#------------------------------------------------------------------------------
#$Date: 2023-05-31 01:56:01 +0300 (Wed, 31 May 2023) $
#$Revision: 284075 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/71/31/7713199.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7713199
loop_
_publ_author_name
'Morrison, Gregory'
'Masachchi, Lakshani W.'
'Tisdale, Hunter B.'
'Chang, Tieyan'
'Jones, Virginia G.'
'Zamorano, K. Pilar'
'Breton, Logan S.'
'Smith, Mark D.'
'Chen, Yu-Sheng'
'Zur Loye, Hans-Conrad'
_publ_section_title
;
 Polymorphism in A3MF6 (A = Rb, Cs; M = Al, Ga) Grown using Mixed Halide
 Fluxes
;
_journal_name_full               'Dalton Transactions'
_journal_paper_doi               10.1039/D3DT00352C
_journal_year                    2023
_chemical_formula_moiety         '0.08(Cs36 F72 Ga12)'
_chemical_formula_sum            'Cs3 F6 Ga'
_chemical_formula_weight         582.45
_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_Hall           '-C 2y'
_space_group_name_H-M_alt        'C 1 2/m 1'
_atom_sites_solution_primary     dual
_audit_creation_date             2022-01-12
_audit_creation_method
;
Olex2 1.2
(compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506)
;
_audit_update_record
;
2022-07-28 deposited with the CCDC.	2023-05-19 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 109.7000(10)
_cell_angle_gamma                90
_cell_formula_units_Z            12
_cell_length_a                   11.3996(3)
_cell_length_b                   19.7132(4)
_cell_length_c                   11.4551(4)
_cell_measurement_reflns_used    9626
_cell_measurement_temperature    300(2)
_cell_measurement_theta_max      36.1275
_cell_measurement_theta_min      3.2644
_cell_volume                     2423.55(12)
_computing_cell_refinement       'SAINT v8.34A (Bruker, 2013)'
_computing_data_collection       'Bruker APEX3 v2016.5-0 (Bruker, 2016)'
_computing_data_reduction        'SAINT v8.34A (Bruker, 013)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      299.94
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0376
_diffrn_reflns_av_unetI/netI     0.0134
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -30
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            102291
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         33.137
_diffrn_reflns_theta_min         2.161
_diffrn_source                   'microfocus sealed X-ray tube'
_exptl_absorpt_coefficient_mu    16.760
_exptl_absorpt_correction_T_max  0.7471
_exptl_absorpt_correction_T_min  0.6246
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS-2016/2 (Bruker,2016) was used for absorption correction.
wR2(int) was 0.0971 before and 0.0580 after correction.
The Ratio of minimum to maximum transmission is 0.8360.
The λ/2 correction factor is Not present.
;
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    4.789
_exptl_crystal_description       polyhedron
_exptl_crystal_F_000             3000
_exptl_crystal_size_max          0.07
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.04
_refine_diff_density_max         4.065
_refine_diff_density_min         -3.099
_refine_diff_density_rms         0.243
_refine_ls_extinction_coef       0.000159(14)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.160
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     166
_refine_ls_number_reflns         4759
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.159
_refine_ls_R_factor_all          0.0307
_refine_ls_R_factor_gt           0.0281
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0291P)²+25.0230P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0685
_refine_ls_wR_factor_ref         0.0717
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4466
_reflns_number_total             4759
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d3dt00352c2.cif
_cod_data_source_block           Cs3GaF6_C2_m
_cod_database_code               7713199
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.554
_shelx_estimated_absorpt_t_min   0.387
_olex2_refinement_description
;
1. Twinned data refinement
 Scales: 0.9297(14)
 0.0703(14)
2. Uiso/Uaniso restraints and constraints
Uanis(F2A) = Uanis(F2B) = Uanis(F2C)
Uanis(Cs1A) = Uanis(Cs1B)
Uanis(F1A) = Uanis(F1B)
3. Others
 2*[Sof(Cs1A)+Sof(Cs1B)+Sof(F1A)+Sof(F2A)+Sof(F2C)]+1*[Sof(F1B)+Sof(F2B)]=1
 with esd of 0.001
 Sof(Cs1A)=1-FVAR(1)
 Sof(Cs1B)=Sof(F1A)=Sof(F2A)=Sof(F2C)=FVAR(1)
 Sof(F1B)=0.5*FVAR(3)
 Sof(F2B)=FVAR(2)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cs1A Cs 0.64015(10) 0.30972(6) 0.85365(10) 0.02317(14) Uani 0.686(4) 1 d . . . .
.
Cs1B Cs 0.6296(2) 0.32274(11) 0.8644(2) 0.02317(14) Uani 0.314(4) 1 d . . . . .
Cs2 Cs 0.14572(4) 0.000000 0.43094(4) 0.02601(8) Uani 1 2 d S T P . .
Cs3 Cs 1.29435(4) 0.500000 1.20995(3) 0.02566(8) Uani 1 2 d S T P . .
Cs4 Cs 0.78423(2) 0.14308(2) 0.77987(2) 0.02593(6) Uani 1 1 d . . . . .
Cs5 Cs 0.91771(5) 0.500000 1.14316(4) 0.03057(9) Uani 1 2 d S T P . .
Cs6 Cs 0.87380(3) 0.33198(2) 0.62028(3) 0.02833(6) Uani 1 1 d . . . . .
Ga1 Ga 1.000000 0.33417(3) 1.000000 0.01375(9) Uani 1 2 d S T P . .
Ga2 Ga 0.000000 0.000000 0.000000 0.01565(13) Uani 1 4 d S T P . .
Ga3 Ga 0.500000 0.000000 0.500000 0.01518(13) Uani 1 4 d S T P . .
Ga4 Ga 1.000000 0.17331(3) 0.500000 0.01429(9) Uani 1 2 d S T P . .
F1A F 0.0407(14) 0.0188(12) 0.1695(17) 0.064(6) Uani 0.314(4) 1 d . . . . .
F1B F 0.085(3) 0.000000 0.171(3) 0.064(6) Uani 0.373(7) 2 d S T P . .
F2A F -0.0474(14) 0.0845(7) 0.0392(14) 0.0542(19) Uani 0.314(4) 1 d . . . . .
F2B F -0.1140(12) 0.0658(6) 0.0171(11) 0.0542(19) Uani 0.373(7) 1 d . . . . .
F2C F 0.1651(12) 0.0292(7) 0.0302(13) 0.0542(19) Uani 0.314(4) 1 d . . . . .
F3 F 0.3995(4) 0.000000 0.6048(4) 0.0336(8) Uani 1 2 d S T P . .
F4 F 0.6031(3) 0.06695(18) 0.5992(3) 0.0442(8) Uani 1 1 d . . . . .
F5 F 0.8998(3) 0.10465(14) 0.3963(3) 0.0318(6) Uani 1 1 d . . . . .
F6 F 1.1022(3) 0.24132(14) 0.6019(3) 0.0290(5) Uani 1 1 d . . . . .
F7 F 0.8975(3) 0.17213(16) 0.5988(3) 0.0335(6) Uani 1 1 d . . . . .
F8 F 0.9001(3) 0.26587(15) 0.8992(3) 0.0354(6) Uani 1 1 d . . . . .
F9 F 1.1015(3) 0.33503(16) 0.8996(3) 0.0356(6) Uani 1 1 d . . . . .
F10 F 1.1033(3) 0.40154(15) 1.1011(3) 0.0356(6) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F2A Cs1A F2B 15.9(3) 7_556 7_556 ?
F2A Cs1A F2C 25.6(4) 7_556 8_556 ?
F2A Cs1A F5 92.2(3) 7_556 7_656 ?
F2A Cs1A F6 137.0(3) 7_556 8_455 ?
F2A Cs1A F7 88.8(3) 7_556 8_455 ?
F2A Cs1A F8 130.0(3) 7_556 . ?
F2A Cs1A F8 77.4(3) 7_556 7_657 ?
F2A Cs1A F8 79.2(3) 7_556 8_455 ?
F2A Cs1A F9 122.6(3) 7_556 8_455 ?
F2A Cs1A F9 82.8(3) 7_556 2_757 ?
F2A Cs1A F10 88.2(3) 7_556 2_757 ?
F2B Cs1A F2C 9.7(3) 7_556 8_556 ?
F2B Cs1A F5 90.1(3) 7_556 7_656 ?
F2B Cs1A F6 140.7(3) 7_556 8_455 ?
F2B Cs1A F7 99.1(2) 7_556 8_455 ?
F2B Cs1A F8 83.1(3) 7_556 7_657 ?
F2B Cs1A F8 114.9(3) 7_556 . ?
F2B Cs1A F8 93.9(3) 7_556 8_455 ?
F2B Cs1A F9 132.1(3) 7_556 8_455 ?
F2B Cs1A F9 70.2(3) 7_556 2_757 ?
F2B Cs1A F10 72.5(3) 7_556 2_757 ?
F5 Cs1A F2C 89.9(2) 7_656 8_556 ?
F5 Cs1A F7 47.99(7) 7_656 8_455 ?
F5 Cs1A F8 119.98(8) 7_656 8_455 ?
F5 Cs1A F8 164.04(9) 7_656 7_657 ?
F5 Cs1A F9 119.40(8) 7_656 2_757 ?
F5 Cs1A F10 72.96(7) 7_656 2_757 ?
F6 Cs1A F2C 141.4(2) 8_455 8_556 ?
F6 Cs1A F5 51.57(7) 8_455 7_656 ?
F6 Cs1A F7 50.76(7) 8_455 8_455 ?
F6 Cs1A F8 83.14(8) 8_455 . ?
F6 Cs1A F8 98.31(9) 8_455 8_455 ?
F6 Cs1A F8 130.99(8) 8_455 7_657 ?
F6 Cs1A F9 132.20(8) 8_455 2_757 ?
F6 Cs1A F9 82.15(9) 8_455 8_455 ?
F6 Cs1A F10 99.75(9) 8_455 2_757 ?
F7 Cs1A F2C 106.0(2) 8_455 8_556 ?
F7 Cs1A F8 118.79(8) 8_455 7_657 ?
F7 Cs1A F8 72.34(7) 8_455 8_455 ?
F7 Cs1A F9 164.74(9) 8_455 2_757 ?
F7 Cs1A F10 120.67(8) 8_455 2_757 ?
F8 Cs1A F2C 85.86(19) 7_657 8_556 ?
F8 Cs1A F2C 105.3(2) . 8_556 ?
F8 Cs1A F2C 102.38(19) 8_455 8_556 ?
F8 Cs1A F5 98.21(10) . 7_656 ?
F8 Cs1A F7 132.81(9) . 8_455 ?
F8 Cs1A F8 46.61(9) 8_455 7_657 ?
F8 Cs1A F8 132.30(6) . 8_455 ?
F8 Cs1A F8 97.75(9) . 7_657 ?
F8 Cs1A F9 83.54(9) . 8_455 ?
F8 Cs1A F9 118.10(8) 8_455 2_757 ?
F8 Cs1A F9 49.74(8) . 2_757 ?
F8 Cs1A F10 161.92(9) 8_455 2_757 ?
F8 Cs1A F10 49.92(8) . 2_757 ?
F9 Cs1A F2C 62.1(2) 2_757 8_556 ?
F9 Cs1A F2C 135.56(19) 8_455 8_556 ?
F9 Cs1A F5 132.69(9) 8_455 7_656 ?
F9 Cs1A F7 97.55(9) 8_455 8_455 ?
F9 Cs1A F8 49.69(8) 8_455 7_657 ?
F9 Cs1A F8 71.80(7) 2_757 7_657 ?
F9 Cs1A F8 50.01(8) 8_455 8_455 ?
F9 Cs1A F9 97.72(9) 8_455 2_757 ?
F9 Cs1A F10 132.21(9) 8_455 2_757 ?
F10 Cs1A F2C 63.22(19) 2_757 8_556 ?
F10 Cs1A F8 118.15(8) 2_757 7_657 ?
F10 Cs1A F9 46.64(7) 2_757 2_757 ?
F2A Cs1B F2B 17.9(4) 7_556 7_556 ?
F2A Cs1B F2C 28.0(4) 7_556 8_556 ?
F2A Cs1B F5 98.5(4) 7_556 7_656 ?
F2A Cs1B F6 141.6(4) 7_556 8_455 ?
F2A Cs1B F7 94.7(4) 7_556 8_455 ?
F2A Cs1B F8 134.5(4) 7_556 . ?
F2A Cs1B F8 82.4(4) 7_556 7_657 ?
F2A Cs1B F8 84.4(4) 7_556 8_455 ?
F2A Cs1B F9 88.1(4) 7_556 2_757 ?
F2A Cs1B F9 126.8(4) 7_556 8_455 ?
F2A Cs1B F10 94.1(4) 7_556 2_757 ?
F2B Cs1B F2C 10.2(4) 7_556 8_556 ?
F2B Cs1B F5 95.9(3) 7_556 7_656 ?
F2B Cs1B F6 145.2(3) 7_556 8_455 ?
F2B Cs1B F7 106.2(3) 7_556 8_455 ?
F2B Cs1B F8 88.6(3) 7_556 7_657 ?
F2B Cs1B F8 117.6(3) 7_556 . ?
F2B Cs1B F8 100.8(3) 7_556 8_455 ?
F2B Cs1B F9 136.9(3) 7_556 8_455 ?
F2B Cs1B F9 74.0(3) 7_556 2_757 ?
F2B Cs1B F10 76.4(3) 7_556 2_757 ?
F5 Cs1B F2C 95.2(2) 7_656 8_556 ?
F5 Cs1B F7 47.98(8) 7_656 8_455 ?
F5 Cs1B F8 120.72(11) 7_656 8_455 ?
F5 Cs1B F8 167.73(12) 7_656 7_657 ?
F5 Cs1B F9 119.81(11) 7_656 2_757 ?
F5 Cs1B F10 72.99(9) 7_656 2_757 ?
F6 Cs1B F2C 144.8(2) 8_455 8_556 ?
F6 Cs1B F5 49.75(8) 8_455 7_656 ?
F6 Cs1B F7 49.16(8) 8_455 8_455 ?
F6 Cs1B F8 123.78(10) 8_455 7_657 ?
F6 Cs1B F8 94.34(11) 8_455 8_455 ?
F6 Cs1B F9 124.37(10) 8_455 2_757 ?
F6 Cs1B F10 95.27(10) 8_455 2_757 ?
F7 Cs1B F2C 113.2(2) 8_455 8_556 ?
F7 Cs1B F8 119.78(11) 8_455 7_657 ?
F7 Cs1B F9 167.73(11) 8_455 2_757 ?
F7 Cs1B F10 120.97(11) 8_455 2_757 ?
F8 Cs1B F2C 109.6(2) 8_455 8_556 ?
F8 Cs1B F2C 91.2(2) 7_657 8_556 ?
F8 Cs1B F2C 107.6(2) . 8_556 ?
F8 Cs1B F5 93.79(11) . 7_656 ?
F8 Cs1B F6 76.12(9) . 8_455 ?
F8 Cs1B F7 124.78(10) . 8_455 ?
F8 Cs1B F7 72.74(9) 8_455 8_455 ?
F8 Cs1B F8 94.20(11) . 7_657 ?
F8 Cs1B F8 47.05(10) 8_455 7_657 ?
F8 Cs1B F8 125.24(8) . 8_455 ?
F8 Cs1B F9 119.45(11) 8_455 2_757 ?
F8 Cs1B F9 48.51(8) . 2_757 ?
F8 Cs1B F9 72.40(9) 7_657 2_757 ?
F8 Cs1B F10 48.53(8) . 2_757 ?
F8 Cs1B F10 166.28(12) 8_455 2_757 ?
F9 Cs1B F2C 139.8(2) 8_455 8_556 ?
F9 Cs1B F2C 65.5(2) 2_757 8_556 ?
F9 Cs1B F5 124.78(11) 8_455 7_656 ?
F9 Cs1B F6 75.43(9) 8_455 8_455 ?
F9 Cs1B F7 93.65(11) 8_455 8_455 ?
F9 Cs1B F8 48.67(8) 8_455 7_657 ?
F9 Cs1B F8 48.87(8) 8_455 8_455 ?
F9 Cs1B F8 76.88(9) 8_455 . ?
F9 Cs1B F9 94.17(11) 8_455 2_757 ?
F9 Cs1B F10 124.90(11) 8_455 2_757 ?
F10 Cs1B F2C 66.7(2) 2_757 8_556 ?
F10 Cs1B F8 119.23(11) 2_757 7_657 ?
F10 Cs1B F9 46.83(8) 2_757 2_757 ?
F1A Cs2 F1A 15.0(9) 6 . ?
F1A Cs2 F3 133.5(3) 6 . ?
F1A Cs2 F3 133.5(3) . . ?
F1A Cs2 F4 90.8(3) 6 2_656 ?
F1A Cs2 F4 90.8(3) . 5_656 ?
F1A Cs2 F4 84.8(3) . 2_656 ?
F1A Cs2 F4 84.8(3) 6 5_656 ?
F1A Cs2 F5 119.7(5) 6 5_656 ?
F1A Cs2 F5 85.3(3) . 6_455 ?
F1A Cs2 F5 119.7(5) . 2_656 ?
F1A Cs2 F5 76.1(4) . 1_455 ?
F1A Cs2 F5 85.3(3) 6 1_455 ?
F1A Cs2 F5 132.3(4) . 5_656 ?
F1A Cs2 F5 76.1(4) 6 6_455 ?
F1A Cs2 F5 132.3(4) 6 2_656 ?
F1A Cs2 F7 76.8(5) . 2_656 ?
F1A Cs2 F7 91.7(5) 6 2_656 ?
F1A Cs2 F7 76.8(5) 6 5_656 ?
F1A Cs2 F7 91.7(5) . 5_656 ?
F1B Cs2 F1A 12.5(5) . . ?
F1B Cs2 F1A 12.5(5) . 6 ?
F1B Cs2 F3 123.9(5) . . ?
F1B Cs2 F4 78.6(5) . 5_656 ?
F1B Cs2 F4 78.6(5) . 2_656 ?
F1B Cs2 F5 88.7(4) . 6_455 ?
F1B Cs2 F5 131.0(2) . 5_656 ?
F1B Cs2 F5 131.0(2) . 2_656 ?
F1B Cs2 F5 88.7(4) . 1_455 ?
F1B Cs2 F7 85.36(8) . 2_656 ?
F1B Cs2 F7 85.36(8) . 5_656 ?
F3 Cs2 F4 50.86(8) . 5_656 ?
F3 Cs2 F4 50.86(8) . 2_656 ?
F3 Cs2 F5 84.39(8) . 2_656 ?
F3 Cs2 F5 132.22(6) . 1_455 ?
F3 Cs2 F5 132.22(6) . 6_455 ?
F3 Cs2 F5 84.39(8) . 5_656 ?
F3 Cs2 F7 98.31(6) . 2_656 ?
F3 Cs2 F7 98.31(6) . 5_656 ?
F4 Cs2 F4 47.53(12) 2_656 5_656 ?
F4 Cs2 F5 161.72(8) 5_656 1_455 ?
F4 Cs2 F5 117.37(7) 5_656 6_455 ?
F4 Cs2 F5 117.37(7) 2_656 1_455 ?
F4 Cs2 F5 161.72(8) 2_656 6_455 ?
F4 Cs2 F7 72.07(7) 5_656 5_656 ?
F4 Cs2 F7 119.32(8) 2_656 5_656 ?
F4 Cs2 F7 119.32(8) 5_656 2_656 ?
F4 Cs2 F7 72.07(7) 2_656 2_656 ?
F5 Cs2 F4 133.89(8) 2_656 5_656 ?
F5 Cs2 F4 98.23(9) 5_656 5_656 ?
F5 Cs2 F4 133.89(8) 5_656 2_656 ?
F5 Cs2 F4 98.23(9) 2_656 2_656 ?
F5 Cs2 F5 74.85(9) 6_455 1_455 ?
F5 Cs2 F5 100.03(7) 5_656 1_455 ?
F5 Cs2 F5 49.03(9) 5_656 6_455 ?
F5 Cs2 F5 86.10(11) 2_656 5_656 ?
F5 Cs2 F5 100.03(7) 2_656 6_455 ?
F5 Cs2 F5 49.03(9) 2_656 1_455 ?
F5 Cs2 F7 45.71(7) 6_455 5_656 ?
F5 Cs2 F7 48.62(7) 5_656 5_656 ?
F5 Cs2 F7 133.63(7) 2_656 5_656 ?
F5 Cs2 F7 48.62(7) 2_656 2_656 ?
F5 Cs2 F7 120.29(7) 6_455 2_656 ?
F5 Cs2 F7 133.63(7) 5_656 2_656 ?
F5 Cs2 F7 120.29(7) 1_455 5_656 ?
F5 Cs2 F7 45.71(7) 1_455 2_656 ?
F7 Cs2 F7 163.38(11) 5_656 2_656 ?
F1A Cs3 F1A 14.1(9) 3_656 8_656 ?
F1A Cs3 F1B 7.2(5) 3_656 3_656 ?
F1A Cs3 F1B 7.2(5) 8_656 3_656 ?
F1A Cs3 F2A 34.3(5) 8_656 8_656 ?
F1A Cs3 F2A 44.9(4) 3_656 8_656 ?
F1A Cs3 F2B 51.3(4) 8_656 3_656 ?
F1A Cs3 F2B 51.3(4) 3_656 8_656 ?
F1A Cs3 F2B 43.1(5) 3_656 3_656 ?
F1A Cs3 F2B 43.1(5) 8_656 8_656 ?
F1B Cs3 F2A 40.4(4) 3_656 8_656 ?
F2B Cs3 F1B 48.1(5) 3_656 3_656 ?
F2B Cs3 F1B 48.1(5) 8_656 3_656 ?
F2B Cs3 F2A 11.6(3) 8_656 8_656 ?
F2B Cs3 F2A 55.1(3) 3_656 8_656 ?
F2B Cs3 F2B 50.6(4) 8_656 3_656 ?
F2C Cs3 F1A 52.8(4) 4_656 3_656 ?
F2C Cs3 F1A 56.2(4) 7_656 3_656 ?
F2C Cs3 F1A 56.2(4) 4_656 8_656 ?
F2C Cs3 F1A 52.8(4) 7_656 8_656 ?
F2C Cs3 F1B 55.7(6) 4_656 3_656 ?
F2C Cs3 F1B 55.7(6) 7_656 3_656 ?
F2C Cs3 F2A 46.3(4) 4_656 8_656 ?
F2C Cs3 F2A 29.1(3) 7_656 8_656 ?
F2C Cs3 F2B 18.5(3) 7_656 8_656 ?
F2C Cs3 F2B 38.3(4) 7_656 3_656 ?
F2C Cs3 F2B 18.5(3) 4_656 3_656 ?
F2C Cs3 F2B 38.3(4) 4_656 8_656 ?
F2C Cs3 F2C 22.1(5) 7_656 4_656 ?
F5 Cs3 F1A 91.4(4) 8_556 3_656 ?
F5 Cs3 F1A 81.4(4) 3_556 3_656 ?
F5 Cs3 F1A 81.4(4) 8_556 8_656 ?
F5 Cs3 F1A 91.4(4) 3_556 8_656 ?
F5 Cs3 F1B 85.3(4) 8_556 3_656 ?
F5 Cs3 F1B 85.3(4) 3_556 3_656 ?
F5 Cs3 F2A 84.8(2) 8_556 8_656 ?
F5 Cs3 F2A 125.6(2) 3_556 8_656 ?
F5 Cs3 F2B 94.2(3) 3_556 3_656 ?
F5 Cs3 F2B 132.5(2) 8_556 3_656 ?
F5 Cs3 F2B 94.2(2) 8_556 8_656 ?
F5 Cs3 F2B 132.5(2) 3_556 8_656 ?
F5 Cs3 F2C 112.5(3) 8_556 7_656 ?
F5 Cs3 F2C 130.9(3) 8_556 4_656 ?
F5 Cs3 F2C 112.5(3) 3_556 4_656 ?
F5 Cs3 F2C 130.9(3) 3_556 7_656 ?
F5 Cs3 F5 89.90(12) 3_556 8_556 ?
F10 Cs3 F1A 128.7(4) 6_565 8_656 ?
F10 Cs3 F1A 128.7(4) . 3_656 ?
F10 Cs3 F1A 117.3(5) . 8_656 ?
F10 Cs3 F1A 117.3(5) 6_565 3_656 ?
F10 Cs3 F1B 124.0(3) . 3_656 ?
F10 Cs3 F1B 124.0(3) 6_565 3_656 ?
F10 Cs3 F2A 83.9(2) . 8_656 ?
F10 Cs3 F2A 122.5(3) 6_565 8_656 ?
F10 Cs3 F2B 78.0(2) 6_565 3_656 ?
F10 Cs3 F2B 78.0(2) . 8_656 ?
F10 Cs3 F2B 111.7(3) . 3_656 ?
F10 Cs3 F2B 111.7(3) 6_565 8_656 ?
F10 Cs3 F2C 78.5(3) . 7_656 ?
F10 Cs3 F2C 78.5(3) 6_565 4_656 ?
F10 Cs3 F2C 93.5(3) 6_565 7_656 ?
F10 Cs3 F2C 93.5(3) . 4_656 ?
F10 Cs3 F5 149.37(9) . 3_556 ?
F10 Cs3 F5 149.37(9) 6_565 8_556 ?
F10 Cs3 F5 84.54(9) 6_565 3_556 ?
F10 Cs3 F5 84.54(9) . 8_556 ?
F10 Cs3 F10 85.12(13) . 6_565 ?
F1A Cs4 F1A 7.0(5) 2_656 5_656 ?
F1A Cs4 F1B 11.3(5) 2_656 5_656 ?
F1A Cs4 F2A 52.0(4) 2_656 1_656 ?
F1A Cs4 F2A 36.3(5) 2_656 2_656 ?
F1A Cs4 F6 154.0(3) 2_656 8_455 ?
F1B Cs4 F1A 4.7(5) 5_656 5_656 ?
F1B Cs4 F2A 53.5(6) 5_656 1_656 ?
F1B Cs4 F2A 44.3(6) 5_656 2_656 ?
F1B Cs4 F6 153.2(6) 5_656 8_455 ?
F2A Cs4 F1A 42.0(4) 2_656 5_656 ?
F2A Cs4 F1A 54.1(4) 1_656 5_656 ?
F2A Cs4 F2A 29.3(5) 1_656 2_656 ?
F2A Cs4 F6 154.3(2) 2_656 8_455 ?
F2A Cs4 F6 153.2(2) 1_656 8_455 ?
F2B Cs4 F1A 52.9(4) 1_656 2_656 ?
F2B Cs4 F1A 52.8(3) 1_656 5_656 ?
F2B Cs4 F1B 50.7(6) 1_656 5_656 ?
F2B Cs4 F2A 40.7(3) 1_656 2_656 ?
F2B Cs4 F2A 14.7(3) 1_656 1_656 ?
F2B Cs4 F2C 18.5(3) 1_656 2_656 ?
F2B Cs4 F6 152.7(2) 1_656 8_455 ?
F2C Cs4 F1A 47.6(4) 2_656 2_656 ?
F2C Cs4 F1A 44.8(4) 2_656 5_656 ?
F2C Cs4 F1B 41.3(6) 2_656 5_656 ?
F2C Cs4 F2A 50.7(3) 2_656 2_656 ?
F2C Cs4 F2A 31.8(4) 2_656 1_656 ?
F2C Cs4 F6 152.0(2) 2_656 8_455 ?
F4 Cs4 F1A 89.0(4) . 2_656 ?
F4 Cs4 F1A 83.0(3) . 5_656 ?
F4 Cs4 F1B 80.8(6) . 5_656 ?
F4 Cs4 F2A 125.0(3) . 2_656 ?
F4 Cs4 F2A 124.0(3) . 1_656 ?
F4 Cs4 F2B 111.1(3) . 1_656 ?
F4 Cs4 F2C 92.7(3) . 2_656 ?
F4 Cs4 F6 76.13(9) . 8_455 ?
F4 Cs4 F7 88.40(10) . . ?
F4 Cs4 F8 154.82(10) . . ?
F4 Cs4 F9 87.76(11) . 8_455 ?
F6 Cs4 F1A 152.7(3) 8_455 5_656 ?
F7 Cs4 F1A 86.3(3) . 5_656 ?
F7 Cs4 F1A 82.7(3) . 2_656 ?
F7 Cs4 F1B 90.3(5) . 5_656 ?
F7 Cs4 F2A 89.3(2) . 2_656 ?
F7 Cs4 F2A 118.5(3) . 1_656 ?
F7 Cs4 F2B 129.3(2) . 1_656 ?
F7 Cs4 F2C 130.2(3) . 2_656 ?
F7 Cs4 F6 75.82(9) . 8_455 ?
F7 Cs4 F8 85.89(10) . . ?
F7 Cs4 F9 153.30(9) . 8_455 ?
F8 Cs4 F1A 120.9(3) . 5_656 ?
F8 Cs4 F1A 114.5(4) . 2_656 ?
F8 Cs4 F1B 123.7(5) . 5_656 ?
F8 Cs4 F2A 79.9(3) . 1_656 ?
F8 Cs4 F2A 79.5(3) . 2_656 ?
F8 Cs4 F2B 91.2(3) . 1_656 ?
F8 Cs4 F2C 109.6(3) . 2_656 ?
F8 Cs4 F6 78.69(8) . 8_455 ?
F8 Cs4 F9 86.43(10) . 8_455 ?
F9 Cs4 F1A 123.6(3) 8_455 2_656 ?
F9 Cs4 F1A 119.4(2) 8_455 5_656 ?
F9 Cs4 F1B 115.1(5) 8_455 5_656 ?
F9 Cs4 F2A 114.3(3) 8_455 2_656 ?
F9 Cs4 F2A 85.1(2) 8_455 1_656 ?
F9 Cs4 F2B 76.4(2) 8_455 1_656 ?
F9 Cs4 F2C 76.4(3) 8_455 2_656 ?
F9 Cs4 F6 77.61(9) 8_455 8_455 ?
F2C Cs5 F2B 10.5(3) 8_556 7_556 ?
F2C Cs5 F2B 33.5(3) 3_556 7_556 ?
F2C Cs5 F2C 23.8(6) 8_556 3_556 ?
F2C Cs5 F3 137.3(3) 3_556 7_657 ?
F2C Cs5 F3 137.3(3) 8_556 7_657 ?
F2C Cs5 F4 87.6(3) 3_556 4_657 ?
F2C Cs5 F4 87.6(3) 8_556 7_657 ?
F2C Cs5 F4 97.0(3) 8_556 4_657 ?
F2C Cs5 F4 97.0(3) 3_556 7_657 ?
F2C Cs5 F9 97.4(3) 3_556 2_757 ?
F2C Cs5 F9 73.8(3) 3_556 5_767 ?
F2C Cs5 F9 97.4(3) 8_556 5_767 ?
F2C Cs5 F9 73.8(3) 8_556 2_757 ?
F2C Cs5 F10 117.5(3) 8_556 . ?
F2C Cs5 F10 73.8(3) 3_556 5_767 ?
F2C Cs5 F10 117.5(3) 3_556 6_565 ?
F2C Cs5 F10 73.8(3) 8_556 2_757 ?
F2C Cs5 F10 136.5(3) 3_556 . ?
F2C Cs5 F10 87.7(3) 3_556 2_757 ?
F2C Cs5 F10 87.7(3) 8_556 5_767 ?
F2C Cs5 F10 136.5(3) 8_556 6_565 ?
F3 Cs5 F2B 138.5(2) 7_657 7_556 ?
F3 Cs5 F4 50.53(8) 7_657 7_657 ?
F3 Cs5 F4 50.53(8) 7_657 4_657 ?
F3 Cs5 F9 97.82(6) 7_657 2_757 ?
F3 Cs5 F9 97.82(6) 7_657 5_767 ?
F3 Cs5 F10 130.47(7) 7_657 2_757 ?
F3 Cs5 F10 81.62(8) 7_657 6_565 ?
F3 Cs5 F10 81.62(8) 7_657 . ?
F3 Cs5 F10 130.47(7) 7_657 5_767 ?
F4 Cs5 F2B 88.0(2) 7_657 7_556 ?
F4 Cs5 F2B 104.74(19) 4_657 7_556 ?
F4 Cs5 F4 46.94(12) 4_657 7_657 ?
F4 Cs5 F10 120.47(7) 7_657 2_757 ?
F4 Cs5 F10 120.47(7) 4_657 5_767 ?
F4 Cs5 F10 165.73(9) 7_657 5_767 ?
F4 Cs5 F10 165.73(9) 4_657 2_757 ?
F9 Cs5 F2B 63.88(19) 2_757 7_556 ?
F9 Cs5 F2B 106.2(2) 5_767 7_556 ?
F9 Cs5 F4 120.39(8) 5_767 7_657 ?
F9 Cs5 F4 73.58(8) 2_757 7_657 ?
F9 Cs5 F4 73.58(8) 5_767 4_657 ?
F9 Cs5 F4 120.39(8) 2_757 4_657 ?
F9 Cs5 F9 163.75(12) 2_757 5_767 ?
F9 Cs5 F10 47.07(7) 5_767 5_767 ?
F9 Cs5 F10 47.07(7) 2_757 2_757 ?
F9 Cs5 F10 117.85(7) 2_757 5_767 ?
F9 Cs5 F10 117.85(7) 5_767 2_757 ?
F10 Cs5 F2B 64.91(18) 2_757 7_556 ?
F10 Cs5 F2B 89.8(2) 5_767 7_556 ?
F10 Cs5 F2B 139.4(2) 6_565 7_556 ?
F10 Cs5 F2B 107.08(17) . 7_556 ?
F10 Cs5 F4 98.63(9) 6_565 4_657 ?
F10 Cs5 F4 131.37(8) 6_565 7_657 ?
F10 Cs5 F4 131.37(8) . 4_657 ?
F10 Cs5 F4 98.63(9) . 7_657 ?
F10 Cs5 F9 128.77(8) . 5_767 ?
F10 Cs5 F9 128.77(8) 6_565 2_757 ?
F10 Cs5 F9 49.94(7) . 2_757 ?
F10 Cs5 F9 49.94(7) 6_565 5_767 ?
F10 Cs5 F10 95.49(8) . 5_767 ?
F10 Cs5 F10 70.90(10) 2_757 5_767 ?
F10 Cs5 F10 49.59(9) . 2_757 ?
F10 Cs5 F10 79.78(12) 6_565 . ?
F10 Cs5 F10 95.49(8) 6_565 2_757 ?
F10 Cs5 F10 49.59(9) 6_565 5_767 ?
F3 Cs6 F4 47.37(9) 3 8 ?
F3 Cs6 F6 121.32(8) 3 8_455 ?
F3 Cs6 F8 116.95(8) 3 . ?
F3 Cs6 F9 88.82(9) 3 . ?
F3 Cs6 F10 70.68(8) 3 2_757 ?
F4 Cs6 F3 47.65(9) 7_656 3 ?
F4 Cs6 F4 47.21(10) 7_656 8 ?
F4 Cs6 F5 92.54(8) 7_656 7_656 ?
F4 Cs6 F6 121.50(7) 7_656 8_455 ?
F4 Cs6 F8 162.80(7) 7_656 . ?
F4 Cs6 F8 118.35(7) 8 . ?
F4 Cs6 F9 71.88(7) 8 . ?
F4 Cs6 F9 118.70(7) 7_656 . ?
F4 Cs6 F10 118.21(7) 7_656 2_757 ?
F4 Cs6 F10 90.73(9) 8 2_757 ?
F5 Cs6 F3 73.73(8) 7_656 3 ?
F5 Cs6 F4 120.91(7) 7_656 8 ?
F5 Cs6 F6 47.70(6) 7_656 8_455 ?
F5 Cs6 F8 88.94(8) 7_656 . ?
F5 Cs6 F9 117.21(7) 7_656 . ?
F5 Cs6 F10 70.99(7) 7_656 2_757 ?
F6 Cs6 F3 117.37(8) . 3 ?
F6 Cs6 F3 118.72(8) 2_756 3 ?
F6 Cs6 F4 166.87(6) 8_455 8 ?
F6 Cs6 F4 70.05(7) . 8 ?
F6 Cs6 F4 71.31(8) 2_756 7_656 ?
F6 Cs6 F4 90.64(9) . 7_656 ?
F6 Cs6 F4 89.83(9) 2_756 8 ?
F6 Cs6 F5 119.86(7) 2_756 7_656 ?
F6 Cs6 F5 166.72(6) . 7_656 ?
F6 Cs6 F6 91.93(8) 2_756 8_455 ?
F6 Cs6 F6 120.351(15) . 8_455 ?
F6 Cs6 F6 49.46(9) 2_756 . ?
F6 Cs6 F7 71.75(7) 2_756 7_656 ?
F6 Cs6 F7 120.88(7) . 7_656 ?
F6 Cs6 F8 122.31(7) 2_756 . ?
F6 Cs6 F8 71.26(7) 8_455 . ?
F6 Cs6 F8 91.83(8) . . ?
F6 Cs6 F9 72.04(7) . . ?
F6 Cs6 F9 121.35(7) 2_756 . ?
F6 Cs6 F9 117.75(7) 8_455 . ?
F6 Cs6 F10 166.48(6) 2_756 2_757 ?
F6 Cs6 F10 118.46(7) . 2_757 ?
F6 Cs6 F10 90.58(7) 8_455 2_757 ?
F7 Cs6 F3 165.68(8) . 3 ?
F7 Cs6 F3 93.52(9) 7_656 3 ?
F7 Cs6 F4 120.71(8) . 7_656 ?
F7 Cs6 F4 74.11(7) 7_656 7_656 ?
F7 Cs6 F4 121.23(7) 7_656 8 ?
F7 Cs6 F4 119.59(8) . 8 ?
F7 Cs6 F5 48.20(7) 7_656 7_656 ?
F7 Cs6 F5 118.25(7) . 7_656 ?
F7 Cs6 F6 70.68(7) . 8_455 ?
F7 Cs6 F6 49.74(7) . . ?
F7 Cs6 F6 49.59(7) . 2_756 ?
F7 Cs6 F6 47.62(7) 7_656 8_455 ?
F7 Cs6 F7 89.95(8) . 7_656 ?
F7 Cs6 F8 72.97(7) . . ?
F7 Cs6 F8 118.58(7) 7_656 . ?
F7 Cs6 F9 163.17(7) 7_656 . ?
F7 Cs6 F9 91.87(8) . . ?
F7 Cs6 F10 119.36(7) . 2_757 ?
F7 Cs6 F10 119.02(7) 7_656 2_757 ?
F8 Cs6 F9 46.63(7) . . ?
F8 Cs6 F10 46.53(7) . 2_757 ?
F9 Cs6 F10 46.50(7) . 2_757 ?
Cs1A Ga1 Cs1A 64.62(3) 8 2_757 ?
Cs1A Ga1 Cs1A 86.69(4) 8 7_657 ?
Cs1A Ga1 Cs1A 64.62(3) 7_657 . ?
Cs1A Ga1 Cs1A 104.42(2) 7_657 2_757 ?
Cs1A Ga1 Cs1A 104.42(2) 8 . ?
Cs1A Ga1 Cs1A 165.81(4) 2_757 . ?
Cs1A Ga1 Cs5 168.25(2) 8 . ?
Cs1A Ga1 Cs5 106.801(19) . 5_767 ?
Cs1A Ga1 Cs5 103.70(2) 7_657 . ?
Cs1A Ga1 Cs5 85.26(2) 2_757 5_767 ?
Cs1A Ga1 Cs5 106.800(19) 2_757 . ?
Cs1A Ga1 Cs5 103.70(2) 8 5_767 ?
Cs1A Ga1 Cs5 85.26(2) . . ?
Cs1A Ga1 Cs5 168.25(2) 7_657 5_767 ?
Cs5 Ga1 Cs5 66.571(13) 5_767 . ?
F8 Ga1 Cs1A 120.33(10) . 2_757 ?
F8 Ga1 Cs1A 57.84(10) . 8 ?
F8 Ga1 Cs1A 59.59(11) 2_757 8 ?
F8 Ga1 Cs1A 47.05(10) 2_757 2_757 ?
F8 Ga1 Cs1A 120.33(10) 2_757 . ?
F8 Ga1 Cs1A 59.59(11) . 7_657 ?
F8 Ga1 Cs1A 57.84(10) 2_757 7_657 ?
F8 Ga1 Cs1A 47.05(10) . . ?
F8 Ga1 Cs5 132.30(10) . . ?
F8 Ga1 Cs5 132.30(10) 2_757 5_767 ?
F8 Ga1 Cs5 121.38(11) . 5_767 ?
F8 Ga1 Cs5 121.38(11) 2_757 . ?
F8 Ga1 F8 88.9(2) . 2_757 ?
F8 Ga1 F9 90.69(15) . 2_757 ?
F8 Ga1 F9 90.05(15) . . ?
F8 Ga1 F9 90.69(15) 2_757 . ?
F8 Ga1 F9 90.05(15) 2_757 2_757 ?
F8 Ga1 F10 90.22(14) 2_757 . ?
F8 Ga1 F10 178.73(14) . . ?
F8 Ga1 F10 178.73(14) 2_757 2_757 ?
F8 Ga1 F10 90.21(14) . 2_757 ?
F9 Ga1 Cs1A 133.85(10) 2_757 8 ?
F9 Ga1 Cs1A 133.85(10) . 7_657 ?
F9 Ga1 Cs1A 120.73(11) 2_757 2_757 ?
F9 Ga1 Cs1A 120.73(11) . . ?
F9 Ga1 Cs1A 47.18(10) . 8 ?
F9 Ga1 Cs1A 59.42(11) . 2_757 ?
F9 Ga1 Cs1A 47.18(10) 2_757 7_657 ?
F9 Ga1 Cs1A 59.42(11) 2_757 . ?
F9 Ga1 Cs5 122.09(10) 2_757 5_767 ?
F9 Ga1 Cs5 122.09(10) . . ?
F9 Ga1 Cs5 56.89(10) . 5_767 ?
F9 Ga1 Cs5 56.89(10) 2_757 . ?
F9 Ga1 F9 179.0(2) 2_757 . ?
F9 Ga1 F10 90.20(15) 2_757 . ?
F9 Ga1 F10 90.20(15) . 2_757 ?
F9 Ga1 F10 89.08(15) 2_757 2_757 ?
F9 Ga1 F10 89.08(15) . . ?
F10 Ga1 Cs1A 58.41(10) . 2_757 ?
F10 Ga1 Cs1A 120.91(10) 2_757 7_657 ?
F10 Ga1 Cs1A 120.56(11) 2_757 8 ?
F10 Ga1 Cs1A 58.41(10) 2_757 . ?
F10 Ga1 Cs1A 120.56(11) . 7_657 ?
F10 Ga1 Cs1A 134.21(10) 2_757 2_757 ?
F10 Ga1 Cs1A 120.91(10) . 8 ?
F10 Ga1 Cs1A 134.21(10) . . ?
F10 Ga1 Cs5 48.97(10) 2_757 5_767 ?
F10 Ga1 Cs5 58.77(11) 2_757 . ?
F10 Ga1 Cs5 58.77(11) . 5_767 ?
F10 Ga1 Cs5 48.97(10) . . ?
F10 Ga1 F10 90.7(2) 2_757 . ?
F1A Ga2 F1A 180.0(14) 6 2 ?
F1A Ga2 F1A 157.1(15) . 2 ?
F1A Ga2 F1A 22.9(15) 5 2 ?
F1A Ga2 F1A 180.0(3) . 5 ?
F1A Ga2 F1A 157.1(15) 5 6 ?
F1A Ga2 F1A 22.9(15) . 6 ?
F1A Ga2 F2C 90.7(6) 6 5 ?
F1A Ga2 F2C 89.3(6) 6 . ?
F1A Ga2 F2C 97.7(6) . 5 ?
F1A Ga2 F2C 82.3(6) 5 5 ?
F1A Ga2 F2C 90.7(6) 2 . ?
F1A Ga2 F2C 82.3(6) . . ?
F1A Ga2 F2C 97.7(6) 5 . ?
F1A Ga2 F2C 89.3(6) 2 5 ?
F1B Ga2 F1A 161.0(7) 5 . ?
F1B Ga2 F1A 161.0(7) 5 6 ?
F1B Ga2 F1A 161.0(7) . 5 ?
F1B Ga2 F1A 161.0(7) . 2 ?
F1B Ga2 F1A 19.0(7) . 6 ?
F1B Ga2 F1A 19.0(7) 5 2 ?
F1B Ga2 F1A 19.0(7) . . ?
F1B Ga2 F1A 19.0(7) 5 5 ?
F1B Ga2 F1B 180.0 . 5 ?
F1B Ga2 F2C 108.9(8) 5 . ?
F1B Ga2 F2C 71.1(8) 5 5 ?
F1B Ga2 F2C 71.1(8) . . ?
F1B Ga2 F2C 108.9(8) . 5 ?
F2A Ga2 F1A 85.3(8) . 6 ?
F2A Ga2 F1A 85.3(8) 6 . ?
F2A Ga2 F1A 64.0(9) 6 6 ?
F2A Ga2 F1A 116.0(9) 6 2 ?
F2A Ga2 F1A 116.0(9) 5 . ?
F2A Ga2 F1A 64.0(9) 2 2 ?
F2A Ga2 F1A 116.0(9) 2 6 ?
F2A Ga2 F1A 64.0(9) . . ?
F2A Ga2 F1A 94.7(8) 2 . ?
F2A Ga2 F1A 64.0(9) 5 5 ?
F2A Ga2 F1A 94.7(8) 5 6 ?
F2A Ga2 F1A 116.0(9) . 5 ?
F2A Ga2 F1A 85.3(8) 5 2 ?
F2A Ga2 F1A 94.7(8) 6 5 ?
F2A Ga2 F1A 85.3(8) 2 5 ?
F2A Ga2 F1A 94.7(8) . 2 ?
F2A Ga2 F1B 99.4(6) 2 . ?
F2A Ga2 F1B 99.4(6) 6 5 ?
F2A Ga2 F1B 80.6(6) 5 5 ?
F2A Ga2 F1B 99.4(6) 5 . ?
F2A Ga2 F1B 80.6(6) 2 5 ?
F2A Ga2 F1B 80.6(6) . . ?
F2A Ga2 F1B 99.4(6) . 5 ?
F2A Ga2 F1B 80.6(6) 6 . ?
F2A Ga2 F2A 128.1(10) 6 . ?
F2A Ga2 F2A 180.0 5 . ?
F2A Ga2 F2A 51.9(10) 2 . ?
F2A Ga2 F2A 180.0(9) 6 2 ?
F2A Ga2 F2A 51.9(10) 6 5 ?
F2A Ga2 F2A 128.1(10) 2 5 ?
F2A Ga2 F2C 92.1(6) 5 5 ?
F2A Ga2 F2C 87.9(6) 5 . ?
F2A Ga2 F2C 54.2(6) 6 5 ?
F2A Ga2 F2C 87.9(6) . 5 ?
F2A Ga2 F2C 92.1(6) . . ?
F2A Ga2 F2C 125.8(6) 6 . ?
F2A Ga2 F2C 54.2(6) 2 . ?
F2A Ga2 F2C 125.8(6) 2 5 ?
F2C Ga2 F2C 180.0 . 5 ?
Cs2 Ga3 Cs2 180.0 5_656 . ?
Cs2 Ga3 Cs5 94.649(9) 5_656 3_444 ?
Cs2 Ga3 Cs5 85.351(9) 5_656 7_657 ?
Cs2 Ga3 Cs5 94.649(9) . 7_657 ?
Cs2 Ga3 Cs5 85.351(9) . 3_444 ?
Cs2 Ga3 Cs6 66.390(5) 5_656 4_646 ?
Cs2 Ga3 Cs6 66.390(5) . 8_455 ?
Cs2 Ga3 Cs6 113.610(5) 5_656 8_455 ?
Cs2 Ga3 Cs6 113.610(5) . 4_646 ?
Cs5 Ga3 Cs5 180.0 7_657 3_444 ?
Cs5 Ga3 Cs6 111.903(5) 7_657 4_646 ?
Cs5 Ga3 Cs6 68.097(5) 7_657 8_455 ?
Cs5 Ga3 Cs6 111.903(5) 3_444 8_455 ?
Cs5 Ga3 Cs6 68.097(5) 3_444 4_646 ?
Cs6 Ga3 Cs6 180.0 4_646 8_455 ?
F3 Ga3 Cs2 132.72(13) . 5_656 ?
F3 Ga3 Cs2 132.73(13) 5_656 . ?
F3 Ga3 Cs2 47.28(13) . . ?
F3 Ga3 Cs2 47.27(13) 5_656 5_656 ?
F3 Ga3 Cs5 47.37(13) 5_656 3_444 ?
F3 Ga3 Cs5 132.63(13) 5_656 7_657 ?
F3 Ga3 Cs5 132.63(13) . 3_444 ?
F3 Ga3 Cs5 47.37(13) . 7_657 ?
F3 Ga3 Cs6 124.792(5) 5_656 8_455 ?
F3 Ga3 Cs6 55.208(5) . 8_455 ?
F3 Ga3 Cs6 124.792(5) . 4_646 ?
F3 Ga3 Cs6 55.208(5) 5_656 4_646 ?
F3 Ga3 F3 180.0 5_656 . ?
F4 Ga3 Cs2 121.68(12) 2_656 5_656 ?
F4 Ga3 Cs2 121.68(12) 6 . ?
F4 Ga3 Cs2 58.32(12) 2_656 . ?
F4 Ga3 Cs2 58.32(12) 5_656 . ?
F4 Ga3 Cs2 121.68(12) . . ?
F4 Ga3 Cs2 121.68(12) 5_656 5_656 ?
F4 Ga3 Cs2 58.32(12) 6 5_656 ?
F4 Ga3 Cs2 58.32(12) . 5_656 ?
F4 Ga3 Cs5 58.73(12) 2_656 3_444 ?
F4 Ga3 Cs5 121.27(12) 6 3_444 ?
F4 Ga3 Cs5 121.27(12) 5_656 7_657 ?
F4 Ga3 Cs5 121.27(12) . 3_444 ?
F4 Ga3 Cs5 58.73(12) 5_656 3_444 ?
F4 Ga3 Cs5 58.73(12) 6 7_657 ?
F4 Ga3 Cs5 121.27(12) 2_656 7_657 ?
F4 Ga3 Cs5 58.73(12) . 7_657 ?
F4 Ga3 Cs6 55.79(12) 5_656 4_646 ?
F4 Ga3 Cs6 124.21(12) 5_656 8_455 ?
F4 Ga3 Cs6 55.79(12) . 8_455 ?
F4 Ga3 Cs6 53.57(12) 6 4_646 ?
F4 Ga3 Cs6 126.43(12) 6 8_455 ?
F4 Ga3 Cs6 126.43(12) 2_656 4_646 ?
F4 Ga3 Cs6 124.21(12) . 4_646 ?
F4 Ga3 Cs6 53.57(12) 2_656 8_455 ?
F4 Ga3 F3 89.70(15) 6 5_656 ?
F4 Ga3 F3 90.30(15) 5_656 5_656 ?
F4 Ga3 F3 90.29(15) . . ?
F4 Ga3 F3 90.30(15) 2_656 5_656 ?
F4 Ga3 F3 89.70(15) 2_656 . ?
F4 Ga3 F3 89.71(15) . 5_656 ?
F4 Ga3 F3 89.70(15) 5_656 . ?
F4 Ga3 F3 90.30(15) 6 . ?
F4 Ga3 F4 180.0(2) 6 2_656 ?
F4 Ga3 F4 89.5(2) 6 . ?
F4 Ga3 F4 90.5(2) 5_656 6 ?
F4 Ga3 F4 90.5(2) 2_656 . ?
F4 Ga3 F4 180.0 5_656 . ?
F4 Ga3 F4 89.5(2) 5_656 2_656 ?
Cs1A Ga4 Cs1A 169.99(4) 8 7_656 ?
Cs1A Ga4 Cs1B 4.58(3) 7_656 7_656 ?
Cs1A Ga4 Cs1B 173.39(5) 7_656 8 ?
Cs1A Ga4 Cs1B 173.39(5) 8 7_656 ?
Cs1A Ga4 Cs1B 4.58(3) 8 8 ?
Cs1A Ga4 Cs6 103.43(2) 8 2_756 ?
Cs1A Ga4 Cs6 103.43(2) 7_656 . ?
Cs1A Ga4 Cs6 68.121(17) 7_656 2_756 ?
Cs1A Ga4 Cs6 68.121(17) 8 . ?
Cs1B Ga4 Cs1B 177.73(7) 8 7_656 ?
Cs6 Ga4 Cs1B 70.06(4) 2_756 7_656 ?
Cs6 Ga4 Cs1B 70.06(4) . 8 ?
Cs6 Ga4 Cs1B 108.01(3) . 7_656 ?
Cs6 Ga4 Cs1B 108.01(3) 2_756 8 ?
Cs6 Ga4 Cs6 72.729(13) 2_756 . ?
F5 Ga4 Cs1A 131.98(9) 2_756 7_656 ?
F5 Ga4 Cs1A 131.98(9) . 8 ?
F5 Ga4 Cs1A 56.97(9) . 7_656 ?
F5 Ga4 Cs1A 56.97(9) 2_756 8 ?
F5 Ga4 Cs1B 127.41(9) . 8 ?
F5 Ga4 Cs1B 54.60(10) . 7_656 ?
F5 Ga4 Cs1B 54.59(10) 2_756 8 ?
F5 Ga4 Cs1B 127.41(10) 2_756 7_656 ?
F5 Ga4 Cs6 124.51(9) . 2_756 ?
F5 Ga4 Cs6 125.24(10) . . ?
F5 Ga4 Cs6 125.24(10) 2_756 2_756 ?
F5 Ga4 Cs6 124.51(9) 2_756 . ?
F5 Ga4 F5 89.52(18) 2_756 . ?
F6 Ga4 Cs1A 122.59(9) . 7_656 ?
F6 Ga4 Cs1A 122.59(9) 2_756 8 ?
F6 Ga4 Cs1A 48.56(9) . 8 ?
F6 Ga4 Cs1A 48.56(9) 2_756 7_656 ?
F6 Ga4 Cs1B 124.89(10) . 7_656 ?
F6 Ga4 Cs1B 53.13(9) . 8 ?
F6 Ga4 Cs1B 124.89(10) 2_756 8 ?
F6 Ga4 Cs1B 53.13(9) 2_756 7_656 ?
F6 Ga4 Cs6 54.90(9) 2_756 . ?
F6 Ga4 Cs6 54.90(9) . 2_756 ?
F6 Ga4 Cs6 55.75(9) 2_756 2_756 ?
F6 Ga4 Cs6 55.74(9) . . ?
F6 Ga4 F5 90.21(12) 2_756 . ?
F6 Ga4 F5 178.87(14) 2_756 2_756 ?
F6 Ga4 F5 178.87(14) . . ?
F6 Ga4 F5 90.21(12) . 2_756 ?
F6 Ga4 F6 90.09(17) 2_756 . ?
F7 Ga4 Cs1A 120.97(10) . 7_656 ?
F7 Ga4 Cs1A 59.17(10) . 8 ?
F7 Ga4 Cs1A 59.18(10) 2_756 7_656 ?
F7 Ga4 Cs1A 120.97(10) 2_756 8 ?
F7 Ga4 Cs1B 123.50(11) 2_756 8 ?
F7 Ga4 Cs1B 56.54(11) . 8 ?
F7 Ga4 Cs1B 123.50(11) . 7_656 ?
F7 Ga4 Cs1B 56.54(11) 2_756 7_656 ?
F7 Ga4 Cs6 127.07(10) 2_756 . ?
F7 Ga4 Cs6 54.35(10) 2_756 2_756 ?
F7 Ga4 Cs6 127.07(10) . 2_756 ?
F7 Ga4 Cs6 54.34(10) . . ?
F7 Ga4 F5 90.16(14) . . ?
F7 Ga4 F5 88.83(14) 2_756 . ?
F7 Ga4 F5 88.83(14) . 2_756 ?
F7 Ga4 F5 90.16(14) 2_756 2_756 ?
F7 Ga4 F6 90.08(14) . 2_756 ?
F7 Ga4 F6 90.08(14) 2_756 . ?
F7 Ga4 F6 90.92(14) 2_756 2_756 ?
F7 Ga4 F6 90.92(14) . . ?
F7 Ga4 F7 178.6(2) . 2_756 ?
Cs1B F1A Cs4 177.2(5) 7_556 5_656 ?
Cs2 F1A Cs1B 104.2(6) . 7_556 ?
Cs2 F1A Cs3 84.6(4) . 3_344 ?
Cs2 F1A Cs4 73.1(5) . 5_656 ?
Cs2 F1A Cs4 83.7(5) . 2_656 ?
Cs3 F1A Cs1B 68.3(4) 3_344 7_556 ?
Cs3 F1A Cs4 130.1(7) 3_344 2_656 ?
Cs3 F1A Cs4 110.5(6) 3_344 5_656 ?
Cs4 F1A Cs1B 68.0(5) 2_656 7_556 ?
Cs4 F1A Cs4 112.0(4) 2_656 5_656 ?
Ga2 F1A Cs1B 97.1(8) . 7_556 ?
Ga2 F1A Cs2 158.7(12) . . ?
Ga2 F1A Cs3 102.5(6) . 3_344 ?
Ga2 F1A Cs4 105.7(7) . 2_656 ?
Ga2 F1A Cs4 85.6(7) . 5_656 ?
F1A F1A Cs1B 149.4(3) 6 7_556 ?
F1A F1A Cs2 82.5(5) 6 . ?
F1A F1A Cs3 82.9(5) 6 3_344 ?
F1A F1A Cs4 142.5(4) 6 2_656 ?
F1A F1A Cs4 30.5(2) 6 5_656 ?
F1A F1A Ga2 78.6(7) 6 . ?
F1B F1A Cs1B 157(3) . 7_556 ?
F1B F1A Cs2 81(5) . . ?
F1B F1A Cs3 135(3) . 3_344 ?
F1B F1A Cs4 90(3) . 2_656 ?
F1B F1A Cs4 25(3) . 5_656 ?
F1B F1A Ga2 80(4) . . ?
F1B F1A F1A 53(3) . 6 ?
Cs2 F1B Cs3 76.9(6) . 3_344 ?
Cs2 F1B Cs4 83.1(7) . 2_656 ?
Cs2 F1B Cs4 83.1(7) . 5_656 ?
Cs4 F1B Cs3 113.0(4) 5_656 3_344 ?
Cs4 F1B Cs3 113.0(4) 2_656 3_344 ?
Cs4 F1B Cs4 127.0(9) 2_656 5_656 ?
Ga2 F1B Cs2 164.3(12) . . ?
Ga2 F1B Cs3 87.5(9) . 3_344 ?
Ga2 F1B Cs4 103.4(7) . 5_656 ?
Ga2 F1B Cs4 103.4(7) . 2_656 ?
F1A F1B Cs2 87(4) 6 . ?
F1A F1B Cs2 87(4) . . ?
F1A F1B Cs3 38(3) . 3_344 ?
F1A F1B Cs3 38(3) 6 3_344 ?
F1A F1B Cs4 151(3) . 5_656 ?
F1A F1B Cs4 78(3) . 2_656 ?
F1A F1B Cs4 151(3) 6 2_656 ?
F1A F1B Cs4 78(3) 6 5_656 ?
F1A F1B Ga2 81(5) . . ?
F1A F1B Ga2 81(5) 6 . ?
F1A F1B F1A 74(6) . 6 ?
Cs1A F2A Cs1B 102.7(4) 7_556 8_454 ?
Cs1A F2A Cs3 76.5(3) 7_556 3_344 ?
Cs1A F2A Cs4 86.6(4) 7_556 1_454 ?
Cs1A F2A Cs4 81.9(4) 7_556 2_656 ?
Cs1B F2A Cs1A 0.58(9) 7_556 7_556 ?
Cs1B F2A Cs1B 103.3(5) 7_556 8_454 ?
Cs1B F2A Cs3 76.0(4) 7_556 3_344 ?
Cs1B F2A Cs4 81.9(4) 7_556 2_656 ?
Cs1B F2A Cs4 87.0(4) 7_556 1_454 ?
Cs3 F2A Cs1B 178.3(5) 3_344 8_454 ?
Cs4 F2A Cs1B 67.6(3) 2_656 8_454 ?
Cs4 F2A Cs1B 65.6(3) 1_454 8_454 ?
Cs4 F2A Cs3 115.8(5) 1_454 3_344 ?
Cs4 F2A Cs3 110.7(4) 2_656 3_344 ?
Cs4 F2A Cs4 127.6(5) 1_454 2_656 ?
Ga2 F2A Cs1A 163.6(8) . 7_556 ?
Ga2 F2A Cs1B 93.2(5) . 8_454 ?
Ga2 F2A Cs1B 163.1(8) . 7_556 ?
Ga2 F2A Cs3 87.4(6) . 3_344 ?
Ga2 F2A Cs4 103.6(6) . 1_454 ?
Ga2 F2A Cs4 101.1(6) . 2_656 ?
F2A F2A Cs1A 131.5(4) 2 7_556 ?
F2A F2A Cs1B 132.0(4) 2 7_556 ?
F2A F2A Cs1B 29.3(2) 2 8_454 ?
F2A F2A Cs3 151.1(3) 2 3_344 ?
F2A F2A Cs4 77.7(10) 2 1_454 ?
F2A F2A Cs4 73.0(10) 2 2_656 ?
F2A F2A Ga2 64.1(5) 2 . ?
F2A F2A F2C 108.0(11) 2 2 ?
F2B F2A Cs1A 91.4(13) . 7_556 ?
F2B F2A Cs1B 91.2(13) . 7_556 ?
F2B F2A Cs1B 132.5(17) . 8_454 ?
F2B F2A Cs3 49.2(15) . 3_344 ?
F2B F2A Cs4 159.9(18) . 2_656 ?
F2B F2A Cs4 70.3(16) . 1_454 ?
F2B F2A Ga2 80.4(14) . . ?
F2B F2A F2A 124(2) . 2 ?
F2B F2A F2C 17.9(11) . 2 ?
F2C F2A Cs1A 109.1(8) 2 7_556 ?
F2C F2A Cs1B 108.9(8) 2 7_556 ?
F2C F2A Cs1B 122.9(8) 2 8_454 ?
F2C F2A Cs3 58.8(6) 2 3_344 ?
F2C F2A Cs4 160.6(9) 2 2_656 ?
F2C F2A Cs4 70.3(7) 2 1_454 ?
F2C F2A Ga2 63.9(7) 2 . ?
Cs1A F2B Cs3 82.6(3) 7_556 3_344 ?
Cs1A F2B Cs4 87.6(3) 7_556 1_454 ?
Cs1A F2B Cs5 108.5(3) 7_556 7_556 ?
Cs1B F2B Cs1A 1.84(8) 7_556 7_556 ?
Cs1B F2B Cs3 83.2(3) 7_556 3_344 ?
Cs1B F2B Cs4 88.3(3) 7_556 1_454 ?
Cs1B F2B Cs5 110.3(3) 7_556 7_556 ?
Cs3 F2B Cs5 73.0(3) 3_344 7_556 ?
Cs4 F2B Cs3 139.2(4) 1_454 3_344 ?
Cs4 F2B Cs5 72.9(3) 1_454 7_556 ?
Ga2 F2B Cs1A 144.7(6) . 7_556 ?
Ga2 F2B Cs1B 142.9(7) . 7_556 ?
Ga2 F2B Cs3 101.5(5) . 3_344 ?
Ga2 F2B Cs4 109.0(5) . 1_454 ?
Ga2 F2B Cs5 106.2(5) . 7_556 ?
F2A F2B Cs1A 72.7(12) . 7_556 ?
F2A F2B Cs1B 71.0(12) . 7_556 ?
F2A F2B Cs3 119.2(17) . 3_344 ?
F2A F2B Cs4 95.0(17) . 1_454 ?
F2A F2B Cs5 167.6(18) . 7_556 ?
F2A F2B Ga2 74.8(12) . . ?
F2A F2B F2C 147.4(19) . 2 ?
F2C F2B Cs1A 139.5(12) 2 7_556 ?
F2C F2B Cs1B 141.3(12) 2 7_556 ?
F2C F2B Cs3 78.5(11) 2 3_344 ?
F2C F2B Cs4 84.0(11) 2 1_454 ?
F2C F2B Cs5 31.5(10) 2 7_556 ?
F2C F2B Ga2 74.7(10) 2 . ?
Cs1B F2C Cs1A 2.26(6) 8_454 8_454 ?
Cs3 F2C Cs1A 70.9(3) 7_656 8_454 ?
Cs3 F2C Cs1B 71.4(3) 7_656 8_454 ?
Cs3 F2C Cs4 138.4(5) 7_656 2_656 ?
Cs4 F2C Cs1A 73.8(3) 2_656 8_454 ?
Cs4 F2C Cs1B 74.1(3) 2_656 8_454 ?
Cs5 F2C Cs1A 107.8(4) 3_444 8_454 ?
Cs5 F2C Cs1B 110.0(4) 3_444 8_454 ?
Cs5 F2C Cs3 86.1(3) 3_444 7_656 ?
Cs5 F2C Cs4 84.4(4) 3_444 2_656 ?
Ga2 F2C Cs1A 105.8(5) . 8_454 ?
Ga2 F2C Cs1B 103.5(5) . 8_454 ?
Ga2 F2C Cs3 103.1(5) . 7_656 ?
Ga2 F2C Cs4 107.1(4) . 2_656 ?
Ga2 F2C Cs5 146.4(7) . 3_444 ?
F2A F2C Cs1A 45.3(5) 2 8_454 ?
F2A F2C Cs1B 43.1(5) 2 8_454 ?
F2A F2C Cs3 92.0(7) 2 7_656 ?
F2A F2C Cs4 77.9(7) 2 2_656 ?
F2A F2C Cs5 151.1(9) 2 3_444 ?
F2A F2C Ga2 61.9(6) 2 . ?
F2B F2C Cs1A 30.8(9) 2 8_454 ?
F2B F2C Cs1B 28.5(9) 2 8_454 ?
F2B F2C Cs3 83.0(12) 2 7_656 ?
F2B F2C Cs4 77.5(11) 2 2_656 ?
F2B F2C Cs5 138.1(13) 2 3_444 ?
F2B F2C Ga2 75.5(10) 2 . ?
F2B F2C F2A 14.8(9) 2 2 ?
F2B F2C F2C 138.1(11) 2 6 ?
F2C F2C Cs1A 148.52(19) 6 8_454 ?
F2C F2C Cs1B 148.3(2) 6 8_454 ?
F2C F2C Cs3 78.9(3) 6 7_656 ?
F2C F2C Cs4 137.6(3) 6 2_656 ?
F2C F2C Cs5 78.1(3) 6 3_444 ?
F2C F2C Ga2 72.2(4) 6 . ?
F2C F2C F2A 129.8(7) 6 2 ?
Cs2 F3 Cs3 74.49(9) . 7_657 ?
Cs2 F3 Cs5 152.38(15) . 7_657 ?
Cs2 F3 Cs6 87.21(7) . 8_455 ?
Cs2 F3 Cs6 87.21(7) . 3_445 ?
Cs5 F3 Cs3 77.89(9) 7_657 7_657 ?
Cs5 F3 Cs6 89.64(7) 7_657 3_445 ?
Cs5 F3 Cs6 89.64(7) 7_657 8_455 ?
Cs6 F3 Cs3 83.36(7) 3_445 7_657 ?
Cs6 F3 Cs3 83.36(7) 8_455 7_657 ?
Cs6 F3 Cs6 166.56(13) 3_445 8_455 ?
Ga3 F3 Cs2 103.73(16) . . ?
Ga3 F3 Cs3 178.22(19) . 7_657 ?
Ga3 F3 Cs5 103.89(16) . 7_657 ?
Ga3 F3 Cs6 96.60(7) . 3_445 ?
Ga3 F3 Cs6 96.60(7) . 8_455 ?
Cs2 F4 Cs5 105.13(11) 5_656 7_657 ?
Cs2 F4 Cs6 167.33(12) 5_656 8_455 ?
Cs2 F4 Cs6 82.26(9) 5_656 7_656 ?
Cs4 F4 Cs2 80.89(9) . 5_656 ?
Cs4 F4 Cs5 79.19(8) . 7_657 ?
Cs4 F4 Cs6 91.53(9) . 8_455 ?
Cs4 F4 Cs6 90.64(9) . 7_656 ?
Cs5 F4 Cs6 83.18(9) 7_657 8_455 ?
Cs6 F4 Cs5 166.13(11) 7_656 7_657 ?
Cs6 F4 Cs6 87.73(9) 7_656 8_455 ?
Ga3 F4 Cs2 92.53(13) . 5_656 ?
Ga3 F4 Cs4 167.4(2) . . ?
Ga3 F4 Cs5 92.35(13) . 7_657 ?
Ga3 F4 Cs6 99.12(14) . 7_656 ?
Ga3 F4 Cs6 96.72(13) . 8_455 ?
Cs1A F5 Cs1B 5.77(3) 7_656 7_656 ?
Cs1A F5 Cs2 106.62(9) 7_656 1_655 ?
Cs1A F5 Cs6 84.43(8) 7_656 7_656 ?
Cs1B F5 Cs2 101.64(10) 7_656 1_655 ?
Cs1B F5 Cs6 88.72(9) 7_656 7_656 ?
Cs2 F5 Cs1A 159.35(10) 5_656 7_656 ?
Cs2 F5 Cs1B 157.22(10) 5_656 7_656 ?
Cs2 F5 Cs2 79.97(7) 5_656 1_655 ?
Cs2 F5 Cs6 85.91(8) 5_656 7_656 ?
Cs3 F5 Cs1A 79.66(7) 3_444 7_656 ?
Cs3 F5 Cs1B 75.41(8) 3_444 7_656 ?
Cs3 F5 Cs2 82.95(7) 3_444 5_656 ?
Cs3 F5 Cs2 77.07(7) 3_444 1_655 ?
Cs3 F5 Cs6 94.42(8) 3_444 7_656 ?
Cs6 F5 Cs2 164.27(10) 7_656 1_655 ?
Ga4 F5 Cs1A 93.28(11) . 7_656 ?
Ga4 F5 Cs1B 96.61(12) . 7_656 ?
Ga4 F5 Cs2 93.49(11) . 1_655 ?
Ga4 F5 Cs2 106.01(11) . 5_656 ?
Ga4 F5 Cs3 165.86(16) . 3_444 ?
Ga4 F5 Cs6 97.07(11) . 7_656 ?
Cs1A F6 Cs1B 4.24(5) 8 8 ?
Cs1A F6 Cs4 77.04(7) 8 8 ?
Cs1A F6 Cs6 87.92(7) 8 8 ?
Cs1A F6 Cs6 88.87(8) 8 . ?
Cs1A F6 Cs6 161.25(10) 8 2_756 ?
Cs1B F6 Cs4 81.28(8) 8 8 ?
Cs1B F6 Cs6 88.97(9) 8 . ?
Cs1B F6 Cs6 88.59(8) 8 8 ?
Cs1B F6 Cs6 165.49(10) 8 2_756 ?
Cs4 F6 Cs6 83.32(6) 8 8 ?
Cs6 F6 Cs4 84.30(6) 2_756 8 ?
Cs6 F6 Cs4 85.98(7) . 8 ?
Cs6 F6 Cs6 91.71(7) 2_756 . ?
Cs6 F6 Cs6 169.26(9) . 8 ?
Cs6 F6 Cs6 88.07(8) 2_756 8 ?
Ga4 F6 Cs1A 102.57(11) . 8 ?
Ga4 F6 Cs1B 98.34(11) . 8 ?
Ga4 F6 Cs4 178.81(14) . 8 ?
Ga4 F6 Cs6 96.04(10) . 2_756 ?
Ga4 F6 Cs6 95.14(11) . . ?
Ga4 F6 Cs6 95.55(11) . 8 ?
Cs1A F7 Cs2 104.19(9) 8 5_656 ?
Cs1B F7 Cs1A 5.65(3) 8 8 ?
Cs1B F7 Cs2 99.56(9) 8 5_656 ?
Cs4 F7 Cs1A 80.09(8) . 8 ?
Cs4 F7 Cs1B 75.73(8) . 8 ?
Cs4 F7 Cs2 77.76(7) . 5_656 ?
Cs4 F7 Cs6 90.59(8) . 7_656 ?
Cs4 F7 Cs6 94.12(8) . . ?
Cs6 F7 Cs1A 83.78(8) . 8 ?
Cs6 F7 Cs1A 168.38(10) 7_656 8 ?
Cs6 F7 Cs1B 87.76(9) . 8 ?
Cs6 F7 Cs1B 165.94(10) 7_656 8 ?
Cs6 F7 Cs2 167.24(10) . 5_656 ?
Cs6 F7 Cs2 80.31(7) 7_656 5_656 ?
Cs6 F7 Cs6 90.05(8) . 7_656 ?
Ga4 F7 Cs1A 91.47(11) . 8 ?
Ga4 F7 Cs1B 94.99(12) . 8 ?
Ga4 F7 Cs2 92.87(11) . 5_656 ?
Ga4 F7 Cs4 165.30(17) . . ?
Ga4 F7 Cs6 99.06(12) . 7_656 ?
Ga4 F7 Cs6 96.92(11) . . ?
Cs1A F8 Cs1A 106.73(10) 8 7_657 ?
Cs1A F8 Cs1A 82.25(9) . 7_657 ?
Cs1A F8 Cs1A 159.41(11) . 8 ?
Cs1A F8 Cs1B 85.77(10) . 7_657 ?
Cs1A F8 Cs1B 4.50(5) . . ?
Cs1A F8 Cs1B 102.00(10) 8 7_657 ?
Cs1A F8 Cs1B 157.88(10) . 8 ?
Cs1A F8 Cs6 167.26(10) 7_657 . ?
Cs1A F8 Cs6 87.48(8) . . ?
Cs1A F8 Cs6 80.72(8) 8 . ?
Cs1B F8 Cs1A 81.94(9) . 7_657 ?
Cs1B F8 Cs1A 5.63(3) 8 8 ?
Cs1B F8 Cs1A 163.44(11) . 8 ?
Cs1B F8 Cs1A 101.95(10) 8 7_657 ?
Cs1B F8 Cs1A 5.53(3) 7_657 7_657 ?
Cs1B F8 Cs1B 85.80(11) . 7_657 ?
Cs1B F8 Cs1B 97.08(11) 8 7_657 ?
Cs1B F8 Cs1B 162.31(12) . 8 ?
Cs1B F8 Cs6 88.40(9) . . ?
Cs1B F8 Cs6 166.39(10) 7_657 . ?
Cs1B F8 Cs6 84.86(9) 8 . ?
Cs4 F8 Cs1A 83.66(8) . . ?
Cs4 F8 Cs1A 81.71(8) . 7_657 ?
Cs4 F8 Cs1A 79.49(8) . 8 ?
Cs4 F8 Cs1B 77.80(9) . 7_657 ?
Cs4 F8 Cs1B 75.59(8) . 8 ?
Cs4 F8 Cs1B 88.06(9) . . ?
Cs4 F8 Cs6 89.72(8) . . ?
Ga1 F8 Cs1A 93.30(11) . 8 ?
Ga1 F8 Cs1A 91.51(12) . 7_657 ?
Ga1 F8 Cs1A 105.15(13) . . ?
Ga1 F8 Cs1B 100.67(13) . . ?
Ga1 F8 Cs1B 96.50(12) . 8 ?
Ga1 F8 Cs1B 94.72(13) . 7_657 ?
Ga1 F8 Cs4 168.15(16) . . ?
Ga1 F8 Cs6 98.45(12) . . ?
Cs1A F9 Cs1A 82.28(9) 8 2_757 ?
Cs1A F9 Cs1B 85.59(10) 8 2_757 ?
Cs1A F9 Cs1B 4.72(5) 8 8 ?
Cs1A F9 Cs5 159.04(10) 8 5_767 ?
Cs1A F9 Cs6 166.13(10) 2_757 . ?
Cs1A F9 Cs6 85.83(9) 8 . ?
Cs1B F9 Cs1A 82.17(9) 8 2_757 ?
Cs1B F9 Cs1A 5.54(3) 2_757 2_757 ?
Cs1B F9 Cs1B 85.83(11) 8 2_757 ?
Cs1B F9 Cs5 163.32(11) 8 5_767 ?
Cs1B F9 Cs6 86.57(10) 8 . ?
Cs1B F9 Cs6 165.54(10) 2_757 . ?
Cs4 F9 Cs1A 83.41(8) 8 8 ?
Cs4 F9 Cs1A 81.58(8) 8 2_757 ?
Cs4 F9 Cs1B 77.48(9) 8 2_757 ?
Cs4 F9 Cs1B 88.06(9) 8 8 ?
Cs4 F9 Cs5 78.68(7) 8 5_767 ?
Cs4 F9 Cs6 89.99(8) 8 . ?
Cs5 F9 Cs1A 105.53(10) 5_767 2_757 ?
Cs5 F9 Cs1B 100.90(10) 5_767 2_757 ?
Cs5 F9 Cs6 83.39(8) 5_767 . ?
Ga1 F9 Cs1A 91.69(12) . 2_757 ?
Ga1 F9 Cs1A 104.97(13) . 8 ?
Ga1 F9 Cs1B 95.16(13) . 2_757 ?
Ga1 F9 Cs1B 100.25(12) . 8 ?
Ga1 F9 Cs4 168.56(17) . 8 ?
Ga1 F9 Cs5 94.36(11) . 5_767 ?
Ga1 F9 Cs6 98.29(13) . . ?
Cs1A F10 Cs5 104.89(10) 2_757 5_767 ?
Cs1A F10 Cs6 81.32(8) 2_757 2_757 ?
Cs1B F10 Cs1A 5.60(3) 2_757 2_757 ?
Cs1B F10 Cs5 100.08(10) 2_757 5_767 ?
Cs1B F10 Cs6 85.55(9) 2_757 2_757 ?
Cs3 F10 Cs1A 78.56(7) . 2_757 ?
Cs3 F10 Cs1B 74.54(8) . 2_757 ?
Cs3 F10 Cs5 88.04(8) . . ?
Cs3 F10 Cs5 78.51(8) . 5_767 ?
Cs3 F10 Cs6 93.32(8) . 2_757 ?
Cs5 F10 Cs1A 161.54(10) . 2_757 ?
Cs5 F10 Cs1B 160.54(10) . 2_757 ?
Cs5 F10 Cs5 84.51(8) . 5_767 ?
Cs5 F10 Cs6 168.32(10) 5_767 2_757 ?
Cs5 F10 Cs6 86.90(8) . 2_757 ?
Ga1 F10 Cs1A 92.66(11) . 2_757 ?
Ga1 F10 Cs1B 95.80(12) . 2_757 ?
Ga1 F10 Cs3 165.09(17) . . ?
Ga1 F10 Cs5 92.36(12) . 5_767 ?
Ga1 F10 Cs5 102.94(12) . . ?
Ga1 F10 Cs6 97.28(12) . 2_757 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cs1A F2A 2.802(12) 7_556 ?
Cs1A F2B 2.933(11) 7_556 ?
Cs1A F2C 3.724(14) 8_556 ?
Cs1A F5 3.221(3) 7_656 ?
Cs1A F6 2.946(3) 8_455 ?
Cs1A F7 3.295(4) 8_455 ?
Cs1A F8 3.308(3) 8_455 ?
Cs1A F8 2.960(3) . ?
Cs1A F8 3.365(4) 7_657 ?
Cs1A F9 3.362(4) 2_757 ?
Cs1A F9 2.961(3) 8_455 ?
Cs1A F10 3.328(3) 2_757 ?
Cs1B F2A 2.478(12) 7_556 ?
Cs1B F2B 2.621(11) 7_556 ?
Cs1B F2C 3.432(14) 8_556 ?
Cs1B F5 3.226(4) 7_656 ?
Cs1B F6 3.179(4) 8_455 ?
Cs1B F7 3.292(4) 8_455 ?
Cs1B F8 3.178(4) . ?
Cs1B F8 3.279(4) 8_455 ?
Cs1B F8 3.335(4) 7_657 ?
Cs1B F9 3.344(5) 2_757 ?
Cs1B F9 3.166(4) 8_455 ?
Cs1B F10 3.322(4) 2_757 ?
Cs2 F1A 2.850(19) . ?
Cs2 F1A 2.850(19) 6 ?
Cs2 F1B 2.82(3) . ?
Cs2 F3 2.908(4) . ?
Cs2 F4 3.275(4) 5_656 ?
Cs2 F4 3.275(4) 2_656 ?
Cs2 F5 3.022(3) 2_656 ?
Cs2 F5 3.022(3) 5_656 ?
Cs2 F5 3.395(3) 6_455 ?
Cs2 F5 3.395(3) 1_455 ?
Cs2 F7 3.429(3) 2_656 ?
Cs2 F7 3.429(3) 5_656 ?
Cs3 F1A 3.019(13) 8_656 ?
Cs3 F1A 3.019(14) 3_656 ?
Cs3 F1B 3.49(2) 3_656 ?
Cs3 F2A 3.498(16) 8_656 ?
Cs3 F2B 3.034(13) 8_656 ?
Cs3 F2B 3.034(13) 3_656 ?
Cs3 F2C 2.995(13) 7_656 ?
Cs3 F2C 2.995(13) 4_656 ?
Cs3 F5 2.920(3) 3_556 ?
Cs3 F5 2.920(3) 8_556 ?
Cs3 F10 2.870(3) . ?
Cs3 F10 2.870(3) 6_565 ?
Cs4 F1A 3.088(19) 2_656 ?
Cs4 F1A 3.71(2) 5_656 ?
Cs4 F1B 3.152(13) 5_656 ?
Cs4 F2A 3.162(15) 1_656 ?
Cs4 F2A 3.231(16) 2_656 ?
Cs4 F2B 2.988(13) 1_656 ?
Cs4 F2C 3.044(12) 2_656 ?
Cs4 F4 2.814(3) . ?
Cs4 F6 3.287(2) 8_455 ?
Cs4 F7 2.846(3) . ?
Cs4 F8 2.873(3) . ?
Cs4 F9 2.887(3) 8_455 ?
Cs5 F2B 3.571(14) 7_556 ?
Cs5 F2C 2.790(13) 3_556 ?
Cs5 F2C 2.790(13) 8_556 ?
Cs5 F3 2.936(4) 7_657 ?
Cs5 F4 3.314(4) 4_657 ?
Cs5 F4 3.314(4) 7_657 ?
Cs5 F9 3.285(3) 5_767 ?
Cs5 F9 3.285(3) 2_757 ?
Cs5 F10 3.027(3) . ?
Cs5 F10 3.027(3) 6_565 ?
Cs5 F10 3.347(4) 5_767 ?
Cs5 F10 3.347(4) 2_757 ?
Cs6 F3 3.3351(6) 3 ?
Cs6 F4 3.359(4) 8 ?
Cs6 F4 3.287(4) 7_656 ?
Cs6 F5 3.305(3) 7_656 ?
Cs6 F6 3.358(3) 8_455 ?
Cs6 F6 3.196(3) 2_756 ?
Cs6 F6 3.224(3) . ?
Cs6 F7 3.262(3) 7_656 ?
Cs6 F7 3.179(3) . ?
Cs6 F8 3.369(4) . ?
Cs6 F9 3.373(4) . ?
Cs6 F10 3.402(4) 2_757 ?
Ga1 F8 1.886(3) . ?
Ga1 F8 1.886(3) 2_757 ?
Ga1 F9 1.887(3) . ?
Ga1 F9 1.886(3) 2_757 ?
Ga1 F10 1.890(3) . ?
Ga1 F10 1.890(3) 2_757 ?
Ga2 F1A 1.875(18) . ?
Ga2 F1A 1.875(18) 6 ?
Ga2 F1A 1.875(18) 5 ?
Ga2 F1A 1.875(18) 2 ?
Ga2 F1B 1.87(3) 5 ?
Ga2 F1B 1.87(3) . ?
Ga2 F2A 1.852(12) . ?
Ga2 F2A 1.852(12) 6 ?
Ga2 F2A 1.852(12) 5 ?
Ga2 F2A 1.852(12) 2 ?
Ga2 F2C 1.885(14) . ?
Ga2 F2C 1.885(14) 5 ?
Ga3 F3 1.919(4) 5_656 ?
Ga3 F3 1.919(4) . ?
Ga3 F4 1.875(3) 2_656 ?
Ga3 F4 1.875(3) 5_656 ?
Ga3 F4 1.875(3) 6 ?
Ga3 F4 1.875(3) . ?
Ga4 F5 1.906(3) . ?
Ga4 F5 1.906(3) 2_756 ?
Ga4 F6 1.897(3) . ?
Ga4 F6 1.897(3) 2_756 ?
Ga4 F7 1.881(3) 2_756 ?
Ga4 F7 1.881(3) . ?
F1A F1A 0.74(5) 6 ?
F1A F1B 0.62(2) . ?
F2A F2A 1.62(3) 2 ?
F2A F2B 0.805(17) . ?
F2A F2C 1.70(2) 2 ?
F2B F2C 0.970(16) 2 ?
F2C F2C 1.15(3) 6 ?
loop_
_twin_individual_id
_twin_individual_mass_fraction_refined
1 0.9297(14)
2 0.0703(14)
