#------------------------------------------------------------------------------
#$Date: 2019-11-17 13:00:14 +0200 (Sun, 17 Nov 2019) $
#$Revision: 230013 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/04/73/7047340.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7047340
loop_
_publ_author_name
'Xu, Qiaofei'
'Li, Yingguang'
'Ban, Ran'
'Li, Zhao'
'Han, Xiao'
'Ma, Pengtao'
'Singh, Vikram'
'Wang, Jingping'
'Niu, Jingyang'
_publ_section_title
;
 Polyoxotungstates incorporated organophosphonate and nickel: synthesis,
 characterization and efficient catalysis for epoxidation of allylic
 alcohols.
;
_journal_issue                   38
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              13479
_journal_page_last               13486
_journal_paper_doi               10.1039/c8dt02590h
_journal_volume                  47
_journal_year                    2018
_chemical_absolute_configuration unk
_chemical_formula_moiety
'0.33(C54 H72 As6 K42 N18 Ni9 O276 P18 W36), 4(O)'
_chemical_formula_sum            'C18 H24 As2 K14 N6 Ni3 O96 P6 W12'
_chemical_formula_weight         5125.82
_space_group_crystal_system      trigonal
_space_group_IT_number           150
_space_group_name_Hall           'P 3 2"'
_space_group_name_H-M_alt        'P 3 2 1'
_symmetry_space_group_name_Hall  'P 3 2"'
_symmetry_space_group_name_H-M   'P 3 2 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_audit_creation_date             2017-03-13
_audit_creation_method
;
Olex2 1.2-beta
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
;
_audit_update_record
;
2018-06-23 deposited with the CCDC.
2018-08-23 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            3
_cell_length_a                   22.6407(11)
_cell_length_b                   22.6407(11)
_cell_length_c                   19.7106(10)
_cell_measurement_reflns_used    9941
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      26.70
_cell_measurement_theta_min      2.31
_cell_volume                     8750.0(7)
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL-2014/7 (Sheldrick, 2008)'
_computing_structure_solution    'ShelXS-1997 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0581
_diffrn_reflns_av_unetI/netI     0.0510
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -27
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            45446
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        25.098
_diffrn_reflns_theta_max         25.098
_diffrn_reflns_theta_min         1.038
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    13.507
_exptl_absorpt_correction_T_max  0.7457
_exptl_absorpt_correction_T_min  0.3707
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.1683 before and 0.0631 after correction.
The Ratio of minimum to maximum transmission is 0.4971.
The λ/2 correction factor is 0.0015.
;
_exptl_crystal_colour            blue
_exptl_crystal_colour_primary    blue
_exptl_crystal_density_diffrn    2.918
_exptl_crystal_description       block
_exptl_crystal_F_000             7008
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.18
_refine_diff_density_max         2.286
_refine_diff_density_min         -1.337
_refine_diff_density_rms         0.270
_refine_ls_abs_structure_details
;
 Flack x determined using 3881 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   0.018(6)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.039
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     402
_refine_ls_number_reflns         10385
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.039
_refine_ls_R_factor_all          0.0505
_refine_ls_R_factor_gt           0.0418
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0449P)²+169.1959P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1018
_refine_ls_wR_factor_ref         0.1067
_reflns_Friedel_coverage         0.847
_reflns_Friedel_fraction_full    0.997
_reflns_Friedel_fraction_max     0.997
_reflns_number_gt                9330
_reflns_number_total             10385
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c8dt02590h2.cif
_cod_data_source_block           njy1
_cod_depositor_comments
'Adding full bibliography for 7047340--7047342.cif.'
_cod_original_cell_volume        8750.0(10)
_cod_database_code               7047340
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.195
_shelx_estimated_absorpt_t_min   0.088
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H,H) groups
2. Others
 Fixed Sof: K4(0.5) K5(0.5) K6(0.5) K7(0.5) K8(0.5) K9(0.5) K10(0.5) K11(0.5)
 K12(0.5) K13(0.5) K14(0.6) K15(0.4)
3.a Secondary CH2 refined with riding coordinates:
 C1(H1A,H1B), C2(H2A,H2B), C4(H4A,H4B), C5(H5A,H5B), C7(H7A,H7B), C8(H8A,H8B)
;
_shelx_shelxl_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'y, x, -z'
'x-y, -y, -z'
'-x, -x+y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
W1 W 0.82877(4) 0.35688(4) 0.53553(4) 0.0197(2) Uani 1 1 d . . . . .
W2 W 0.69986(4) 0.19959(4) 0.53738(4) 0.01990(19) Uani 1 1 d . . . . .
W3 W 0.84266(5) 0.42219(5) 1.11514(4) 0.0271(2) Uani 1 1 d . . . . .
W4 W 0.76302(5) 0.25536(5) 1.11745(4) 0.0285(2) Uani 1 1 d . . . . .
W5 W 0.87662(4) 0.04574(4) 1.21283(4) 0.01884(19) Uani 1 1 d . . . . .
W6 W 0.82877(4) -0.11608(4) 1.21372(4) 0.01960(19) Uani 1 1 d . . . . .
As1 As 0.6667 0.3333 0.58945(17) 0.0167(7) Uani 1 3 d S T P . .
As2 As 0.6667 0.3333 1.06169(17) 0.0221(8) Uani 1 3 d S T P . .
As3 As 1.0000 0.0000 1.26894(15) 0.0126(7) Uani 1 3 d S T P A .
Ni1 Ni 0.83916(14) 0.29803(15) 0.82630(13) 0.0227(6) Uani 1 1 d . . . . .
Ni2 Ni 0.80313(16) 0.0000 1.5000 0.0173(7) Uani 1 2 d S T P . .
P1 P 0.7799(3) 0.2724(3) 0.6841(3) 0.0219(11) Uani 1 1 d . . . . .
P2 P 0.8232(3) 0.3384(3) 0.9686(3) 0.0293(14) Uani 1 1 d . . . . .
P3 P 0.8278(3) -0.0393(3) 1.3610(3) 0.0221(11) Uani 1 1 d . . . . .
K1 K 1.0000 0.0000 1.1000(5) 0.055(3) Uani 1 3 d S T P A .
K2 K 0.6667 0.3333 0.2293(4) 0.042(2) Uani 1 3 d S T P . .
K3 K 0.6667 0.3333 0.4218(4) 0.047(3) Uani 1 3 d S T P . .
K4 K 0.9585(5) 0.5438(5) 1.2393(5) 0.023(2) Uiso 0.5 1 d . . . . .
K5 K 0.8143(6) 0.1021(6) 1.0713(6) 0.035(2) Uiso 0.5 1 d . . . A .
K6 K 0.9540(7) 0.4076(8) 0.4051(7) 0.043(3) Uiso 0.5 1 d . . . . .
K7 K 0.9616(9) 0.4370(10) 0.4099(9) 0.065(5) Uiso 0.5 1 d . . . . .
K8 K 0.2457(10) 0.4696(9) 0.6638(9) 0.060(5) Uiso 0.5 1 d . . . . .
K9 K 0.2261(10) 0.4741(9) 0.6526(9) 0.064(5) Uiso 0.5 1 d . . . . .
K10 K 0.1494(8) 0.6017(8) 0.2901(8) 0.058(4) Uiso 0.5 1 d . . . . .
K11 K 0.1818(9) 0.6162(9) 0.2650(9) 0.068(4) Uiso 0.5 1 d . . . . .
K12 K 0.3024(8) 0.0875(8) 0.2678(8) 0.060(4) Uiso 0.5 1 d . . . . .
K13 K 0.1364(8) 0.0328(8) 0.4140(8) 0.063(4) Uiso 0.5 1 d . . . . .
K14 K 0.6708(8) 0.1555(8) 0.9532(8) 0.077(4) Uiso 0.6 1 d . . . A 1
K15 K 0.6727(12) 0.2215(13) 0.9078(12) 0.083(6) Uiso 0.4 1 d . . . A 2
O1 O 0.8214(8) 0.3652(8) 0.4485(8) 0.032(4) Uiso 1 1 d . . . . .
O2 O 0.8337(8) 0.4023(8) 1.0060(8) 0.034(4) Uiso 1 1 d . . . . .
O3 O 0.7166(8) 0.2200(8) 0.6462(8) 0.030(4) Uiso 1 1 d . . . . .
O4 O 0.8359(9) 0.4289(9) 1.2005(8) 0.040(4) Uiso 1 1 d . . . . .
O5 O 0.6867(8) 0.1995(9) 0.4508(9) 0.036(4) Uiso 1 1 d . . . . .
O6 O 0.8177(7) 0.3385(7) 0.6437(7) 0.024(3) Uiso 1 1 d . . . . .
O7 O 0.7457(9) 0.2533(9) 1.2033(8) 0.042(4) Uiso 1 1 d . . . . .
O8 O 0.9056(8) 0.3957(8) 0.7922(8) 0.031(4) Uiso 1 1 d . . . . .
O9 O 0.9145(9) 0.3849(9) 0.5438(8) 0.035(4) Uiso 1 1 d . . . . .
O10 O 0.8034(8) 0.4756(8) 1.0876(8) 0.033(4) Uiso 1 1 d . . . . .
O11 O 0.7778(8) 0.2744(8) 1.0087(8) 0.035(4) Uiso 1 1 d . . . . .
O12 O 0.7155(7) 0.3052(7) 0.5427(6) 0.017(3) Uiso 1 1 d . . . . .
O13 O 0.7655(8) 0.2857(8) 0.7541(8) 0.028(4) Uiso 1 1 d . . . . .
O14 O 0.7968(7) 0.2595(7) 0.5350(7) 0.021(3) Uiso 1 1 d . . . . .
O15 O 0.8261(8) 0.4352(8) 0.5663(8) 0.027(4) Uiso 1 1 d . . . . .
O16 O 0.7830(10) 0.1991(10) 0.8620(9) 0.044(4) Uiso 1 1 d . . . . .
O17 O 0.7982(8) 0.3365(8) 0.8969(8) 0.029(4) Uiso 1 1 d . . . . .
O18 O 0.8477(9) 0.3394(9) 1.1193(8) 0.035(4) Uiso 1 1 d . . . . .
O19 O 0.7358(8) 0.3358(7) 1.1091(7) 0.024(3) Uiso 1 1 d . . . . .
O20 O 0.6966(9) 0.1222(8) 0.5491(8) 0.035(4) Uiso 1 1 d . . . . .
O21 O 0.7960(11) 0.2017(11) 1.1114(9) 0.053(5) Uiso 1 1 d . . . . .
O22 O 0.9287(10) 0.4813(10) 1.1036(9) 0.044(5) Uiso 1 1 d . . . . .
O23 O 0.9897(12) 0.4565(12) 0.7196(12) 0.069(7) Uiso 1 1 d . . . . .
O24 O 0.7840(14) 0.1271(14) 0.9391(13) 0.078(7) Uiso 1 1 d . . . . .
O25 O 0.8933(8) 0.0499(8) 1.1257(8) 0.028(4) Uiso 1 1 d . . . . .
O26 O 0.8423(8) -0.1175(8) 1.1269(7) 0.026(3) Uiso 1 1 d . . . . .
O27 O 0.8645(7) 0.0272(7) 1.3217(7) 0.024(3) Uiso 1 1 d . . . . .
O28 O 0.9244(7) -0.0185(7) 1.2232(7) 0.018(3) Uiso 1 1 d . . . . .
O29 O 0.9628(7) 0.1177(7) 1.2426(7) 0.020(3) Uiso 1 1 d . . . . .
O30 O 0.8290(8) -0.0985(8) 1.3230(7) 0.028(3) Uiso 1 1 d . . . . .
O31 O 0.8299(8) 0.0876(8) 1.2167(8) 0.032(4) Uiso 1 1 d . . . . .
O32 O 0.8438(7) 0.0959(8) 1.4579(8) 0.026(3) Uiso 1 1 d . . . . .
O33 O 0.8028(7) -0.0478(7) 1.2102(7) 0.019(3) Uiso 1 1 d . . . . .
O34 O 0.8532(7) -0.0314(8) 1.4331(7) 0.026(3) Uiso 1 1 d . . . . .
O35 O 0.7496(8) -0.1876(9) 1.2246(8) 0.033(4) Uiso 1 1 d . . . . .
O36 O 0.8274(12) 0.1580(12) 1.3862(10) 0.061(6) Uiso 1 1 d . . . . .
N1 N 0.8835(9) 0.2730(9) 0.7484(9) 0.019(4) Uiso 1 1 d . . . . .
N2 N 0.9064(10) 0.3027(10) 0.9029(10) 0.029(4) Uiso 1 1 d . . . . .
N3 N 0.7287(8) -0.0229(9) 1.4219(8) 0.018(4) Uiso 1 1 d . . . . .
C1 C 0.8338(11) 0.2365(11) 0.6960(11) 0.026(5) Uiso 1 1 d . . . . .
H1A H 0.8063 0.1888 0.7086 0.031 Uiso 1 1 calc R . . . .
H1B H 0.8570 0.2389 0.6538 0.031 Uiso 1 1 calc R . . . .
C2 C 0.9427(13) 0.3359(12) 0.7236(13) 0.035(6) Uiso 1 1 d . . . . .
H2A H 0.9839 0.3366 0.7385 0.042 Uiso 1 1 calc R . . . .
H2B H 0.9423 0.3350 0.6744 0.042 Uiso 1 1 calc R . . . .
C3 C 0.9456(13) 0.3991(13) 0.7462(12) 0.032(6) Uiso 1 1 d . . . . .
C4 C 0.9078(13) 0.3509(13) 0.9591(13) 0.035(6) Uiso 1 1 d . . . . .
H4A H 0.9394 0.3980 0.9470 0.042 Uiso 1 1 calc R . . . .
H4B H 0.9228 0.3411 1.0016 0.042 Uiso 1 1 calc R . . . .
C5 C 0.8817(15) 0.2312(15) 0.9237(15) 0.047(7) Uiso 1 1 d . . . . .
H5A H 0.9103 0.2159 0.9026 0.056 Uiso 1 1 calc R . . . .
H5B H 0.8872 0.2303 0.9725 0.056 Uiso 1 1 calc R . . . .
C6 C 0.8150(16) 0.1859(16) 0.9078(14) 0.048(7) Uiso 1 1 d . . . . .
C7 C 0.7396(12) -0.0625(12) 1.3690(12) 0.030(5) Uiso 1 1 d . . . . .
H7A H 0.7236 -0.0552 1.3259 0.036 Uiso 1 1 calc R . . . .
H7B H 0.7128 -0.1106 1.3798 0.036 Uiso 1 1 calc R . . . .
C8 C 0.7385(12) 0.0402(11) 1.3981(12) 0.029(5) Uiso 1 1 d . . . . .
H8A H 0.7028 0.0471 1.4169 0.034 Uiso 1 1 calc R . . . .
H8B H 0.7330 0.0374 1.3492 0.034 Uiso 1 1 calc R . . . .
C9 C 0.8074(11) 0.1028(11) 1.4148(11) 0.023(5) Uiso 1 1 d . . . . .
O1W O 0.2161(12) 0.0429(12) 0.3646(12) 0.067(6) Uiso 1 1 d . . . . .
O2W O 0.0481(12) 0.3500(12) 0.8633(11) 0.064(6) Uiso 1 1 d . . . . .
O3W O 0.6200(12) 0.2290(11) 0.3273(11) 0.064(6) Uiso 1 1 d . . . . .
O4W O 0.9576(13) 0.2014(12) 1.0608(13) 0.072(7) Uiso 1 1 d . . . . .
O5W O 1.0620(14) 0.6442(14) 1.3154(14) 0.087(8) Uiso 1 1 d . . . . .
O6W O 0.1221(13) 0.4542(13) 0.7216(12) 0.074(7) Uiso 1 1 d . . . . .
O7W O 0.9151(14) 0.5159(14) 1.3729(14) 0.084(8) Uiso 1 1 d . . . . .
O8W O 0.8830(14) 0.0646(13) 0.9776(14) 0.084(8) Uiso 1 1 d . . . . .
O9W O 0.1018(15) 0.3265(14) 0.4707(14) 0.085(8) Uiso 1 1 d . . . . .
O10W O 0.8831(15) 0.6075(15) 1.2402(15) 0.096(9) Uiso 1 1 d . . . . .
O11W O 1.0694(17) 0.7336(18) 1.2103(17) 0.111(10) Uiso 1 1 d . . . . .
O12W O 1.0630(19) 0.5772(19) 1.1395(18) 0.127(12) Uiso 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
K6 W1 K3 99.4(2) . .
K6 W1 K7 9.7(3) . .
K6 W1 K10 126.0(3) . 6_656
K7 W1 K3 99.0(3) . .
K7 W1 K10 118.5(4) . 6_656
K10 W1 K3 113.9(2) 6_656 .
O1 W1 K3 49.4(6) . .
O1 W1 K6 50.1(6) . .
O1 W1 K7 51.0(6) . .
O1 W1 K10 142.1(6) . 6_656
O1 W1 O6 169.4(7) . .
O1 W1 O12 88.4(6) . .
O1 W1 O14 96.6(7) . .
O1 W1 O15 99.4(7) . .
O6 W1 K3 120.2(4) . .
O6 W1 K6 140.3(4) . .
O6 W1 K7 139.5(5) . .
O6 W1 K10 38.7(4) . 6_656
O6 W1 O12 81.0(5) . .
O9 W1 K3 150.5(6) . .
O9 W1 K6 51.8(6) . .
O9 W1 K7 51.5(6) . .
O9 W1 K10 84.6(6) . 6_656
O9 W1 O1 101.8(8) . .
O9 W1 O6 88.8(7) . .
O9 W1 O12 167.6(7) . .
O9 W1 O14 97.5(7) . .
O9 W1 O15 100.5(7) . .
O12 W1 K3 41.1(3) . .
O12 W1 K6 137.4(4) . .
O12 W1 K7 139.4(4) . .
O12 W1 K10 91.6(4) . 6_656
O14 W1 K3 92.8(4) . .
O14 W1 K6 98.4(5) . .
O14 W1 K7 108.1(5) . .
O14 W1 K10 119.8(5) . 6_656
O14 W1 O6 81.1(6) . .
O14 W1 O12 74.2(5) . .
O15 W1 K3 81.5(5) . .
O15 W1 K6 108.7(5) . .
O15 W1 K7 99.0(6) . .
O15 W1 K10 43.0(5) . 6_656
O15 W1 O6 79.1(6) . .
O15 W1 O12 84.5(6) . .
O15 W1 O14 152.9(6) . .
K9 W2 K8 7.7(3) 6_656 6_656
K10 W2 K8 165.5(4) 4_556 6_656
K10 W2 K9 171.1(3) 4_556 6_656
O3 W2 K8 155.5(5) . 6_656
O3 W2 K9 148.3(5) . 6_656
O3 W2 K10 38.9(5) . 4_556
O3 W2 O12 79.1(5) . .
O5 W2 K8 24.3(6) . 6_656
O5 W2 K9 29.7(6) . 6_656
O5 W2 K10 141.7(6) . 4_556
O5 W2 O3 168.0(7) . .
O5 W2 O12 89.0(7) . .
O5 W2 O14 96.4(7) . .
O5 W2 O15 97.7(7) . 3_665
O12 W2 K8 91.5(4) . 6_656
O12 W2 K9 86.1(4) . 6_656
O12 W2 K10 91.9(4) . 4_556
O14 W2 K8 73.8(5) . 6_656
O14 W2 K9 67.1(5) . 6_656
O14 W2 K10 120.7(5) . 4_556
O14 W2 O3 81.9(6) . .
O14 W2 O12 74.5(5) . .
O14 W2 O15 153.3(6) . 3_665
O15 W2 K8 122.0(5) 3_665 6_656
O15 W2 K9 126.5(5) 3_665 6_656
O15 W2 K10 44.5(5) 3_665 4_556
O15 W2 O3 79.6(6) 3_665 .
O15 W2 O12 83.3(6) 3_665 .
O20 W2 K8 97.1(6) . 6_656
O20 W2 K9 101.6(6) . 6_656
O20 W2 K10 81.9(6) . 4_556
O20 W2 O3 89.9(7) . .
O20 W2 O5 102.2(8) . .
O20 W2 O12 168.1(6) . .
O20 W2 O14 100.0(7) . .
O20 W2 O15 99.0(7) . 3_665
K4 W3 K2 99.05(18) . 1_556
K4 W3 K14 109.9(3) . 2_655
K14 W3 K2 117.9(2) 2_655 1_556
O2 W3 K2 118.0(4) . 1_556
O2 W3 K4 140.9(5) . .
O2 W3 K14 42.7(5) . 2_655
O2 W3 O19 79.5(6) . .
O4 W3 K2 52.8(6) . 1_556
O4 W3 K4 48.0(6) . .
O4 W3 K14 138.9(6) . 2_655
O4 W3 O2 170.8(7) . .
O4 W3 O10 97.7(8) . .
O4 W3 O18 95.5(8) . .
O4 W3 O19 91.4(7) . .
O4 W3 O22 100.1(8) . .
O10 W3 K2 79.7(5) . 1_556
O10 W3 K4 95.7(5) . .
O10 W3 K14 44.7(6) . 2_655
O10 W3 O2 79.9(7) . .
O10 W3 O18 154.1(8) . .
O10 W3 O19 84.0(6) . .
O18 W3 K2 90.8(5) . 1_556
O18 W3 K4 109.6(5) . .
O18 W3 K14 125.5(5) . 2_655
O18 W3 O2 83.5(6) . .
O18 W3 O19 73.5(6) . .
O19 W3 K2 40.5(4) . 1_556
O19 W3 K4 139.1(4) . .
O19 W3 K14 98.5(4) . 2_655
O22 W3 K2 152.1(6) . 1_556
O22 W3 K4 53.1(6) . .
O22 W3 K14 76.5(6) . 2_655
O22 W3 O2 89.0(7) . .
O22 W3 O10 99.9(8) . .
O22 W3 O18 99.6(8) . .
O22 W3 O19 167.1(7) . .
K14 W4 K2 116.9(2) . 1_556
O7 W4 K2 47.1(6) . 1_556
O7 W4 K14 138.3(7) . .
O7 W4 O10 97.6(8) . 3_665
O7 W4 O11 167.6(7) . .
O7 W4 O18 96.3(8) . .
O7 W4 O19 86.7(7) . .
O10 W4 K2 81.0(5) 3_665 1_556
O10 W4 K14 42.2(6) 3_665 .
O10 W4 O11 80.7(7) 3_665 .
O10 W4 O18 154.0(7) 3_665 .
O10 W4 O19 84.4(6) 3_665 .
O11 W4 K2 120.6(5) . 1_556
O11 W4 K14 44.2(5) . .
O11 W4 O19 80.9(6) . .
O18 W4 K2 92.6(5) . 1_556
O18 W4 K14 124.9(5) . .
O18 W4 O11 81.0(7) . .
O18 W4 O19 74.6(6) . .
O19 W4 K2 41.4(4) . 1_556
O19 W4 K14 97.3(4) . .
O21 W4 K2 149.3(6) . 1_556
O21 W4 K14 80.1(7) . .
O21 W4 O7 102.8(8) . .
O21 W4 O10 100.6(9) . 3_665
O21 W4 O11 89.6(8) . .
O21 W4 O18 97.5(9) . .
O21 W4 O19 168.4(8) . .
K5 W5 K1 96.1(2) . .
K5 W5 K12 77.4(3) . 2_656
K12 W5 K1 127.1(2) 2_656 .
O25 W5 K1 47.4(5) . .
O25 W5 K5 48.6(5) . .
O25 W5 K12 107.7(6) . 2_656
O25 W5 O27 168.5(6) . .
O25 W5 O28 87.9(6) . .
O25 W5 O29 98.9(6) . .
O25 W5 O33 94.5(6) . .
O27 W5 K1 121.6(4) . .
O27 W5 K5 142.2(4) . .
O27 W5 K12 81.4(4) . 2_656
O27 W5 O28 80.7(5) . .
O28 W5 K1 42.6(4) . .
O28 W5 K5 134.8(4) . .
O28 W5 K12 137.3(4) . 2_656
O29 W5 K1 81.2(4) . .
O29 W5 K5 110.4(5) . .
O29 W5 K12 54.3(5) . 2_656
O29 W5 O27 80.7(6) . .
O29 W5 O28 84.6(6) . .
O29 W5 O33 154.1(6) . .
O31 W5 K1 147.2(5) . .
O31 W5 K5 52.7(6) . .
O31 W5 K12 45.1(6) . 2_656
O31 W5 O25 100.8(7) . .
O31 W5 O27 90.5(7) . .
O31 W5 O28 169.7(7) . .
O31 W5 O29 99.4(7) . .
O31 W5 O33 99.8(7) . .
O33 W5 K1 91.9(4) . .
O33 W5 K5 95.1(4) . .
O33 W5 K12 140.5(5) . 2_656
O33 W5 O27 81.9(6) . .
O33 W5 O28 73.8(6) . .
K12 W6 K1 118.8(2) 3_656 .
O26 W6 K1 49.9(5) . .
O26 W6 K12 101.3(5) . 3_656
O26 W6 O28 90.5(6) . .
O26 W6 O29 97.3(6) . 2_645
O26 W6 O30 170.2(6) . .
O26 W6 O33 96.2(6) . .
O28 W6 K1 42.3(4) . .
O28 W6 K12 130.0(4) . 3_656
O29 W6 K1 81.0(4) 2_645 .
O29 W6 K12 46.1(5) 2_645 3_656
O29 W6 O28 84.5(6) 2_645 .
O29 W6 O30 81.1(6) 2_645 .
O29 W6 O33 155.3(6) 2_645 .
O30 W6 K1 120.4(4) . .
O30 W6 K12 84.6(4) . 3_656
O30 W6 O28 79.7(5) . .
O33 W6 K1 92.1(4) . .
O33 W6 K12 148.9(5) . 3_656
O33 W6 O28 74.7(5) . .
O33 W6 O30 82.1(6) . .
O35 W6 K1 151.2(6) . .
O35 W6 K12 51.6(6) . 3_656
O35 W6 O26 102.4(7) . .
O35 W6 O28 166.5(6) . .
O35 W6 O29 97.6(7) . 2_645
O35 W6 O30 87.4(7) . .
O35 W6 O33 99.7(7) . .
O12 As1 K3 58.9(4) 3_665 .
O12 As1 K3 58.9(4) . .
O12 As1 K3 58.9(4) 2_655 .
O12 As1 O12 95.7(6) 3_665 2_655
O12 As1 O12 95.7(6) . 2_655
O12 As1 O12 95.7(6) . 3_665
O19 As2 K2 58.7(5) 2_655 1_556
O19 As2 K2 58.7(5) 3_665 1_556
O19 As2 K2 58.7(5) . 1_556
O19 As2 O19 95.5(6) . 2_655
O19 As2 O19 95.5(6) . 3_665
O19 As2 O19 95.5(6) 3_665 2_655
O28 As3 K1 59.8(4) 2_645 .
O28 As3 K1 59.8(4) 3_765 .
O28 As3 K1 59.8(4) . .
O28 As3 O28 96.9(6) . 3_765
O28 As3 O28 96.9(6) . 2_645
O28 As3 O28 96.9(6) 2_645 3_765
K15 Ni1 K11 94.3(5) . 6_656
O8 Ni1 K11 45.4(5) . 6_656
O8 Ni1 K15 132.7(6) . .
O8 Ni1 O13 91.5(6) . .
O8 Ni1 O16 173.1(7) . .
O8 Ni1 O17 90.4(6) . .
O8 Ni1 N2 93.4(7) . .
O13 Ni1 K11 51.3(5) . 6_656
O13 Ni1 K15 70.8(6) . .
O13 Ni1 N2 175.0(7) . .
O16 Ni1 K11 141.4(6) . 6_656
O16 Ni1 K15 53.5(6) . .
O16 Ni1 O13 93.9(7) . .
O16 Ni1 O17 93.7(7) . .
O16 Ni1 N2 81.3(7) . .
O17 Ni1 K11 73.4(5) . 6_656
O17 Ni1 K15 48.3(6) . .
O17 Ni1 O13 91.1(6) . .
O17 Ni1 N2 87.8(7) . .
N1 Ni1 K11 98.4(6) . 6_656
N1 Ni1 K15 136.7(6) . .
N1 Ni1 O8 81.9(7) . .
N1 Ni1 O13 85.6(6) . .
N1 Ni1 O16 94.3(7) . .
N1 Ni1 O17 171.5(7) . .
N1 Ni1 N2 96.2(7) . .
N2 Ni1 K11 132.7(6) . 6_656
N2 Ni1 K15 104.9(7) . .
K13 Ni2 K13 92.3(5) 2_656 6_657
O32 Ni2 K13 138.3(5) 5_558 2_656
O32 Ni2 K13 50.5(5) . 2_656
O32 Ni2 K13 50.5(5) 5_558 6_657
O32 Ni2 K13 138.3(5) . 6_657
O32 Ni2 O32 170.9(9) 5_558 .
O32 Ni2 O34 92.4(6) . 5_558
O32 Ni2 O34 94.1(6) . .
O32 Ni2 O34 92.4(6) 5_558 .
O32 Ni2 O34 94.1(6) 5_558 5_558
O32 Ni2 N3 81.3(6) . .
O32 Ni2 N3 81.3(6) 5_558 5_558
O32 Ni2 N3 92.6(6) . 5_558
O32 Ni2 N3 92.6(6) 5_558 .
O34 Ni2 K13 68.5(5) . 6_657
O34 Ni2 K13 51.4(5) 5_558 6_657
O34 Ni2 K13 68.5(5) 5_558 2_656
O34 Ni2 K13 51.4(5) . 2_656
O34 Ni2 O34 88.7(8) . 5_558
O34 Ni2 N3 172.5(6) . 5_558
O34 Ni2 N3 87.7(6) . .
O34 Ni2 N3 172.5(6) 5_558 .
O34 Ni2 N3 87.7(6) 5_558 5_558
N3 Ni2 K13 132.5(5) 5_558 2_656
N3 Ni2 K13 132.5(5) . 6_657
N3 Ni2 K13 104.2(5) . 2_656
N3 Ni2 K13 104.2(5) 5_558 6_657
N3 Ni2 N3 96.7(9) 5_558 .
K10 P1 K10 123.1(5) 6_656 4_556
K11 P1 K10 13.0(3) 6_656 6_656
K11 P1 K10 112.3(5) 4_556 6_656
K11 P1 K10 12.6(3) 4_556 4_556
K11 P1 K10 111.5(5) 6_656 4_556
K11 P1 K11 100.1(6) 4_556 6_656
O3 P1 K10 131.7(7) . 6_656
O3 P1 K10 38.3(7) . 4_556
O3 P1 K11 49.6(7) . 4_556
O3 P1 K11 127.3(7) . 6_656
O3 P1 O6 110.9(8) . .
O3 P1 C1 107.4(10) . .
O6 P1 K10 133.8(7) . 4_556
O6 P1 K10 41.2(6) . 6_656
O6 P1 K11 131.2(7) . 4_556
O6 P1 K11 52.6(7) . 6_656
O6 P1 C1 109.9(10) . .
O13 P1 K10 75.6(7) . 4_556
O13 P1 K10 69.9(7) . 6_656
O13 P1 K11 63.9(7) . 4_556
O13 P1 K11 58.7(7) . 6_656
O13 P1 O3 113.4(9) . .
O13 P1 O6 111.0(9) . .
O13 P1 C1 103.9(10) . .
C1 P1 K10 112.6(8) . 4_556
C1 P1 K10 118.6(8) . 6_656
C1 P1 K11 125.2(8) . 6_656
C1 P1 K11 118.5(8) . 4_556
K14 P2 K14 134.4(4) 2_655 .
K15 P2 K15 84.2(9) . 2_655
O2 P2 K14 133.2(7) . .
O2 P2 K14 33.4(6) . 2_655
O2 P2 K15 122.5(8) . .
O2 P2 K15 54.8(7) . 2_655
O2 P2 C4 104.5(11) . .
O11 P2 K14 36.7(7) . .
O11 P2 K14 135.9(7) . 2_655
O11 P2 K15 126.0(8) . 2_655
O11 P2 K15 59.4(8) . .
O11 P2 O2 111.3(9) . .
O11 P2 O17 113.3(9) . .
O11 P2 C4 111.5(11) . .
O17 P2 K14 77.0(7) . .
O17 P2 K14 78.6(7) . 2_655
O17 P2 K15 56.3(7) . 2_655
O17 P2 K15 54.6(8) . .
O17 P2 O2 110.7(9) . .
O17 P2 C4 105.2(11) . .
C4 P2 K14 105.1(9) . 2_655
C4 P2 K14 118.2(9) . .
C4 P2 K15 132.5(9) . .
C4 P2 K15 122.5(10) . 2_655
K13 P3 K13 90.8(5) 2_656 3_656
O27 P3 K13 126.3(7) . 3_656
O27 P3 K13 54.5(6) . 2_656
O27 P3 O30 111.9(8) . .
O27 P3 C7 108.2(10) . .
O30 P3 K13 51.8(6) . 3_656
O30 P3 K13 124.6(7) . 2_656
O30 P3 C7 106.8(10) . .
O34 P3 K13 58.3(7) . 2_656
O34 P3 K13 61.4(7) . 3_656
O34 P3 O27 112.0(9) . .
O34 P3 O30 112.8(9) . .
O34 P3 C7 104.7(10) . .
C7 P3 K13 125.4(9) . 3_656
C7 P3 K13 128.6(8) . 2_656
As3 K1 W5 57.04(11) . .
As3 K1 K1 180.0 . 4_647
K1 K1 W5 122.96(11) 4_647 .
O25 K1 W5 106.8(3) 2_645 .
O25 K1 W5 24.0(3) . .
O25 K1 W5 111.4(3) 3_765 .
O25 K1 As3 80.8(3) . .
O25 K1 As3 80.8(3) 3_765 .
O25 K1 As3 80.8(3) 2_645 .
O25 K1 K1 99.2(3) . 4_647
O25 K1 K1 99.2(3) 2_645 4_647
O25 K1 K1 99.2(3) 3_765 4_647
O25 K1 O25 117.51(17) 3_765 .
O25 K1 O25 117.51(17) 2_645 .
O25 K1 O25 117.51(17) 3_765 2_645
O25 K1 O26 161.0(5) . 2_645
O25 K1 O26 63.1(4) 2_645 2_645
O25 K1 O26 63.1(4) 3_765 3_765
O25 K1 O26 161.1(5) 3_765 .
O25 K1 O26 63.1(4) . .
O25 K1 O26 55.2(4) . 3_765
O25 K1 O26 161.1(5) 2_645 3_765
O25 K1 O26 55.2(4) 2_645 .
O25 K1 O26 55.2(4) 3_765 2_645
O26 K1 W5 137.7(4) 2_645 .
O26 K1 W5 59.0(3) 3_765 .
O26 K1 W5 60.6(3) . .
O26 K1 As3 80.6(3) 3_765 .
O26 K1 As3 80.6(3) 2_645 .
O26 K1 As3 80.6(3) . .
O26 K1 K1 99.4(3) 3_765 4_647
O26 K1 K1 99.4(3) 2_645 4_647
O26 K1 K1 99.4(3) . 4_647
O26 K1 O26 117.41(17) . 3_765
O26 K1 O26 117.41(17) . 2_645
O26 K1 O26 117.41(17) 3_765 2_645
O28 K1 W5 63.3(3) 3_765 .
O28 K1 W5 31.4(3) . .
O28 K1 W5 85.7(3) 2_645 .
O28 K1 As3 32.5(3) 2_645 .
O28 K1 As3 32.5(3) . .
O28 K1 As3 32.5(3) 3_765 .
O28 K1 K1 147.5(3) 3_765 4_647
O28 K1 K1 147.5(3) 2_645 4_647
O28 K1 K1 147.5(3) . 4_647
O28 K1 O25 81.3(4) 2_645 3_765
O28 K1 O25 109.4(5) . 3_765
O28 K1 O25 109.4(5) 2_645 .
O28 K1 O25 81.3(4) . 2_645
O28 K1 O25 54.2(4) 2_645 2_645
O28 K1 O25 54.2(4) 3_765 3_765
O28 K1 O25 109.4(5) 3_765 2_645
O28 K1 O25 81.3(4) 3_765 .
O28 K1 O25 54.2(4) . .
O28 K1 O26 80.9(4) 3_765 2_645
O28 K1 O26 109.4(4) 2_645 3_765
O28 K1 O26 80.9(4) . 3_765
O28 K1 O26 54.2(4) . .
O28 K1 O26 109.4(4) 3_765 .
O28 K1 O26 54.2(4) 3_765 3_765
O28 K1 O26 80.9(4) 2_645 .
O28 K1 O26 54.2(4) 2_645 2_645
O28 K1 O26 109.4(4) . 2_645
O28 K1 O28 55.4(5) 3_765 2_645
O28 K1 O28 55.4(5) . 3_765
O28 K1 O28 55.4(5) . 2_645
As2 K2 O4 80.3(3) 1_554 1_554
As2 K2 O4 80.3(3) 1_554 3_664
O4 K2 O4 117.22(18) 3_664 1_554
O7 K2 As2 80.7(3) 2_654 1_554
O7 K2 As2 80.7(3) 3_664 1_554
O7 K2 As2 80.7(3) 1_554 1_554
O7 K2 O4 54.7(5) 2_654 1_554
O7 K2 O4 160.4(5) 2_654 3_664
O7 K2 O4 63.5(5) 3_664 3_664
O7 K2 O4 54.7(5) 1_554 3_664
O7 K2 O4 63.5(5) 1_554 1_554
O7 K2 O4 160.4(5) 3_664 1_554
O7 K2 O7 117.42(18) 1_554 2_654
O7 K2 O7 117.42(18) 1_554 3_664
O7 K2 O7 117.42(18) 3_664 2_654
O19 K2 As2 33.0(3) 1_554 1_554
O19 K2 As2 33.0(3) 2_654 1_554
O19 K2 As2 33.0(3) 3_664 1_554
O19 K2 O4 53.6(4) 3_664 3_664
O19 K2 O4 80.5(4) 1_554 3_664
O19 K2 O4 53.6(4) 1_554 1_554
O19 K2 O4 109.6(5) 3_664 1_554
O19 K2 O4 80.5(4) 2_654 1_554
O19 K2 O4 109.6(5) 2_654 3_664
O19 K2 O7 109.8(5) 2_654 1_554
O19 K2 O7 53.7(4) 3_664 3_664
O19 K2 O7 53.7(4) 1_554 1_554
O19 K2 O7 109.8(5) 1_554 3_664
O19 K2 O7 109.8(5) 3_664 2_654
O19 K2 O7 81.1(5) 2_654 3_664
O19 K2 O7 81.1(4) 3_664 1_554
O19 K2 O7 53.7(4) 2_654 2_654
O19 K2 O7 81.1(5) 1_554 2_654
O19 K2 O19 56.3(5) 1_554 3_664
O19 K2 O19 56.3(5) 3_664 2_654
O19 K2 O19 56.3(5) 1_554 2_654
O3W K2 As2 133.3(5) 2_655 1_554
O3W K2 As2 133.3(5) 3_665 1_554
O3W K2 As2 133.3(5) . 1_554
O3W K2 O4 117.7(6) 2_655 3_664
O3W K2 O4 53.0(5) . 3_664
O3W K2 O4 118.9(6) . 1_554
O3W K2 O4 117.7(6) 3_665 1_554
O3W K2 O4 118.9(6) 3_665 3_664
O3W K2 O4 53.0(5) 2_655 1_554
O3W K2 O7 73.3(6) 2_655 2_654
O3W K2 O7 145.9(6) 3_665 1_554
O3W K2 O7 78.1(6) . 3_664
O3W K2 O7 73.3(6) . 1_554
O3W K2 O7 78.1(6) 3_665 2_654
O3W K2 O7 73.3(6) 3_665 3_664
O3W K2 O7 78.1(6) 2_655 1_554
O3W K2 O7 145.9(6) . 2_654
O3W K2 O7 145.9(6) 2_655 3_664
O3W K2 O19 103.8(5) . 3_664
O3W K2 O19 103.8(5) 2_655 1_554
O3W K2 O19 124.3(6) . 1_554
O3W K2 O19 157.5(6) 3_665 1_554
O3W K2 O19 157.5(6) 2_655 3_664
O3W K2 O19 103.8(5) 3_665 2_654
O3W K2 O19 157.5(6) . 2_654
O3W K2 O19 124.3(6) 2_655 2_654
O3W K2 O19 124.3(6) 3_665 3_664
O3W K2 O3W 78.1(7) . 3_665
O3W K2 O3W 78.1(7) 2_655 3_665
O3W K2 O3W 78.1(7) 2_655 .
As1 K3 O5 80.1(3) . .
As1 K3 O5 80.1(3) . 2_655
O1 K3 As1 80.7(3) 3_665 .
O1 K3 As1 80.7(3) 2_655 .
O1 K3 As1 80.7(3) . .
O1 K3 O1 117.44(17) 3_665 2_655
O1 K3 O1 117.44(17) . 2_655
O1 K3 O1 117.44(17) . 3_665
O1 K3 O5 63.4(4) . .
O1 K3 O5 160.3(5) 2_655 .
O1 K3 O5 160.3(5) 3_665 2_655
O1 K3 O5 63.4(4) 2_655 2_655
O1 K3 O5 54.8(4) 3_665 .
O1 K3 O5 54.8(4) . 2_655
O5 K3 O5 117.12(19) . 2_655
O12 K3 As1 32.7(3) 2_655 .
O12 K3 As1 32.7(3) 3_665 .
O12 K3 As1 32.7(3) . .
O12 K3 O1 80.9(4) 2_655 .
O12 K3 O1 109.6(4) 2_655 3_665
O12 K3 O1 54.2(4) . .
O12 K3 O1 54.2(4) 3_665 3_665
O12 K3 O1 54.2(4) 2_655 2_655
O12 K3 O1 80.9(4) 3_665 2_655
O12 K3 O1 109.6(4) 3_665 .
O12 K3 O1 80.9(4) . 3_665
O12 K3 O1 109.6(4) . 2_655
O12 K3 O5 53.5(4) . .
O12 K3 O5 108.9(4) 2_655 .
O12 K3 O5 80.7(4) 3_665 .
O12 K3 O5 53.5(4) 2_655 2_655
O12 K3 O5 80.7(4) . 2_655
O12 K3 O5 108.9(5) 3_665 2_655
O12 K3 O12 55.7(5) . 2_655
O12 K3 O12 55.7(5) . 3_665
O12 K3 O12 55.7(5) 3_665 2_655
O3W K3 As1 132.3(5) 3_665 .
O3W K3 As1 132.3(5) 2_655 .
O3W K3 As1 132.3(5) . .
O3W K3 O1 133.3(6) 2_655 3_665
O3W K3 O1 55.5(5) . 3_665
O3W K3 O1 133.3(6) 3_665 .
O3W K3 O1 55.5(5) 2_655 .
O3W K3 O1 102.0(6) . .
O3W K3 O1 102.0(6) 3_665 3_665
O3W K3 O1 55.5(5) 3_665 2_655
O3W K3 O1 102.0(6) 2_655 2_655
O3W K3 O1 133.3(6) . 2_655
O3W K3 O5 140.1(6) 3_665 .
O3W K3 O5 94.1(6) 2_655 .
O3W K3 O5 94.1(6) 3_665 2_655
O3W K3 O5 60.5(6) . .
O3W K3 O5 140.1(6) . 2_655
O3W K3 O5 60.5(6) 2_655 2_655
O3W K3 O12 109.6(5) . 3_665
O3W K3 O12 164.6(6) 2_655 3_665
O3W K3 O12 109.6(5) 3_665 2_655
O3W K3 O12 164.6(6) 3_665 .
O3W K3 O12 109.6(5) 2_655 .
O3W K3 O12 113.6(5) 2_655 2_655
O3W K3 O12 164.6(6) . 2_655
O3W K3 O12 113.6(5) 3_665 3_665
O3W K3 O12 113.6(5) . .
O3W K3 O3W 79.7(7) . 3_665
O3W K3 O3W 79.7(7) 2_655 .
O3W K3 O3W 79.7(7) 2_655 3_665
W3 K4 K6 102.2(3) . 1_556
W3 K4 K7 108.6(4) . 1_556
W3 K4 K8 86.8(3) . 5_667
W3 K4 K10 132.4(3) . 1_656
K7 K4 K6 7.0(3) 1_556 1_556
K7 K4 K8 84.1(4) 1_556 5_667
K8 K4 K6 86.5(3) 5_667 1_556
K10 K4 K6 71.8(3) 1_656 1_556
K10 K4 K7 69.9(4) 1_656 1_556
K10 K4 K8 137.7(4) 1_656 5_667
O4 K4 W3 26.9(4) . .
O4 K4 K6 83.6(5) . 1_556
O4 K4 K7 88.7(5) . 1_556
O4 K4 K8 66.2(5) . 5_667
O4 K4 K10 141.8(5) . 1_656
O4 K4 O22 54.7(5) . .
O4 K4 O12W 111.1(9) . .
O22 K4 W3 28.2(4) . .
O22 K4 K6 114.4(5) . 1_556
O22 K4 K7 121.4(5) . 1_556
O22 K4 K8 112.2(5) . 5_667
O22 K4 K10 109.8(5) . 1_656
O23 K4 W3 95.5(6) 6_767 .
O23 K4 K6 36.0(6) 6_767 1_556
O23 K4 K7 40.0(6) 6_767 1_556
O23 K4 K8 121.6(6) 6_767 5_667
O23 K4 K10 51.4(6) 6_767 1_656
O23 K4 O4 91.8(7) 6_767 .
O23 K4 O22 91.8(7) 6_767 .
O23 K4 O5W 84.4(8) 6_767 .
O23 K4 O7W 77.5(8) 6_767 .
O23 K4 O10W 159.8(9) 6_767 .
O23 K4 O12W 78.8(9) 6_767 .
O5W K4 W3 170.2(7) . .
O5W K4 K6 83.5(7) . 1_556
O5W K4 K7 77.6(7) . 1_556
O5W K4 K8 101.6(7) . 5_667
O5W K4 K10 41.7(6) . 1_656
O5W K4 O4 162.8(8) . .
O5W K4 O22 142.0(8) . .
O5W K4 O7W 74.3(8) . .
O5W K4 O12W 84.7(10) . .
O7W K4 W3 115.3(6) . .
O7W K4 K6 42.5(6) . 1_556
O7W K4 K7 37.5(6) . 1_556
O7W K4 K8 50.3(6) . 5_667
O7W K4 K10 92.2(7) . 1_656
O7W K4 O4 88.5(7) . .
O7W K4 O22 141.7(8) . .
O7W K4 O12W 149.5(10) . .
O10W K4 W3 90.0(7) . .
O10W K4 K6 123.8(7) . 1_556
O10W K4 K7 119.9(7) . 1_556
O10W K4 K8 39.1(7) . 5_667
O10W K4 K10 133.6(7) . 1_656
O10W K4 O4 84.4(8) . .
O10W K4 O22 101.9(8) . .
O10W K4 O5W 93.4(9) . .
O10W K4 O7W 82.6(9) . .
O10W K4 O12W 121.1(10) . .
O12W K4 W3 85.7(8) . .
O12W K4 K6 114.5(8) . 1_556
O12W K4 K7 117.0(8) . 1_556
O12W K4 K8 158.8(8) . 5_667
O12W K4 K10 57.8(8) . 1_656
O12W K4 O22 57.6(8) . .
W5 K5 K5 101.1(3) . 5_557
W5 K5 K12 51.6(2) . 2_656
W5 K5 K14 157.8(4) . .
K12 K5 K5 152.3(4) 2_656 5_557
K12 K5 K14 119.4(4) 2_656 .
K14 K5 K5 84.0(3) . 5_557
O21 K5 W5 109.2(5) . .
O21 K5 K5 141.8(5) . 5_557
O21 K5 K12 60.2(5) . 2_656
O21 K5 K14 59.4(5) . .
O21 K5 O24 87.0(8) . .
O21 K5 O25 131.2(7) . .
O21 K5 O31 83.2(6) . .
O21 K5 O4W 87.2(8) . .
O21 K5 O8W 144.3(8) . .
O24 K5 W5 162.7(7) . .
O24 K5 K5 67.1(6) . 5_557
O24 K5 K12 140.5(7) . 2_656
O24 K5 K14 37.8(6) . .
O24 K5 O31 169.0(8) . .
O24 K5 O4W 93.9(8) . .
O25 K5 W5 28.0(3) . .
O25 K5 K5 85.5(4) . 5_557
O25 K5 K12 71.1(4) . 2_656
O25 K5 K14 169.4(5) . .
O25 K5 O24 135.0(7) . .
O25 K5 O31 56.0(5) . .
O25 K5 O4W 69.5(6) . .
O25 K5 O8W 63.7(7) . .
O31 K5 W5 28.2(3) . .
O31 K5 K5 118.9(5) . 5_557
O31 K5 K12 34.8(4) . 2_656
O31 K5 K14 131.5(5) . .
O4W K5 W5 81.2(6) . .
O4W K5 K5 120.7(6) . 5_557
O4W K5 K12 65.3(6) . 2_656
O4W K5 K14 115.0(6) . .
O4W K5 O31 90.4(7) . .
O8W K5 W5 91.6(6) . .
O8W K5 K5 53.6(6) . 5_557
O8W K5 K12 122.7(7) . 2_656
O8W K5 K14 108.4(7) . .
O8W K5 O24 71.3(8) . .
O8W K5 O31 119.7(8) . .
O8W K5 O4W 67.1(8) . .
W1 K6 K4 119.3(4) . 1_554
W1 K6 K6 69.5(4) . 6_766
W1 K6 K7 67.7(3) . 6_766
W1 K6 K9 68.2(3) . 6_656
K6 K6 K4 130.7(3) 6_766 1_554
K7 K6 W1 89(3) . .
K7 K6 K4 123.7(4) 6_766 1_554
K7 K6 K4 57(2) . 1_554
K7 K6 K6 76(2) . 6_766
K7 K6 K6 8.4(3) 6_766 6_766
K7 K6 K7 68(2) . 6_766
K7 K6 K9 129(3) . 6_656
K7 K6 O1 90(3) . .
K7 K6 O9 87(3) . .
K7 K6 O9 75(3) . 6_766
K7 K6 O23 78(3) . 6_766
K7 K6 O6W 121(3) . 6_656
K7 K6 O7W 36(2) . 1_554
K9 K6 K4 94.4(4) 6_656 1_554
K9 K6 K6 129.4(5) 6_656 6_766
K9 K6 K7 132.0(4) 6_656 6_766
O1 K6 W1 28.7(4) . .
O1 K6 K4 96.3(5) . 1_554
O1 K6 K6 97.4(6) . 6_766
O1 K6 K7 94.4(5) . 6_766
O1 K6 K9 49.1(5) . 6_656
O1 K6 O9 57.1(5) . .
O1 K6 O6W 81.2(7) . 6_656
O1 K6 O7W 69.4(7) . 1_554
O9 K6 W1 28.4(4) . .
O9 K6 W1 112.4(5) 6_766 .
O9 K6 K4 136.5(6) . 1_554
O9 K6 K4 105.3(5) 6_766 1_554
O9 K6 K6 41.6(4) . 6_766
O9 K6 K6 42.9(4) 6_766 6_766
O9 K6 K7 41.2(5) . 6_766
O9 K6 K7 45.2(5) 6_766 6_766
O9 K6 K9 155.4(7) 6_766 6_656
O9 K6 K9 91.4(6) . 6_656
O9 K6 O1 139.6(7) 6_766 .
O9 K6 O9 84.4(6) 6_766 .
O9 K6 O23 87.6(7) 6_766 6_766
O9 K6 O6W 138.7(8) 6_766 6_656
O9 K6 O6W 130.7(8) . 6_656
O9 K6 O7W 109.3(8) 6_766 1_554
O9 K6 O7W 98.8(7) . 1_554
O23 K6 W1 152.9(7) 6_766 .
O23 K6 K4 34.2(5) 6_766 1_554
O23 K6 K6 128.5(8) 6_766 6_766
O23 K6 K7 126.7(7) 6_766 6_766
O23 K6 K9 101.4(7) 6_766 6_656
O23 K6 O1 126.2(8) 6_766 .
O23 K6 O9 164.3(9) 6_766 .
O23 K6 O6W 62.5(7) 6_766 6_656
O23 K6 O7W 71.1(8) 6_766 1_554
O6W K6 W1 106.0(6) 6_656 .
O6W K6 K4 66.1(6) 6_656 1_554
O6W K6 K6 163.0(6) 6_656 6_766
O6W K6 K7 169.8(7) 6_656 6_766
O6W K6 K9 39.4(6) 6_656 6_656
O6W K6 O7W 88.3(8) 6_656 1_554
O7W K6 W1 84.6(6) 1_554 .
O7W K6 K4 37.8(5) 1_554 1_554
O7W K6 K6 107.2(6) 1_554 6_766
O7W K6 K7 98.8(6) 1_554 6_766
O7W K6 K9 95.3(7) 1_554 6_656
W1 K7 K4 126.5(5) . 1_554
W1 K7 K6 70.4(3) . 6_766
W1 K7 K7 69.5(5) . 6_766
W1 K7 K9 63.2(4) . 6_656
K4 K7 K9 92.9(4) 1_554 6_656
K6 K7 W1 81(2) . .
K6 K7 K4 116(3) . 1_554
K6 K7 K4 145.0(5) 6_766 1_554
K6 K7 K6 96(3) . 6_766
K6 K7 K7 104(2) . 6_766
K6 K7 K9 121.3(5) 6_766 6_656
K6 K7 K9 45(2) . 6_656
K6 K7 O1 78(3) . .
K6 K7 O9 81(3) . .
K6 K7 O9 93(3) . 6_766
K6 K7 O23 89(3) . 6_766
K6 K7 O6W 50(2) . 6_656
K6 K7 O7W 136(3) . 1_554
K7 K7 K4 138.6(4) 6_766 1_554
K7 K7 K6 8.4(3) 6_766 6_766
K7 K7 K9 125.4(6) 6_766 6_656
O1 K7 W1 28.4(4) . .
O1 K7 K4 102.1(6) . 1_554
O1 K7 K6 98.7(6) . 6_766
O1 K7 K7 97.5(7) . 6_766
O1 K7 K9 43.0(5) . 6_656
O1 K7 O9 56.1(6) . .
O1 K7 O6W 74.4(7) . 6_656
O9 K7 W1 113.6(7) 6_766 .
O9 K7 W1 28.0(4) . .
O9 K7 K4 150.6(7) . 1_554
O9 K7 K4 115.6(7) 6_766 1_554
O9 K7 K6 44.5(5) 6_766 6_766
O9 K7 K6 43.1(5) . 6_766
O9 K7 K7 43.8(5) . 6_766
O9 K7 K7 48.0(5) 6_766 6_766
O9 K7 K9 136.9(8) 6_766 6_656
O9 K7 K9 83.0(6) . 6_656
O9 K7 O1 141.3(9) 6_766 .
O9 K7 O9 85.6(7) 6_766 .
O9 K7 O23 90.7(8) 6_766 6_766
O9 K7 O6W 117.0(8) . 6_656
O9 K7 O6W 126.9(9) 6_766 6_656
O23 K7 W1 154.0(8) 6_766 .
O23 K7 K4 39.0(6) 6_766 1_554
O23 K7 K6 135.0(8) 6_766 6_766
O23 K7 K7 136.5(10) 6_766 6_766
O23 K7 K9 93.0(7) 6_766 6_656
O23 K7 O1 125.9(9) 6_766 .
O23 K7 O9 169.5(10) 6_766 .
O23 K7 O6W 58.1(7) 6_766 6_656
O6W K7 W1 98.0(6) 6_656 .
O6W K7 K4 67.8(5) 6_656 1_554
O6W K7 K6 145.9(7) 6_656 6_766
O6W K7 K7 153.4(6) 6_656 6_766
O6W K7 K9 35.0(5) 6_656 6_656
O7W K7 W1 90.9(8) 1_554 .
O7W K7 K4 40.7(7) 1_554 1_554
O7W K7 K6 121.7(8) 1_554 6_766
O7W K7 K7 113.3(7) 1_554 6_766
O7W K7 K9 93.6(8) 1_554 6_656
O7W K7 O1 75.4(8) 1_554 .
O7W K7 O9 129.2(10) 1_554 6_766
O7W K7 O9 110.3(9) 1_554 .
O7W K7 O23 79.6(9) 1_554 6_766
O7W K7 O6W 89.4(9) 1_554 6_656
W2 K8 K2 110.4(4) 6_666 4_556
W2 K8 K3 59.7(3) 6_666 4_556
K3 K8 K2 52.1(3) 4_556 4_556
K9 K8 W2 78(3) . 6_666
K9 K8 K2 90(3) . 4_556
K9 K8 K3 69(3) . 4_556
K9 K8 K12 83(3) . 4_556
K9 K8 O5 88(3) . 6_666
K9 K8 O7 105(3) . 6_667
K9 K8 O36 89(3) . 6_667
K9 K8 O3W 108(3) . 6_666
K9 K8 O6W 50(3) . .
K9 K8 O7W 141(3) . 5_567
K9 K8 O10W 147(3) . 5_567
K12 K8 W2 123.0(5) 4_556 6_666
K12 K8 K2 122.9(5) 4_556 4_556
K12 K8 K3 151.1(6) 4_556 4_556
O5 K8 W2 15.8(4) 6_666 6_666
O5 K8 K2 98.7(6) 6_666 4_556
O5 K8 K3 52.0(5) 6_666 4_556
O5 K8 K12 137.3(7) 6_666 4_556
O5 K8 O7 140.4(9) 6_666 6_667
O5 K8 O36 91.3(8) 6_666 6_667
O5 K8 O3W 65.1(7) 6_666 6_666
O5 K8 O6W 137.3(10) 6_666 .
O5 K8 O7W 53.5(7) 6_666 5_567
O5 K8 O10W 121.5(10) 6_666 5_567
O7 K8 W2 154.8(7) 6_667 6_666
O7 K8 K2 45.4(5) 6_667 4_556
O7 K8 K3 97.4(6) 6_667 4_556
O7 K8 K12 82.0(6) 6_667 4_556
O7 K8 O36 125.4(8) 6_667 6_667
O7 K8 O3W 75.3(7) 6_667 6_666
O7 K8 O6W 64.6(7) 6_667 .
O7 K8 O7W 105.4(8) 6_667 5_567
O7 K8 O10W 63.8(8) 6_667 5_567
O36 K8 W2 79.2(6) 6_667 6_666
O36 K8 K2 170.0(7) 6_667 4_556
O36 K8 K3 136.3(7) 6_667 4_556
O36 K8 K12 47.1(6) 6_667 4_556
O36 K8 O3W 149.4(9) 6_667 6_666
O36 K8 O7W 92.0(8) 6_667 5_567
O3W K8 W2 80.0(5) 6_666 6_666
O3W K8 K2 39.4(4) 6_666 4_556
O3W K8 K3 41.0(5) 6_666 4_556
O3W K8 K12 156.6(7) 6_666 4_556
O3W K8 O7W 58.7(7) 6_666 5_567
O6W K8 W2 126.5(8) . 6_666
O6W K8 K2 81.5(6) . 4_556
O6W K8 K3 101.6(7) . 4_556
O6W K8 K12 52.0(6) . 4_556
O6W K8 O36 90.6(9) . 6_667
O6W K8 O3W 120.0(9) . 6_666
O6W K8 O7W 168.9(9) . 5_567
O7W K8 W2 64.6(5) 5_567 6_666
O7W K8 K2 94.8(6) 5_567 4_556
O7W K8 K3 84.0(6) 5_567 4_556
O7W K8 K12 124.2(7) 5_567 4_556
O10W K8 W2 126.5(8) 5_567 6_666
O10W K8 K2 100.2(8) 5_567 4_556
O10W K8 K3 140.9(9) 5_567 4_556
O10W K8 K12 64.3(7) 5_567 4_556
O10W K8 O36 75.2(9) 5_567 6_667
O10W K8 O3W 99.9(9) 5_567 6_666
O10W K8 O6W 100.1(9) 5_567 .
O10W K8 O7W 70.1(9) 5_567 5_567
W2 K9 K6 94.5(4) 6_666 6_666
K8 K9 W2 95(3) . 6_666
K8 K9 K6 163(3) . 6_666
K8 K9 K12 89(3) . 4_556
K8 K9 O1 152(3) . 6_666
K8 K9 O5 80(3) . 6_666
K8 K9 O7 64(3) . 6_667
K8 K9 O36 80(3) . 6_667
K8 K9 O3W 63(3) . 6_666
K8 K9 O3W 122(3) . 4_556
K8 K9 O6W 121(3) . .
K8 K9 O10W 28(3) . 5_567
K12 K9 W2 126.0(5) 4_556 6_666
K12 K9 K6 74.7(5) 4_556 6_666
O1 K9 W2 63.1(4) 6_666 6_666
O1 K9 K6 43.7(5) 6_666 6_666
O1 K9 K12 117.5(7) 6_666 4_556
O1 K9 O3W 52.8(6) 6_666 4_556
O1 K9 O3W 94.7(7) 6_666 6_666
O1 K9 O10W 177.9(9) 6_666 5_567
O5 K9 W2 18.8(4) 6_666 6_666
O5 K9 K6 111.3(7) 6_666 6_666
O5 K9 K12 137.0(8) 6_666 4_556
O5 K9 O1 74.0(6) 6_666 6_666
O5 K9 O7 128.9(9) 6_666 6_667
O5 K9 O36 89.6(8) 6_666 6_667
O5 K9 O3W 61.5(6) 6_666 6_666
O5 K9 O3W 97.0(8) 6_666 4_556
O5 K9 O10W 105.5(9) 6_666 5_567
O7 K9 W2 147.6(7) 6_667 6_666
O7 K9 K6 112.4(7) 6_667 6_666
O7 K9 K12 80.2(6) 6_667 4_556
O7 K9 O1 125.9(8) 6_667 6_666
O7 K9 O36 117.0(8) 6_667 6_667
O7 K9 O3W 69.6(6) 6_667 6_666
O7 K9 O3W 74.4(6) 6_667 4_556
O7 K9 O10W 56.0(7) 6_667 5_567
O36 K9 W2 80.2(6) 6_667 6_666
O36 K9 K6 88.0(7) 6_667 6_666
O36 K9 K12 47.4(6) 6_667 4_556
O36 K9 O1 110.1(8) 6_667 6_666
O36 K9 O3W 158.2(10) 6_667 4_556
O36 K9 O3W 135.3(9) 6_667 6_666
O36 K9 O10W 67.8(8) 6_667 5_567
O3W K9 W2 99.8(6) 4_556 6_666
O3W K9 W2 79.0(5) 6_666 6_666
O3W K9 K6 70.2(6) 4_556 6_666
O3W K9 K6 132.6(7) 6_666 6_666
O3W K9 K12 145.2(7) 6_666 4_556
O3W K9 K12 123.6(7) 4_556 4_556
O3W K9 O3W 65.0(8) 4_556 6_666
O3W K9 O10W 129.2(8) 4_556 5_567
O3W K9 O10W 86.8(8) 6_666 5_567
O6W K9 W2 143.2(9) . 6_666
O6W K9 K6 48.7(7) . 6_666
O6W K9 K12 53.1(7) . 4_556
O6W K9 O1 84.6(8) . 6_666
O6W K9 O5 158.6(11) . 6_666
O6W K9 O7 65.9(8) . 6_667
O6W K9 O36 96.3(9) . 6_667
O6W K9 O3W 123.3(9) . 6_666
O6W K9 O3W 70.6(8) . 4_556
O6W K9 O10W 95.8(9) . 5_567
O10W K9 W2 115.9(7) 5_567 6_666
O10W K9 K6 135.5(8) 5_567 6_666
O10W K9 K12 61.4(6) 5_567 4_556
P1 K10 W2 53.1(2) 4_556 4_556
P1 K10 W2 99.5(4) 6_666 4_556
P1 K10 P1 112.9(5) 6_666 4_556
K11 K10 W2 110.8(19) . 4_556
K11 K10 P1 66.1(17) . 4_556
K11 K10 P1 74.9(17) . 6_666
K11 K10 O3 84.8(18) . 4_556
K11 K10 O6 94.1(18) . 6_666
K11 K10 O8 85.0(18) . 6_666
K11 K10 O13 54.1(17) . 6_666
K11 K10 O15 118.1(19) . 6_666
K11 K10 O23 129(2) . 6_666
K11 K10 C3 107.7(19) . 6_666
K11 K10 O5W 131(2) . 1_454
O3 K10 W2 31.9(4) 4_556 4_556
O3 K10 P1 111.0(6) 4_556 6_666
O3 K10 P1 21.3(4) 4_556 4_556
O3 K10 O6 102.1(7) 4_556 6_666
O3 K10 O8 169.9(9) 4_556 6_666
O3 K10 O13 116.0(7) 4_556 6_666
O3 K10 O15 57.4(5) 4_556 6_666
O3 K10 O23 145.8(9) 4_556 6_666
O3 K10 C3 164.6(9) 4_556 6_666
O3 K10 O5W 75.0(8) 4_556 1_454
O6 K10 W2 82.1(5) 6_666 4_556
O6 K10 P1 22.3(3) 6_666 6_666
O6 K10 P1 112.2(6) 6_666 4_556
O6 K10 O8 78.9(6) 6_666 6_666
O6 K10 O13 46.6(5) 6_666 6_666
O6 K10 O15 56.0(5) 6_666 6_666
O6 K10 O23 81.3(7) 6_666 6_666
O6 K10 C3 68.8(7) 6_666 6_666
O6 K10 O5W 132.9(9) 6_666 1_454
O8 K10 W2 156.1(6) 6_666 4_556
O8 K10 P1 66.4(5) 6_666 6_666
O8 K10 P1 149.2(7) 6_666 4_556
O8 K10 O13 57.4(5) 6_666 6_666
O8 K10 O15 128.8(7) 6_666 6_666
O8 K10 O23 44.3(6) 6_666 6_666
O8 K10 C3 24.5(6) 6_666 6_666
O13 K10 W2 116.8(5) 6_666 4_556
O13 K10 P1 108.3(5) 6_666 4_556
O13 K10 P1 24.3(3) 6_666 6_666
O15 K10 W2 28.0(3) 6_666 4_556
O15 K10 P1 77.1(5) 6_666 4_556
O15 K10 P1 76.2(5) 6_666 6_666
O15 K10 O13 98.0(6) 6_666 6_666
O15 K10 O23 100.9(7) 6_666 6_666
O15 K10 C3 107.9(7) 6_666 6_666
O23 K10 W2 118.4(7) 6_666 4_556
O23 K10 P1 160.4(7) 6_666 4_556
O23 K10 P1 85.1(6) 6_666 6_666
O23 K10 O13 91.3(6) 6_666 6_666
C3 K10 W2 132.8(7) 6_666 4_556
C3 K10 P1 173.7(7) 6_666 4_556
C3 K10 P1 65.5(6) 6_666 6_666
C3 K10 O13 67.5(6) 6_666 6_666
C3 K10 O23 24.2(6) 6_666 6_666
O5W K10 W2 71.7(7) 1_454 4_556
O5W K10 P1 82.3(7) 1_454 4_556
O5W K10 P1 153.6(9) 1_454 6_666
O5W K10 O8 111.8(9) 1_454 6_666
O5W K10 O13 168.9(9) 1_454 6_666
O5W K10 O15 87.2(8) 1_454 6_666
O5W K10 O23 78.1(9) 1_454 6_666
O5W K10 C3 101.6(9) 1_454 6_666
P1 K11 P1 122.8(5) 4_556 6_666
P1 K11 O12W 117.8(8) 4_556 1_454
K10 K11 P1 92.1(18) . 6_666
K10 K11 P1 101.2(18) . 4_556
K10 K11 O3 77.5(18) . 4_556
K10 K11 O6 69.3(17) . 6_666
K10 K11 O8 78.1(18) . 6_666
K10 K11 O13 124.9(19) . 4_556
K10 K11 O13 113.2(19) . 6_666
K10 K11 O15 49.6(17) . 6_666
K10 K11 C3 59.1(17) . 6_666
K10 K11 O5W 37.8(16) . 1_454
K10 K11 O12W 84.3(19) . 1_454
O3 K11 P1 26.0(4) 4_556 4_556
O3 K11 P1 113.3(6) 4_556 6_666
O3 K11 O6 96.4(7) 4_556 6_666
O3 K11 O8 155.7(9) 4_556 6_666
O3 K11 O13 52.1(5) 4_556 4_556
O3 K11 O13 129.2(8) 4_556 6_666
O3 K11 O15 50.8(5) 4_556 6_666
O3 K11 C3 135.7(9) 4_556 6_666
O3 K11 O5W 64.8(7) 4_556 1_454
O3 K11 O12W 125.1(9) 4_556 1_454
O6 K11 P1 114.8(6) 6_666 4_556
O6 K11 P1 25.5(3) 6_666 6_666
O6 K11 O13 129.6(7) 6_666 4_556
O6 K11 O13 50.5(5) 6_666 6_666
O6 K11 O15 49.1(5) 6_666 6_666
O6 K11 C3 62.1(6) 6_666 6_666
O6 K11 O5W 106.2(8) 6_666 1_454
O6 K11 O12W 124.5(9) 6_666 1_454
O8 K11 P1 67.9(5) 6_666 6_666
O8 K11 P1 169.2(7) 6_666 4_556
O8 K11 O6 75.2(6) 6_666 6_666
O8 K11 O13 62.5(6) 6_666 6_666
O8 K11 O13 148.9(8) 6_666 4_556
O8 K11 O15 111.3(7) 6_666 6_666
O8 K11 C3 21.0(5) 6_666 6_666
O8 K11 O5W 95.2(8) 6_666 1_454
O8 K11 O12W 51.5(8) 6_666 1_454
O13 K11 P1 25.2(3) 6_666 6_666
O13 K11 P1 126.5(7) 6_666 4_556
O13 K11 P1 26.1(3) 4_556 4_556
O13 K11 P1 124.7(6) 4_556 6_666
O13 K11 O13 115.4(8) 6_666 4_556
O13 K11 O15 97.0(6) 6_666 6_666
O13 K11 O15 99.8(6) 4_556 6_666
O13 K11 C3 167.9(8) 4_556 6_666
O13 K11 C3 68.3(6) 6_666 6_666
O13 K11 O5W 149.6(9) 6_666 1_454
O13 K11 O5W 94.5(7) 4_556 1_454
O13 K11 O12W 105.6(8) 4_556 1_454
O13 K11 O12W 105.6(8) 6_666 1_454
O15 K11 P1 72.6(4) 6_666 6_666
O15 K11 P1 75.2(4) 6_666 4_556
O15 K11 C3 90.9(7) 6_666 6_666
O15 K11 O12W 133.8(9) 6_666 1_454
C3 K11 P1 160.3(7) 6_666 4_556
C3 K11 P1 63.8(5) 6_666 6_666
C3 K11 O12W 62.5(8) 6_666 1_454
O5W K11 P1 129.9(8) 1_454 6_666
O5W K11 P1 78.6(6) 1_454 4_556
O5W K11 O15 70.9(7) 1_454 6_666
O5W K11 C3 83.7(8) 1_454 6_666
O5W K11 O12W 69.2(9) 1_454 1_454
O12W K11 P1 118.8(8) 1_454 6_666
W5 K12 W6 56.1(2) 3_664 2_544
W5 K12 K8 115.1(5) 3_664 4_556
W5 K12 K9 122.8(5) 3_664 4_556
W5 K12 K13 64.7(3) 3_664 .
W6 K12 K13 62.3(3) 2_544 .
K8 K12 W6 169.3(5) 4_556 2_544
K8 K12 K13 109.3(5) 4_556 .
K9 K12 W6 171.5(5) 4_556 2_544
K9 K12 K8 8.0(3) 4_556 4_556
K9 K12 K13 109.3(5) 4_556 .
O29 K12 W5 31.3(3) 3_664 3_664
O29 K12 W6 27.4(3) 3_664 2_544
O29 K12 K8 142.2(6) 3_664 4_556
O29 K12 K9 148.1(6) 3_664 4_556
O29 K12 K13 50.6(4) 3_664 .
O29 K12 O35 52.4(5) 3_664 2_544
O29 K12 O2W 103.6(7) 3_664 4_556
O29 K12 O6W 171.0(8) 3_664 4_556
O31 K12 W5 26.9(4) 3_664 3_664
O31 K12 W6 81.4(5) 3_664 2_544
O31 K12 K8 91.1(6) 3_664 4_556
O31 K12 K9 99.2(6) 3_664 4_556
O31 K12 K13 82.9(5) 3_664 .
O31 K12 O29 58.1(5) 3_664 3_664
O31 K12 O35 104.4(6) 3_664 2_544
O31 K12 O36 82.8(7) 3_664 3_664
O31 K12 O2W 101.0(7) 3_664 4_556
O31 K12 O6W 126.3(8) 3_664 4_556
O35 K12 W5 80.6(4) 2_544 3_664
O35 K12 W6 25.1(3) 2_544 2_544
O35 K12 K8 164.3(6) 2_544 4_556
O35 K12 K9 156.4(6) 2_544 4_556
O35 K12 K13 75.5(5) 2_544 .
O36 K12 W5 91.3(6) 3_664 3_664
O36 K12 W6 123.4(6) 3_664 2_544
O36 K12 K8 47.4(5) 3_664 4_556
O36 K12 K9 48.6(5) 3_664 4_556
O36 K12 K13 62.0(5) 3_664 .
O36 K12 O29 102.8(7) 3_664 3_664
O36 K12 O35 135.8(7) 3_664 2_544
O36 K12 O2W 150.9(8) 3_664 4_556
O36 K12 O6W 86.0(7) 3_664 4_556
O1W K12 W5 75.9(6) . 3_664
O1W K12 W6 65.6(6) . 2_544
O1W K12 K8 107.6(7) . 4_556
O1W K12 K9 106.0(7) . 4_556
O1W K12 K13 11.4(6) . .
O1W K12 O29 58.9(7) . 3_664
O1W K12 O31 94.2(8) . 3_664
O1W K12 O35 74.0(7) . 2_544
O1W K12 O36 61.9(8) . 3_664
O1W K12 O2W 144.9(9) . 4_556
O1W K12 O6W 125.3(9) . 4_556
O2W K12 W5 105.1(6) 4_556 3_664
O2W K12 W6 85.6(5) 4_556 2_544
O2W K12 K8 103.5(6) 4_556 4_556
O2W K12 K9 102.5(6) 4_556 4_556
O2W K12 K13 146.9(7) 4_556 .
O2W K12 O35 71.7(6) 4_556 2_544
O2W K12 O6W 68.3(7) 4_556 4_556
O6W K12 W5 152.8(7) 4_556 3_664
O6W K12 W6 144.1(7) 4_556 2_544
O6W K12 K8 46.5(6) 4_556 4_556
O6W K12 K9 40.8(6) 4_556 4_556
O6W K12 K13 134.8(7) 4_556 .
O6W K12 O35 119.4(7) 4_556 2_544
Ni2 K13 K12 100.6(4) 3_664 .
P3 K13 Ni2 50.6(2) 3_664 3_664
P3 K13 Ni2 163.6(5) 2_544 3_664
P3 K13 P3 129.0(5) 3_664 2_544
P3 K13 K12 87.1(4) 3_664 .
P3 K13 K12 95.6(4) 2_544 .
P3 K13 K13 87.0(5) 2_544 5_556
P3 K13 K13 125.4(6) 3_664 5_556
P3 K13 O29 74.0(4) 3_664 3_664
K13 K13 Ni2 83.1(5) 5_556 3_664
K13 K13 K12 134.4(3) 5_556 .
O27 K13 Ni2 68.9(4) 3_664 3_664
O27 K13 P3 26.5(3) 3_664 3_664
O27 K13 P3 117.9(6) 3_664 2_544
O27 K13 K12 62.5(5) 3_664 .
O27 K13 K13 150.7(8) 3_664 5_556
O27 K13 O29 49.6(5) 3_664 3_664
O27 K13 O32 70.8(6) 3_664 3_664
O27 K13 O34 52.8(5) 3_664 3_664
O27 K13 O34 137.3(7) 3_664 2_544
O29 K13 Ni2 116.8(5) 3_664 3_664
O29 K13 P3 74.4(4) 3_664 2_544
O29 K13 K12 42.6(4) 3_664 .
O29 K13 K13 159.7(7) 3_664 5_556
O30 K13 Ni2 166.9(6) 2_544 3_664
O30 K13 P3 26.2(3) 2_544 2_544
O30 K13 P3 117.8(6) 2_544 3_664
O30 K13 K12 70.7(5) 2_544 .
O30 K13 K13 110.0(7) 2_544 5_556
O30 K13 O27 98.1(7) 2_544 3_664
O30 K13 O29 50.1(5) 2_544 3_664
O30 K13 O32 141.5(7) 2_544 3_664
O30 K13 O34 52.2(5) 2_544 2_544
O30 K13 O34 137.9(7) 2_544 3_664
O32 K13 Ni2 34.0(3) 3_664 3_664
O32 K13 P3 67.4(4) 3_664 3_664
O32 K13 P3 159.9(6) 3_664 2_544
O32 K13 K12 71.7(5) 3_664 .
O32 K13 K13 91.0(6) 3_664 5_556
O32 K13 O29 103.5(6) 3_664 3_664
O32 K13 O34 151.9(7) 3_664 2_544
O32 K13 O34 64.1(5) 3_664 3_664
O34 K13 Ni2 139.2(6) 2_544 3_664
O34 K13 Ni2 34.5(3) 3_664 3_664
O34 K13 P3 136.0(6) 3_664 2_544
O34 K13 P3 135.1(6) 2_544 3_664
O34 K13 P3 26.6(3) 3_664 3_664
O34 K13 P3 26.1(3) 2_544 2_544
O34 K13 K12 109.6(5) 3_664 .
O34 K13 K12 118.9(6) 2_544 .
O34 K13 K13 62.7(5) 2_544 5_556
O34 K13 K13 98.9(6) 3_664 5_556
O34 K13 O29 100.0(6) 2_544 3_664
O34 K13 O29 100.2(6) 3_664 3_664
O34 K13 O34 126.2(7) 3_664 2_544
O1W K13 Ni2 104.8(9) . 3_664
O1W K13 P3 91.4(9) . 2_544
O1W K13 P3 100.9(9) . 3_664
O1W K13 K12 14.9(8) . .
O1W K13 K13 120.0(8) . 5_556
O1W K13 O27 77.1(9) . 3_664
O1W K13 O29 53.9(8) . 3_664
O1W K13 O30 69.4(9) . 2_544
O1W K13 O32 72.2(9) . 3_664
O1W K13 O34 111.1(10) . 2_544
O1W K13 O34 121.1(10) . 3_664
W3 K14 W4 55.6(2) 3_665 .
W3 K14 P2 97.0(3) 3_665 .
W3 K14 K11 126.8(4) 3_665 4_556
W4 K14 K11 143.3(5) . 4_556
P2 K14 W3 52.4(2) 3_665 3_665
P2 K14 W4 51.7(2) . .
P2 K14 W4 97.0(4) 3_665 .
P2 K14 P2 104.3(4) 3_665 .
P2 K14 K11 95.1(4) . 4_556
P2 K14 K11 74.4(3) 3_665 4_556
O2 K14 W3 33.9(4) 3_665 3_665
O2 K14 W4 81.9(5) 3_665 .
O2 K14 P2 102.9(6) 3_665 .
O2 K14 P2 18.5(4) 3_665 3_665
O2 K14 K11 92.9(6) 3_665 4_556
O2 K14 O10 57.6(6) 3_665 3_665
O2 K14 O11 97.7(7) 3_665 .
O2 K14 O16 151.6(8) 3_665 .
O2 K14 O24 161.4(9) 3_665 .
O2 K14 C6 163.2(9) 3_665 .
O2 K14 O12W 87.4(10) 3_665 4_547
O10 K14 W3 28.5(4) 3_665 3_665
O10 K14 W4 27.1(4) 3_665 .
O10 K14 P2 74.9(5) 3_665 3_665
O10 K14 P2 73.4(5) 3_665 .
O10 K14 K11 143.2(6) 3_665 4_556
O10 K14 O16 128.4(7) 3_665 .
O10 K14 O24 107.1(8) 3_665 .
O10 K14 C6 111.3(8) 3_665 .
O11 K14 W3 82.8(5) . 3_665
O11 K14 W4 33.0(4) . .
O11 K14 P2 18.9(4) . .
O11 K14 P2 105.0(6) . 3_665
O11 K14 K11 113.7(6) . 4_556
O11 K14 O10 56.6(6) . 3_665
O11 K14 O16 73.8(6) . .
O11 K14 O24 79.5(7) . .
O11 K14 C6 65.8(7) . .
O16 K14 W3 156.4(6) . 3_665
O16 K14 W4 101.3(5) . .
O16 K14 P2 136.7(6) . 3_665
O16 K14 P2 60.9(5) . .
O16 K14 K11 67.4(5) . 4_556
O16 K14 O24 45.3(7) . .
O16 K14 C6 24.3(6) . .
O24 K14 W3 128.0(7) . 3_665
O24 K14 W4 86.2(6) . .
O24 K14 P2 175.3(7) . 3_665
O24 K14 P2 80.4(6) . .
O24 K14 K11 105.1(7) . 4_556
O24 K14 C6 24.8(7) . .
C6 K14 W3 138.8(7) . 3_665
C6 K14 W4 85.0(6) . .
C6 K14 P2 158.7(7) . 3_665
C6 K14 P2 60.5(6) . .
C6 K14 K11 91.3(6) . 4_556
O12W K14 W3 110.1(9) 4_547 3_665
O12W K14 W4 164.5(9) 4_547 .
O12W K14 P2 142.6(9) 4_547 .
O12W K14 P2 75.1(9) 4_547 3_665
O12W K14 K11 48.1(8) 4_547 4_556
O12W K14 O10 138.2(10) 4_547 3_665
O12W K14 O11 161.5(11) 4_547 .
O12W K14 O16 93.3(10) 4_547 .
O12W K14 O24 101.1(11) 4_547 .
O12W K14 C6 107.3(11) 4_547 .
Ni1 K15 K10 83.1(5) . 4_556
Ni1 K15 K15 68.0(7) . 2_655
P2 K15 Ni1 168.2(8) 3_665 .
P2 K15 Ni1 51.3(4) . .
P2 K15 P2 128.0(8) . 3_665
P2 K15 K10 94.0(6) 3_665 4_556
P2 K15 K10 133.0(7) . 4_556
P2 K15 K11 129.6(8) . 4_556
P2 K15 K11 94.0(6) 3_665 4_556
P2 K15 K15 102.5(5) 3_665 2_655
P2 K15 K15 48.7(6) . 2_655
K10 K15 K15 109.0(4) 4_556 2_655
K11 K15 Ni1 81.7(6) 4_556 .
K11 K15 K10 7.3(4) 4_556 4_556
K11 K15 K15 101.9(5) 4_556 2_655
O2 K15 Ni1 162.3(9) 3_665 .
O2 K15 P2 113.8(8) 3_665 .
O2 K15 P2 26.5(4) 3_665 3_665
O2 K15 K10 113.0(8) 3_665 4_556
O2 K15 K11 115.3(8) 3_665 4_556
O2 K15 K15 110.9(6) 3_665 2_655
O2 K15 O11 92.5(8) 3_665 .
O2 K15 O16 137.1(10) 3_665 .
O2 K15 O17 52.5(6) 3_665 3_665
O2 K15 O12W 76.1(9) 3_665 4_547
O11 K15 Ni1 70.2(6) . .
O11 K15 P2 27.1(4) . .
O11 K15 P2 114.1(8) . 3_665
O11 K15 K10 151.5(9) . 4_556
O11 K15 K11 151.8(9) . 4_556
O11 K15 K15 70.5(8) . 2_655
O11 K15 O16 71.6(7) . .
O11 K15 O12W 127.8(11) . 4_547
O16 K15 Ni1 34.6(5) . .
O16 K15 P2 156.2(10) . 3_665
O16 K15 P2 68.0(6) . .
O16 K15 K10 80.9(7) . 4_556
O16 K15 K11 83.8(7) . 4_556
O16 K15 K15 101.1(10) . 2_655
O16 K15 O12W 82.8(10) . 4_547
O17 K15 Ni1 34.7(4) . .
O17 K15 Ni1 144.1(9) 3_665 .
O17 K15 P2 138.2(10) . 3_665
O17 K15 P2 137.8(9) 3_665 .
O17 K15 P2 26.2(4) 3_665 3_665
O17 K15 P2 26.8(4) . .
O17 K15 K10 72.5(6) 3_665 4_556
O17 K15 K10 108.0(8) . 4_556
O17 K15 K11 70.8(7) 3_665 4_556
O17 K15 K11 103.5(9) . 4_556
O17 K15 K15 37.2(7) . 2_655
O17 K15 K15 95.2(6) 3_665 2_655
O17 K15 O2 135.8(11) . 3_665
O17 K15 O11 135.7(10) 3_665 .
O17 K15 O11 53.6(6) . .
O17 K15 O16 64.6(7) . .
O17 K15 O16 152.2(11) 3_665 .
O17 K15 O17 131.4(11) . 3_665
O17 K15 O12W 145.6(12) . 4_547
O17 K15 O12W 74.8(9) 3_665 4_547
O12W K15 Ni1 110.9(9) 4_547 .
O12W K15 P2 75.7(8) 4_547 3_665
O12W K15 P2 146.1(10) 4_547 .
O12W K15 K10 52.9(8) 4_547 4_556
O12W K15 K11 59.8(8) 4_547 4_556
O12W K15 K15 161.0(8) 4_547 2_655
W1 O1 K3 106.6(7) . .
W1 O1 K6 101.2(7) . .
W1 O1 K7 100.6(8) . .
W1 O1 K9 124.1(8) . 6_656
K6 O1 K3 152.0(7) . .
K6 O1 K7 12.3(4) . .
K6 O1 K9 87.1(6) . 6_656
K7 O1 K3 148.5(7) . .
K7 O1 K9 97.4(7) . 6_656
K9 O1 K3 80.2(5) 6_656 .
W3 O2 K14 103.5(7) . 2_655
W3 O2 K15 127.6(8) . 2_655
P2 O2 W3 128.4(9) . .
P2 O2 K14 128.1(9) . 2_655
P2 O2 K15 98.7(9) . 2_655
W2 O3 K10 109.3(7) . 4_556
W2 O3 K11 123.3(8) . 4_556
P1 O3 W2 129.9(9) . .
P1 O3 K10 120.3(9) . 4_556
P1 O3 K11 104.5(9) . 4_556
K10 O3 K11 17.6(4) 4_556 4_556
W3 O4 K2 103.5(7) . 1_556
W3 O4 K4 105.2(8) . .
K4 O4 K2 146.1(6) . 1_556
W2 O5 K3 105.7(7) . .
W2 O5 K8 139.9(9) . 6_656
W2 O5 K9 131.4(9) . 6_656
K8 O5 K3 89.5(6) 6_656 .
K8 O5 K9 11.9(5) 6_656 6_656
K9 O5 K3 84.5(6) 6_656 .
W1 O6 K10 110.5(7) . 6_656
W1 O6 K11 121.8(7) . 6_656
P1 O6 W1 131.1(9) . .
P1 O6 K10 116.5(8) . 6_656
P1 O6 K11 102.0(8) . 6_656
K10 O6 K11 16.6(4) 6_656 6_656
W4 O7 K2 109.2(7) . 1_556
W4 O7 K8 154.1(10) . 6_657
W4 O7 K9 153.9(10) . 6_657
K8 O7 K2 96.5(6) 6_657 1_556
K8 O7 K9 10.4(5) 6_657 6_657
K9 O7 K2 93.7(6) 6_657 1_556
Ni1 O8 K10 115.9(8) . 6_656
Ni1 O8 K11 102.6(7) . 6_656
K10 O8 K11 16.8(4) 6_656 6_656
C3 O8 Ni1 114.6(15) . .
C3 O8 K10 91.4(14) . 6_656
C3 O8 K11 107.0(15) . 6_656
W1 O9 K6 159.8(9) . 6_766
W1 O9 K6 99.8(7) . .
W1 O9 K7 150.6(10) . 6_766
W1 O9 K7 100.5(8) . .
K6 O9 K6 95.5(6) 6_766 .
K6 O9 K7 91.7(7) 6_766 .
K6 O9 K7 12.2(4) . .
K7 O9 K6 12.7(4) 6_766 6_766
K7 O9 K6 94.3(7) 6_766 .
K7 O9 K7 88.1(8) 6_766 .
W3 O10 K14 106.8(7) . 2_655
W4 O10 W3 142.5(9) 2_655 .
W4 O10 K14 110.7(8) 2_655 2_655
W4 O11 K14 102.8(7) . .
W4 O11 K15 126.0(8) . .
P2 O11 W4 131.8(10) . .
P2 O11 K14 124.4(9) . .
P2 O11 K15 93.6(9) . .
W1 O12 W2 94.8(5) . .
W1 O12 K3 107.7(5) . .
W2 O12 K3 109.3(5) . .
As1 O12 W1 127.0(7) . .
As1 O12 W2 127.7(7) . .
As1 O12 K3 88.4(5) . .
Ni1 O13 K10 93.1(6) . 6_656
Ni1 O13 K11 95.3(6) . 6_656
Ni1 O13 K11 133.7(7) . 4_556
P1 O13 Ni1 114.6(9) . .
P1 O13 K10 85.8(7) . 6_656
P1 O13 K11 96.2(8) . 6_656
P1 O13 K11 90.0(8) . 4_556
K11 O13 K10 12.7(4) 6_656 6_656
K11 O13 K10 128.8(6) 4_556 6_656
K11 O13 K11 121.5(8) 6_656 4_556
W2 O14 W1 116.5(7) . .
W1 O15 W2 141.5(8) . 2_655
W1 O15 K10 110.2(7) . 6_656
W1 O15 K11 109.8(7) . 6_656
W2 O15 K10 107.5(7) 2_655 6_656
W2 O15 K11 105.3(6) 2_655 6_656
K10 O15 K11 12.3(4) 6_656 6_656
Ni1 O16 K14 123.2(8) . .
Ni1 O16 K15 91.9(8) . .
C6 O16 Ni1 112.2(19) . .
C6 O16 K14 89.1(16) . .
C6 O16 K15 116.9(17) . .
Ni1 O17 K15 97.0(8) . .
Ni1 O17 K15 137.2(9) . 2_655
P2 O17 Ni1 113.3(9) . .
P2 O17 K15 97.6(9) . 2_655
P2 O17 K15 98.6(9) . .
K15 O17 K15 107.4(11) . 2_655
W4 O18 W3 116.7(9) . .
W3 O19 K2 108.7(5) . 1_556
W4 O19 W3 95.3(6) . .
W4 O19 K2 107.6(6) . 1_556
As2 O19 W3 126.9(8) . .
As2 O19 W4 127.8(8) . .
As2 O19 K2 88.3(6) . 1_556
W4 O21 K5 160.8(11) . .
W3 O22 K4 98.7(8) . .
K4 O23 K6 109.8(9) 6_767 6_766
K4 O23 K7 101.0(9) 6_767 6_766
K4 O23 K10 86.4(8) 6_767 6_656
K6 O23 K10 114.4(9) 6_766 6_656
K7 O23 K6 12.6(4) 6_766 6_766
K7 O23 K10 105.7(9) 6_766 6_656
C3 O23 K4 132.4(19) . 6_767
C3 O23 K6 117.8(18) . 6_766
C3 O23 K7 125.9(19) . 6_766
C3 O23 K10 74.4(16) . 6_656
K5 O24 K14 106.3(9) . .
C6 O24 K5 125(2) . .
C6 O24 K14 84.4(18) . .
W5 O25 K1 108.6(7) . .
W5 O25 K5 103.4(7) . .
K5 O25 K1 148.0(6) . .
W6 O26 K1 106.0(6) . .
W5 O27 K13 122.8(7) . 2_656
P3 O27 W5 130.4(9) . .
P3 O27 K13 99.0(8) . 2_656
W5 O28 K1 106.1(5) . .
W6 O28 W5 95.3(5) . .
W6 O28 K1 106.8(5) . .
As3 O28 W5 128.1(7) . .
As3 O28 W6 128.7(7) . .
As3 O28 K1 87.8(5) . .
W5 O29 W6 141.3(8) . 3_765
W5 O29 K12 94.4(6) . 2_656
W5 O29 K13 107.0(6) . 2_656
W6 O29 K12 106.4(6) 3_765 2_656
W6 O29 K13 106.4(6) 3_765 2_656
K12 O29 K13 86.8(5) 2_656 2_656
W6 O30 K13 122.4(7) . 3_656
P3 O30 W6 129.3(9) . .
P3 O30 K13 102.0(8) . 3_656
W5 O31 K5 99.1(7) . .
W5 O31 K12 108.0(8) . 2_656
K12 O31 K5 107.5(7) 2_656 .
Ni2 O32 K13 95.4(6) . 2_656
C9 O32 Ni2 115.5(14) . .
C9 O32 K13 118.4(14) . 2_656
W6 O33 W5 116.0(7) . .
Ni2 O34 K13 94.2(6) . 2_656
Ni2 O34 K13 142.7(7) . 3_656
P3 O34 Ni2 113.3(8) . .
P3 O34 K13 95.2(8) . 2_656
P3 O34 K13 92.5(7) . 3_656
K13 O34 K13 110.5(7) 2_656 3_656
W6 O35 K12 103.3(7) . 3_656
K8 O36 K9 10.8(4) 6_657 6_657
K12 O36 K8 85.5(7) 2_656 6_657
K12 O36 K9 84.0(7) 2_656 6_657
C9 O36 K8 131.5(18) . 6_657
C9 O36 K9 138.7(18) . 6_657
C9 O36 K12 130.3(17) . 2_656
C1 N1 Ni1 110.0(13) . .
C1 N1 C2 112.9(18) . .
C2 N1 Ni1 108.3(14) . .
C4 N2 Ni1 107.9(14) . .
C5 N2 Ni1 106.0(16) . .
C5 N2 C4 116(2) . .
C7 N3 Ni2 107.7(13) . .
C8 N3 Ni2 106.6(13) . .
C8 N3 C7 113.0(17) . .
P1 C1 H1A 109.6 . .
P1 C1 H1B 109.6 . .
N1 C1 P1 110.3(15) . .
N1 C1 H1A 109.6 . .
N1 C1 H1B 109.6 . .
H1A C1 H1B 108.1 . .
N1 C2 H2A 108.6 . .
N1 C2 H2B 108.6 . .
H2A C2 H2B 107.5 . .
C3 C2 N1 115(2) . .
C3 C2 H2A 108.6 . .
C3 C2 H2B 108.6 . .
K10 C3 K11 13.2(4) 6_656 6_656
O8 C3 K10 64.0(13) . 6_656
O8 C3 K11 52.1(12) . 6_656
O8 C3 O23 122(2) . .
O8 C3 C2 119(2) . .
O23 C3 K10 81.4(16) . 6_656
O23 C3 K11 93.4(17) . 6_656
O23 C3 C2 120(2) . .
C2 C3 K10 128.4(17) . 6_656
C2 C3 K11 125.9(17) . 6_656
P2 C4 H4A 110.0 . .
P2 C4 H4B 110.0 . .
N2 C4 P2 108.5(16) . .
N2 C4 H4A 110.0 . .
N2 C4 H4B 110.0 . .
H4A C4 H4B 108.4 . .
N2 C5 H5A 108.5 . .
N2 C5 H5B 108.5 . .
H5A C5 H5B 107.5 . .
C6 C5 N2 115(2) . .
C6 C5 H5A 108.5 . .
C6 C5 H5B 108.5 . .
O16 C6 K14 66.6(15) . .
O16 C6 O24 120(3) . .
O16 C6 C5 122(3) . .
O24 C6 K14 70.8(17) . .
O24 C6 C5 119(3) . .
C5 C6 K14 138(2) . .
P3 C7 H7A 109.1 . .
P3 C7 H7B 109.1 . .
N3 C7 P3 112.6(16) . .
N3 C7 H7A 109.1 . .
N3 C7 H7B 109.1 . .
H7A C7 H7B 107.8 . .
N3 C8 H8A 108.3 . .
N3 C8 H8B 108.3 . .
N3 C8 C9 115.9(19) . .
H8A C8 H8B 107.4 . .
C9 C8 H8A 108.3 . .
C9 C8 H8B 108.3 . .
O32 C9 C8 117.6(19) . .
O36 C9 O32 121(2) . .
O36 C9 C8 122(2) . .
K13 O1W K12 153.6(13) . .
K2 O3W K8 96.1(7) . 6_656
K2 O3W K9 93.0(7) . 4_556
K2 O3W K9 92.5(7) . 6_656
K3 O3W K2 85.6(6) . .
K3 O3W K8 91.7(7) . 6_656
K3 O3W K9 83.1(7) . 6_656
K3 O3W K9 83.5(7) . 4_556
K8 O3W K9 9.1(4) 6_656 6_656
K8 O3W K9 169.4(8) 6_656 4_556
K9 O3W K9 165.1(10) 4_556 6_656
K4 O5W K11 97.0(9) . 1_656
K10 O5W K4 94.6(9) 1_656 .
K10 O5W K11 10.8(5) 1_656 1_656
K6 O6W K7 8.8(4) 6_666 6_666
K6 O6W K12 102.7(8) 6_666 4_556
K8 O6W K6 101.0(9) . 6_666
K8 O6W K7 105.1(9) . 6_666
K8 O6W K12 81.6(8) . 4_556
K9 O6W K6 91.9(9) . 6_666
K9 O6W K7 95.7(9) . 6_666
K9 O6W K8 9.4(6) . .
K9 O6W K12 86.1(9) . 4_556
K12 O6W K7 110.9(8) 4_556 6_666
K4 O7W K6 99.7(9) . 1_556
K4 O7W K8 90.9(8) . 5_667
K6 O7W K8 140.6(10) 1_556 5_667
K7 O7W K4 101.8(10) 1_556 .
K7 O7W K6 7.9(5) 1_556 1_556
K7 O7W K8 147.3(11) 1_556 5_667
K4 O10W K8 104.1(11) . 5_667
K4 O10W K9 109.2(10) . 5_667
K8 O10W K9 5.2(5) 5_667 5_667
K4 O12W K11 90.6(10) . 1_656
K4 O12W K15 149.0(14) . 4_657
K14 O12W K4 148.8(15) 4_657 .
K14 O12W K11 94.7(11) 4_657 1_656
K15 O12W K11 64.8(9) 4_657 1_656
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 K3 4.101(5) .
W1 K6 3.565(14) .
W1 K7 3.608(18) .
W1 K10 3.957(15) 6_656
W1 O1 1.743(16) .
W1 O6 2.163(14) .
W1 O9 1.723(17) .
W1 O12 2.229(13) .
W1 O14 1.946(14) .
W1 O15 1.903(15) .
W2 K8 4.106(17) 6_656
W2 K9 4.024(17) 6_656
W2 K10 3.908(15) 4_556
W2 O3 2.186(15) .
W2 O5 1.732(17) .
W2 O12 2.237(13) .
W2 O14 1.919(14) .
W2 O15 1.921(15) 3_665
W2 O20 1.731(16) .
W3 K2 4.120(5) 1_556
W3 K4 3.637(10) .
W3 K14 3.815(15) 2_655
W3 O2 2.187(16) .
W3 O4 1.702(17) .
W3 O10 1.902(16) .
W3 O18 1.935(17) .
W3 O19 2.228(15) .
W3 O22 1.741(19) .
W4 K2 4.073(5) 1_556
W4 K14 3.903(15) .
W4 O7 1.732(16) .
W4 O10 1.901(16) 3_665
W4 O11 2.180(16) .
W4 O18 1.910(17) .
W4 O19 2.200(15) .
W4 O21 1.72(2) .
W5 K1 4.089(5) .
W5 K5 3.633(11) .
W5 K12 3.659(15) 2_656
W5 O25 1.752(15) .
W5 O27 2.177(14) .
W5 O28 2.214(13) .
W5 O29 1.904(14) .
W5 O31 1.740(16) .
W5 O33 1.935(14) .
W6 K1 4.096(5) .
W6 K12 3.967(15) 3_656
W6 O26 1.742(15) .
W6 O28 2.196(14) .
W6 O29 1.906(13) 2_645
W6 O30 2.190(14) .
W6 O33 1.910(14) .
W6 O35 1.726(17) .
As1 K3 3.304(9) .
As1 O12 1.783(13) .
As1 O12 1.783(13) 3_665
As1 O12 1.783(13) 2_655
As2 K2 3.304(9) 1_556
As2 O19 1.800(15) .
As2 O19 1.800(15) 2_655
As2 O19 1.800(15) 3_665
As3 K1 3.330(10) .
As3 O28 1.789(14) 2_645
As3 O28 1.789(14) 3_765
As3 O28 1.789(14) .
Ni1 K11 3.802(17) 6_656
Ni1 K15 3.64(2) .
Ni1 O8 2.068(17) .
Ni1 O13 2.102(15) .
Ni1 O16 2.068(19) .
Ni1 O17 2.089(16) .
Ni1 N1 2.063(17) .
Ni1 N2 2.11(2) .
Ni2 K13 3.668(16) 2_656
Ni2 K13 3.668(15) 6_657
Ni2 O32 2.061(15) .
Ni2 O32 2.061(15) 5_558
Ni2 O34 2.082(15) 5_558
Ni2 O34 2.082(15) .
Ni2 N3 2.146(16) 5_558
Ni2 N3 2.146(17) .
P1 K10 3.614(16) 4_556
P1 K10 3.590(16) 6_656
P1 K11 3.468(17) 6_656
P1 K11 3.370(18) 4_556
P1 O3 1.524(16) .
P1 O6 1.524(15) .
P1 O13 1.483(16) .
P1 C1 1.79(2) .
P2 K14 3.801(17) 2_655
P2 K14 3.853(16) .
P2 K15 3.32(2) .
P2 K15 3.40(2) 2_655
P2 O2 1.534(17) .
P2 O11 1.513(18) .
P2 O17 1.515(17) .
P2 C4 1.80(3) .
P3 K13 3.429(16) 3_656
P3 K13 3.363(17) 2_656
P3 O27 1.519(16) .
P3 O30 1.548(16) .
P3 O34 1.510(16) .
P3 C7 1.80(2) .
K1 K1 3.941(19) 4_647
K1 O25 3.178(15) 2_645
K1 O25 3.178(15) .
K1 O25 3.178(16) 3_765
K1 O26 3.258(15) 2_645
K1 O26 3.258(15) 3_765
K1 O26 3.258(15) .
K1 O28 2.879(15) .
K1 O28 2.879(15) 2_645
K1 O28 2.879(16) 3_765
K2 As2 3.304(9) 1_554
K2 O4 3.376(17) 3_664
K2 O4 3.376(17) 1_554
K2 O7 3.161(17) 2_654
K2 O7 3.161(17) 3_664
K2 O7 3.161(17) 1_554
K2 O19 2.825(16) 3_664
K2 O19 2.825(16) 2_654
K2 O19 2.825(16) 1_554
K2 O3W 2.82(2) 3_665
K2 O3W 2.82(2) .
K2 O3W 2.82(2) 2_655
K3 O1 3.247(17) 3_665
K3 O1 3.247(16) .
K3 O1 3.247(16) 2_655
K3 O5 3.329(17) .
K3 O5 3.329(17) 2_655
K3 O12 2.830(15) 2_655
K3 O12 2.830(15) 3_665
K3 O12 2.830(15) .
K3 O3W 2.77(2) .
K3 O3W 2.77(2) 3_665
K3 O3W 2.77(2) 2_655
K4 K6 4.461(17) 1_556
K4 K7 4.16(2) 1_556
K4 K8 4.42(2) 5_667
K4 K10 3.968(19) 1_656
K4 O4 2.80(2) .
K4 O22 2.94(2) .
K4 O23 2.67(3) 6_767
K4 O5W 2.75(3) .
K4 O7W 2.77(3) .
K4 O10W 2.73(3) .
K4 O12W 2.87(4) .
K5 K5 4.89(2) 5_557
K5 K12 4.558(19) 2_656
K5 K14 4.622(19) .
K5 O21 2.61(2) .
K5 O24 2.82(3) .
K5 O25 2.803(19) .
K5 O31 2.926(19) .
K5 O4W 2.89(3) .
K5 O8W 2.81(3) .
K6 K4 4.461(17) 1_554
K6 K6 4.15(3) 6_766
K6 K7 4.046(18) 6_766
K6 K7 0.607(19) .
K6 K9 4.03(3) 6_656
K6 O1 2.79(2) .
K6 O9 2.77(2) 6_766
K6 O9 2.84(2) .
K6 O23 2.79(3) 6_766
K6 O6W 3.03(3) 6_656
K6 O7W 3.06(3) 1_554
K7 K4 4.16(2) 1_554
K7 K6 4.046(18) 6_766
K7 K7 3.86(4) 6_766
K7 K9 4.44(3) 6_656
K7 O1 2.85(2) .
K7 O9 2.67(2) 6_766
K7 O9 2.87(2) .
K7 O23 2.73(3) 6_766
K7 O6W 3.38(3) 6_656
K7 O7W 2.59(3) 1_554
K8 W2 4.106(17) 6_666
K8 K2 4.408(18) 4_556
K8 K3 4.224(18) 4_556
K8 K9 0.55(2) .
K8 K12 3.93(2) 4_556
K8 O5 2.63(2) 6_666
K8 O7 2.74(2) 6_667
K8 O36 2.90(3) 6_667
K8 O3W 3.10(3) 6_666
K8 O6W 2.88(3) .
K8 O7W 3.40(3) 5_567
K8 O10W 2.88(4) 5_567
K9 W2 4.024(17) 6_666
K9 K6 4.03(3) 6_666
K9 K12 3.90(2) 4_556
K9 O1 3.05(3) 6_666
K9 O5 2.66(2) 6_666
K9 O7 2.93(2) 6_667
K9 O36 2.94(3) 6_667
K9 O3W 3.32(3) 6_666
K9 O3W 3.30(3) 4_556
K9 O6W 2.56(3) .
K9 O10W 3.35(4) 5_567
K10 W2 3.908(15) 4_556
K10 P1 3.590(16) 6_666
K10 P1 3.614(16) 4_556
K10 K11 0.806(19) .
K10 O3 2.60(2) 4_556
K10 O6 2.64(2) 6_666
K10 O8 2.72(2) 6_666
K10 O13 3.38(2) 6_666
K10 O15 2.87(2) 6_666
K10 O23 3.11(3) 6_666
K10 C3 3.03(3) 6_666
K10 O5W 2.65(3) 1_454
K11 P1 3.468(17) 6_666
K11 P1 3.370(18) 4_556
K11 O3 2.65(2) 4_556
K11 O6 2.82(2) 6_666
K11 O8 2.77(2) 6_666
K11 O13 2.98(2) 6_666
K11 O13 3.03(2) 4_556
K11 O15 3.33(2) 6_666
K11 C3 3.36(3) 6_666
K11 O5W 3.24(3) 1_454
K11 O12W 3.43(4) 1_454
K12 W5 3.659(15) 3_664
K12 W6 3.967(15) 2_544
K12 K8 3.93(2) 4_556
K12 K9 3.90(2) 4_556
K12 K13 4.39(2) .
K12 O29 2.98(2) 3_664
K12 O31 2.73(2) 3_664
K12 O35 3.20(2) 2_544
K12 O36 2.89(3) 3_664
K12 O1W 2.55(3) .
K12 O2W 3.10(3) 4_556
K12 O6W 3.13(3) 4_556
K13 Ni2 3.668(15) 3_664
K13 P3 3.429(16) 2_544
K13 P3 3.363(16) 3_664
K13 K13 3.63(3) 5_556
K13 O27 2.77(2) 3_664
K13 O29 3.40(2) 3_664
K13 O30 2.76(2) 2_544
K13 O32 2.84(2) 3_664
K13 O34 2.87(2) 3_664
K13 O34 3.01(2) 2_544
K13 O1W 1.96(3) .
K14 W3 3.815(15) 3_665
K14 P2 3.801(17) 3_665
K14 K11 4.60(2) 4_556
K14 O2 2.66(2) 3_665
K14 O10 2.80(2) 3_665
K14 O11 2.79(2) .
K14 O16 2.85(2) .
K14 O24 2.95(3) .
K14 C6 3.11(3) .
K14 O12W 2.79(4) 4_547
K15 P2 3.40(2) 3_665
K15 K10 4.22(3) 4_556
K15 K11 3.59(3) 4_556
K15 K15 4.51(4) 2_655
K15 O2 2.81(3) 3_665
K15 O11 2.86(3) .
K15 O16 2.93(3) .
K15 O17 2.85(3) 3_665
K15 O17 2.74(3) .
K15 O12W 3.27(4) 4_547
O1 K9 3.05(3) 6_656
O2 K14 2.66(2) 2_655
O2 K15 2.81(3) 2_655
O3 K10 2.60(2) 4_556
O3 K11 2.65(2) 4_556
O4 K2 3.375(17) 1_556
O5 K8 2.63(2) 6_656
O5 K9 2.66(2) 6_656
O6 K10 2.64(2) 6_656
O6 K11 2.82(2) 6_656
O7 K2 3.161(17) 1_556
O7 K8 2.74(2) 6_657
O7 K9 2.93(2) 6_657
O8 K10 2.72(2) 6_656
O8 K11 2.77(2) 6_656
O8 C3 1.26(3) .
O9 K6 2.77(2) 6_766
O9 K7 2.67(2) 6_766
O10 W4 1.901(16) 2_655
O10 K14 2.80(2) 2_655
O13 K10 3.38(2) 6_656
O13 K11 3.03(2) 4_556
O13 K11 2.98(2) 6_656
O15 W2 1.921(15) 2_655
O15 K10 2.87(2) 6_656
O15 K11 3.33(2) 6_656
O16 C6 1.28(3) .
O17 K15 2.85(3) 2_655
O19 K2 2.825(16) 1_556
O23 K4 2.67(3) 6_767
O23 K6 2.79(3) 6_766
O23 K7 2.73(3) 6_766
O23 K10 3.11(3) 6_656
O23 C3 1.29(3) .
O24 C6 1.31(4) .
O27 K13 2.77(2) 2_656
O29 W6 1.906(13) 3_765
O29 K12 2.98(2) 2_656
O29 K13 3.40(2) 2_656
O30 K13 2.76(2) 3_656
O31 K12 2.73(2) 2_656
O32 K13 2.84(2) 2_656
O32 C9 1.25(3) .
O34 K13 3.01(2) 3_656
O34 K13 2.87(2) 2_656
O35 K12 3.20(2) 3_656
O36 K8 2.90(3) 6_657
O36 K9 2.94(3) 6_657
O36 K12 2.89(3) 2_656
O36 C9 1.23(3) .
N1 C1 1.45(3) .
N1 C2 1.47(3) .
N2 C4 1.55(3) .
N2 C5 1.48(3) .
N3 C7 1.47(3) .
N3 C8 1.41(3) .
C1 H1A 0.9700 .
C1 H1B 0.9700 .
C2 H2A 0.9700 .
C2 H2B 0.9700 .
C2 C3 1.47(3) .
C3 K10 3.03(3) 6_656
C3 K11 3.36(3) 6_656
C4 H4A 0.9700 .
C4 H4B 0.9700 .
C5 H5A 0.9700 .
C5 H5B 0.9700 .
C5 C6 1.37(4) .
C7 H7A 0.9700 .
C7 H7B 0.9700 .
C8 H8A 0.9700 .
C8 H8B 0.9700 .
C8 C9 1.53(3) .
O2W K12 3.10(3) 4_556
O3W K8 3.10(3) 6_656
O3W K9 3.32(3) 6_656
O3W K9 3.30(3) 4_556
O5W K10 2.65(3) 1_656
O5W K11 3.24(3) 1_656
O6W K6 3.03(3) 6_666
O6W K7 3.38(3) 6_666
O6W K12 3.13(3) 4_556
O7W K6 3.06(3) 1_556
O7W K7 2.59(3) 1_556
O7W K8 3.40(3) 5_667
O10W K8 2.88(4) 5_667
O10W K9 3.35(4) 5_667
O12W K11 3.43(4) 1_656
O12W K14 2.79(4) 4_657
O12W K15 3.27(4) 4_657
