#------------------------------------------------------------------------------
#$Date: 2016-03-05 11:48:34 +0200 (Sat, 05 Mar 2016) $
#$Revision: 177811 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/77/7037702.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7037702
loop_
_publ_author_name
'Wang, Xiuli'
'Sun, Junjun'
'Lin, Hongyan'
'Chang, Zhihan'
'Tian, Aixiang'
'Liu, Guocheng'
'Wang, Xiang'
_publ_section_title
;
 Novel Anderson-type [TeMo6O24](6-)-based metal-organic complexes tuned by
 different species and their coordination modes: assembly, various
 architectures and properties.
;
_journal_issue                   6
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2709
_journal_page_last               2719
_journal_paper_doi               10.1039/c5dt04074d
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C30 H56 Cu3 Mo6 N8 O40 Te'
_chemical_formula_weight         2062.68
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2015-11-18 deposited with the CCDC.
2015-12-21 downloaded from the CCDC.
;
_cell_angle_alpha                101.9420(10)
_cell_angle_beta                 102.6950(10)
_cell_angle_gamma                97.6270(10)
_cell_formula_units_Z            1
_cell_length_a                   8.3800(5)
_cell_length_b                   12.9090(7)
_cell_length_c                   14.8370(8)
_cell_measurement_reflns_used    7239
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      28.2906
_cell_measurement_theta_min      2.4420
_cell_volume                     1504.97(15)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0110
_diffrn_reflns_av_unetI/netI     0.0196
_diffrn_reflns_laue_measured_fraction_full 0.994
_diffrn_reflns_laue_measured_fraction_max 0.994
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            8414
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.994
_diffrn_reflns_theta_full        24.998
_diffrn_reflns_theta_max         24.998
_diffrn_reflns_theta_min         1.641
_diffrn_source                   'sealed tube'
_exptl_absorpt_coefficient_mu    2.826
_exptl_absorpt_correction_T_max  0.654
_exptl_absorpt_correction_T_min  0.513
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'ABSCOR by T.Higashi    8  March, 1995'
_exptl_crystal_colour            BLUE
_exptl_crystal_density_diffrn    2.276
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       BLOCK
_exptl_crystal_F_000             1003
_exptl_crystal_size_max          0.350
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.150
_refine_diff_density_max         0.496
_refine_diff_density_min         -0.567
_refine_diff_density_rms         0.081
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.959
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     410
_refine_ls_number_reflns         5269
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.959
_refine_ls_R_factor_all          0.0223
_refine_ls_R_factor_gt           0.0194
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0256P)²+2.6675P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0501
_refine_ls_wR_factor_ref         0.0514
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4835
_reflns_number_total             5300
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c5dt04074d2.cif
_cod_data_source_block           complex4
_cod_depositor_comments
'Adding full bibliography for 7037699--7037702.cif.'
_cod_database_code               7037702
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.438
_shelx_estimated_absorpt_t_max   0.676
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Te1 Te 1.0000 0.0000 0.0000 0.00911(6) Uani 1 2 d S . P
Cu1 Cu 1.37435(5) -0.03451(3) -0.26201(2) 0.02292(9) Uani 1 1 d . . .
N1 N 1.3497(3) -0.1047(2) -0.40006(18) 0.0267(6) Uani 1 1 d . . .
O1 O 1.1229(2) -0.14119(16) -0.27236(14) 0.0203(4) Uani 1 1 d . . .
Mo1 Mo 0.95721(3) -0.12313(2) -0.22338(2) 0.01260(6) Uani 1 1 d . . .
O1W O 1.3977(3) 0.0402(2) -0.12969(16) 0.0438(7) Uani 1 1 d . . .
H1WA H 1.4937 0.0770 -0.0950 0.046(12) Uiso 1 1 d R . .
H1WB H 1.3200 0.0276 -0.1010 0.046(12) Uiso 1 1 d R . .
C1 C 0.4541(4) -0.4388(3) -0.1174(3) 0.0347(8) Uani 1 1 d . . .
H1A H 0.3482 -0.4257 -0.1407 0.042 Uiso 1 1 calc R U .
Cu2 Cu 1.0000 -0.5000 0.0000 0.01588(11) Uani 1 2 d S . P
O2W O 1.4885(3) -0.14975(19) -0.21523(15) 0.0300(5) Uani 1 1 d . . .
H2WA H 1.5918 -0.1336 -0.1854 0.053(13) Uiso 1 1 d R . .
H2WB H 1.4332 -0.1787 -0.1801 0.060(14) Uiso 1 1 d R . .
C2 C 1.3216(5) -0.1951(4) -0.5906(2) 0.0468(10) Uani 1 1 d . . .
H2A H 1.3105 -0.2259 -0.6547 0.056 Uiso 1 1 calc R U .
Mo2 Mo 1.14823(3) -0.21899(2) -0.05115(2) 0.01198(6) Uani 1 1 d . . .
N2 N 0.7694(3) -0.47637(19) -0.04822(17) 0.0198(5) Uani 1 1 d . . .
O2 O 1.6393(2) 0.04877(16) -0.25445(14) 0.0201(4) Uani 1 1 d . . .
N3 N 0.2625(3) -0.6027(2) -0.28894(19) 0.0296(6) Uani 1 1 d . . .
H3B H 0.2497 -0.5367 -0.2801 0.036 Uiso 1 1 calc R U .
Mo3 Mo 0.82397(3) 0.10421(2) -0.17013(2) 0.01248(6) Uani 1 1 d . . .
O3W O 1.2416(3) 0.07678(18) -0.29727(16) 0.0302(5) Uani 1 1 d . . .
H3WA H 1.2855 0.1452 -0.2780 0.060(14) Uiso 1 1 d R . .
H3WB H 1.1559 0.0811 -0.2699 0.068(15) Uiso 1 1 d R . .
C3 C 0.7287(4) -0.3808(2) -0.0167(2) 0.0254(7) Uani 1 1 d . . .
H3A H 0.8088 -0.3268 0.0280 0.030 Uiso 1 1 calc R U .
O3 O 1.0963(3) -0.34136(16) -0.02632(14) 0.0214(4) Uani 1 1 d . . .
O4 O 0.9750(2) 0.02915(15) -0.22622(13) 0.0162(4) Uani 1 1 d . . .
N4 N 1.6314(4) -0.3339(3) -0.4938(2) 0.0445(8) Uani 1 1 d . . .
H4A H 1.6673 -0.2842 -0.4418 0.053 Uiso 1 1 calc R U .
C4 C 1.4835(5) -0.3336(3) -0.5496(2) 0.0357(8) Uani 1 1 d . . .
O4W O 1.0162(3) -0.56026(16) -0.13576(15) 0.0243(5) Uani 1 1 d . . .
H4WA H 0.9628 -0.6312 -0.1559 0.041(11) Uiso 1 1 d R . .
H4WB H 0.9698 -0.5264 -0.1757 0.053(13) Uiso 1 1 d R . .
O5 O 0.7818(3) -0.17827(17) -0.31302(14) 0.0245(5) Uani 1 1 d . . .
C5 C 1.8886(5) -0.3644(3) -0.5429(3) 0.0475(10) Uani 1 1 d . . .
H5A H 1.9576 -0.3081 -0.4894 0.057 Uiso 1 1 calc R U .
H5B H 1.9533 -0.4200 -0.5563 0.057 Uiso 1 1 calc R U .
O5W O 0.1686(5) -0.3923(3) -0.3142(2) 0.0693(9) Uani 1 1 d . . .
H5WA H 0.0645 -0.4130 -0.3230 0.083 Uiso 1 1 d R U .
H5WB H 0.2056 -0.3517 -0.2583 0.083 Uiso 1 1 d R U .
O6 O 0.9577(2) -0.23683(14) -0.15853(13) 0.0154(4) Uani 1 1 d . . .
C6 C 1.4055(4) -0.2380(3) -0.5214(2) 0.0329(8) Uani 1 1 d . . .
O6W O 0.8669(4) -0.4540(2) -0.26227(19) 0.0465(7) Uani 1 1 d . . .
H6WA H 0.7706 -0.4915 -0.3014 0.11(2) Uiso 1 1 d R . .
H6WB H 0.8579 -0.3997 -0.2283 0.062(16) Uiso 1 1 d R . .
O7 O 0.8878(3) 0.22787(16) -0.18922(14) 0.0225(4) Uani 1 1 d . . .
C7 C 1.2543(6) -0.1060(4) -0.5640(3) 0.0614(13) Uani 1 1 d . . .
H7A H 1.1989 -0.0748 -0.6099 0.074 Uiso 1 1 calc R U .
O8 O 0.8253(2) -0.05106(15) -0.11833(12) 0.0126(4) Uani 1 1 d . . .
C8 C 0.6543(4) -0.5532(2) -0.1132(2) 0.0221(6) Uani 1 1 d . . .
H8A H 0.6820 -0.6200 -0.1337 0.026 Uiso 1 1 calc R U .
O9 O 1.1454(2) -0.05166(14) -0.07532(13) 0.0121(4) Uani 1 1 d . . .
C9 C 1.4151(4) -0.1908(3) -0.4261(2) 0.0305(7) Uani 1 1 d . . .
H9A H 1.4696 -0.2210 -0.3792 0.037 Uiso 1 1 calc R U .
O10 O 1.0143(2) 0.13731(14) -0.03207(13) 0.0122(4) Uani 1 1 d . . .
C10 C 0.4960(4) -0.5375(3) -0.1514(2) 0.0246(7) Uani 1 1 d . . .
O11 O 1.3002(2) -0.23167(16) -0.11149(14) 0.0204(4) Uani 1 1 d . . .
C11 C 0.1526(5) -0.6824(3) -0.3712(3) 0.0436(9) Uani 1 1 d . . .
H11A H 0.0505 -0.7079 -0.3555 0.052 Uiso 1 1 calc R U .
H11B H 0.2061 -0.7436 -0.3866 0.052 Uiso 1 1 calc R U .
O12 O 0.4065(3) -0.7216(2) -0.2314(2) 0.0526(8) Uani 1 1 d . . .
C12 C 0.3815(4) -0.6289(3) -0.2275(2) 0.0286(7) Uani 1 1 d . . .
O13 O 1.4156(3) -0.4045(2) -0.62259(18) 0.0524(8) Uani 1 1 d . . .
C13 C 1.2693(5) -0.0630(4) -0.4689(3) 0.0459(10) Uani 1 1 d . . .
H13A H 1.2222 -0.0030 -0.4517 0.055 Uiso 1 1 calc R U .
O14 O 1.2916(2) -0.14350(15) 0.07050(13) 0.0159(4) Uani 1 1 d . . .
C14 C 0.5719(4) -0.3605(3) -0.0486(3) 0.0358(8) Uani 1 1 d . . .
H14A H 0.5455 -0.2945 -0.0240 0.043 Uiso 1 1 calc R U .
C15 C 1.7374(5) -0.4124(3) -0.5143(3) 0.0449(10) Uani 1 1 d . . .
H15A H 1.6728 -0.4730 -0.5655 0.054 Uiso 1 1 calc R U .
H15B H 1.7741 -0.4393 -0.4583 0.054 Uiso 1 1 calc R U .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Te Te -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O9 Te1 O9 180.0 . 2_755
O9 Te1 O10 85.67(8) . 2_755
O9 Te1 O10 94.33(8) 2_755 2_755
O9 Te1 O10 94.34(8) . .
O9 Te1 O10 85.67(8) 2_755 .
O10 Te1 O10 180.0 2_755 .
O9 Te1 O8 94.77(8) . 2_755
O9 Te1 O8 85.23(8) 2_755 2_755
O10 Te1 O8 85.12(8) 2_755 2_755
O10 Te1 O8 94.88(8) . 2_755
O9 Te1 O8 85.23(8) . .
O9 Te1 O8 94.77(8) 2_755 .
O10 Te1 O8 94.88(8) 2_755 .
O10 Te1 O8 85.12(8) . .
O8 Te1 O8 180.00(11) 2_755 .
O1W Cu1 O3W 86.09(11) . .
O1W Cu1 N1 177.27(12) . .
O3W Cu1 N1 91.54(10) . .
O1W Cu1 O2W 89.21(11) . .
O3W Cu1 O2W 172.55(9) . .
N1 Cu1 O2W 93.29(10) . .
O1W Cu1 O2 90.54(8) . .
O3W Cu1 O2 100.99(8) . .
N1 Cu1 O2 88.58(9) . .
O2W Cu1 O2 84.82(8) . .
O1W Cu1 O1 92.92(8) . .
O3W Cu1 O1 86.78(8) . .
N1 Cu1 O1 88.29(9) . .
O2W Cu1 O1 87.70(8) . .
O2 Cu1 O1 171.71(7) . .
C9 N1 C13 118.0(3) . .
C9 N1 Cu1 121.8(2) . .
C13 N1 Cu1 120.2(2) . .
Mo1 O1 Cu1 134.75(11) . .
O5 Mo1 O1 106.26(10) . .
O5 Mo1 O6 98.40(9) . .
O1 Mo1 O6 99.57(9) . .
O5 Mo1 O4 100.33(9) . .
O1 Mo1 O4 94.21(9) . .
O6 Mo1 O4 152.58(8) . .
O5 Mo1 O8 95.55(8) . .
O1 Mo1 O8 156.96(8) . .
O6 Mo1 O8 84.14(7) . .
O4 Mo1 O8 74.29(7) . .
O5 Mo1 O9 164.25(8) . .
O1 Mo1 O9 88.82(8) . .
O6 Mo1 O9 74.10(7) . .
O4 Mo1 O9 82.66(7) . .
O8 Mo1 O9 70.20(6) . .
C14 C1 C10 119.1(3) . .
N2 Cu2 N2 180.0 . 2_745
N2 Cu2 O4W 91.21(9) . .
N2 Cu2 O4W 88.79(9) 2_745 .
N2 Cu2 O4W 88.79(9) . 2_745
N2 Cu2 O4W 91.21(9) 2_745 2_745
O4W Cu2 O4W 180.0 . 2_745
N2 Cu2 O3 88.38(9) . .
N2 Cu2 O3 91.62(9) 2_745 .
O4W Cu2 O3 83.63(8) . .
O4W Cu2 O3 96.37(8) 2_745 .
N2 Cu2 O3 91.62(9) . 2_745
N2 Cu2 O3 88.38(9) 2_745 2_745
O4W Cu2 O3 96.37(8) . 2_745
O4W Cu2 O3 83.63(8) 2_745 2_745
O3 Cu2 O3 180.0 . 2_745
C6 C2 C7 119.0(3) . .
O11 Mo2 O3 106.50(9) . .
O11 Mo2 O14 97.19(9) . .
O3 Mo2 O14 98.73(9) . .
O11 Mo2 O6 99.15(9) . .
O3 Mo2 O6 96.93(9) . .
O14 Mo2 O6 153.11(8) . .
O11 Mo2 O10 158.49(8) . 2_755
O3 Mo2 O10 94.31(8) . 2_755
O14 Mo2 O10 73.84(7) . 2_755
O6 Mo2 O10 83.31(7) . 2_755
O11 Mo2 O9 89.18(8) . .
O3 Mo2 O9 163.52(8) . .
O14 Mo2 O9 83.93(7) . .
O6 Mo2 O9 75.11(7) . .
O10 Mo2 O9 70.68(6) 2_755 .
C8 N2 C3 118.8(3) . .
C8 N2 Cu2 121.4(2) . .
C3 N2 Cu2 119.8(2) . .
Mo3 O2 Cu1 138.59(10) 1_655 .
C12 N3 C11 122.1(3) . .
O7 Mo3 O2 106.04(10) . 1_455
O7 Mo3 O4 97.66(9) . .
O2 Mo3 O4 100.67(9) 1_455 .
O7 Mo3 O14 101.17(9) . 2_755
O2 Mo3 O14 91.96(8) 1_455 2_755
O4 Mo3 O14 153.45(8) . 2_755
O7 Mo3 O10 93.11(8) . .
O2 Mo3 O10 158.15(8) 1_455 .
O4 Mo3 O10 86.79(7) . .
O14 Mo3 O10 73.73(7) 2_755 .
O7 Mo3 O8 161.80(8) . .
O2 Mo3 O8 91.39(8) 1_455 .
O4 Mo3 O8 73.47(7) . .
O14 Mo3 O8 83.05(7) 2_755 .
O10 Mo3 O8 70.90(6) . .
N2 C3 C14 121.8(3) . .
Mo2 O3 Cu2 173.89(12) . .
Mo3 O4 Mo1 115.53(9) . .
C4 N4 C15 124.9(3) . .
O13 C4 N4 123.0(4) . .
O13 C4 C6 120.8(3) . .
N4 C4 C6 116.1(3) . .
C11 C5 C15 114.2(3) 2_744 .
Mo1 O6 Mo2 115.67(9) . .
C2 C6 C9 118.6(3) . .
C2 C6 C4 119.4(3) . .
C9 C6 C4 122.1(3) . .
C2 C7 C13 119.5(4) . .
Te1 O8 Mo1 103.64(8) . .
Te1 O8 Mo3 100.39(8) . .
Mo1 O8 Mo3 93.30(7) . .
N2 C8 C10 122.7(3) . .
Te1 O9 Mo2 101.69(8) . .
Te1 O9 Mo1 100.88(7) . .
Mo2 O9 Mo1 90.64(6) . .
N1 C9 C6 122.6(3) . .
Te1 O10 Mo3 103.59(8) . .
Te1 O10 Mo2 101.96(8) . 2_755
Mo3 O10 Mo2 93.27(7) . 2_755
C8 C10 C1 118.0(3) . .
C8 C10 C12 117.3(3) . .
C1 C10 C12 124.7(3) . .
N3 C11 C5 111.5(3) . 2_744
O12 C12 N3 124.2(3) . .
O12 C12 C10 119.1(3) . .
N3 C12 C10 116.6(3) . .
N1 C13 C7 122.3(4) . .
Mo2 O14 Mo3 114.44(9) . 2_755
C3 C14 C1 119.5(3) . .
N4 C15 C5 112.3(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Te1 O9 1.9192(17) .
Te1 O9 1.9192(17) 2_755
Te1 O10 1.9236(18) 2_755
Te1 O10 1.9236(18) .
Te1 O8 1.9481(17) 2_755
Te1 O8 1.9481(17) .
Cu1 O1W 1.955(2) .
Cu1 O3W 2.014(2) .
Cu1 N1 2.014(2) .
Cu1 O2W 2.030(2) .
Cu1 O2 2.304(2) .
Cu1 O1 2.316(2) .
N1 C9 1.328(4) .
N1 C13 1.345(4) .
O1 Mo1 1.7229(19) .
Mo1 O5 1.705(2) .
Mo1 O6 1.9143(19) .
Mo1 O4 1.9615(19) .
Mo1 O8 2.2241(18) .
Mo1 O9 2.3273(18) .
C1 C14 1.380(5) .
C1 C10 1.390(5) .
Cu2 N2 1.995(2) .
Cu2 N2 1.995(2) 2_745
Cu2 O4W 2.045(2) .
Cu2 O4W 2.045(2) 2_745
Cu2 O3 2.242(2) .
Cu2 O3 2.242(2) 2_745
C2 C6 1.370(5) .
C2 C7 1.371(6) .
Mo2 O11 1.7162(19) .
Mo2 O3 1.7173(19) .
Mo2 O14 1.9129(19) .
Mo2 O6 1.9426(18) .
Mo2 O10 2.2525(18) 2_755
Mo2 O9 2.2640(18) .
N2 C8 1.336(4) .
N2 C3 1.342(4) .
O2 Mo3 1.7193(19) 1_655
N3 C12 1.325(4) .
N3 C11 1.460(4) .
Mo3 O7 1.715(2) .
Mo3 O2 1.7193(19) 1_455
Mo3 O4 1.9203(18) .
Mo3 O14 1.9571(18) 2_755
Mo3 O10 2.2234(18) .
Mo3 O8 2.2908(18) .
C3 C14 1.374(4) .
N4 C4 1.331(5) .
N4 C15 1.462(5) .
C4 O13 1.231(4) .
C4 C6 1.499(5) .
C5 C11 1.513(6) 2_744
C5 C15 1.518(6) .
C6 C9 1.398(4) .
C7 C13 1.376(5) .
C8 C10 1.383(4) .
O10 Mo2 2.2525(18) 2_755
C10 C12 1.503(4) .
C11 C5 1.513(6) 2_744
O12 C12 1.234(4) .
O14 Mo3 1.9571(18) 2_755
