#------------------------------------------------------------------------------
#$Date: 2016-03-26 01:59:01 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180117 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/15/7101538.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7101538
loop_
_publ_author_name
P.Govindaswamy
D.Linder
J.Lacour
G.Suss-Fink
B.Therrien
_publ_section_title
;
Self-assembled hexanuclear arene ruthenium
metallo-prisms with unexpected double helical chirality
;
_journal_issue                   45
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b610155k
_journal_year                    2006
_chemical_formula_moiety         'C114 H132 N12 O12 Ru6, (C F3 O3 S)6'
_chemical_formula_sum            'C120 H132 F18 N12 O30 Ru6 S6'
_chemical_formula_weight         3363.16
_chemical_name_systematic
;
?
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 99.68(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   27.333(5)
_cell_length_b                   19.941(4)
_cell_length_c                   28.163(6)
_cell_measurement_reflns_used    75152
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      25.59
_cell_measurement_theta_min      1.27
_cell_volume                     15132(5)
_computing_cell_refinement       X-Area
_computing_data_collection       X-Area
_computing_data_reduction        X-RED
_computing_molecular_graphics    'PLATON03 (Spek, 2003)'
_computing_publication_material  SHELXL-97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_detector_area_resol_mean 0.81\%A
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'STOE IPDS-2'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0389
_diffrn_reflns_av_sigmaI/netI    0.0250
_diffrn_reflns_limit_h_max       32
_diffrn_reflns_limit_h_min       -32
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            55313
_diffrn_reflns_theta_full        25.15
_diffrn_reflns_theta_max         25.15
_diffrn_reflns_theta_min         1.27
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.757
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.476
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             6792
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.212
_refine_diff_density_min         -1.381
_refine_diff_density_rms         0.102
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.038
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     667
_refine_ls_number_reflns         13447
_refine_ls_number_restraints     16
_refine_ls_restrained_S_all      1.038
_refine_ls_R_factor_all          0.0598
_refine_ls_R_factor_gt           0.0525
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0936P)²+46.8945P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1503
_refine_ls_wR_factor_ref         0.1568
_reflns_number_gt                11378
_reflns_number_total             13447
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b610155k.txt
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               7101538
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.40046(17) 1.4013(2) 0.02545(15) 0.0429(9) Uani 1 1 d .
C2 C 0.37236(18) 1.3382(2) 0.00507(15) 0.0452(10) Uani 1 1 d .
C3 C 0.49230(15) 0.79430(19) 0.27532(14) 0.0378(8) Uani 1 1 d .
C4 C 0.37666(19) 1.3727(2) 0.14605(17) 0.0540(11) Uani 1 1 d .
H4 H 0.3818 1.4188 0.1469 0.065 Uiso 1 1 calc R
C5 C 0.40161(19) 1.3341(2) 0.18342(17) 0.0545(11) Uani 1 1 d .
H5 H 0.4224 1.3539 0.2092 0.065 Uiso 1 1 calc R
C6 C 0.39466(18) 1.2652(2) 0.18124(16) 0.0490(10) Uani 1 1 d .
C7 C 0.36444(19) 1.2376(2) 0.14184(18) 0.0558(12) Uani 1 1 d .
H7 H 0.3607 1.1913 0.1388 0.067 Uiso 1 1 calc R
C8 C 0.3402(2) 1.2796(2) 0.10751(18) 0.0593(12) Uani 1 1 d .
H8 H 0.3187 1.2610 0.0817 0.071 Uiso 1 1 calc R
C9 C 0.50493(18) 1.3263(2) 0.10160(17) 0.0489(10) Uani 1 1 d .
H9 H 0.5095 1.3714 0.0951 0.059 Uiso 1 1 calc R
C10 C 0.52305(18) 1.3026(2) 0.14697(17) 0.0490(10) Uani 1 1 d .
H10 H 0.5394 1.3311 0.1705 0.059 Uiso 1 1 calc R
C11 C 0.51657(16) 1.2355(2) 0.15711(15) 0.0457(10) Uani 1 1 d .
C12 C 0.4880(2) 1.1960(2) 0.12178(17) 0.0543(11) Uani 1 1 d .
H12 H 0.4805 1.1518 0.1283 0.065 Uiso 1 1 calc R
C13 C 0.4711(2) 1.2236(2) 0.07718(16) 0.0523(11) Uani 1 1 d .
H13 H 0.4522 1.1972 0.0537 0.063 Uiso 1 1 calc R
C14 C 0.4251(2) 0.9488(3) 0.18979(16) 0.0566(12) Uani 1 1 d .
H14 H 0.4259 0.9310 0.1594 0.068 Uiso 1 1 calc R
C15 C 0.4305(2) 1.0176(3) 0.19628(17) 0.0599(13) Uani 1 1 d .
H15 H 0.4325 1.0457 0.1703 0.072 Uiso 1 1 calc R
C16 C 0.43288(17) 1.0429(2) 0.24151(16) 0.0468(10) Uani 1 1 d .
C17 C 0.4283(2) 1.0008(2) 0.27920(18) 0.0551(11) Uani 1 1 d .
H17 H 0.4303 1.0172 0.3104 0.066 Uiso 1 1 calc R
C18 C 0.42038(19) 0.9321(2) 0.26918(16) 0.0526(11) Uani 1 1 d .
H18 H 0.4162 0.9031 0.2940 0.063 Uiso 1 1 calc R
C19 C 0.43665(17) 1.1168(2) 0.24882(16) 0.0473(10) Uani 1 1 d .
C20 C 0.41923(19) 1.2210(2) 0.22132(16) 0.0510(11) Uani 1 1 d .
C21 C 0.46013(17) 1.2067(2) 0.29638(16) 0.0470(10) Uani 1 1 d .
C22 C 0.5207(5) 1.2400(3) -0.0284(4) 0.122(4) Uani 1 1 d .
C23 C 0.4813(4) 1.2534(4) -0.0669(3) 0.109(3) Uani 1 1 d .
C24 C 0.4741(3) 1.3211(3) -0.0847(2) 0.0784(18) Uani 1 1 d .
C25 C 0.5055(2) 1.3735(2) -0.06178(17) 0.0577(12) Uani 1 1 d .
C26 C 0.5425(2) 1.3593(3) -0.02216(19) 0.0604(12) Uani 1 1 d .
C27 C 0.5502(3) 1.2914(4) -0.0065(3) 0.090(2) Uani 1 1 d .
C28 C 0.5308(6) 1.1688(4) -0.0088(5) 0.218(9) Uani 1 1 d .
H28A H 0.5659 1.1621 0.0001 0.327 Uiso 1 1 calc R
H28B H 0.5176 1.1369 -0.0332 0.327 Uiso 1 1 calc R
H28C H 0.5151 1.1627 0.0189 0.327 Uiso 1 1 calc R
C29 C 0.4477(5) 1.1984(5) -0.0871(4) 0.203(8) Uani 1 1 d .
H29A H 0.4154 1.2163 -0.0990 0.305 Uiso 1 1 calc R
H29B H 0.4454 1.1659 -0.0624 0.305 Uiso 1 1 calc R
H29C H 0.4607 1.1773 -0.1130 0.305 Uiso 1 1 calc R
C30 C 0.4357(4) 1.3342(6) -0.1260(2) 0.133(4) Uani 1 1 d .
H30A H 0.4466 1.3690 -0.1453 0.199 Uiso 1 1 calc R
H30B H 0.4059 1.3482 -0.1150 0.199 Uiso 1 1 calc R
H30C H 0.4293 1.2941 -0.1449 0.199 Uiso 1 1 calc R
C31 C 0.4955(3) 1.4454(3) -0.0765(3) 0.086(2) Uani 1 1 d .
H31A H 0.4951 1.4724 -0.0484 0.130 Uiso 1 1 calc R
H31B H 0.4639 1.4485 -0.0973 0.130 Uiso 1 1 calc R
H31C H 0.5211 1.4611 -0.0933 0.130 Uiso 1 1 calc R
C32 C 0.5728(3) 1.4167(4) 0.0023(3) 0.098(2) Uani 1 1 d .
H32A H 0.5763 1.4506 -0.0210 0.147 Uiso 1 1 calc R
H32B H 0.6050 1.4006 0.0167 0.147 Uiso 1 1 calc R
H32C H 0.5564 1.4352 0.0268 0.147 Uiso 1 1 calc R
C33 C 0.5918(4) 1.2788(6) 0.0375(4) 0.156(5) Uani 1 1 d .
H33A H 0.5840 1.2394 0.0543 0.235 Uiso 1 1 calc R
H33B H 0.5941 1.3167 0.0587 0.235 Uiso 1 1 calc R
H33C H 0.6229 1.2726 0.0265 0.235 Uiso 1 1 calc R
C34 C 0.2558(3) 1.4423(5) 0.1033(3) 0.092(2) Uani 1 1 d .
C35 C 0.2754(2) 1.4975(3) 0.0795(4) 0.094(3) Uani 1 1 d .
C36 C 0.2696(3) 1.5003(3) 0.0279(4) 0.091(2) Uani 1 1 d .
C37 C 0.2456(3) 1.4516(5) 0.0026(3) 0.095(2) Uani 1 1 d .
C38 C 0.2276(2) 1.3935(3) 0.0249(3) 0.0777(18) Uani 1 1 d .
C39 C 0.2316(2) 1.3903(4) 0.0741(3) 0.084(2) Uani 1 1 d .
C40 C 0.2608(4) 1.4303(10) 0.1570(4) 0.241(10) Uani 1 1 d .
H40A H 0.2365 1.4565 0.1696 0.361 Uiso 1 1 calc R
H40B H 0.2934 1.4431 0.1725 0.361 Uiso 1 1 calc R
H40C H 0.2555 1.3836 0.1628 0.361 Uiso 1 1 calc R
C41 C 0.3020(4) 1.5527(5) 0.1122(5) 0.163(5) Uani 1 1 d .
H41A H 0.3331 1.5631 0.1023 0.245 Uiso 1 1 calc R
H41B H 0.3080 1.5373 0.1449 0.245 Uiso 1 1 calc R
H41C H 0.2816 1.5921 0.1098 0.245 Uiso 1 1 calc R
C42 C 0.2931(4) 1.5582(4) 0.0044(5) 0.185(7) Uani 1 1 d .
H42A H 0.3148 1.5407 -0.0162 0.278 Uiso 1 1 calc R
H42B H 0.3118 1.5858 0.0289 0.278 Uiso 1 1 calc R
H42C H 0.2676 1.5846 -0.0144 0.278 Uiso 1 1 calc R
C43 C 0.2415(4) 1.4563(8) -0.0523(4) 0.194(7) Uani 1 1 d .
H43A H 0.2533 1.4993 -0.0607 0.291 Uiso 1 1 calc R
H43B H 0.2074 1.4510 -0.0671 0.291 Uiso 1 1 calc R
H43C H 0.2611 1.4216 -0.0634 0.291 Uiso 1 1 calc R
C44 C 0.2080(3) 1.3372(5) -0.0100(4) 0.137(4) Uani 1 1 d .
H44A H 0.2205 1.2950 0.0031 0.206 Uiso 1 1 calc R
H44B H 0.2186 1.3446 -0.0403 0.206 Uiso 1 1 calc R
H44C H 0.1724 1.3367 -0.0146 0.206 Uiso 1 1 calc R
C45 C 0.2106(3) 1.3274(4) 0.0950(5) 0.161(6) Uani 1 1 d .
H45A H 0.1861 1.3403 0.1140 0.241 Uiso 1 1 calc R
H45B H 0.2370 1.3037 0.1149 0.241 Uiso 1 1 calc R
H45C H 0.1957 1.2988 0.0691 0.241 Uiso 1 1 calc R
C46 C 0.33273(19) 0.8291(3) 0.1586(2) 0.0686(15) Uani 1 1 d .
C47 C 0.36085(18) 0.7838(3) 0.13705(17) 0.0611(13) Uani 1 1 d .
C48 C 0.37564(18) 0.7213(3) 0.16143(18) 0.0583(12) Uani 1 1 d .
C49 C 0.36397(19) 0.7060(2) 0.20723(19) 0.0564(12) Uani 1 1 d .
C50 C 0.33804(18) 0.7559(3) 0.23026(18) 0.0576(12) Uani 1 1 d .
C51 C 0.32132(17) 0.8169(3) 0.2053(2) 0.0597(13) Uani 1 1 d .
C52 C 0.3147(3) 0.8930(4) 0.1329(3) 0.116(3) Uani 1 1 d .
H52A H 0.3396 0.9271 0.1403 0.174 Uiso 1 1 calc R
H52B H 0.2847 0.9073 0.1434 0.174 Uiso 1 1 calc R
H52C H 0.3083 0.8852 0.0988 0.174 Uiso 1 1 calc R
C53 C 0.3792(3) 0.7999(5) 0.09102(19) 0.099(3) Uani 1 1 d .
H53A H 0.3758 0.8472 0.0847 0.149 Uiso 1 1 calc R
H53B H 0.3600 0.7755 0.0649 0.149 Uiso 1 1 calc R
H53C H 0.4135 0.7874 0.0939 0.149 Uiso 1 1 calc R
C54 C 0.4078(2) 0.6721(4) 0.1383(3) 0.092(2) Uani 1 1 d .
H54A H 0.4414 0.6739 0.1551 0.139 Uiso 1 1 calc R
H54B H 0.4071 0.6841 0.1051 0.139 Uiso 1 1 calc R
H54C H 0.3952 0.6274 0.1400 0.139 Uiso 1 1 calc R
C55 C 0.3819(3) 0.6439(3) 0.2338(3) 0.0842(18) Uani 1 1 d .
H55A H 0.3898 0.6108 0.2115 0.126 Uiso 1 1 calc R
H55B H 0.3565 0.6268 0.2503 0.126 Uiso 1 1 calc R
H55C H 0.4111 0.6539 0.2569 0.126 Uiso 1 1 calc R
C56 C 0.3294(3) 0.7459(4) 0.2817(2) 0.087(2) Uani 1 1 d .
H56A H 0.3399 0.7851 0.3004 0.131 Uiso 1 1 calc R
H56B H 0.3480 0.7078 0.2956 0.131 Uiso 1 1 calc R
H56C H 0.2947 0.7383 0.2818 0.131 Uiso 1 1 calc R
C57 C 0.2944(2) 0.8706(4) 0.2304(3) 0.100(2) Uani 1 1 d .
H57A H 0.2593 0.8620 0.2242 0.150 Uiso 1 1 calc R
H57B H 0.3008 0.9141 0.2183 0.150 Uiso 1 1 calc R
H57C H 0.3062 0.8691 0.2645 0.150 Uiso 1 1 calc R
N1 N 0.48097(14) 1.28740(18) 0.06625(13) 0.0461(8) Uani 1 1 d .
N2 N 0.34590(14) 1.34705(19) 0.10918(14) 0.0494(9) Uani 1 1 d .
N3 N 0.41876(13) 0.90772(18) 0.22488(12) 0.0447(8) Uani 1 1 d .
N4 N 0.41716(15) 1.15475(19) 0.21206(13) 0.0507(9) Uani 1 1 d .
N5 N 0.44077(15) 1.24959(19) 0.26183(14) 0.0512(9) Uani 1 1 d .
N6 N 0.45919(14) 1.13939(19) 0.29261(13) 0.0476(8) Uani 1 1 d .
O1 O 0.44459(12) 1.40741(14) 0.01995(11) 0.0467(7) Uani 1 1 d .
O2 O 0.39669(13) 1.29452(15) -0.01294(11) 0.0507(7) Uani 1 1 d .
O3 O 0.32674(12) 1.33412(16) 0.00857(12) 0.0528(8) Uani 1 1 d .
O4 O 0.37636(11) 1.44257(14) 0.04626(11) 0.0448(7) Uani 1 1 d .
O5 O 0.47311(11) 0.79885(15) 0.18928(10) 0.0429(6) Uani 1 1 d .
O6 O 0.44745(10) 0.78935(15) 0.27719(10) 0.0413(6) Uani 1 1 d .
Ru1 Ru 0.473273(15) 1.318307(17) -0.006565(13) 0.04837(12) Uani 1 1 d .
Ru2 Ru 0.304822(13) 1.406839(18) 0.055213(14) 0.04784(12) Uani 1 1 d .
Ru3 Ru 0.401220(12) 0.805225(17) 0.209119(11) 0.03937(11) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 C1 O4 125.9(4) . .
O1 C1 C2 117.8(4) . .
O4 C1 C2 116.2(4) . .
O2 C2 O3 125.5(4) . .
O2 C2 C1 117.1(4) . .
O3 C2 C1 117.4(4) . .
O6 C3 O5 126.1(4) . 2_655
O6 C3 C3 117.5(4) . 2_655
O5 C3 C3 116.4(4) 2_655 2_655
N2 C4 C5 123.2(4) . .
N2 C4 H4 118.4 . .
C5 C4 H4 118.4 . .
C4 C5 C6 118.0(4) . .
C4 C5 H5 121.0 . .
C6 C5 H5 121.0 . .
C7 C6 C5 119.3(4) . .
C7 C6 C20 120.1(4) . .
C5 C6 C20 120.6(4) . .
C8 C7 C6 118.5(4) . .
C8 C7 H7 120.7 . .
C6 C7 H7 120.7 . .
N2 C8 C7 123.1(5) . .
N2 C8 H8 118.4 . .
C7 C8 H8 118.4 . .
N1 C9 C10 123.0(4) . .
N1 C9 H9 118.5 . .
C10 C9 H9 118.5 . .
C9 C10 C11 119.0(4) . .
C9 C10 H10 120.5 . .
C11 C10 H10 120.5 . .
C10 C11 C12 118.2(4) . .
C10 C11 C21 120.6(4) . 2_655
C12 C11 C21 121.2(4) . 2_655
C13 C12 C11 118.9(4) . .
C13 C12 H12 120.6 . .
C11 C12 H12 120.6 . .
N1 C13 C12 122.5(4) . .
N1 C13 H13 118.7 . .
C12 C13 H13 118.7 . .
N3 C14 C15 122.7(5) . .
N3 C14 H14 118.6 . .
C15 C14 H14 118.6 . .
C16 C15 C14 118.4(4) . .
C16 C15 H15 120.8 . .
C14 C15 H15 120.8 . .
C15 C16 C17 120.0(4) . .
C15 C16 C19 119.2(4) . .
C17 C16 C19 120.7(4) . .
C16 C17 C18 118.0(4) . .
C16 C17 H17 121.0 . .
C18 C17 H17 121.0 . .
N3 C18 C17 121.5(4) . .
N3 C18 H18 119.3 . .
C17 C18 H18 119.3 . .
N4 C19 N6 125.6(4) . .
N4 C19 C16 116.7(4) . .
N6 C19 C16 117.7(4) . .
N5 C20 N4 126.1(4) . .
N5 C20 C6 118.3(4) . .
N4 C20 C6 115.6(4) . .
N5 C21 N6 125.5(4) . .
N5 C21 C11 117.2(4) . 2_655
N6 C21 C11 117.3(4) . 2_655
C27 C22 C23 120.8(6) . .
C27 C22 C28 118.0(12) . .
C23 C22 C28 121.1(12) . .
C27 C22 Ru1 70.9(4) . .
C23 C22 Ru1 70.7(5) . .
C28 C22 Ru1 129.8(5) . .
C22 C23 C24 118.9(7) . .
C22 C23 C29 119.7(11) . .
C24 C23 C29 121.3(11) . .
C22 C23 Ru1 71.3(4) . .
C24 C23 Ru1 71.9(3) . .
C29 C23 Ru1 127.2(5) . .
C25 C24 C23 119.3(7) . .
C25 C24 C30 121.7(7) . .
C23 C24 C30 119.0(8) . .
C25 C24 Ru1 71.0(3) . .
C23 C24 Ru1 69.6(4) . .
C30 C24 Ru1 132.5(5) . .
C26 C25 C24 120.5(5) . .
C26 C25 C31 119.0(5) . .
C24 C25 C31 120.2(6) . .
C26 C25 Ru1 70.1(3) . .
C24 C25 Ru1 71.1(3) . .
C31 C25 Ru1 126.5(4) . .
C25 C26 C27 119.0(6) . .
C25 C26 C32 118.5(6) . .
C27 C26 C32 122.5(7) . .
C25 C26 Ru1 72.5(3) . .
C27 C26 Ru1 70.7(4) . .
C32 C26 Ru1 128.5(4) . .
C22 C27 C26 121.3(7) . .
C22 C27 C33 122.0(8) . .
C26 C27 C33 116.7(9) . .
C22 C27 Ru1 72.0(5) . .
C26 C27 Ru1 70.9(3) . .
C33 C27 Ru1 128.3(5) . .
C22 C28 H28A 109.5 . .
C22 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
C22 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
C23 C29 H29A 109.5 . .
C23 C29 H29B 109.5 . .
H29A C29 H29B 109.5 . .
C23 C29 H29C 109.5 . .
H29A C29 H29C 109.5 . .
H29B C29 H29C 109.5 . .
C24 C30 H30A 109.5 . .
C24 C30 H30B 109.5 . .
H30A C30 H30B 109.5 . .
C24 C30 H30C 109.5 . .
H30A C30 H30C 109.5 . .
H30B C30 H30C 109.5 . .
C25 C31 H31A 109.5 . .
C25 C31 H31B 109.5 . .
H31A C31 H31B 109.5 . .
C25 C31 H31C 109.5 . .
H31A C31 H31C 109.5 . .
H31B C31 H31C 109.5 . .
C26 C32 H32A 109.5 . .
C26 C32 H32B 109.5 . .
H32A C32 H32B 109.5 . .
C26 C32 H32C 109.5 . .
H32A C32 H32C 109.5 . .
H32B C32 H32C 109.5 . .
C27 C33 H33A 109.5 . .
C27 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
C27 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
C39 C34 C35 117.6(7) . .
C39 C34 C40 114.8(10) . .
C35 C34 C40 127.5(11) . .
C39 C34 Ru2 71.1(4) . .
C35 C34 Ru2 69.0(4) . .
C40 C34 Ru2 127.5(6) . .
C36 C35 C34 121.0(6) . .
C36 C35 C41 122.6(9) . .
C34 C35 C41 116.4(10) . .
C36 C35 Ru2 72.1(4) . .
C34 C35 Ru2 72.1(4) . .
C41 C35 Ru2 129.2(5) . .
C37 C36 C35 118.7(6) . .
C37 C36 C42 122.2(10) . .
C35 C36 C42 119.0(10) . .
C37 C36 Ru2 73.1(4) . .
C35 C36 Ru2 69.0(4) . .
C42 C36 Ru2 127.4(5) . .
C36 C37 C38 122.2(7) . .
C36 C37 C43 116.5(9) . .
C38 C37 C43 121.1(10) . .
C36 C37 Ru2 72.0(4) . .
C38 C37 Ru2 69.3(3) . .
C43 C37 Ru2 128.9(6) . .
C39 C38 C37 120.2(7) . .
C39 C38 C44 125.0(8) . .
C37 C38 C44 114.7(8) . .
C39 C38 Ru2 72.6(4) . .
C37 C38 Ru2 72.0(3) . .
C44 C38 Ru2 124.1(5) . .
C38 C39 C34 120.1(6) . .
C38 C39 C45 116.9(9) . .
C34 C39 C45 122.9(9) . .
C38 C39 Ru2 70.5(3) . .
C34 C39 Ru2 70.9(4) . .
C45 C39 Ru2 129.3(4) . .
C34 C40 H40A 109.5 . .
C34 C40 H40B 109.5 . .
H40A C40 H40B 109.5 . .
C34 C40 H40C 109.5 . .
H40A C40 H40C 109.5 . .
H40B C40 H40C 109.5 . .
C35 C41 H41A 109.5 . .
C35 C41 H41B 109.5 . .
H41A C41 H41B 109.5 . .
C35 C41 H41C 109.5 . .
H41A C41 H41C 109.5 . .
H41B C41 H41C 109.5 . .
C36 C42 H42A 109.5 . .
C36 C42 H42B 109.5 . .
H42A C42 H42B 109.5 . .
C36 C42 H42C 109.5 . .
H42A C42 H42C 109.5 . .
H42B C42 H42C 109.5 . .
C37 C43 H43A 109.5 . .
C37 C43 H43B 109.5 . .
H43A C43 H43B 109.5 . .
C37 C43 H43C 109.5 . .
H43A C43 H43C 109.5 . .
H43B C43 H43C 109.5 . .
C38 C44 H44A 109.5 . .
C38 C44 H44B 109.5 . .
H44A C44 H44B 109.5 . .
C38 C44 H44C 109.5 . .
H44A C44 H44C 109.5 . .
H44B C44 H44C 109.5 . .
C39 C45 H45A 109.5 . .
C39 C45 H45B 109.5 . .
H45A C45 H45B 109.5 . .
C39 C45 H45C 109.5 . .
H45A C45 H45C 109.5 . .
H45B C45 H45C 109.5 . .
C47 C46 C51 121.0(5) . .
C47 C46 C52 120.0(6) . .
C51 C46 C52 119.0(6) . .
C47 C46 Ru3 70.7(3) . .
C51 C46 Ru3 70.2(3) . .
C52 C46 Ru3 131.8(4) . .
C46 C47 C48 118.9(5) . .
C46 C47 C53 121.9(6) . .
C48 C47 C53 119.1(6) . .
C46 C47 Ru3 72.4(3) . .
C48 C47 Ru3 70.8(3) . .
C53 C47 Ru3 124.8(4) . .
C49 C48 C47 122.0(5) . .
C49 C48 C54 119.0(6) . .
C47 C48 C54 118.9(5) . .
C49 C48 Ru3 72.7(3) . .
C47 C48 Ru3 70.5(3) . .
C54 C48 Ru3 127.1(4) . .
C48 C49 C50 117.9(5) . .
C48 C49 C55 122.2(5) . .
C50 C49 C55 119.7(5) . .
C48 C49 Ru3 70.0(3) . .
C50 C49 Ru3 68.4(3) . .
C55 C49 Ru3 128.2(4) . .
C49 C50 C51 120.3(5) . .
C49 C50 C56 120.4(5) . .
C51 C50 C56 119.3(5) . .
C49 C50 Ru3 73.3(3) . .
C51 C50 Ru3 71.5(3) . .
C56 C50 Ru3 125.7(4) . .
C46 C51 C50 119.7(5) . .
C46 C51 C57 120.1(6) . .
C50 C51 C57 120.0(6) . .
C46 C51 Ru3 72.0(3) . .
C50 C51 Ru3 69.7(3) . .
C57 C51 Ru3 127.2(4) . .
C46 C52 H52A 109.5 . .
C46 C52 H52B 109.5 . .
H52A C52 H52B 109.5 . .
C46 C52 H52C 109.5 . .
H52A C52 H52C 109.5 . .
H52B C52 H52C 109.5 . .
C47 C53 H53A 109.5 . .
C47 C53 H53B 109.5 . .
H53A C53 H53B 109.5 . .
C47 C53 H53C 109.5 . .
H53A C53 H53C 109.5 . .
H53B C53 H53C 109.5 . .
C48 C54 H54A 109.5 . .
C48 C54 H54B 109.5 . .
H54A C54 H54B 109.5 . .
C48 C54 H54C 109.5 . .
H54A C54 H54C 109.5 . .
H54B C54 H54C 109.5 . .
C49 C55 H55A 109.5 . .
C49 C55 H55B 109.5 . .
H55A C55 H55B 109.5 . .
C49 C55 H55C 109.5 . .
H55A C55 H55C 109.5 . .
H55B C55 H55C 109.5 . .
C50 C56 H56A 109.5 . .
C50 C56 H56B 109.5 . .
H56A C56 H56B 109.5 . .
C50 C56 H56C 109.5 . .
H56A C56 H56C 109.5 . .
H56B C56 H56C 109.5 . .
C51 C57 H57A 109.5 . .
C51 C57 H57B 109.5 . .
H57A C57 H57B 109.5 . .
C51 C57 H57C 109.5 . .
H57A C57 H57C 109.5 . .
H57B C57 H57C 109.5 . .
C9 N1 C13 117.9(4) . .
C9 N1 Ru1 120.4(3) . .
C13 N1 Ru1 120.3(3) . .
C4 N2 C8 117.7(4) . .
C4 N2 Ru2 122.6(3) . .
C8 N2 Ru2 119.6(3) . .
C14 N3 C18 119.2(4) . .
C14 N3 Ru3 119.6(3) . .
C18 N3 Ru3 121.1(3) . .
C19 N4 C20 114.4(4) . .
C20 N5 C21 114.6(4) . .
C21 N6 C19 113.7(4) . .
C1 O1 Ru1 112.6(3) . .
C2 O2 Ru1 113.1(3) . .
C2 O3 Ru2 112.9(3) . .
C1 O4 Ru2 113.5(3) . .
C3 O5 Ru3 113.6(3) 2_655 .
C3 O6 Ru3 113.0(2) . .
N1 Ru1 O2 87.30(14) . .
N1 Ru1 O1 83.43(13) . .
O2 Ru1 O1 78.47(12) . .
N1 Ru1 C27 89.4(2) . .
O2 Ru1 C27 152.4(3) . .
O1 Ru1 C27 128.4(3) . .
N1 Ru1 C26 110.91(18) . .
O2 Ru1 C26 161.13(17) . .
O1 Ru1 C26 98.17(16) . .
C27 Ru1 C26 38.4(2) . .
N1 Ru1 C23 125.2(3) . .
O2 Ru1 C23 91.6(3) . .
O1 Ru1 C23 149.6(3) . .
C27 Ru1 C23 68.2(4) . .
C26 Ru1 C23 82.0(3) . .
N1 Ru1 C22 95.6(3) . .
O2 Ru1 C22 116.1(3) . .
O1 Ru1 C22 165.4(4) . .
C27 Ru1 C22 37.1(4) . .
C26 Ru1 C22 68.5(3) . .
C23 Ru1 C22 38.0(4) . .
N1 Ru1 C25 147.31(18) . .
O2 Ru1 C25 123.79(18) . .
O1 Ru1 C25 92.60(15) . .
C27 Ru1 C25 67.8(2) . .
C26 Ru1 C25 37.4(2) . .
C23 Ru1 C25 69.0(2) . .
C22 Ru1 C25 80.3(2) . .
N1 Ru1 C24 163.3(2) . .
O2 Ru1 C24 95.6(2) . .
O1 Ru1 C24 113.3(2) . .
C27 Ru1 C24 80.5(3) . .
C26 Ru1 C24 68.5(2) . .
C23 Ru1 C24 38.4(3) . .
C22 Ru1 C24 68.3(3) . .
C25 Ru1 C24 37.9(2) . .
N2 Ru2 O3 83.53(14) . .
N2 Ru2 O4 83.47(13) . .
O3 Ru2 O4 78.13(12) . .
N2 Ru2 C35 115.6(3) . .
O3 Ru2 C35 160.4(3) . .
O4 Ru2 C35 99.03(19) . .
N2 Ru2 C38 125.8(2) . .
O3 Ru2 C38 91.7(2) . .
O4 Ru2 C38 148.1(2) . .
C35 Ru2 C38 80.5(2) . .
N2 Ru2 C36 153.1(3) . .
O3 Ru2 C36 121.5(3) . .
O4 Ru2 C36 91.8(2) . .
C35 Ru2 C36 38.9(3) . .
C38 Ru2 C36 67.7(3) . .
N2 Ru2 C34 92.5(2) . .
O3 Ru2 C34 151.5(3) . .
O4 Ru2 C34 129.6(3) . .
C35 Ru2 C34 38.9(3) . .
C38 Ru2 C34 67.8(3) . .
C36 Ru2 C34 70.2(3) . .
N2 Ru2 C39 97.9(2) . .
O3 Ru2 C39 114.6(2) . .
O4 Ru2 C39 167.3(2) . .
C35 Ru2 C39 68.9(3) . .
C38 Ru2 C39 36.9(3) . .
C36 Ru2 C39 81.2(3) . .
C34 Ru2 C39 37.9(3) . .
N2 Ru2 C37 164.5(2) . .
O3 Ru2 C37 96.5(3) . .
O4 Ru2 C37 111.8(2) . .
C35 Ru2 C37 66.3(3) . .
C38 Ru2 C37 38.8(3) . .
C36 Ru2 C37 35.0(3) . .
C34 Ru2 C37 80.1(3) . .
C39 Ru2 C37 67.9(3) . .
N3 Ru3 O6 82.91(12) . .
N3 Ru3 O5 85.80(13) . .
O6 Ru3 O5 78.13(11) . .
N3 Ru3 C50 122.89(18) . .
O6 Ru3 C50 93.72(16) . .
O5 Ru3 C50 149.32(17) . .
N3 Ru3 C51 95.55(17) . .
O6 Ru3 C51 119.78(18) . .
O5 Ru3 C51 162.08(17) . .
C50 Ru3 C51 38.8(2) . .
N3 Ru3 C47 116.26(19) . .
O6 Ru3 C47 159.43(19) . .
O5 Ru3 C47 95.09(16) . .
C50 Ru3 C47 82.21(19) . .
C51 Ru3 C47 68.2(2) . .
N3 Ru3 C48 154.26(18) . .
O6 Ru3 C48 121.19(17) . .
O5 Ru3 C48 90.40(15) . .
C50 Ru3 C48 68.41(19) . .
C51 Ru3 C48 80.6(2) . .
C47 Ru3 C48 38.7(2) . .
N3 Ru3 C46 93.67(19) . .
O6 Ru3 C46 157.17(19) . .
O5 Ru3 C46 124.27(19) . .
C50 Ru3 C46 69.2(2) . .
C51 Ru3 C46 37.9(2) . .
C47 Ru3 C46 36.9(2) . .
C48 Ru3 C46 67.7(2) . .
N3 Ru3 C49 161.11(17) . .
O6 Ru3 C49 95.11(16) . .
O5 Ru3 C49 112.27(16) . .
C50 Ru3 C49 38.3(2) . .
C51 Ru3 C49 69.0(2) . .
C47 Ru3 C49 69.2(2) . .
C48 Ru3 C49 37.38(19) . .
C46 Ru3 C49 80.8(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O1 1.247(5) .
C1 O4 1.258(5) .
C1 C2 1.534(6) .
C2 O2 1.254(6) .
C2 O3 1.270(6) .
C3 O6 1.240(5) .
C3 O5 1.257(5) 2_655
C3 C3 1.553(8) 2_655
C4 N2 1.324(6) .
C4 C5 1.387(6) .
C4 H4 0.9300 .
C5 C6 1.388(7) .
C5 H5 0.9300 .
C6 C7 1.382(7) .
C6 C20 1.499(6) .
C7 C8 1.364(7) .
C7 H7 0.9300 .
C8 N2 1.354(6) .
C8 H8 0.9300 .
C9 N1 1.343(6) .
C9 C10 1.375(7) .
C9 H9 0.9300 .
C10 C11 1.385(6) .
C10 H10 0.9300 .
C11 C12 1.400(6) .
C11 C21 1.473(6) 2_655
C12 C13 1.378(7) .
C12 H12 0.9300 .
C13 N1 1.346(6) .
C13 H13 0.9300 .
C14 N3 1.317(6) .
C14 C15 1.389(7) .
C14 H14 0.9300 .
C15 C16 1.361(7) .
C15 H15 0.9300 .
C16 C17 1.375(6) .
C16 C19 1.489(6) .
C17 C18 1.408(6) .
C17 H17 0.9300 .
C18 N3 1.333(6) .
C18 H18 0.9300 .
C19 N4 1.321(6) .
C19 N6 1.360(6) .
C20 N5 1.322(6) .
C20 N4 1.345(6) .
C21 N5 1.336(6) .
C21 N6 1.347(6) .
C21 C11 1.473(6) 2_655
C22 C27 1.384(14) .
C22 C23 1.418(14) .
C22 C28 1.532(10) .
C22 Ru1 2.183(7) .
C23 C24 1.443(11) .
C23 C29 1.481(11) .
C23 Ru1 2.176(6) .
C24 C25 1.433(8) .
C24 C30 1.453(11) .
C24 Ru1 2.206(6) .
C25 C26 1.404(8) .
C25 C31 1.505(8) .
C25 Ru1 2.205(5) .
C26 C27 1.428(9) .
C26 C32 1.509(8) .
C26 Ru1 2.173(5) .
C27 C33 1.553(12) .
C27 Ru1 2.170(7) .
C28 H28A 0.9600 .
C28 H28B 0.9600 .
C28 H28C 0.9600 .
C29 H29A 0.9600 .
C29 H29B 0.9600 .
C29 H29C 0.9600 .
C30 H30A 0.9600 .
C30 H30B 0.9600 .
C30 H30C 0.9600 .
C31 H31A 0.9600 .
C31 H31B 0.9600 .
C31 H31C 0.9600 .
C32 H32A 0.9600 .
C32 H32B 0.9600 .
C32 H32C 0.9600 .
C33 H33A 0.9600 .
C33 H33B 0.9600 .
C33 H33C 0.9600 .
C34 C39 1.416(11) .
C34 C35 1.440(11) .
C34 C40 1.512(12) .
C34 Ru2 2.179(6) .
C35 C36 1.438(12) .
C35 C41 1.536(11) .
C35 Ru2 2.137(6) .
C36 C37 1.312(11) .
C36 C42 1.526(10) .
C36 Ru2 2.178(6) .
C37 C38 1.443(10) .
C37 C43 1.533(13) .
C37 Ru2 2.191(5) .
C38 C39 1.374(10) .
C38 C44 1.529(11) .
C38 Ru2 2.155(5) .
C39 C45 1.537(10) .
C39 Ru2 2.181(6) .
C40 H40A 0.9600 .
C40 H40B 0.9600 .
C40 H40C 0.9600 .
C41 H41A 0.9600 .
C41 H41B 0.9600 .
C41 H41C 0.9600 .
C42 H42A 0.9600 .
C42 H42B 0.9600 .
C42 H42C 0.9600 .
C43 H43A 0.9600 .
C43 H43B 0.9600 .
C43 H43C 0.9600 .
C44 H44A 0.9600 .
C44 H44B 0.9600 .
C44 H44C 0.9600 .
C45 H45A 0.9600 .
C45 H45B 0.9600 .
C45 H45C 0.9600 .
C46 C47 1.390(8) .
C46 C51 1.422(8) .
C46 C52 1.506(8) .
C46 Ru3 2.204(5) .
C47 C48 1.448(8) .
C47 C53 1.501(8) .
C47 Ru3 2.183(4) .
C48 C49 1.413(7) .
C48 C54 1.535(8) .
C48 Ru3 2.186(5) .
C49 C50 1.438(7) .
C49 C55 1.488(8) .
C49 Ru3 2.221(5) .
C50 C51 1.440(8) .
C50 C56 1.521(8) .
C50 Ru3 2.156(5) .
C51 C57 1.539(8) .
C51 Ru3 2.181(5) .
C52 H52A 0.9600 .
C52 H52B 0.9600 .
C52 H52C 0.9600 .
C53 H53A 0.9600 .
C53 H53B 0.9600 .
C53 H53C 0.9600 .
C54 H54A 0.9600 .
C54 H54B 0.9600 .
C54 H54C 0.9600 .
C55 H55A 0.9600 .
C55 H55B 0.9600 .
C55 H55C 0.9600 .
C56 H56A 0.9600 .
C56 H56B 0.9600 .
C56 H56C 0.9600 .
C57 H57A 0.9600 .
C57 H57B 0.9600 .
C57 H57C 0.9600 .
N1 Ru1 2.118(4) .
N2 Ru2 2.102(4) .
N3 Ru3 2.129(4) .
O1 Ru1 2.127(3) .
O2 Ru1 2.124(3) .
O3 Ru2 2.110(4) .
O4 Ru2 2.136(3) .
O5 C3 1.257(5) 2_655
O5 Ru3 2.135(3) .
O6 Ru3 2.135(3) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O1 C1 C2 O2 4.8(6) . .
O4 C1 C2 O2 -175.4(4) . .
O1 C1 C2 O3 -176.4(4) . .
O4 C1 C2 O3 3.4(5) . .
N2 C4 C5 C6 1.5(8) . .
C4 C5 C6 C7 1.5(8) . .
C4 C5 C6 C20 -177.9(5) . .
C5 C6 C7 C8 -3.6(8) . .
C20 C6 C7 C8 175.9(5) . .
C6 C7 C8 N2 2.8(8) . .
N1 C9 C10 C11 0.1(7) . .
C9 C10 C11 C12 -5.4(7) . .
C9 C10 C11 C21 173.7(4) . 2_655
C10 C11 C12 C13 5.5(7) . .
C21 C11 C12 C13 -173.6(5) 2_655 .
C11 C12 C13 N1 -0.2(8) . .
N3 C14 C15 C16 4.6(8) . .
C14 C15 C16 C17 -2.1(8) . .
C14 C15 C16 C19 -177.5(5) . .
C15 C16 C17 C18 -1.0(8) . .
C19 C16 C17 C18 174.4(4) . .
C16 C17 C18 N3 1.9(8) . .
C15 C16 C19 N4 27.8(7) . .
C17 C16 C19 N4 -147.6(5) . .
C15 C16 C19 N6 -152.9(5) . .
C17 C16 C19 N6 31.7(7) . .
C7 C6 C20 N5 -168.6(5) . .
C5 C6 C20 N5 10.8(7) . .
C7 C6 C20 N4 11.6(7) . .
C5 C6 C20 N4 -169.0(5) . .
C27 C22 C23 C24 3.6(10) . .
C28 C22 C23 C24 -178.6(6) . .
Ru1 C22 C23 C24 55.9(5) . .
C27 C22 C23 C29 -175.1(6) . .
C28 C22 C23 C29 2.8(11) . .
Ru1 C22 C23 C29 -122.8(6) . .
C27 C22 C23 Ru1 -52.3(6) . .
C28 C22 C23 Ru1 125.5(7) . .
C22 C23 C24 C25 -2.9(9) . .
C29 C23 C24 C25 175.7(6) . .
Ru1 C23 C24 C25 52.7(5) . .
C22 C23 C24 C30 176.3(7) . .
C29 C23 C24 C30 -5.1(10) . .
Ru1 C23 C24 C30 -128.2(6) . .
C22 C23 C24 Ru1 -55.6(5) . .
C29 C23 C24 Ru1 123.0(7) . .
C23 C24 C25 C26 -0.4(8) . .
C30 C24 C25 C26 -179.6(6) . .
Ru1 C24 C25 C26 51.6(4) . .
C23 C24 C25 C31 -173.9(5) . .
C30 C24 C25 C31 7.0(9) . .
Ru1 C24 C25 C31 -121.8(5) . .
C23 C24 C25 Ru1 -52.1(5) . .
C30 C24 C25 Ru1 128.8(6) . .
C24 C25 C26 C27 3.1(7) . .
C31 C25 C26 C27 176.6(5) . .
Ru1 C25 C26 C27 55.1(4) . .
C24 C25 C26 C32 -177.0(5) . .
C31 C25 C26 C32 -3.4(7) . .
Ru1 C25 C26 C32 -124.9(5) . .
C24 C25 C26 Ru1 -52.1(4) . .
C31 C25 C26 Ru1 121.5(5) . .
C23 C22 C27 C26 -1.0(10) . .
C28 C22 C27 C26 -178.9(6) . .
Ru1 C22 C27 C26 -53.2(5) . .
C23 C22 C27 C33 176.6(6) . .
C28 C22 C27 C33 -1.3(10) . .
Ru1 C22 C27 C33 124.4(6) . .
C23 C22 C27 Ru1 52.2(6) . .
C28 C22 C27 Ru1 -125.7(6) . .
C25 C26 C27 C22 -2.4(8) . .
C32 C26 C27 C22 177.6(6) . .
Ru1 C26 C27 C22 53.6(5) . .
C25 C26 C27 C33 179.9(5) . .
C32 C26 C27 C33 -0.1(8) . .
Ru1 C26 C27 C33 -124.1(5) . .
C25 C26 C27 Ru1 -56.0(4) . .
C32 C26 C27 Ru1 124.0(5) . .
C39 C34 C35 C36 1.4(9) . .
C40 C34 C35 C36 176.9(8) . .
Ru2 C34 C35 C36 55.1(5) . .
C39 C34 C35 C41 -179.2(6) . .
C40 C34 C35 C41 -3.7(11) . .
Ru2 C34 C35 C41 -125.5(6) . .
C39 C34 C35 Ru2 -53.7(5) . .
C40 C34 C35 Ru2 121.8(8) . .
C34 C35 C36 C37 0.4(9) . .
C41 C35 C36 C37 -178.9(7) . .
Ru2 C35 C36 C37 55.6(6) . .
C34 C35 C36 C42 -177.2(6) . .
C41 C35 C36 C42 3.4(10) . .
Ru2 C35 C36 C42 -122.1(6) . .
C34 C35 C36 Ru2 -55.1(5) . .
C41 C35 C36 Ru2 125.5(7) . .
C35 C36 C37 C38 -3.8(10) . .
C42 C36 C37 C38 173.8(6) . .
Ru2 C36 C37 C38 49.8(6) . .
C35 C36 C37 C43 -178.8(7) . .
C42 C36 C37 C43 -1.2(10) . .
Ru2 C36 C37 C43 -125.2(7) . .
C35 C36 C37 Ru2 -53.6(5) . .
C42 C36 C37 Ru2 124.0(7) . .
C36 C37 C38 C39 5.4(9) . .
C43 C37 C38 C39 -179.8(7) . .
Ru2 C37 C38 C39 56.4(5) . .
C36 C37 C38 C44 -170.9(7) . .
C43 C37 C38 C44 3.9(9) . .
Ru2 C37 C38 C44 -119.9(5) . .
C36 C37 C38 Ru2 -51.0(6) . .
C43 C37 C38 Ru2 123.8(7) . .
C37 C38 C39 C34 -3.4(9) . .
C44 C38 C39 C34 172.5(6) . .
Ru2 C38 C39 C34 52.7(5) . .
C37 C38 C39 C45 178.9(5) . .
C44 C38 C39 C45 -5.3(9) . .
Ru2 C38 C39 C45 -125.0(5) . .
C37 C38 C39 Ru2 -56.1(5) . .
C44 C38 C39 Ru2 119.8(6) . .
C35 C34 C39 C38 0.2(9) . .
C40 C34 C39 C38 -175.9(7) . .
Ru2 C34 C39 C38 -52.5(5) . .
C35 C34 C39 C45 177.8(5) . .
C40 C34 C39 C45 1.7(10) . .
Ru2 C34 C39 C45 125.1(6) . .
C35 C34 C39 Ru2 52.7(5) . .
C40 C34 C39 Ru2 -123.4(7) . .
C51 C46 C47 C48 4.2(7) . .
C52 C46 C47 C48 -177.0(5) . .
Ru3 C46 C47 C48 55.2(4) . .
C51 C46 C47 C53 -171.5(5) . .
C52 C46 C47 C53 7.3(8) . .
Ru3 C46 C47 C53 -120.5(5) . .
C51 C46 C47 Ru3 -51.0(4) . .
C52 C46 C47 Ru3 127.8(5) . .
C46 C47 C48 C49 -2.4(7) . .
C53 C47 C48 C49 173.4(5) . .
Ru3 C47 C48 C49 53.6(4) . .
C46 C47 C48 C54 -178.4(5) . .
C53 C47 C48 C54 -2.6(7) . .
Ru3 C47 C48 C54 -122.4(4) . .
C46 C47 C48 Ru3 -56.0(4) . .
C53 C47 C48 Ru3 119.9(4) . .
C47 C48 C49 C50 -2.1(7) . .
C54 C48 C49 C50 173.9(4) . .
Ru3 C48 C49 C50 50.5(4) . .
C47 C48 C49 C55 -175.9(5) . .
C54 C48 C49 C55 0.1(7) . .
Ru3 C48 C49 C55 -123.3(5) . .
C47 C48 C49 Ru3 -52.6(4) . .
C54 C48 C49 Ru3 123.4(4) . .
C48 C49 C50 C51 4.8(7) . .
C55 C49 C50 C51 178.8(5) . .
Ru3 C49 C50 C51 56.1(4) . .
C48 C49 C50 C56 -173.3(5) . .
C55 C49 C50 C56 0.7(7) . .
Ru3 C49 C50 C56 -122.0(5) . .
C48 C49 C50 Ru3 -51.2(4) . .
C55 C49 C50 Ru3 122.7(5) . .
C47 C46 C51 C50 -1.5(7) . .
C52 C46 C51 C50 179.7(5) . .
Ru3 C46 C51 C50 -52.7(4) . .
C47 C46 C51 C57 174.3(5) . .
C52 C46 C51 C57 -4.5(8) . .
Ru3 C46 C51 C57 123.1(5) . .
C47 C46 C51 Ru3 51.2(4) . .
C52 C46 C51 Ru3 -127.6(5) . .
C49 C50 C51 C46 -3.2(7) . .
C56 C50 C51 C46 175.0(5) . .
Ru3 C50 C51 C46 53.8(4) . .
C49 C50 C51 C57 -179.0(5) . .
C56 C50 C51 C57 -0.8(7) . .
Ru3 C50 C51 C57 -122.0(5) . .
C49 C50 C51 Ru3 -56.9(4) . .
C56 C50 C51 Ru3 121.2(5) . .
C10 C9 N1 C13 5.2(7) . .
C10 C9 N1 Ru1 -161.6(4) . .
C12 C13 N1 C9 -5.1(7) . .
C12 C13 N1 Ru1 161.7(4) . .
C5 C4 N2 C8 -2.3(8) . .
C5 C4 N2 Ru2 175.9(4) . .
C7 C8 N2 C4 0.1(8) . .
C7 C8 N2 Ru2 -178.2(4) . .
C15 C14 N3 C18 -3.8(8) . .
C15 C14 N3 Ru3 171.9(4) . .
C17 C18 N3 C14 0.5(7) . .
C17 C18 N3 Ru3 -175.2(4) . .
N6 C19 N4 C20 -2.5(7) . .
C16 C19 N4 C20 176.7(4) . .
N5 C20 N4 C19 3.8(7) . .
C6 C20 N4 C19 -176.4(4) . .
N4 C20 N5 C21 -2.7(7) . .
C6 C20 N5 C21 177.6(4) . .
N6 C21 N5 C20 0.2(7) . .
C11 C21 N5 C20 -178.3(4) 2_655 .
N5 C21 N6 C19 0.9(7) . .
C11 C21 N6 C19 179.4(4) 2_655 .
N4 C19 N6 C21 0.4(7) . .
C16 C19 N6 C21 -178.8(4) . .
O4 C1 O1 Ru1 170.2(3) . .
C2 C1 O1 Ru1 -10.0(4) . .
O3 C2 O2 Ru1 -175.5(3) . .
C1 C2 O2 Ru1 3.2(4) . .
O2 C2 O3 Ru2 166.4(3) . .
C1 C2 O3 Ru2 -12.3(4) . .
O1 C1 O4 Ru2 -172.9(3) . .
C2 C1 O4 Ru2 7.4(4) . .
O5 C3 O6 Ru3 166.9(3) 2_655 .
C3 C3 O6 Ru3 -13.6(3) 2_655 .
C9 N1 Ru1 O2 -131.1(4) . .
C13 N1 Ru1 O2 62.4(4) . .
C9 N1 Ru1 O1 -52.4(3) . .
C13 N1 Ru1 O1 141.1(4) . .
C9 N1 Ru1 C27 76.3(4) . .
C13 N1 Ru1 C27 -90.2(4) . .
C9 N1 Ru1 C26 43.8(4) . .
C13 N1 Ru1 C26 -122.7(4) . .
C9 N1 Ru1 C23 138.8(5) . .
C13 N1 Ru1 C23 -27.7(5) . .
C9 N1 Ru1 C22 112.9(5) . .
C13 N1 Ru1 C22 -53.6(5) . .
C9 N1 Ru1 C25 32.1(5) . .
C13 N1 Ru1 C25 -134.4(4) . .
C9 N1 Ru1 C24 128.5(7) . .
C13 N1 Ru1 C24 -38.0(9) . .
C2 O2 Ru1 N1 77.6(3) . .
C2 O2 Ru1 O1 -6.3(3) . .
C2 O2 Ru1 C27 161.0(4) . .
C2 O2 Ru1 C26 -87.7(6) . .
C2 O2 Ru1 C23 -157.3(4) . .
C2 O2 Ru1 C22 172.5(4) . .
C2 O2 Ru1 C25 -91.6(3) . .
C2 O2 Ru1 C24 -118.9(3) . .
C1 O1 Ru1 N1 -79.7(3) . .
C1 O1 Ru1 O2 8.9(3) . .
C1 O1 Ru1 C27 -163.6(3) . .
C1 O1 Ru1 C26 170.0(3) . .
C1 O1 Ru1 C23 82.0(5) . .
C1 O1 Ru1 C22 -166.8(10) . .
C1 O1 Ru1 C25 132.9(3) . .
C1 O1 Ru1 C24 100.0(3) . .
C22 C27 Ru1 N1 100.2(4) . .
C26 C27 Ru1 N1 -126.1(4) . .
C33 C27 Ru1 N1 -16.7(9) . .
C22 C27 Ru1 O2 17.3(7) . .
C26 C27 Ru1 O2 151.0(3) . .
C33 C27 Ru1 O2 -99.6(10) . .
C22 C27 Ru1 O1 -178.7(4) . .
C26 C27 Ru1 O1 -45.0(4) . .
C33 C27 Ru1 O1 64.4(9) . .
C22 C27 Ru1 C26 -133.7(6) . .
C33 C27 Ru1 C26 109.4(10) . .
C22 C27 Ru1 C23 -28.4(4) . .
C26 C27 Ru1 C23 105.2(4) . .
C33 C27 Ru1 C23 -145.4(10) . .
C26 C27 Ru1 C22 133.7(6) . .
C33 C27 Ru1 C22 -116.9(10) . .
C22 C27 Ru1 C25 -103.8(5) . .
C26 C27 Ru1 C25 29.9(3) . .
C33 C27 Ru1 C25 139.3(9) . .
C22 C27 Ru1 C24 -66.4(5) . .
C26 C27 Ru1 C24 67.2(4) . .
C33 C27 Ru1 C24 176.6(9) . .
C25 C26 Ru1 N1 -169.6(3) . .
C27 C26 Ru1 N1 59.9(4) . .
C32 C26 Ru1 N1 -56.7(6) . .
C25 C26 Ru1 O2 -5.4(7) . .
C27 C26 Ru1 O2 -135.9(6) . .
C32 C26 Ru1 O2 107.5(7) . .
C25 C26 Ru1 O1 -83.5(3) . .
C27 C26 Ru1 O1 145.9(4) . .
C32 C26 Ru1 O1 29.3(6) . .
C25 C26 Ru1 C27 130.5(5) . .
C32 C26 Ru1 C27 -116.6(8) . .
C25 C26 Ru1 C23 65.7(4) . .
C27 C26 Ru1 C23 -64.8(5) . .
C32 C26 Ru1 C23 178.6(7) . .
C25 C26 Ru1 C22 102.6(5) . .
C27 C26 Ru1 C22 -28.0(5) . .
C32 C26 Ru1 C22 -144.6(7) . .
C27 C26 Ru1 C25 -130.5(5) . .
C32 C26 Ru1 C25 112.9(7) . .
C25 C26 Ru1 C24 28.3(3) . .
C27 C26 Ru1 C24 -102.2(4) . .
C32 C26 Ru1 C24 141.2(7) . .
C22 C23 Ru1 N1 -44.9(5) . .
C24 C23 Ru1 N1 -175.2(4) . .
C29 C23 Ru1 N1 68.7(13) . .
C22 C23 Ru1 O2 -132.8(5) . .
C24 C23 Ru1 O2 96.9(5) . .
C29 C23 Ru1 O2 -19.1(12) . .
C22 C23 Ru1 O1 157.5(5) . .
C24 C23 Ru1 O1 27.2(8) . .
C29 C23 Ru1 O1 -88.8(11) . .
C22 C23 Ru1 C27 27.8(4) . .
C24 C23 Ru1 C27 -102.5(5) . .
C29 C23 Ru1 C27 141.4(13) . .
C22 C23 Ru1 C26 65.1(5) . .
C24 C23 Ru1 C26 -65.3(5) . .
C29 C23 Ru1 C26 178.7(12) . .
C24 C23 Ru1 C22 -130.3(7) . .
C29 C23 Ru1 C22 113.6(14) . .
C22 C23 Ru1 C25 101.4(5) . .
C24 C23 Ru1 C25 -28.9(4) . .
C29 C23 Ru1 C25 -144.9(13) . .
C22 C23 Ru1 C24 130.3(7) . .
C29 C23 Ru1 C24 -116.0(14) . .
C27 C22 Ru1 N1 -81.4(4) . .
C23 C22 Ru1 N1 144.6(4) . .
C28 C22 Ru1 N1 29.6(14) . .
C27 C22 Ru1 O2 -171.2(3) . .
C23 C22 Ru1 O2 54.8(4) . .
C28 C22 Ru1 O2 -60.1(15) . .
C27 C22 Ru1 O1 4.2(13) . .
C23 C22 Ru1 O1 -129.9(11) . .
C28 C22 Ru1 O1 115.2(12) . .
C23 C22 Ru1 C27 -134.0(6) . .
C28 C22 Ru1 C27 111.0(16) . .
C27 C22 Ru1 C26 28.9(4) . .
C23 C22 Ru1 C26 -105.2(4) . .
C28 C22 Ru1 C26 139.9(15) . .
C27 C22 Ru1 C23 134.0(6) . .
C28 C22 Ru1 C23 -114.9(16) . .
C27 C22 Ru1 C25 65.9(4) . .
C23 C22 Ru1 C25 -68.2(4) . .
C28 C22 Ru1 C25 176.9(14) . .
C27 C22 Ru1 C24 103.4(4) . .
C23 C22 Ru1 C24 -30.7(4) . .
C28 C22 Ru1 C24 -145.6(15) . .
C26 C25 Ru1 N1 18.2(5) . .
C24 C25 Ru1 N1 152.3(4) . .
C31 C25 Ru1 N1 -93.7(6) . .
C26 C25 Ru1 O2 177.9(3) . .
C24 C25 Ru1 O2 -48.0(4) . .
C31 C25 Ru1 O2 66.0(6) . .
C26 C25 Ru1 O1 100.1(3) . .
C24 C25 Ru1 O1 -125.9(4) . .
C31 C25 Ru1 O1 -11.8(6) . .
C26 C25 Ru1 C27 -30.7(4) . .
C24 C25 Ru1 C27 103.4(5) . .
C31 C25 Ru1 C27 -142.6(6) . .
C24 C25 Ru1 C26 134.1(5) . .
C31 C25 Ru1 C26 -111.9(7) . .
C26 C25 Ru1 C23 -104.8(5) . .
C24 C25 Ru1 C23 29.3(5) . .
C31 C25 Ru1 C23 143.3(7) . .
C26 C25 Ru1 C22 -67.1(5) . .
C24 C25 Ru1 C22 67.0(5) . .
C31 C25 Ru1 C22 -179.0(7) . .
C26 C25 Ru1 C24 -134.1(5) . .
C31 C25 Ru1 C24 114.0(7) . .
C25 C24 Ru1 N1 -119.2(6) . .
C23 C24 Ru1 N1 13.6(10) . .
C30 C24 Ru1 N1 124.8(9) . .
C25 C24 Ru1 O2 141.6(3) . .
C23 C24 Ru1 O2 -85.6(5) . .
C30 C24 Ru1 O2 25.6(8) . .
C25 C24 Ru1 O1 61.8(4) . .
C23 C24 Ru1 O1 -165.4(5) . .
C30 C24 Ru1 O1 -54.2(8) . .
C25 C24 Ru1 C27 -66.0(4) . .
C23 C24 Ru1 C27 66.8(5) . .
C30 C24 Ru1 C27 178.0(8) . .
C25 C24 Ru1 C26 -28.0(3) . .
C23 C24 Ru1 C26 104.8(5) . .
C30 C24 Ru1 C26 -144.0(8) . .
C25 C24 Ru1 C23 -132.8(7) . .
C30 C24 Ru1 C23 111.2(10) . .
C25 C24 Ru1 C22 -102.5(5) . .
C23 C24 Ru1 C22 30.3(5) . .
C30 C24 Ru1 C22 141.5(9) . .
C23 C24 Ru1 C25 132.8(7) . .
C30 C24 Ru1 C25 -116.0(9) . .
C4 N2 Ru2 O3 136.3(4) . .
C8 N2 Ru2 O3 -45.5(4) . .
C4 N2 Ru2 O4 57.6(4) . .
C8 N2 Ru2 O4 -124.2(4) . .
C4 N2 Ru2 C35 -39.3(5) . .
C8 N2 Ru2 C35 138.9(4) . .
C4 N2 Ru2 C38 -136.2(4) . .
C8 N2 Ru2 C38 42.0(5) . .
C4 N2 Ru2 C36 -23.5(7) . .
C8 N2 Ru2 C36 154.6(5) . .
C4 N2 Ru2 C34 -71.9(5) . .
C8 N2 Ru2 C34 106.2(5) . .
C4 N2 Ru2 C39 -109.6(4) . .
C8 N2 Ru2 C39 68.5(4) . .
C4 N2 Ru2 C37 -132.7(10) . .
C8 N2 Ru2 C37 45.5(11) . .
C2 O3 Ru2 N2 -72.5(3) . .
C2 O3 Ru2 O4 12.2(3) . .
C2 O3 Ru2 C35 95.7(6) . .
C2 O3 Ru2 C38 161.7(3) . .
C2 O3 Ru2 C36 97.0(4) . .
C2 O3 Ru2 C34 -155.8(4) . .
C2 O3 Ru2 C39 -168.3(3) . .
C2 O3 Ru2 C37 123.1(3) . .
C1 O4 Ru2 N2 74.3(3) . .
C1 O4 Ru2 O3 -10.4(3) . .
C1 O4 Ru2 C35 -170.7(4) . .
C1 O4 Ru2 C38 -84.2(4) . .
C1 O4 Ru2 C36 -132.3(4) . .
C1 O4 Ru2 C34 162.2(3) . .
C1 O4 Ru2 C39 171.4(9) . .
C1 O4 Ru2 C37 -102.8(4) . .
C36 C35 Ru2 N2 168.7(4) . .
C34 C35 Ru2 N2 -59.0(4) . .
C41 C35 Ru2 N2 50.9(11) . .
C36 C35 Ru2 O3 1.7(8) . .
C34 C35 Ru2 O3 134.0(6) . .
C41 C35 Ru2 O3 -116.1(10) . .
C36 C35 Ru2 O4 81.6(4) . .
C34 C35 Ru2 O4 -146.0(4) . .
C41 C35 Ru2 O4 -36.2(11) . .
C36 C35 Ru2 C38 -66.0(4) . .
C34 C35 Ru2 C38 66.3(4) . .
C41 C35 Ru2 C38 176.1(11) . .
C34 C35 Ru2 C36 132.3(6) . .
C41 C35 Ru2 C36 -117.8(12) . .
C36 C35 Ru2 C34 -132.3(6) . .
C41 C35 Ru2 C34 109.8(12) . .
C36 C35 Ru2 C39 -102.5(4) . .
C34 C35 Ru2 C39 29.8(4) . .
C41 C35 Ru2 C39 139.7(11) . .
C36 C35 Ru2 C37 -28.2(4) . .
C34 C35 Ru2 C37 104.1(5) . .
C41 C35 Ru2 C37 -146.1(11) . .
C39 C38 Ru2 N2 47.5(5) . .
C37 C38 Ru2 N2 178.5(4) . .
C44 C38 Ru2 N2 -73.4(8) . .
C39 C38 Ru2 O3 130.8(4) . .
C37 C38 Ru2 O3 -98.2(5) . .
C44 C38 Ru2 O3 9.9(7) . .
C39 C38 Ru2 O4 -159.2(4) . .
C37 C38 Ru2 O4 -28.1(7) . .
C44 C38 Ru2 O4 80.0(8) . .
C39 C38 Ru2 C35 -67.3(5) . .
C37 C38 Ru2 C35 63.7(5) . .
C44 C38 Ru2 C35 171.8(8) . .
C39 C38 Ru2 C36 -105.7(5) . .
C37 C38 Ru2 C36 25.3(5) . .
C44 C38 Ru2 C36 133.5(8) . .
C39 C38 Ru2 C34 -28.9(4) . .
C37 C38 Ru2 C34 102.1(5) . .
C44 C38 Ru2 C34 -149.7(8) . .
C37 C38 Ru2 C39 131.0(6) . .
C44 C38 Ru2 C39 -120.8(9) . .
C39 C38 Ru2 C37 -131.0(6) . .
C44 C38 Ru2 C37 108.1(9) . .
C37 C36 Ru2 N2 -153.9(5) . .
C35 C36 Ru2 N2 -23.0(7) . .
C42 C36 Ru2 N2 88.1(12) . .
C37 C36 Ru2 O3 49.8(5) . .
C35 C36 Ru2 O3 -179.3(3) . .
C42 C36 Ru2 O3 -68.2(11) . .
C37 C36 Ru2 O4 127.0(5) . .
C35 C36 Ru2 O4 -102.1(4) . .
C42 C36 Ru2 O4 9.0(11) . .
C37 C36 Ru2 C35 -130.9(6) . .
C42 C36 Ru2 C35 111.1(12) . .
C37 C36 Ru2 C38 -27.9(5) . .
C35 C36 Ru2 C38 103.0(4) . .
C42 C36 Ru2 C38 -145.9(11) . .
C37 C36 Ru2 C34 -101.3(5) . .
C35 C36 Ru2 C34 29.6(4) . .
C42 C36 Ru2 C34 140.7(11) . .
C37 C36 Ru2 C39 -63.7(5) . .
C35 C36 Ru2 C39 67.2(4) . .
C42 C36 Ru2 C39 178.3(11) . .
C35 C36 Ru2 C37 130.9(6) . .
C42 C36 Ru2 C37 -118.0(13) . .
C39 C34 Ru2 N2 -99.7(4) . .
C35 C34 Ru2 N2 129.3(4) . .
C40 C34 Ru2 N2 7.6(11) . .
C39 C34 Ru2 O3 -18.7(7) . .
C35 C34 Ru2 O3 -149.6(5) . .
C40 C34 Ru2 O3 88.6(12) . .
C39 C34 Ru2 O4 176.7(3) . .
C35 C34 Ru2 O4 45.7(5) . .
C40 C34 Ru2 O4 -76.1(12) . .
C39 C34 Ru2 C35 131.0(6) . .
C40 C34 Ru2 C35 -121.8(13) . .
C39 C34 Ru2 C38 28.2(4) . .
C35 C34 Ru2 C38 -102.8(5) . .
C40 C34 Ru2 C38 135.5(12) . .
C39 C34 Ru2 C36 101.4(5) . .
C35 C34 Ru2 C36 -29.6(4) . .
C40 C34 Ru2 C36 -151.4(12) . .
C35 C34 Ru2 C39 -131.0(6) . .
C40 C34 Ru2 C39 107.3(13) . .
C39 C34 Ru2 C37 66.6(5) . .
C35 C34 Ru2 C37 -64.4(5) . .
C40 C34 Ru2 C37 173.9(12) . .
C38 C39 Ru2 N2 -142.9(4) . .
C34 C39 Ru2 N2 83.9(4) . .
C45 C39 Ru2 N2 -33.5(10) . .
C38 C39 Ru2 O3 -56.4(4) . .
C34 C39 Ru2 O3 170.3(4) . .
C45 C39 Ru2 O3 53.0(10) . .
C38 C39 Ru2 O4 121.6(9) . .
C34 C39 Ru2 O4 -11.7(11) . .
C45 C39 Ru2 O4 -129.0(10) . .
C38 C39 Ru2 C35 102.7(5) . .
C34 C39 Ru2 C35 -30.6(5) . .
C45 C39 Ru2 C35 -148.0(10) . .
C34 C39 Ru2 C38 -133.3(6) . .
C45 C39 Ru2 C38 109.4(11) . .
C38 C39 Ru2 C36 64.3(5) . .
C34 C39 Ru2 C36 -69.0(5) . .
C45 C39 Ru2 C36 173.7(10) . .
C38 C39 Ru2 C34 133.3(6) . .
C45 C39 Ru2 C34 -117.4(11) . .
C38 C39 Ru2 C37 30.6(4) . .
C34 C39 Ru2 C37 -102.6(5) . .
C45 C39 Ru2 C37 140.0(10) . .
C36 C37 Ru2 N2 131.8(10) . .
C38 C37 Ru2 N2 -4.5(13) . .
C43 C37 Ru2 N2 -118.3(11) . .
C36 C37 Ru2 O3 -139.1(5) . .
C38 C37 Ru2 O3 84.7(4) . .
C43 C37 Ru2 O3 -29.1(11) . .
C36 C37 Ru2 O4 -59.3(5) . .
C38 C37 Ru2 O4 164.4(4) . .
C43 C37 Ru2 O4 50.7(11) . .
C36 C37 Ru2 C35 31.3(5) . .
C38 C37 Ru2 C35 -105.0(5) . .
C43 C37 Ru2 C35 141.2(11) . .
C36 C37 Ru2 C38 136.3(7) . .
C43 C37 Ru2 C38 -113.8(12) . .
C38 C37 Ru2 C36 -136.3(7) . .
C43 C37 Ru2 C36 109.9(12) . .
C36 C37 Ru2 C34 69.5(5) . .
C38 C37 Ru2 C34 -66.8(5) . .
C43 C37 Ru2 C34 179.4(11) . .
C36 C37 Ru2 C39 107.0(6) . .
C38 C37 Ru2 C39 -29.3(4) . .
C43 C37 Ru2 C39 -143.1(11) . .
C14 N3 Ru3 O6 143.6(4) . .
C18 N3 Ru3 O6 -40.7(4) . .
C14 N3 Ru3 O5 65.1(4) . .
C18 N3 Ru3 O5 -119.2(4) . .
C14 N3 Ru3 C50 -126.5(4) . .
C18 N3 Ru3 C50 49.2(4) . .
C14 N3 Ru3 C51 -97.0(4) . .
C18 N3 Ru3 C51 78.7(4) . .
C14 N3 Ru3 C47 -28.5(4) . .
C18 N3 Ru3 C47 147.1(4) . .
C14 N3 Ru3 C48 -17.1(6) . .
C18 N3 Ru3 C48 158.6(4) . .
C14 N3 Ru3 C46 -59.0(4) . .
C18 N3 Ru3 C46 116.6(4) . .
C14 N3 Ru3 C49 -131.3(5) . .
C18 N3 Ru3 C49 44.4(7) . .
C3 O6 Ru3 N3 -76.8(3) . .
C3 O6 Ru3 O5 10.4(3) . .
C3 O6 Ru3 C50 160.5(3) . .
C3 O6 Ru3 C51 -169.1(3) . .
C3 O6 Ru3 C47 82.8(5) . .
C3 O6 Ru3 C48 93.6(3) . .
C3 O6 Ru3 C46 -159.4(5) . .
C3 O6 Ru3 C49 122.1(3) . .
C3 O5 Ru3 N3 78.6(3) 2_655 .
C3 O5 Ru3 O6 -5.0(3) 2_655 .
C3 O5 Ru3 C50 -82.0(4) 2_655 .
C3 O5 Ru3 C51 173.7(5) 2_655 .
C3 O5 Ru3 C47 -165.3(3) 2_655 .
C3 O5 Ru3 C48 -126.8(3) 2_655 .
C3 O5 Ru3 C46 170.2(3) 2_655 .
C3 O5 Ru3 C49 -95.7(3) 2_655 .
C49 C50 Ru3 N3 -177.5(3) . .
C51 C50 Ru3 N3 51.6(3) . .
C56 C50 Ru3 N3 -61.7(6) . .
C49 C50 Ru3 O6 -93.5(3) . .
C51 C50 Ru3 O6 135.6(3) . .
C56 C50 Ru3 O6 22.3(5) . .
C49 C50 Ru3 O5 -20.6(5) . .
C51 C50 Ru3 O5 -151.6(3) . .
C56 C50 Ru3 O5 95.2(6) . .
C49 C50 Ru3 C51 130.9(4) . .
C56 C50 Ru3 C51 -113.3(6) . .
C49 C50 Ru3 C47 66.2(3) . .
C51 C50 Ru3 C47 -64.7(3) . .
C56 C50 Ru3 C47 -178.0(6) . .
C49 C50 Ru3 C48 28.6(3) . .
C51 C50 Ru3 C48 -102.3(3) . .
C56 C50 Ru3 C48 144.5(6) . .
C49 C50 Ru3 C46 102.0(3) . .
C51 C50 Ru3 C46 -28.9(3) . .
C56 C50 Ru3 C46 -142.2(6) . .
C51 C50 Ru3 C49 -130.9(4) . .
C56 C50 Ru3 C49 115.8(7) . .
C46 C51 Ru3 N3 88.8(3) . .
C50 C51 Ru3 N3 -138.6(3) . .
C57 C51 Ru3 N3 -25.7(6) . .
C46 C51 Ru3 O6 173.8(3) . .
C50 C51 Ru3 O6 -53.6(3) . .
C57 C51 Ru3 O6 59.3(6) . .
C46 C51 Ru3 O5 -4.7(7) . .
C50 C51 Ru3 O5 127.8(5) . .
C57 C51 Ru3 O5 -119.3(7) . .
C46 C51 Ru3 C50 -132.5(5) . .
C57 C51 Ru3 C50 112.9(7) . .
C46 C51 Ru3 C47 -27.2(3) . .
C50 C51 Ru3 C47 105.3(3) . .
C57 C51 Ru3 C47 -141.8(6) . .
C46 C51 Ru3 C48 -65.5(4) . .
C50 C51 Ru3 C48 67.1(3) . .
C57 C51 Ru3 C48 179.9(6) . .
C50 C51 Ru3 C46 132.5(5) . .
C57 C51 Ru3 C46 -114.6(7) . .
C46 C51 Ru3 C49 -102.4(4) . .
C50 C51 Ru3 C49 30.1(3) . .
C57 C51 Ru3 C49 143.0(6) . .
C46 C47 Ru3 N3 -57.5(4) . .
C48 C47 Ru3 N3 172.1(3) . .
C53 C47 Ru3 N3 59.5(7) . .
C46 C47 Ru3 O6 145.2(4) . .
C48 C47 Ru3 O6 14.8(6) . .
C53 C47 Ru3 O6 -97.9(7) . .
C46 C47 Ru3 O5 -145.3(3) . .
C48 C47 Ru3 O5 84.3(3) . .
C53 C47 Ru3 O5 -28.4(6) . .
C46 C47 Ru3 C50 65.4(4) . .
C48 C47 Ru3 C50 -65.0(3) . .
C53 C47 Ru3 C50 -177.6(6) . .
C46 C47 Ru3 C51 27.9(3) . .
C48 C47 Ru3 C51 -102.5(3) . .
C53 C47 Ru3 C51 144.8(7) . .
C46 C47 Ru3 C48 130.4(5) . .
C53 C47 Ru3 C48 -112.6(7) . .
C48 C47 Ru3 C46 -130.4(5) . .
C53 C47 Ru3 C46 117.0(8) . .
C46 C47 Ru3 C49 102.8(4) . .
C48 C47 Ru3 C49 -27.6(3) . .
C53 C47 Ru3 C49 -140.3(7) . .
C49 C48 Ru3 N3 -150.9(4) . .
C47 C48 Ru3 N3 -16.5(6) . .
C54 C48 Ru3 N3 95.5(7) . .
C49 C48 Ru3 O6 51.6(3) . .
C47 C48 Ru3 O6 -174.0(3) . .
C54 C48 Ru3 O6 -62.0(6) . .
C49 C48 Ru3 O5 128.0(3) . .
C47 C48 Ru3 O5 -97.7(3) . .
C54 C48 Ru3 O5 14.4(6) . .
C49 C48 Ru3 C50 -29.3(3) . .
C47 C48 Ru3 C50 105.1(3) . .
C54 C48 Ru3 C50 -142.9(6) . .
C49 C48 Ru3 C51 -67.6(3) . .
C47 C48 Ru3 C51 66.8(3) . .
C54 C48 Ru3 C51 178.8(6) . .
C49 C48 Ru3 C47 -134.4(5) . .
C54 C48 Ru3 C47 112.0(7) . .
C49 C48 Ru3 C46 -104.7(4) . .
C47 C48 Ru3 C46 29.6(3) . .
C54 C48 Ru3 C46 141.7(6) . .
C47 C48 Ru3 C49 134.4(5) . .
C54 C48 Ru3 C49 -113.6(7) . .
C47 C46 Ru3 N3 130.7(3) . .
C51 C46 Ru3 N3 -94.3(3) . .
C52 C46 Ru3 N3 17.3(8) . .
C47 C46 Ru3 O6 -148.9(4) . .
C51 C46 Ru3 O6 -13.9(7) . .
C52 C46 Ru3 O6 97.7(8) . .
C47 C46 Ru3 O5 43.3(4) . .
C51 C46 Ru3 O5 178.3(3) . .
C52 C46 Ru3 O5 -70.2(8) . .
C47 C46 Ru3 C50 -105.4(4) . .
C51 C46 Ru3 C50 29.6(3) . .
C52 C46 Ru3 C50 141.2(8) . .
C47 C46 Ru3 C51 -135.0(5) . .
C52 C46 Ru3 C51 111.6(9) . .
C51 C46 Ru3 C47 135.0(5) . .
C52 C46 Ru3 C47 -113.4(9) . .
C47 C46 Ru3 C48 -31.0(3) . .
C51 C46 Ru3 C48 104.0(4) . .
C52 C46 Ru3 C48 -144.4(8) . .
C47 C46 Ru3 C49 -67.5(3) . .
C51 C46 Ru3 C49 67.5(3) . .
C52 C46 Ru3 C49 179.1(8) . .
C48 C49 Ru3 N3 139.3(5) . .
C50 C49 Ru3 N3 6.5(7) . .
C55 C49 Ru3 N3 -105.0(7) . .
C48 C49 Ru3 O6 -137.7(3) . .
C50 C49 Ru3 O6 89.5(3) . .
C55 C49 Ru3 O6 -21.9(5) . .
C48 C49 Ru3 O5 -58.4(3) . .
C50 C49 Ru3 O5 168.8(3) . .
C55 C49 Ru3 O5 57.3(6) . .
C48 C49 Ru3 C50 132.8(5) . .
C55 C49 Ru3 C50 -111.5(6) . .
C48 C49 Ru3 C51 102.3(3) . .
C50 C49 Ru3 C51 -30.4(3) . .
C55 C49 Ru3 C51 -141.9(6) . .
C48 C49 Ru3 C47 28.6(3) . .
C50 C49 Ru3 C47 -104.2(3) . .
C55 C49 Ru3 C47 144.3(6) . .
C50 C49 Ru3 C48 -132.8(5) . .
C55 C49 Ru3 C48 115.8(6) . .
C48 C49 Ru3 C46 65.0(3) . .
C50 C49 Ru3 C46 -67.8(3) . .
C55 C49 Ru3 C46 -179.3(6) . .
