4(4) 2 .
N10 K2 C50 84.7(2) . .
N10 K2 C64 24.93(18) . .
C50 K2 C64 109.3(2) . .
N10 K2 N4 59.61(18) . .
C50 K2 N4 25.2(2) . .
C64 K2 N4 84.1(2) . .
N10 K2 C16 120.0(3) . 3
C50 K2 C16 94.7(3) . 3
C64 K2 C16 119.8(4) . 3
N4 K2 C16 108.6(3) . 3
N10 K2 N9 24.52(18) . .
C50 K2 N9 79.3(2) . .
C64 K2 N9 40.9(2) . .
N4 K2 N9 57.90(19) . .
C16 K2 N9 96.3(3) 3 .
N10 K2 C17 106.7(3) . 3
C50 K2 C17 112.9(4) . 3
C64 K2 C17 99.8(3) . 3
N4 K2 C17 119.7(3) . 3
C16 K2 C17 22.5(3) 3 3
N9 K2 C17 86.7(3) . 3
N10 K2 C18 112.0(3) . 3
C50 K2 C18 135.6(3) . 3
C64 K2 C18 95.6(3) . 3
N4 K2 C18 143.5(3) . 3
C16 K2 C18 41.0(3) 3 3
N9 K2 C18 99.1(3) . 3
C17 K2 C18 24.2(3) 3 3
N10 K2 C13 93.9(3) . 3
C50 K2 C13 107.0(3) . 3
C64 K2 C13 82.9(4) . 3
N4 K2 C13 104.0(3) . 3
C16 K2 C13 141.5(3) 3 3
N9 K2 C13 118.4(3) . 3
C17 K2 C13 136.3(3) 3 3
C18 K2 C13 112.2(3) 3 3
N10 K2 C15 143.6(3) . 3
C50 K2 C15 94.6(3) . 3
C64 K2 C15 140.1(3) . 3
N4 K2 C15 115.9(2) . 3
C16 K2 C15 23.6(3) 3 3
N9 K2 C15 119.6(2) . 3
C17 K2 C15 40.5(3) 3 3
C18 K2 C15 47.3(3) 3 3
C13 K2 C15 120.7(3) 3 3
N10 K2 C19 132.5(2) . 3
C50 K2 C19 134.6(3) . 3
C64 K2 C19 111.6(3) . 3
N4 K2 C19 155.6(2) . 3
C16 K2 C19 47.7(3) 3 3
N9 K2 C19 122.3(3) . 3
C17 K2 C19 41.6(3) 3 3
C18 K2 C19 23.3(3) 3 3
C13 K2 C19 96.6(3) 3 3
C15 K2 C19 40.4(3) 3 3
N10 K2 C51 94.9(2) . .
C50 K2 C51 24.4(3) . .
C64 K2 C51 119.2(3) . .
N4 K2 C51 42.6(2) . .
C16 K2 C51 70.4(3) 3 .
N9 K2 C51 80.4(2) . .
C17 K2 C51 88.7(3) 3 .
C18 K2 C51 111.2(3) 3 .
C13 K2 C51 128.2(3) 3 .
C15 K2 C51 73.4(3) 3 .
C19 K2 C51 113.6(3) 3 .
C36 N1 N2 116.7(7) . .
C36 N1 Eu1 166.8(6) . .
N2 N1 Eu1 75.5(4) . .
C36 N1 K1 81.6(5) . 2_554
N2 N1 K1 89.2(5) . 2_554
Eu1 N1 K1 104.5(2) . 2_554
N1 N2 C35 109.9(7) . .
N1 N2 Eu1 73.3(4) . .
C35 N2 Eu1 175.0(6) . .
N1 N2 K1 66.6(4) . 2_554
C35 N2 K1 88.2(5) . 2_554
Eu1 N2 K1 96.7(2) . 2_554
C49 N3 N4 113.5(7) . .
C49 N3 Eu1 170.8(7) . .
N4 N3 Eu1 73.9(4) . .
N3 N4 C50 114.7(8) . .
N3 N4 Eu1 75.0(4) . .
C50 N4 Eu1 170.1(7) . .
N3 N4 K2 96.6(5) . .
C50 N4 K2 72.5(5) . .
Eu1 N4 K2 109.6(2) . .
N6 N5 C7 114.6(7) . .
N6 N5 Eu1 69.2(4) . .
C7 N5 Eu1 171.3(6) . .
N6 N5 K1 70.2(4) . 2_554
C7 N5 K1 91.6(5) . 2_554
Eu1 N5 K1 97.1(2) . 2_554
N5 N6 C8 111.2(7) . .
N5 N6 Eu1 80.6(5) . .
C8 N6 Eu1 165.6(5) . .
N5 N6 K1 84.5(4) . 2_554
C8 N6 K1 85.1(5) . 2_554
Eu1 N6 K1 104.9(2) . 2_554
C21 N7 N8 112.8(7) . .
C21 N7 Eu1 175.7(6) . .
N8 N7 Eu1 71.3(4) . .
N7 N8 C22 113.3(7) . .
N7 N8 Eu1 76.8(4) . .
C22 N8 Eu1 169.7(7) . .
C63 N9 N10 112.1(8) . .
C63 N9 Eu1 167.0(7) . .
N10 N9 Eu1 71.9(4) . .
C63 N9 K2 89.1(6) . .
N10 N9 K2 66.9(4) . .
Eu1 N9 K2 103.7(3) . .
C64 N10 N9 113.0(8) . .
C64 N10 Eu1 162.8(6) . .
N9 N10 Eu1 76.5(4) . .
C64 N10 K2 82.2(5) . .
N9 N10 K2 88.6(4) . .
Eu1 N10 K2 113.2(2) . .
C8 P1 C7 88.7(4) . .
C8 P1 K1 60.1(3) . 2_554
C7 P1 K1 69.8(3) . 2_554
C36 P2 C35 87.3(4) . .
C36 P2 K1 60.3(3) . 2_554
C35 P2 K1 73.6(3) . 2_554
C22 P3 C21 85.4(4) . .
C50 P4 C49 87.3(5) . .
C50 P4 K2 58.0(3) . .
C49 P4 K2 83.4(3) . .
C64 P5 C63 85.9(4) . .
C64 P5 K2 61.0(3) . .
C63 P5 K2 73.5(4) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 C6 1.364(12) .
C1 C2 1.369(15) .
C1 H1 0.9300 .
C2 C3 1.375(18) .
C2 H2 0.9300 .
C3 C4 1.366(17) .
C3 H3 0.9300 .
C4 C5 1.405(13) .
C4 H4 0.9300 .
C5 C6 1.365(14) .
C5 H5 0.9300 .
C6 C7 1.480(12) .
C7 N5 1.361(11) .
C7 P1 1.737(10) .
C7 K1 3.464(9) 2_554
C8 N6 1.385(11) .
C8 C9 1.470(12) .
C8 P1 1.723(8) .
C8 K1 3.173(9) 2_554
C9 C14 1.412(12) .
C9 C10 1.426(12) .
C10 C11 1.383(13) .
C10 H10 0.9300 .
C11 C12 1.387(15) .
C11 H11 0.9300 .
C12 C13 1.472(18) .
C12 H12 0.9300 .
C13 C14 1.315(14) .
C13 K2 3.374(13) 3_545
C13 H13 0.9800 .
C14 K2 3.490(11) 3_545
C14 H14 0.9800 .
C15 C16 1.391(17) .
C15 C20 1.432(13) .
C15 K2 3.445(13) 3_545
C15 H15 0.9800 .
C16 C17 1.306(17) .
C16 K2 3.328(13) 3_545
C16 H16 0.9800 .
C17 C18 1.412(17) .
C17 K2 3.357(16) 3_545
C17 H17 0.9800 .
C18 C19 1.384(15) .
C18 K2 3.369(14) 3_545
C18 H18 0.9800 .
C19 C20 1.393(14) .
C19 K2 3.475(11) 3_545
C19 H19 0.9800 .
C20 C21 1.444(13) .
C21 N7 1.302(10) .
C21 P3 1.776(10) .
C22 N8 1.356(11) .
C22 C23 1.470(13) .
C22 P3 1.757(10) .
C23 C28 1.387(13) .
C23 C24 1.404(12) .
C24 C25 1.378(15) .
C24 K1 3.482(10) .
C24 H24 0.9800 .
C25 C26 1.449(17) .
C25 K1 3.303(12) .
C25 H25 0.9800 .
C26 C27 1.374(16) .
C26 H26 0.9300 .
C27 C28 1.328(14) .
C27 H27 0.9300 .
C28 H28 0.9300 .
C29 C34 1.348(18) .
C29 C30 1.449(18) .
C29 H29 0.9300 .
C30 C31 1.30(2) .
C30 H30 0.9300 .
C31 C32 1.307(19) .
C31 H31 0.9300 .
C32 C33 1.404(17) .
C32 H32 0.9300 .
C33 C34 1.354(19) .
C33 H33 0.9300 .
C34 C35 1.465(15) .
C35 N2 1.377(11) .
C35 P2 1.757(10) .
C35 K1 3.516(10) 2_554
C36 N1 1.344(9) .
C36 C37 1.484(12) .
C36 P2 1.751(9) .
C36 K1 3.112(10) 2_554
C37 C38 1.380(13) .
C37 C42 1.390(12) .
C38 C39 1.399(14) .
C38 H38 0.9300 .
C39 C40 1.287(15) .
C39 H39 0.9300 .
C40 C41 1.396(18) .
C40 H40 0.9300 .
C41 C42 1.326(14) .
C41 H41 0.9300 .
C42 H42 0.9300 .
C43 C48 1.423(17) .
C43 C44 1.443(19) .
C43 H43 0.9300 .
C44 C45 1.44(2) .
C44 H44 0.9300 .
C45 C46 1.354(18) .
C45 H45 0.9300 .
C46 C47 1.387(18) .
C46 H46 0.9300 .
C47 C48 1.373(18) .
C47 H47 0.9300 .
C48 C49 1.491(16) .
C49 N3 1.321(11) .
C49 P4 1.788(11) .
C50 N4 1.377(11) .
C50 C51 1.441(15) .
C50 P4 1.749(12) .
C50 K2 3.081(10) .
C51 C52 1.328(16) .
C51 C56 1.348(15) .
C51 K2 3.483(12) .
C52 C53 1.48(3) .
C52 H52 0.9300 .
C53 C54 1.29(3) .
C53 H53 0.9300 .
C54 C55 1.26(2) .
C54 H54 0.9300 .
C55 C56 1.444(16) .
C55 H55 0.9300 .
C56 H56 0.9300 .
C57 C58 1.3900 .
C57 C62 1.3900 .
C57 H57 0.9300 .
C58 C59 1.3900 .
C58 H58 0.9300 .
C59 C60 1.3900 .
C59 H59 0.9300 .
C60 C61 1.3900 .
C60 H60 0.9300 .
C61 C62 1.3900 .
C61 H61 0.9300 .
C62 C63 1.488(13) .
C63 N9 1.320(11) .
C63 P5 1.776(12) .
C64 N10 1.354(9) .
C64 C65 1.510(15) .
C64 P5 1.759(12) .
C64 K2 3.181(9) .
C65 C70 1.357(16) .
C65 C66 1.386(14) .
C66 C67 1.40(2) .
C66 H66 0.9300 .
C67 C68 1.34(2) .
C67 H67 0.9300 .
C68 C69 1.32(2) .
C68 H68 0.9300 .
C69 C70 1.361(16) .
C69 H69 0.9300 .
C70 H70 0.9300 .
C71 C72 1.35(2) .
C71 C76 1.45(2) .
C71 K1 3.285(16) .
C71 H71 0.9800 .
C72 C73 1.32(2) .
C72 K1 3.242(16) .
C72 H72 0.9800 .
C73 C74 1.39(2) .
C73 K1 3.273(15) .
C73 H73 0.9800 .
C74 C75 1.43(2) .
C74 K1 3.191(15) .
C74 H74 0.9800 .
C75 C76 1.39(2) .
C75 K1 3.187(14) .
C75 H75 0.9800 .
C76 C77 1.49(2) .
C76 K1 3.225(17) .
C77 H77A 0.9600 .
C77 H77B 0.9600 .
C77 H77C 0.9600 .
Eu1 N8 2.431(6) .
Eu1 N1 2.482(6) .
Eu1 N4 2.484(7) .
Eu1 N3 2.497(7) .
Eu1 N7 2.499(6) .
Eu1 N6 2.506(8) .
Eu1 N10 2.508(7) .
Eu1 N2 2.509(8) .
Eu1 N9 2.566(7) .
Eu1 N5 2.645(8) .
Eu1 K1 4.356(2) 2_554
Eu1 K2 4.665(3) .
K1 N6 2.976(7) 2
K1 N1 3.011(8) 2
K1 C36 3.112(10) 2
K1 N5 3.148(7) 2
K1 C8 3.173(9) 2
K1 N2 3.280(8) 2
K2 N10 3.069(8) .
K2 N4 3.200(8) .
K2 C16 3.328(13) 3
K2 N9 3.335(8) .
K2 C17 3.357(16) 3
K2 C18 3.369(14) 3
K2 C13 3.374(13) 3
K2 C15 3.444(13) 3
K2 C19 3.475(11) 3
N1 N2 1.345(9) .
N1 K1 3.011(8) 2_554
N2 K1 3.280(8) 2_554
N3 N4 1.339(9) .
N5 N6 1.351(9) .
N5 K1 3.148(7) 2_554
N6 K1 2.976(7) 2_554
N7 N8 1.355(9) .
N9 N10 1.384(10) .
P1 K1 3.657(4) 2_554
P2 K1 3.583(4) 2_554
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C6 C1 C2 C3 1(2) . .
C1 C2 C3 C4 -4(2) . .
C2 C3 C4 C5 5(2) . .
C3 C4 C5 C6 -3.6(18) . .
C2 C1 C6 C5 0.2(16) . .
C2 C1 C6 C7 179.5(10) . .
C4 C5 C6 C1 0.9(15) . .
C4 C5 C6 C7 -178.4(9) . .
C1 C6 C7 N5 160.4(8) . .
C5 C6 C7 N5 -20.3(13) . .
C1 C6 C7 P1 -23.3(13) . .
C5 C6 C7 P1 156.0(8) . .
C1 C6 C7 K1 83.2(10) . 2_554
C5 C6 C7 K1 -97.4(10) . 2_554
N6 C8 C9 C14 174.8(8) . .
P1 C8 C9 C14 -3.3(13) . .
K1 C8 C9 C14 -110.2(8) 2_554 .
N6 C8 C9 C10 -9.7(12) . .
P1 C8 C9 C10 172.2(7) . .
K1 C8 C9 C10 65.3(9) 2_554 .
C14 C9 C10 C11 -6.4(14) . .
C8 C9 C10 C11 177.9(9) . .
C9 C10 C11 C12 9.8(18) . .
C10 C11 C12 C13 -7.9(19) . .
C11 C12 C13 C14 2.9(19) . .
C11 C12 C13 K2 -83.6(12) . 3_545
C12 C13 C14 C9 0.2(19) . .
K2 C13 C14 C9 94.2(11) 3_545 .
C12 C13 C14 K2 -94.0(11) . 3_545
C10 C9 C14 C13 1.5(17) . .
C8 C9 C14 C13 177.4(11) . .
C10 C9 C14 K2 80.9(8) . 3_545
C8 C9 C14 K2 -103.3(7) . 3_545
C20 C15 C16 C17 -3(2) . .
K2 C15 C16 C17 -73.6(15) 3_545 .
C20 C15 C16 K2 70.7(12) . 3_545
C15 C16 C17 C18 6(2) . .
K2 C16 C17 C18 -68.8(14) 3_545 .
C15 C16 C17 K2 75.1(14) . 3_545
C16 C17 C18 C19 -5(2) . .
K2 C17 C18 C19 -73.6(12) 3_545 .
C16 C17 C18 K2 68.3(15) . 3_545
C17 C18 C19 C20 1(2) . .
K2 C18 C19 C20 -70.1(10) 3_545 .
C17 C18 C19 K2 70.7(13) . 3_545
C18 C19 C20 C15 2.6(17) . .
K2 C19 C20 C15 -63.2(9) 3_545 .
C18 C19 C20 C21 178.7(11) . .
K2 C19 C20 C21 112.9(10) 3_545 .
C16 C15 C20 C19 -1.7(18) . .
K2 C15 C20 C19 64.0(9) 3_545 .
C16 C15 C20 C21 -177.7(12) . .
K2 C15 C20 C21 -112.0(10) 3_545 .
C19 C20 C21 N7 25.9(15) . .
C15 C20 C21 N7 -158.3(11) . .
C19 C20 C21 P3 -153.2(9) . .
C15 C20 C21 P3 22.6(15) . .
N8 C22 C23 C28 18.8(13) . .
P3 C22 C23 C28 -160.2(8) . .
N8 C22 C23 C24 -166.5(9) . .
P3 C22 C23 C24 14.5(13) . .
C28 C23 C24 C25 -1.2(15) . .
C22 C23 C24 C25 -176.1(10) . .
C28 C23 C24 K1 85.1(12) . .
C22 C23 C24 K1 -89.8(10) . .
C23 C24 C25 C26 1.8(18) . .
K1 C24 C25 C26 -120.3(13) . .
C23 C24 C25 K1 122.0(9) . .
C24 C25 C26 C27 -3(2) . .
K1 C25 C26 C27 -106.5(12) . .
C25 C26 C27 C28 3(2) . .
C26 C27 C28 C23 -3(2) . .
C24 C23 C28 C27 1.9(17) . .
C22 C23 C28 C27 176.6(11) . .
C34 C29 C30 C31 -1(3) . .
C29 C30 C31 C32 -2(3) . .
C30 C31 C32 C33 4(3) . .
C31 C32 C33 C34 -4(3) . .
C30 C29 C34 C33 1(2) . .
C30 C29 C34 C35 -176.6(13) . .
C32 C33 C34 C29 2(2) . .
C32 C33 C34 C35 178.9(13) . .
C29 C34 C35 N2 -140.7(14) . .
C33 C34 C35 N2 42(2) . .
C29 C34 C35 P2 37(2) . .
C33 C34 C35 P2 -140.0(12) . .
C29 C34 C35 K1 136.4(13) . 2_554
C33 C34 C35 K1 -40.8(17) . 2_554
N1 C36 C37 C38 -20.3(14) . .
P2 C36 C37 C38 155.6(8) . .
K1 C36 C37 C38 56.4(9) 2_554 .
N1 C36 C37 C42 160.1(9) . .
P2 C36 C37 C42 -23.9(13) . .
K1 C36 C37 C42 -123.1(8) 2_554 .
C42 C37 C38 C39 -0.3(15) . .
C36 C37 C38 C39 -179.9(9) . .
C37 C38 C39 C40 4.1(18) . .
C38 C39 C40 C41 -8(2) . .
C39 C40 C41 C42 8(2) . .
C40 C41 C42 C37 -4.4(19) . .
C38 C37 C42 C41 0.7(16) . .
C36 C37 C42 C41 -179.8(10) . .
C48 C43 C44 C45 8(2) . .
C43 C44 C45 C46 4(2) . .
C44 C45 C46 C47 -9(2) . .
C45 C46 C47 C48 0(2) . .
C46 C47 C48 C43 13(2) . .
C46 C47 C48 C49 -178.8(13) . .
C44 C43 C48 C47 -17(2) . .
C44 C43 C48 C49 174.5(13) . .
C47 C48 C49 N3 27.7(18) . .
C43 C48 C49 N3 -163.8(11) . .
C47 C48 C49 P4 -151.1(11) . .
C43 C48 C49 P4 17.4(16) . .
N4 C50 C51 C52 167.8(10) . .
P4 C50 C51 C52 -12.0(17) . .
K2 C50 C51 C52 -109.1(11) . .
N4 C50 C51 C56 -9.1(16) . .
P4 C50 C51 C56 171.1(9) . .
K2 C50 C51 C56 74.0(11) . .
N4 C50 C51 K2 -83.2(8) . .
P4 C50 C51 K2 97.1(9) . .
C56 C51 C52 C53 -4(2) . .
C50 C51 C52 C53 178.6(13) . .
K2 C51 C52 C53 106.0(14) . .
C51 C52 C53 C54 6(3) . .
C52 C53 C54 C55 -4(4) . .
C53 C54 C55 C56 1(3) . .
C52 C51 C56 C55 1.2(19) . .
C50 C51 C56 C55 178.1(10) . .
K2 C51 C56 C55 -123.7(10) . .
C54 C55 C56 C51 1(2) . .
C62 C57 C58 C59 0.0 . .
C57 C58 C59 C60 0.0 . .
C58 C59 C60 C61 0.0 . .
C59 C60 C61 C62 0.0 . .
C60 C61 C62 C57 0.0 . .
C60 C61 C62 C63 -176.9(9) . .
C58 C57 C62 C61 0.0 . .
C58 C57 C62 C63 176.9(9) . .
C61 C62 C63 N9 -2.7(13) . .
C57 C62 C63 N9 -179.6(8) . .
C61 C62 C63 P5 177.1(6) . .
C57 C62 C63 P5 0.2(12) . .
N10 C64 C65 C70 8.2(16) . .
P5 C64 C65 C70 -168.1(10) . .
K2 C64 C65 C70 87.9(12) . .
N10 C64 C65 C66 -170.8(9) . .
P5 C64 C65 C66 12.9(14) . .
K2 C64 C65 C66 -91.1(9) . .
C70 C65 C66 C67 2.3(17) . .
C64 C65 C66 C67 -178.7(10) . .
C65 C66 C67 C68 -6(2) . .
C66 C67 C68 C69 5(3) . .
C67 C68 C69 C70 0(3) . .
C66 C65 C70 C69 2(2) . .
C64 C65 C70 C69 -177.4(11) . .
C68 C69 C70 C65 -3(2) . .
C76 C71 C72 C73 -4(3) . .
K1 C71 C72 C73 -68.0(18) . .
C76 C71 C72 K1 64.4(14) . .
C71 C72 C73 C74 2(3) . .
K1 C72 C73 C74 -66.3(12) . .
C71 C72 C73 K1 68.1(18) . .
C72 C73 C74 C75 1(2) . .
K1 C73 C74 C75 -66.4(14) . .
C72 C73 C74 K1 67.9(13) . .
C73 C74 C75 C76 -3(2) . .
K1 C74 C75 C76 -71.0(13) . .
C73 C74 C75 K1 68.4(14) . .
C74 C75 C76 C71 1(2) . .
K1 C75 C76 C71 -69.2(14) . .
C74 C75 C76 C77 178.7(13) . .
K1 C75 C76 C77 108.8(13) . .
C74 C75 C76 K1 69.9(12) . .
C72 C71 C76 C75 2(2) . .
K1 C71 C76 C75 67.3(14) . .
C72 C71 C76 C77 -175.5(16) . .
K1 C71 C76 C77 -110.2(18) . .
C72 C71 C76 K1 -65.2(14) . .
C76 C75 K1 N6 -2.8(16) . 2
C74 C75 K1 N6 -122.5(10) . 2
C76 C75 K1 N1 138.3(11) . 2
C74 C75 K1 N1 18.6(14) . 2
C76 C75 K1 C36 158.4(11) . 2
C74 C75 K1 C36 38.7(12) . 2
C76 C75 K1 N5 -45.1(16) . 2
C74 C75 K1 N5 -164.8(8) . 2
C76 C75 K1 C8 -9.4(14) . 2
C74 C75 K1 C8 -129.1(10) . 2
C76 C75 K1 C74 119.7(18) . .
C74 C75 K1 C76 -119.7(18) . .
C76 C75 K1 C72 62.4(12) . .
C74 C75 K1 C72 -57.2(10) . .
C76 C75 K1 C73 93.3(13) . .
C74 C75 K1 C73 -26.4(9) . .
C76 C75 K1 N2 103.2(13) . 2
C74 C75 K1 N2 -16.5(13) . 2
C76 C75 K1 C71 31.0(12) . .
C74 C75 K1 C71 -88.7(12) . .
C73 C74 K1 N6 -37.0(16) . 2
C75 C74 K1 N6 93.4(11) . 2
C73 C74 K1 N1 61.3(12) . 2
C75 C74 K1 N1 -168.3(9) . 2
C73 C74 K1 C36 81.0(12) . 2
C75 C74 K1 C36 -148.5(10) . 2
C73 C74 K1 N5 -68(3) . 2
C75 C74 K1 N5 62(3) . 2
C73 C74 K1 C8 -65.3(13) . 2
C75 C74 K1 C8 65.2(11) . 2
C73 C74 K1 C75 -130.4(18) . .
C73 C74 K1 C76 -98.3(13) . .
C75 C74 K1 C76 32.1(10) . .
C73 C74 K1 C72 -31.8(10) . .
C75 C74 K1 C72 98.6(13) . .
C75 C74 K1 C73 130.4(18) . .
C73 C74 K1 N2 37.4(12) . 2
C75 C74 K1 N2 167.8(9) . 2
C73 C74 K1 C71 -63.5(11) . .
C75 C74 K1 C71 66.9(11) . .
C75 C76 K1 N6 178.0(11) . 2
C71 C76 K1 N6 -58.1(13) . 2
C77 C76 K1 N6 70.6(13) . 2
C75 C76 K1 N1 -89.1(16) . 2
C71 C76 K1 N1 35(2) . 2
C77 C76 K1 N1 163.6(9) . 2
C75 C76 K1 C36 -34.6(17) . 2
C71 C76 K1 C36 89.2(14) . 2
C77 C76 K1 C36 -142.0(11) . 2
C75 C76 K1 N5 152.2(11) . 2
C71 C76 K1 N5 -84.0(13) . 2
C77 C76 K1 N5 44.8(14) . 2
C75 C76 K1 C8 171.5(12) . 2
C71 C76 K1 C8 -64.6(12) . 2
C77 C76 K1 C8 64.1(12) . 2
C71 C76 K1 C75 124(2) . .
C77 C76 K1 C75 -107.4(19) . .
C75 C76 K1 C74 -33.4(11) . .
C71 C76 K1 C74 90.4(13) . .
C77 C76 K1 C74 -140.8(16) . .
C75 C76 K1 C72 -94.7(14) . .
C71 C76 K1 C72 29.2(11) . .
C77 C76 K1 C72 157.9(16) . .
C75 C76 K1 C73 -65.1(12) . .
C71 C76 K1 C73 58.8(11) . .
C77 C76 K1 C73 -172.5(15) . .
C75 C76 K1 N2 -103.3(12) . 2
C71 C76 K1 N2 20.6(15) . 2
C77 C76 K1 N2 149.3(10) . 2
C75 C76 K1 C71 -124(2) . .
C77 C76 K1 C71 129(2) . .
C73 C72 K1 N6 -149.2(11) . 2
C71 C72 K1 N6 78.6(12) . 2
C73 C72 K1 N1 -77.0(12) . 2
C71 C72 K1 N1 150.8(10) . 2
C73 C72 K1 C36 -48.9(12) . 2
C71 C72 K1 C36 178.9(10) . 2
C73 C72 K1 N5 -153.3(10) . 2
C71 C72 K1 N5 74.5(12) . 2
C73 C72 K1 C8 -171.5(11) . 2
C71 C72 K1 C8 56.2(12) . 2
C73 C72 K1 C75 67.8(11) . .
C71 C72 K1 C75 -64.5(11) . .
C73 C72 K1 C74 33.7(11) . .
C71 C72 K1 C74 -98.5(13) . .
C73 C72 K1 C76 100.8(13) . .
C71 C72 K1 C76 -31.5(11) . .
C71 C72 K1 C73 -132.2(19) . .
C73 C72 K1 N2 -85.2(12) . 2
C71 C72 K1 N2 142.6(11) . 2
C73 C72 K1 C71 132.2(19) . .
C72 C73 K1 N6 37.4(13) . 2
C74 C73 K1 N6 156.5(10) . 2
C72 C73 K1 N1 112.2(11) . 2
C74 C73 K1 N1 -128.7(11) . 2
C72 C73 K1 C36 136.6(11) . 2
C74 C73 K1 C36 -104.3(12) . 2
C72 C73 K1 N5 43.9(16) . 2
C74 C73 K1 N5 163.0(9) . 2
C72 C73 K1 C8 9.4(13) . 2
C74 C73 K1 C8 128.5(11) . 2
C72 C73 K1 C75 -91.4(13) . .
C74 C73 K1 C75 27.7(11) . .
C72 C73 K1 C74 -119.1(18) . .
C72 C73 K1 C76 -59.0(11) . .
C74 C73 K1 C76 60.1(11) . .
C74 C73 K1 C72 119.1(18) . .
C72 C73 K1 N2 95.5(12) . 2
C74 C73 K1 N2 -145.4(12) . 2
C72 C73 K1 C71 -26.1(11) . .
C74 C73 K1 C71 93.1(13) . .
C72 C71 K1 N6 -107.1(11) . 2
C76 C71 K1 N6 128.9(12) . 2
C72 C71 K1 N1 -39.0(14) . 2
C76 C71 K1 N1 -163.1(10) . 2
C72 C71 K1 C36 -1.5(14) . 2
C76 C71 K1 C36 -125.6(11) . 2
C72 C71 K1 N5 -122.1(11) . 2
C76 C71 K1 N5 113.9(12) . 2
C72 C71 K1 C8 -122.5(12) . 2
C76 C71 K1 C8 113.4(12) . 2
C72 C71 K1 C75 94.0(13) . .
C76 C71 K1 C75 -30.1(11) . .
C72 C71 K1 C74 58.8(11) . .
C76 C71 K1 C74 -65.2(12) . .
C72 C71 K1 C76 124.1(19) . .
C76 C71 K1 C72 -124.1(19) . .
C72 C71 K1 C73 25.5(10) . .
C76 C71 K1 C73 -98.6(13) . .
C72 C71 K1 N2 -40.7(12) . 2
C76 C71 K1 N2 -164.8(11) . 2
N4 C50 K2 N10 5.5(6) . .
C51 C50 K2 N10 -114.4(7) . .
P4 C50 K2 N10 116.6(4) . .
N4 C50 K2 C64 1.4(7) . .
C51 C50 K2 C64 -118.5(7) . .
P4 C50 K2 C64 112.5(4) . .
C51 C50 K2 N4 -119.9(10) . .
P4 C50 K2 N4 111.1(8) . .
N4 C50 K2 C16 125.3(6) . 3
C51 C50 K2 C16 5.4(7) . 3
P4 C50 K2 C16 -123.6(5) . 3
N4 C50 K2 N9 29.7(6) . .
C51 C50 K2 N9 -90.2(7) . .
P4 C50 K2 N9 140.8(4) . .
N4 C50 K2 C17 111.5(7) . 3
C51 C50 K2 C17 -8.4(7) . 3
P4 C50 K2 C17 -137.4(4) . 3
N4 C50 K2 C18 121.8(6) . 3
C51 C50 K2 C18 1.9(8) . 3
P4 C50 K2 C18 -127.1(5) . 3
N4 C50 K2 C13 -86.9(7) . 3
C51 C50 K2 C13 153.2(7) . 3
P4 C50 K2 C13 24.2(5) . 3
N4 C50 K2 C15 149.0(6) . 3
C51 C50 K2 C15 29.1(7) . 3
P4 C50 K2 C15 -99.9(4) . 3
N4 C50 K2 C19 155.0(5) . 3
C51 C50 K2 C19 35.1(8) . 3
P4 C50 K2 C19 -93.9(6) . 3
N4 C50 K2 C51 119.9(10) . .
P4 C50 K2 C51 -129.0(8) . .
C65 C64 K2 N10 -115.6(10) . .
P5 C64 K2 N10 114.9(8) . .
N10 C64 K2 C50 9.7(7) . .
C65 C64 K2 C50 -105.9(7) . .
P5 C64 K2 C50 124.6(4) . .
N10 C64 K2 N4 10.3(6) . .
C65 C64 K2 N4 -105.2(7) . .
P5 C64 K2 N4 125.2(4) . .
N10 C64 K2 C16 -97.8(6) . 3
C65 C64 K2 C16 146.6(7) . 3
P5 C64 K2 C16 17.1(5) . 3
N10 C64 K2 N9 -35.5(5) . .
C65 C64 K2 N9 -151.1(8) . .
P5 C64 K2 N9 79.4(5) . .
N10 C64 K2 C17 -108.8(7) . 3
C65 C64 K2 C17 135.6(7) . 3
P5 C64 K2 C17 6.1(4) . 3
N10 C64 K2 C18 -132.9(6) . 3
C65 C64 K2 C18 111.5(7) . 3
P5 C64 K2 C18 -18.0(4) . 3
N10 C64 K2 C13 115.3(7) . 3
C65 C64 K2 C13 -0.2(7) . 3
P5 C64 K2 C13 -129.8(4) . 3
N10 C64 K2 C15 -113.8(6) . 3
C65 C64 K2 C15 130.6(7) . 3
P5 C64 K2 C15 1.1(6) . 3
N10 C64 K2 C19 -150.4(6) . 3
C65 C64 K2 C19 94.1(7) . 3
P5 C64 K2 C19 -35.5(5) . 3
N10 C64 K2 C51 -14.8(8) . .
C65 C64 K2 C51 -130.4(7) . .
P5 C64 K2 C51 100.1(4) . .
C52 C51 K2 N10 176.3(12) . .
C56 C51 K2 N10 -59.1(8) . .
C50 C51 K2 N10 65.5(7) . .
C52 C51 K2 C50 110.7(15) . .
C56 C51 K2 C50 -124.6(11) . .
C52 C51 K2 C64 -177.5(12) . .
C56 C51 K2 C64 -52.9(8) . .
C50 C51 K2 C64 71.7(7) . .
C52 C51 K2 N4 143.8(14) . .
C56 C51 K2 N4 -91.5(8) . .
C50 C51 K2 N4 33.1(6) . .
C52 C51 K2 C16 -63.6(12) . 3
C56 C51 K2 C16 61.0(8) . 3
C50 C51 K2 C16 -174.3(7) . 3
C52 C51 K2 N9 -163.9(13) . .
C56 C51 K2 N9 -39.3(7) . .
C50 C51 K2 N9 85.3(6) . .
C52 C51 K2 C17 -77.0(12) . 3
C56 C51 K2 C17 47.6(8) . 3
C50 C51 K2 C17 172.2(7) . 3
C52 C51 K2 C18 -67.8(13) . 3
C56 C51 K2 C18 56.8(8) . 3
C50 C51 K2 C18 -178.6(6) . 3
C52 C51 K2 C13 77.4(13) . 3
C56 C51 K2 C13 -158.0(7) . 3
C50 C51 K2 C13 -33.3(8) . 3
C52 C51 K2 C15 -38.9(12) . 3
C56 C51 K2 C15 85.7(8) . 3
C50 C51 K2 C15 -149.6(7) . 3
C52 C51 K2 C19 -42.8(13) . 3
C56 C51 K2 C19 81.9(8) . 3
C50 C51 K2 C19 -153.5(6) . 3
C37 C36 N1 N2 177.9(8) . .
P2 C36 N1 N2 1.3(10) . .
K1 C36 N1 N2 84.8(7) 2_554 .
C37 C36 N1 Eu1 -26(3) . .
P2 C36 N1 Eu1 158(2) . .
K1 C36 N1 Eu1 -119(3) 2_554 .
C37 C36 N1 K1 93.1(8) . 2_554
P2 C36 N1 K1 -83.5(5) . 2_554
N8 Eu1 N1 C36 -161(3) . .
N4 Eu1 N1 C36 -2(3) . .
N3 Eu1 N1 C36 13(3) . .
N7 Eu1 N1 C36 167(3) . .
N6 Eu1 N1 C36 113(3) . .
N10 Eu1 N1 C36 -78(3) . .
N2 Eu1 N1 C36 -158(3) . .
N9 Eu1 N1 C36 -79(3) . .
N5 Eu1 N1 C36 83(3) . .
K1 Eu1 N1 C36 116(3) 2_554 .
K2 Eu1 N1 C36 -40(3) . .
N8 Eu1 N1 N2 -3.0(5) . .
N4 Eu1 N1 N2 156.6(5) . .
N3 Eu1 N1 N2 171.7(4) . .
N7 Eu1 N1 N2 -34.9(6) . .
N6 Eu1 N1 N2 -88.5(5) . .
N10 Eu1 N1 N2 80.6(5) . .
N9 Eu1 N1 N2 79.0(5) . .
N5 Eu1 N1 N2 -118.8(5) . .
K1 Eu1 N1 N2 -85.3(5) 2_554 .
K2 Eu1 N1 N2 118.8(4) . .
N8 Eu1 N1 K1 82.3(3) . 2_554
N4 Eu1 N1 K1 -118.2(3) . 2_554
N3 Eu1 N1 K1 -103.1(3) . 2_554
N7 Eu1 N1 K1 50.3(4) . 2_554
N6 Eu1 N1 K1 -3.3(2) . 2_554
N10 Eu1 N1 K1 165.9(2) . 2_554
N2 Eu1 N1 K1 85.3(5) . 2_554
N9 Eu1 N1 K1 164.3(2) . 2_554
N5 Eu1 N1 K1 -33.5(2) . 2_554
K2 Eu1 N1 K1 -155.91(15) . 2_554
C36 N1 N2 C35 -1.3(11) . .
Eu1 N1 N2 C35 -176.0(7) . .
K1 N1 N2 C35 78.8(7) 2_554 .
C36 N1 N2 Eu1 174.6(8) . .
K1 N1 N2 Eu1 -105.2(2) 2_554 .
C36 N1 N2 K1 -80.1(7) . 2_554
Eu1 N1 N2 K1 105.2(2) . 2_554
C34 C35 N2 N1 178.8(10) . .
P2 C35 N2 N1 0.8(10) . .
K1 C35 N2 N1 -64.3(6) 2_554 .
C34 C35 N2 Eu1 49(8) . .
P2 C35 N2 Eu1 -129(8) . .
K1 C35 N2 Eu1 166(8) 2_554 .
C34 C35 N2 K1 -116.9(11) . 2_554
P2 C35 N2 K1 65.1(6) . 2_554
N8 Eu1 N2 N1 177.4(5) . .
N4 Eu1 N2 N1 -27.1(5) . .
N3 Eu1 N2 N1 -14.4(8) . .
N7 Eu1 N2 N1 156.3(4) . .
N6 Eu1 N2 N1 87.7(5) . .
N10 Eu1 N2 N1 -112.9(5) . .
N9 Eu1 N2 N1 -97.6(5) . .
N5 Eu1 N2 N1 59.3(5) . .
K1 Eu1 N2 N1 63.1(4) 2_554 .
K2 Eu1 N2 N1 -73.3(5) . .
N8 Eu1 N2 C35 -52(8) . .
N1 Eu1 N2 C35 131(8) . .
N4 Eu1 N2 C35 104(8) . .
N3 Eu1 N2 C35 116(8) . .
N7 Eu1 N2 C35 -73(8) . .
N6 Eu1 N2 C35 -142(8) . .
N10 Eu1 N2 C35 18(8) . .
N9 Eu1 N2 C35 33(8) . .
N5 Eu1 N2 C35 -170(8) . .
K1 Eu1 N2 C35 -166(8) 2_554 .
K2 Eu1 N2 C35 57(8) . .
N8 Eu1 N2 K1 114.3(2) . 2_554
N1 Eu1 N2 K1 -63.1(4) . 2_554
N4 Eu1 N2 K1 -90.2(3) . 2_554
N3 Eu1 N2 K1 -77.5(5) . 2_554
N7 Eu1 N2 K1 93.2(2) . 2_554
N6 Eu1 N2 K1 24.6(2) . 2_554
N10 Eu1 N2 K1 -175.99(19) . 2_554
N9 Eu1 N2 K1 -160.7(2) . 2_554
N5 Eu1 N2 K1 -3.8(2) . 2_554
K2 Eu1 N2 K1 -136.41(13) . 2_554
C48 C49 N3 N4 176.8(9) . .
P4 C49 N3 N4 -4.2(9) . .
C48 C49 N3 Eu1 35(4) . .
P4 C49 N3 Eu1 -146(3) . .
N8 Eu1 N3 C49 -72(4) . .
N1 Eu1 N3 C49 114(4) . .
N4 Eu1 N3 C49 144(4) . .
N7 Eu1 N3 C49 -49(4) . .
N6 Eu1 N3 C49 25(4) . .
N10 Eu1 N3 C49 -131(4) . .
N2 Eu1 N3 C49 122(4) . .
N9 Eu1 N3 C49 -158(4) . .
N5 Eu1 N3 C49 44(4) . .
K1 Eu1 N3 C49 65(4) 2_554 .
K2 Eu1 N3 C49 -159(4) . .
N8 Eu1 N3 N4 144.2(4) . .
N1 Eu1 N3 N4 -30.2(5) . .
N7 Eu1 N3 N4 166.9(4) . .
N6 Eu1 N3 N4 -118.8(4) . .
N10 Eu1 N3 N4 85.4(5) . .
N2 Eu1 N3 N4 -21.8(7) . .
N9 Eu1 N3 N4 58.0(4) . .
N5 Eu1 N3 N4 -99.8(4) . .
K1 Eu1 N3 N4 -78.4(5) 2_554 .
K2 Eu1 N3 N4 57.5(4) . .
C49 N3 N4 C50 3.5(10) . .
Eu1 N3 N4 C50 177.6(7) . .
C49 N3 N4 Eu1 -174.1(7) . .
C49 N3 N4 K2 77.3(7) . .
Eu1 N3 N4 K2 -108.6(2) . .
C51 C50 N4 N3 179.1(8) . .
P4 C50 N4 N3 -1.2(10) . .
K2 C50 N4 N3 89.3(6) . .
C51 C50 N4 Eu1 -14(4) . .
P4 C50 N4 Eu1 165(3) . .
K2 C50 N4 Eu1 -104(4) . .
C51 C50 N4 K2 89.7(9) . .
P4 C50 N4 K2 -90.5(5) . .
N8 Eu1 N4 N3 -58.2(6) . .
N1 Eu1 N4 N3 153.7(4) . .
N7 Eu1 N4 N3 -16.7(5) . .
N6 Eu1 N4 N3 70.9(5) . .
N10 Eu1 N4 N3 -87.6(5) . .
N2 Eu1 N4 N3 167.4(4) . .
N9 Eu1 N4 N3 -120.0(4) . .
N5 Eu1 N4 N3 75.5(4) . .
K1 Eu1 N4 N3 115.1(4) 2_554 .
K2 Eu1 N4 N3 -91.8(4) . .
N8 Eu1 N4 C50 134(4) . .
N1 Eu1 N4 C50 -14(4) . .
N3 Eu1 N4 C50 -167(4) . .
N7 Eu1 N4 C50 176(4) . .
N6 Eu1 N4 C50 -97(4) . .
N10 Eu1 N4 C50 105(4) . .
N2 Eu1 N4 C50 0(4) . .
N9 Eu1 N4 C50 73(4) . .
N5 Eu1 N4 C50 -92(4) . .
K1 Eu1 N4 C50 -52(4) 2_554 .
K2 Eu1 N4 C50 101(4) . .
N8 Eu1 N4 K2 33.5(6) . .
N1 Eu1 N4 K2 -114.5(3) . .
N3 Eu1 N4 K2 91.8(4) . .
N7 Eu1 N4 K2 75.1(4) . .
N6 Eu1 N4 K2 162.7(2) . .
N10 Eu1 N4 K2 4.2(3) . .
N2 Eu1 N4 K2 -100.9(3) . .
N9 Eu1 N4 K2 -28.3(2) . .
N5 Eu1 N4 K2 167.3(3) . .
K1 Eu1 N4 K2 -153.10(17) 2_554 .
N10 K2 N4 N3 72.5(5) . .
C50 K2 N4 N3 -113.9(8) . .
C64 K2 N4 N3 67.5(5) . .
C16 K2 N4 N3 -173.0(5) 3 .
N9 K2 N4 N3 101.2(5) . .
C17 K2 N4 N3 165.4(5) 3 .
C18 K2 N4 N3 159.0(5) 3 .
C13 K2 N4 N3 -13.7(6) 3 .
C15 K2 N4 N3 -148.7(5) 3 .
C19 K2 N4 N3 -160.5(6) 3 .
C51 K2 N4 N3 -145.8(6) . .
N10 K2 N4 C50 -173.6(7) . .
C64 K2 N4 C50 -178.7(7) . .
C16 K2 N4 C50 -59.2(7) 3 .
N9 K2 N4 C50 -144.9(7) . .
C17 K2 N4 C50 -80.8(7) 3 .
C18 K2 N4 C50 -87.2(8) 3 .
C13 K2 N4 C50 100.2(7) 3 .
C15 K2 N4 C50 -34.8(7) 3 .
C19 K2 N4 C50 -46.7(9) 3 .
C51 K2 N4 C50 -31.9(6) . .
N10 K2 N4 Eu1 -3.9(2) . .
C50 K2 N4 Eu1 169.8(8) . .
C64 K2 N4 Eu1 -8.9(3) . .
C16 K2 N4 Eu1 110.6(4) 3 .
N9 K2 N4 Eu1 24.8(2) . .
C17 K2 N4 Eu1 89.0(4) 3 .
C18 K2 N4 Eu1 82.6(5) 3 .
C13 K2 N4 Eu1 -90.1(4) 3 .
C15 K2 N4 Eu1 134.9(3) 3 .
C19 K2 N4 Eu1 123.1(6) 3 .
C51 K2 N4 Eu1 137.9(5) . .
C6 C7 N5 N6 177.6(7) . .
P1 C7 N5 N6 0.7(9) . .
K1 C7 N5 N6 -68.9(5) 2_554 .
C6 C7 N5 Eu1 64(4) . .
P1 C7 N5 Eu1 -113(4) . .
K1 C7 N5 Eu1 177(4) 2_554 .
C6 C7 N5 K1 -113.5(7) . 2_554
P1 C7 N5 K1 69.6(5) . 2_554
N8 Eu1 N5 N6 -19.9(5) . .
N1 Eu1 N5 N6 96.7(4) . .
N4 Eu1 N5 N6 -171.6(4) . .
N3 Eu1 N5 N6 -140.8(4) . .
N7 Eu1 N5 N6 -42.9(4) . .
N10 Eu1 N5 N6 -128.4(6) . .
N2 Eu1 N5 N6 69.5(4) . .
N9 Eu1 N5 N6 147.0(6) . .
K1 Eu1 N5 N6 65.6(4) 2_554 .
K2 Eu1 N5 N6 -161.7(3) . .
N8 Eu1 N5 C7 97(4) . .
N1 Eu1 N5 C7 -146(4) . .
N4 Eu1 N5 C7 -54(4) . .
N3 Eu1 N5 C7 -23(4) . .
N7 Eu1 N5 C7 74(4) . .
N6 Eu1 N5 C7 117(4) . .
N10 Eu1 N5 C7 -11(4) . .
N2 Eu1 N5 C7 -173(4) . .
N9 Eu1 N5 C7 -96(4) . .
K1 Eu1 N5 C7 -177(4) 2_554 .
K2 Eu1 N5 C7 -44(4) . .
N8 Eu1 N5 K1 -85.5(3) . 2_554
N1 Eu1 N5 K1 31.0(2) . 2_554
N4 Eu1 N5 K1 122.8(2) . 2_554
N3 Eu1 N5 K1 153.6(2) . 2_554
N7 Eu1 N5 K1 -108.5(3) . 2_554
N6 Eu1 N5 K1 -65.6(4) . 2_554
N10 Eu1 N5 K1 165.9(4) . 2_554
N2 Eu1 N5 K1 3.9(2) . 2_554
N9 Eu1 N5 K1 81.4(6) . 2_554
K2 Eu1 N5 K1 132.66(13) . 2_554
C7 N5 N6 C8 -0.2(9) . .
Eu1 N5 N6 C8 171.3(6) . .
K1 N5 N6 C8 -82.6(6) 2_554 .
C7 N5 N6 Eu1 -171.5(6) . .
K1 N5 N6 Eu1 106.17(19) 2_554 .
C7 N5 N6 K1 82.4(6) . 2_554
Eu1 N5 N6 K1 -106.17(19) . 2_554
C9 C8 N6 N5 -178.8(7) . .
P1 C8 N6 N5 -0.4(8) . .
K1 C8 N6 N5 82.1(5) 2_554 .
C9 C8 N6 Eu1 -36(3) . .
P1 C8 N6 Eu1 142.7(19) . .
K1 C8 N6 Eu1 -135(2) 2_554 .
C9 C8 N6 K1 99.1(7) . 2_554
P1 C8 N6 K1 -82.6(5) . 2_554
N8 Eu1 N6 N5 162.6(4) . .
N1 Eu1 N6 N5 -78.3(4) . .
N4 Eu1 N6 N5 9.2(5) . .
N3 Eu1 N6 N5 39.2(4) . .
N7 Eu1 N6 N5 134.8(4) . .
N10 Eu1 N6 N5 126.2(6) . .
N2 Eu1 N6 N5 -109.8(4) . .
N9 Eu1 N6 N5 -129.1(7) . .
K1 Eu1 N6 N5 -81.7(4) 2_554 .
K2 Eu1 N6 N5 33.2(6) . .
N8 Eu1 N6 C8 17(2) . .
N1 Eu1 N6 C8 136(2) . .
N4 Eu1 N6 C8 -136(2) . .
N3 Eu1 N6 C8 -106(2) . .
N7 Eu1 N6 C8 -11(2) . .
N10 Eu1 N6 C8 -19(2) . .
N2 Eu1 N6 C8 105(2) . .
N9 Eu1 N6 C8 86(2) . .
N5 Eu1 N6 C8 -145(2) . .
K1 Eu1 N6 C8 133(2) 2_554 .
K2 Eu1 N6 C8 -112(2) . .
N8 Eu1 N6 K1 -115.8(3) . 2_554
N1 Eu1 N6 K1 3.3(2) . 2_554
N4 Eu1 N6 K1 90.9(3) . 2_554
N3 Eu1 N6 K1 120.9(2) . 2_554
N7 Eu1 N6 K1 -143.5(3) . 2_554
N10 Eu1 N6 K1 -152.2(5) . 2_554
N2 Eu1 N6 K1 -28.2(2) . 2_554
N9 Eu1 N6 K1 -47.4(8) . 2_554
N5 Eu1 N6 K1 81.7(4) . 2_554
K2 Eu1 N6 K1 114.9(3) . 2_554
C20 C21 N7 N8 -179.0(8) . .
P3 C21 N7 N8 0.2(10) . .
C20 C21 N7 Eu1 -14(10) . .
P3 C21 N7 Eu1 165(9) . .
N8 Eu1 N7 C21 -165(9) . .
N1 Eu1 N7 C21 -104(9) . .
N4 Eu1 N7 C21 61(9) . .
N3 Eu1 N7 C21 53(9) . .
N6 Eu1 N7 C21 -47(9) . .
N10 Eu1 N7 C21 129(9) . .
N2 Eu1 N7 C21 -123(9) . .
N9 Eu1 N7 C21 150(9) . .
N5 Eu1 N7 C21 -26(9) . .
K1 Eu1 N7 C21 -71(9) 2_554 .
K2 Eu1 N7 C21 103(9) . .
N1 Eu1 N7 N8 61.5(6) . .
N4 Eu1 N7 N8 -133.4(5) . .
N3 Eu1 N7 N8 -142.0(5) . .
N6 Eu1 N7 N8 118.2(5) . .
N10 Eu1 N7 N8 -65.3(5) . .
N2 Eu1 N7 N8 42.8(5) . .
N9 Eu1 N7 N8 -44.9(5) . .
N5 Eu1 N7 N8 139.2(5) . .
K1 Eu1 N7 N8 94.0(4) 2_554 .
K2 Eu1 N7 N8 -91.6(4) . .
C21 N7 N8 C22 0.5(10) . .
Eu1 N7 N8 C22 -178.3(7) . .
C21 N7 N8 Eu1 178.8(7) . .
C23 C22 N8 N7 179.9(8) . .
P3 C22 N8 N7 -1.1(9) . .
C23 C22 N8 Eu1 9(4) . .
P3 C22 N8 Eu1 -172(3) . .
N1 Eu1 N8 N7 -139.3(4) . .
N4 Eu1 N8 N7 77.8(6) . .
N3 Eu1 N8 N7 46.3(5) . .
N6 Eu1 N8 N7 -57.4(5) . .
N10 Eu1 N8 N7 108.1(5) . .
N2 Eu1 N8 N7 -140.9(5) . .
N9 Eu1 N8 N7 137.6(5) . .
N5 Eu1 N8 N7 -47.6(5) . .
K1 Eu1 N8 N7 -95.7(4) 2_554 .
K2 Eu1 N8 N7 99.9(4) . .
N1 Eu1 N8 C22 32(3) . .
N4 Eu1 N8 C22 -111(3) . .
N3 Eu1 N8 C22 -143(3) . .
N7 Eu1 N8 C22 171(4) . .
N6 Eu1 N8 C22 114(3) . .
N10 Eu1 N8 C22 -81(3) . .
N2 Eu1 N8 C22 30(3) . .
N9 Eu1 N8 C22 -51(3) . .
N5 Eu1 N8 C22 124(3) . .
K1 Eu1 N8 C22 75(3) 2_554 .
K2 Eu1 N8 C22 -89(3) . .
C62 C63 N9 N10 -179.8(8) . .
P5 C63 N9 N10 0.3(11) . .
C62 C63 N9 Eu1 75(3) . .
P5 C63 N9 Eu1 -105(3) . .
C62 C63 N9 K2 -115.3(9) . .
P5 C63 N9 K2 64.9(7) . .
N8 Eu1 N9 C63 47(3) . .
N1 Eu1 N9 C63 -73(3) . .
N4 Eu1 N9 C63 -164(3) . .
N3 Eu1 N9 C63 169(3) . .
N7 Eu1 N9 C63 69(3) . .
N6 Eu1 N9 C63 -22(3) . .
N10 Eu1 N9 C63 110(3) . .
N2 Eu1 N9 C63 -42(3) . .
N5 Eu1 N9 C63 -122(3) . .
K1 Eu1 N9 C63 -59(3) 2_554 .
K2 Eu1 N9 C63 170(3) . .
N8 Eu1 N9 N10 -63.3(5) . .
N1 Eu1 N9 N10 177.3(4) . .
N4 Eu1 N9 N10 85.9(5) . .
N3 Eu1 N9 N10 59.2(4) . .
N7 Eu1 N9 N10 -41.4(5) . .
N6 Eu1 N9 N10 -132.3(8) . .
N2 Eu1 N9 N10 -151.7(5) . .
N5 Eu1 N9 N10 128.3(5) . .
K1 Eu1 N9 N10 -169.6(4) 2_554 .
K2 Eu1 N9 N10 59.7(4) . .
N8 Eu1 N9 K2 -123.0(2) . .
N1 Eu1 N9 K2 117.6(2) . .
N4 Eu1 N9 K2 26.1(2) . .
N3 Eu1 N9 K2 -0.5(2) . .
N7 Eu1 N9 K2 -101.1(2) . .
N6 Eu1 N9 K2 168.0(7) . .
N10 Eu1 N9 K2 -59.7(4) . .
N2 Eu1 N9 K2 148.6(2) . .
N5 Eu1 N9 K2 68.6(6) . .
K1 Eu1 N9 K2 130.69(16) 2_554 .
N10 K2 N9 C63 -114.6(7) . .
C50 K2 N9 C63 144.6(6) . .
C64 K2 N9 C63 -78.4(6) . .
N4 K2 N9 C63 159.1(6) . .
C16 K2 N9 C63 51.0(6) 3 .
C17 K2 N9 C63 30.6(6) 3 .
C18 K2 N9 C63 9.7(6) 3 .
C13 K2 N9 C63 -111.7(6) 3 .
C15 K2 N9 C63 55.3(6) 3 .
C19 K2 N9 C63 8.0(6) 3 .
C51 K2 N9 C63 119.9(6) . .
C50 K2 N9 N10 -100.8(5) . .
C64 K2 N9 N10 36.2(4) . .
N4 K2 N9 N10 -86.4(5) . .
C16 K2 N9 N10 165.6(5) 3 .
C17 K2 N9 N10 145.2(5) 3 .
C18 K2 N9 N10 124.3(5) 3 .
C13 K2 N9 N10 2.9(5) 3 .
C15 K2 N9 N10 169.9(4) 3 .
C19 K2 N9 N10 122.6(5) 3 .
C51 K2 N9 N10 -125.5(5) . .
N10 K2 N9 Eu1 63.1(4) . .
C50 K2 N9 Eu1 -37.7(3) . .
C64 K2 N9 Eu1 99.3(4) . .
N4 K2 N9 Eu1 -23.2(2) . .
C16 K2 N9 Eu1 -131.3(3) 3 .
C17 K2 N9 Eu1 -151.7(3) 3 .
C18 K2 N9 Eu1 -172.6(3) 3 .
C13 K2 N9 Eu1 66.0(3) 3 .
C15 K2 N9 Eu1 -126.9(3) 3 .
C19 K2 N9 Eu1 -174.3(3) 3 .
C51 K2 N9 Eu1 -62.4(3) . .
C65 C64 N10 N9 -174.0(8) . .
P5 C64 N10 N9 2.7(9) . .
K2 C64 N10 N9 85.1(6) . .
C65 C64 N10 Eu1 -53(3) . .
P5 C64 N10 Eu1 123(2) . .
K2 C64 N10 Eu1 -154(3) . .
C65 C64 N10 K2 100.9(8) . .
P5 C64 N10 K2 -82.4(5) . .
C63 N9 N10 C64 -1.9(11) . .
Eu1 N9 N10 C64 164.9(7) . .
K2 N9 N10 C64 -80.9(6) . .
C63 N9 N10 Eu1 -166.8(7) . .
K2 N9 N10 Eu1 114.2(2) . .
C63 N9 N10 K2 78.9(7) . .
Eu1 N9 N10 K2 -114.2(2) . .
N8 Eu1 N10 C64 -15(3) . .
N1 Eu1 N10 C64 -129(3) . .
N4 Eu1 N10 C64 148(3) . .
N3 Eu1 N10 C64 116(3) . .
N7 Eu1 N10 C64 15(3) . .
N6 Eu1 N10 C64 24(3) . .
N2 Eu1 N10 C64 -96(3) . .
N9 Eu1 N10 C64 -126(3) . .
N5 Eu1 N10 C64 103(3) . .
K1 Eu1 N10 C64 -104(3) 2_554 .
K2 Eu1 N10 C64 152(3) . .
N8 Eu1 N10 N9 110.5(5) . .
N1 Eu1 N10 N9 -3.0(5) . .
N4 Eu1 N10 N9 -86.9(4) . .
N3 Eu1 N10 N9 -118.9(4) . .
N7 Eu1 N10 N9 140.8(5) . .
N6 Eu1 N10 N9 149.1(5) . .
N2 Eu1 N10 N9 29.8(5) . .
N5 Eu1 N10 N9 -131.2(6) . .
K1 Eu1 N10 N9 22.0(7) 2_554 .
K2 Eu1 N10 N9 -82.5(4) . .
N8 Eu1 N10 K2 -167.1(4) . .
N1 Eu1 N10 K2 79.4(4) . .
N4 Eu1 N10 K2 -4.5(3) . .
N3 Eu1 N10 K2 -36.4(3) . .
N7 Eu1 N10 K2 -136.7(3) . .
N6 Eu1 N10 K2 -128.4(5) . .
N2 Eu1 N10 K2 112.3(3) . .
N9 Eu1 N10 K2 82.5(4) . .
N5 Eu1 N10 K2 -48.7(7) . .
K1 Eu1 N10 K2 104.5(4) 2_554 .
C50 K2 N10 C64 -170.8(7) . .
N4 K2 N10 C64 -168.1(7) . .
C16 K2 N10 C64 96.8(7) 3 .
N9 K2 N10 C64 113.4(8) . .
C17 K2 N10 C64 76.9(7) 3 .
C18 K2 N10 C64 51.8(7) 3 .
C13 K2 N10 C64 -64.0(7) 3 .
C15 K2 N10 C64 98.6(7) 3 .
C19 K2 N10 C64 38.5(8) 3 .
C51 K2 N10 C64 167.0(7) . .
C50 K2 N10 N9 75.8(5) . .
C64 K2 N10 N9 -113.4(8) . .
N4 K2 N10 N9 78.5(4) . .
C16 K2 N10 N9 -16.6(5) 3 .
C17 K2 N10 N9 -36.5(5) 3 .
C18 K2 N10 N9 -61.6(5) 3 .
C13 K2 N10 N9 -177.4(5) 3 .
C15 K2 N10 N9 -14.8(6) 3 .
C19 K2 N10 N9 -74.9(5) 3 .
C51 K2 N10 N9 53.6(5) . .
C50 K2 N10 Eu1 1.2(4) . .
C64 K2 N10 Eu1 172.0(8) . .
N4 K2 N10 Eu1 3.9(3) . .
C16 K2 N10 Eu1 -91.2(4) 3 .
N9 K2 N10 Eu1 -74.6(4) . .
C17 K2 N10 Eu1 -111.1(4) 3 .
C18 K2 N10 Eu1 -136.2(3) 3 .
C13 K2 N10 Eu1 107.9(4) 3 .
C15 K2 N10 Eu1 -89.5(5) 3 .
C19 K2 N10 Eu1 -149.5(3) 3 .
C51 K2 N10 Eu1 -21.0(4) . .
N6 C8 P1 C7 0.7(6) . .
C9 C8 P1 C7 178.8(8) . .
K1 C8 P1 C7 -67.3(4) 2_554 .
N6 C8 P1 K1 68.0(6) . 2_554
C9 C8 P1 K1 -113.9(8) . 2_554
N5 C7 P1 C8 -0.8(6) . .
C6 C7 P1 C8 -177.3(8) . .
K1 C7 P1 C8 58.5(3) 2_554 .
N5 C7 P1 K1 -59.3(5) . 2_554
C6 C7 P1 K1 124.2(8) . 2_554
N1 C36 P2 C35 -0.7(7) . .
C37 C36 P2 C35 -176.9(9) . .
K1 C36 P2 C35 -72.6(4) 2_554 .
N1 C36 P2 K1 71.9(6) . 2_554
C37 C36 P2 K1 -104.3(8) . 2_554
N2 C35 P2 C36 -0.1(8) . .
C34 C35 P2 C36 -178.0(12) . .
K1 C35 P2 C36 59.8(3) 2_554 .
N2 C35 P2 K1 -59.9(7) . 2_554
C34 C35 P2 K1 122.2(11) . 2_554
N8 C22 P3 C21 0.9(7) . .
C23 C22 P3 C21 179.9(8) . .
N7 C21 P3 C22 -0.7(8) . .
C20 C21 P3 C22 178.5(9) . .
N4 C50 P4 C49 -0.9(7) . .
C51 C50 P4 C49 178.8(10) . .
K2 C50 P4 C49 -83.9(4) . .
N4 C50 P4 K2 82.9(6) . .
C51 C50 P4 K2 -97.3(10) . .
N3 C49 P4 C50 2.9(7) . .
C48 C49 P4 C50 -178.1(9) . .
N3 C49 P4 K2 -55.2(6) . .
C48 C49 P4 K2 123.8(9) . .
N10 K2 P4 C50 -64.0(5) . .
C64 K2 P4 C50 -79.8(5) . .
N4 K2 P4 C50 -34.9(4) . .
C16 K2 P4 C50 61.8(5) 3 .
N9 K2 P4 C50 -39.4(4) . .
C17 K2 P4 C50 56.8(6) 3 .
C18 K2 P4 C50 87.3(6) 3 .
C13 K2 P4 C50 -156.6(5) 3 .
C15 K2 P4 C50 83.5(5) 3 .
C19 K2 P4 C50 112.6(5) 3 .
C51 K2 P4 C50 25.7(5) . .
N10 K2 P4 C49 27.0(4) . .
C50 K2 P4 C49 91.0(5) . .
C64 K2 P4 C49 11.2(4) . .
N4 K2 P4 C49 56.1(4) . .
C16 K2 P4 C49 152.8(4) 3 .
N9 K2 P4 C49 51.6(4) . .
C17 K2 P4 C49 147.8(5) 3 .
C18 K2 P4 C49 178.3(5) 3 .
C13 K2 P4 C49 -65.6(4) 3 .
C15 K2 P4 C49 174.5(4) 3 .
C19 K2 P4 C49 -156.4(4) 3 .
C51 K2 P4 C49 116.7(4) . .
N10 C64 P5 C63 -2.0(7) . .
C65 C64 P5 C63 174.4(9) . .
K2 C64 P5 C63 -73.4(4) . .
N10 C64 P5 K2 71.3(6) . .
C65 C64 P5 K2 -112.3(9) . .
N9 C63 P5 C64 0.9(8) . .
C62 C63 P5 C64 -178.9(9) . .
N9 C63 P5 K2 -59.9(7) . .
C62 C63 P5 K2 120.2(9) . .
N10 K2 P5 C64 -32.8(4) . .
C50 K2 P5 C64 -68.3(5) . .
N4 K2 P5 C64 -55.8(4) . .
C16 K2 P5 C64 -165.2(4) 3 .
N9 K2 P5 C64 -68.1(4) . .
C17 K2 P5 C64 -173.7(5) 3 .
C18 K2 P5 C64 160.6(4) 3 .
C13 K2 P5 C64 51.1(4) 3 .
C15 K2 P5 C64 -179.3(4) 3 .
C19 K2 P5 C64 147.3(4) 3 .
C51 K2 P5 C64 -96.8(4) . .
N10 K2 P5 C63 61.8(4) . .
C50 K2 P5 C63 26.3(4) . .
C64 K2 P5 C63 94.6(5) . .
N4 K2 P5 C63 38.8(4) . .
C16 K2 P5 C63 -70.6(4) 3 .
N9 K2 P5 C63 26.5(4) . .
C17 K2 P5 C63 -79.1(4) 3 .
C18 K2 P5 C63 -104.8(4) 3 .
C13 K2 P5 C63 145.7(4) 3 .
C15 K2 P5 C63 -84.7(4) 3 .
C19 K2 P5 C63 -118.1(4) 3 .
C51 K2 P5 C63 -2.2(4) . .
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 -0.129 0.250 0.500 1067 141 ' '
2 0.088 0.750 0.000 1067 141 ' '
