#------------------------------------------------------------------------------
#$Date: 2016-08-07 12:09:17 +0300 (Sun, 07 Aug 2016) $
#$Revision: 185452 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/03/98/7039817.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7039817
loop_
_publ_author_name
'Wang, Xiuli'
'Sun, Junjun'
'Lin, Hongyan'
'Chang, Zhihan'
'Wang, Xiang'
'Liu, Guocheng'
_publ_section_title
;
 A series of Anderson-type polyoxometalate-based metal-organic complexes:
 their pH-dependent electrochemical behaviour, and as electrocatalysts and
 photocatalysts.
;
_journal_issue                   31
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              12465
_journal_page_last               12478
_journal_paper_doi               10.1039/c6dt02216b
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C32 H60 Cu3 Mo6 N8 O40 Te'
_chemical_formula_weight         2090.74
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2016-06-20 deposited with the CCDC.
2016-07-06 downloaded from the CCDC.
;
_cell_angle_alpha                102.275(2)
_cell_angle_beta                 104.021(2)
_cell_angle_gamma                97.420(2)
_cell_formula_units_Z            1
_cell_length_a                   8.4320(7)
_cell_length_b                   12.9540(12)
_cell_length_c                   15.0230(14)
_cell_measurement_reflns_used    5460
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      28.3311
_cell_measurement_theta_min      2.4441
_cell_volume                     1527.1(2)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0160
_diffrn_reflns_av_unetI/netI     0.0273
_diffrn_reflns_Laue_measured_fraction_full 0.992
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            8695
_diffrn_reflns_point_group_measured_fraction_full 0.992
_diffrn_reflns_point_group_measured_fraction_max 0.992
_diffrn_reflns_theta_full        24.998
_diffrn_reflns_theta_max         24.998
_diffrn_reflns_theta_min         1.890
_diffrn_source                   'sealed tube'
_exptl_absorpt_coefficient_mu    2.787
_exptl_absorpt_correction_T_max  0.606
_exptl_absorpt_correction_T_min  0.422
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'ABSCOR by T.Higashi    8  March, 1995'
_exptl_crystal_colour            BLUE
_exptl_crystal_density_diffrn    2.273
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       BLOCK
_exptl_crystal_F_000             1019
_exptl_crystal_size_max          0.350
_exptl_crystal_size_mid          0.270
_exptl_crystal_size_min          0.180
_refine_diff_density_max         1.316
_refine_diff_density_min         -0.596
_refine_diff_density_rms         0.129
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.004
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     411
_refine_ls_number_reflns         5323
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.004
_refine_ls_R_factor_all          0.0366
_refine_ls_R_factor_gt           0.0308
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0515P)²+4.7925P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0868
_refine_ls_wR_factor_ref         0.0898
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4632
_reflns_number_total             5364
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c6dt02216b2.cif
_cod_data_source_block           complex6
_cod_depositor_comments
'Adding full bibliography for 7039813--7039819.cif.'
_cod_database_code               7039817
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.442
_shelx_estimated_absorpt_t_max   0.634
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Te1 Te 0.0000 0.0000 0.0000 0.01091(11) Uani 1 2 d S . P
Mo1 Mo -0.18644(4) 0.10236(3) -0.16837(3) 0.01427(11) Uani 1 1 d . . .
Cu1 Cu 0.0000 0.5000 0.0000 0.01919(18) Uani 1 2 d S . P
O1 O -0.0996(4) 0.3402(3) 0.0280(2) 0.0235(7) Uani 1 1 d . . .
O1W O -0.0069(4) 0.5633(3) 0.1328(2) 0.0285(8) Uani 1 1 d . . .
H1WA H 0.0043 0.6285 0.1630 0.034 Uiso 1 1 d R U .
H1WB H -0.0159 0.5242 0.1707 0.034 Uiso 1 1 d R U .
N1 N -0.2302(5) 0.5248(3) -0.0483(3) 0.0231(9) Uani 1 1 d . . .
C1 C -0.4249(7) 0.6418(4) -0.0471(4) 0.0390(14) Uani 1 1 d . . .
H1A H -0.4480 0.7088 -0.0233 0.047 Uiso 1 1 calc R U .
Mo2 Mo -0.14808(4) 0.21826(3) 0.05210(3) 0.01397(11) Uani 1 1 d . . .
Cu2 Cu -0.64074(7) -0.03363(5) -0.26042(4) 0.02601(15) Uani 1 1 d . . .
C2 C -0.7010(9) 0.4134(6) -0.4855(5) 0.0564(18) Uani 1 1 d . . .
H2B H -0.7062 0.4618 -0.5268 0.068 Uiso 1 1 calc R U .
H2A H -0.6547 0.4561 -0.4205 0.068 Uiso 1 1 calc R U .
O2W O -0.7753(4) 0.0767(3) -0.2925(3) 0.0333(8) Uani 1 1 d . . .
H2WB H -0.8770 0.0605 -0.2940 0.040 Uiso 1 1 d R U .
H2WA H -0.7519 0.1444 -0.2849 0.040 Uiso 1 1 d R U .
N2 N -0.6640(5) -0.0978(4) -0.3982(3) 0.0295(10) Uani 1 1 d . . .
O2 O -0.3742(4) 0.0475(3) -0.2520(2) 0.0239(7) Uani 1 1 d . . .
Mo3 Mo 0.05523(4) 0.12457(3) 0.22283(3) 0.01483(11) Uani 1 1 d . . .
N3 N -0.5921(7) 0.3369(5) -0.5084(4) 0.0541(14) Uani 1 1 d . . .
H3B H -0.6182 0.2975 -0.5655 0.065 Uiso 1 1 calc R U .
C3 C -0.7163(10) -0.0445(5) -0.4636(4) 0.0548(18) Uani 1 1 d . . .
H3A H -0.7491 0.0204 -0.4441 0.066 Uiso 1 1 calc R U .
O3W O -0.5259(4) -0.1494(3) -0.2170(3) 0.0340(9) Uani 1 1 d . . .
H3WA H -0.4520 -0.1867 -0.2244 0.041 Uiso 1 1 d R U .
H3WB H -0.5821 -0.1772 -0.1852 0.041 Uiso 1 1 d R U .
O3 O -0.8954(4) -0.1422(3) -0.2737(2) 0.0224(7) Uani 1 1 d . . .
N4 N -0.7585(5) 0.3964(4) -0.2753(3) 0.0349(10) Uani 1 1 d . . .
H4B H -0.7551 0.4631 -0.2752 0.042 Uiso 1 1 calc R U .
C4 C -0.7243(11) -0.0799(6) -0.5576(5) 0.065(2) Uani 1 1 d . . .
H4A H -0.7607 -0.0399 -0.6004 0.077 Uiso 1 1 calc R U .
O4W O -0.6093(5) 0.0378(4) -0.1277(3) 0.0488(12) Uani 1 1 d . . .
H4WB H -0.5211 0.0852 -0.1128 0.059 Uiso 1 1 d R U .
H4WA H -0.6470 0.0440 -0.0796 0.059 Uiso 1 1 d R U .
O4 O -0.1253(4) 0.2259(3) -0.1861(2) 0.0237(7) Uani 1 1 d . . .
C5 C -0.6767(8) -0.1768(6) -0.5869(4) 0.0515(17) Uani 1 1 d . . .
H5A H -0.6867 -0.2057 -0.6506 0.062 Uiso 1 1 calc R U .
O5 O 0.0095(4) 0.1366(2) -0.0315(2) 0.0145(6) Uani 1 1 d . . .
O5W O -0.8765(7) -0.5472(4) -0.7411(3) 0.0648(14) Uani 1 1 d . . .
H5WA H -0.7722 -0.5311 -0.7149 0.078 Uiso 1 1 d R U .
H5WB H -0.9023 -0.6150 -0.7634 0.078 Uiso 1 1 d R U .
C6 C -0.6162(8) -0.2277(6) -0.5217(4) 0.0481(16) Uani 1 1 d . . .
O6 O -0.2963(4) 0.1413(2) -0.0685(2) 0.0183(6) Uani 1 1 d . . .
O6W O -0.8215(8) 0.6045(4) -0.3106(4) 0.0851(19) Uani 1 1 d . . .
H66 H -0.9224 0.5770 -0.3180 0.102 Uiso 1 1 d R U .
H67 H -0.7968 0.6630 -0.2674 0.102 Uiso 1 1 d R U .
O7 O -0.6207(5) 0.2784(3) -0.2131(4) 0.0565(13) Uani 1 1 d . . .
C7 C -0.5457(9) -0.3241(6) -0.5535(4) 0.0509(16) Uani 1 1 d . . .
O8 O 0.2356(4) 0.1804(3) 0.3103(2) 0.0266(8) Uani 1 1 d . . .
C8 C -0.8856(9) 0.2746(6) -0.4384(5) 0.0591(19) Uani 1 1 d . . .
H8A H -0.9822 0.2185 -0.4727 0.07(2) Uiso 1 1 calc R . .
H8B H -0.7884 0.2412 -0.4329 0.08(3) Uiso 1 1 calc R . .
O9 O -0.6125(7) -0.3879(5) -0.6323(3) 0.0777(18) Uani 1 1 d . . .
C9 C -0.3508(6) 0.4472(4) -0.1101(4) 0.0262(11) Uani 1 1 d . . .
H9A H -0.3262 0.3796 -0.1297 0.031 Uiso 1 1 calc R U .
O10 O -0.2951(4) 0.2318(3) 0.1136(2) 0.0227(7) Uani 1 1 d . . .
C10 C -0.5488(7) 0.5626(4) -0.1123(4) 0.0384(13) Uani 1 1 d . . .
H10A H -0.6557 0.5756 -0.1332 0.046 Uiso 1 1 calc R U .
O11 O -0.1796(4) -0.0516(2) -0.1172(2) 0.0148(6) Uani 1 1 d . . .
C11 C -0.5109(6) 0.4633(4) -0.1460(4) 0.0277(11) Uani 1 1 d . . .
O12 O 0.0474(4) 0.2372(2) 0.1582(2) 0.0175(6) Uani 1 1 d . . .
C12 C -0.6355(6) 0.3714(4) -0.2152(4) 0.0341(12) Uani 1 1 d . . .
O13 O -0.1396(4) 0.0521(2) 0.0762(2) 0.0138(6) Uani 1 1 d . . .
C13 C -0.2671(6) 0.6215(4) -0.0173(4) 0.0286(11) Uani 1 1 d . . .
H13A H -0.1838 0.6761 0.0255 0.034 Uiso 1 1 calc R U .
O14 O -0.0402(4) 0.0277(2) -0.2255(2) 0.0172(6) Uani 1 1 d . . .
C14 C -0.9001(7) 0.3174(5) -0.3420(4) 0.0433(14) Uani 1 1 d . . .
H14B H -0.9981 0.3501 -0.3477 0.052 Uiso 1 1 calc R U .
H14A H -0.9192 0.2572 -0.3145 0.052 Uiso 1 1 calc R U .
C15 C -0.8717(9) 0.3548(6) -0.4976(5) 0.0608(19) Uani 1 1 d . . .
H15B H -0.9188 0.3169 -0.5639 0.073 Uiso 1 1 calc R U .
H15A H -0.9395 0.4075 -0.4827 0.073 Uiso 1 1 calc R U .
C16 C -0.6158(8) -0.1874(6) -0.4275(4) 0.0460(16) Uani 1 1 d . . .
H16A H -0.5795 -0.2264 -0.3838 0.055 Uiso 1 1 calc R U .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Te Te -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O13 Te1 O13 180.0 . 2
O13 Te1 O5 85.34(12) . .
O13 Te1 O5 94.66(12) 2 .
O13 Te1 O5 94.66(12) . 2
O13 Te1 O5 85.34(12) 2 2
O5 Te1 O5 180.0 . 2
O13 Te1 O11 94.91(12) . .
O13 Te1 O11 85.09(12) 2 .
O5 Te1 O11 84.81(12) . .
O5 Te1 O11 95.19(12) 2 .
O13 Te1 O11 85.09(12) . 2
O13 Te1 O11 94.91(12) 2 2
O5 Te1 O11 95.19(12) . 2
O5 Te1 O11 84.81(12) 2 2
O11 Te1 O11 180.00(14) . 2
O4 Mo1 O2 105.80(16) . .
O4 Mo1 O14 97.92(14) . .
O2 Mo1 O14 100.75(14) . .
O4 Mo1 O6 101.01(15) . .
O2 Mo1 O6 91.75(14) . .
O14 Mo1 O6 153.52(13) . .
O4 Mo1 O5 92.75(13) . .
O2 Mo1 O5 158.46(13) . .
O14 Mo1 O5 87.12(12) . .
O6 Mo1 O5 73.70(11) . .
O4 Mo1 O11 161.41(13) . .
O2 Mo1 O11 92.15(13) . .
O14 Mo1 O11 73.50(11) . .
O6 Mo1 O11 82.87(12) . .
O5 Mo1 O11 70.71(10) . .
N1 Cu1 N1 180.0 2_565 .
N1 Cu1 O1W 89.22(15) 2_565 2_565
N1 Cu1 O1W 90.78(15) . 2_565
N1 Cu1 O1W 90.78(15) 2_565 .
N1 Cu1 O1W 89.23(15) . .
O1W Cu1 O1W 180.0 2_565 .
N1 Cu1 O1 91.55(14) 2_565 2_565
N1 Cu1 O1 88.44(14) . 2_565
O1W Cu1 O1 84.02(13) 2_565 2_565
O1W Cu1 O1 95.99(13) . 2_565
N1 Cu1 O1 88.44(14) 2_565 .
N1 Cu1 O1 91.56(14) . .
O1W Cu1 O1 95.99(12) 2_565 .
O1W Cu1 O1 84.01(13) . .
O1 Cu1 O1 180.0 2_565 .
Mo2 O1 Cu1 172.63(19) . .
C9 N1 C13 118.6(4) . .
C9 N1 Cu1 121.8(3) . .
C13 N1 Cu1 119.5(3) . .
C13 C1 C10 119.9(5) . .
O1 Mo2 O10 106.08(15) . .
O1 Mo2 O6 99.15(15) . .
O10 Mo2 O6 97.54(14) . .
O1 Mo2 O12 96.80(14) . .
O10 Mo2 O12 98.99(14) . .
O6 Mo2 O12 152.83(13) . .
O1 Mo2 O5 94.57(13) . .
O10 Mo2 O5 158.75(13) . .
O6 Mo2 O5 73.82(11) . .
O12 Mo2 O5 83.13(12) . .
O1 Mo2 O13 163.29(13) . .
O10 Mo2 O13 89.64(13) . .
O6 Mo2 O13 84.02(12) . .
O12 Mo2 O13 74.70(11) . .
O5 Mo2 O13 70.41(10) . .
O4W Cu2 O2W 86.84(18) . .
O4W Cu2 N2 175.94(18) . .
O2W Cu2 N2 91.44(17) . .
O4W Cu2 O3W 88.51(18) . .
O2W Cu2 O3W 172.11(14) . .
N2 Cu2 O3W 93.60(17) . .
O4W Cu2 O2 90.60(14) . .
O2W Cu2 O2 102.47(13) . .
N2 Cu2 O2 86.17(14) . .
O3W Cu2 O2 83.94(13) . .
O4W Cu2 O3 93.50(14) . .
O2W Cu2 O3 86.07(13) . .
N2 Cu2 O3 90.05(14) . .
O3W Cu2 O3 87.86(13) . .
O2 Cu2 O3 170.73(12) . .
N3 C2 C15 110.7(6) . .
C16 N2 C3 116.5(5) . .
C16 N2 Cu2 122.4(4) . .
C3 N2 Cu2 120.8(4) . .
Mo1 O2 Cu2 139.09(18) . .
O8 Mo3 O3 106.52(16) . 2_455
O8 Mo3 O12 98.46(15) . .
O3 Mo3 O12 99.74(14) 2_455 .
O8 Mo3 O14 100.25(15) . 2
O3 Mo3 O14 93.97(14) 2_455 2
O12 Mo3 O14 152.57(13) . 2
O8 Mo3 O11 94.95(14) . 2
O3 Mo3 O11 157.09(13) 2_455 2
O12 Mo3 O11 84.57(12) . 2
O14 Mo3 O11 74.01(11) 2 2
O8 Mo3 O13 163.47(14) . .
O3 Mo3 O13 89.35(13) 2_455 .
O12 Mo3 O13 73.74(11) . .
O14 Mo3 O13 82.83(11) 2 .
O11 Mo3 O13 70.12(10) 2 .
C7 N3 C2 125.2(6) 2_454 .
N2 C3 C4 124.0(7) . .
Mo3 O3 Cu2 134.04(17) 2_455 .
C12 N4 C14 124.0(5) . .
C3 C4 C5 118.1(7) . .
C6 C5 C4 118.5(6) . .
Te1 O5 Mo1 103.79(12) . .
Te1 O5 Mo2 102.28(12) . .
Mo1 O5 Mo2 93.25(11) . .
C5 C6 C16 119.6(6) . .
C5 C6 C7 117.1(6) . .
C16 C6 C7 123.2(6) . .
Mo2 O6 Mo1 114.31(15) . .
O9 C7 N3 123.4(7) . 2_454
O9 C7 C6 120.6(6) . .
N3 C7 C6 116.0(6) 2_454 .
C14 C8 C15 116.6(6) . .
N1 C9 C11 122.8(5) . .
C1 C10 C11 118.8(5) . .
Te1 O11 Mo3 103.77(12) . 2
Te1 O11 Mo1 100.68(12) . .
Mo3 O11 Mo1 93.52(11) 2 .
C10 C11 C9 118.1(5) . .
C10 C11 C12 123.3(5) . .
C9 C11 C12 118.5(5) . .
Mo3 O12 Mo2 116.11(15) . .
O7 C12 N4 124.0(5) . .
O7 C12 C11 119.5(5) . .
N4 C12 C11 116.5(5) . .
Te1 O13 Mo2 101.97(12) . .
Te1 O13 Mo3 100.96(12) . .
Mo2 O13 Mo3 91.03(10) . .
N1 C13 C1 121.6(5) . .
Mo1 O14 Mo3 115.58(14) . 2
N4 C14 C8 116.9(5) . .
C2 C15 C8 116.3(6) . .
N2 C16 C6 123.1(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Te1 O13 1.919(3) .
Te1 O13 1.919(3) 2
Te1 O5 1.923(3) .
Te1 O5 1.923(3) 2
Te1 O11 1.946(3) .
Te1 O11 1.946(3) 2
Mo1 O4 1.712(3) .
Mo1 O2 1.719(3) .
Mo1 O14 1.913(3) .
Mo1 O6 1.958(3) .
Mo1 O5 2.221(3) .
Mo1 O11 2.287(3) .
Cu1 N1 1.994(4) 2_565
Cu1 N1 1.994(4) .
Cu1 O1W 2.007(3) 2_565
Cu1 O1W 2.007(3) .
Cu1 O1 2.293(3) 2_565
Cu1 O1 2.293(3) .
O1 Mo2 1.715(3) .
N1 C9 1.337(6) .
N1 C13 1.343(6) .
C1 C13 1.375(7) .
C1 C10 1.379(8) .
Mo2 O10 1.722(3) .
Mo2 O6 1.911(3) .
Mo2 O12 1.943(3) .
Mo2 O5 2.252(3) .
Mo2 O13 2.264(3) .
Cu2 O4W 1.949(4) .
Cu2 O2W 2.002(4) .
Cu2 N2 2.011(4) .
Cu2 O3W 2.024(4) .
Cu2 O2 2.317(3) .
Cu2 O3 2.350(3) .
C2 N3 1.478(8) .
C2 C15 1.487(10) .
N2 C16 1.303(7) .
N2 C3 1.339(8) .
Mo3 O8 1.704(3) .
Mo3 O3 1.720(3) 2_455
Mo3 O12 1.916(3) .
Mo3 O14 1.969(3) 2
Mo3 O11 2.222(3) 2
Mo3 O13 2.324(3) .
N3 C7 1.354(8) 2_454
C3 C4 1.371(9) .
O3 Mo3 1.720(3) 2_455
N4 C12 1.324(7) .
N4 C14 1.465(7) .
C4 C5 1.381(10) .
C5 C6 1.332(9) .
C6 C16 1.399(8) .
C6 C7 1.489(9) .
O7 C12 1.234(7) .
C7 O9 1.241(8) .
C7 N3 1.354(8) 2_454
C8 C14 1.478(9) .
C8 C15 1.515(11) .
C9 C11 1.388(7) .
C10 C11 1.386(7) .
O11 Mo3 2.222(3) 2
C11 C12 1.491(7) .
O14 Mo3 1.969(3) 2
