#------------------------------------------------------------------------------
#$Date: 2018-10-05 15:19:55 +0300 (Fri, 05 Oct 2018) $
#$Revision: 211332 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/15/00/7150007.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7150007
loop_
_publ_author_name
'Elliott, Eric L.'
'Hernández, Gerardo A'
'Linden, Anthony'
'Siegel, Jay S.'
_publ_section_title
;
 Anion mediated structural motifs in silver(I) complexes with
 corannulene.
;
_journal_issue                   3
_journal_name_full               'Organic & biomolecular chemistry'
_journal_page_first              407
_journal_page_last               413
_journal_paper_doi               10.1039/b411987h
_journal_volume                  3
_journal_year                    2005
_chemical_formula_moiety         'C20 H10, 2(Ag 1+), 2(B F4 1-)'
_chemical_formula_sum            'C20 H10 Ag2 B2 F8'
_chemical_formula_weight         639.64
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             03-05-05
_audit_creation_method           SHELXL-97
_cell_angle_alpha                98.3042(13)
_cell_angle_beta                 110.3937(13)
_cell_angle_gamma                101.4884(9)
_cell_formula_units_Z            2
_cell_length_a                   9.5741(2)
_cell_length_b                   9.6621(2)
_cell_length_c                   10.6735(2)
_cell_measurement_reflns_used    30014
_cell_measurement_temperature    160(1)
_cell_measurement_theta_max      30.0
_cell_measurement_theta_min      2.0
_cell_volume                     882.01(3)
_computing_cell_refinement       'DENZO-SMN (Otwinowski & Minor, 1997)'
_computing_data_collection       'COLLECT (Nonius, 2000)'
_computing_data_reduction
'DENZO-SMN and SCALEPACK (Otwinowski & Minor, 1997)'
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_computing_publication_material  'SHELXL97 and PLATON (Spek, 2003)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SIR92 (Altomare et al., 1994)'
_diffrn_ambient_temperature      160(1)
_diffrn_detector                 '65 mm CCD camera on \k goniostat'
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type
'Nonius KappaCCD area-detector diffractometer'
_diffrn_measurement_method       'φ and ω scans with κ offsets'
_diffrn_radiation_monochromator  'horizontally mounted graphite crystal'
_diffrn_radiation_source         'Nonius FR590 sealed tube generator'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0497
_diffrn_reflns_av_sigmaI/netI    0.0322
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            24787
_diffrn_reflns_theta_full        30.04
_diffrn_reflns_theta_max         30.04
_diffrn_reflns_theta_min         2.09
_diffrn_standards_decay_%        0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.309
_exptl_absorpt_correction_T_max  0.869
_exptl_absorpt_correction_T_min  0.745
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Blessing, 1995)'
_exptl_crystal_colour            pale-yellow
_exptl_crystal_density_diffrn    2.408
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             612
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.071
_refine_diff_density_min         -1.080
_refine_diff_density_rms         0.112
_refine_ls_extinction_coef       0.0048(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.025
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     318
_refine_ls_number_reflns         5144
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.025
_refine_ls_R_factor_all          0.0400
_refine_ls_R_factor_gt           0.0301
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0323P)²+1.2366P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0705
_refine_ls_wR_factor_ref         0.0752
_reflns_number_gt                4337
_reflns_number_total             5144
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            b411987h.txt
_cod_data_source_block           4_(SG0311)
_cod_depositor_comments
;
The following automatic conversions were performed:

'_atom_sites_solution_hydrogens' value 'geom & difmap' was changed to
'mixed'.

Automatic conversion script
Id: cif_fix_values 6452 2018-10-05 10:23:21Z andrius 
;
_cod_original_sg_symbol_H-M      'P -1         '
_cod_database_code               7150007
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.36731(2) 0.36920(2) 0.67760(2) 0.03190(8) Uani 1 1 d . . .
Ag2 Ag 0.24467(2) 0.24313(2) 0.10321(2) 0.02479(7) Uani 1 1 d . . .
C1 C 0.1928(3) 0.0301(3) 0.3533(2) 0.0190(5) Uani 1 1 d . . .
C2 C 0.0863(3) -0.0710(3) 0.2306(2) 0.0188(4) Uani 1 1 d . A .
C3 C -0.0130(3) -0.1739(3) 0.2661(2) 0.0187(4) Uani 1 1 d . . .
C4 C 0.0345(3) -0.1370(3) 0.4110(2) 0.0192(5) Uani 1 1 d . A .
C5 C 0.1610(3) -0.0120(3) 0.4644(3) 0.0200(5) Uani 1 1 d . . .
C6 C 0.4150(3) 0.1242(3) 0.6178(3) 0.0248(5) Uani 1 1 d . A .
H6 H 0.4899 0.1647 0.7088 0.030 Uiso 1 1 d R . .
C7 C 0.4462(3) 0.1646(3) 0.5083(3) 0.0253(5) Uani 1 1 d . . .
H7 H 0.5424 0.2309 0.5262 0.030 Uiso 1 1 calc R A .
C8 C 0.3359(3) 0.1081(3) 0.3680(3) 0.0220(5) Uani 1 1 d . A .
C9 C 0.3644(3) 0.0932(3) 0.2420(3) 0.0244(5) Uani 1 1 d . . .
H9 H 0.4560 0.1531 0.2418 0.029 Uiso 1 1 d R A .
C10 C 0.2600(3) -0.0075(3) 0.1208(3) 0.0238(5) Uani 1 1 d . A .
H10 H 0.2823 -0.0146 0.0404 0.029 Uiso 1 1 d R . .
C11 C 0.1181(3) -0.1015(3) 0.1159(3) 0.0212(5) Uani 1 1 d . . .
C12 C 0.0263(3) -0.2411(3) 0.0224(3) 0.0236(5) Uani 1 1 d . . .
H12 H 0.0338 -0.2645 -0.0642 0.028 Uiso 1 1 d R . .
C13 C -0.0734(3) -0.3426(3) 0.0568(3) 0.0237(5) Uani 1 1 d . . .
H13 H -0.1323 -0.4324 -0.0073 0.028 Uiso 1 1 d R A .
C14 C -0.0878(3) -0.3126(3) 0.1888(3) 0.0209(5) Uani 1 1 d . A .
C15 C -0.1379(3) -0.4137(3) 0.2613(3) 0.0244(5) Uani 1 1 d . . .
H15 H -0.2040 -0.5073 0.2109 0.029 Uiso 1 1 d R A .
C16 C -0.0913(3) -0.3772(3) 0.4045(3) 0.0252(5) Uani 1 1 d . . .
H16 H -0.1273 -0.4464 0.4488 0.030 Uiso 1 1 d R . .
C17 C 0.0105(3) -0.2365(3) 0.4863(3) 0.0222(5) Uani 1 1 d . . .
C18 C 0.1115(3) -0.1932(3) 0.6305(3) 0.0267(5) Uani 1 1 d . A .
H18 H 0.0921 -0.2506 0.6909 0.032 Uiso 1 1 calc R . .
C19 C 0.2354(3) -0.0705(3) 0.6827(3) 0.0258(5) Uani 1 1 d . . .
H19 H 0.2989 -0.0462 0.7780 0.031 Uiso 1 1 calc R A .
C20 C 0.2714(3) 0.0221(3) 0.5968(3) 0.0227(5) Uani 1 1 d . A .
F1A F 0.5194(7) 0.1243(5) 1.0092(6) 0.0394(16) Uani 0.357(5) 1 d P A 1
F2A F 0.6679(7) 0.3276(7) 0.9932(7) 0.055(2) Uani 0.357(5) 1 d P A 1
F3A F 0.4073(8) 0.2759(9) 0.8987(6) 0.058(2) Uani 0.357(5) 1 d P A 1
F1B F 0.4059(4) 0.1808(5) 0.9379(4) 0.0565(14) Uani 0.643(5) 1 d P A 2
F2B F 0.6645(4) 0.2427(4) 1.0690(3) 0.0518(11) Uani 0.643(5) 1 d P A 2
F3B F 0.5654(4) 0.3784(4) 0.9257(3) 0.0485(10) Uani 0.643(5) 1 d P A 2
F4 F 0.5184(2) 0.3622(3) 1.1216(2) 0.0525(6) Uani 1 1 d . . .
B1 B 0.5378(4) 0.2843(4) 1.0105(3) 0.0305(7) Uani 1 1 d . . .
F5 F 0.7773(3) 0.3787(3) 0.7010(2) 0.0550(6) Uani 1 1 d . A .
F6 F 0.6221(2) 0.5245(2) 0.70676(19) 0.0368(4) Uani 1 1 d . . .
F7 F 0.8576(2) 0.6184(2) 0.7073(2) 0.0506(6) Uani 1 1 d . A .
F8 F 0.6701(2) 0.4644(2) 0.51419(18) 0.0405(5) Uani 1 1 d . A .
B2 B 0.7338(4) 0.4946(4) 0.6568(3) 0.0279(6) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 40 0.0033 0.0016
; International Tables for Crystallography (1992).
Vol. C, Tables 4.2.6.8 and 6.1.1.4
;
H H 20 0.0000 0.0000
; International Tables for Crystallography (1992).
Vol. C, Tables 4.2.6.8 and 6.1.1.4
;
Ag Ag 4 -0.8971 1.1015
; International Tables for Crystallography (1992).
Vol. C, Tables 4.2.6.8 and 6.1.1.4
;
B B 4 0.0013 0.0007
; International Tables for Crystallography (1992).
Vol. C, Tables 4.2.6.8 and 6.1.1.4
;
F F 16 0.0171 0.0103
; International Tables for Crystallography (1992).
Vol. C, Tables 4.2.6.8 and 6.1.1.4
;
loop_
_diffrn_standard_refln_index_h
_diffrn_standard_refln_index_k
_diffrn_standard_refln_index_l
? ? ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F6 Ag1 C16 138.25(8) . 2_556 ?
F6 Ag1 C6 98.09(8) . . ?
C16 Ag1 C6 116.50(9) 2_556 . ?
F6 Ag1 F3A 107.05(18) . . ?
C16 Ag1 F3A 103.27(18) 2_556 . ?
C6 Ag1 F3A 76.74(17) . . ?
F6 Ag1 C15 134.77(7) . 2_556 ?
C16 Ag1 C15 31.89(9) 2_556 2_556 ?
C6 Ag1 C15 125.75(9) . 2_556 ?
F3A Ag1 C15 76.66(17) . 2_556 ?
C13 Ag2 C9 166.24(9) 2 . ?
C13 Ag2 C12 33.72(9) 2 2 ?
C9 Ag2 C12 133.84(9) . 2 ?
C13 Ag2 C10 134.31(9) 2 . ?
C9 Ag2 C10 33.37(9) . . ?
C12 Ag2 C10 109.71(9) 2 . ?
C13 Ag2 F6 96.77(8) 2 2_666 ?
C9 Ag2 F6 94.29(8) . 2_666 ?
C12 Ag2 F6 108.87(7) 2 2_666 ?
C10 Ag2 F6 127.45(8) . 2_666 ?
C13 Ag2 F4 106.34(9) 2 1_554 ?
C9 Ag2 F4 85.47(9) . 1_554 ?
C12 Ag2 F4 140.01(9) 2 1_554 ?
C10 Ag2 F4 101.56(8) . 1_554 ?
F6 Ag2 F4 67.43(6) 2_666 1_554 ?
C8 C1 C5 122.8(2) . . ?
C8 C1 C2 123.6(2) . . ?
C5 C1 C2 107.8(2) . . ?
C11 C2 C1 123.0(2) . . ?
C11 C2 C3 123.1(2) . . ?
C1 C2 C3 108.1(2) . . ?
C14 C3 C4 122.7(2) . . ?
C14 C3 C2 123.8(2) . . ?
C4 C3 C2 107.7(2) . . ?
C17 C4 C5 122.8(2) . . ?
C17 C4 C3 123.3(2) . . ?
C5 C4 C3 108.2(2) . . ?
C20 C5 C4 123.3(2) . . ?
C20 C5 C1 123.0(2) . . ?
C4 C5 C1 108.3(2) . . ?
C7 C6 C20 121.7(2) . . ?
C7 C6 Ag1 89.21(17) . . ?
C20 C6 Ag1 103.49(17) . . ?
C7 C6 H6 119.2 . . ?
C20 C6 H6 119.2 . . ?
Ag1 C6 H6 77.0 . . ?
C6 C7 C8 121.7(2) . . ?
C6 C7 H7 119.2 . . ?
C8 C7 H7 119.2 . . ?
C1 C8 C7 115.0(2) . . ?
C1 C8 C9 114.6(2) . . ?
C7 C8 C9 128.7(2) . . ?
C10 C9 C8 121.6(2) . . ?
C10 C9 Ag2 77.10(16) . . ?
C8 C9 Ag2 110.39(17) . . ?
C10 C9 H9 119.2 . . ?
C8 C9 H9 119.2 . . ?
Ag2 C9 H9 82.6 . . ?
C9 C10 C11 121.2(2) . . ?
C9 C10 Ag2 69.53(15) . . ?
C11 C10 Ag2 113.77(17) . . ?
C9 C10 H10 119.4 . . ?
C11 C10 H10 119.4 . . ?
Ag2 C10 H10 86.9 . . ?
C2 C11 C12 114.7(2) . . ?
C2 C11 C10 115.1(2) . . ?
C12 C11 C10 128.5(2) . . ?
C13 C12 C11 121.8(2) . . ?
C13 C12 Ag2 69.96(15) . 2 ?
C11 C12 Ag2 112.39(17) . 2 ?
C13 C12 H12 119.1 . . ?
C11 C12 H12 119.1 . . ?
Ag2 C12 H12 87.7 2 . ?
C12 C13 C14 121.2(2) . . ?
C12 C13 Ag2 76.32(16) . 2 ?
C14 C13 Ag2 109.88(17) . 2 ?
C12 C13 H13 119.4 . . ?
C14 C13 H13 119.4 . . ?
Ag2 C13 H13 83.9 2 . ?
C3 C14 C15 115.1(2) . . ?
C3 C14 C13 114.6(2) . . ?
C15 C14 C13 128.7(2) . . ?
C16 C15 C14 121.6(2) . . ?
C16 C15 Ag1 70.31(15) . 2_556 ?
C14 C15 Ag1 113.64(18) . 2_556 ?
C16 C15 H15 119.2 . . ?
C14 C15 H15 119.2 . . ?
Ag1 C15 H15 86.2 2_556 . ?
C15 C16 C17 121.4(2) . . ?
C15 C16 Ag1 77.79(15) . 2_556 ?
C17 C16 Ag1 110.56(17) . 2_556 ?
C15 C16 H16 119.3 . . ?
C17 C16 H16 119.3 . . ?
Ag1 C16 H16 81.8 2_556 . ?
C4 C17 C18 114.8(2) . . ?
C4 C17 C16 114.4(2) . . ?
C18 C17 C16 129.7(2) . . ?
C19 C18 C17 121.7(2) . . ?
C19 C18 H18 119.1 . . ?
C17 C18 H18 119.1 . . ?
C18 C19 C20 122.1(2) . . ?
C18 C19 H19 118.9 . . ?
C20 C19 H19 118.9 . . ?
C5 C20 C6 114.4(2) . . ?
C5 C20 C19 114.2(2) . . ?
C6 C20 C19 130.2(2) . . ?
B1 F3A Ag1 132.2(6) . . ?
B1 F4 Ag2 106.59(17) . 1_556 ?
F2B B1 F1B 117.8(4) . . ?
F2A B1 F3A 114.1(6) . . ?
F2A B1 F4 118.7(4) . . ?
F2B B1 F4 103.8(3) . . ?
F1B B1 F4 107.3(3) . . ?
F3A B1 F4 104.3(4) . . ?
F2B B1 F3B 109.1(3) . . ?
F1B B1 F3B 108.9(3) . . ?
F4 B1 F3B 109.6(3) . . ?
F2A B1 F1A 104.8(5) . . ?
F3A B1 F1A 100.3(5) . . ?
F4 B1 F1A 113.3(3) . . ?
B2 F6 Ag1 130.95(16) . . ?
B2 F6 Ag2 106.67(15) . 2_666 ?
Ag1 F6 Ag2 120.65(7) . 2_666 ?
F5 B2 F8 110.5(3) . . ?
F5 B2 F7 111.6(3) . . ?
F8 B2 F7 109.7(3) . . ?
F5 B2 F6 108.6(3) . . ?
F8 B2 F6 109.0(2) . . ?
F7 B2 F6 107.3(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 F6 2.4856(17) . ?
Ag1 C16 2.499(3) 2_556 ?
Ag1 C6 2.533(3) . ?
Ag1 F3A 2.579(8) . ?
Ag1 C15 2.594(3) 2_556 ?
Ag2 C13 2.383(3) 2 ?
Ag2 C9 2.389(3) . ?
Ag2 C12 2.465(3) 2 ?
Ag2 C10 2.485(3) . ?
Ag2 F6 2.5539(17) 2_666 ?
Ag2 F4 2.5702(19) 1_554 ?
C1 C8 1.369(3) . ?
C1 C5 1.416(3) . ?
C1 C2 1.418(3) . ?
C2 C11 1.368(3) . ?
C2 C3 1.420(3) . ?
C3 C14 1.369(3) . ?
C3 C4 1.419(3) . ?
C4 C17 1.373(4) . ?
C4 C5 1.410(3) . ?
C5 C20 1.382(4) . ?
C6 C7 1.392(4) . ?
C6 C20 1.447(4) . ?
C6 H6 0.9500 . ?
C7 C8 1.445(4) . ?
C7 H7 0.9500 . ?
C8 C9 1.456(4) . ?
C9 C10 1.403(4) . ?
C9 H9 0.9500 . ?
C10 C11 1.455(4) . ?
C10 H10 0.9500 . ?
C11 C12 1.455(4) . ?
C12 C13 1.408(4) . ?
C12 H12 0.9500 . ?
C13 C14 1.456(4) . ?
C13 H13 0.9500 . ?
C14 C15 1.440(4) . ?
C15 C16 1.402(4) . ?
C15 H15 0.9500 . ?
C16 C17 1.448(4) . ?
C16 H16 0.9500 . ?
C17 C18 1.448(4) . ?
C18 C19 1.382(4) . ?
C18 H18 0.9500 . ?
C19 C20 1.447(4) . ?
C19 H19 0.9500 . ?
F1A B1 1.518(6) . ?
F2A B1 1.317(6) . ?
F3A B1 1.373(7) . ?
F1B B1 1.337(5) . ?
F2B B1 1.327(5) . ?
F3B B1 1.422(5) . ?
F4 B1 1.400(4) . ?
F5 B2 1.361(4) . ?
F6 B2 1.410(4) . ?
F7 B2 1.389(4) . ?
F8 B2 1.388(4) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C8 C1 C2 C11 1.0(4) . . . . ?
C5 C1 C2 C11 -152.6(2) . . . . ?
C8 C1 C2 C3 154.7(2) . . . . ?
C5 C1 C2 C3 1.0(3) . . . . ?
C11 C2 C3 C14 -0.7(4) . . . . ?
C1 C2 C3 C14 -154.3(2) . . . . ?
C11 C2 C3 C4 152.7(2) . . . . ?
C1 C2 C3 C4 -0.9(3) . . . . ?
C14 C3 C4 C17 0.3(4) . . . . ?
C2 C3 C4 C17 -153.4(2) . . . . ?
C14 C3 C4 C5 154.2(2) . . . . ?
C2 C3 C4 C5 0.5(3) . . . . ?
C17 C4 C5 C20 -0.3(4) . . . . ?
C3 C4 C5 C20 -154.3(2) . . . . ?
C17 C4 C5 C1 154.2(2) . . . . ?
C3 C4 C5 C1 0.2(3) . . . . ?
C8 C1 C5 C20 0.0(4) . . . . ?
C2 C1 C5 C20 153.9(2) . . . . ?
C8 C1 C5 C4 -154.6(2) . . . . ?
C2 C1 C5 C4 -0.8(3) . . . . ?
F6 Ag1 C6 C7 -57.07(16) . . . . ?
C16 Ag1 C6 C7 98.83(17) 2_556 . . . ?
F3A Ag1 C6 C7 -162.8(2) . . . . ?
C15 Ag1 C6 C7 134.72(16) 2_556 . . . ?
F6 Ag1 C6 C20 -179.54(17) . . . . ?
C16 Ag1 C6 C20 -23.6(2) 2_556 . . . ?
F3A Ag1 C6 C20 74.7(2) . . . . ?
C15 Ag1 C6 C20 12.3(2) 2_556 . . . ?
C20 C6 C7 C8 0.8(4) . . . . ?
Ag1 C6 C7 C8 -104.6(2) . . . . ?
C5 C1 C8 C7 -9.4(4) . . . . ?
C2 C1 C8 C7 -159.2(2) . . . . ?
C5 C1 C8 C9 157.0(2) . . . . ?
C2 C1 C8 C9 7.2(4) . . . . ?
C6 C7 C8 C1 8.9(4) . . . . ?
C6 C7 C8 C9 -155.3(3) . . . . ?
C1 C8 C9 C10 -7.6(4) . . . . ?
C7 C8 C9 C10 156.6(3) . . . . ?
C1 C8 C9 Ag2 79.5(2) . . . . ?
C7 C8 C9 Ag2 -116.3(3) . . . . ?
C13 Ag2 C9 C10 30.6(5) 2 . . . ?
C12 Ag2 C9 C10 52.58(19) 2 . . . ?
F6 Ag2 C9 C10 174.02(14) 2_666 . . . ?
F4 Ag2 C9 C10 -119.06(15) 1_554 . . . ?
C13 Ag2 C9 C8 -88.6(4) 2 . . . ?
C12 Ag2 C9 C8 -66.6(2) 2 . . . ?
C10 Ag2 C9 C8 -119.2(2) . . . . ?
F6 Ag2 C9 C8 54.82(18) 2_666 . . . ?
F4 Ag2 C9 C8 121.74(18) 1_554 . . . ?
C8 C9 C10 C11 0.1(4) . . . . ?
Ag2 C9 C10 C11 -106.1(2) . . . . ?
C8 C9 C10 Ag2 106.2(2) . . . . ?
C13 Ag2 C10 C9 -170.26(15) 2 . . . ?
C12 Ag2 C10 C9 -142.52(15) 2 . . . ?
F6 Ag2 C10 C9 -7.52(18) 2_666 . . . ?
F4 Ag2 C10 C9 62.80(15) 1_554 . . . ?
C13 Ag2 C10 C11 -54.1(2) 2 . . . ?
C9 Ag2 C10 C11 116.1(2) . . . . ?
C12 Ag2 C10 C11 -26.4(2) 2 . . . ?
F6 Ag2 C10 C11 108.60(18) 2_666 . . . ?
F4 Ag2 C10 C11 178.92(17) 1_554 . . . ?
C1 C2 C11 C12 157.7(2) . . . . ?
C3 C2 C11 C12 7.9(4) . . . . ?
C1 C2 C11 C10 -8.6(4) . . . . ?
C3 C2 C11 C10 -158.4(2) . . . . ?
C9 C10 C11 C2 7.9(4) . . . . ?
Ag2 C10 C11 C2 -71.7(3) . . . . ?
C9 C10 C11 C12 -156.1(3) . . . . ?
Ag2 C10 C11 C12 124.2(2) . . . . ?
C2 C11 C12 C13 -7.1(4) . . . . ?
C10 C11 C12 C13 157.0(3) . . . . ?
C2 C11 C12 Ag2 72.4(2) . . . 2 ?
C10 C11 C12 Ag2 -123.4(2) . . . 2 ?
C11 C12 C13 C14 -0.6(4) . . . . ?
Ag2 C12 C13 C14 -105.2(2) 2 . . . ?
C11 C12 C13 Ag2 104.5(2) . . . 2 ?
C4 C3 C14 C15 9.9(4) . . . . ?
C2 C3 C14 C15 159.4(2) . . . . ?
C4 C3 C14 C13 -156.8(2) . . . . ?
C2 C3 C14 C13 -7.3(4) . . . . ?
C12 C13 C14 C3 7.7(4) . . . . ?
Ag2 C13 C14 C3 -78.0(2) 2 . . . ?
C12 C13 C14 C15 -156.8(3) . . . . ?
Ag2 C13 C14 C15 117.5(3) 2 . . . ?
C3 C14 C15 C16 -9.7(4) . . . . ?
C13 C14 C15 C16 154.8(3) . . . . ?
C3 C14 C15 Ag1 71.0(2) . . . 2_556 ?
C13 C14 C15 Ag1 -124.6(2) . . . 2_556 ?
C14 C15 C16 C17 -0.5(4) . . . . ?
Ag1 C15 C16 C17 -106.8(2) 2_556 . . . ?
C14 C15 C16 Ag1 106.3(2) . . . 2_556 ?
C5 C4 C17 C18 8.7(4) . . . . ?
C3 C4 C17 C18 158.8(2) . . . . ?
C5 C4 C17 C16 -160.7(2) . . . . ?
C3 C4 C17 C16 -10.5(4) . . . . ?
C15 C16 C17 C4 10.5(4) . . . . ?
Ag1 C16 C17 C4 -77.5(2) 2_556 . . . ?
C15 C16 C17 C18 -156.9(3) . . . . ?
Ag1 C16 C17 C18 115.1(3) 2_556 . . . ?
C4 C17 C18 C19 -8.5(4) . . . . ?
C16 C17 C18 C19 158.8(3) . . . . ?
C17 C18 C19 C20 0.2(4) . . . . ?
C4 C5 C20 C6 160.6(2) . . . . ?
C1 C5 C20 C6 9.7(4) . . . . ?
C4 C5 C20 C19 -8.1(4) . . . . ?
C1 C5 C20 C19 -158.9(2) . . . . ?
C7 C6 C20 C5 -10.0(4) . . . . ?
Ag1 C6 C20 C5 87.6(2) . . . . ?
C7 C6 C20 C19 156.4(3) . . . . ?
Ag1 C6 C20 C19 -106.0(3) . . . . ?
C18 C19 C20 C5 8.0(4) . . . . ?
C18 C19 C20 C6 -158.4(3) . . . . ?
F6 Ag1 F3A B1 -8.4(6) . . . . ?
C16 Ag1 F3A B1 -159.3(5) 2_556 . . . ?
C6 Ag1 F3A B1 86.1(6) . . . . ?
C15 Ag1 F3A B1 -141.6(6) 2_556 . . . ?
Ag1 F3A B1 F2A -12.2(8) . . . . ?
Ag1 F3A B1 F4 118.9(5) . . . . ?
Ag1 F3A B1 F1A -123.7(5) . . . . ?
Ag2 F4 B1 F2A 177.4(5) 1_556 . . . ?
Ag2 F4 B1 F2B -124.3(3) 1_556 . . . ?
Ag2 F4 B1 F1B 1.1(4) 1_556 . . . ?
Ag2 F4 B1 F3A 49.1(5) 1_556 . . . ?
Ag2 F4 B1 F3B 119.2(3) 1_556 . . . ?
Ag2 F4 B1 F1A -59.0(4) 1_556 . . . ?
C16 Ag1 F6 B2 -125.2(3) 2_556 . . . ?
C6 Ag1 F6 B2 21.5(3) . . . . ?
F3A Ag1 F6 B2 100.0(3) . . . . ?
C15 Ag1 F6 B2 -172.0(2) 2_556 . . . ?
C16 Ag1 F6 Ag2 71.92(15) 2_556 . . 2_666 ?
C6 Ag1 F6 Ag2 -141.36(10) . . . 2_666 ?
F3A Ag1 F6 Ag2 -62.83(18) . . . 2_666 ?
C15 Ag1 F6 Ag2 25.12(15) 2_556 . . 2_666 ?
Ag1 F6 B2 F5 -57.3(3) . . . . ?
Ag2 F6 B2 F5 107.3(2) 2_666 . . . ?
Ag1 F6 B2 F8 63.2(3) . . . . ?
Ag2 F6 B2 F8 -132.15(19) 2_666 . . . ?
Ag1 F6 B2 F7 -178.08(17) . . . . ?
Ag2 F6 B2 F7 -13.4(3) 2_666 . . . ?
