#------------------------------------------------------------------------------
#$Date: 2023-09-13 01:56:30 +0300 (Wed, 13 Sep 2023) $
#$Revision: 286309 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/71/39/7713930.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7713930
loop_
_publ_author_name
'Armenis, Alexandros'
'Alexandropoulos, Dimitris'
'Worrell, Anne'
'Cunha-Silva, Luis'
'Dunbar, Kim R.'
'Stamatatos, Theocharis'
_publ_section_title
;
 Peripheral site modification in a family of dinuclear
 [Dy2(hynad)2-6(NO3)0-6(sol)0-2]0/2- single-molecule magnets bearing a
 {Dy2(μ-OR)2}4+ diamond-shaped core and exhibiting dissimilar magnetic
 dynamics
;
_journal_name_full               'Dalton Transactions'
_journal_paper_doi               10.1039/D3DT02596A
_journal_year                    2023
_chemical_formula_moiety         'C30 H26 Dy2 N8 O20'
_chemical_formula_sum            'C30 H26 Dy2 N8 O20'
_chemical_formula_weight         1143.59
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_audit_creation_date             2018-06-07
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_audit_update_record
;
2023-06-30 deposited with the CCDC.	2023-09-12 downloaded from the CCDC.
;
_cell_angle_alpha                91.834(2)
_cell_angle_beta                 112.263(2)
_cell_angle_gamma                112.030(3)
_cell_formula_units_Z            1
_cell_length_a                   9.7495(3)
_cell_length_b                   10.3059(3)
_cell_length_c                   10.8266(2)
_cell_measurement_reflns_used    6878
_cell_measurement_temperature    293.0(1)
_cell_measurement_theta_max      76.6690
_cell_measurement_theta_min      4.5000
_cell_volume                     913.81(5)
_computing_cell_refinement       'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)'
_computing_data_collection       'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)'
_computing_data_reduction        'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      293.0(1)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 28.5714
_diffrn_detector_type            HyPix
_diffrn_measured_fraction_theta_full 0.975
_diffrn_measured_fraction_theta_max 0.986
_diffrn_measurement_details
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω    -61.00 -24.00   0.50    0.05    --  -48.45  11.00 -93.00   74
  2  ω   -116.00 -50.00   0.50    0.05    --  -48.45 -11.00  93.00  132
  3  ω     65.00 119.00   0.50    0.05    --   48.45  11.00 -93.00  108
  4  ω   -102.00 -74.00   0.50    0.20    --  -86.25  11.00 -93.00   56
  5  ω   -158.00 -99.00   0.50    0.20    --  -86.25 -11.00  93.00  118
  6  ω    -67.00 -41.00   0.50    0.20    --  -86.25  11.00 -93.00   52
  7  ω    151.00 177.00   0.50    0.20    --  107.75  11.00 -93.00   52
  8  ω    114.00 146.00   0.50    0.20    --  107.75  11.00 -93.00   64
  9  ω     -8.00  20.00   0.50    0.05    --  -48.45  11.00 -93.00   56
 10  ω    -63.00  19.00   0.50    0.05    --  -48.45  57.00 -90.00  164
 11  ω     -5.00  20.00   0.50    0.05    --   48.45 -11.00  93.00   50
 12  ω   -105.00 -17.00   0.50    0.20    --  -86.25  77.00 120.00  176
 13  ω    -99.00 -16.00   0.50    0.20    --  -86.25  37.00 -90.00  166
 14  ω     36.00 120.00   0.50    0.20    --  107.75 -37.00 -90.00  168
 15  ω     95.00 176.00   0.50    0.20    --  107.75  19.00 120.00  162
 16  ω     95.00 124.00   0.50    0.20    --  107.75 -11.00  93.00   58
 17  ω     92.00 117.00   0.50    0.20    --  107.75-125.00 120.00   50
 18  ω     44.00  85.00   0.50    0.20    --  107.75-125.00 120.00   82
 19  ω     50.00  87.00   0.50    0.20    --  107.75 -99.00-150.00   74
 20  ω     37.00 108.00   0.50    0.20    --  107.75 -77.00 -90.00  142
 21  ω     51.00 108.00   0.50    0.20    --  107.75 -99.00 150.00  114
 22  ω     41.00 119.00   0.50    0.20    --  107.75 -57.00 -60.00  156
 23  ω     37.00 108.00   0.50    0.20    --  107.75 -99.00 -90.00  142
 24  ω     49.00  92.00   0.50    0.20    --  107.75 -11.00  93.00   86
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'XtaLAB Synergy, Dualflex, HyPix'
_diffrn_measurement_method       'ω scans'
_diffrn_measurement_specimen_support 'Mitegen 50um'
_diffrn_orient_matrix_type
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      -0.1676846000
_diffrn_orient_matrix_UB_12      -0.1157469000
_diffrn_orient_matrix_UB_13      -0.0223152000
_diffrn_orient_matrix_UB_21      -0.0639685000
_diffrn_orient_matrix_UB_22      0.1158742000
_diffrn_orient_matrix_UB_23      -0.0000976000
_diffrn_orient_matrix_UB_31      -0.0560124000
_diffrn_orient_matrix_UB_32      -0.0172191000
_diffrn_orient_matrix_UB_33      -0.1554298000
_diffrn_radiation_collimation    0.3
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0344
_diffrn_reflns_av_unetI/netI     0.0372
_diffrn_reflns_Laue_measured_fraction_full 0.975
_diffrn_reflns_Laue_measured_fraction_max 0.986
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       8
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            8071
_diffrn_reflns_point_group_measured_fraction_full 0.975
_diffrn_reflns_point_group_measured_fraction_max 0.986
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         67.063
_diffrn_reflns_theta_min         4.507
_diffrn_source                   'micro-focus sealed X-ray tube'
_diffrn_source_current           24.0
_diffrn_source_power             1.2
_diffrn_source_target            Mo
_diffrn_source_type              'PhotonJet (Cu) X-ray Source'
_diffrn_source_voltage           50.0
_exptl_absorpt_coefficient_mu    22.497
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.41328
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            'clear light yellow'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    2.078
_exptl_crystal_description       block
_exptl_crystal_F_000             554
_exptl_crystal_size_max          0.05
_exptl_crystal_size_mid          0.02
_exptl_crystal_size_min          0.01
_refine_diff_density_max         0.759
_refine_diff_density_min         -0.388
_refine_diff_density_rms         0.100
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.032
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     273
_refine_ls_number_reflns         3221
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.032
_refine_ls_R_factor_all          0.0288
_refine_ls_R_factor_gt           0.0241
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0309P)²+0.4383P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0570
_refine_ls_wR_factor_ref         0.0596
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3037
_reflns_number_total             3221
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d3dt02596a2.cif
_cod_data_source_block           180607a
_cod_database_code               7713930
_shelxl_version_number           2013-4
_chemical_oxdiff_formula         DyNOC
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.806
_shelx_estimated_absorpt_t_min   0.399
_reflns_odcompleteness_completeness 99.11
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     66.97
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C3(H3), C4(H4), C5(H5), C8(H8), C9(H9), C10(H10), C13(H13)
2.b Idealised Me refined as rotating group:
 C14(H14A,H14B,H14C), C15(H15A,H15B,H15C)
;
_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 1.798
_oxdiff_exptl_absorpt_empirical_full_min 0.719
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.7091(4) 0.3097(3) 0.1890(3) 0.0290(6) Uani 1 1 d . . . . .
C2 C 0.5600(4) 0.2642(3) 0.0643(3) 0.0311(6) Uani 1 1 d . . . . .
C3 C 0.5278(4) 0.1655(4) -0.0433(4) 0.0387(7) Uani 1 1 d . . . . .
H3 H 0.6025 0.1274 -0.0365 0.046 Uiso 1 1 calc R . . . .
C4 C 0.3841(5) 0.1222(4) -0.1625(4) 0.0448(8) Uani 1 1 d . . . . .
H4 H 0.3638 0.0557 -0.2346 0.054 Uiso 1 1 calc R . . . .
C5 C 0.2727(4) 0.1772(4) -0.1735(4) 0.0418(8) Uani 1 1 d . . . . .
H5 H 0.1765 0.1462 -0.2527 0.050 Uiso 1 1 calc R . . . .
C6 C 0.3018(4) 0.2796(4) -0.0672(3) 0.0337(7) Uani 1 1 d . . . . .
C7 C 0.4485(4) 0.3253(3) 0.0539(3) 0.0292(6) Uani 1 1 d . . . . .
C8 C 0.1922(4) 0.3421(4) -0.0767(3) 0.0353(7) Uani 1 1 d . . . . .
H8 H 0.0955 0.3132 -0.1551 0.042 Uiso 1 1 calc R . . . .
C9 C 0.2265(4) 0.4454(4) 0.0284(4) 0.0367(7) Uani 1 1 d . . . . .
H9 H 0.1526 0.4846 0.0205 0.044 Uiso 1 1 calc R . . . .
C10 C 0.3723(4) 0.4914(4) 0.1468(3) 0.0340(7) Uani 1 1 d . . . . .
H10 H 0.3954 0.5618 0.2168 0.041 Uiso 1 1 calc R . . . .
C11 C 0.4819(4) 0.4320(3) 0.1598(3) 0.0297(6) Uani 1 1 d . . . . .
C12 C 0.6345(4) 0.4813(3) 0.2821(3) 0.0292(6) Uani 1 1 d . . . . .
C13 C 0.6909(4) 0.7605(4) 0.6374(3) 0.0344(7) Uani 1 1 d . . . . .
H13 H 0.6037 0.7129 0.5533 0.041 Uiso 1 1 calc R . . . .
C14 C 0.5530(5) 0.9072(4) 0.6551(4) 0.0440(8) Uani 1 1 d . . . . .
H14A H 0.5937 1.0029 0.6401 0.066 Uiso 1 1 calc GR . . . .
H14B H 0.5069 0.9041 0.7197 0.066 Uiso 1 1 calc GR . . . .
H14C H 0.4705 0.8437 0.5705 0.066 Uiso 1 1 calc GR . . . .
C15 C 0.8240(5) 0.9505(5) 0.8350(4) 0.0516(9) Uani 1 1 d . . . . .
H15A H 0.8710 1.0468 0.8233 0.077 Uiso 1 1 calc GR . . . .
H15B H 0.9047 0.9125 0.8598 0.077 Uiso 1 1 calc GR . . . .
H15C H 0.7872 0.9499 0.9057 0.077 Uiso 1 1 calc GR . . . .
Dy1 Dy 0.92896(2) 0.62597(2) 0.58267(2) 0.02827(8) Uani 1 1 d . . . . .
N1 N 0.6863(3) 0.8630(3) 0.7080(3) 0.0343(6) Uani 1 1 d . . . . .
N2 N 0.7951(4) 0.3849(3) 0.6976(3) 0.0369(6) Uani 1 1 d . . . . .
N3 N 1.1035(4) 0.8763(3) 0.5023(3) 0.0385(6) Uani 1 1 d . . . . .
N4 N 0.7339(3) 0.4134(3) 0.2881(3) 0.0289(5) Uani 1 1 d . . . . .
O1 O 0.8064(3) 0.7229(3) 0.6770(2) 0.0370(5) Uani 1 1 d . . . . .
O2 O 1.0474(3) 0.8828(3) 0.5894(3) 0.0469(6) Uani 1 1 d . . . . .
O3 O 1.2024(4) 0.9816(3) 0.4874(3) 0.0619(8) Uani 1 1 d . . . . .
O4 O 1.0515(4) 0.7534(3) 0.4345(3) 0.0519(7) Uani 1 1 d . . . . .
O5 O 0.7088(3) 0.4044(3) 0.5845(2) 0.0418(5) Uani 1 1 d . . . . .
O6 O 0.9375(3) 0.4839(3) 0.7611(2) 0.0390(5) Uani 1 1 d . . . . .
O7 O 0.7447(4) 0.2800(3) 0.7436(3) 0.0517(7) Uani 1 1 d . . . . .
O8 O 0.8730(3) 0.4549(2) 0.4033(2) 0.0332(5) Uani 1 1 d . . . . .
O9 O 0.6802(3) 0.5769(3) 0.3808(2) 0.0354(5) Uani 1 1 d . . . . .
O10 O 0.8121(3) 0.2603(3) 0.2127(2) 0.0358(5) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -9.8046 9.8477 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N4 C1 C2 116.8(3) . . ?
O10 C1 C2 124.9(3) . . ?
O10 C1 N4 118.3(3) . . ?
C3 C2 C1 121.1(3) . . ?
C3 C2 C7 120.2(3) . . ?
C7 C2 C1 118.8(3) . . ?
C2 C3 C4 120.6(3) . . ?
C5 C4 C3 120.3(3) . . ?
C4 C5 C6 121.0(3) . . ?
C5 C6 C7 119.1(3) . . ?
C5 C6 C8 122.5(3) . . ?
C7 C6 C8 118.3(3) . . ?
C6 C7 C2 118.8(3) . . ?
C11 C7 C2 121.5(3) . . ?
C11 C7 C6 119.6(3) . . ?
C9 C8 C6 121.1(3) . . ?
C8 C9 C10 120.3(3) . . ?
C11 C10 C9 120.1(3) . . ?
C7 C11 C12 119.4(3) . . ?
C10 C11 C7 120.5(3) . . ?
C10 C11 C12 120.1(3) . . ?
N4 C12 C11 116.1(3) . . ?
O9 C12 C11 125.7(3) . . ?
O9 C12 N4 118.2(3) . . ?
O1 C13 N1 123.6(3) . . ?
N3 Dy1 N2 171.99(8) . . ?
O1 Dy1 N2 82.78(8) . . ?
O1 Dy1 N3 98.16(9) . . ?
O1 Dy1 O2 73.47(9) . . ?
O1 Dy1 O4 119.55(9) . . ?
O1 Dy1 O5 79.89(9) . . ?
O1 Dy1 O6 84.38(8) . . ?
O1 Dy1 O8 142.49(8) . . ?
O1 Dy1 O8 152.74(8) . 2_766 ?
O1 Dy1 O9 80.90(8) . . ?
O1 Dy1 O10 90.88(8) . 2_766 ?
O2 Dy1 N2 151.42(8) . . ?
O2 Dy1 N3 25.95(9) . . ?
O2 Dy1 O4 51.30(9) . . ?
O2 Dy1 O5 151.62(9) . . ?
O2 Dy1 O6 133.01(8) . . ?
O2 Dy1 O10 71.19(9) . 2_766 ?
O4 Dy1 N2 156.64(8) . . ?
O4 Dy1 N3 25.77(9) . . ?
O4 Dy1 O5 143.44(9) . . ?
O5 Dy1 N2 25.79(8) . . ?
O5 Dy1 N3 162.22(8) . . ?
O6 Dy1 N2 25.72(8) . . ?
O6 Dy1 N3 146.30(8) . . ?
O6 Dy1 O4 150.34(9) . . ?
O6 Dy1 O5 51.42(8) . . ?
O6 Dy1 O10 68.23(8) . 2_766 ?
O8 Dy1 N2 85.63(8) . . ?
O8 Dy1 N2 87.12(8) 2_766 . ?
O8 Dy1 N3 98.15(9) . . ?
O8 Dy1 N3 88.55(9) 2_766 . ?
O8 Dy1 O2 106.85(9) 2_766 . ?
O8 Dy1 O2 122.94(8) . . ?
O8 Dy1 O4 75.50(9) 2_766 . ?
O8 Dy1 O4 72.40(9) . . ?
O8 Dy1 O5 101.29(8) 2_766 . ?
O8 Dy1 O5 74.43(8) . . ?
O8 Dy1 O6 99.87(8) . . ?
O8 Dy1 O6 75.83(8) 2_766 . ?
O8 Dy1 O8 60.99(8) . 2_766 ?
O8 Dy1 O9 65.36(7) . . ?
O8 Dy1 O9 125.63(7) 2_766 . ?
O8 Dy1 O10 125.51(7) . 2_766 ?
O8 Dy1 O10 64.56(7) 2_766 2_766 ?
O9 Dy1 N2 97.30(8) . . ?
O9 Dy1 N3 90.70(8) . . ?
O9 Dy1 O2 94.46(9) . . ?
O9 Dy1 O4 80.95(9) . . ?
O9 Dy1 O5 71.52(8) . . ?
O9 Dy1 O6 122.71(8) . . ?
O9 Dy1 O10 165.10(8) . 2_766 ?
O10 Dy1 N2 93.94(8) 2_766 . ?
O10 Dy1 N3 78.11(8) 2_766 . ?
O10 Dy1 O4 92.54(10) 2_766 . ?
O10 Dy1 O5 119.45(8) 2_766 . ?
C13 N1 C14 121.6(3) . . ?
C13 N1 C15 121.4(3) . . ?
C14 N1 C15 116.5(3) . . ?
O5 N2 Dy1 58.50(16) . . ?
O5 N2 O6 115.4(3) . . ?
O6 N2 Dy1 57.13(16) . . ?
O7 N2 Dy1 175.8(2) . . ?
O7 N2 O5 122.6(3) . . ?
O7 N2 O6 122.0(3) . . ?
O2 N3 Dy1 57.59(16) . . ?
O3 N3 Dy1 168.0(2) . . ?
O3 N3 O2 122.1(3) . . ?
O3 N3 O4 122.7(3) . . ?
O4 N3 Dy1 58.98(17) . . ?
O4 N3 O2 115.2(3) . . ?
C1 N4 C12 127.3(3) . . ?
O8 N4 C1 116.2(2) . . ?
O8 N4 C12 116.5(2) . . ?
C13 O1 Dy1 138.1(2) . . ?
N3 O2 Dy1 96.5(2) . . ?
N3 O4 Dy1 95.26(19) . . ?
N2 O5 Dy1 95.71(18) . . ?
N2 O6 Dy1 97.15(18) . . ?
Dy1 O8 Dy1 119.01(8) . 2_766 ?
N4 O8 Dy1 120.61(17) . 2_766 ?
N4 O8 Dy1 120.11(17) . . ?
C12 O9 Dy1 119.6(2) . . ?
C1 O10 Dy1 119.3(2) . 2_766 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C2 1.455(4) . ?
C1 N4 1.374(4) . ?
C1 O10 1.238(4) . ?
C2 C3 1.377(5) . ?
C2 C7 1.421(5) . ?
C3 C4 1.397(5) . ?
C4 C5 1.372(6) . ?
C5 C6 1.404(5) . ?
C6 C7 1.421(4) . ?
C6 C8 1.416(5) . ?
C7 C11 1.413(5) . ?
C8 C9 1.381(5) . ?
C9 C10 1.401(5) . ?
C10 C11 1.386(5) . ?
C11 C12 1.457(4) . ?
C12 N4 1.377(4) . ?
C12 O9 1.247(4) . ?
C13 N1 1.308(4) . ?
C13 O1 1.254(4) . ?
C14 N1 1.457(5) . ?
C15 N1 1.456(5) . ?
Dy1 N2 2.901(3) . ?
Dy1 N3 2.878(3) . ?
Dy1 O1 2.286(2) . ?
Dy1 O2 2.445(3) . ?
Dy1 O4 2.476(3) . ?
Dy1 O5 2.486(3) . ?
Dy1 O6 2.456(2) . ?
Dy1 O8 2.332(2) 2_766 ?
Dy1 O8 2.331(2) . ?
Dy1 O9 2.430(2) . ?
Dy1 O10 2.456(2) 2_766 ?
N2 O5 1.269(4) . ?
N2 O6 1.269(4) . ?
N2 O7 1.216(4) . ?
N3 O2 1.267(4) . ?
N3 O3 1.216(4) . ?
N3 O4 1.256(4) . ?
N4 O8 1.352(3) . ?
O8 Dy1 2.332(2) 2_766 ?
O10 Dy1 2.456(2) 2_766 ?
