#------------------------------------------------------------------------------
#$Date: 2016-04-05 19:07:58 +0300 (Tue, 05 Apr 2016) $
#$Revision: 181657 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/78/7037817.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7037817
loop_
_publ_author_name
'Bortoluzzi, Marco'
'Ceriotti, Alessandro'
'Ciabatti, Iacopo'
'Della Pergola, Roberto'
'Femoni, Cristina'
'Carmela Iapalucci, Maria'
'Storione, Alba'
'Zacchini, Stefano'
_publ_section_title
;
 Platinum carbonyl clusters stabilized by Sn(ii)-based fragments:
 syntheses and structures of [Pt6(CO)6(SnCl2)2(SnCl3)4](4-),
 [Pt9(CO)8(SnCl2)3(SnCl3)2(Cl2SnOCOSnCl2)](4-) and
 [Pt10(CO)14{Cl2Sn(OH)SnCl2}2](2.).
;
_journal_issue                   12
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5001
_journal_page_last               5013
_journal_paper_doi               10.1039/c5dt04696c
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C54 H52 Cl14 O2 P2 Pt Sn5'
_chemical_formula_weight         2079.74
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-12-25 deposited with the CCDC.
2016-01-04 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 112.334(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   20.3822(7)
_cell_length_b                   14.5461(5)
_cell_length_c                   26.2602(11)
_cell_measurement_reflns_used    7759
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      22.1465
_cell_measurement_theta_min      2.1605
_cell_volume                     7201.6(5)
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_molecular_graphics    'SCHAKAL99 (Keller, 1999)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0759
_diffrn_reflns_av_unetI/netI     0.0434
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            56014
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         1.68
_exptl_absorpt_coefficient_mu    4.242
_exptl_absorpt_correction_T_max  0.6526
_exptl_absorpt_correction_T_min  0.5686
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details
;
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption corrections SADABS).
 R(int) = 0.1391 (selected reflections only, before parameter refinement)
 R(int) = 0.0599 (selected reflections only, after parameter refinement)
;
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.918
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             3952
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.11
_refine_diff_density_max         0.988
_refine_diff_density_min         -0.754
_refine_diff_density_rms         0.132
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.076
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     305
_refine_ls_number_reflns         7084
_refine_ls_number_restraints     108
_refine_ls_restrained_S_all      1.095
_refine_ls_R_factor_all          0.0741
_refine_ls_R_factor_gt           0.0472
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0374P)²+65.7748P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1013
_refine_ls_wR_factor_ref         0.1129
_reflns_number_gt                5160
_reflns_number_total             7084
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5dt04696c1.cif
_cod_data_source_block           PtSn6
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4268 2015-11-12 08:31:59Z antanas 

 Adding full bibliography for 7037810--7037817.cif.
;
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7037817
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt 0.0000 0.75728(3) 0.7500 0.03763(12) Uani 1 2 d S
Sn1 Sn 0.05013(3) 0.75200(5) 0.85534(2) 0.05525(18) Uani 1 1 d .
Sn2 Sn 0.10479(3) 0.85369(4) 0.74879(3) 0.05148(17) Uani 1 1 d .
Sn3 Sn 0.0000 0.58043(6) 0.7500 0.0528(2) Uani 1 2 d S
Cl1 Cl -0.02136(15) 0.6709(2) 0.89263(11) 0.0914(9) Uani 1 1 d .
Cl2 Cl 0.15926(14) 0.6811(2) 0.90458(12) 0.0889(9) Uani 1 1 d .
Cl3 Cl 0.06475(19) 0.8849(2) 0.90870(11) 0.0973(10) Uani 1 1 d .
Cl4 Cl 0.18842(15) 0.9096(2) 0.83379(12) 0.0984(10) Uani 1 1 d .
Cl5 Cl 0.18849(19) 0.8000(3) 0.7135(2) 0.1317(16) Uani 1 1 d .
Cl6 Cl 0.08189(15) 0.99793(18) 0.70313(11) 0.0753(7) Uani 1 1 d .
Cl7 Cl 0.0424(2) 0.4765(2) 0.82336(14) 0.1094(11) Uani 1 1 d .
O1 O 0.1151(4) 0.5695(6) 0.7520(4) 0.103(2) Uani 1 1 d U
C1 C 0.1581(7) 0.5364(10) 0.7382(6) 0.104(3) Uani 1 1 d U
C2 C 0.1395(10) 0.4664(14) 0.6970(8) 0.182(7) Uani 1 1 d U
H2A H 0.0897 0.4538 0.6847 0.273 Uiso 1 1 calc R
H2B H 0.1658 0.4115 0.7122 0.273 Uiso 1 1 calc R
H2C H 0.1506 0.4869 0.6665 0.273 Uiso 1 1 calc R
C3 C 0.2330(10) 0.5592(13) 0.7614(8) 0.172(6) Uani 1 1 d U
H3A H 0.2407 0.6091 0.7869 0.257 Uiso 1 1 calc R
H3B H 0.2482 0.5769 0.7324 0.257 Uiso 1 1 calc R
H3C H 0.2596 0.5065 0.7803 0.257 Uiso 1 1 calc R
P1 P 0.92266(13) 0.76873(16) 0.04455(9) 0.0501(5) Uani 1 1 d .
C101 C 1.0180(3) 0.7649(5) 0.0706(3) 0.054(2) Uani 1 1 d G
C102 C 1.0512(4) 0.7562(5) 0.0334(2) 0.089(4) Uani 1 1 d G
H102 H 1.0243 0.7541 -0.0042 0.106 Uiso 1 1 calc R
C103 C 1.1247(4) 0.7508(6) 0.0524(3) 0.094(4) Uani 1 1 d G
H103 H 1.1470 0.7450 0.0276 0.113 Uiso 1 1 calc R
C104 C 1.1650(3) 0.7539(5) 0.1086(4) 0.088(4) Uani 1 1 d G
H104 H 1.2142 0.7503 0.1213 0.105 Uiso 1 1 calc R
C105 C 1.1317(4) 0.7626(6) 0.1458(2) 0.101(4) Uani 1 1 d GU
H105 H 1.1586 0.7648 0.1834 0.122 Uiso 1 1 calc R
C106 C 1.0582(4) 0.7681(5) 0.1268(2) 0.089(3) Uani 1 1 d GU
H106 H 1.0359 0.7739 0.1516 0.106 Uiso 1 1 calc R
C107 C 0.8911(3) 0.6663(4) 0.0056(2) 0.053(2) Uani 1 1 d G
C108 C 0.8322(3) 0.6683(4) -0.0436(2) 0.070(3) Uani 1 1 d G
H108 H 0.8104 0.7240 -0.0576 0.085 Uiso 1 1 calc R
C109 C 0.8057(3) 0.5870(5) -0.0718(2) 0.087(4) Uani 1 1 d G
H109 H 0.7663 0.5884 -0.1046 0.104 Uiso 1 1 calc R
C110 C 0.8383(4) 0.5038(4) -0.0508(3) 0.095(4) Uani 1 1 d G
H110 H 0.8206 0.4494 -0.0696 0.114 Uiso 1 1 calc R
C111 C 0.8972(4) 0.5018(3) -0.0016(3) 0.086(3) Uani 1 1 d G
H111 H 0.9190 0.4461 0.0124 0.103 Uiso 1 1 calc R
C112 C 0.9237(3) 0.5831(4) 0.0265(2) 0.074(3) Uani 1 1 d G
H112 H 0.9631 0.5818 0.0594 0.088 Uiso 1 1 calc R
C113 C 0.8937(3) 0.7731(4) 0.1005(2) 0.056(2) Uani 1 1 d G
C114 C 0.8510(3) 0.7040(4) 0.1079(3) 0.065(3) Uani 1 1 d G
H114 H 0.8375 0.6547 0.0836 0.078 Uiso 1 1 calc R
C115 C 0.8284(4) 0.7088(5) 0.1515(3) 0.095(4) Uani 1 1 d GU
H115 H 0.7998 0.6626 0.1564 0.114 Uiso 1 1 calc R
C116 C 0.8485(4) 0.7826(6) 0.1878(3) 0.099(4) Uani 1 1 d GU
H116 H 0.8333 0.7858 0.2170 0.119 Uiso 1 1 calc R
C117 C 0.8912(4) 0.8516(5) 0.1805(3) 0.111(4) Uani 1 1 d GU
H117 H 0.9046 0.9010 0.2048 0.134 Uiso 1 1 calc R
C118 C 0.9138(4) 0.8469(4) 0.1368(3) 0.088(4) Uani 1 1 d G
H118 H 0.9424 0.8931 0.1319 0.106 Uiso 1 1 calc R
C119 C 0.8868(4) 0.8671(5) 0.0025(3) 0.067(3) Uani 1 1 d G
C120 C 0.8263(4) 0.9082(5) 0.0045(3) 0.088(3) Uani 1 1 d G
H120 H 0.8075 0.8877 0.0297 0.105 Uiso 1 1 calc R
C121 C 0.7939(4) 0.9800(6) -0.0311(4) 0.106(4) Uani 1 1 d GU
H121 H 0.7534 1.0076 -0.0297 0.127 Uiso 1 1 calc R
C122 C 0.8219(5) 1.0107(5) -0.0687(3) 0.123(4) Uani 1 1 d GU
H122 H 0.8002 1.0588 -0.0925 0.147 Uiso 1 1 calc R
C123 C 0.8824(5) 0.9696(7) -0.0708(3) 0.134(4) Uani 1 1 d GU
H123 H 0.9012 0.9901 -0.0959 0.161 Uiso 1 1 calc R
C124 C 0.9149(4) 0.8977(6) -0.0352(4) 0.124(5) Uani 1 1 d GU
H124 H 0.9553 0.8702 -0.0365 0.149 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Sn1 Pt1 Sn1 176.57(4) 2_556 .
Sn1 Pt1 Sn2 89.73(2) 2_556 .
Sn1 Pt1 Sn2 92.14(2) . .
Sn1 Pt1 Sn2 92.14(2) 2_556 2_556
Sn1 Pt1 Sn2 89.73(2) . 2_556
Sn2 Pt1 Sn2 113.72(3) . 2_556
Sn1 Pt1 Sn3 88.283(18) 2_556 .
Sn1 Pt1 Sn3 88.283(18) . .
Sn2 Pt1 Sn3 123.139(16) . .
Sn2 Pt1 Sn3 123.139(16) 2_556 .
Cl3 Sn1 Cl2 98.90(12) . .
Cl3 Sn1 Cl1 97.04(12) . .
Cl2 Sn1 Cl1 99.07(11) . .
Cl3 Sn1 Pt1 122.03(8) . .
Cl2 Sn1 Pt1 120.97(8) . .
Cl1 Sn1 Pt1 114.07(7) . .
Cl5 Sn2 Cl6 97.27(13) . .
Cl5 Sn2 Cl4 96.56(14) . .
Cl6 Sn2 Cl4 96.04(10) . .
Cl5 Sn2 Pt1 123.57(10) . .
Cl6 Sn2 Pt1 118.99(7) . .
Cl4 Sn2 Pt1 118.58(8) . .
O1 Sn3 O1 172.2(4) . 2_556
O1 Sn3 Cl7 91.7(2) . 2_556
O1 Sn3 Cl7 83.3(2) 2_556 2_556
O1 Sn3 Cl7 83.3(2) . .
O1 Sn3 Cl7 91.7(2) 2_556 .
Cl7 Sn3 Cl7 99.5(2) 2_556 .
O1 Sn3 Pt1 93.9(2) . .
O1 Sn3 Pt1 93.9(2) 2_556 .
Cl7 Sn3 Pt1 130.25(10) 2_556 .
Cl7 Sn3 Pt1 130.25(10) . .
C1 O1 Sn3 152.3(10) . .
O1 C1 C2 120.9(15) . .
O1 C1 C3 124.6(16) . .
C2 C1 C3 114.5(14) . .
C1 C2 H2A 109.5 . .
C1 C2 H2B 109.5 . .
H2A C2 H2B 109.5 . .
C1 C2 H2C 109.5 . .
H2A C2 H2C 109.5 . .
H2B C2 H2C 109.5 . .
C1 C3 H3A 109.5 . .
C1 C3 H3B 109.5 . .
H3A C3 H3B 109.5 . .
C1 C3 H3C 109.5 . .
H3A C3 H3C 109.5 . .
H3B C3 H3C 109.5 . .
C113 P1 C107 110.1(3) . .
C113 P1 C119 107.2(3) . .
C107 P1 C119 109.9(3) . .
C113 P1 C101 109.7(3) . .
C107 P1 C101 107.1(3) . .
C119 P1 C101 112.9(4) . .
C102 C101 C106 120.0 . .
C102 C101 P1 118.7(4) . .
C106 C101 P1 121.3(4) . .
C103 C102 C101 120.0 . .
C103 C102 H102 120.0 . .
C101 C102 H102 120.0 . .
C102 C103 C104 120.0 . .
C102 C103 H103 120.0 . .
C104 C103 H103 120.0 . .
C103 C104 C105 120.0 . .
C103 C104 H104 120.0 . .
C105 C104 H104 120.0 . .
C106 C105 C104 120.0 . .
C106 C105 H105 120.0 . .
C104 C105 H105 120.0 . .
C105 C106 C101 120.0 . .
C105 C106 H106 120.0 . .
C101 C106 H106 120.0 . .
C108 C107 C112 120.0 . .
C108 C107 P1 120.8(4) . .
C112 C107 P1 119.1(4) . .
C107 C108 C109 120.0 . .
C107 C108 H108 120.0 . .
C109 C108 H108 120.0 . .
C108 C109 C110 120.0 . .
C108 C109 H109 120.0 . .
C110 C109 H109 120.0 . .
C109 C110 C111 120.0 . .
C109 C110 H110 120.0 . .
C111 C110 H110 120.0 . .
C112 C111 C110 120.0 . .
C112 C111 H111 120.0 . .
C110 C111 H111 120.0 . .
C111 C112 C107 120.0 . .
C111 C112 H112 120.0 . .
C107 C112 H112 120.0 . .
C114 C113 C118 120.0 . .
C114 C113 P1 120.7(4) . .
C118 C113 P1 119.3(4) . .
C113 C114 C115 120.0 . .
C113 C114 H114 120.0 . .
C115 C114 H114 120.0 . .
C114 C115 C116 120.0 . .
C114 C115 H115 120.0 . .
C116 C115 H115 120.0 . .
C115 C116 C117 120.0 . .
C115 C116 H116 120.0 . .
C117 C116 H116 120.0 . .
C118 C117 C116 120.0 . .
C118 C117 H117 120.0 . .
C116 C117 H117 120.0 . .
C117 C118 C113 120.0 . .
C117 C118 H118 120.0 . .
C113 C118 H118 120.0 . .
C120 C119 C124 120.0 . .
C120 C119 P1 118.8(5) . .
C124 C119 P1 121.0(5) . .
C121 C120 C119 120.0 . .
C121 C120 H120 120.0 . .
C119 C120 H120 120.0 . .
C122 C121 C120 120.0 . .
C122 C121 H121 120.0 . .
C120 C121 H121 120.0 . .
C123 C122 C121 120.0 . .
C123 C122 H122 120.0 . .
C121 C122 H122 120.0 . .
C122 C123 C124 120.0 . .
C122 C123 H123 120.0 . .
C124 C123 H123 120.0 . .
C123 C124 C119 120.0 . .
C123 C124 H124 120.0 . .
C119 C124 H124 120.0 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 Sn1 2.5600(6) 2_556
Pt1 Sn1 2.5600(6) .
Pt1 Sn2 2.5654(6) .
Pt1 Sn2 2.5654(6) 2_556
Pt1 Sn3 2.5724(10) .
Sn1 Cl3 2.339(3) .
Sn1 Cl2 2.344(3) .
Sn1 Cl1 2.357(3) .
Sn2 Cl5 2.362(3) .
Sn2 Cl6 2.373(3) .
Sn2 Cl4 2.378(3) .
Sn3 O1 2.332(8) .
Sn3 O1 2.332(8) 2_556
Sn3 Cl7 2.341(3) 2_556
Sn3 Cl7 2.341(3) .
O1 C1 1.172(13) .
C1 C2 1.43(2) .
C1 C3 1.45(2) .
C2 H2A 0.9600 .
C2 H2B 0.9600 .
C2 H2C 0.9600 .
C3 H3A 0.9600 .
C3 H3B 0.9600 .
C3 H3C 0.9600 .
P1 C113 1.782(5) .
P1 C107 1.783(5) .
P1 C119 1.786(6) .
P1 C101 1.798(5) .
C101 C102 1.3900 .
C101 C106 1.3900 .
C102 C103 1.3900 .
C102 H102 0.9300 .
C103 C104 1.3900 .
C103 H103 0.9300 .
C104 C105 1.3900 .
C104 H104 0.9300 .
C105 C106 1.3900 .
C105 H105 0.9300 .
C106 H106 0.9300 .
C107 C108 1.3900 .
C107 C112 1.3900 .
C108 C109 1.3900 .
C108 H108 0.9300 .
C109 C110 1.3900 .
C109 H109 0.9300 .
C110 C111 1.3900 .
C110 H110 0.9300 .
C111 C112 1.3900 .
C111 H111 0.9300 .
C112 H112 0.9300 .
C113 C114 1.3900 .
C113 C118 1.3900 .
C114 C115 1.3900 .
C114 H114 0.9300 .
C115 C116 1.3900 .
C115 H115 0.9300 .
C116 C117 1.3900 .
C116 H116 0.9300 .
C117 C118 1.3900 .
C117 H117 0.9300 .
C118 H118 0.9300 .
C119 C120 1.3900 .
C119 C124 1.3900 .
C120 C121 1.3900 .
C120 H120 0.9300 .
C121 C122 1.3900 .
C121 H121 0.9300 .
C122 C123 1.3900 .
C122 H122 0.9300 .
C123 C124 1.3900 .
C123 H123 0.9300 .
C124 H124 0.9300 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Sn1 Pt1 Sn1 Cl3 -173.64(11) 2_556 .
Sn2 Pt1 Sn1 Cl3 63.26(11) . .
Sn2 Pt1 Sn1 Cl3 -50.47(11) 2_556 .
Sn3 Pt1 Sn1 Cl3 -173.64(11) . .
Sn1 Pt1 Sn1 Cl2 60.33(10) 2_556 .
Sn2 Pt1 Sn1 Cl2 -62.78(10) . .
Sn2 Pt1 Sn1 Cl2 -176.51(10) 2_556 .
Sn3 Pt1 Sn1 Cl2 60.33(10) . .
Sn1 Pt1 Sn1 Cl1 -57.68(10) 2_556 .
Sn2 Pt1 Sn1 Cl1 179.21(10) . .
Sn2 Pt1 Sn1 Cl1 65.49(10) 2_556 .
Sn3 Pt1 Sn1 Cl1 -57.68(10) . .
Sn1 Pt1 Sn2 Cl5 -62.86(15) 2_556 .
Sn1 Pt1 Sn2 Cl5 114.27(15) . .
Sn2 Pt1 Sn2 Cl5 -155.08(15) 2_556 .
Sn3 Pt1 Sn2 Cl5 24.92(15) . .
Sn1 Pt1 Sn2 Cl6 59.93(8) 2_556 .
Sn1 Pt1 Sn2 Cl6 -122.95(8) . .
Sn2 Pt1 Sn2 Cl6 -32.30(8) 2_556 .
Sn3 Pt1 Sn2 Cl6 147.70(8) . .
Sn1 Pt1 Sn2 Cl4 175.95(10) 2_556 .
Sn1 Pt1 Sn2 Cl4 -6.92(10) . .
Sn2 Pt1 Sn2 Cl4 83.73(10) 2_556 .
Sn3 Pt1 Sn2 Cl4 -96.27(10) . .
Sn1 Pt1 Sn3 O1 90.6(2) 2_556 .
Sn1 Pt1 Sn3 O1 -89.4(2) . .
Sn2 Pt1 Sn3 O1 2.0(2) . .
Sn2 Pt1 Sn3 O1 -178.0(2) 2_556 .
Sn1 Pt1 Sn3 O1 -89.4(2) 2_556 2_556
Sn1 Pt1 Sn3 O1 90.6(2) . 2_556
Sn2 Pt1 Sn3 O1 -178.0(2) . 2_556
Sn2 Pt1 Sn3 O1 2.0(2) 2_556 2_556
Sn1 Pt1 Sn3 Cl7 -4.93(12) 2_556 2_556
Sn1 Pt1 Sn3 Cl7 175.07(12) . 2_556
Sn2 Pt1 Sn3 Cl7 -93.49(12) . 2_556
Sn2 Pt1 Sn3 Cl7 86.51(12) 2_556 2_556
Sn1 Pt1 Sn3 Cl7 175.07(12) 2_556 .
Sn1 Pt1 Sn3 Cl7 -4.93(12) . .
Sn2 Pt1 Sn3 Cl7 86.51(12) . .
Sn2 Pt1 Sn3 Cl7 -93.49(12) 2_556 .
O1 Sn3 O1 C1 41(2) 2_556 .
Cl7 Sn3 O1 C1 -9(2) 2_556 .
Cl7 Sn3 O1 C1 91(2) . .
Pt1 Sn3 O1 C1 -139(2) . .
Sn3 O1 C1 C2 4(3) . .
Sn3 O1 C1 C3 -173.8(14) . .
C113 P1 C101 C102 176.6(4) . .
C107 P1 C101 C102 57.1(5) . .
C119 P1 C101 C102 -63.9(5) . .
C113 P1 C101 C106 -1.8(5) . .
C107 P1 C101 C106 -121.2(4) . .
C119 P1 C101 C106 117.7(5) . .
C106 C101 C102 C103 0.0 . .
P1 C101 C102 C103 -178.4(5) . .
C101 C102 C103 C104 0.0 . .
C102 C103 C104 C105 0.0 . .
C103 C104 C105 C106 0.0 . .
C104 C105 C106 C101 0.0 . .
C102 C101 C106 C105 0.0 . .
P1 C101 C106 C105 178.3(5) . .
C113 P1 C107 C108 100.6(4) . .
C119 P1 C107 C108 -17.3(5) . .
C101 P1 C107 C108 -140.2(4) . .
C113 P1 C107 C112 -75.5(4) . .
C119 P1 C107 C112 166.6(4) . .
C101 P1 C107 C112 43.6(5) . .
C112 C107 C108 C109 0.0 . .
P1 C107 C108 C109 -176.1(5) . .
C107 C108 C109 C110 0.0 . .
C108 C109 C110 C111 0.0 . .
C109 C110 C111 C112 0.0 . .
C110 C111 C112 C107 0.0 . .
C108 C107 C112 C111 0.0 . .
P1 C107 C112 C111 176.2(5) . .
C107 P1 C113 C114 -1.7(5) . .
C119 P1 C113 C114 117.8(5) . .
C101 P1 C113 C114 -119.3(4) . .
C107 P1 C113 C118 178.8(4) . .
C119 P1 C113 C118 -61.7(5) . .
C101 P1 C113 C118 61.2(5) . .
C118 C113 C114 C115 0.0 . .
P1 C113 C114 C115 -179.5(5) . .
C113 C114 C115 C116 0.0 . .
C114 C115 C116 C117 0.0 . .
C115 C116 C117 C118 0.0 . .
C116 C117 C118 C113 0.0 . .
C114 C113 C118 C117 0.0 . .
P1 C113 C118 C117 179.5(5) . .
C113 P1 C119 C120 -23.6(6) . .
C107 P1 C119 C120 96.0(5) . .
C101 P1 C119 C120 -144.5(5) . .
C113 P1 C119 C124 161.8(5) . .
C107 P1 C119 C124 -78.6(5) . .
C101 P1 C119 C124 40.9(6) . .
C124 C119 C120 C121 0.0 . .
P1 C119 C120 C121 -174.7(6) . .
C119 C120 C121 C122 0.0 . .
C120 C121 C122 C123 0.0 . .
C121 C122 C123 C124 0.0 . .
C122 C123 C124 C119 0.0 . .
C120 C119 C124 C123 0.0 . .
P1 C119 C124 C123 174.6(6) . .
