#------------------------------------------------------------------------------
#$Date: 2022-04-16 01:49:42 +0300 (Sat, 16 Apr 2022) $
#$Revision: 274558 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/71/00/7710050.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7710050
loop_
_publ_author_name
'Staub, Liane Hildegard'
'Lambert, Jessica'
'Müller, Carsten'
'Morgenstern, Bernd'
'Zimmer, Michael'
'Warken, Joshua'
'Koldemir, Aylin'
'Block, Theresa'
'Pöttgen, Rainer'
'Schäfer, André'
_publ_section_title
;
 Bis(di-tert-butylindenyl)tetrelocenes.
;
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_paper_doi               10.1039/d2dt00582d
_journal_year                    2022
_chemical_formula_moiety         'C34 H46 Pb'
_chemical_formula_sum            'C34 H46 Pb'
_chemical_formula_weight         661.90
_chemical_name_systematic        bis(di-tert-butylindenyl)plumbocene
_chemical_properties_physical    Air-sensitive,Moisture-sensitive
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2022-02-23 deposited with the CCDC.	2022-04-08 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 106.1980(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   11.1603(4)
_cell_length_b                   14.9272(5)
_cell_length_c                   18.8917(7)
_cell_measurement_reflns_used    9959
_cell_measurement_temperature    133(2)
_cell_measurement_theta_max      28.71
_cell_measurement_theta_min      2.63
_cell_volume                     3022.27(19)
_computing_cell_refinement       'SAINT V8.40A (Bruker Nano, Inc., 2019)'
_computing_data_collection       'APEX 3 (Bruker Nano, Inc., 2019)'
_computing_data_reduction        'SAINT V8.40A (Bruker Nano, Inc., 2019)'
_computing_publication_material  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_structure_refinement
;
SHELXL-2018/3 (Sheldrick, 2018),                                              
SHELXLe Rev 1000 (Huebschle et al., 2011)
;
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      133(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker AXS D8 Venture, Photon II'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0351
_diffrn_reflns_av_unetI/netI     0.0222
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            50956
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         28.725
_diffrn_reflns_theta_min         2.245
_diffrn_source                   'INCOATEC I\^A?S microfocus sealed tube'
_exptl_absorpt_coefficient_mu    5.601
_exptl_absorpt_correction_T_max  0.7458
_exptl_absorpt_correction_T_min  0.6242
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
 SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D.,
 J. Appl. Cryst. 48 (2015) 3-10
;
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.455
_exptl_crystal_density_meas      ?
_exptl_crystal_description       block
_exptl_crystal_F_000             1328
_exptl_crystal_size_max          0.148
_exptl_crystal_size_mid          0.142
_exptl_crystal_size_min          0.092
_refine_diff_density_max         0.358
_refine_diff_density_min         -0.797
_refine_diff_density_rms         0.076
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.065
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     328
_refine_ls_number_reflns         7815
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.065
_refine_ls_R_factor_all          0.0290
_refine_ls_R_factor_gt           0.0190
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0097P)²+2.0099P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0377
_refine_ls_wR_factor_ref         0.0408
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6262
_reflns_number_total             7815
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d2dt00582d2.cif
_cod_data_source_block           sh4749_a
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_crystal_density_meas' value 'not measured' was
changed to '?' -- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7710050
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.491
_shelx_estimated_absorpt_t_max   0.627
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pb1 Pb 0.50133(2) 0.75240(2) 0.30428(2) 0.01965(3) Uani 1 1 d . . . . .
C1 C 0.56990(19) 0.92262(13) 0.27958(11) 0.0184(4) Uani 1 1 d . . . . .
H1 H 0.521546 0.969935 0.291064 0.022 Uiso 1 1 calc R U . . .
C2 C 0.54562(19) 0.88169(13) 0.20991(11) 0.0178(4) Uani 1 1 d . . . . .
C3 C 0.64426(19) 0.81829(14) 0.21461(12) 0.0200(4) Uani 1 1 d . . . . .
C4 C 0.6731(2) 0.75975(16) 0.16287(14) 0.0298(5) Uani 1 1 d . . . . .
H4 H 0.621867 0.758166 0.113417 0.036 Uiso 1 1 calc R U . . .
C5 C 0.7764(2) 0.70493(17) 0.18484(17) 0.0376(6) Uani 1 1 d . . . . .
H5 H 0.795789 0.665640 0.150022 0.045 Uiso 1 1 calc R U . . .
C6 C 0.8534(2) 0.70607(17) 0.25759(17) 0.0367(6) Uani 1 1 d . . . . .
H6 H 0.923019 0.666742 0.271331 0.044 Uiso 1 1 calc R U . . .
C7 C 0.8303(2) 0.76262(16) 0.30894(15) 0.0314(5) Uani 1 1 d . . . . .
H7 H 0.884558 0.763523 0.357622 0.038 Uiso 1 1 calc R U . . .
C8 C 0.72489(19) 0.82006(14) 0.28949(12) 0.0219(4) Uani 1 1 d . . . . .
C9 C 0.67576(19) 0.88429(14) 0.33054(12) 0.0207(4) Uani 1 1 d . . . . .
C10 C 0.7336(2) 0.91613(16) 0.40935(13) 0.0297(5) Uani 1 1 d . . . . .
C11 C 0.8558(3) 0.9656(2) 0.41304(16) 0.0476(8) Uani 1 1 d . . . . .
H11A H 0.914192 0.924437 0.399485 0.071 Uiso 1 1 calc R U . . .
H11B H 0.892716 0.987657 0.463267 0.071 Uiso 1 1 calc R U . . .
H11C H 0.838590 1.016289 0.378708 0.071 Uiso 1 1 calc R U . . .
C12 C 0.6455(3) 0.98022(17) 0.43341(14) 0.0370(6) Uani 1 1 d . . . . .
H12A H 0.567122 0.949290 0.431232 0.056 Uiso 1 1 calc R U . . .
H12B H 0.628451 1.032191 0.400415 0.056 Uiso 1 1 calc R U . . .
H12C H 0.684541 1.000259 0.484001 0.056 Uiso 1 1 calc R U . . .
C13 C 0.7610(3) 0.83765(19) 0.46427(14) 0.0440(7) Uani 1 1 d . . . . .
H13A H 0.815316 0.794232 0.449429 0.066 Uiso 1 1 calc R U . . .
H13B H 0.682555 0.808479 0.464656 0.066 Uiso 1 1 calc R U . . .
H13C H 0.802721 0.860234 0.513725 0.066 Uiso 1 1 calc R U . . .
C14 C 0.4402(2) 0.90634(14) 0.14180(11) 0.0215(4) Uani 1 1 d . . . . .
C15 C 0.3534(2) 0.97447(17) 0.16110(14) 0.0314(5) Uani 1 1 d . . . . .
H15A H 0.320722 0.950439 0.200279 0.047 Uiso 1 1 calc R U . . .
H15B H 0.284020 0.987053 0.117384 0.047 Uiso 1 1 calc R U . . .
H15C H 0.399471 1.029926 0.178108 0.047 Uiso 1 1 calc R U . . .
C16 C 0.4962(2) 0.94737(19) 0.08367(14) 0.0372(6) Uani 1 1 d . . . . .
H16A H 0.550618 0.903391 0.069620 0.056 Uiso 1 1 calc R U . . .
H16B H 0.544847 1.000670 0.104123 0.056 Uiso 1 1 calc R U . . .
H16C H 0.428808 0.964243 0.040122 0.056 Uiso 1 1 calc R U . . .
C17 C 0.3623(2) 0.82361(17) 0.10919(14) 0.0348(6) Uani 1 1 d . . . . .
H17A H 0.416913 0.777479 0.098164 0.052 Uiso 1 1 calc R U . . .
H17B H 0.299019 0.840483 0.063751 0.052 Uiso 1 1 calc R U . . .
H17C H 0.321132 0.800107 0.144860 0.052 Uiso 1 1 calc R U . . .
C18 C 0.44055(18) 0.63284(13) 0.39913(11) 0.0173(4) Uani 1 1 d . . . . .
H18 H 0.493669 0.631240 0.448117 0.021 Uiso 1 1 calc R U . . .
C19 C 0.33569(18) 0.69078(13) 0.37502(11) 0.0167(4) Uani 1 1 d . . . . .
C20 C 0.27775(18) 0.66691(13) 0.29932(11) 0.0160(4) Uani 1 1 d . . . . .
C21 C 0.16688(19) 0.69609(14) 0.24700(12) 0.0204(4) Uani 1 1 d . . . . .
H21 H 0.117375 0.741863 0.259625 0.025 Uiso 1 1 calc R U . . .
C22 C 0.1314(2) 0.65812(15) 0.17828(12) 0.0259(5) Uani 1 1 d . . . . .
H22 H 0.056519 0.677429 0.143775 0.031 Uiso 1 1 calc R U . . .
C23 C 0.2038(2) 0.59111(16) 0.15791(12) 0.0279(5) Uani 1 1 d . . . . .
H23 H 0.176940 0.565729 0.109960 0.034 Uiso 1 1 calc R U . . .
C24 C 0.3127(2) 0.56180(14) 0.20616(12) 0.0234(4) Uani 1 1 d . . . . .
H24 H 0.361698 0.517540 0.191172 0.028 Uiso 1 1 calc R U . . .
C25 C 0.35192(18) 0.59766(13) 0.27846(11) 0.0174(4) Uani 1 1 d . . . . .
C26 C 0.45593(18) 0.57822(13) 0.34155(11) 0.0174(4) Uani 1 1 d . . . . .
C27 C 0.5551(2) 0.50671(14) 0.34732(13) 0.0237(4) Uani 1 1 d . . . . .
C28 C 0.6274(2) 0.52097(18) 0.28984(15) 0.0366(6) Uani 1 1 d . . . . .
H28A H 0.685099 0.470916 0.292007 0.055 Uiso 1 1 calc R U . . .
H28B H 0.674561 0.577093 0.300359 0.055 Uiso 1 1 calc R U . . .
H28C H 0.568501 0.523989 0.240512 0.055 Uiso 1 1 calc R U . . .
C29 C 0.6490(2) 0.50783(17) 0.42390(14) 0.0334(6) Uani 1 1 d . . . . .
H29A H 0.605533 0.495854 0.461361 0.050 Uiso 1 1 calc R U . . .
H29B H 0.689230 0.566730 0.432902 0.050 Uiso 1 1 calc R U . . .
H29C H 0.712496 0.461637 0.426425 0.050 Uiso 1 1 calc R U . . .
C30 C 0.4924(2) 0.41389(15) 0.33560(15) 0.0340(6) Uani 1 1 d . . . . .
H30A H 0.450314 0.403124 0.373919 0.051 Uiso 1 1 calc R U . . .
H30B H 0.555931 0.367656 0.338404 0.051 Uiso 1 1 calc R U . . .
H30C H 0.431164 0.411802 0.287032 0.051 Uiso 1 1 calc R U . . .
C31 C 0.28434(19) 0.75263(14) 0.42336(11) 0.0219(4) Uani 1 1 d . . . . .
C32 C 0.2513(3) 0.84522(16) 0.38817(14) 0.0359(6) Uani 1 1 d . . . . .
H32A H 0.326834 0.873821 0.382041 0.054 Uiso 1 1 calc R U . . .
H32B H 0.215928 0.882412 0.420079 0.054 Uiso 1 1 calc R U . . .
H32C H 0.190095 0.838602 0.339908 0.054 Uiso 1 1 calc R U . . .
C33 C 0.3808(2) 0.76627(16) 0.49836(12) 0.0321(5) Uani 1 1 d . . . . .
H33A H 0.399190 0.708558 0.523815 0.048 Uiso 1 1 calc R U . . .
H33B H 0.347222 0.807706 0.528266 0.048 Uiso 1 1 calc R U . . .
H33C H 0.457554 0.791240 0.490870 0.048 Uiso 1 1 calc R U . . .
C34 C 0.1671(2) 0.70966(18) 0.43673(14) 0.0328(5) Uani 1 1 d . . . . .
H34A H 0.132713 0.749622 0.467301 0.049 Uiso 1 1 calc R U . . .
H34B H 0.189351 0.652164 0.462022 0.049 Uiso 1 1 calc R U . . .
H34C H 0.104600 0.699839 0.389359 0.049 Uiso 1 1 calc R U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C9 Pb1 C19 134.82(6) . . ?
C9 Pb1 C1 30.22(6) . . ?
C19 Pb1 C1 131.19(6) . . ?
C9 Pb1 C18 130.34(6) . . ?
C19 Pb1 C18 30.17(6) . . ?
C1 Pb1 C18 148.05(6) . . ?
C9 Pb1 C2 50.46(6) . . ?
C19 Pb1 C2 145.06(6) . . ?
C1 Pb1 C2 29.67(6) . . ?
C18 Pb1 C2 175.09(6) . . ?
C9 Pb1 C26 143.59(6) . . ?
C19 Pb1 C26 50.43(6) . . ?
C1 Pb1 C26 173.74(6) . . ?
C18 Pb1 C26 29.53(6) . . ?
C2 Pb1 C26 153.56(6) . . ?
C9 Pb1 C8 30.26(6) . . ?
C19 Pb1 C8 157.43(6) . . ?
C1 Pb1 C8 48.85(6) . . ?
C18 Pb1 C8 134.00(6) . . ?
C2 Pb1 C8 49.74(6) . . ?
C26 Pb1 C8 126.77(6) . . ?
C9 Pb1 C20 158.39(6) . . ?
C19 Pb1 C20 30.31(6) . . ?
C1 Pb1 C20 135.46(6) . . ?
C18 Pb1 C20 48.76(6) . . ?
C2 Pb1 C20 128.24(6) . . ?
C26 Pb1 C20 49.72(6) . . ?
C8 Pb1 C20 170.54(6) . . ?
C9 Pb1 C3 50.02(6) . . ?
C19 Pb1 C3 172.28(6) . . ?
C1 Pb1 C3 48.53(6) . . ?
C18 Pb1 C3 155.06(6) . . ?
C2 Pb1 C3 29.84(6) . . ?
C26 Pb1 C3 130.94(6) . . ?
C8 Pb1 C3 30.08(6) . . ?
C20 Pb1 C3 142.71(6) . . ?
C9 Pb1 C25 171.10(6) . . ?
C19 Pb1 C25 49.99(6) . . ?
C1 Pb1 C25 156.33(6) . . ?
C18 Pb1 C25 48.42(6) . . ?
C2 Pb1 C25 131.77(6) . . ?
C26 Pb1 C25 29.91(6) . . ?
C8 Pb1 C25 141.96(6) . . ?
C20 Pb1 C25 29.97(6) . . ?
C3 Pb1 C25 126.32(6) . . ?
C2 C1 C9 111.47(18) . . ?
C2 C1 Pb1 76.46(11) . . ?
C9 C1 Pb1 74.28(11) . . ?
C1 C2 C3 106.51(18) . . ?
C1 C2 C14 125.86(19) . . ?
C3 C2 C14 127.47(19) . . ?
C1 C2 Pb1 73.87(12) . . ?
C3 C2 Pb1 76.81(12) . . ?
C14 C2 Pb1 118.53(13) . . ?
C4 C3 C2 133.1(2) . . ?
C4 C3 C8 119.1(2) . . ?
C2 C3 C8 107.75(18) . . ?
C4 C3 Pb1 118.55(14) . . ?
C2 C3 Pb1 73.35(12) . . ?
C8 C3 Pb1 73.75(12) . . ?
C5 C4 C3 119.4(2) . . ?
C4 C5 C6 121.3(2) . . ?
C7 C6 C5 121.2(2) . . ?
C6 C7 C8 119.9(2) . . ?
C7 C8 C9 132.7(2) . . ?
C7 C8 C3 119.1(2) . . ?
C9 C8 C3 108.23(18) . . ?
C7 C8 Pb1 117.21(14) . . ?
C9 C8 Pb1 72.49(11) . . ?
C3 C8 Pb1 76.17(11) . . ?
C1 C9 C8 105.90(18) . . ?
C1 C9 C10 125.6(2) . . ?
C8 C9 C10 127.94(19) . . ?
C1 C9 Pb1 75.50(11) . . ?
C8 C9 Pb1 77.25(12) . . ?
C10 C9 Pb1 119.42(14) . . ?
C9 C10 C12 110.69(19) . . ?
C9 C10 C11 108.8(2) . . ?
C12 C10 C11 108.8(2) . . ?
C9 C10 C13 111.8(2) . . ?
C12 C10 C13 107.4(2) . . ?
C11 C10 C13 109.2(2) . . ?
C15 C14 C2 110.63(18) . . ?
C15 C14 C16 108.6(2) . . ?
C2 C14 C16 109.14(18) . . ?
C15 C14 C17 107.87(19) . . ?
C2 C14 C17 111.17(18) . . ?
C16 C14 C17 109.4(2) . . ?
C26 C18 C19 111.79(17) . . ?
C26 C18 Pb1 76.50(12) . . ?
C19 C18 Pb1 74.16(11) . . ?
C18 C19 C20 105.58(17) . . ?
C18 C19 C31 126.24(17) . . ?
C20 C19 C31 127.38(18) . . ?
C18 C19 Pb1 75.67(11) . . ?
C20 C19 Pb1 76.97(11) . . ?
C31 C19 Pb1 120.73(13) . . ?
C21 C20 C19 132.70(19) . . ?
C21 C20 C25 118.92(18) . . ?
C19 C20 C25 108.35(17) . . ?
C21 C20 Pb1 118.84(13) . . ?
C19 C20 Pb1 72.72(11) . . ?
C25 C20 Pb1 76.16(11) . . ?
C22 C21 C20 119.9(2) . . ?
C21 C22 C23 121.2(2) . . ?
C24 C23 C22 121.0(2) . . ?
C23 C24 C25 119.9(2) . . ?
C24 C25 C26 132.94(19) . . ?
C24 C25 C20 119.08(18) . . ?
C26 C25 C20 107.97(17) . . ?
C24 C25 Pb1 119.10(14) . . ?
C26 C25 Pb1 73.75(11) . . ?
C20 C25 Pb1 73.87(11) . . ?
C18 C26 C25 106.17(17) . . ?
C18 C26 C27 126.50(18) . . ?
C25 C26 C27 127.07(18) . . ?
C18 C26 Pb1 73.97(11) . . ?
C25 C26 Pb1 76.34(11) . . ?
C27 C26 Pb1 119.69(13) . . ?
C26 C27 C29 110.68(18) . . ?
C26 C27 C28 111.54(18) . . ?
C29 C27 C28 108.0(2) . . ?
C26 C27 C30 109.24(18) . . ?
C29 C27 C30 108.02(19) . . ?
C28 C27 C30 109.2(2) . . ?
C19 C31 C32 111.88(18) . . ?
C19 C31 C33 110.51(17) . . ?
C32 C31 C33 107.60(19) . . ?
C19 C31 C34 109.01(18) . . ?
C32 C31 C34 109.52(19) . . ?
C33 C31 C34 108.24(19) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pb1 C9 2.715(2) . ?
Pb1 C19 2.725(2) . ?
Pb1 C1 2.7311(19) . ?
Pb1 C18 2.745(2) . ?
Pb1 C2 2.764(2) . ?
Pb1 C26 2.7770(19) . ?
Pb1 C8 2.777(2) . ?
Pb1 C20 2.7808(19) . ?
Pb1 C3 2.809(2) . ?
Pb1 C25 2.8107(19) . ?
C1 C2 1.407(3) . ?
C1 C9 1.420(3) . ?
C2 C3 1.436(3) . ?
C2 C14 1.527(3) . ?
C3 C4 1.414(3) . ?
C3 C8 1.450(3) . ?
C4 C5 1.380(3) . ?
C5 C6 1.403(4) . ?
C6 C7 1.364(4) . ?
C7 C8 1.418(3) . ?
C8 C9 1.435(3) . ?
C9 C10 1.524(3) . ?
C10 C12 1.529(4) . ?
C10 C11 1.536(4) . ?
C10 C13 1.538(3) . ?
C14 C15 1.518(3) . ?
C14 C16 1.534(3) . ?
C14 C17 1.537(3) . ?
C18 C26 1.408(3) . ?
C18 C19 1.424(3) . ?
C19 C20 1.440(3) . ?
C19 C31 1.519(3) . ?
C20 C21 1.420(3) . ?
C20 C25 1.446(3) . ?
C21 C22 1.370(3) . ?
C22 C23 1.405(3) . ?
C23 C24 1.371(3) . ?
C24 C25 1.418(3) . ?
C25 C26 1.442(3) . ?
C26 C27 1.519(3) . ?
C27 C29 1.532(3) . ?
C27 C28 1.538(3) . ?
C27 C30 1.540(3) . ?
C31 C32 1.533(3) . ?
C31 C33 1.535(3) . ?
C31 C34 1.540(3) . ?
