#------------------------------------------------------------------------------
#$Date: 2016-04-05 18:49:04 +0300 (Tue, 05 Apr 2016) $
#$Revision: 181646 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/86/7038618.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7038618
loop_
_publ_author_name
'Wang, Shi'
'Xu, Wu-Tan'
'He, Wen-Rui'
'Takaishi, Shinya'
'Li, Yong-Hua'
'Yamashita, Masahiro'
'Huang, Wei'
_publ_section_title
;
 Structural insights into the counterion effects on the manganese(iii)
 spin crossover system with hexadentate Schiff-base ligands.
;
_journal_issue                   13
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5676
_journal_page_last               5688
_journal_paper_doi               10.1039/c5dt04824a
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C24 H32 Cl Mn N4 O8'
_chemical_formula_weight         594.93
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yc'
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2016-01-12 deposited with the CCDC.
2016-02-18 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 96.05(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.925(4)
_cell_length_b                   8.5661(17)
_cell_length_c                   17.723(4)
_cell_measurement_reflns_used    9322
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      28.22
_cell_measurement_theta_min      2.59
_cell_volume                     2706.2(10)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  SHELXL
_computing_structure_solution    SHELXS
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0401
_diffrn_reflns_av_sigmaI/netI    0.0446
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            21576
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.07
_exptl_absorpt_coefficient_mu    0.640
_exptl_absorpt_correction_T_max  0.932
_exptl_absorpt_correction_T_min  0.891
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS; Bruker, 2000'
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.460
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1240
_exptl_crystal_size_max          0.33
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.11
_refine_diff_density_max         1.017
_refine_diff_density_min         -0.509
_refine_diff_density_rms         0.075
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.097
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     354
_refine_ls_number_reflns         6190
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.097
_refine_ls_R_factor_all          0.1151
_refine_ls_R_factor_gt           0.0798
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1354P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2196
_refine_ls_wR_factor_ref         0.2544
_reflns_number_gt                3957
_reflns_number_total             6190
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5dt04824a2.cif
_cod_data_source_block           m2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4268 2015-11-12 08:31:59Z antanas 

 Adding full bibliography for 7038613--7038620.cif.
;
_cod_original_sg_symbol_H-M      P2/c
_cod_database_code               7038618
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.7732(5) 1.3026(8) 0.3769(4) 0.118(2) Uani 1 1 d .
H1 H 0.8147 1.3450 0.3535 0.176 Uiso 1 1 calc R
H2 H 0.7530 1.3814 0.4075 0.176 Uiso 1 1 calc R
H3 H 0.7351 1.2685 0.3383 0.176 Uiso 1 1 calc R
O1 O 0.7983(2) 1.1729(4) 0.4237(2) 0.0855(10) Uani 1 1 d .
C2 C 0.8261(2) 1.0479(5) 0.3881(3) 0.0655(11) Uani 1 1 d .
C3 C 0.8350(2) 0.9123(6) 0.4340(3) 0.0693(12) Uani 1 1 d .
H4 H 0.8208 0.9140 0.4830 0.083 Uiso 1 1 calc R
C4 C 0.8643(3) 0.7793(5) 0.4067(3) 0.0650(11) Uani 1 1 d .
H5 H 0.8673 0.6898 0.4365 0.078 Uiso 1 1 calc R
C5 C 0.8452(2) 1.0433(5) 0.3159(3) 0.0607(10) Uani 1 1 d .
H6 H 0.8368 1.1298 0.2845 0.073 Uiso 1 1 calc R
C6 C 0.8781(2) 0.9062(5) 0.2883(2) 0.0546(9) Uani 1 1 d .
C7 C 0.8899(2) 0.7745(5) 0.3349(2) 0.0556(10) Uani 1 1 d .
C8 C 0.8914(2) 0.8996(5) 0.2091(2) 0.0585(10) Uani 1 1 d .
H7 H 0.8664 0.9710 0.1759 0.070 Uiso 1 1 calc R
O2 O 0.92185(15) 0.6437(3) 0.31225(16) 0.0577(7) Uani 1 1 d .
Mn1 Mn 1.0000 0.64823(10) 0.2500 0.0515(3) Uani 1 2 d S
N1 N 0.9357(2) 0.8008(4) 0.1819(2) 0.0594(8) Uani 1 1 d .
C9 C 0.9321(3) 0.7851(5) 0.0983(3) 0.0663(11) Uani 1 1 d .
H8 H 0.9821 0.7942 0.0825 0.080 Uiso 1 1 calc R
H9 H 0.9014 0.8680 0.0742 0.080 Uiso 1 1 calc R
C10 C 0.8987(3) 0.6271(6) 0.0740(3) 0.0782(14) Uani 1 1 d .
H10 H 0.8503 0.6172 0.0936 0.094 Uiso 1 1 calc R
H11 H 0.8898 0.6253 0.0191 0.094 Uiso 1 1 calc R
C11 C 0.9458(3) 0.4865(6) 0.0996(3) 0.0721(12) Uani 1 1 d .
H12 H 0.9242 0.3942 0.0741 0.087 Uiso 1 1 calc R
H13 H 0.9959 0.5001 0.0845 0.087 Uiso 1 1 calc R
C12 C 1.0080(3) 0.3198(6) 0.2934(3) 0.0752(13) Uani 1 1 d .
H14 H 0.9611 0.3153 0.3162 0.090 Uiso 1 1 calc R
H15 H 1.0376 0.2288 0.3098 0.090 Uiso 1 1 calc R
N2 N 1.0488(2) 0.4615(5) 0.3175(2) 0.0651(9) Uani 1 1 d D
H16 H 1.0906(19) 0.453(4) 0.306(2) 0.046(11) Uiso 1 1 d D
C13 C 0.4140(10) 1.4025(12) -0.0095(5) 0.244(9) Uani 1 1 d .
H17 H 0.4327 1.4231 0.0423 0.366 Uiso 1 1 calc R
H18 H 0.3760 1.4775 -0.0259 0.366 Uiso 1 1 calc R
H19 H 0.4544 1.4101 -0.0408 0.366 Uiso 1 1 calc R
O3 O 0.3890(4) 1.2795(7) -0.0142(3) 0.151(3) Uani 1 1 d .
C14 C 0.4116(4) 1.1516(7) 0.0290(3) 0.0936(18) Uani 1 1 d .
C15 C 0.4781(4) 1.1356(6) 0.0733(3) 0.0805(15) Uani 1 1 d .
H20 H 0.5130 1.2162 0.0752 0.097 Uiso 1 1 calc R
C16 C 0.4949(3) 0.9994(5) 0.1163(2) 0.0636(11) Uani 1 1 d .
C17 C 0.3619(3) 1.0280(8) 0.0230(3) 0.0926(17) Uani 1 1 d .
H21 H 0.3172 1.0368 -0.0083 0.111 Uiso 1 1 calc R
C18 C 0.3775(3) 0.8934(7) 0.0622(3) 0.0770(13) Uani 1 1 d .
H22 H 0.3434 0.8112 0.0563 0.092 Uiso 1 1 calc R
C19 C 0.4436(2) 0.8754(5) 0.1112(2) 0.0604(10) Uani 1 1 d .
O4 O 0.45557(17) 0.7417(3) 0.14964(18) 0.0630(8) Uani 1 1 d .
Mn2 Mn 0.5000 0.74220(10) 0.2500 0.0555(3) Uani 1 2 d S
C20 C 0.5675(3) 0.9827(5) 0.1575(3) 0.0673(11) Uani 1 1 d .
H23 H 0.6055 1.0480 0.1443 0.081 Uiso 1 1 calc R
N4 N 0.58434(19) 0.8841(4) 0.2117(2) 0.0616(9) Uani 1 1 d .
C21 C 0.6636(2) 0.8643(6) 0.2416(3) 0.0763(13) Uani 1 1 d .
H24 H 0.6689 0.8785 0.2962 0.092 Uiso 1 1 calc R
H25 H 0.6938 0.9429 0.2198 0.092 Uiso 1 1 calc R
C22 C 0.6916(3) 0.7021(7) 0.2227(3) 0.0844(15) Uani 1 1 d .
H26 H 0.6832 0.6874 0.1682 0.101 Uiso 1 1 calc R
H27 H 0.7454 0.6980 0.2369 0.101 Uiso 1 1 calc R
C23 C 0.6556(3) 0.5680(7) 0.2607(3) 0.0828(15) Uani 1 1 d .
H28 H 0.6839 0.4735 0.2538 0.099 Uiso 1 1 calc R
H29 H 0.6581 0.5886 0.3147 0.099 Uiso 1 1 calc R
N3 N 0.5752(2) 0.5419(5) 0.2302(2) 0.0683(10) Uani 1 1 d .
C24 C 0.5416(3) 0.4021(6) 0.2613(3) 0.0823(14) Uani 1 1 d .
H31 H 0.5515 0.4019 0.3162 0.099 Uiso 1 1 calc R
H32 H 0.5638 0.3089 0.2421 0.099 Uiso 1 1 calc R
Cl1 Cl 0.74756(6) 1.28652(14) 0.11925(7) 0.0664(3) Uani 1 1 d .
O5 O 0.67009(19) 1.3050(4) 0.1296(2) 0.0835(10) Uani 1 1 d .
O6 O 0.7626(2) 1.3607(5) 0.0506(2) 0.0935(12) Uani 1 1 d .
O7 O 0.7926(2) 1.3537(5) 0.1834(2) 0.0972(12) Uani 1 1 d .
O8 O 0.7634(3) 1.1249(5) 0.1140(3) 0.1024(13) Uani 1 1 d .
H33 H 0.573(2) 0.525(5) 0.182(3) 0.062(13) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 C1 H1 109.5 . .
O1 C1 H2 109.5 . .
H1 C1 H2 109.5 . .
O1 C1 H3 109.5 . .
H1 C1 H3 109.5 . .
H2 C1 H3 109.5 . .
C2 O1 C1 116.7(4) . .
C5 C2 O1 126.8(4) . .
C5 C2 C3 119.5(4) . .
O1 C2 C3 113.7(4) . .
C4 C3 C2 120.3(4) . .
C4 C3 H4 119.8 . .
C2 C3 H4 119.8 . .
C3 C4 C7 121.6(4) . .
C3 C4 H5 119.2 . .
C7 C4 H5 119.2 . .
C2 C5 C6 120.1(4) . .
C2 C5 H6 119.9 . .
C6 C5 H6 119.9 . .
C7 C6 C5 120.3(4) . .
C7 C6 C8 120.6(4) . .
C5 C6 C8 118.8(4) . .
O2 C7 C4 119.3(4) . .
O2 C7 C6 122.7(4) . .
C4 C7 C6 117.9(4) . .
N1 C8 C6 123.9(4) . .
N1 C8 H7 118.0 . .
C6 C8 H7 118.0 . .
C7 O2 Mn1 122.0(2) . .
O2 Mn1 O2 177.62(17) 2_755 .
O2 Mn1 N1 87.17(13) 2_755 2_755
O2 Mn1 N1 94.35(13) . 2_755
O2 Mn1 N1 94.35(13) 2_755 .
O2 Mn1 N1 87.17(13) . .
N1 Mn1 N1 100.7(2) 2_755 .
O2 Mn1 N2 86.64(14) 2_755 2_755
O2 Mn1 N2 91.57(15) . 2_755
N1 Mn1 N2 169.13(15) 2_755 2_755
N1 Mn1 N2 88.63(15) . 2_755
O2 Mn1 N2 91.57(15) 2_755 .
O2 Mn1 N2 86.64(14) . .
N1 Mn1 N2 88.63(14) 2_755 .
N1 Mn1 N2 169.13(15) . .
N2 Mn1 N2 82.6(2) 2_755 .
C8 N1 C9 118.0(4) . .
C8 N1 Mn1 122.0(3) . .
C9 N1 Mn1 119.5(3) . .
N1 C9 C10 109.7(4) . .
N1 C9 H8 109.7 . .
C10 C9 H8 109.7 . .
N1 C9 H9 109.7 . .
C10 C9 H9 109.7 . .
H8 C9 H9 108.2 . .
C11 C10 C9 115.6(4) . .
C11 C10 H10 108.4 . .
C9 C10 H10 108.4 . .
C11 C10 H11 108.4 . .
C9 C10 H11 108.4 . .
H10 C10 H11 107.5 . .
N2 C11 C10 112.9(4) 2_755 .
N2 C11 H12 109.0 2_755 .
C10 C11 H12 109.0 . .
N2 C11 H13 109.0 2_755 .
C10 C11 H13 109.0 . .
H12 C11 H13 107.8 . .
N2 C12 C12 109.2(3) . 2_755
N2 C12 H14 109.8 . .
C12 C12 H14 109.8 2_755 .
N2 C12 H15 109.8 . .
C12 C12 H15 109.8 2_755 .
H14 C12 H15 108.3 . .
C12 N2 C11 113.0(4) . 2_755
C12 N2 Mn1 107.3(3) . .
C11 N2 Mn1 115.5(3) 2_755 .
C12 N2 H16 108(3) . .
C11 N2 H16 107(3) 2_755 .
Mn1 N2 H16 106(3) . .
O3 C13 H17 109.5 . .
O3 C13 H18 109.5 . .
H17 C13 H18 109.5 . .
O3 C13 H19 109.5 . .
H17 C13 H19 109.5 . .
H18 C13 H19 109.5 . .
C13 O3 C14 127.2(9) . .
C15 C14 O3 126.1(7) . .
C15 C14 C17 119.0(5) . .
O3 C14 C17 114.8(6) . .
C14 C15 C16 121.2(5) . .
C14 C15 H20 119.4 . .
C16 C15 H20 119.4 . .
C19 C16 C15 119.4(4) . .
C19 C16 C20 120.9(4) . .
C15 C16 C20 119.3(4) . .
C18 C17 C14 121.1(5) . .
C18 C17 H21 119.5 . .
C14 C17 H21 119.5 . .
C17 C18 C19 121.6(5) . .
C17 C18 H22 119.2 . .
C19 C18 H22 119.2 . .
O4 C19 C16 123.1(4) . .
O4 C19 C18 119.3(4) . .
C16 C19 C18 117.6(4) . .
C19 O4 Mn2 120.7(3) . .
O4 Mn2 O4 179.73(18) . 2_655
O4 Mn2 N4 86.72(14) . .
O4 Mn2 N4 93.44(14) 2_655 .
O4 Mn2 N4 93.44(14) . 2_655
O4 Mn2 N4 86.72(14) 2_655 2_655
N4 Mn2 N4 109.5(2) . 2_655
O4 Mn2 N3 93.01(15) . .
O4 Mn2 N3 86.78(14) 2_655 .
N4 Mn2 N3 85.84(15) . .
N4 Mn2 N3 163.63(16) 2_655 .
O4 Mn2 N3 86.78(14) . 2_655
O4 Mn2 N3 93.01(15) 2_655 2_655
N4 Mn2 N3 163.63(16) . 2_655
N4 Mn2 N3 85.84(15) 2_655 2_655
N3 Mn2 N3 79.5(2) . 2_655
N4 C20 C16 125.0(4) . .
N4 C20 H23 117.5 . .
C16 C20 H23 117.5 . .
C20 N4 C21 119.0(4) . .
C20 N4 Mn2 119.9(3) . .
C21 N4 Mn2 121.0(3) . .
N4 C21 C22 110.7(4) . .
N4 C21 H24 109.5 . .
C22 C21 H24 109.5 . .
N4 C21 H25 109.5 . .
C22 C21 H25 109.5 . .
H24 C21 H25 108.1 . .
C23 C22 C21 115.3(4) . .
C23 C22 H26 108.4 . .
C21 C22 H26 108.4 . .
C23 C22 H27 108.4 . .
C21 C22 H27 108.4 . .
H26 C22 H27 107.5 . .
N3 C23 C22 113.1(4) . .
N3 C23 H28 109.0 . .
C22 C23 H28 109.0 . .
N3 C23 H29 109.0 . .
C22 C23 H29 109.0 . .
H28 C23 H29 107.8 . .
C24 N3 C23 113.7(4) . .
C24 N3 Mn2 106.8(3) . .
C23 N3 Mn2 113.7(3) . .
C24 N3 H33 105(3) . .
C23 N3 H33 108(3) . .
Mn2 N3 H33 109(3) . .
N3 C24 C24 109.4(4) . 2_655
N3 C24 H31 109.8 . .
C24 C24 H31 109.8 2_655 .
N3 C24 H32 109.8 . .
C24 C24 H32 109.8 2_655 .
H31 C24 H32 108.2 . .
O8 Cl1 O6 108.8(3) . .
O8 Cl1 O5 108.7(3) . .
O6 Cl1 O5 109.5(3) . .
O8 Cl1 O7 110.0(3) . .
O6 Cl1 O7 110.8(3) . .
O5 Cl1 O7 109.0(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O1 1.430(7) .
C1 H1 0.9600 .
C1 H2 0.9600 .
C1 H3 0.9600 .
O1 C2 1.364(5) .
C2 C5 1.359(6) .
C2 C3 1.417(7) .
C3 C4 1.365(6) .
C3 H4 0.9300 .
C4 C7 1.398(6) .
C4 H5 0.9300 .
C5 C6 1.423(6) .
C5 H6 0.9300 .
C6 C7 1.401(6) .
C6 C8 1.451(6) .
C7 O2 1.339(5) .
C8 N1 1.288(5) .
C8 H7 0.9300 .
O2 Mn1 1.873(3) .
Mn1 O2 1.873(3) 2_755
Mn1 N1 2.049(4) 2_755
Mn1 N1 2.049(4) .
Mn1 N2 2.129(4) 2_755
Mn1 N2 2.129(4) .
N1 C9 1.482(5) .
C9 C10 1.524(7) .
C9 H8 0.9700 .
C9 H9 0.9700 .
C10 C11 1.513(7) .
C10 H10 0.9700 .
C10 H11 0.9700 .
C11 N2 1.477(6) 2_755
C11 H12 0.9700 .
C11 H13 0.9700 .
C12 N2 1.458(6) .
C12 C12 1.533(10) 2_755
C12 H14 0.9700 .
C12 H15 0.9700 .
N2 C11 1.477(6) 2_755
N2 H16 0.80(3) .
C13 O3 1.145(13) .
C13 H17 0.9600 .
C13 H18 0.9600 .
C13 H19 0.9600 .
O3 C14 1.372(7) .
C14 C15 1.363(9) .
C14 C17 1.380(9) .
C15 C16 1.410(6) .
C15 H20 0.9300 .
C16 C19 1.401(6) .
C16 C20 1.431(7) .
C17 C18 1.359(8) .
C17 H21 0.9300 .
C18 C19 1.402(6) .
C18 H22 0.9300 .
C19 O4 1.339(5) .
O4 Mn2 1.871(3) .
Mn2 O4 1.871(3) 2_655
Mn2 N4 2.108(4) .
Mn2 N4 2.108(3) 2_655
Mn2 N3 2.232(4) .
Mn2 N3 2.232(4) 2_655
C20 N4 1.289(6) .
C20 H23 0.9300 .
N4 C21 1.473(5) .
C21 C22 1.527(8) .
C21 H24 0.9700 .
C21 H25 0.9700 .
C22 C23 1.511(8) .
C22 H26 0.9700 .
C22 H27 0.9700 .
C23 N3 1.502(6) .
C23 H28 0.9700 .
C23 H29 0.9700 .
N3 C24 1.473(6) .
N3 H33 0.87(4) .
C24 C24 1.504(11) 2_655
C24 H31 0.9700 .
C24 H32 0.9700 .
Cl1 O8 1.418(4) .
Cl1 O6 1.423(4) .
Cl1 O5 1.429(4) .
Cl1 O7 1.443(4) .
