#------------------------------------------------------------------------------
#$Date: 2016-09-10 02:31:56 +0300 (Sat, 10 Sep 2016) $
#$Revision: 186399 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/03/97/7039725.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7039725
loop_
_publ_author_name
'Sroor, Farid M.'
'Hrib, Cristian G.'
'Liebing, Phil'
'Hilfert, Liane'
'Busse, Sabine'
'Edelmann, Frank T.'
_publ_section_title
;
 Five different types of η(8)-cyclooctatetraenyl-lanthanide half-sandwich
 complexes from one ligand set, including a "giant neodymium
 wheel".
;
_journal_issue                   34
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              13332
_journal_page_last               13346
_journal_paper_doi               10.1039/c6dt01974a
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C190 H264 Cl8 N16 Nd8'
_chemical_formula_weight         4209.69
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-04-01 deposited with the CCDC.
2016-06-28 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 125.03(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   44.794(9)
_cell_length_b                   21.617(4)
_cell_length_c                   32.326(7)
_cell_measurement_reflns_used    79042
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      75.2450
_cell_measurement_theta_min      3.2670
_cell_volume                     25631(13)
_computing_cell_refinement
; 
CrysAlisPro, Agilent Technologies, 
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET) 
(compiled Feb  1 2013,16:14:44) 
;
_computing_data_collection
; 
CrysAlisPro, Agilent Technologies, 
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET) 
(compiled Feb  1 2013,16:14:44) 
;
_computing_data_reduction
; 
CrysAlisPro, Agilent Technologies, 
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET) 
(compiled Feb  1 2013,16:14:44) 
;
_computing_molecular_graphics    'Bruker XP'
_computing_publication_material  SHELXL-97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 10.3543
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Xcalibur, Atlas, Nova'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0925
_diffrn_reflns_av_sigmaI/netI    0.0316
_diffrn_reflns_limit_h_max       56
_diffrn_reflns_limit_h_min       -55
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_l_max       40
_diffrn_reflns_limit_l_min       -40
_diffrn_reflns_number            451720
_diffrn_reflns_theta_full        26.56
_diffrn_reflns_theta_max         26.56
_diffrn_reflns_theta_min         1.51
_exptl_absorpt_coefficient_mu    1.712
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.52253
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
; 
CrysAlisPro, Agilent Technologies, 
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET) 
(compiled Feb  1 2013,16:14:44) 
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.091
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             8528
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.11
_refine_diff_density_max         2.533
_refine_diff_density_min         -1.664
_refine_diff_density_rms         0.131
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.056
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1001
_refine_ls_number_reflns         26581
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.056
_refine_ls_R_factor_all          0.0554
_refine_ls_R_factor_gt           0.0478
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0644P)²+178.5040P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1160
_refine_ls_wR_factor_ref         0.1205
_reflns_number_gt                24025
_reflns_number_total             26581
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c6dt01974a2.cif
_cod_data_source_block           magd112
_cod_depositor_comments
'Adding full bibliography for 7039717--7039725.cif.'
_cod_original_cell_volume        25631(9)
_cod_database_code               7039725
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Nd1 Nd 0.053896(6) 0.348199(10) 0.319911(8) 0.01670(6) Uani 1 1 d .
Nd2 Nd 0.126458(6) 0.189954(10) 0.403036(8) 0.01520(6) Uani 1 1 d .
Nd3 Nd 0.137778(6) 0.002907(10) 0.365445(8) 0.01630(6) Uani 1 1 d .
Nd4 Nd 0.055743(6) -0.137312(10) 0.272740(8) 0.01628(6) Uani 1 1 d .
Cl1 Cl 0.06414(3) 0.24747(5) 0.38270(4) 0.01906(19) Uani 1 1 d .
Cl2 Cl 0.10916(3) 0.27816(4) 0.32753(4) 0.01646(18) Uani 1 1 d .
Cl3 Cl 0.08452(3) -0.02870(5) 0.26437(4) 0.01880(19) Uani 1 1 d .
Cl4 Cl 0.10392(3) -0.09849(4) 0.37465(4) 0.01665(18) Uani 1 1 d .
N1 N 0.09379(10) 0.43682(17) 0.34372(14) 0.0205(7) Uani 1 1 d .
N2 N 0.07520(11) 0.41048(17) 0.39350(14) 0.0215(8) Uani 1 1 d .
N3 N 0.14861(10) 0.21019(17) 0.49034(14) 0.0198(7) Uani 1 1 d .
N4 N 0.17710(10) 0.25498(17) 0.45841(13) 0.0186(7) Uani 1 1 d .
N5 N 0.19304(10) -0.05664(17) 0.42263(13) 0.0186(7) Uani 1 1 d .
N6 N 0.17934(10) -0.03033(17) 0.34547(14) 0.0192(7) Uani 1 1 d .
N7 N 0.09807(10) -0.21955(16) 0.29386(14) 0.0204(7) Uani 1 1 d .
N8 N 0.06968(11) -0.17878(17) 0.21617(14) 0.0216(8) Uani 1 1 d .
C1 C 0.09686(12) 0.4454(2) 0.38679(17) 0.0215(9) Uani 1 1 d .
C2 C 0.12256(13) 0.4887(2) 0.42501(17) 0.0225(9) Uani 1 1 d .
C3 C 0.14339(13) 0.5228(2) 0.45974(18) 0.0240(9) Uani 1 1 d .
C4 C 0.16646(15) 0.5615(2) 0.50215(19) 0.0327(11) Uani 1 1 d .
H4 H 0.1856 0.5848 0.5019 0.039 Uiso 1 1 calc R
C5 C 0.1752(2) 0.5455(3) 0.5523(2) 0.0535(18) Uani 1 1 d .
H5A H 0.1657 0.5058 0.5555 0.064 Uiso 1 1 calc R
H5B H 0.1997 0.5567 0.5822 0.064 Uiso 1 1 calc R
C6 C 0.1492(2) 0.5953(4) 0.5257(3) 0.062(2) Uani 1 1 d .
H6A H 0.1574 0.6381 0.5382 0.074 Uiso 1 1 calc R
H6B H 0.1233 0.5869 0.5114 0.074 Uiso 1 1 calc R
C7 C 0.11608(13) 0.4734(2) 0.33286(17) 0.0224(9) Uani 1 1 d .
H7 H 0.1401 0.4826 0.3653 0.027 Uiso 1 1 calc R
C8 C 0.12271(14) 0.4360(2) 0.29890(19) 0.0268(10) Uani 1 1 d .
H8A H 0.0990 0.4238 0.2680 0.032 Uiso 1 1 calc R
H8B H 0.1361 0.3977 0.3167 0.032 Uiso 1 1 calc R
C9 C 0.14444(16) 0.4722(2) 0.2840(2) 0.0343(12) Uani 1 1 d .
H9A H 0.1692 0.4805 0.3146 0.041 Uiso 1 1 calc R
H9B H 0.1469 0.4470 0.2606 0.041 Uiso 1 1 calc R
C10 C 0.12591(17) 0.5331(3) 0.2589(2) 0.0382(13) Uani 1 1 d .
H10A H 0.1023 0.5248 0.2264 0.046 Uiso 1 1 calc R
H10B H 0.1413 0.5568 0.2516 0.046 Uiso 1 1 calc R
C11 C 0.11962(16) 0.5711(2) 0.2928(2) 0.0341(12) Uani 1 1 d .
H11A H 0.1065 0.6096 0.2752 0.041 Uiso 1 1 calc R
H11B H 0.1434 0.5827 0.3239 0.041 Uiso 1 1 calc R
C12 C 0.09732(14) 0.5345(2) 0.30704(19) 0.0254(10) Uani 1 1 d .
H12A H 0.0944 0.5597 0.3301 0.030 Uiso 1 1 calc R
H12B H 0.0728 0.5259 0.2762 0.030 Uiso 1 1 calc R
C13 C 0.07715(13) 0.4157(2) 0.44044(17) 0.0238(9) Uani 1 1 d .
H13 H 0.0824 0.4598 0.4519 0.029 Uiso 1 1 calc R
C14 C 0.04019(14) 0.3987(3) 0.4287(2) 0.0301(11) Uani 1 1 d .
H14A H 0.0337 0.3563 0.4147 0.036 Uiso 1 1 calc R
H14B H 0.0215 0.4273 0.4028 0.036 Uiso 1 1 calc R
C15 C 0.04014(15) 0.4019(3) 0.4761(2) 0.0348(12) Uani 1 1 d .
H15A H 0.0435 0.4454 0.4876 0.042 Uiso 1 1 calc R
H15B H 0.0163 0.3875 0.4677 0.042 Uiso 1 1 calc R
C16 C 0.07033(17) 0.3622(3) 0.5184(2) 0.0382(12) Uani 1 1 d .
H16A H 0.0651 0.3181 0.5086 0.046 Uiso 1 1 calc R
H16B H 0.0709 0.3680 0.5492 0.046 Uiso 1 1 calc R
C17 C 0.10761(15) 0.3788(3) 0.52997(19) 0.0335(11) Uani 1 1 d .
H17A H 0.1143 0.4213 0.5439 0.040 Uiso 1 1 calc R
H17B H 0.1262 0.3501 0.5558 0.040 Uiso 1 1 calc R
C18 C 0.10732(14) 0.3751(2) 0.48272(18) 0.0268(10) Uani 1 1 d .
H18A H 0.1035 0.3317 0.4710 0.032 Uiso 1 1 calc R
H18B H 0.1312 0.3888 0.4909 0.032 Uiso 1 1 calc R
C19 C 0.00716(16) 0.4268(3) 0.2362(2) 0.0516(19) Uani 1 1 d .
H19 H 0.0102 0.4675 0.2281 0.062 Uiso 1 1 calc R
C20 C 0.01841(15) 0.3820(4) 0.2172(2) 0.0504(19) Uani 1 1 d .
H20 H 0.0282 0.3992 0.2003 0.061 Uiso 1 1 calc R
C21 C 0.01870(13) 0.3170(4) 0.21714(19) 0.0431(16) Uani 1 1 d .
H21 H 0.0283 0.3007 0.1997 0.052 Uiso 1 1 calc R
C22 C 0.00834(16) 0.2708(3) 0.2365(2) 0.0480(17) Uani 1 1 d .
H22 H 0.0134 0.2303 0.2305 0.058 Uiso 1 1 calc R
C23 C 0.17301(12) 0.25084(19) 0.49635(16) 0.0197(8) Uani 1 1 d .
C24 C 0.19467(13) 0.2893(2) 0.54095(18) 0.0264(10) Uani 1 1 d .
C25 C 0.21461(14) 0.3211(3) 0.57648(19) 0.0316(11) Uani 1 1 d .
C26 C 0.23908(16) 0.3620(3) 0.6179(2) 0.0396(13) Uani 1 1 d .
H26 H 0.2631 0.3433 0.6446 0.047 Uiso 1 1 calc R
C27 C 0.2409(2) 0.4250(4) 0.6053(3) 0.068(2) Uani 1 1 d .
H27A H 0.2237 0.4383 0.5698 0.082 Uiso 1 1 calc R
H27B H 0.2651 0.4454 0.6239 0.082 Uiso 1 1 calc R
C28 C 0.2241(2) 0.4059(3) 0.6370(3) 0.066(2) Uani 1 1 d .
H28A H 0.2388 0.4148 0.6737 0.079 Uiso 1 1 calc R
H28B H 0.1974 0.4076 0.6195 0.079 Uiso 1 1 calc R
C29 C 0.14212(14) 0.2031(2) 0.52943(17) 0.0247(10) Uani 1 1 d .
H29 H 0.1465 0.2438 0.5467 0.030 Uiso 1 1 calc R
C30 C 0.10296(14) 0.1841(3) 0.50611(19) 0.0301(11) Uani 1 1 d .
H30A H 0.0979 0.1450 0.4872 0.036 Uiso 1 1 calc R
H30B H 0.0865 0.2163 0.4818 0.036 Uiso 1 1 calc R
C31 C 0.09487(16) 0.1752(3) 0.5453(2) 0.0378(13) Uani 1 1 d .
H31A H 0.0695 0.1604 0.5285 0.045 Uiso 1 1 calc R
H31B H 0.0971 0.2153 0.5616 0.045 Uiso 1 1 calc R
C32 C 0.12105(17) 0.1284(3) 0.5857(2) 0.0462(16) Uani 1 1 d .
H32A H 0.1165 0.0869 0.5702 0.055 Uiso 1 1 calc R
H32B H 0.1165 0.1261 0.6123 0.055 Uiso 1 1 calc R
C33 C 0.16108(17) 0.1471(3) 0.6097(2) 0.0409(14) Uani 1 1 d .
H33A H 0.1664 0.1864 0.6285 0.049 Uiso 1 1 calc R
H33B H 0.1775 0.1149 0.6339 0.049 Uiso 1 1 calc R
C34 C 0.16822(14) 0.1552(2) 0.56902(18) 0.0288(10) Uani 1 1 d .
H34A H 0.1650 0.1150 0.5522 0.035 Uiso 1 1 calc R
H34B H 0.1937 0.1688 0.5850 0.035 Uiso 1 1 calc R
C35 C 0.20157(12) 0.3007(2) 0.46019(18) 0.0227(9) Uani 1 1 d .
H35 H 0.2238 0.3033 0.4957 0.027 Uiso 1 1 calc R
C36 C 0.21341(12) 0.2801(2) 0.42637(18) 0.0239(9) Uani 1 1 d .
H36A H 0.1917 0.2767 0.3910 0.029 Uiso 1 1 calc R
H36B H 0.2250 0.2388 0.4373 0.029 Uiso 1 1 calc R
C37 C 0.24034(13) 0.3263(2) 0.4289(2) 0.0306(11) Uani 1 1 d .
H37A H 0.2464 0.3134 0.4052 0.037 Uiso 1 1 calc R
H37B H 0.2631 0.3264 0.4634 0.037 Uiso 1 1 calc R
C38 C 0.22418(15) 0.3918(3) 0.4154(2) 0.0364(12) Uani 1 1 d .
H38A H 0.2430 0.4213 0.4208 0.044 Uiso 1 1 calc R
H38B H 0.2037 0.3931 0.3791 0.044 Uiso 1 1 calc R
C39 C 0.21063(14) 0.4113(2) 0.4470(2) 0.0329(11) Uani 1 1 d .
H39A H 0.1983 0.4519 0.4348 0.039 Uiso 1 1 calc R
H39B H 0.2317 0.4164 0.4825 0.039 Uiso 1 1 calc R
C40 C 0.18425(13) 0.3643(2) 0.44445(19) 0.0247(9) Uani 1 1 d .
H40A H 0.1772 0.3776 0.4670 0.030 Uiso 1 1 calc R
H40B H 0.1619 0.3625 0.4095 0.030 Uiso 1 1 calc R
C41 C 0.12051(19) 0.1227(2) 0.3224(2) 0.0384(14) Uani 1 1 d .
H41 H 0.1151 0.1342 0.2904 0.046 Uiso 1 1 calc R
C42 C 0.09001(17) 0.1074(2) 0.3207(2) 0.0444(16) Uani 1 1 d .
H42 H 0.0682 0.1146 0.2882 0.053 Uiso 1 1 calc R
C43 C 0.08269(15) 0.0836(2) 0.3551(3) 0.0455(17) Uani 1 1 d .
H43 H 0.0574 0.0766 0.3396 0.055 Uiso 1 1 calc R
C44 C 0.1040(2) 0.0683(2) 0.4058(3) 0.0451(17) Uani 1 1 d .
H44 H 0.0899 0.0548 0.4177 0.054 Uiso 1 1 calc R
C45 C 0.1421(2) 0.0682(2) 0.4443(2) 0.0463(17) Uani 1 1 d .
H45 H 0.1478 0.0516 0.4753 0.056 Uiso 1 1 calc R
C46 C 0.17353(16) 0.0871(2) 0.4473(2) 0.0438(17) Uani 1 1 d .
H46 H 0.1952 0.0840 0.4805 0.053 Uiso 1 1 calc R
C47 C 0.17999(15) 0.1090(2) 0.4129(3) 0.0424(15) Uani 1 1 d .
H47 H 0.2053 0.1146 0.4276 0.051 Uiso 1 1 calc R
C48 C 0.15845(19) 0.1251(2) 0.3616(3) 0.0414(15) Uani 1 1 d .
H48 H 0.1724 0.1413 0.3505 0.050 Uiso 1 1 calc R
C49 C 0.19981(12) -0.06370(19) 0.38758(17) 0.0203(9) Uani 1 1 d .
C50 C 0.22692(13) -0.1072(2) 0.39382(18) 0.0249(9) Uani 1 1 d .
C51 C 0.24614(14) -0.1471(2) 0.3957(2) 0.0289(10) Uani 1 1 d .
C52 C 0.26794(18) -0.1952(3) 0.3941(3) 0.0421(14) Uani 1 1 d .
H52 H 0.2881 -0.2127 0.4273 0.050 Uiso 1 1 calc R
C53 C 0.2497(2) -0.2387(3) 0.3504(3) 0.062(2) Uani 1 1 d .
H53A H 0.2582 -0.2822 0.3568 0.074 Uiso 1 1 calc R
H53B H 0.2233 -0.2331 0.3244 0.074 Uiso 1 1 calc R
C54 C 0.2749(3) -0.1906(4) 0.3542(4) 0.082(3) Uani 1 1 d .
H54A H 0.2640 -0.1551 0.3306 0.099 Uiso 1 1 calc R
H54B H 0.2989 -0.2042 0.3630 0.099 Uiso 1 1 calc R
C55 C 0.21594(13) -0.0878(2) 0.47113(17) 0.0224(9) Uani 1 1 d .
H55 H 0.2253 -0.1270 0.4661 0.027 Uiso 1 1 calc R
C56 C 0.19410(13) -0.1037(2) 0.49240(18) 0.0255(10) Uani 1 1 d .
H56A H 0.1737 -0.1315 0.4687 0.031 Uiso 1 1 calc R
H56B H 0.1837 -0.0654 0.4961 0.031 Uiso 1 1 calc R
C57 C 0.21852(14) -0.1354(2) 0.54385(19) 0.0321(11) Uani 1 1 d .
H57A H 0.2042 -0.1437 0.5578 0.039 Uiso 1 1 calc R
H57B H 0.2269 -0.1756 0.5394 0.039 Uiso 1 1 calc R
C58 C 0.25163(15) -0.0958(3) 0.58131(19) 0.0353(12) Uani 1 1 d .
H58A H 0.2676 -0.1192 0.6131 0.042 Uiso 1 1 calc R
H58B H 0.2434 -0.0579 0.5892 0.042 Uiso 1 1 calc R
C59 C 0.27326(14) -0.0779(2) 0.5596(2) 0.0326(11) Uani 1 1 d .
H59A H 0.2932 -0.0492 0.5831 0.039 Uiso 1 1 calc R
H59B H 0.2843 -0.1153 0.5560 0.039 Uiso 1 1 calc R
C60 C 0.24838(13) -0.0471(2) 0.50838(19) 0.0263(10) Uani 1 1 d .
H60A H 0.2625 -0.0376 0.4943 0.032 Uiso 1 1 calc R
H60B H 0.2393 -0.0075 0.5127 0.032 Uiso 1 1 calc R
C61 C 0.18439(13) -0.0362(2) 0.30436(18) 0.0225(9) Uani 1 1 d .
H61 H 0.2111 -0.0401 0.3197 0.027 Uiso 1 1 calc R
C62 C 0.17045(14) 0.0231(2) 0.27291(19) 0.0266(10) Uani 1 1 d .
H62A H 0.1443 0.0285 0.2587 0.032 Uiso 1 1 calc R
H62B H 0.1839 0.0590 0.2949 0.032 Uiso 1 1 calc R
C63 C 0.17543(17) 0.0207(2) 0.2301(2) 0.0344(12) Uani 1 1 d .
H63A H 0.2017 0.0188 0.2443 0.041 Uiso 1 1 calc R
H63B H 0.1653 0.0587 0.2094 0.041 Uiso 1 1 calc R
C64 C 0.15622(18) -0.0358(3) 0.1968(2) 0.0394(13) Uani 1 1 d .
H64A H 0.1609 -0.0379 0.1703 0.047 Uiso 1 1 calc R
H64B H 0.1296 -0.0318 0.1798 0.047 Uiso 1 1 calc R
C65 C 0.16978(16) -0.0956(2) 0.2282(2) 0.0335(12) Uani 1 1 d .
H65A H 0.1561 -0.1313 0.2061 0.040 Uiso 1 1 calc R
H65B H 0.1959 -0.1017 0.2424 0.040 Uiso 1 1 calc R
C66 C 0.16482(15) -0.0929(2) 0.27088(19) 0.0272(10) Uani 1 1 d .
H66A H 0.1748 -0.1309 0.2915 0.033 Uiso 1 1 calc R
H66B H 0.1385 -0.0906 0.2566 0.033 Uiso 1 1 calc R
C67 C 0.09544(12) -0.2167(2) 0.25083(17) 0.0204(9) Uani 1 1 d .
C68 C 0.11837(13) -0.2528(2) 0.24184(18) 0.0239(9) Uani 1 1 d .
C69 C 0.13615(14) -0.2840(2) 0.2328(2) 0.0272(10) Uani 1 1 d .
C70 C 0.15640(17) -0.3212(2) 0.2202(2) 0.0384(13) Uani 1 1 d .
H70 H 0.1774 -0.3451 0.2485 0.046 Uiso 1 1 calc R
C71 C 0.1356(3) -0.3516(5) 0.1692(3) 0.087(3) Uani 1 1 d .
H71A H 0.1433 -0.3936 0.1667 0.104 Uiso 1 1 calc R
H71B H 0.1091 -0.3438 0.1464 0.104 Uiso 1 1 calc R
C72 C 0.1601(4) -0.3005(4) 0.1795(5) 0.109(5) Uani 1 1 d .
H72A H 0.1489 -0.2603 0.1630 0.130 Uiso 1 1 calc R
H72B H 0.1831 -0.3101 0.1833 0.130 Uiso 1 1 calc R
C73 C 0.12691(12) -0.25699(19) 0.33648(17) 0.0208(9) Uani 1 1 d .
H73 H 0.1321 -0.2935 0.3226 0.025 Uiso 1 1 calc R
C74 C 0.11310(14) -0.2801(2) 0.36681(19) 0.0280(10) Uani 1 1 d .
H74A H 0.0912 -0.3060 0.3449 0.034 Uiso 1 1 calc R
H74B H 0.1057 -0.2442 0.3781 0.034 Uiso 1 1 calc R
C75 C 0.14176(14) -0.3179(2) 0.41312(19) 0.0288(10) Uani 1 1 d .
H75A H 0.1322 -0.3289 0.4332 0.035 Uiso 1 1 calc R
H75B H 0.1468 -0.3567 0.4020 0.035 Uiso 1 1 calc R
C76 C 0.17679(16) -0.2810(2) 0.44570(19) 0.0333(12) Uani 1 1 d .
H76A H 0.1956 -0.3072 0.4739 0.040 Uiso 1 1 calc R
H76B H 0.1723 -0.2450 0.4603 0.040 Uiso 1 1 calc R
C77 C 0.19073(14) -0.2585(2) 0.41483(19) 0.0298(10) Uani 1 1 d .
H77A H 0.2130 -0.2333 0.4366 0.036 Uiso 1 1 calc R
H77B H 0.1973 -0.2946 0.4028 0.036 Uiso 1 1 calc R
C78 C 0.16207(13) -0.2203(2) 0.36992(19) 0.0261(10) Uani 1 1 d .
H78A H 0.1714 -0.2076 0.3499 0.031 Uiso 1 1 calc R
H78B H 0.1570 -0.1824 0.3821 0.031 Uiso 1 1 calc R
C79 C 0.06264(14) -0.1748(2) 0.16593(17) 0.0248(9) Uani 1 1 d .
H79 H 0.0861 -0.1805 0.1693 0.030 Uiso 1 1 calc R
C80 C 0.04708(15) -0.1107(2) 0.14362(19) 0.0315(11) Uani 1 1 d .
H80A H 0.0253 -0.1032 0.1438 0.038 Uiso 1 1 calc R
H80B H 0.0655 -0.0788 0.1651 0.038 Uiso 1 1 calc R
C81 C 0.03651(18) -0.1044(3) 0.0900(2) 0.0422(14) Uani 1 1 d .
H81A H 0.0587 -0.1067 0.0903 0.051 Uiso 1 1 calc R
H81B H 0.0252 -0.0633 0.0765 0.051 Uiso 1 1 calc R
C82 C 0.00995(19) -0.1546(4) 0.0554(2) 0.0538(18) Uani 1 1 d .
H82A H 0.0052 -0.1507 0.0215 0.065 Uiso 1 1 calc R
H82B H -0.0135 -0.1493 0.0516 0.065 Uiso 1 1 calc R
C83 C 0.02565(19) -0.2191(3) 0.0772(2) 0.0457(15) Uani 1 1 d .
H83A H 0.0074 -0.2511 0.0555 0.055 Uiso 1 1 calc R
H83B H 0.0476 -0.2262 0.0775 0.055 Uiso 1 1 calc R
C84 C 0.03566(16) -0.2249(3) 0.1310(2) 0.0356(12) Uani 1 1 d .
H84A H 0.0132 -0.2216 0.1301 0.043 Uiso 1 1 calc R
H84B H 0.0465 -0.2661 0.1447 0.043 Uiso 1 1 calc R
C85 C -0.01562(13) -0.1372(2) 0.18374(18) 0.0279(10) Uani 1 1 d .
H85 H -0.0236 -0.1371 0.1494 0.034 Uiso 1 1 calc R
C86 C -0.01057(13) -0.0769(2) 0.20339(19) 0.0264(10) Uani 1 1 d .
H86 H -0.0155 -0.0459 0.1794 0.032 Uiso 1 1 calc R
C87 C 0.0000 -0.0518(3) 0.2500 0.0273(14) Uani 1 2 d S
H87 H 0.0000 -0.0079 0.2500 0.033 Uiso 1 2 calc SR
C88 C 0.01163(12) -0.1979(2) 0.29719(18) 0.0239(9) Uani 1 1 d .
H88 H 0.0184 -0.2287 0.3221 0.029 Uiso 1 1 calc R
C89 C 0.0000 -0.2238(3) 0.2500 0.0254(14) Uani 1 2 d S
H89 H 0.0000 -0.2678 0.2500 0.031 Uiso 1 2 calc SR
C101 C 0.2111(2) -0.0320(3) 0.6435(3) 0.0493(16) Uani 1 1 d .
C102 C 0.2205(2) -0.0833(3) 0.6740(3) 0.0513(16) Uani 1 1 d .
H102 H 0.2041 -0.1173 0.6621 0.062 Uiso 1 1 calc R
C103 C 0.2533(3) -0.0867(5) 0.7217(3) 0.076(3) Uani 1 1 d .
H103 H 0.2591 -0.1231 0.7414 0.091 Uiso 1 1 calc R
C104 C 0.2770(3) -0.0382(5) 0.7404(5) 0.091(3) Uani 1 1 d .
H104 H 0.2988 -0.0397 0.7735 0.110 Uiso 1 1 calc R
C105 C 0.2685(3) 0.0139(5) 0.7099(5) 0.085(3) Uani 1 1 d .
H105 H 0.2851 0.0476 0.7218 0.102 Uiso 1 1 calc R
C106 C 0.2357(3) 0.0165(4) 0.6618(4) 0.067(2) Uani 1 1 d .
H106 H 0.2302 0.0521 0.6414 0.081 Uiso 1 1 calc R
C107 C 0.1762(3) -0.0287(4) 0.5929(3) 0.074(3) Uani 1 1 d .
H10C H 0.1624 -0.0668 0.5865 0.112 Uiso 1 1 calc R
H10D H 0.1811 -0.0238 0.5672 0.112 Uiso 1 1 calc R
H10E H 0.1621 0.0068 0.5916 0.112 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Nd Nd -0.1943 3.0179 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Nd1 N1 56.05(12) . .
N2 Nd1 Cl2 112.87(10) . .
N1 Nd1 Cl2 86.89(10) . .
N2 Nd1 C22 159.91(18) . .
N1 Nd1 C22 140.46(18) . .
Cl2 Nd1 C22 83.13(12) . .
N2 Nd1 C19 89.26(16) . 2
N1 Nd1 C19 89.67(16) . 2
Cl2 Nd1 C19 150.11(16) . 2
C22 Nd1 C19 80.78(16) . 2
N2 Nd1 C21 159.25(18) . .
N1 Nd1 C21 111.99(18) . .
Cl2 Nd1 C21 80.92(11) . .
C22 Nd1 C21 28.6(2) . .
C19 Nd1 C21 72.91(18) 2 .
N2 Nd1 C21 105.04(17) . 2
N1 Nd1 C21 141.44(18) . 2
Cl2 Nd1 C21 130.90(16) . 2
C22 Nd1 C21 55.1(2) . 2
C19 Nd1 C21 54.3(2) 2 2
C21 Nd1 C21 73.4(2) . 2
N2 Nd1 C20 89.00(15) . 2
N1 Nd1 C20 112.75(19) . 2
Cl2 Nd1 C20 156.87(14) . 2
C22 Nd1 C20 73.94(18) . 2
C19 Nd1 C20 28.5(2) 2 2
C21 Nd1 C20 80.36(15) . 2
C21 Nd1 C20 28.7(2) 2 2
N2 Nd1 Cl1 84.97(9) . .
N1 Nd1 Cl1 126.44(10) . .
Cl2 Nd1 Cl1 75.44(3) . .
C22 Nd1 Cl1 87.68(14) . .
C19 Nd1 Cl1 128.55(16) 2 .
C21 Nd1 Cl1 114.32(16) . .
C21 Nd1 Cl1 78.11(13) 2 .
C20 Nd1 Cl1 100.22(17) 2 .
N2 Nd1 C1 28.21(13) . .
N1 Nd1 C1 28.00(13) . .
Cl2 Nd1 C1 98.94(10) . .
C22 Nd1 C1 166.98(17) . .
C19 Nd1 C1 91.58(15) 2 .
C21 Nd1 C1 138.75(18) . .
C21 Nd1 C1 127.80(18) 2 .
C20 Nd1 C1 104.09(17) 2 .
Cl1 Nd1 C1 105.31(10) . .
N2 Nd1 C20 130.7(2) . .
N1 Nd1 C20 89.08(16) . .
Cl2 Nd1 C20 96.65(16) . .
C22 Nd1 C20 54.5(2) . .
C19 Nd1 C20 53.6(2) 2 .
C21 Nd1 C20 28.7(2) . .
C21 Nd1 C20 80.20(16) 2 .
C20 Nd1 C20 72.6(2) 2 .
Cl1 Nd1 C20 142.19(16) . .
C1 Nd1 C20 112.47(18) . .
N2 Nd1 C22 130.65(18) . 2
N1 Nd1 C22 160.54(14) . 2
Cl2 Nd1 C22 103.37(15) . 2
C22 Nd1 C22 29.5(3) . 2
C19 Nd1 C22 73.14(18) 2 2
C21 Nd1 C22 54.8(2) . 2
C21 Nd1 C22 28.5(2) 2 2
C20 Nd1 C22 54.3(2) 2 2
Cl1 Nd1 C22 72.66(11) . 2
C1 Nd1 C22 156.11(18) . 2
C20 Nd1 C22 73.49(17) . 2
N4 Nd2 N3 56.19(12) . .
N4 Nd2 Cl1 108.01(9) . .
N3 Nd2 Cl1 83.05(10) . .
N4 Nd2 C42 150.40(18) . .
N3 Nd2 C42 146.97(17) . .
Cl1 Nd2 C42 95.83(13) . .
N4 Nd2 C23 28.33(13) . .
N3 Nd2 C23 28.03(13) . .
Cl1 Nd2 C23 94.02(9) . .
C42 Nd2 C23 167.70(14) . .
N4 Nd2 C46 88.39(15) . .
N3 Nd2 C46 82.25(15) . .
Cl1 Nd2 C46 146.29(16) . .
C42 Nd2 C46 80.76(15) . .
C23 Nd2 C46 86.95(13) . .
N4 Nd2 C48 97.22(16) . .
N3 Nd2 C48 131.07(18) . .
Cl1 Nd2 C48 145.63(15) . .
C42 Nd2 C48 54.3(2) . .
C23 Nd2 C48 118.20(17) . .
C46 Nd2 C48 54.3(2) . .
N4 Nd2 Cl2 85.51(9) . .
N3 Nd2 Cl2 127.29(9) . .
Cl1 Nd2 Cl2 75.72(4) . .
C42 Nd2 Cl2 83.60(14) . .
C23 Nd2 Cl2 106.02(9) . .
C46 Nd2 Cl2 136.23(16) . .
C48 Nd2 Cl2 83.60(13) . .
N4 Nd2 C47 84.29(14) . .
N3 Nd2 C47 103.02(17) . .
Cl1 Nd2 C47 167.56(11) . .
C42 Nd2 C47 73.11(17) . .
C23 Nd2 C47 96.29(15) . .
C46 Nd2 C47 28.3(2) . .
C48 Nd2 C47 28.6(2) . .
Cl2 Nd2 C47 107.90(15) . .
N4 Nd2 C43 162.05(16) . .
N3 Nd2 C43 118.26(19) . .
Cl1 Nd2 C43 87.01(11) . .
C42 Nd2 C43 29.2(2) . .
C23 Nd2 C43 144.84(19) . .
C46 Nd2 C43 73.72(17) . .
C48 Nd2 C43 73.64(17) . .
Cl2 Nd2 C43 108.25(17) . .
C47 Nd2 C43 80.55(15) . .
N4 Nd2 C44 136.58(19) . .
N3 Nd2 C44 92.61(16) . .
Cl1 Nd2 C44 95.50(13) . .
C42 Nd2 C44 54.5(2) . .
C23 Nd2 C44 117.16(18) . .
C46 Nd2 C44 55.2(2) . .
C48 Nd2 C44 80.85(14) . .
Cl2 Nd2 C44 136.49(16) . .
C47 Nd2 C44 73.58(17) . .
C43 Nd2 C44 28.3(2) . .
N4 Nd2 C45 108.74(18) . .
N3 Nd2 C45 78.22(14) . .
Cl1 Nd2 C45 117.96(16) . .
C42 Nd2 C45 73.23(18) . .
C23 Nd2 C45 95.62(16) . .
C46 Nd2 C45 28.9(2) . .
C48 Nd2 C45 73.09(17) . .
Cl2 Nd2 C45 153.81(11) . .
C47 Nd2 C45 54.1(2) . .
C43 Nd2 C45 54.2(2) . .
C44 Nd2 C45 29.0(2) . .
N6 Nd3 N5 55.96(12) . .
N6 Nd3 Cl4 110.35(9) . .
N5 Nd3 Cl4 83.19(9) . .
N6 Nd3 C47 90.47(15) . .
N5 Nd3 C47 86.84(15) . .
Cl4 Nd3 C47 145.66(15) . .
N6 Nd3 Cl3 83.48(9) . .
N5 Nd3 Cl3 124.63(9) . .
Cl4 Nd3 Cl3 77.36(3) . .
C47 Nd3 Cl3 133.72(15) . .
N6 Nd3 C45 136.91(19) . .
N5 Nd3 C45 93.78(16) . .
Cl4 Nd3 C45 93.21(14) . .
C47 Nd3 C45 54.7(2) . .
Cl3 Nd3 C45 138.14(16) . .
N6 Nd3 C48 86.78(14) . .
N5 Nd3 C48 108.12(17) . .
Cl4 Nd3 C48 162.85(11) . .
C47 Nd3 C48 28.8(2) . .
Cl3 Nd3 C48 104.93(15) . .
C45 Nd3 C48 73.61(17) . .
N6 Nd3 C41 100.19(15) . .
N5 Nd3 C41 136.70(17) . .
Cl4 Nd3 C41 139.74(15) . .
C47 Nd3 C41 55.11(19) . .
Cl3 Nd3 C41 80.84(12) . .
C45 Nd3 C41 81.03(15) . .
C48 Nd3 C41 29.15(19) . .
N6 Nd3 C46 109.47(17) . .
N5 Nd3 C46 81.22(14) . .
Cl4 Nd3 C46 117.26(16) . .
C47 Nd3 C46 28.4(2) . .
Cl3 Nd3 C46 153.00(11) . .
C45 Nd3 C46 29.0(2) . .
C48 Nd3 C46 54.3(2) . .
C41 Nd3 C46 73.70(16) . .
N6 Nd3 C49 28.03(13) . .
N5 Nd3 C49 28.18(12) . .
Cl4 Nd3 C49 95.09(9) . .
C47 Nd3 C49 91.26(14) . .
Cl3 Nd3 C49 103.02(10) . .
C45 Nd3 C49 118.52(18) . .
C48 Nd3 C49 100.82(15) . .
C41 Nd3 C49 122.77(16) . .
C46 Nd3 C49 98.28(15) . .
N6 Nd3 C42 124.64(18) . .
N5 Nd3 C42 159.56(14) . .
Cl4 Nd3 C42 112.38(15) . .
C47 Nd3 C42 72.83(17) . .
Cl3 Nd3 C42 73.45(11) . .
C45 Nd3 C42 72.92(17) . .
C48 Nd3 C42 53.82(19) . .
C41 Nd3 C42 27.92(19) . .
C46 Nd3 C42 79.81(15) . .
C49 Nd3 C42 150.18(18) . .
N6 Nd3 C44 163.72(15) . .
N5 Nd3 C44 119.03(18) . .
Cl4 Nd3 C44 82.93(10) . .
C47 Nd3 C44 73.45(17) . .
Cl3 Nd3 C44 109.32(16) . .
C45 Nd3 C44 28.9(2) . .
C48 Nd3 C44 80.30(14) . .
C41 Nd3 C44 72.94(16) . .
C46 Nd3 C44 54.7(2) . .
C49 Nd3 C44 146.22(19) . .
C42 Nd3 C44 53.6(2) . .
N7 Nd4 N8 55.57(13) . .
N7 Nd4 Cl3 108.71(10) . .
N8 Nd4 Cl3 84.46(10) . .
N7 Nd4 C86 150.81(14) . .
N8 Nd4 C86 100.51(14) . .
Cl3 Nd4 C86 82.31(10) . .
N7 Nd4 C85 122.69(14) . .
N8 Nd4 C85 82.07(14) . .
Cl3 Nd4 C85 102.64(11) . .
C86 Nd4 C85 29.03(15) . .
N7 Nd4 C88 98.16(13) . .
N8 Nd4 C88 124.28(14) . .
Cl3 Nd4 C88 149.12(10) . .
C86 Nd4 C88 81.41(13) . .
C85 Nd4 C88 73.81(14) . .
N7 Nd4 C67 27.80(13) . .
N8 Nd4 C67 27.92(13) . .
Cl3 Nd4 C67 95.43(9) . .
C86 Nd4 C67 127.46(14) . .
C85 Nd4 C67 104.58(14) . .
C88 Nd4 C67 115.29(13) . .
N7 Nd4 Cl4 86.48(10) . .
N8 Nd4 Cl4 129.28(10) . .
Cl3 Nd4 Cl4 77.05(3) . .
C86 Nd4 Cl4 122.65(11) . .
C85 Nd4 Cl4 147.82(10) . .
C88 Nd4 Cl4 90.02(10) . .
C67 Nd4 Cl4 107.50(10) . .
N7 Nd4 C87 172.03(13) . .
N8 Nd4 C87 127.96(9) . .
Cl3 Nd4 C87 79.19(9) . .
C86 Nd4 C87 28.73(11) . .
C85 Nd4 C87 54.71(12) . .
C88 Nd4 C87 73.93(13) . .
C67 Nd4 C87 155.72(9) . .
Cl4 Nd4 C87 94.46(6) . .
N7 Nd4 C88 100.93(13) . 2
N8 Nd4 C88 81.09(14) . 2
Cl3 Nd4 C88 130.87(10) . 2
C86 Nd4 C88 55.08(14) . 2
C85 Nd4 C88 28.97(14) . 2
C88 Nd4 C88 54.39(18) . 2
C67 Nd4 C88 93.10(13) . 2
Cl4 Nd4 C88 144.21(10) . 2
C87 Nd4 C88 73.77(12) . 2
N7 Nd4 C85 118.72(14) . 2
N8 Nd4 C85 152.10(14) . 2
Cl3 Nd4 C85 120.64(11) . 2
C86 Nd4 C85 73.52(14) . 2
C85 Nd4 C85 80.60(15) . 2
C88 Nd4 C85 28.87(14) . 2
C67 Nd4 C85 141.93(14) . 2
Cl4 Nd4 C85 72.62(10) . 2
C87 Nd4 C85 54.39(12) . 2
C88 Nd4 C85 73.18(14) 2 2
N7 Nd4 C89 91.11(13) . .
N8 Nd4 C89 97.45(11) . .
Cl3 Nd4 C89 156.64(8) . .
C86 Nd4 C89 74.44(13) . .
C85 Nd4 C89 54.98(12) . .
C88 Nd4 C89 28.76(10) . .
C67 Nd4 C89 96.92(12) . .
Cl4 Nd4 C89 117.52(3) . .
C87 Nd4 C89 81.42(13) . .
C88 Nd4 C89 28.70(10) 2 .
C85 Nd4 C89 54.66(12) 2 .
Nd2 Cl1 Nd1 104.02(4) . .
Nd1 Cl2 Nd2 103.38(4) . .
Nd4 Cl3 Nd3 103.01(3) . .
Nd3 Cl4 Nd4 101.96(3) . .
C1 N1 C7 120.0(4) . .
C1 N1 Nd1 93.2(3) . .
C7 N1 Nd1 146.1(3) . .
C1 N2 C13 120.1(4) . .
C1 N2 Nd1 93.9(3) . .
C13 N2 Nd1 144.9(3) . .
C23 N3 C29 120.0(4) . .
C23 N3 Nd2 92.4(3) . .
C29 N3 Nd2 146.5(3) . .
C23 N4 C35 120.3(4) . .
C23 N4 Nd2 94.4(3) . .
C35 N4 Nd2 143.5(3) . .
C49 N5 C55 119.8(4) . .
C49 N5 Nd3 92.5(3) . .
C55 N5 Nd3 147.3(3) . .
C49 N6 C61 120.1(4) . .
C49 N6 Nd3 94.1(3) . .
C61 N6 Nd3 144.1(3) . .
C67 N7 C73 120.5(4) . .
C67 N7 Nd4 95.0(3) . .
C73 N7 Nd4 143.0(3) . .
C67 N8 C79 119.9(4) . .
C67 N8 Nd4 93.8(3) . .
C79 N8 Nd4 146.1(3) . .
N1 C1 N2 116.2(4) . .
N1 C1 C2 122.4(4) . .
N2 C1 C2 121.4(4) . .
N1 C1 Nd1 58.8(2) . .
N2 C1 Nd1 57.9(2) . .
C2 C1 Nd1 172.2(3) . .
C3 C2 C1 174.4(5) . .
C2 C3 C4 175.7(5) . .
C3 C4 C5 120.7(5) . .
C3 C4 C6 117.5(5) . .
C5 C4 C6 57.3(5) . .
C6 C5 C4 63.8(5) . .
C5 C6 C4 58.9(4) . .
N1 C7 C8 109.1(3) . .
N1 C7 C12 111.1(4) . .
C8 C7 C12 109.8(4) . .
C7 C8 C9 112.2(4) . .
C10 C9 C8 111.2(5) . .
C9 C10 C11 110.6(4) . .
C10 C11 C12 111.1(4) . .
C7 C12 C11 111.0(4) . .
N2 C13 C14 108.2(4) . .
N2 C13 C18 112.0(4) . .
C14 C13 C18 111.2(4) . .
C13 C14 C15 111.5(4) . .
C16 C15 C14 111.2(4) . .
C15 C16 C17 111.7(5) . .
C18 C17 C16 111.3(4) . .
C17 C18 C13 111.1(4) . .
C19 C19 C20 135.7(4) 2 .
C19 C19 Nd1 77.0(4) 2 2
C20 C19 Nd1 76.1(3) . 2
C19 C19 Nd1 75.2(4) 2 .
C20 C19 Nd1 75.4(3) . .
Nd1 C19 Nd1 99.49(17) 2 .
C19 C20 C21 134.8(5) . .
C19 C20 Nd1 75.5(3) . 2
C21 C20 Nd1 75.6(3) . 2
C19 C20 Nd1 76.2(3) . .
C21 C20 Nd1 75.2(3) . .
Nd1 C20 Nd1 99.55(18) 2 .
C22 C21 C20 135.4(5) . .
C22 C21 Nd1 75.4(3) . .
C20 C21 Nd1 76.1(3) . .
C22 C21 Nd1 76.3(3) . 2
C20 C21 Nd1 75.7(3) . 2
Nd1 C21 Nd1 99.86(16) . 2
C21 C22 C22 134.1(3) . 2
C21 C22 Nd1 76.0(3) . .
C22 C22 Nd1 76.2(3) 2 .
C21 C22 Nd1 75.3(3) . 2
C22 C22 Nd1 74.3(4) 2 2
Nd1 C22 Nd1 99.74(16) . 2
N3 C23 N4 116.3(4) . .
N3 C23 C24 123.3(4) . .
N4 C23 C24 120.4(4) . .
N3 C23 Nd2 59.6(2) . .
N4 C23 Nd2 57.3(2) . .
C24 C23 Nd2 172.8(3) . .
C25 C24 C23 174.2(5) . .
C24 C25 C26 176.9(6) . .
C27 C26 C25 116.9(6) . .
C27 C26 C28 67.9(6) . .
C25 C26 C28 119.5(6) . .
C26 C27 C28 57.4(5) . .
C26 C28 C27 54.7(5) . .
N3 C29 C30 110.3(4) . .
N3 C29 C34 111.0(4) . .
C30 C29 C34 110.0(4) . .
C29 C30 C31 112.5(4) . .
C30 C31 C32 111.2(4) . .
C31 C32 C33 110.8(5) . .
C34 C33 C32 110.7(5) . .
C33 C34 C29 111.0(4) . .
N4 C35 C40 112.0(4) . .
N4 C35 C36 109.8(4) . .
C40 C35 C36 110.1(4) . .
C35 C36 C37 111.0(4) . .
C36 C37 C38 111.0(4) . .
C39 C38 C37 111.7(4) . .
C38 C39 C40 112.1(4) . .
C35 C40 C39 110.8(4) . .
C42 C41 C48 134.1(5) . .
C42 C41 Nd3 77.6(3) . .
C48 C41 Nd3 75.2(3) . .
C42 C41 Nd2 74.3(3) . .
C48 C41 Nd2 74.4(3) . .
Nd3 C41 Nd2 99.28(15) . .
C41 C42 C43 136.4(5) . .
C41 C42 Nd2 77.6(3) . .
C43 C42 Nd2 76.1(3) . .
C41 C42 Nd3 74.5(3) . .
C43 C42 Nd3 76.1(3) . .
Nd2 C42 Nd3 99.33(17) . .
C44 C43 C42 134.6(5) . .
C44 C43 Nd2 75.9(3) . .
C42 C43 Nd2 74.7(3) . .
C44 C43 Nd3 75.9(3) . .
C42 C43 Nd3 75.2(3) . .
Nd2 C43 Nd3 98.64(16) . .
C43 C44 C45 134.5(5) . .
C43 C44 Nd2 75.9(3) . .
C45 C44 Nd2 76.1(3) . .
C43 C44 Nd3 76.3(3) . .
C45 C44 Nd3 73.5(3) . .
Nd2 C44 Nd3 98.75(16) . .
C46 C45 C44 134.9(5) . .
C46 C45 Nd3 75.8(3) . .
C44 C45 Nd3 77.6(3) . .
C46 C45 Nd2 74.5(3) . .
C44 C45 Nd2 74.9(3) . .
Nd3 C45 Nd2 99.63(17) . .
C47 C46 C45 134.7(5) . .
C47 C46 Nd2 76.3(3) . .
C45 C46 Nd2 76.6(3) . .
C47 C46 Nd3 74.7(3) . .
C45 C46 Nd3 75.2(3) . .
Nd2 C46 Nd3 100.09(16) . .
C46 C47 C48 135.7(5) . .
C46 C47 Nd3 76.9(3) . .
C48 C47 Nd3 76.4(3) . .
C46 C47 Nd2 75.4(3) . .
C48 C47 Nd2 75.5(3) . .
Nd3 C47 Nd2 100.49(17) . .
C47 C48 C41 134.8(5) . .
C47 C48 Nd3 74.8(3) . .
C41 C48 Nd3 75.6(3) . .
C47 C48 Nd2 75.9(3) . .
C41 C48 Nd2 76.6(3) . .
Nd3 C48 Nd2 100.09(16) . .
N6 C49 N5 116.4(4) . .
N6 C49 C50 121.4(4) . .
N5 C49 C50 122.2(4) . .
N6 C49 Nd3 57.8(2) . .
N5 C49 Nd3 59.3(2) . .
C50 C49 Nd3 169.4(3) . .
C51 C50 C49 173.0(5) . .
C50 C51 C52 176.0(6) . .
C51 C52 C53 118.2(6) . .
C51 C52 C54 117.4(6) . .
C53 C52 C54 59.7(6) . .
C54 C53 C52 60.2(5) . .
C53 C54 C52 60.0(5) . .
N5 C55 C56 110.7(4) . .
N5 C55 C60 110.3(4) . .
C56 C55 C60 110.0(4) . .
C55 C56 C57 110.4(4) . .
C58 C57 C56 111.9(4) . .
C57 C58 C59 111.0(4) . .
C60 C59 C58 110.4(4) . .
C59 C60 C55 112.2(4) . .
N6 C61 C62 108.2(3) . .
N6 C61 C66 112.5(4) . .
C62 C61 C66 110.5(4) . .
C63 C62 C61 111.0(4) . .
C62 C63 C64 110.5(4) . .
C63 C64 C65 111.0(5) . .
C66 C65 C64 111.0(4) . .
C65 C66 C61 110.5(4) . .
N7 C67 N8 115.0(4) . .
N7 C67 C68 122.6(4) . .
N8 C67 C68 122.4(4) . .
N7 C67 Nd4 57.2(2) . .
N8 C67 Nd4 58.3(2) . .
C68 C67 Nd4 174.6(3) . .
C69 C68 C67 177.3(6) . .
C68 C69 C70 177.9(6) . .
C69 C70 C72 119.6(5) . .
C69 C70 C71 117.6(6) . .
C72 C70 C71 58.2(7) . .
C72 C71 C70 60.3(6) . .
C71 C72 C70 61.4(5) . .
N7 C73 C74 108.8(4) . .
N7 C73 C78 111.8(3) . .
C74 C73 C78 110.6(4) . .
C73 C74 C75 112.6(4) . .
C76 C75 C74 110.5(4) . .
C75 C76 C77 111.1(4) . .
C78 C77 C76 111.1(4) . .
C77 C78 C73 110.9(4) . .
N8 C79 C84 110.6(4) . .
N8 C79 C80 108.9(4) . .
C84 C79 C80 109.8(4) . .
C81 C80 C79 112.2(4) . .
C80 C81 C82 112.0(5) . .
C81 C82 C83 110.5(5) . .
C84 C83 C82 110.7(5) . .
C79 C84 C83 111.9(5) . .
C86 C85 C88 135.4(4) . 2
C86 C85 Nd4 75.3(3) . .
C88 C85 Nd4 76.7(3) 2 .
C86 C85 Nd4 76.2(3) . 2
C88 C85 Nd4 75.1(3) 2 2
Nd4 C85 Nd4 99.40(15) . 2
C87 C86 C85 135.1(5) . .
C87 C86 Nd4 76.8(2) . .
C85 C86 Nd4 75.7(3) . .
C87 C86 Nd4 75.0(2) . 2
C85 C86 Nd4 75.2(3) . 2
Nd4 C86 Nd4 99.21(14) . 2
C86 C87 C86 134.6(6) . 2
C86 C87 Nd4 74.4(3) . .
C86 C87 Nd4 76.5(3) 2 .
C86 C87 Nd4 76.5(3) . 2
C86 C87 Nd4 74.4(3) 2 2
Nd4 C87 Nd4 98.92(19) . 2
C89 C88 C85 135.4(5) . 2
C89 C88 Nd4 76.5(2) . .
C85 C88 Nd4 76.1(3) 2 .
C89 C88 Nd4 76.1(2) . 2
C85 C88 Nd4 74.4(3) 2 2
Nd4 C88 Nd4 99.01(14) . 2
C88 C89 C88 133.4(6) 2 .
C88 C89 Nd4 75.2(3) 2 .
C88 C89 Nd4 74.8(3) . .
C88 C89 Nd4 74.8(3) 2 2
C88 C89 Nd4 75.2(3) . 2
Nd4 C89 Nd4 98.24(19) . 2
C102 C101 C106 117.6(8) . .
C102 C101 C107 121.5(7) . .
C106 C101 C107 120.9(7) . .
C101 C102 C103 121.8(8) . .
C104 C103 C102 120.6(9) . .
C103 C104 C105 118.7(10) . .
C104 C105 C106 120.1(9) . .
C101 C106 C105 121.1(8) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Nd1 N2 2.403(4) .
Nd1 N1 2.424(4) .
Nd1 Cl2 2.7895(11) .
Nd1 C22 2.815(5) .
Nd1 C19 2.822(6) 2
Nd1 C21 2.822(5) .
Nd1 C21 2.827(5) 2
Nd1 C20 2.829(5) 2
Nd1 Cl1 2.8289(11) .
Nd1 C1 2.831(5) .
Nd1 C20 2.833(5) .
Nd1 C22 2.839(5) 2
Nd2 N4 2.380(4) .
Nd2 N3 2.434(4) .
Nd2 Cl1 2.7684(12) .
Nd2 C42 2.819(5) .
Nd2 C23 2.821(4) .
Nd2 C46 2.824(5) .
Nd2 C48 2.831(5) .
Nd2 Cl2 2.8324(11) .
Nd2 C47 2.835(5) .
Nd2 C43 2.836(5) .
Nd2 C44 2.836(5) .
Nd2 C45 2.851(5) .
Nd3 N6 2.404(3) .
Nd3 N5 2.439(4) .
Nd3 Cl4 2.7771(11) .
Nd3 C47 2.804(5) .
Nd3 Cl3 2.8081(16) .
Nd3 C45 2.823(5) .
Nd3 C48 2.824(5) .
Nd3 C41 2.829(5) .
Nd3 C46 2.831(5) .
Nd3 C49 2.833(4) .
Nd3 C42 2.867(5) .
Nd3 C44 2.875(5) .
Nd4 N7 2.395(3) .
Nd4 N8 2.418(4) .
Nd4 Cl3 2.7655(11) .
Nd4 C86 2.812(5) .
Nd4 C85 2.817(5) .
Nd4 C88 2.836(5) .
Nd4 C67 2.838(4) .
Nd4 Cl4 2.8377(15) .
Nd4 C87 2.843(4) .
Nd4 C88 2.847(5) 2
Nd4 C85 2.848(5) 2
Nd4 C89 2.858(4) .
N1 C1 1.331(6) .
N1 C7 1.466(6) .
N2 C1 1.341(6) .
N2 C13 1.474(6) .
N3 C23 1.327(6) .
N3 C29 1.458(5) .
N4 C23 1.343(6) .
N4 C35 1.452(5) .
N5 C49 1.339(6) .
N5 C55 1.455(6) .
N6 C49 1.335(6) .
N6 C61 1.476(5) .
N7 C67 1.328(6) .
N7 C73 1.476(5) .
N8 C67 1.331(6) .
N8 C79 1.468(5) .
C1 C2 1.448(6) .
C2 C3 1.214(7) .
C3 C4 1.421(7) .
C4 C5 1.476(7) .
C4 C6 1.547(9) .
C5 C6 1.450(11) .
C7 C8 1.524(7) .
C7 C12 1.530(6) .
C8 C9 1.526(6) .
C9 C10 1.519(8) .
C10 C11 1.522(8) .
C11 C12 1.536(7) .
C13 C14 1.516(7) .
C13 C18 1.531(7) .
C14 C15 1.534(7) .
C15 C16 1.521(8) .
C16 C17 1.530(8) .
C17 C18 1.522(7) .
C19 C19 1.363(16) 2
C19 C20 1.389(10) .
C19 Nd1 2.822(6) 2
C20 C21 1.404(10) .
C20 Nd1 2.829(5) 2
C21 C22 1.393(10) .
C21 Nd1 2.827(5) 2
C22 C22 1.439(15) 2
C22 Nd1 2.839(5) 2
C23 C24 1.450(6) .
C24 C25 1.189(7) .
C25 C26 1.447(7) .
C26 C27 1.437(10) .
C26 C28 1.482(9) .
C27 C28 1.631(12) .
C29 C30 1.515(7) .
C29 C34 1.536(6) .
C30 C31 1.518(6) .
C31 C32 1.531(8) .
C32 C33 1.544(9) .
C33 C34 1.531(6) .
C35 C40 1.517(6) .
C35 C36 1.529(7) .
C36 C37 1.531(6) .
C37 C38 1.534(7) .
C38 C39 1.517(8) .
C39 C40 1.525(7) .
C41 C42 1.375(9) .
C41 C48 1.423(9) .
C42 C43 1.423(10) .
C43 C44 1.385(10) .
C44 C45 1.423(10) .
C45 C46 1.416(10) .
C46 C47 1.385(10) .
C47 C48 1.400(10) .
C49 C50 1.456(6) .
C50 C51 1.195(7) .
C51 C52 1.447(7) .
C52 C53 1.489(9) .
C52 C54 1.492(10) .
C53 C54 1.485(12) .
C55 C56 1.523(6) .
C55 C60 1.525(6) .
C56 C57 1.531(7) .
C57 C58 1.528(8) .
C58 C59 1.538(8) .
C59 C60 1.519(7) .
C61 C62 1.528(7) .
C61 C66 1.534(6) .
C62 C63 1.524(6) .
C63 C64 1.526(8) .
C64 C65 1.537(8) .
C65 C66 1.520(6) .
C67 C68 1.446(6) .
C68 C69 1.201(7) .
C69 C70 1.436(7) .
C70 C72 1.485(9) .
C70 C71 1.501(11) .
C71 C72 1.453(15) .
C73 C74 1.513(6) .
C73 C78 1.525(7) .
C74 C75 1.533(7) .
C75 C76 1.520(8) .
C76 C77 1.529(7) .
C77 C78 1.517(6) .
C79 C84 1.530(7) .
C79 C80 1.533(7) .
C80 C81 1.519(7) .
C81 C82 1.522(10) .
C82 C83 1.539(10) .
C83 C84 1.531(7) .
C85 C86 1.411(7) .
C85 C88 1.417(7) 2
C85 Nd4 2.848(5) 2
C86 C87 1.403(6) .
C86 Nd4 2.862(4) 2
C87 C86 1.403(6) 2
C87 Nd4 2.843(4) 2
C88 C89 1.414(5) .
C88 C85 1.417(7) 2
C88 Nd4 2.847(5) 2
C89 C88 1.414(5) 2
C89 Nd4 2.858(4) 2
C101 C102 1.381(9) .
C101 C106 1.381(11) .
C101 C107 1.479(11) .
C102 C103 1.393(12) .
C103 C104 1.363(14) .
C104 C105 1.399(15) .
C105 C106 1.400(14) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N4 Nd2 Cl1 Nd1 71.17(10) . .
N3 Nd2 Cl1 Nd1 122.19(9) . .
C42 Nd2 Cl1 Nd1 -91.04(15) . .
C23 Nd2 Cl1 Nd1 96.35(10) . .
C46 Nd2 Cl1 Nd1 -173.12(18) . .
C48 Nd2 Cl1 Nd1 -64.01(18) . .
Cl2 Nd2 Cl1 Nd1 -9.17(3) . .
C47 Nd2 Cl1 Nd1 -117.7(7) . .
C43 Nd2 Cl1 Nd1 -118.86(17) . .
C44 Nd2 Cl1 Nd1 -145.84(15) . .
C45 Nd2 Cl1 Nd1 -165.12(14) . .
N2 Nd1 Cl1 Nd2 -105.88(10) . .
N1 Nd1 Cl1 Nd2 -65.51(12) . .
Cl2 Nd1 Cl1 Nd2 9.33(3) . .
C22 Nd1 Cl1 Nd2 92.83(14) . .
C19 Nd1 Cl1 Nd2 169.10(15) 2 .
C21 Nd1 Cl1 Nd2 82.09(12) . .
C21 Nd1 Cl1 Nd2 147.57(15) 2 .
C20 Nd1 Cl1 Nd2 166.05(12) 2 .
C1 Nd1 Cl1 Nd2 -86.15(10) . .
C20 Nd1 Cl1 Nd2 91.3(2) . .
C22 Nd1 Cl1 Nd2 118.68(17) 2 .
N2 Nd1 Cl2 Nd2 68.91(10) . .
N1 Nd1 Cl2 Nd2 119.87(9) . .
C22 Nd1 Cl2 Nd2 -98.47(16) . .
C19 Nd1 Cl2 Nd2 -156.2(3) 2 .
C21 Nd1 Cl2 Nd2 -127.28(16) . .
C21 Nd1 Cl2 Nd2 -68.65(14) 2 .
C20 Nd1 Cl2 Nd2 -91.0(4) 2 .
Cl1 Nd1 Cl2 Nd2 -9.09(3) . .
C1 Nd1 Cl2 Nd2 94.51(10) . .
C20 Nd1 Cl2 Nd2 -151.42(14) . .
C22 Nd1 Cl2 Nd2 -76.87(12) 2 .
N4 Nd2 Cl2 Nd1 -100.59(9) . .
N3 Nd2 Cl2 Nd1 -60.18(12) . .
Cl1 Nd2 Cl2 Nd1 9.28(3) . .
C42 Nd2 Cl2 Nd1 106.98(14) . .
C23 Nd2 Cl2 Nd1 -80.84(10) . .
C46 Nd2 Cl2 Nd1 176.46(16) . .
C48 Nd2 Cl2 Nd1 161.61(14) . .
C47 Nd2 Cl2 Nd1 176.89(11) . .
C43 Nd2 Cl2 Nd1 91.20(12) . .
C44 Nd2 Cl2 Nd1 92.13(17) . .
C45 Nd2 Cl2 Nd1 134.6(4) . .
N7 Nd4 Cl3 Nd3 -75.69(11) . .
N8 Nd4 Cl3 Nd3 -126.45(10) . .
C86 Nd4 Cl3 Nd3 132.14(11) . .
C85 Nd4 Cl3 Nd3 152.98(10) . .
C88 Nd4 Cl3 Nd3 73.44(19) . .
C67 Nd4 Cl3 Nd3 -100.74(10) . .
Cl4 Nd4 Cl3 Nd3 6.01(3) . .
C87 Nd4 Cl3 Nd3 103.19(5) . .
C88 Nd4 Cl3 Nd3 160.40(12) 2 .
C85 Nd4 Cl3 Nd3 66.51(12) 2 .
C89 Nd4 Cl3 Nd3 137.58(14) . .
N6 Nd3 Cl3 Nd4 106.48(9) . .
N5 Nd3 Cl3 Nd4 66.26(11) . .
Cl4 Nd3 Cl3 Nd4 -6.13(3) . .
C47 Nd3 Cl3 Nd4 -169.15(16) . .
C45 Nd3 Cl3 Nd4 -86.68(18) . .
C48 Nd3 Cl3 Nd4 -168.63(11) . .
C41 Nd3 Cl3 Nd4 -152.06(13) . .
C46 Nd3 Cl3 Nd4 -132.5(4) . .
C49 Nd3 Cl3 Nd4 86.24(9) . .
C42 Nd3 Cl3 Nd4 -124.41(17) . .
C44 Nd3 Cl3 Nd4 -83.87(11) . .
N6 Nd3 Cl4 Nd4 -72.08(10) . .
N5 Nd3 Cl4 Nd4 -121.88(9) . .
C47 Nd3 Cl4 Nd4 164.0(2) . .
Cl3 Nd3 Cl4 Nd4 5.95(3) . .
C45 Nd3 Cl4 Nd4 144.70(15) . .
C48 Nd3 Cl4 Nd4 105.7(5) . .
C41 Nd3 Cl4 Nd4 64.80(16) . .
C46 Nd3 Cl4 Nd4 161.68(12) . .
C49 Nd3 Cl4 Nd4 -96.28(10) . .
C42 Nd3 Cl4 Nd4 71.86(13) . .
C44 Nd3 Cl4 Nd4 117.64(17) . .
N7 Nd4 Cl4 Nd3 104.07(9) . .
N8 Nd4 Cl4 Nd3 65.53(12) . .
Cl3 Nd4 Cl4 Nd3 -6.05(3) . .
C86 Nd4 Cl4 Nd3 -77.96(11) . .
C85 Nd4 Cl4 Nd3 -99.3(2) . .
C88 Nd4 Cl4 Nd3 -157.76(10) . .
C67 Nd4 Cl4 Nd3 85.63(10) . .
C87 Nd4 Cl4 Nd3 -83.87(9) . .
C88 Nd4 Cl4 Nd3 -152.07(16) 2 .
C85 Nd4 Cl4 Nd3 -134.35(12) 2 .
C89 Nd4 Cl4 Nd3 -166.51(11) . .
N2 Nd1 N1 C1 4.7(2) . .
Cl2 Nd1 N1 C1 -115.7(3) . .
C22 Nd1 N1 C1 169.0(3) . .
C19 Nd1 N1 C1 94.0(3) 2 .
C21 Nd1 N1 C1 165.4(3) . .
C21 Nd1 N1 C1 74.6(3) 2 .
C20 Nd1 N1 C1 76.9(3) 2 .
Cl1 Nd1 N1 C1 -46.4(3) . .
C20 Nd1 N1 C1 147.6(3) . .
C22 Nd1 N1 C1 121.5(6) 2 .
N2 Nd1 N1 C7 173.7(6) . .
Cl2 Nd1 N1 C7 53.3(5) . .
C22 Nd1 N1 C7 -21.9(6) . .
C19 Nd1 N1 C7 -97.0(5) 2 .
C21 Nd1 N1 C7 -25.6(6) . .
C21 Nd1 N1 C7 -116.3(5) 2 .
C20 Nd1 N1 C7 -114.0(5) 2 .
Cl1 Nd1 N1 C7 122.7(5) . .
C1 Nd1 N1 C7 169.0(7) . .
C20 Nd1 N1 C7 -43.4(6) . .
C22 Nd1 N1 C7 -69.4(8) 2 .
N1 Nd1 N2 C1 -4.6(2) . .
Cl2 Nd1 N2 C1 64.6(3) . .
C22 Nd1 N2 C1 -154.6(4) . .
C19 Nd1 N2 C1 -94.7(3) 2 .
C21 Nd1 N2 C1 -64.4(5) . .
C21 Nd1 N2 C1 -147.3(3) 2 .
C20 Nd1 N2 C1 -123.2(3) 2 .
Cl1 Nd1 N2 C1 136.4(3) . .
C20 Nd1 N2 C1 -57.4(3) . .
C22 Nd1 N2 C1 -161.6(3) 2 .
N1 Nd1 N2 C13 -171.0(6) . .
Cl2 Nd1 N2 C13 -101.8(5) . .
C22 Nd1 N2 C13 39.1(8) . .
C19 Nd1 N2 C13 98.9(5) 2 .
C21 Nd1 N2 C13 129.2(5) . .
C21 Nd1 N2 C13 46.4(6) 2 .
C20 Nd1 N2 C13 70.5(5) 2 .
Cl1 Nd1 N2 C13 -29.9(5) . .
C1 Nd1 N2 C13 -166.3(7) . .
C20 Nd1 N2 C13 136.3(5) . .
C22 Nd1 N2 C13 32.1(6) 2 .
N4 Nd2 N3 C23 4.9(2) . .
Cl1 Nd2 N3 C23 -112.3(2) . .
C42 Nd2 N3 C23 157.7(3) . .
C46 Nd2 N3 C23 98.1(3) . .
C48 Nd2 N3 C23 72.4(3) . .
Cl2 Nd2 N3 C23 -46.2(3) . .
C47 Nd2 N3 C23 78.8(3) . .
C43 Nd2 N3 C23 164.9(2) . .
C44 Nd2 N3 C23 152.5(3) . .
C45 Nd2 N3 C23 127.2(3) . .
N4 Nd2 N3 C29 171.2(6) . .
Cl1 Nd2 N3 C29 54.0(5) . .
C42 Nd2 N3 C29 -36.0(7) . .
C23 Nd2 N3 C29 166.3(7) . .
C46 Nd2 N3 C29 -95.6(5) . .
C48 Nd2 N3 C29 -121.3(5) . .
Cl2 Nd2 N3 C29 120.1(5) . .
C47 Nd2 N3 C29 -114.9(5) . .
C43 Nd2 N3 C29 -28.8(6) . .
C44 Nd2 N3 C29 -41.2(5) . .
C45 Nd2 N3 C29 -66.5(5) . .
N3 Nd2 N4 C23 -4.8(2) . .
Cl1 Nd2 N4 C23 63.4(3) . .
C42 Nd2 N4 C23 -154.6(3) . .
C46 Nd2 N4 C23 -86.6(3) . .
C48 Nd2 N4 C23 -140.2(3) . .
Cl2 Nd2 N4 C23 136.8(2) . .
C47 Nd2 N4 C23 -114.7(3) . .
C43 Nd2 N4 C23 -82.2(6) . .
C44 Nd2 N4 C23 -55.9(3) . .
C45 Nd2 N4 C23 -65.7(3) . .
N3 Nd2 N4 C35 -167.5(5) . .
Cl1 Nd2 N4 C35 -99.3(5) . .
C42 Nd2 N4 C35 42.7(6) . .
C23 Nd2 N4 C35 -162.7(6) . .
C46 Nd2 N4 C35 110.7(5) . .
C48 Nd2 N4 C35 57.1(5) . .
Cl2 Nd2 N4 C35 -25.9(5) . .
C47 Nd2 N4 C35 82.7(5) . .
C43 Nd2 N4 C35 115.1(7) . .
C44 Nd2 N4 C35 141.4(5) . .
C45 Nd2 N4 C35 131.6(5) . .
N6 Nd3 N5 C49 -5.9(2) . .
Cl4 Nd3 N5 C49 114.3(2) . .
C47 Nd3 N5 C49 -98.6(3) . .
Cl3 Nd3 N5 C49 44.8(3) . .
C45 Nd3 N5 C49 -152.9(3) . .
C48 Nd3 N5 C49 -78.9(3) . .
C41 Nd3 N5 C49 -72.0(3) . .
C46 Nd3 N5 C49 -126.7(3) . .
C42 Nd3 N5 C49 -104.6(5) . .
C44 Nd3 N5 C49 -167.7(2) . .
N6 Nd3 N5 C55 -177.5(6) . .
Cl4 Nd3 N5 C55 -57.2(5) . .
C47 Nd3 N5 C55 89.8(5) . .
Cl3 Nd3 N5 C55 -126.7(5) . .
C45 Nd3 N5 C55 35.6(5) . .
C48 Nd3 N5 C55 109.5(5) . .
C41 Nd3 N5 C55 116.5(5) . .
C46 Nd3 N5 C55 61.8(5) . .
C49 Nd3 N5 C55 -171.6(7) . .
C42 Nd3 N5 C55 83.8(7) . .
C44 Nd3 N5 C55 20.8(6) . .
N5 Nd3 N6 C49 5.9(2) . .
Cl4 Nd3 N6 C49 -60.3(3) . .
C47 Nd3 N6 C49 91.8(3) . .
Cl3 Nd3 N6 C49 -134.2(2) . .
C45 Nd3 N6 C49 58.6(3) . .
C48 Nd3 N6 C49 120.4(3) . .
C41 Nd3 N6 C49 146.4(3) . .
C46 Nd3 N6 C49 70.2(3) . .
C42 Nd3 N6 C49 161.1(2) . .
C44 Nd3 N6 C49 83.0(6) . .
N5 Nd3 N6 C61 169.1(5) . .
Cl4 Nd3 N6 C61 102.9(5) . .
C47 Nd3 N6 C61 -105.0(5) . .
Cl3 Nd3 N6 C61 29.0(5) . .
C45 Nd3 N6 C61 -138.2(4) . .
C48 Nd3 N6 C61 -76.4(5) . .
C41 Nd3 N6 C61 -50.5(5) . .
C46 Nd3 N6 C61 -126.6(5) . .
C49 Nd3 N6 C61 163.2(6) . .
C42 Nd3 N6 C61 -35.7(5) . .
C44 Nd3 N6 C61 -113.8(7) . .
N8 Nd4 N7 C67 4.5(3) . .
Cl3 Nd4 N7 C67 -64.6(3) . .
C86 Nd4 N7 C67 43.8(4) . .
C85 Nd4 N7 C67 54.8(3) . .
C88 Nd4 N7 C67 130.8(3) . .
Cl4 Nd4 N7 C67 -139.7(3) . .
C87 Nd4 N7 C67 123.3(7) . .
C88 Nd4 N7 C67 75.6(3) 2 .
C85 Nd4 N7 C67 152.3(3) 2 .
C89 Nd4 N7 C67 102.8(3) . .
N8 Nd4 N7 C73 168.6(5) . .
Cl3 Nd4 N7 C73 99.4(5) . .
C86 Nd4 N7 C73 -152.1(4) . .
C85 Nd4 N7 C73 -141.1(5) . .
C88 Nd4 N7 C73 -65.1(5) . .
C67 Nd4 N7 C73 164.1(6) . .
Cl4 Nd4 N7 C73 24.4(5) . .
C87 Nd4 N7 C73 -72.6(10) . .
C88 Nd4 N7 C73 -120.3(5) 2 .
C85 Nd4 N7 C73 -43.6(5) 2 .
C89 Nd4 N7 C73 -93.1(5) . .
N7 Nd4 N8 C67 -4.5(2) . .
Cl3 Nd4 N8 C67 112.7(3) . .
C86 Nd4 N8 C67 -166.2(3) . .
C85 Nd4 N8 C67 -143.7(3) . .
C88 Nd4 N8 C67 -79.5(3) . .
Cl4 Nd4 N8 C67 44.4(3) . .
C87 Nd4 N8 C67 -175.6(2) . .
C88 Nd4 N8 C67 -114.4(3) 2 .
C85 Nd4 N8 C67 -91.6(4) 2 .
C89 Nd4 N8 C67 -90.7(3) . .
N7 Nd4 N8 C79 -179.1(6) . .
Cl3 Nd4 N8 C79 -61.9(6) . .
C86 Nd4 N8 C79 19.2(6) . .
C85 Nd4 N8 C79 41.7(6) . .
C88 Nd4 N8 C79 105.9(6) . .
C67 Nd4 N8 C79 -174.6(7) . .
Cl4 Nd4 N8 C79 -130.2(5) . .
C87 Nd4 N8 C79 9.8(6) . .
C88 Nd4 N8 C79 71.0(6) 2 .
C85 Nd4 N8 C79 93.7(6) 2 .
C89 Nd4 N8 C79 94.7(6) . .
C7 N1 C1 N2 179.3(4) . .
Nd1 N1 C1 N2 -7.8(4) . .
C7 N1 C1 C2 -2.0(6) . .
Nd1 N1 C1 C2 170.9(4) . .
C7 N1 C1 Nd1 -173.0(4) . .
C13 N2 C1 N1 178.8(4) . .
Nd1 N2 C1 N1 7.8(4) . .
C13 N2 C1 C2 0.1(6) . .
Nd1 N2 C1 C2 -170.9(4) . .
C13 N2 C1 Nd1 171.0(5) . .
N2 Nd1 C1 N1 -171.8(4) . .
Cl2 Nd1 C1 N1 65.6(3) . .
C22 Nd1 C1 N1 -32.6(8) . .
C19 Nd1 C1 N1 -86.3(3) 2 .
C21 Nd1 C1 N1 -20.8(4) . .
C21 Nd1 C1 N1 -130.5(3) 2 .
C20 Nd1 C1 N1 -112.2(3) 2 .
Cl1 Nd1 C1 N1 142.9(2) . .
C20 Nd1 C1 N1 -35.4(3) . .
C22 Nd1 C1 N1 -135.5(4) 2 .
N1 Nd1 C1 N2 171.8(4) . .
Cl2 Nd1 C1 N2 -122.6(3) . .
C22 Nd1 C1 N2 139.2(7) . .
C19 Nd1 C1 N2 85.5(3) 2 .
C21 Nd1 C1 N2 151.0(3) . .
C21 Nd1 C1 N2 41.3(3) 2 .
C20 Nd1 C1 N2 59.6(3) 2 .
Cl1 Nd1 C1 N2 -45.4(3) . .
C20 Nd1 C1 N2 136.3(3) . .
C22 Nd1 C1 N2 36.3(5) 2 .
N2 Nd1 C1 C2 87(2) . .
N1 Nd1 C1 C2 -101(3) . .
Cl2 Nd1 C1 C2 -36(3) . .
C22 Nd1 C1 C2 -134(2) . .
C19 Nd1 C1 C2 172(2) 2 .
C21 Nd1 C1 C2 -122(2) . .
C21 Nd1 C1 C2 128(2) 2 .
C20 Nd1 C1 C2 147(2) 2 .
Cl1 Nd1 C1 C2 42(3) . .
C20 Nd1 C1 C2 -137(2) . .
C22 Nd1 C1 C2 123(2) 2 .
N1 C1 C2 C3 -170(5) . .
N2 C1 C2 C3 9(6) . .
Nd1 C1 C2 C3 -74(6) . .
C1 C2 C3 C4 -15(11) . .
C2 C3 C4 C5 29(8) . .
C2 C3 C4 C6 -37(8) . .
C3 C4 C5 C6 -104.9(7) . .
C3 C4 C6 C5 110.4(6) . .
C1 N1 C7 C8 151.3(4) . .
Nd1 N1 C7 C8 -16.1(7) . .
C1 N1 C7 C12 -87.5(5) . .
Nd1 N1 C7 C12 105.1(5) . .
N1 C7 C8 C9 177.6(4) . .
C12 C7 C8 C9 55.6(6) . .
C7 C8 C9 C10 -56.0(6) . .
C8 C9 C10 C11 55.6(6) . .
C9 C10 C11 C12 -56.4(6) . .
N1 C7 C12 C11 -176.6(4) . .
C8 C7 C12 C11 -55.9(5) . .
C10 C11 C12 C7 57.1(6) . .
C1 N2 C13 C14 152.2(4) . .
Nd1 N2 C13 C14 -43.6(7) . .
C1 N2 C13 C18 -84.9(5) . .
Nd1 N2 C13 C18 79.3(6) . .
N2 C13 C14 C15 179.0(4) . .
C18 C13 C14 C15 55.5(5) . .
C13 C14 C15 C16 -54.8(6) . .
C14 C15 C16 C17 54.3(6) . .
C15 C16 C17 C18 -54.9(6) . .
C16 C17 C18 C13 55.3(6) . .
N2 C13 C18 C17 -177.2(4) . .
C14 C13 C18 C17 -55.9(5) . .
N2 Nd1 C19 C19 -56.8(3) . 2
N1 Nd1 C19 C19 -107.6(3) . 2
Cl2 Nd1 C19 C19 172.3(3) . 2
C22 Nd1 C19 C19 102.3(3) . 2
C21 Nd1 C19 C19 126.4(4) . 2
C21 Nd1 C19 C19 44.5(3) 2 2
C20 Nd1 C19 C19 20.1(3) 2 2
Cl1 Nd1 C19 C19 50.6(4) . 2
C1 Nd1 C19 C19 -83.6(3) . 2
C20 Nd1 C19 C19 146.5(5) . 2
C22 Nd1 C19 C19 72.8(3) 2 2
N2 Nd1 C19 C20 156.7(3) . .
N1 Nd1 C19 C20 105.9(3) . .
Cl2 Nd1 C19 C20 25.8(4) . .
C22 Nd1 C19 C20 -44.2(3) . .
C19 Nd1 C19 C20 -146.5(5) 2 .
C21 Nd1 C19 C20 -20.1(3) . .
C21 Nd1 C19 C20 -102.0(4) 2 .
C20 Nd1 C19 C20 -126.4(4) 2 .
Cl1 Nd1 C19 C20 -95.9(5) . .
C1 Nd1 C19 C20 129.9(3) . .
C22 Nd1 C19 C20 -73.7(4) 2 .
N2 Nd1 C19 Nd1 -130.52(19) . 2
N1 Nd1 C19 Nd1 178.7(2) . 2
Cl2 Nd1 C19 Nd1 98.61(19) . 2
C22 Nd1 C19 Nd1 28.6(2) . 2
C19 Nd1 C19 Nd1 -73.7(3) 2 2
C21 Nd1 C19 Nd1 52.7(2) . 2
C21 Nd1 C19 Nd1 -29.2(2) 2 2
C20 Nd1 C19 Nd1 -53.6(2) 2 2
Cl1 Nd1 C19 Nd1 -23.1(5) . 2
C1 Nd1 C19 Nd1 -157.3(2) . 2
C20 Nd1 C19 Nd1 72.8(3) . 2
C22 Nd1 C19 Nd1 -0.9(2) 2 2
C19 C19 C20 C21 2.3(14) 2 .
Nd1 C19 C20 C21 -51.7(7) 2 .
Nd1 C19 C20 C21 52.2(6) . .
C19 C19 C20 Nd1 54.0(9) 2 2
Nd1 C19 C20 Nd1 103.88(14) . 2
C19 C19 C20 Nd1 -49.9(9) 2 .
Nd1 C19 C20 Nd1 -103.88(14) 2 .
N2 Nd1 C20 C19 -30.3(4) . .
N1 Nd1 C20 C19 -71.6(3) . .
Cl2 Nd1 C20 C19 -158.3(3) . .
C22 Nd1 C20 C19 125.0(4) . .
C19 Nd1 C20 C19 18.7(3) 2 .
C21 Nd1 C20 C19 144.5(5) . .
C21 Nd1 C20 C19 71.2(4) 2 .
C20 Nd1 C20 C19 42.6(4) 2 .
Cl1 Nd1 C20 C19 126.9(4) . .
C1 Nd1 C20 C19 -55.8(4) . .
C22 Nd1 C20 C19 99.6(4) 2 .
N2 Nd1 C20 C21 -174.8(3) . .
N1 Nd1 C20 C21 143.9(3) . .
Cl2 Nd1 C20 C21 57.1(3) . .
C22 Nd1 C20 C21 -19.5(3) . .
C19 Nd1 C20 C21 -125.9(4) 2 .
C21 Nd1 C20 C21 -73.3(4) 2 .
C20 Nd1 C20 C21 -101.9(4) 2 .
Cl1 Nd1 C20 C21 -17.7(5) . .
C1 Nd1 C20 C21 159.7(3) . .
C22 Nd1 C20 C21 -44.9(3) 2 .
N2 Nd1 C20 Nd1 -102.6(2) . 2
N1 Nd1 C20 Nd1 -143.9(2) . 2
Cl2 Nd1 C20 Nd1 129.3(2) . 2
C22 Nd1 C20 Nd1 52.6(2) . 2
C19 Nd1 C20 Nd1 -53.7(2) 2 2
C21 Nd1 C20 Nd1 72.2(3) . 2
C21 Nd1 C20 Nd1 -1.2(3) 2 2
C20 Nd1 C20 Nd1 -29.7(3) 2 2
Cl1 Nd1 C20 Nd1 54.5(4) . 2
C1 Nd1 C20 Nd1 -128.14(19) . 2
C22 Nd1 C20 Nd1 27.3(2) 2 2
C19 C20 C21 C22 -0.9(11) . .
Nd1 C20 C21 C22 -52.6(6) 2 .
Nd1 C20 C21 C22 51.6(6) . .
C19 C20 C21 Nd1 -52.5(7) . .
Nd1 C20 C21 Nd1 -104.20(14) 2 .
C19 C20 C21 Nd1 51.7(7) . 2
Nd1 C20 C21 Nd1 104.20(14) . 2
N2 Nd1 C21 C22 -134.2(5) . .
N1 Nd1 C21 C22 175.2(3) . .
Cl2 Nd1 C21 C22 92.3(3) . .
C19 Nd1 C21 C22 -102.3(4) 2 .
C21 Nd1 C21 C22 -45.4(4) 2 .
C20 Nd1 C21 C22 -74.1(4) 2 .
Cl1 Nd1 C21 C22 22.9(3) . .
C1 Nd1 C21 C22 -174.5(3) . .
C20 Nd1 C21 C22 -145.3(5) . .
C22 Nd1 C21 C22 -21.2(3) 2 .
N2 Nd1 C21 C20 11.2(6) . .
N1 Nd1 C21 C20 -39.5(4) . .
Cl2 Nd1 C21 C20 -122.4(3) . .
C22 Nd1 C21 C20 145.3(5) . .
C19 Nd1 C21 C20 43.0(4) 2 .
C21 Nd1 C21 C20 100.0(4) 2 .
C20 Nd1 C21 C20 71.3(4) 2 .
Cl1 Nd1 C21 C20 168.2(3) . .
C1 Nd1 C21 C20 -29.1(4) . .
C22 Nd1 C21 C20 124.1(4) 2 .
N2 Nd1 C21 Nd1 -61.3(5) . 2
N1 Nd1 C21 Nd1 -111.9(2) . 2
Cl2 Nd1 C21 Nd1 165.2(2) . 2
C22 Nd1 C21 Nd1 72.9(3) . 2
C19 Nd1 C21 Nd1 -29.4(2) 2 2
C21 Nd1 C21 Nd1 27.5(3) 2 2
C20 Nd1 C21 Nd1 -1.2(3) 2 2
Cl1 Nd1 C21 Nd1 95.77(19) . 2
C1 Nd1 C21 Nd1 -101.6(2) . 2
C20 Nd1 C21 Nd1 -72.5(3) . 2
C22 Nd1 C21 Nd1 51.7(2) 2 2
C20 C21 C22 C22 2.5(13) . 2
Nd1 C21 C22 C22 54.3(8) . 2
Nd1 C21 C22 C22 -49.9(8) 2 2
C20 C21 C22 Nd1 -51.8(6) . .
Nd1 C21 C22 Nd1 -104.23(13) 2 .
C20 C21 C22 Nd1 52.4(6) . 2
Nd1 C21 C22 Nd1 104.23(13) . 2
N2 Nd1 C22 C21 132.3(5) . .
N1 Nd1 C22 C21 -7.0(4) . .
Cl2 Nd1 C22 C21 -83.6(3) . .
C19 Nd1 C22 C21 71.1(4) 2 .
C21 Nd1 C22 C21 123.7(4) 2 .
C20 Nd1 C22 C21 99.4(4) 2 .
Cl1 Nd1 C22 C21 -159.2(3) . .
C1 Nd1 C22 C21 16.4(9) . .
C20 Nd1 C22 C21 19.6(3) . .
C22 Nd1 C22 C21 143.1(5) 2 .
N2 Nd1 C22 C22 -10.8(5) . 2
N1 Nd1 C22 C22 -150.1(2) . 2
Cl2 Nd1 C22 C22 133.3(3) . 2
C19 Nd1 C22 C22 -72.0(3) 2 2
C21 Nd1 C22 C22 -143.1(5) . 2
C21 Nd1 C22 C22 -19.4(3) 2 2
C20 Nd1 C22 C22 -43.6(3) 2 2
Cl1 Nd1 C22 C22 57.7(2) . 2
C1 Nd1 C22 C22 -126.7(6) . 2
C20 Nd1 C22 C22 -123.4(4) . 2
N2 Nd1 C22 Nd1 60.2(5) . 2
N1 Nd1 C22 Nd1 -79.0(3) . 2
Cl2 Nd1 C22 Nd1 -155.6(2) . 2
C19 Nd1 C22 Nd1 -0.9(2) 2 2
C21 Nd1 C22 Nd1 -72.0(3) . 2
C21 Nd1 C22 Nd1 51.7(2) 2 2
C20 Nd1 C22 Nd1 27.4(2) 2 2
Cl1 Nd1 C22 Nd1 128.75(19) . 2
C1 Nd1 C22 Nd1 -55.6(8) . 2
C20 Nd1 C22 Nd1 -52.4(2) . 2
C22 Nd1 C22 Nd1 71.0(3) 2 2
C29 N3 C23 N4 -179.4(4) . .
Nd2 N3 C23 N4 -8.0(4) . .
C29 N3 C23 C24 0.9(6) . .
Nd2 N3 C23 C24 172.2(4) . .
C29 N3 C23 Nd2 -171.3(4) . .
C35 N4 C23 N3 176.4(4) . .
Nd2 N4 C23 N3 8.2(4) . .
C35 N4 C23 C24 -3.9(6) . .
Nd2 N4 C23 C24 -172.0(4) . .
C35 N4 C23 Nd2 168.2(4) . .
N4 Nd2 C23 N3 -171.4(4) . .
Cl1 Nd2 C23 N3 67.0(2) . .
C42 Nd2 C23 N3 -76.1(9) . .
C46 Nd2 C23 N3 -79.2(3) . .
C48 Nd2 C23 N3 -125.4(3) . .
Cl2 Nd2 C23 N3 143.3(2) . .
C47 Nd2 C23 N3 -106.0(3) . .
C43 Nd2 C23 N3 -23.5(4) . .
C44 Nd2 C23 N3 -31.2(3) . .
C45 Nd2 C23 N3 -51.6(3) . .
N3 Nd2 C23 N4 171.4(4) . .
Cl1 Nd2 C23 N4 -121.5(2) . .
C42 Nd2 C23 N4 95.4(9) . .
C46 Nd2 C23 N4 92.3(3) . .
C48 Nd2 C23 N4 46.1(3) . .
Cl2 Nd2 C23 N4 -45.2(3) . .
C47 Nd2 C23 N4 65.5(3) . .
C43 Nd2 C23 N4 148.0(3) . .
C44 Nd2 C23 N4 140.2(3) . .
C45 Nd2 C23 N4 119.9(3) . .
N4 Nd2 C23 C24 73(3) . .
N3 Nd2 C23 C24 -116(3) . .
Cl1 Nd2 C23 C24 -49(3) . .
C42 Nd2 C23 C24 168(2) . .
C46 Nd2 C23 C24 165(3) . .
C48 Nd2 C23 C24 119(3) . .
Cl2 Nd2 C23 C24 28(3) . .
C47 Nd2 C23 C24 138(3) . .
C43 Nd2 C23 C24 -139(3) . .
C44 Nd2 C23 C24 -147(3) . .
C45 Nd2 C23 C24 -167(3) . .
N3 C23 C24 C25 156(5) . .
N4 C23 C24 C25 -23(6) . .
Nd2 C23 C24 C25 -92(6) . .
C23 C24 C25 C26 45(16) . .
C24 C25 C26 C27 26(13) . .
C24 C25 C26 C28 104(12) . .
C25 C26 C27 C28 113.0(7) . .
C25 C26 C28 C27 -109.3(7) . .
C23 N3 C29 C30 149.5(4) . .
Nd2 N3 C29 C30 -14.7(7) . .
C23 N3 C29 C34 -88.3(5) . .
Nd2 N3 C29 C34 107.5(6) . .
N3 C29 C30 C31 179.2(4) . .
C34 C29 C30 C31 56.4(6) . .
C29 C30 C31 C32 -55.7(7) . .
C30 C31 C32 C33 54.4(7) . .
C31 C32 C33 C34 -55.4(7) . .
C32 C33 C34 C29 56.9(6) . .
N3 C29 C34 C33 -179.3(5) . .
C30 C29 C34 C33 -56.9(6) . .
C23 N4 C35 C40 -80.4(5) . .
Nd2 N4 C35 C40 79.5(6) . .
C23 N4 C35 C36 157.0(4) . .
Nd2 N4 C35 C36 -43.1(6) . .
N4 C35 C36 C37 -178.0(4) . .
C40 C35 C36 C37 58.3(5) . .
C35 C36 C37 C38 -55.7(6) . .
C36 C37 C38 C39 53.0(6) . .
C37 C38 C39 C40 -53.3(6) . .
N4 C35 C40 C39 179.7(4) . .
C36 C35 C40 C39 -57.9(5) . .
C38 C39 C40 C35 55.9(6) . .
N6 Nd3 C41 C42 153.4(3) . .
N5 Nd3 C41 C42 -156.3(3) . .
Cl4 Nd3 C41 C42 14.0(4) . .
C47 Nd3 C41 C42 -123.2(4) . .
Cl3 Nd3 C41 C42 71.8(3) . .
C45 Nd3 C41 C42 -70.3(3) . .
C48 Nd3 C41 C42 -142.6(5) . .
C46 Nd3 C41 C42 -99.1(3) . .
C49 Nd3 C41 C42 171.5(3) . .
C44 Nd3 C41 C42 -41.8(3) . .
N6 Nd3 C41 C48 -63.9(3) . .
N5 Nd3 C41 C48 -13.6(4) . .
Cl4 Nd3 C41 C48 156.7(2) . .
C47 Nd3 C41 C48 19.4(3) . .
Cl3 Nd3 C41 C48 -145.6(3) . .
C45 Nd3 C41 C48 72.3(3) . .
C46 Nd3 C41 C48 43.5(3) . .
C49 Nd3 C41 C48 -45.9(3) . .
C42 Nd3 C41 C48 142.6(5) . .
C44 Nd3 C41 C48 100.9(3) . .
N6 Nd3 C41 Nd2 -134.99(18) . .
N5 Nd3 C41 Nd2 -84.7(2) . .
Cl4 Nd3 C41 Nd2 85.6(2) . .
C47 Nd3 C41 Nd2 -51.6(2) . .
Cl3 Nd3 C41 Nd2 143.40(19) . .
C45 Nd3 C41 Nd2 1.3(2) . .
C48 Nd3 C41 Nd2 -71.0(3) . .
C46 Nd3 C41 Nd2 -27.5(2) . .
C49 Nd3 C41 Nd2 -116.95(17) . .
C42 Nd3 C41 Nd2 71.6(3) . .
C44 Nd3 C41 Nd2 29.8(2) . .
N4 Nd2 C41 C42 178.9(3) . .
N3 Nd2 C41 C42 100.2(5) . .
Cl1 Nd2 C41 C42 -43.5(3) . .
C23 Nd2 C41 C42 157.9(3) . .
C46 Nd2 C41 C42 101.9(4) . .
C48 Nd2 C41 C42 145.9(5) . .
Cl2 Nd2 C41 C42 -107.4(3) . .
C47 Nd2 C41 C42 125.6(4) . .
C43 Nd2 C41 C42 20.2(3) . .
C44 Nd2 C41 C42 44.0(3) . .
C45 Nd2 C41 C42 72.9(4) . .
N4 Nd2 C41 C48 32.9(3) . .
N3 Nd2 C41 C48 -45.7(5) . .
Cl1 Nd2 C41 C48 170.6(3) . .
C42 Nd2 C41 C48 -145.9(5) . .
C23 Nd2 C41 C48 12.0(4) . .
C46 Nd2 C41 C48 -44.1(3) . .
Cl2 Nd2 C41 C48 106.6(3) . .
C47 Nd2 C41 C48 -20.3(3) . .
C43 Nd2 C41 C48 -125.7(4) . .
C44 Nd2 C41 C48 -102.0(3) . .
C45 Nd2 C41 C48 -73.0(3) . .
N4 Nd2 C41 Nd3 104.66(19) . .
N3 Nd2 C41 Nd3 26.0(5) . .
Cl1 Nd2 C41 Nd3 -117.71(15) . .
C42 Nd2 C41 Nd3 -74.2(3) . .
C23 Nd2 C41 Nd3 83.7(3) . .
C46 Nd2 C41 Nd3 27.6(2) . .
C48 Nd2 C41 Nd3 71.7(3) . .
Cl2 Nd2 C41 Nd3 178.3(2) . .
C47 Nd2 C41 Nd3 51.38(19) . .
C43 Nd2 C41 Nd3 -54.0(2) . .
C44 Nd2 C41 Nd3 -30.2(2) . .
C45 Nd2 C41 Nd3 -1.3(2) . .
C48 C41 C42 C43 -5.4(11) . .
Nd3 C41 C42 C43 49.4(6) . .
Nd2 C41 C42 C43 -54.1(6) . .
C48 C41 C42 Nd2 48.7(6) . .
Nd3 C41 C42 Nd2 103.48(13) . .
C48 C41 C42 Nd3 -54.8(6) . .
Nd2 C41 C42 Nd3 -103.48(13) . .
N4 Nd2 C42 C41 -1.9(5) . .
N3 Nd2 C42 C41 -131.7(4) . .
Cl1 Nd2 C42 C41 142.1(3) . .
C23 Nd2 C42 C41 -74.9(10) . .
C46 Nd2 C42 C41 -71.8(3) . .
C48 Nd2 C42 C41 -19.5(3) . .
Cl2 Nd2 C42 C41 67.2(3) . .
C47 Nd2 C42 C41 -43.7(3) . .
C43 Nd2 C42 C41 -144.8(5) . .
C44 Nd2 C42 C41 -125.3(4) . .
C45 Nd2 C42 C41 -100.5(3) . .
N4 Nd2 C42 C43 142.9(3) . .
N3 Nd2 C42 C43 13.1(5) . .
Cl1 Nd2 C42 C43 -73.1(3) . .
C23 Nd2 C42 C43 69.9(10) . .
C46 Nd2 C42 C43 73.0(4) . .
C48 Nd2 C42 C43 125.3(4) . .
Cl2 Nd2 C42 C43 -148.0(3) . .
C47 Nd2 C42 C43 101.1(3) . .
C44 Nd2 C42 C43 19.5(3) . .
C45 Nd2 C42 C43 44.4(3) . .
N4 Nd2 C42 Nd3 69.8(4) . .
N3 Nd2 C42 Nd3 -60.0(4) . .
Cl1 Nd2 C42 Nd3 -146.21(17) . .
C23 Nd2 C42 Nd3 -3.2(10) . .
C46 Nd2 C42 Nd3 -0.1(2) . .
C48 Nd2 C42 Nd3 52.2(2) . .
Cl2 Nd2 C42 Nd3 138.9(2) . .
C47 Nd2 C42 Nd3 28.0(2) . .
C43 Nd2 C42 Nd3 -73.1(3) . .
C44 Nd2 C42 Nd3 -53.6(2) . .
C45 Nd2 C42 Nd3 -28.7(2) . .
N6 Nd3 C42 C41 -32.4(4) . .
N5 Nd3 C42 C41 52.2(7) . .
Cl4 Nd3 C42 C41 -170.2(3) . .
C47 Nd3 C42 C41 45.9(3) . .
Cl3 Nd3 C42 C41 -101.9(3) . .
C45 Nd3 C42 C41 103.4(4) . .
C48 Nd3 C42 C41 21.5(3) . .
C46 Nd3 C42 C41 74.4(3) . .
C49 Nd3 C42 C41 -14.5(5) . .
C44 Nd3 C42 C41 127.7(4) . .
N6 Nd3 C42 C43 -179.7(3) . .
N5 Nd3 C42 C43 -95.1(6) . .
Cl4 Nd3 C42 C43 42.4(3) . .
C47 Nd3 C42 C43 -101.4(3) . .
Cl3 Nd3 C42 C43 110.7(3) . .
C45 Nd3 C42 C43 -44.0(3) . .
C48 Nd3 C42 C43 -125.9(4) . .
C41 Nd3 C42 C43 -147.4(5) . .
C46 Nd3 C42 C43 -73.0(3) . .
C49 Nd3 C42 C43 -161.9(3) . .
C44 Nd3 C42 C43 -19.6(3) . .
N6 Nd3 C42 Nd2 -106.6(2) . .
N5 Nd3 C42 Nd2 -22.1(6) . .
Cl4 Nd3 C42 Nd2 115.48(17) . .
C47 Nd3 C42 Nd2 -28.4(2) . .
Cl3 Nd3 C42 Nd2 -176.2(2) . .
C45 Nd3 C42 Nd2 29.1(2) . .
C48 Nd3 C42 Nd2 -52.8(2) . .
C41 Nd3 C42 Nd2 -74.3(3) . .
C46 Nd3 C42 Nd2 0.1(2) . .
C49 Nd3 C42 Nd2 -88.8(3) . .
C44 Nd3 C42 Nd2 53.4(2) . .
C41 C42 C43 C44 3.2(11) . .
Nd2 C42 C43 C44 -51.4(6) . .
Nd3 C42 C43 C44 52.1(6) . .
C41 C42 C43 Nd2 54.6(6) . .
Nd3 C42 C43 Nd2 103.48(14) . .
C41 C42 C43 Nd3 -48.9(6) . .
Nd2 C42 C43 Nd3 -103.48(14) . .
N4 Nd2 C43 C44 40.0(7) . .
N3 Nd2 C43 C44 -27.0(4) . .
Cl1 Nd2 C43 C44 -107.5(3) . .
C42 Nd2 C43 C44 145.0(5) . .
C23 Nd2 C43 C44 -14.7(5) . .
C46 Nd2 C43 C44 44.6(3) . .
C48 Nd2 C43 C44 101.3(3) . .
Cl2 Nd2 C43 C44 178.7(3) . .
C47 Nd2 C43 C44 72.8(3) . .
C45 Nd2 C43 C44 20.6(3) . .
N4 Nd2 C43 C42 -104.9(6) . .
N3 Nd2 C43 C42 -171.9(3) . .
Cl1 Nd2 C43 C42 107.6(3) . .
C23 Nd2 C43 C42 -159.7(3) . .
C46 Nd2 C43 C42 -100.4(4) . .
C48 Nd2 C43 C42 -43.6(3) . .
Cl2 Nd2 C43 C42 33.7(3) . .
C47 Nd2 C43 C42 -72.2(3) . .
C44 Nd2 C43 C42 -145.0(5) . .
C45 Nd2 C43 C42 -124.3(4) . .
N4 Nd2 C43 Nd3 -32.9(7) . .
N3 Nd2 C43 Nd3 -100.0(2) . .
Cl1 Nd2 C43 Nd3 179.6(2) . .
C42 Nd2 C43 Nd3 72.0(3) . .
C23 Nd2 C43 Nd3 -87.7(3) . .
C46 Nd2 C43 Nd3 -28.4(2) . .
C48 Nd2 C43 Nd3 28.3(2) . .
Cl2 Nd2 C43 Nd3 105.67(18) . .
C47 Nd2 C43 Nd3 -0.2(2) . .
C44 Nd2 C43 Nd3 -73.0(3) . .
C45 Nd2 C43 Nd3 -52.4(2) . .
N6 Nd3 C43 C44 -144.1(4) . .
N5 Nd3 C43 C44 -4.1(5) . .
Cl4 Nd3 C43 C44 74.0(3) . .
C47 Nd3 C43 C44 -72.8(3) . .
Cl3 Nd3 C43 C44 151.3(3) . .
C45 Nd3 C43 C44 -19.7(3) . .
C48 Nd3 C43 C44 -101.5(3) . .
C41 Nd3 C43 C44 -126.4(4) . .
C46 Nd3 C43 C44 -44.5(3) . .
C49 Nd3 C43 C44 -54.0(13) . .
C42 Nd3 C43 C44 -144.6(5) . .
N6 Nd3 C43 C42 0.5(5) . .
N5 Nd3 C43 C42 140.5(3) . .
Cl4 Nd3 C43 C42 -141.4(3) . .
C47 Nd3 C43 C42 71.8(3) . .
Cl3 Nd3 C43 C42 -64.1(3) . .
C45 Nd3 C43 C42 124.9(4) . .
C48 Nd3 C43 C42 43.1(3) . .
C41 Nd3 C43 C42 18.2(3) . .
C46 Nd3 C43 C42 100.1(3) . .
C49 Nd3 C43 C42 90.6(13) . .
C44 Nd3 C43 C42 144.6(5) . .
N6 Nd3 C43 Nd2 -71.1(4) . .
N5 Nd3 C43 Nd2 68.9(4) . .
Cl4 Nd3 C43 Nd2 146.97(19) . .
C47 Nd3 C43 Nd2 0.2(2) . .
Cl3 Nd3 C43 Nd2 -135.8(2) . .
C45 Nd3 C43 Nd2 53.3(2) . .
C48 Nd3 C43 Nd2 -28.5(2) . .
C41 Nd3 C43 Nd2 -53.5(2) . .
C46 Nd3 C43 Nd2 28.5(2) . .
C49 Nd3 C43 Nd2 19.0(13) . .
C42 Nd3 C43 Nd2 -71.6(3) . .
C44 Nd3 C43 Nd2 73.0(3) . .
C42 C43 C44 C45 -2.4(10) . .
Nd2 C43 C44 C45 -53.4(6) . .
Nd3 C43 C44 C45 49.5(6) . .
C42 C43 C44 Nd2 51.1(6) . .
Nd3 C43 C44 Nd2 102.88(13) . .
C42 C43 C44 Nd3 -51.8(6) . .
Nd2 C43 C44 Nd3 -102.88(13) . .
N4 Nd2 C44 C43 -163.2(3) . .
N3 Nd2 C44 C43 156.4(3) . .
Cl1 Nd2 C44 C43 73.2(3) . .
C42 Nd2 C44 C43 -20.1(3) . .
C23 Nd2 C44 C43 170.5(3) . .
C46 Nd2 C44 C43 -124.9(4) . .
C48 Nd2 C44 C43 -72.4(3) . .
Cl2 Nd2 C44 C43 -1.9(4) . .
C47 Nd2 C44 C43 -100.8(3) . .
C45 Nd2 C44 C43 -143.9(5) . .
N4 Nd2 C44 C45 -19.4(4) . .
N3 Nd2 C44 C45 -59.7(3) . .
Cl1 Nd2 C44 C45 -143.0(3) . .
C42 Nd2 C44 C45 123.8(4) . .
C23 Nd2 C44 C45 -45.6(3) . .
C46 Nd2 C44 C45 19.0(3) . .
C48 Nd2 C44 C45 71.5(3) . .
Cl2 Nd2 C44 C45 142.0(3) . .
C47 Nd2 C44 C45 43.1(3) . .
C43 Nd2 C44 C45 143.9(5) . .
N4 Nd2 C44 Nd3 -89.9(2) . .
N3 Nd2 C44 Nd3 -130.2(2) . .
Cl1 Nd2 C44 Nd3 146.52(18) . .
C42 Nd2 C44 Nd3 53.3(2) . .
C23 Nd2 C44 Nd3 -116.10(19) . .
C46 Nd2 C44 Nd3 -51.5(2) . .
C48 Nd2 C44 Nd3 1.0(2) . .
Cl2 Nd2 C44 Nd3 71.5(3) . .
C47 Nd2 C44 Nd3 -27.4(2) . .
C43 Nd2 C44 Nd3 73.4(3) . .
C45 Nd2 C44 Nd3 -70.5(3) . .
N6 Nd3 C44 C43 110.0(7) . .
N5 Nd3 C44 C43 177.4(3) . .
Cl4 Nd3 C44 C43 -104.4(3) . .
C47 Nd3 C44 C43 100.8(3) . .
Cl3 Nd3 C44 C43 -30.5(3) . .
C45 Nd3 C44 C43 145.6(5) . .
C48 Nd3 C44 C43 72.0(3) . .
C41 Nd3 C44 C43 43.0(3) . .
C46 Nd3 C44 C43 124.8(4) . .
C49 Nd3 C44 C43 167.0(3) . .
C42 Nd3 C44 C43 20.2(3) . .
N6 Nd3 C44 C45 -35.6(8) . .
N5 Nd3 C44 C45 31.8(3) . .
Cl4 Nd3 C44 C45 110.0(3) . .
C47 Nd3 C44 C45 -44.8(3) . .
Cl3 Nd3 C44 C45 -176.1(3) . .
C48 Nd3 C44 C45 -73.6(3) . .
C41 Nd3 C44 C45 -102.6(3) . .
C46 Nd3 C44 C45 -20.8(3) . .
C49 Nd3 C44 C45 21.4(4) . .
C42 Nd3 C44 C45 -125.4(4) . .
N6 Nd3 C44 Nd2 37.0(7) . .
N5 Nd3 C44 Nd2 104.4(2) . .
Cl4 Nd3 C44 Nd2 -177.4(2) . .
C47 Nd3 C44 Nd2 27.8(2) . .
Cl3 Nd3 C44 Nd2 -103.53(18) . .
C45 Nd3 C44 Nd2 72.6(3) . .
C48 Nd3 C44 Nd2 -1.0(2) . .
C41 Nd3 C44 Nd2 -30.0(2) . .
C46 Nd3 C44 Nd2 51.8(2) . .
C49 Nd3 C44 Nd2 94.0(3) . .
C42 Nd3 C44 Nd2 -52.8(2) . .
C43 C44 C45 C46 4.6(10) . .
Nd2 C44 C45 C46 -48.7(6) . .
Nd3 C44 C45 C46 55.0(6) . .
C43 C44 C45 Nd3 -50.3(6) . .
Nd2 C44 C45 Nd3 -103.69(13) . .
C43 C44 C45 Nd2 53.4(6) . .
Nd3 C44 C45 Nd2 103.69(13) . .
N6 Nd3 C45 C46 22.9(4) . .
N5 Nd3 C45 C46 64.2(3) . .
Cl4 Nd3 C45 C46 147.6(3) . .
C47 Nd3 C45 C46 -19.2(3) . .
Cl3 Nd3 C45 C46 -137.8(3) . .
C48 Nd3 C45 C46 -43.5(3) . .
C41 Nd3 C45 C46 -72.5(3) . .
C49 Nd3 C45 C46 50.1(3) . .
C42 Nd3 C45 C46 -99.9(3) . .
C44 Nd3 C45 C46 -143.3(5) . .
N6 Nd3 C45 C44 166.2(3) . .
N5 Nd3 C45 C44 -152.5(3) . .
Cl4 Nd3 C45 C44 -69.1(3) . .
C47 Nd3 C45 C44 124.1(4) . .
Cl3 Nd3 C45 C44 5.5(4) . .
C48 Nd3 C45 C44 99.7(3) . .
C41 Nd3 C45 C44 70.8(3) . .
C46 Nd3 C45 C44 143.3(5) . .
C49 Nd3 C45 C44 -166.6(3) . .
C42 Nd3 C45 C44 43.3(3) . .
N6 Nd3 C45 Nd2 94.1(2) . .
N5 Nd3 C45 Nd2 135.4(2) . .
Cl4 Nd3 C45 Nd2 -141.20(19) . .
C47 Nd3 C45 Nd2 52.0(2) . .
Cl3 Nd3 C45 Nd2 -66.6(3) . .
C48 Nd3 C45 Nd2 27.6(2) . .
C41 Nd3 C45 Nd2 -1.3(2) . .
C46 Nd3 C45 Nd2 71.2(3) . .
C49 Nd3 C45 Nd2 121.24(18) . .
C42 Nd3 C45 Nd2 -28.8(2) . .
C44 Nd3 C45 Nd2 -72.1(3) . .
N4 Nd2 C45 C46 -47.5(3) . .
N3 Nd2 C45 C46 -95.3(3) . .
Cl1 Nd2 C45 C46 -170.8(3) . .
C42 Nd2 C45 C46 101.5(3) . .
C23 Nd2 C45 C46 -73.2(3) . .
C48 Nd2 C45 C46 44.6(3) . .
Cl2 Nd2 C45 C46 72.7(5) . .
C47 Nd2 C45 C46 20.5(3) . .
C43 Nd2 C45 C46 126.3(4) . .
C44 Nd2 C45 C46 146.5(5) . .
N4 Nd2 C45 C44 166.1(3) . .
N3 Nd2 C45 C44 118.2(3) . .
Cl1 Nd2 C45 C44 42.7(3) . .
C42 Nd2 C45 C44 -45.0(3) . .
C23 Nd2 C45 C44 140.3(3) . .
C46 Nd2 C45 C44 -146.5(5) . .
C48 Nd2 C45 C44 -101.9(3) . .
Cl2 Nd2 C45 C44 -73.8(5) . .
C47 Nd2 C45 C44 -126.0(4) . .
C43 Nd2 C45 C44 -20.1(3) . .
N4 Nd2 C45 Nd3 -119.7(2) . .
N3 Nd2 C45 Nd3 -167.5(2) . .
Cl1 Nd2 C45 Nd3 116.97(17) . .
C42 Nd2 C45 Nd3 29.3(2) . .
C23 Nd2 C45 Nd3 -145.5(2) . .
C46 Nd2 C45 Nd3 -72.2(3) . .
C48 Nd2 C45 Nd3 -27.6(2) . .
Cl2 Nd2 C45 Nd3 0.5(5) . .
C47 Nd2 C45 Nd3 -51.7(2) . .
C43 Nd2 C45 Nd3 54.1(2) . .
C44 Nd2 C45 Nd3 74.2(3) . .
C44 C45 C46 C47 -5.8(10) . .
Nd3 C45 C46 C47 49.8(6) . .
Nd2 C45 C46 C47 -54.7(6) . .
C44 C45 C46 Nd2 48.9(6) . .
Nd3 C45 C46 Nd2 104.44(14) . .
C44 C45 C46 Nd3 -55.6(6) . .
Nd2 C45 C46 Nd3 -104.44(14) . .
N4 Nd2 C46 C47 -80.9(3) . .
N3 Nd2 C46 C47 -137.0(3) . .
Cl1 Nd2 C46 C47 158.1(3) . .
C42 Nd2 C46 C47 71.4(3) . .
C23 Nd2 C46 C47 -109.3(3) . .
C48 Nd2 C46 C47 19.2(3) . .
Cl2 Nd2 C46 C47 0.9(4) . .
C43 Nd2 C46 C47 100.5(3) . .
C44 Nd2 C46 C47 124.3(4) . .
C45 Nd2 C46 C47 143.3(5) . .
N4 Nd2 C46 C45 135.7(3) . .
N3 Nd2 C46 C45 79.6(3) . .
Cl1 Nd2 C46 C45 14.7(4) . .
C42 Nd2 C46 C45 -71.9(3) . .
C23 Nd2 C46 C45 107.4(3) . .
C48 Nd2 C46 C45 -124.2(4) . .
Cl2 Nd2 C46 C45 -142.5(3) . .
C47 Nd2 C46 C45 -143.3(5) . .
C43 Nd2 C46 C45 -42.9(3) . .
C44 Nd2 C46 C45 -19.0(3) . .
N4 Nd2 C46 Nd3 -152.3(2) . .
N3 Nd2 C46 Nd3 151.6(2) . .
Cl1 Nd2 C46 Nd3 86.7(3) . .
C42 Nd2 C46 Nd3 0.1(2) . .
C23 Nd2 C46 Nd3 179.4(2) . .
C48 Nd2 C46 Nd3 -52.2(2) . .
Cl2 Nd2 C46 Nd3 -70.5(3) . .
C47 Nd2 C46 Nd3 -71.4(3) . .
C43 Nd2 C46 Nd3 29.1(2) . .
C44 Nd2 C46 Nd3 53.0(2) . .
C45 Nd2 C46 Nd3 72.0(3) . .
N6 Nd3 C46 C47 50.6(3) . .
N5 Nd3 C46 C47 99.7(3) . .
Cl4 Nd3 C46 C47 177.3(3) . .
Cl3 Nd3 C46 C47 -64.8(5) . .
C45 Nd3 C46 C47 -145.7(5) . .
C48 Nd3 C46 C47 -20.2(3) . .
C41 Nd3 C46 C47 -44.7(3) . .
C49 Nd3 C46 C47 77.2(3) . .
C42 Nd3 C46 C47 -72.7(3) . .
C44 Nd3 C46 C47 -125.0(4) . .
N6 Nd3 C46 C45 -163.6(3) . .
N5 Nd3 C46 C45 -114.6(3) . .
Cl4 Nd3 C46 C45 -37.0(3) . .
C47 Nd3 C46 C45 145.7(5) . .
Cl3 Nd3 C46 C45 81.0(5) . .
C48 Nd3 C46 C45 125.5(4) . .
C41 Nd3 C46 C45 101.1(3) . .
C49 Nd3 C46 C45 -137.1(3) . .
C42 Nd3 C46 C45 73.1(3) . .
C44 Nd3 C46 C45 20.7(3) . .
N6 Nd3 C46 Nd2 123.25(19) . .
N5 Nd3 C46 Nd2 172.3(2) . .
Cl4 Nd3 C46 Nd2 -110.09(17) . .
C47 Nd3 C46 Nd2 72.6(3) . .
Cl3 Nd3 C46 Nd2 7.9(5) . .
C45 Nd3 C46 Nd2 -73.1(3) . .
C48 Nd3 C46 Nd2 52.4(2) . .
C41 Nd3 C46 Nd2 28.0(2) . .
C49 Nd3 C46 Nd2 149.8(2) . .
C42 Nd3 C46 Nd2 -0.1(2) . .
C44 Nd3 C46 Nd2 -52.4(2) . .
C45 C46 C47 C48 4.3(11) . .
Nd2 C46 C47 C48 -50.5(6) . .
Nd3 C46 C47 C48 54.2(6) . .
C45 C46 C47 Nd3 -49.9(6) . .
Nd2 C46 C47 Nd3 -104.71(14) . .
C45 C46 C47 Nd2 54.8(6) . .
Nd3 C46 C47 Nd2 104.71(14) . .
N6 Nd3 C47 C46 -133.2(3) . .
N5 Nd3 C47 C46 -77.3(3) . .
Cl4 Nd3 C47 C46 -4.3(4) . .
Cl3 Nd3 C47 C46 145.4(3) . .
C45 Nd3 C47 C46 19.5(3) . .
C48 Nd3 C47 C46 144.3(5) . .
C41 Nd3 C47 C46 124.7(4) . .
C49 Nd3 C47 C46 -105.2(3) . .
C42 Nd3 C47 C46 100.5(4) . .
C44 Nd3 C47 C46 44.2(3) . .
N6 Nd3 C47 C48 82.5(3) . .
N5 Nd3 C47 C48 138.3(3) . .
Cl4 Nd3 C47 C48 -148.6(3) . .
Cl3 Nd3 C47 C48 1.0(4) . .
C45 Nd3 C47 C48 -124.8(4) . .
C41 Nd3 C47 C48 -19.7(3) . .
C46 Nd3 C47 C48 -144.3(5) . .
C49 Nd3 C47 C48 110.5(3) . .
C42 Nd3 C47 C48 -43.9(3) . .
C44 Nd3 C47 C48 -100.1(3) . .
N6 Nd3 C47 Nd2 154.6(2) . .
N5 Nd3 C47 Nd2 -149.5(2) . .
Cl4 Nd3 C47 Nd2 -76.4(3) . .
Cl3 Nd3 C47 Nd2 73.2(3) . .
C45 Nd3 C47 Nd2 -52.6(2) . .
C48 Nd3 C47 Nd2 72.2(3) . .
C41 Nd3 C47 Nd2 52.51(19) . .
C46 Nd3 C47 Nd2 -72.2(3) . .
C49 Nd3 C47 Nd2 -177.3(2) . .
C42 Nd3 C47 Nd2 28.3(2) . .
C44 Nd3 C47 Nd2 -27.9(2) . .
N4 Nd2 C47 C46 97.2(3) . .
N3 Nd2 C47 C46 43.9(3) . .
Cl1 Nd2 C47 C46 -74.3(8) . .
C42 Nd2 C47 C46 -102.1(3) . .
C23 Nd2 C47 C46 71.5(3) . .
C48 Nd2 C47 C46 -146.2(5) . .
Cl2 Nd2 C47 C46 -179.4(3) . .
C43 Nd2 C47 C46 -73.1(3) . .
C44 Nd2 C47 C46 -45.0(3) . .
C45 Nd2 C47 C46 -20.9(3) . .
N4 Nd2 C47 C48 -116.6(3) . .
N3 Nd2 C47 C48 -169.9(3) . .
Cl1 Nd2 C47 C48 71.9(8) . .
C42 Nd2 C47 C48 44.1(3) . .
C23 Nd2 C47 C48 -142.3(3) . .
C46 Nd2 C47 C48 146.2(5) . .
Cl2 Nd2 C47 C48 -33.2(3) . .
C43 Nd2 C47 C48 73.1(3) . .
C44 Nd2 C47 C48 101.2(3) . .
C45 Nd2 C47 C48 125.3(4) . .
N4 Nd2 C47 Nd3 170.6(2) . .
N3 Nd2 C47 Nd3 117.22(19) . .
Cl1 Nd2 C47 Nd3 -0.9(9) . .
C42 Nd2 C47 Nd3 -28.8(2) . .
C23 Nd2 C47 Nd3 144.84(19) . .
C46 Nd2 C47 Nd3 73.3(3) . .
C48 Nd2 C47 Nd3 -72.9(3) . .
Cl2 Nd2 C47 Nd3 -106.05(18) . .
C43 Nd2 C47 Nd3 0.2(2) . .
C44 Nd2 C47 Nd3 28.3(2) . .
C45 Nd2 C47 Nd3 52.4(2) . .
C46 C47 C48 C41 -3.7(11) . .
Nd3 C47 C48 C41 50.7(6) . .
Nd2 C47 C48 C41 -54.1(6) . .
C46 C47 C48 Nd3 -54.4(6) . .
Nd2 C47 C48 Nd3 -104.82(14) . .
C46 C47 C48 Nd2 50.4(6) . .
Nd3 C47 C48 Nd2 104.82(14) . .
C42 C41 C48 C47 5.2(10) . .
Nd3 C41 C48 C47 -50.4(6) . .
Nd2 C41 C48 C47 53.8(6) . .
C42 C41 C48 Nd3 55.6(6) . .
Nd2 C41 C48 Nd3 104.28(13) . .
C42 C41 C48 Nd2 -48.7(6) . .
Nd3 C41 C48 Nd2 -104.28(13) . .
N6 Nd3 C48 C47 -96.8(3) . .
N5 Nd3 C48 C47 -44.3(3) . .
Cl4 Nd3 C48 C47 85.3(6) . .
Cl3 Nd3 C48 C47 -179.2(3) . .
C45 Nd3 C48 C47 44.3(3) . .
C41 Nd3 C48 C47 145.5(5) . .
C46 Nd3 C48 C47 20.0(3) . .
C49 Nd3 C48 C47 -72.5(3) . .
C42 Nd3 C48 C47 124.9(4) . .
C44 Nd3 C48 C47 73.2(4) . .
N6 Nd3 C48 C41 117.7(3) . .
N5 Nd3 C48 C41 170.2(3) . .
Cl4 Nd3 C48 C41 -60.2(7) . .
C47 Nd3 C48 C41 -145.5(5) . .
Cl3 Nd3 C48 C41 35.3(3) . .
C45 Nd3 C48 C41 -101.2(3) . .
C46 Nd3 C48 C41 -125.5(4) . .
C49 Nd3 C48 C41 142.1(3) . .
C42 Nd3 C48 C41 -20.6(3) . .
C44 Nd3 C48 C41 -72.3(3) . .
N6 Nd3 C48 Nd2 -169.1(2) . .
N5 Nd3 C48 Nd2 -116.52(19) . .
Cl4 Nd3 C48 Nd2 13.1(7) . .
C47 Nd3 C48 Nd2 -72.2(3) . .
Cl3 Nd3 C48 Nd2 108.57(17) . .
C45 Nd3 C48 Nd2 -27.9(2) . .
C41 Nd3 C48 Nd2 73.3(3) . .
C46 Nd3 C48 Nd2 -52.2(2) . .
C49 Nd3 C48 Nd2 -144.67(18) . .
C42 Nd3 C48 Nd2 52.7(2) . .
C44 Nd3 C48 Nd2 1.0(2) . .
N4 Nd2 C48 C47 63.8(3) . .
N3 Nd2 C48 C47 13.1(4) . .
Cl1 Nd2 C48 C47 -158.7(3) . .
C42 Nd2 C48 C47 -124.9(4) . .
C23 Nd2 C48 C47 43.6(3) . .
C46 Nd2 C48 C47 -19.0(3) . .
Cl2 Nd2 C48 C47 148.4(3) . .
C43 Nd2 C48 C47 -100.4(3) . .
C44 Nd2 C48 C47 -72.4(3) . .
C45 Nd2 C48 C47 -43.7(3) . .
N4 Nd2 C48 C41 -152.4(3) . .
N3 Nd2 C48 C41 156.9(3) . .
Cl1 Nd2 C48 C41 -14.9(4) . .
C42 Nd2 C48 C41 18.9(3) . .
C23 Nd2 C48 C41 -172.6(3) . .
C46 Nd2 C48 C41 124.8(3) . .
Cl2 Nd2 C48 C41 -67.8(3) . .
C47 Nd2 C48 C41 143.8(5) . .
C43 Nd2 C48 C41 43.4(3) . .
C44 Nd2 C48 C41 71.4(3) . .
C45 Nd2 C48 C41 100.1(3) . .
N4 Nd2 C48 Nd3 135.13(19) . .
N3 Nd2 C48 Nd3 84.4(2) . .
Cl1 Nd2 C48 Nd3 -87.4(2) . .
C42 Nd2 C48 Nd3 -53.5(2) . .
C23 Nd2 C48 Nd3 114.98(18) . .
C46 Nd2 C48 Nd3 52.4(2) . .
Cl2 Nd2 C48 Nd3 -140.2(2) . .
C47 Nd2 C48 Nd3 71.4(3) . .
C43 Nd2 C48 Nd3 -29.1(2) . .
C44 Nd2 C48 Nd3 -1.0(2) . .
C45 Nd2 C48 Nd3 27.7(2) . .
C61 N6 C49 N5 -178.7(4) . .
Nd3 N6 C49 N5 -10.0(4) . .
C61 N6 C49 C50 -1.2(6) . .
Nd3 N6 C49 C50 167.5(4) . .
C61 N6 C49 Nd3 -168.7(4) . .
C55 N5 C49 N6 -175.4(4) . .
Nd3 N5 C49 N6 9.9(4) . .
C55 N5 C49 C50 7.1(6) . .
Nd3 N5 C49 C50 -167.6(4) . .
C55 N5 C49 Nd3 174.8(4) . .
N5 Nd3 C49 N6 -169.6(4) . .
Cl4 Nd3 C49 N6 125.2(2) . .
C47 Nd3 C49 N6 -88.6(3) . .
Cl3 Nd3 C49 N6 47.0(3) . .
C45 Nd3 C49 N6 -138.4(3) . .
C48 Nd3 C49 N6 -61.3(3) . .
C41 Nd3 C49 N6 -40.4(3) . .
C46 Nd3 C49 N6 -116.3(3) . .
C42 Nd3 C49 N6 -32.4(4) . .
C44 Nd3 C49 N6 -150.0(3) . .
N6 Nd3 C49 N5 169.6(4) . .
Cl4 Nd3 C49 N5 -65.3(2) . .
C47 Nd3 C49 N5 80.9(3) . .
Cl3 Nd3 C49 N5 -143.5(2) . .
C45 Nd3 C49 N5 31.2(3) . .
C48 Nd3 C49 N5 108.3(3) . .
C41 Nd3 C49 N5 129.1(3) . .
C46 Nd3 C49 N5 53.2(3) . .
C42 Nd3 C49 N5 137.2(3) . .
C44 Nd3 C49 N5 19.6(4) . .
N6 Nd3 C49 C50 -89.1(18) . .
N5 Nd3 C49 C50 101.3(18) . .
Cl4 Nd3 C49 C50 36.0(18) . .
C47 Nd3 C49 C50 -178(100) . .
Cl3 Nd3 C49 C50 -42.1(18) . .
C45 Nd3 C49 C50 132.5(18) . .
C48 Nd3 C49 C50 -150.4(18) . .
C41 Nd3 C49 C50 -129.5(18) . .
C46 Nd3 C49 C50 154.6(18) . .
C42 Nd3 C49 C50 -121.5(18) . .
C44 Nd3 C49 C50 120.9(18) . .
N6 C49 C50 C51 -77(4) . .
N5 C49 C50 C51 100(4) . .
Nd3 C49 C50 C51 5(6) . .
C49 C50 C51 C52 57(10) . .
C50 C51 C52 C53 -33(8) . .
C50 C51 C52 C54 35(8) . .
C51 C52 C53 C54 107.0(7) . .
C51 C52 C54 C53 -108.3(7) . .
C49 N5 C55 C56 -149.1(4) . .
Nd3 N5 C55 C56 21.2(7) . .
C49 N5 C55 C60 89.0(5) . .
Nd3 N5 C55 C60 -100.8(6) . .
N5 C55 C56 C57 -179.0(4) . .
C60 C55 C56 C57 -56.9(5) . .
C55 C56 C57 C58 56.4(6) . .
C56 C57 C58 C59 -54.9(6) . .
C57 C58 C59 C60 54.0(6) . .
C58 C59 C60 C55 -56.3(6) . .
N5 C55 C60 C59 -179.6(4) . .
C56 C55 C60 C59 58.0(5) . .
C49 N6 C61 C62 -156.6(4) . .
Nd3 N6 C61 C62 42.9(6) . .
C49 N6 C61 C66 81.0(5) . .
Nd3 N6 C61 C66 -79.5(6) . .
N6 C61 C62 C63 179.1(4) . .
C66 C61 C62 C63 -57.4(5) . .
C61 C62 C63 C64 56.9(6) . .
C62 C63 C64 C65 -56.0(6) . .
C63 C64 C65 C66 56.3(6) . .
C64 C65 C66 C61 -56.5(6) . .
N6 C61 C66 C65 178.1(4) . .
C62 C61 C66 C65 57.1(5) . .
C73 N7 C67 N8 -176.4(4) . .
Nd4 N7 C67 N8 -7.5(4) . .
C73 N7 C67 C68 4.7(7) . .
Nd4 N7 C67 C68 173.6(4) . .
C73 N7 C67 Nd4 -168.9(4) . .
C79 N8 C67 N7 -176.1(4) . .
Nd4 N8 C67 N7 7.4(4) . .
C79 N8 C67 C68 2.8(7) . .
Nd4 N8 C67 C68 -173.7(4) . .
C79 N8 C67 Nd4 176.5(5) . .
N8 Nd4 C67 N7 -172.0(4) . .
Cl3 Nd4 C67 N7 120.7(3) . .
C86 Nd4 C67 N7 -154.8(3) . .
C85 Nd4 C67 N7 -134.7(3) . .
C88 Nd4 C67 N7 -56.0(3) . .
Cl4 Nd4 C67 N7 42.6(3) . .
C87 Nd4 C67 N7 -163.6(3) . .
C88 Nd4 C67 N7 -107.7(3) 2 .
C85 Nd4 C67 N7 -41.4(4) 2 .
C89 Nd4 C67 N7 -79.2(3) . .
N7 Nd4 C67 N8 172.0(4) . .
Cl3 Nd4 C67 N8 -67.3(3) . .
C86 Nd4 C67 N8 17.2(3) . .
C85 Nd4 C67 N8 37.3(3) . .
C88 Nd4 C67 N8 116.0(3) . .
Cl4 Nd4 C67 N8 -145.4(3) . .
C87 Nd4 C67 N8 8.4(5) . .
C88 Nd4 C67 N8 64.3(3) 2 .
C85 Nd4 C67 N8 130.7(3) 2 .
C89 Nd4 C67 N8 92.9(3) . .
N7 Nd4 C67 C68 -90(3) . .
N8 Nd4 C67 C68 98(4) . .
Cl3 Nd4 C67 C68 31(3) . .
C86 Nd4 C67 C68 116(3) . .
C85 Nd4 C67 C68 136(3) . .
C88 Nd4 C67 C68 -146(3) . .
Cl4 Nd4 C67 C68 -47(4) . .
C87 Nd4 C67 C68 107(3) . .
C88 Nd4 C67 C68 163(3) 2 .
C85 Nd4 C67 C68 -131(3) 2 .
C89 Nd4 C67 C68 -169(3) . .
N7 C67 C68 C69 115(11) . .
N8 C67 C68 C69 -64(11) . .
Nd4 C67 C68 C69 -159(9) . .
C67 C68 C69 C70 41(23) . .
C68 C69 C70 C72 45(15) . .
C68 C69 C70 C71 -22(15) . .
C69 C70 C71 C72 109.3(7) . .
C69 C70 C72 C71 -106.0(7) . .
C67 N7 C73 C74 -150.1(4) . .
Nd4 N7 C73 C74 48.4(6) . .
C67 N7 C73 C78 87.5(5) . .
Nd4 N7 C73 C78 -74.0(6) . .
N7 C73 C74 C75 -178.1(4) . .
C78 C73 C74 C75 -55.0(5) . .
C73 C74 C75 C76 54.5(6) . .
C74 C75 C76 C77 -54.6(5) . .
C75 C76 C77 C78 56.8(5) . .
C76 C77 C78 C73 -57.1(5) . .
N7 C73 C78 C77 177.3(4) . .
C74 C73 C78 C77 55.9(5) . .
C67 N8 C79 C84 86.2(5) . .
Nd4 N8 C79 C84 -100.0(6) . .
C67 N8 C79 C80 -153.0(4) . .
Nd4 N8 C79 C80 20.8(8) . .
N8 C79 C80 C81 -175.9(5) . .
C84 C79 C80 C81 -54.6(6) . .
C79 C80 C81 C82 55.3(7) . .
C80 C81 C82 C83 -55.1(7) . .
C81 C82 C83 C84 55.5(7) . .
N8 C79 C84 C83 176.0(5) . .
C80 C79 C84 C83 55.7(6) . .
C82 C83 C84 C79 -56.8(7) . .
N7 Nd4 C85 C86 -168.9(2) . .
N8 Nd4 C85 C86 -129.1(3) . .
Cl3 Nd4 C85 C86 -46.6(3) . .
C88 Nd4 C85 C86 101.7(3) . .
C67 Nd4 C85 C86 -145.7(3) . .
Cl4 Nd4 C85 C86 39.1(4) . .
C87 Nd4 C85 C86 20.2(2) . .
C88 Nd4 C85 C86 145.0(4) 2 .
C85 Nd4 C85 C86 72.9(3) 2 .
C89 Nd4 C85 C86 126.0(3) . .
N7 Nd4 C85 C88 46.1(3) . 2
N8 Nd4 C85 C88 85.9(3) . 2
Cl3 Nd4 C85 C88 168.4(2) . 2
C86 Nd4 C85 C88 -145.0(4) . 2
C88 Nd4 C85 C88 -43.3(3) . 2
C67 Nd4 C85 C88 69.2(3) . 2
Cl4 Nd4 C85 C88 -105.9(3) . 2
C87 Nd4 C85 C88 -124.8(3) . 2
C85 Nd4 C85 C88 -72.1(3) 2 2
C89 Nd4 C85 C88 -19.0(2) . 2
N7 Nd4 C85 Nd4 118.12(15) . 2
N8 Nd4 C85 Nd4 157.98(17) . 2
Cl3 Nd4 C85 Nd4 -119.56(12) . 2
C86 Nd4 C85 Nd4 -72.9(3) . 2
C88 Nd4 C85 Nd4 28.73(14) . 2
C67 Nd4 C85 Nd4 141.32(14) . 2
Cl4 Nd4 C85 Nd4 -33.8(3) . 2
C87 Nd4 C85 Nd4 -52.78(13) . 2
C88 Nd4 C85 Nd4 72.1(3) 2 2
C85 Nd4 C85 Nd4 -0.1(2) 2 2
C89 Nd4 C85 Nd4 53.06(13) . 2
C88 C85 C86 C87 -1.3(10) 2 .
Nd4 C85 C86 C87 -53.9(5) . .
Nd4 C85 C86 C87 49.9(5) 2 .
C88 C85 C86 Nd4 52.7(6) 2 .
Nd4 C85 C86 Nd4 103.79(11) 2 .
C88 C85 C86 Nd4 -51.1(6) 2 2
Nd4 C85 C86 Nd4 -103.79(11) . 2
N7 Nd4 C86 C87 163.5(3) . .
N8 Nd4 C86 C87 -164.4(3) . .
Cl3 Nd4 C86 C87 -81.5(2) . .
C85 Nd4 C86 C87 144.2(4) . .
C88 Nd4 C86 C87 72.1(3) . .
C67 Nd4 C86 C87 -172.5(2) . .
Cl4 Nd4 C86 C87 -12.3(3) . .
C88 Nd4 C86 C87 124.4(3) 2 .
C85 Nd4 C86 C87 43.7(3) 2 .
C89 Nd4 C86 C87 100.7(3) . .
N7 Nd4 C86 C85 19.4(4) . .
N8 Nd4 C86 C85 51.4(3) . .
Cl3 Nd4 C86 C85 134.3(3) . .
C88 Nd4 C86 C85 -72.0(3) . .
C67 Nd4 C86 C85 43.4(3) . .
Cl4 Nd4 C86 C85 -156.5(2) . .
C87 Nd4 C86 C85 -144.2(4) . .
C88 Nd4 C86 C85 -19.8(3) 2 .
C85 Nd4 C86 C85 -100.5(3) 2 .
C89 Nd4 C86 C85 -43.4(3) . .
N7 Nd4 C86 Nd4 91.4(3) . 2
N8 Nd4 C86 Nd4 123.46(15) . 2
Cl3 Nd4 C86 Nd4 -153.67(14) . 2
C85 Nd4 C86 Nd4 72.0(3) . 2
C88 Nd4 C86 Nd4 0.00(15) . 2
C67 Nd4 C86 Nd4 115.37(16) . 2
Cl4 Nd4 C86 Nd4 -84.47(15) . 2
C87 Nd4 C86 Nd4 -72.1(3) . 2
C88 Nd4 C86 Nd4 52.22(15) 2 2
C85 Nd4 C86 Nd4 -28.49(15) 2 2
C89 Nd4 C86 Nd4 28.57(11) . 2
C85 C86 C87 C86 1.5(5) . 2
Nd4 C86 C87 C86 -52.06(8) . 2
Nd4 C86 C87 C86 51.39(8) 2 2
C85 C86 C87 Nd4 53.5(5) . .
Nd4 C86 C87 Nd4 103.45(12) 2 .
C85 C86 C87 Nd4 -49.9(5) . 2
Nd4 C86 C87 Nd4 -103.45(12) . 2
N7 Nd4 C87 C86 -93.9(7) . .
N8 Nd4 C87 C86 19.6(3) . .
Cl3 Nd4 C87 C86 93.7(2) . .
C85 Nd4 C87 C86 -20.4(3) . .
C88 Nd4 C87 C86 -101.7(3) . .
C67 Nd4 C87 C86 14.6(5) . .
Cl4 Nd4 C87 C86 169.6(2) . .
C88 Nd4 C87 C86 -44.8(3) 2 .
C85 Nd4 C87 C86 -125.5(3) 2 .
C89 Nd4 C87 C86 -73.2(2) . .
N7 Nd4 C87 C86 50.8(8) . 2
N8 Nd4 C87 C86 164.3(2) . 2
Cl3 Nd4 C87 C86 -121.6(3) . 2
C86 Nd4 C87 C86 144.7(4) . 2
C85 Nd4 C87 C86 124.3(3) . 2
C88 Nd4 C87 C86 43.0(3) . 2
C67 Nd4 C87 C86 159.3(3) . 2
Cl4 Nd4 C87 C86 -45.7(3) . 2
C88 Nd4 C87 C86 99.9(3) 2 2
C85 Nd4 C87 C86 19.2(3) 2 2
C89 Nd4 C87 C86 71.5(3) . 2
N7 Nd4 C87 Nd4 -20.7(7) . 2
N8 Nd4 C87 Nd4 92.79(14) . 2
Cl3 Nd4 C87 Nd4 166.91(2) . 2
C86 Nd4 C87 Nd4 73.2(2) . 2
C85 Nd4 C87 Nd4 52.82(13) . 2
C88 Nd4 C87 Nd4 -28.46(10) . 2
C67 Nd4 C87 Nd4 87.8(3) . 2
Cl4 Nd4 C87 Nd4 -117.19(3) . 2
C88 Nd4 C87 Nd4 28.36(10) 2 2
C85 Nd4 C87 Nd4 -52.30(14) 2 2
C89 Nd4 C87 Nd4 0.0 . 2
N7 Nd4 C88 C89 -77.3(3) . .
N8 Nd4 C88 C89 -23.7(3) . .
Cl3 Nd4 C88 C89 132.1(2) . .
C86 Nd4 C88 C89 73.2(3) . .
C85 Nd4 C88 C89 44.5(3) . .
C67 Nd4 C88 C89 -54.3(3) . .
Cl4 Nd4 C88 C89 -163.7(3) . .
C87 Nd4 C88 C89 101.7(3) . .
C88 Nd4 C88 C89 20.4(3) 2 .
C85 Nd4 C88 C89 144.5(4) 2 .
N7 Nd4 C88 C85 138.2(3) . 2
N8 Nd4 C88 C85 -168.2(3) . 2
Cl3 Nd4 C88 C85 -12.4(4) . 2
C86 Nd4 C88 C85 -71.3(3) . 2
C85 Nd4 C88 C85 -100.0(3) . 2
C67 Nd4 C88 C85 161.2(3) . 2
Cl4 Nd4 C88 C85 51.7(3) . 2
C87 Nd4 C88 C85 -42.9(3) . 2
C88 Nd4 C88 C85 -124.2(3) 2 2
C89 Nd4 C88 C85 -144.5(4) . 2
N7 Nd4 C88 Nd4 -150.49(14) . 2
N8 Nd4 C88 Nd4 -96.90(17) . 2
Cl3 Nd4 C88 Nd4 58.9(2) . 2
C86 Nd4 C88 Nd4 0.00(15) . 2
C85 Nd4 C88 Nd4 -28.72(14) . 2
C67 Nd4 C88 Nd4 -127.50(14) . 2
Cl4 Nd4 C88 Nd4 123.07(12) . 2
C87 Nd4 C88 Nd4 28.43(10) . 2
C88 Nd4 C88 Nd4 -52.85(17) 2 2
C85 Nd4 C88 Nd4 71.3(3) 2 2
C89 Nd4 C88 Nd4 -73.2(3) . 2
C85 C88 C89 C88 1.8(5) 2 2
Nd4 C88 C89 C88 -51.60(8) . 2
Nd4 C88 C89 C88 51.44(8) 2 2
C85 C88 C89 Nd4 53.3(5) 2 .
Nd4 C88 C89 Nd4 103.04(12) 2 .
C85 C88 C89 Nd4 -49.7(5) 2 2
Nd4 C88 C89 Nd4 -103.04(12) . 2
N7 Nd4 C89 C88 -111.1(3) . 2
N8 Nd4 C89 C88 -55.7(3) . 2
Cl3 Nd4 C89 C88 37.6(3) . 2
C86 Nd4 C89 C88 43.2(3) . 2
C85 Nd4 C89 C88 19.2(2) . 2
C88 Nd4 C89 C88 143.9(4) . 2
C67 Nd4 C89 C88 -83.8(3) . 2
Cl4 Nd4 C89 C88 162.3(2) . 2
C87 Nd4 C89 C88 71.8(2) . 2
C85 Nd4 C89 C88 123.8(3) 2 2
N7 Nd4 C89 C88 105.0(3) . .
N8 Nd4 C89 C88 160.5(3) . .
Cl3 Nd4 C89 C88 -106.3(2) . .
C86 Nd4 C89 C88 -100.7(3) . .
C85 Nd4 C89 C88 -124.7(3) . .
C67 Nd4 C89 C88 132.3(3) . .
Cl4 Nd4 C89 C88 18.4(3) . .
C87 Nd4 C89 C88 -72.1(3) . .
C88 Nd4 C89 C88 -143.9(4) 2 .
C85 Nd4 C89 C88 -20.1(3) 2 .
N7 Nd4 C89 Nd4 177.18(9) . 2
N8 Nd4 C89 Nd4 -127.41(9) . 2
Cl3 Nd4 C89 Nd4 -34.13(13) . 2
C86 Nd4 C89 Nd4 -28.53(11) . 2
C85 Nd4 C89 Nd4 -52.57(13) . 2
C88 Nd4 C89 Nd4 72.1(3) . 2
C67 Nd4 C89 Nd4 -155.55(9) . 2
Cl4 Nd4 C89 Nd4 90.57(6) . 2
C87 Nd4 C89 Nd4 0.0 . 2
C88 Nd4 C89 Nd4 -71.8(2) 2 2
C85 Nd4 C89 Nd4 52.06(14) 2 2
C106 C101 C102 C103 0.4(10) . .
C107 C101 C102 C103 -179.8(7) . .
C101 C102 C103 C104 1.6(12) . .
C102 C103 C104 C105 -2.9(14) . .
C103 C104 C105 C106 2.2(14) . .
C102 C101 C106 C105 -1.1(10) . .
C107 C101 C106 C105 179.1(7) . .
C104 C105 C106 C101 -0.2(13) . .
