#------------------------------------------------------------------------------
#$Date: 2016-03-26 23:11:40 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180531 $
#$URL: svn://www.crystallography.net/cod/cif/7/22/00/7220065.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7220065
loop_
_publ_author_name
'Zhang, Huijie'
'Fan, Ruiqing'
'Wang, Ping'
'Wang, Xinming'
'Gao, Song'
'Dong, Yuwei'
'Wang, Yulei'
'Yang, Yulin'
_publ_section_title
;
 Structure variations of series lanthanide complexes constructed from
 quinoline carboxylate ligand: photoluminescent properties and PMMA
 matrices doping
;
_journal_name_full               'RSC Adv.'
_journal_paper_doi               10.1039/C5RA01796C
_journal_year                    2015
_chemical_formula_sum            'C34 H27 Cl Eu N5 O6'
_chemical_formula_weight         789.02
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2015-03-03 deposited with the CCDC.
2015-04-07 downloaded from the CCDC.
;
_cell_angle_alpha                111.9660(10)
_cell_angle_beta                 91.3200(10)
_cell_angle_gamma                111.1270(10)
_cell_formula_units_Z            2
_cell_length_a                   11.1063(4)
_cell_length_b                   11.3995(5)
_cell_length_c                   14.9133(6)
_cell_measurement_reflns_used    5948
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      25.76
_cell_measurement_theta_min      3.00
_cell_volume                     1605.93(11)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.967
_diffrn_measurement_device_type  'Bruker Smart APEX CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0314
_diffrn_reflns_av_sigmaI/netI    0.0386
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            14047
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.76
_diffrn_reflns_theta_min         3.00
_exptl_absorpt_coefficient_mu    2.090
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.632
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             788
_exptl_crystal_size_max          0.214
_exptl_crystal_size_mid          0.183
_exptl_crystal_size_min          0.151
_refine_diff_density_max         1.157
_refine_diff_density_min         -0.847
_refine_diff_density_rms         0.116
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.072
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     410
_refine_ls_number_reflns         5948
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.072
_refine_ls_R_factor_all          0.0363
_refine_ls_R_factor_gt           0.0282
_refine_ls_shift/su_max          0.017
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0350P)²+2.9435P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0657
_refine_ls_wR_factor_ref         0.0757
_reflns_number_gt                5301
_reflns_number_total             5948
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5ra01796c2.cif
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_sg_symbol_H-M      'P-1   '
_cod_database_code               7220065
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Eu1 Eu 1.081799(17) 0.845139(19) 0.439241(13) 0.01254(7) Uani 1 1 d .
N1 N 1.0277(3) 0.6408(3) 0.2688(2) 0.0213(7) Uani 1 1 d .
N2 N 1.2553(3) 0.8686(3) 0.3214(2) 0.0181(7) Uani 1 1 d .
N3 N 0.9089(4) 0.8526(4) 0.0488(3) 0.0337(9) Uani 1 1 d .
N4 N 0.4033(3) 0.6779(3) 0.3859(3) 0.0206(7) Uani 1 1 d .
N5 N 0.6364(7) 0.6405(8) 0.1239(5) 0.088(2) Uiso 1 1 d .
Cl1 Cl 1.23341(10) 0.66603(11) 0.62868(8) 0.0272(2) Uani 1 1 d .
O1 O 1.0067(3) 0.9235(3) 0.3359(2) 0.0274(7) Uani 1 1 d .
O2 O 0.9284(3) 1.0873(3) 0.39208(19) 0.0223(6) Uani 1 1 d .
O3 O 0.8513(2) 0.7389(3) 0.4200(2) 0.0219(6) Uani 1 1 d .
O4 O 1.2056(3) 1.0821(3) 0.5138(2) 0.0226(6) Uani 1 1 d .
O5 O 1.2787(2) 0.8321(3) 0.4998(2) 0.0209(6) Uani 1 1 d .
H5A H 1.2707 0.8214 0.5531 0.031 Uiso 1 1 d R
H5D H 1.3443 0.9064 0.5104 0.031 Uiso 1 1 d R
O6 O 1.0195(3) 0.6304(3) 0.4660(2) 0.0219(6) Uani 1 1 d .
H6A H 0.9640 0.6284 0.5042 0.033 Uiso 1 1 d R
H6D H 1.0875 0.6285 0.4918 0.033 Uiso 1 1 d R
C1 C 1.3655(4) 0.9796(4) 0.3449(3) 0.0219(9) Uani 1 1 d .
H1A H 1.3767 1.0587 0.4025 0.026 Uiso 1 1 calc R
C2 C 1.4670(4) 0.9874(5) 0.2896(3) 0.0290(10) Uani 1 1 d .
H2A H 1.5438 1.0699 0.3094 0.035 Uiso 1 1 calc R
C3 C 1.4527(4) 0.8741(5) 0.2071(3) 0.0311(10) Uani 1 1 d .
H3B H 1.5205 0.8756 0.1694 0.037 Uiso 1 1 calc R
C4 C 1.3362(4) 0.7551(5) 0.1789(3) 0.0260(9) Uani 1 1 d .
C5 C 1.3139(5) 0.6321(5) 0.0928(4) 0.0443(14) Uani 1 1 d .
H5B H 1.3794 0.6309 0.0531 0.053 Uiso 1 1 calc R
C6 C 1.2024(5) 0.5188(6) 0.0673(4) 0.0486(15) Uani 1 1 d .
H6B H 1.1908 0.4387 0.0103 0.058 Uiso 1 1 calc R
C7 C 1.1009(5) 0.5170(5) 0.1249(3) 0.0355(11) Uani 1 1 d .
C8 C 0.9810(5) 0.4022(5) 0.1004(4) 0.0483(15) Uani 1 1 d .
H8A H 0.9647 0.3197 0.0440 0.058 Uiso 1 1 calc R
C9 C 0.8893(5) 0.4107(5) 0.1580(4) 0.0492(15) Uani 1 1 d .
H9A H 0.8072 0.3347 0.1414 0.059 Uiso 1 1 calc R
C10 C 0.9156(4) 0.5311(5) 0.2415(3) 0.0320(11) Uani 1 1 d .
H10A H 0.8499 0.5348 0.2809 0.038 Uiso 1 1 calc R
C11 C 1.1196(4) 0.6361(4) 0.2101(3) 0.0212(9) Uani 1 1 d .
C12 C 1.2396(4) 0.7563(4) 0.2377(3) 0.0199(8) Uani 1 1 d .
C13 C 0.9417(4) 0.8810(5) 0.1415(3) 0.0270(10) Uani 1 1 d .
H13A H 0.9938 0.8384 0.1568 0.032 Uiso 1 1 calc R
C14 C 0.9061(4) 0.9699(4) 0.2209(3) 0.0168(8) Uani 1 1 d .
C15 C 0.8270(4) 1.0285(4) 0.1995(3) 0.0181(8) Uani 1 1 d .
H15A H 0.8004 1.0883 0.2508 0.022 Uiso 1 1 calc R
C16 C 0.7856(4) 0.9987(4) 0.1003(3) 0.0211(9) Uani 1 1 d .
C17 C 0.7013(4) 1.0519(5) 0.0726(3) 0.0312(10) Uani 1 1 d .
H17A H 0.6677 1.1070 0.1213 0.037 Uiso 1 1 calc R
C18 C 0.6675(5) 1.0243(6) -0.0248(4) 0.0417(13) Uani 1 1 d .
H18A H 0.6118 1.0614 -0.0431 0.050 Uiso 1 1 calc R
C19 C 0.7158(6) 0.9409(6) -0.0971(4) 0.0491(14) Uani 1 1 d .
H19A H 0.6931 0.9229 -0.1642 0.059 Uiso 1 1 calc R
C20 C 0.7946(5) 0.8857(6) -0.0725(3) 0.0412(12) Uani 1 1 d .
H20A H 0.8256 0.8291 -0.1225 0.049 Uiso 1 1 calc R
C21 C 0.8309(4) 0.9116(5) 0.0266(3) 0.0292(10) Uani 1 1 d .
C22 C 0.9499(3) 0.9956(4) 0.3244(3) 0.0163(8) Uani 1 1 d .
C23 C 0.5306(4) 0.7498(4) 0.4044(3) 0.0192(8) Uani 1 1 d .
H23A H 0.5609 0.8440 0.4149 0.023 Uiso 1 1 calc R
C24 C 0.6250(4) 0.6958(4) 0.4095(3) 0.0155(8) Uani 1 1 d .
C25 C 0.5828(4) 0.5599(4) 0.3936(3) 0.0163(8) Uani 1 1 d .
H25A H 0.6446 0.5207 0.3958 0.020 Uiso 1 1 calc R
C26 C 0.4471(4) 0.4786(4) 0.3740(3) 0.0169(8) Uani 1 1 d .
C27 C 0.3956(4) 0.3380(4) 0.3598(3) 0.0225(9) Uani 1 1 d .
H27A H 0.4535 0.2941 0.3611 0.027 Uiso 1 1 calc R
C28 C 0.2626(4) 0.2656(4) 0.3443(3) 0.0256(9) Uani 1 1 d .
H28A H 0.2288 0.1717 0.3352 0.031 Uiso 1 1 calc R
C29 C 0.1765(4) 0.3288(4) 0.3417(3) 0.0275(10) Uani 1 1 d .
H29A H 0.0846 0.2774 0.3312 0.033 Uiso 1 1 calc R
C30 C 0.2223(4) 0.4634(4) 0.3541(3) 0.0232(9) Uani 1 1 d .
H30A H 0.1623 0.5044 0.3513 0.028 Uiso 1 1 calc R
C31 C 0.3593(4) 0.5417(4) 0.3712(3) 0.0189(8) Uani 1 1 d .
C32 C 0.7674(4) 0.7913(4) 0.4402(3) 0.0165(8) Uani 1 1 d .
C33 C 0.4854(9) 0.4112(10) 0.1261(7) 0.108(3) Uiso 1 1 d .
H33A H 0.4353 0.3506 0.0594 0.163 Uiso 1 1 calc R
H33B H 0.4250 0.4276 0.1714 0.163 Uiso 1 1 calc R
H33C H 0.5357 0.3674 0.1464 0.163 Uiso 1 1 calc R
C34 C 0.5745(7) 0.5412(8) 0.1276(5) 0.0714(19) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Eu1 O4 77.39(10) . .
O1 Eu1 O2 125.54(10) . 2_776
O4 Eu1 O2 74.03(10) . 2_776
O1 Eu1 O3 76.72(10) . .
O4 Eu1 O3 124.91(9) . .
O2 Eu1 O3 83.14(10) 2_776 .
O1 Eu1 O5 141.42(10) . .
O4 Eu1 O5 83.71(10) . .
O2 Eu1 O5 79.38(9) 2_776 .
O3 Eu1 O5 140.33(10) . .
O1 Eu1 O6 138.38(10) . .
O4 Eu1 O6 142.97(10) . .
O2 Eu1 O6 74.97(9) 2_776 .
O3 Eu1 O6 70.08(9) . .
O5 Eu1 O6 71.08(9) . .
O1 Eu1 N1 77.86(11) . .
O4 Eu1 N1 139.10(10) . .
O2 Eu1 N1 146.36(10) 2_776 .
O3 Eu1 N1 79.46(10) . .
O5 Eu1 N1 96.15(10) . .
O6 Eu1 N1 72.11(10) . .
O1 Eu1 N2 75.12(10) . .
O4 Eu1 N2 79.92(10) . .
O2 Eu1 N2 140.52(10) 2_776 .
O3 Eu1 N2 136.34(10) . .
O5 Eu1 N2 68.60(10) . .
O6 Eu1 N2 113.47(9) . .
N1 Eu1 N2 62.49(10) . .
O1 Eu1 Eu1 60.89(7) . 2_776
O4 Eu1 Eu1 55.47(7) . 2_776
O2 Eu1 Eu1 64.69(7) 2_776 2_776
O3 Eu1 Eu1 69.45(7) . 2_776
O5 Eu1 Eu1 130.67(7) . 2_776
O6 Eu1 Eu1 125.00(6) . 2_776
N1 Eu1 Eu1 132.45(8) . 2_776
N2 Eu1 Eu1 121.49(7) . 2_776
C10 N1 C11 118.0(3) . .
C10 N1 Eu1 120.7(3) . .
C11 N1 Eu1 120.9(2) . .
C1 N2 C12 117.4(3) . .
C1 N2 Eu1 123.1(2) . .
C12 N2 Eu1 119.1(2) . .
C13 N3 C21 117.1(4) . .
C23 N4 C31 118.1(3) . .
C22 O1 Eu1 148.4(3) . .
C22 O2 Eu1 138.8(3) . 2_776
C32 O3 Eu1 130.4(2) . .
C32 O4 Eu1 159.5(2) 2_776 .
Eu1 O5 H5A 109.3 . .
Eu1 O5 H5D 109.3 . .
H5A O5 H5D 109.5 . .
Eu1 O6 H6A 109.4 . .
Eu1 O6 H6D 109.4 . .
H6A O6 H6D 109.5 . .
N2 C1 C2 124.0(4) . .
N2 C1 H1A 118.0 . .
C2 C1 H1A 118.0 . .
C3 C2 C1 118.7(4) . .
C3 C2 H2A 120.7 . .
C1 C2 H2A 120.7 . .
C2 C3 C4 119.0(4) . .
C2 C3 H3B 120.5 . .
C4 C3 H3B 120.5 . .
C12 C4 C3 118.7(4) . .
C12 C4 C5 119.1(4) . .
C3 C4 C5 122.2(4) . .
C6 C5 C4 121.5(4) . .
C6 C5 H5B 119.3 . .
C4 C5 H5B 119.3 . .
C5 C6 C7 120.9(4) . .
C5 C6 H6B 119.6 . .
C7 C6 H6B 119.6 . .
C11 C7 C8 117.6(4) . .
C11 C7 C6 119.2(4) . .
C8 C7 C6 123.3(4) . .
C9 C8 C7 119.3(4) . .
C9 C8 H8A 120.4 . .
C7 C8 H8A 120.4 . .
C8 C9 C10 119.8(5) . .
C8 C9 H9A 120.1 . .
C10 C9 H9A 120.1 . .
N1 C10 C9 123.2(4) . .
N1 C10 H10A 118.4 . .
C9 C10 H10A 118.4 . .
N1 C11 C7 122.1(4) . .
N1 C11 C12 118.2(3) . .
C7 C11 C12 119.7(4) . .
N2 C12 C4 122.3(4) . .
N2 C12 C11 118.1(3) . .
C4 C12 C11 119.7(4) . .
N3 C13 C14 125.5(4) . .
N3 C13 H13A 117.2 . .
C14 C13 H13A 117.2 . .
C15 C14 C13 117.8(4) . .
C15 C14 C22 121.2(3) . .
C13 C14 C22 120.9(4) . .
C14 C15 C16 119.2(3) . .
C14 C15 H15A 120.4 . .
C16 C15 H15A 120.4 . .
C17 C16 C15 122.4(4) . .
C17 C16 C21 119.5(4) . .
C15 C16 C21 118.1(4) . .
C18 C17 C16 120.4(5) . .
C18 C17 H17A 119.8 . .
C16 C17 H17A 119.8 . .
C17 C18 C19 119.8(5) . .
C17 C18 H18A 120.1 . .
C19 C18 H18A 120.1 . .
C20 C19 C18 121.0(4) . .
C20 C19 H19A 119.5 . .
C18 C19 H19A 119.5 . .
C19 C20 C21 120.8(5) . .
C19 C20 H20A 119.6 . .
C21 C20 H20A 119.6 . .
N3 C21 C20 119.3(4) . .
N3 C21 C16 122.2(4) . .
C20 C21 C16 118.6(4) . .
O2 C22 O1 125.6(4) . .
O2 C22 C14 117.8(3) . .
O1 C22 C14 116.6(3) . .
N4 C23 C24 124.0(4) . .
N4 C23 H23A 118.0 . .
C24 C23 H23A 118.0 . .
C25 C24 C23 118.6(3) . .
C25 C24 C32 122.2(3) . .
C23 C24 C32 119.0(3) . .
C24 C25 C26 119.5(3) . .
C24 C25 H25A 120.2 . .
C26 C25 H25A 120.2 . .
C31 C26 C25 118.0(3) . .
C31 C26 C27 119.0(3) . .
C25 C26 C27 122.9(4) . .
C28 C27 C26 120.2(4) . .
C28 C27 H27A 119.9 . .
C26 C27 H27A 119.9 . .
C27 C28 C29 120.4(4) . .
C27 C28 H28A 119.8 . .
C29 C28 H28A 119.8 . .
C30 C29 C28 121.1(4) . .
C30 C29 H29A 119.5 . .
C28 C29 H29A 119.5 . .
C29 C30 C31 120.0(4) . .
C29 C30 H30A 120.0 . .
C31 C30 H30A 120.0 . .
N4 C31 C26 121.7(3) . .
N4 C31 C30 119.0(4) . .
C26 C31 C30 119.3(4) . .
O3 C32 O4 124.8(3) . 2_776
O3 C32 C24 117.9(3) . .
O4 C32 C24 117.3(3) 2_776 .
C34 C33 H33A 109.5 . .
C34 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
C34 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
N5 C34 C33 174.9(9) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Eu1 O1 2.319(3) .
Eu1 O4 2.330(3) .
Eu1 O2 2.358(3) 2_776
Eu1 O3 2.361(3) .
Eu1 O5 2.421(3) .
Eu1 O6 2.480(3) .
Eu1 N1 2.596(3) .
Eu1 N2 2.647(3) .
Eu1 Eu1 4.3636(4) 2_776
N1 C10 1.324(5) .
N1 C11 1.362(5) .
N2 C1 1.324(5) .
N2 C12 1.364(5) .
N3 C13 1.306(6) .
N3 C21 1.373(6) .
N4 C23 1.313(5) .
N4 C31 1.376(5) .
N5 C34 1.116(9) .
O1 C22 1.256(5) .
O2 C22 1.253(5) .
O2 Eu1 2.358(3) 2_776
O3 C32 1.262(4) .
O4 C32 1.258(5) 2_776
O5 H5A 0.8500 .
O5 H5D 0.8500 .
O6 H6A 0.8501 .
O6 H6D 0.8499 .
C1 C2 1.408(6) .
C1 H1A 0.9500 .
C2 C3 1.364(7) .
C2 H2A 0.9500 .
C3 C4 1.404(6) .
C3 H3B 0.9500 .
C4 C12 1.402(5) .
C4 C5 1.436(6) .
C5 C6 1.343(7) .
C5 H5B 0.9500 .
C6 C7 1.432(6) .
C6 H6B 0.9500 .
C7 C11 1.413(6) .
C7 C8 1.408(7) .
C8 C9 1.355(7) .
C8 H8A 0.9500 .
C9 C10 1.391(6) .
C9 H9A 0.9500 .
C10 H10A 0.9500 .
C11 C12 1.435(6) .
C13 C14 1.413(5) .
C13 H13A 0.9500 .
C14 C15 1.375(5) .
C14 C22 1.492(5) .
C15 C16 1.413(5) .
C15 H15A 0.9500 .
C16 C17 1.412(6) .
C16 C21 1.421(6) .
C17 C18 1.377(6) .
C17 H17A 0.9500 .
C18 C19 1.408(8) .
C18 H18A 0.9500 .
C19 C20 1.361(8) .
C19 H19A 0.9500 .
C20 C21 1.412(6) .
C20 H20A 0.9500 .
C23 C24 1.407(5) .
C23 H23A 0.9500 .
C24 C25 1.369(5) .
C24 C32 1.500(5) .
C25 C26 1.410(5) .
C25 H25A 0.9500 .
C26 C31 1.413(5) .
C26 C27 1.421(5) .
C27 C28 1.370(6) .
C27 H27A 0.9500 .
C28 C29 1.397(6) .
C28 H28A 0.9500 .
C29 C30 1.367(6) .
C29 H29A 0.9500 .
C30 C31 1.417(5) .
C30 H30A 0.9500 .
C32 O4 1.258(5) 2_776
C33 C34 1.447(11) .
C33 H33A 0.9800 .
C33 H33B 0.9800 .
C33 H33C 0.9800 .
