#------------------------------------------------------------------------------
#$Date: 2024-02-04 13:44:02 +0200 (Sun, 04 Feb 2024) $
#$Revision: 289462 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/71/44/7714465.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7714465
loop_
_publ_author_name
'Tschernuth, Florian S.'
'Kostenko, Arseni'
'Stigler, Sebastian'
'Gradenegger, Anna'
'Inoue, Shigeyoshi'
_publ_section_title
;
 A neutral germanium-centred hard and soft lewis superacid and its unique
 reactivity towards hydrosilanes.
;
_journal_issue                   1
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              74
_journal_page_last               81
_journal_paper_doi               10.1039/d3dt03626j
_journal_volume                  53
_journal_year                    2023
_chemical_compound_source        'see text'
_chemical_formula_moiety
'C24 H22.774 F24.997 Ge K O10, C24 H24 F25 Ge K O10'
_chemical_formula_sum            'C48 H46.78 F49.99 Ge2 K2 O20'
_chemical_formula_weight         2116.91
_chemical_name_systematic
;
[K(18-c-6)][F-1]
;
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   difmap
_audit_update_record
;
2023-08-30 deposited with the CCDC.	2023-11-15 downloaded from the CCDC.
;
_cell_angle_alpha                107.062(3)
_cell_angle_beta                 102.834(3)
_cell_angle_gamma                95.235(3)
_cell_formula_units_Z            2
_cell_length_a                   11.2001(10)
_cell_length_b                   15.7831(14)
_cell_length_c                   22.3057(19)
_cell_measurement_reflns_used    9510
_cell_measurement_temperature    100
_cell_measurement_theta_max      25.72
_cell_measurement_theta_min      2.33
_cell_volume                     3623.2(6)
_computing_cell_refinement       'SAINT (Bruker, 2017)'
_computing_data_collection       'APEX III Control Software (Bruker, 2016)'
_computing_data_reduction        'SAINT (Bruker, 2017)'
_computing_molecular_graphics    'PLATON (Spek, 2011), MERCURY (Wood, 2020)'
_computing_publication_material  'PLATON (Spek, 2011)'
_computing_structure_refinement
'OLEX2 (Puschmann, 2015),SHELXL (Sheldrick, 2017), SHELXLE (Huebschle, 2011)'
_computing_structure_solution    'SHELXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      100
_diffrn_detector_area_resol_mean 16
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker Photon CMOS'
_diffrn_measurement_method       'phi- and omega-rotation'
_diffrn_radiation_monochromator  'Helios optic'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'IMS microsource'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0472
_diffrn_reflns_av_unetI/netI     0.0238
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            133009
_diffrn_reflns_reduction_process
;
;
_diffrn_reflns_theta_full        25.24
_diffrn_reflns_theta_max         25.35
_diffrn_reflns_theta_min         1.98
_exptl_absorpt_coefficient_mu    1.141
_exptl_absorpt_correction_T_max  0.745
_exptl_absorpt_correction_T_min  0.635
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS 2016/2, Bruker, 2016'
_exptl_crystal_colour            'clear colourless'
_exptl_crystal_density_diffrn    1.940
_exptl_crystal_density_method    'Not Measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2093
_exptl_crystal_size_max          0.580
_exptl_crystal_size_mid          0.318
_exptl_crystal_size_min          0.279
_refine_diff_density_max         0.548
_refine_diff_density_min         -0.484
_refine_diff_density_rms         0.067
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.087
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1277
_refine_ls_number_reflns         13270
_refine_ls_number_restraints     56
_refine_ls_restrained_S_all      1.087
_refine_ls_R_factor_all          0.0451
_refine_ls_R_factor_gt           0.0348
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'W=1/[Σ²(FO²)+(0.0165P)²+7.4261P] WHERE P=(FO²+2FC²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0717
_refine_ls_wR_factor_ref         0.0765
_reflns_number_gt                11373
_reflns_number_total             13270
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            d3dt03626j2.cif
_cod_data_source_block           mo_tscfl29_0m
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value ' multi-scan' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 

 Adding full bibliography for 7714462--7714466.cif.
;
_cod_database_code               7714465
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x,-y,-z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_thermal_displace_type
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ge1 Ge Uani 0.70928(3) 0.74577(2) 0.87867(2) 1.000 0.0154(1) d . . .
Ge2 Ge Uani 0.14247(2) 0.76294(2) 0.37613(2) 1.000 0.0147(1) d . . .
K1 K Uani 1.09944(5) 0.73902(4) 0.87868(3) 1.000 0.0195(2) d . . .
K2 K Uani 0.53297(5) 0.76394(4) 0.37336(3) 1.000 0.0199(2) d D . .
F1 F Uani 0.86535(15) 0.74279(13) 0.90561(8) 1.000 0.0298(6) d . . .
F2 F Uani 0.41876(16) 0.69921(13) 0.85858(8) 1.000 0.0313(6) d . . .
F3 F Uani 0.40800(18) 0.82363(14) 0.92622(10) 1.000 0.0414(7) d . . .
F4 F Uani 0.34294(16) 0.70025(15) 0.93987(10) 1.000 0.0415(7) d . . .
F5 F Uani 0.5216(2) 0.86491(13) 1.04322(10) 1.000 0.0445(7) d . . .
F6 F Uani 0.68660(19) 0.81406(13) 1.07210(8) 1.000 0.0383(6) d . . .
F7 F Uani 0.50851(19) 0.73660(13) 1.05822(9) 1.000 0.0393(7) d . . .
F8 F Uani 0.42198(18) 0.54926(13) 0.87269(9) 1.000 0.0390(6) d . . .
F9 F Uani 0.45087(17) 0.57121(12) 0.97501(8) 1.000 0.0301(6) d . . .
F10 F Uani 0.5584(2) 0.48858(12) 0.92086(10) 1.000 0.0426(7) d . . .
F11 F Uani 0.69269(17) 0.63116(14) 1.04823(9) 1.000 0.0362(6) d . . .
F12 F Uani 0.7760(2) 0.56950(15) 0.97188(11) 1.000 0.0474(8) d . . .
F13 F Uani 0.81207(15) 0.71159(14) 1.01416(9) 1.000 0.0366(6) d . . .
F14 F Uani 0.57725(16) 0.76733(13) 0.65440(8) 1.000 0.0348(6) d . . .
F15 F Uani 0.58304(17) 0.63130(13) 0.65290(8) 1.000 0.0358(6) d . . .
F16 F Uani 0.45996(15) 0.70498(13) 0.69951(8) 1.000 0.0321(6) d . . .
F17 F Uani 0.82268(17) 0.75271(15) 0.69010(9) 1.000 0.0398(7) d . . .
F18 F Uani 0.80003(18) 0.63614(13) 0.71978(10) 1.000 0.0400(7) d . . .
F19 F Uani 0.89790(15) 0.76030(12) 0.78916(8) 1.000 0.0259(5) d . . .
F20 F Uani 0.49947(17) 0.88986(14) 0.74352(10) 1.000 0.0378(7) d . . .
F21 F Uani 0.56679(19) 0.95561(12) 0.84676(10) 1.000 0.0398(7) d . . .
F22 F Uani 0.48225(15) 0.81817(12) 0.81064(9) 1.000 0.0286(5) d . . .
F23 F Uani 0.74860(18) 1.00404(12) 0.81176(11) 1.000 0.0406(7) d . . .
F24 F Uani 0.8874(8) 0.9171(13) 0.7959(9) 0.56(8) 0.028(3) d DP A 1
F24A F Uani 0.8861(12) 0.931(2) 0.815(2) 0.44(8) 0.041(5) d DP A 2
F25 F Uani 0.7308(7) 0.9142(3) 0.71964(13) 0.80(2) 0.0318(12) d DP A 1
F25A F Uani 0.792(3) 0.8940(12) 0.7262(6) 0.20(2) 0.031(5) d DP A 2
O1 O Uani 0.64382(17) 0.80052(13) 0.94440(9) 1.000 0.0196(6) d . . .
O2 O Uani 0.64833(19) 0.63878(13) 0.88717(9) 1.000 0.0217(6) d . . .
O3 O Uani 0.65068(17) 0.69339(12) 0.79164(9) 1.000 0.0180(6) d . . .
O4 O Uani 0.73914(18) 0.85282(13) 0.86236(9) 1.000 0.0201(6) d . . .
O9 O Uani 1.16382(19) 0.92043(14) 0.89854(10) 1.000 0.0274(7) d . . .
O10 O Uani 1.1693(2) 0.85765(14) 1.00632(10) 1.000 0.0291(7) d . . .
O11 O Uani 1.08588(19) 0.67441(14) 0.98062(10) 1.000 0.0264(7) d . . .
O12 O Uani 1.0813(2) 0.55465(14) 0.86085(10) 1.000 0.0280(7) d . . .
O13 O Uani 1.09986(18) 0.61779(14) 0.75702(10) 1.000 0.0249(6) d . . .
O14 O Uani 1.19561(18) 0.79811(14) 0.78732(10) 1.000 0.0241(6) d . . .
F26 F Uani 0.28152(16) 0.54162(12) 0.36758(9) 1.000 0.0292(6) d . . .
F27 F Uani 0.09113(16) 0.47256(11) 0.38726(9) 1.000 0.0285(6) d . . .
F28 F Uani -0.03553(14) 0.55415(11) 0.42328(8) 1.000 0.0229(5) d . . .
F29 F Uani 0.12056(15) 0.53245(12) 0.49019(8) 1.000 0.0267(5) d . . .
F30 F Uani -0.18404(15) 0.82575(12) 0.39754(8) 1.000 0.0287(6) d . . .
F31 F Uani 0.14838(17) 0.80262(13) 0.21017(8) 1.000 0.0326(6) d . . .
F32 F Uani -0.26826(15) 0.78676(12) 0.29525(9) 1.000 0.0310(6) d . . .
F33 F Uani 0.27506(17) 0.81301(13) 0.60014(8) 1.000 0.0340(6) d . . .
F34 F Uani 0.02886(16) 0.99720(11) 0.34374(9) 1.000 0.0310(6) d . . .
F35 F Uani 0.27541(17) 0.67118(13) 0.57600(8) 0.997(7) 0.0330(7) d . . .
F36 F Uani -0.14728(14) 0.70569(11) 0.33474(8) 1.000 0.0236(5) d . . .
F37 F Uani -0.11188(18) 0.97650(12) 0.39028(9) 1.000 0.0366(6) d . . .
F38 F Uani -0.15845(16) 0.94290(12) 0.28659(9) 1.000 0.0348(6) d . . .
F39 F Uani -0.18529(16) 0.79157(13) 0.19032(9) 1.000 0.0341(6) d . . .
F40 F Uani 0.39368(15) 0.75361(13) 0.54338(8) 1.000 0.0331(6) d . . .
F41 F Uani 0.37188(14) 0.67460(11) 0.42551(8) 1.000 0.0245(5) d . . .
F42 F Uani 0.28733(14) 0.79622(11) 0.36763(8) 1.000 0.0242(5) d . . .
F43 F Uani 0.34901(15) 0.57270(12) 0.47111(9) 1.000 0.0304(6) d . . .
F44 F Uani -0.04172(14) 0.72080(11) 0.45802(8) 1.000 0.0244(5) d . . .
F45 F Uani 0.02519(16) 0.68245(13) 0.54347(8) 1.000 0.0311(6) d . . .
F46 F Uani 0.05733(17) 0.82064(12) 0.54708(9) 1.000 0.0345(6) d . . .
F47 F Uani -0.17309(16) 0.66881(12) 0.21314(8) 1.000 0.0316(6) d . . .
F48 F Uani -0.05927(18) 0.70564(13) 0.15672(8) 1.000 0.0362(6) d . . .
F49 F Uani 0.03205(16) 0.90460(13) 0.22070(9) 1.000 0.0326(6) d . . .
F50 F Uani 0.17874(15) 0.90382(11) 0.30203(8) 1.000 0.0268(5) d . . .
C1 C Uani 0.5657(2) 0.74416(18) 0.96228(13) 1.000 0.0178(8) d . . .
C2 C Uani 0.6101(3) 0.64697(19) 0.94278(13) 1.000 0.0196(8) d . . .
C3 C Uani 0.6762(2) 0.74607(19) 0.75442(13) 1.000 0.0183(8) d . . .
C4 C Uani 0.6870(3) 0.84966(19) 0.79956(14) 1.000 0.0195(8) d . . .
O5 O Uani 0.20133(17) 0.79279(12) 0.46534(9) 1.000 0.0187(6) d . . .
C5 C Uani 0.4319(3) 0.7419(2) 0.92167(16) 1.000 0.0289(10) d . . .
C6 C Uani 0.5716(3) 0.7899(2) 1.03508(15) 1.000 0.0294(10) d . . .
O6 O Uani 0.11189(16) 0.64718(12) 0.37414(9) 1.000 0.0163(5) d . . .
C7 C Uani 0.5082(3) 0.5636(2) 0.92784(15) 1.000 0.0283(10) d . . .
O7 O Uani 0.06265(17) 0.72698(12) 0.28829(9) 1.000 0.0181(6) d . . .
O8 O Uani 0.04837(17) 0.85121(12) 0.38674(9) 1.000 0.0177(5) d . . .
C8 C Uani 0.7236(3) 0.6401(2) 0.99547(16) 1.000 0.0296(10) d . . .
C9 C Uani 0.5722(3) 0.7128(2) 0.68959(14) 1.000 0.0260(9) d . . .
C10 C Uani 0.8006(3) 0.7234(2) 0.73783(14) 1.000 0.0239(9) d . . .
C11 C Uani 0.5569(3) 0.8786(2) 0.79954(16) 1.000 0.0281(10) d . . .
C12 C Uani 0.7674(3) 0.9215(2) 0.78339(15) 1.000 0.0264(9) d D . .
C13 C Uani 1.2059(3) 0.9775(2) 0.96449(16) 1.000 0.0370(11) d . . .
C14 C Uani 1.1355(3) 0.9418(2) 1.00413(16) 1.000 0.0362(11) d . . .
O15 O Uani 0.6903(3) 0.7098(3) 0.46683(17) 0.774(4) 0.0255(10) d DP B 1
C15 C Uani 1.1131(4) 0.8244(2) 1.04810(16) 1.000 0.0367(10) d . . .
O15A O Uani 0.6946(9) 0.7650(8) 0.4934(6) 0.226(4) 0.027(4) d DP B 2
O16 O Uani 0.5562(3) 0.5800(2) 0.35042(18) 0.774(4) 0.0288(10) d DP B 1
C16 C Uani 1.1442(3) 0.7336(2) 1.04439(15) 1.000 0.0340(11) d . . .
O16A O Uani 0.5941(9) 0.5991(6) 0.3969(5) 0.226(4) 0.022(3) d DP B 2
O17 O Uani 0.4593(3) 0.6410(2) 0.24594(16) 0.774(4) 0.0299(10) d DP B 1
C17 C Uani 1.1024(3) 0.5848(2) 0.97310(17) 1.000 0.0343(11) d . . .
O17A O Uani 0.5029(10) 0.6022(6) 0.2710(4) 0.226(4) 0.028(3) d DP B 2
C18 C Uani 1.0291(4) 0.5281(2) 0.90632(17) 1.000 0.0381(11) d . . .
O18 O Uani 0.4452(3) 0.8217(2) 0.26735(15) 0.774(4) 0.0293(10) d DP B 1
O18A O Uani 0.4336(9) 0.7567(8) 0.2465(5) 0.226(4) 0.033(4) d DP B 2
C19 C Uani 1.0203(3) 0.5047(2) 0.79483(15) 1.000 0.0299(10) d . . .
O19 O Uani 0.5914(3) 0.9451(2) 0.38436(19) 0.774(4) 0.0261(10) d DP B 1
O19A O Uani 0.5560(10) 0.9197(7) 0.3413(6) 0.226(4) 0.030(3) d DP B 2
O20 O Uani 0.6526(3) 0.8896(2) 0.49484(16) 0.774(4) 0.0256(10) d DP B 1
C20 C Uani 1.1004(3) 0.5261(2) 0.75408(15) 1.000 0.0291(9) d . . .
O20A O Uani 0.6295(10) 0.9235(7) 0.4719(6) 0.226(4) 0.031(4) d DP B 2
C21 C Uani 1.1809(3) 0.6461(2) 0.72283(15) 1.000 0.0274(9) d . . .
C22 C Uani 1.1627(3) 0.7385(2) 0.72227(14) 1.000 0.0284(9) d . . .
C23 C Uani 1.1816(3) 0.8879(2) 0.79010(16) 1.000 0.0298(10) d . . .
C24 C Uani 1.2310(3) 0.9485(2) 0.85835(16) 1.000 0.0304(10) d . . .
C13A C Uani 0.3939(16) 0.5983(11) 0.2220(7) 0.226(4) 0.043(6) d DP B 2
C14A C Uani 0.420(2) 0.6740(11) 0.1962(8) 0.226(4) 0.036(6) d DP B 2
C16A C Uani 0.4741(14) 0.8312(9) 0.2292(7) 0.226(4) 0.038(6) d DP B 2
C17A C Uani 0.478(3) 0.9153(16) 0.2810(10) 0.226(4) 0.0393(17) d DP B 2
C19A C Uani 0.5449(14) 0.9919(10) 0.3941(7) 0.226(4) 0.036(6) d DP B 2
C20A C Uani 0.648(2) 1.0025(15) 0.4536(12) 0.226(4) 0.035(8) d DP B 2
C22A C Uani 0.7270(16) 0.9242(11) 0.5249(8) 0.226(4) 0.044(7) d DP B 2
C23A C Uani 0.700(2) 0.8434(13) 0.5454(9) 0.226(4) 0.040(8) d DP B 2
C25 C Uani 0.0841(3) 0.54670(19) 0.43332(14) 1.000 0.0205(8) d . . .
C25A C Uani 0.6761(14) 0.6843(10) 0.5087(6) 0.226(4) 0.035(5) d DP B 2
C26 C Uani 0.6629(4) 0.5636(3) 0.3907(3) 0.774(4) 0.0348(16) d DP B 1
C26A C Uani 0.689(4) 0.609(2) 0.4533(13) 0.226(4) 0.039(11) d DP B 2
C27 C Uani 0.0903(3) 0.8510(2) 0.25035(15) 1.000 0.0250(9) d . . .
C28 C Uani 0.1650(2) 0.63087(18) 0.43139(13) 1.000 0.0169(8) d . . .
C29 C Uani 0.5334(10) 0.5262(5) 0.2836(4) 0.774(4) 0.032(2) d DP B 1
C29A C Uani 0.6118(13) 0.5334(8) 0.3409(7) 0.226(4) 0.032(6) d DP B 2
C30 C Uani 0.1767(2) 0.72431(19) 0.48976(13) 1.000 0.0188(8) d . . .
C31 C Uani 0.4243(4) 0.5519(3) 0.2451(2) 0.774(4) 0.0331(16) d DP B 1
C31A C Uani 0.501(3) 0.5222(15) 0.2867(13) 0.226(4) 0.045(10) d DP B 2
C32 C Uani 0.4978(8) 0.9083(5) 0.2715(3) 0.774(4) 0.044(2) d DP B 1
C33 C Uani 0.2821(3) 0.7400(2) 0.55270(14) 1.000 0.0248(9) d . . .
C34 C Uani 0.0530(3) 0.7362(2) 0.50974(14) 1.000 0.0244(9) d . . .
C35 C Uani 0.2941(3) 0.6045(2) 0.42442(14) 1.000 0.0227(9) d . . .
C36 C Uani -0.0016(2) 0.78992(19) 0.26974(13) 1.000 0.0191(8) d . . .
C37 C Uani 0.4234(4) 0.7598(3) 0.2040(2) 0.774(4) 0.0340(14) d DP B 1
C38 C Uani -0.0466(2) 0.84415(18) 0.33234(13) 1.000 0.0181(8) d . . .
C39 C Uani 0.6732(13) 0.6158(7) 0.4596(5) 0.774(4) 0.031(3) d DP B 1
C40 C Uani 0.5065(4) 0.9709(3) 0.3375(2) 0.774(4) 0.0393(17) d DP B 1
C41 C Uani -0.1632(3) 0.7905(2) 0.33968(14) 1.000 0.0225(9) d . . .
C42 C Uani 0.6035(7) 1.0037(5) 0.4482(4) 0.774(4) 0.034(2) d DP B 1
C43 C Uani 0.6967(4) 0.9778(3) 0.4960(2) 0.774(4) 0.0322(16) d DP B 1
C44 C Uani -0.0722(3) 0.9416(2) 0.33811(15) 1.000 0.0240(9) d . . .
C45 C Uani 0.7413(5) 0.8608(5) 0.5383(3) 0.774(4) 0.0323(19) d DP B 1
C46 C Uani 0.6992(4) 0.7647(4) 0.5310(3) 0.774(4) 0.0329(18) d DP B 1
C47 C Uani -0.1068(3) 0.7385(2) 0.20696(14) 1.000 0.0267(9) d . . .
C48 C Uani 0.3681(5) 0.6702(4) 0.2046(3) 0.774(4) 0.0330(17) d DP B 1
H13C H Uiso 1.19191 1.03950 0.96752 1.000 0.0440 c RU . .
H13D H Uiso 1.29598 0.97903 0.98112 1.000 0.0440 c RU . .
H14C H Uiso 1.15494 0.98494 1.04873 1.000 0.0430 c RU . .
H14D H Uiso 1.04507 0.93387 0.98450 1.000 0.0430 c RU . .
H15A H Uiso 1.02188 0.82063 1.03460 1.000 0.0440 c RU . .
H15B H Uiso 1.14417 0.86562 1.09334 1.000 0.0440 c RU . .
H16B H Uiso 1.23536 0.73603 1.05373 1.000 0.0410 c RU . .
H16C H Uiso 1.11409 0.71216 1.07675 1.000 0.0410 c RU . .
H17C H Uiso 1.07302 0.56443 1.00607 1.000 0.0410 c RU . .
H17D H Uiso 1.19149 0.58005 0.97873 1.000 0.0410 c RU . .
H18A H Uiso 1.03231 0.46382 0.90057 1.000 0.0460 c RU . .
H18B H Uiso 0.94116 0.53655 0.89961 1.000 0.0460 c RU . .
H19C H Uiso 0.93765 0.52161 0.78233 1.000 0.0360 c RU . .
H19D H Uiso 1.00876 0.43945 0.78874 1.000 0.0360 c RU . .
H20C H Uiso 1.18622 0.51692 0.77058 1.000 0.0350 c RU . .
H20D H Uiso 1.06793 0.48601 0.70857 1.000 0.0350 c RU . .
H21A H Uiso 1.16142 0.60427 0.67779 1.000 0.0330 c RU . .
H21B H Uiso 1.26832 0.64661 0.74465 1.000 0.0330 c RU . .
H22C H Uiso 1.21523 0.75894 0.69721 1.000 0.0340 c RU . .
H22D H Uiso 1.07483 0.73794 0.70121 1.000 0.0340 c RU . .
H23B H Uiso 1.09267 0.89094 0.77435 1.000 0.0360 c RU . .
H23C H Uiso 1.22727 0.90725 0.76185 1.000 0.0360 c RU . .
H24A H Uiso 1.32033 0.94632 0.87380 1.000 0.0360 c RU . .
H24B H Uiso 1.22234 1.01112 0.86068 1.000 0.0360 c RU . .
H13A H Uiso 0.32162 0.60524 0.24060 0.226(4) 0.0510 c RUP B 2
H13B H Uiso 0.37554 0.53988 0.18665 0.226(4) 0.0510 c RUP B 2
H14A H Uiso 0.49726 0.66999 0.18159 0.226(4) 0.0420 c RUP B 2
H14B H Uiso 0.35095 0.67026 0.15868 0.226(4) 0.0420 c RUP B 2
H16A H Uiso 0.49558 0.82761 0.18980 0.226(4) 0.0450 c RUP B 2
H17A H Uiso 0.50848 0.96681 0.26840 0.226(4) 0.0470 c RUP B 2
H17B H Uiso 0.39318 0.92066 0.28567 0.226(4) 0.0470 c RUP B 2
H19A H Uiso 0.46346 0.98015 0.40314 0.226(4) 0.0430 c RUP B 2
H19B H Uiso 0.54942 1.04818 0.38291 0.226(4) 0.0430 c RUP B 2
H20A H Uiso 0.72970 1.00933 0.44391 0.226(4) 0.0420 c RUP B 2
H20B H Uiso 0.64570 1.05658 0.48947 0.226(4) 0.0420 c RUP B 2
H22A H Uiso 0.73576 0.97972 0.56185 0.226(4) 0.0530 c RUP B 2
H22B H Uiso 0.80623 0.92377 0.51220 0.226(4) 0.0530 c RUP B 2
H23A H Uiso 0.68847 0.84483 0.58656 0.226(4) 0.0470 c RUP B 2
H25A H Uiso 0.59237 0.67445 0.51565 0.226(4) 0.0410 c RUP B 2
H25B H Uiso 0.73856 0.68812 0.54893 0.226(4) 0.0410 c RUP B 2
H26A H Uiso 0.73827 0.58200 0.37829 0.774(4) 0.0420 c RUP B 1
H26B H Uiso 0.65562 0.49864 0.38531 0.774(4) 0.0420 c RUP B 1
H26C H Uiso 0.77115 0.62074 0.44504 0.226(4) 0.0450 c RUP B 2
H26D H Uiso 0.68366 0.55234 0.46417 0.226(4) 0.0450 c RUP B 2
H29A H Uiso 0.51613 0.46168 0.27913 0.774(4) 0.0380 c RUP B 1
H29B H Uiso 0.60726 0.53653 0.26761 0.774(4) 0.0380 c RUP B 1
H29C H Uiso 0.61955 0.47559 0.34922 0.226(4) 0.0380 c RUP B 2
H29D H Uiso 0.68815 0.55423 0.33031 0.226(4) 0.0380 c RUP B 2
H31A H Uiso 0.39926 0.51029 0.19983 0.774(4) 0.0400 c RUP B 1
H31B H Uiso 0.35308 0.54862 0.26434 0.774(4) 0.0400 c RUP B 1
H31C H Uiso 0.50279 0.47133 0.24846 0.226(4) 0.0520 c RUP B 2
H31D H Uiso 0.42448 0.50915 0.29981 0.226(4) 0.0520 c RUP B 2
H32 H Uiso 0.52343 0.92423 0.23788 0.774(4) 0.0520 c RUP B 1
H37A H Uiso 0.50237 0.75573 0.19114 0.774(4) 0.0410 c RUP B 1
H37B H Uiso 0.36564 0.77988 0.17241 0.774(4) 0.0410 c RUP B 1
H39A H Uiso 0.59687 0.59878 0.47173 0.774(4) 0.0370 c RUP B 1
H39B H Uiso 0.74467 0.60263 0.48857 0.774(4) 0.0370 c RUP B 1
H40A H Uiso 0.53595 1.03333 0.34018 0.774(4) 0.0470 c RUP B 1
H40B H Uiso 0.42361 0.96837 0.34632 0.774(4) 0.0470 c RUP B 1
H42A H Uiso 0.52220 0.99995 0.45866 0.774(4) 0.0400 c RUP B 1
H42B H Uiso 0.63045 1.06643 0.45078 0.774(4) 0.0400 c RUP B 1
H43A H Uiso 0.77727 0.97911 0.48456 0.774(4) 0.0380 c RUP B 1
H43B H Uiso 0.70950 1.02099 0.54008 0.774(4) 0.0380 c RUP B 1
H45A H Uiso 0.75070 0.89906 0.58360 0.774(4) 0.0390 c RUP B 1
H45B H Uiso 0.82310 0.86716 0.52857 0.774(4) 0.0390 c RUP B 1
H46A H Uiso 0.75912 0.74559 0.56229 0.774(4) 0.0400 c RUP B 1
H46B H Uiso 0.61722 0.75824 0.54055 0.774(4) 0.0400 c RUP B 1
H48A H Uiso 0.29296 0.67534 0.22100 0.774(4) 0.0400 c RUP B 1
H48B H Uiso 0.34411 0.62639 0.16009 0.774(4) 0.0400 c RUP B 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F1 Ge1 O1 112.26(9) . . . yes
F1 Ge1 O2 97.51(10) . . . yes
F1 Ge1 O3 112.28(9) . . . yes
F1 Ge1 O4 93.38(10) . . . yes
O1 Ge1 O2 86.71(9) . . . yes
O1 Ge1 O3 135.46(9) . . . yes
O1 Ge1 O4 90.59(9) . . . yes
O2 Ge1 O3 87.58(9) . . . yes
O2 Ge1 O4 169.01(9) . . . yes
O3 Ge1 O4 86.89(9) . . . yes
O5 Ge2 O6 86.92(9) . . . yes
O5 Ge2 O7 172.04(9) . . . yes
O5 Ge2 O8 90.36(9) . . . yes
F42 Ge2 O5 92.36(8) . . . yes
F42 Ge2 O6 114.79(9) . . . yes
F42 Ge2 O7 95.58(8) . . . yes
F42 Ge2 O8 113.85(9) . . . yes
O6 Ge2 O7 89.19(9) . . . yes
O6 Ge2 O8 131.36(9) . . . yes
O7 Ge2 O8 87.01(9) . . . yes
F1 K1 F19 59.76(5) . . . yes
F1 K1 O9 98.29(7) . . . yes
F1 K1 O10 79.87(6) . . . yes
F19 K1 O14 72.98(6) . . . yes
F4 K1 F19 163.09(6) 1_655 . . yes
O9 K1 O10 61.54(6) . . . yes
O9 K1 O11 121.73(7) . . . yes
O9 K1 O12 169.36(7) . . . yes
F1 K1 O11 67.91(6) . . . yes
F1 K1 O12 91.88(7) . . . yes
F1 K1 O13 115.35(6) . . . yes
F1 K1 O14 130.76(6) . . . yes
F1 K1 F4 135.93(6) . . 1_655 yes
F19 K1 O9 81.07(6) . . . yes
F19 K1 O10 119.82(6) . . . yes
F19 K1 O11 125.59(6) . . . yes
F19 K1 O12 106.98(6) . . . yes
F19 K1 O13 74.04(6) . . . yes
O11 K1 O14 161.18(7) . . . yes
F4 K1 O11 68.35(6) 1_655 . . yes
O12 K1 O13 60.06(6) . . . yes
O12 K1 O14 115.64(7) . . . yes
F4 K1 O12 70.38(7) 1_655 . . yes
O13 K1 O14 58.60(7) . . . yes
F4 K1 O13 90.84(6) 1_655 . . yes
F4 K1 O14 92.84(6) 1_655 . . yes
O9 K1 O14 59.33(6) . . . yes
F4 K1 O9 99.87(7) 1_655 . . yes
O10 K1 O11 60.35(7) . . . yes
O10 K1 O12 117.74(7) . . . yes
O10 K1 O13 164.16(7) . . . yes
O10 K1 O14 115.67(7) . . . yes
F4 K1 O10 74.29(6) 1_655 . . yes
O11 K1 O12 59.53(6) . . . yes
O11 K1 O13 119.58(7) . . . yes
O9 K1 O13 117.34(7) . . . yes
F42 K2 O19 86.00(8) . . . yes
F42 K2 O20 98.91(8) . . . yes
F42 K2 O16A 117.5(2) . . . yes
F42 K2 O17A 103.6(2) . . . yes
F42 K2 O15A 120.4(2) . . . yes
F41 K2 O16A 62.2(2) . . . yes
F41 K2 O17A 88.7(2) . . . yes
F41 K2 O18A 114.6(2) . . . yes
F41 K2 O19A 138.0(2) . . . yes
F41 K2 O20A 102.9(3) . . . yes
F42 K2 O15 127.87(8) . . . yes
F42 K2 O16 113.54(8) . . . yes
F42 K2 O17 91.53(8) . . . yes
F42 K2 O18 70.28(8) . . . yes
O16 K2 O19 159.42(10) . . . yes
O16 K2 O20 119.26(10) . . . yes
O17 K2 O18 59.30(10) . . . yes
O17 K2 O19 116.09(11) . . . yes
O17 K2 O20 168.56(10) . . . yes
O18 K2 O19 60.05(10) . . . yes
O18 K2 O20 120.02(10) . . . yes
O19 K2 O20 60.45(11) . . . yes
O15A K2 O16A 57.9(3) . . . yes
O15A K2 O17A 113.4(3) . . . yes
O15A K2 O18A 164.8(3) . . . yes
O15A K2 O19A 117.0(4) . . . yes
O15A K2 O20A 60.0(4) . . . yes
O16A K2 O17A 58.1(3) . . . yes
O16A K2 O18A 118.1(3) . . . yes
O16A K2 O19A 159.6(3) . . . yes
O16A K2 O20A 117.8(3) . . . yes
O17A K2 O18A 60.0(3) . . . yes
O17A K2 O19A 116.0(3) . . . yes
O17A K2 O20A 164.1(3) . . . yes
O18A K2 O19A 60.9(4) . . . yes
F42 K2 O18A 74.8(2) . . . yes
F42 K2 O19A 82.6(2) . . . yes
F42 K2 O20A 91.9(2) . . . yes
O15 K2 O16 59.18(12) . . . yes
O15 K2 O17 116.30(11) . . . yes
O15 K2 O18 161.76(10) . . . yes
O15 K2 O19 114.63(12) . . . yes
O15 K2 O20 60.30(11) . . . yes
O16 K2 O17 59.59(10) . . . yes
O16 K2 O18 118.84(10) . . . yes
F41 K2 F42 57.85(5) . . . yes
F41 K2 O15 74.89(9) . . . yes
F41 K2 O16 67.43(8) . . . yes
F41 K2 O17 96.80(8) . . . yes
F41 K2 O18 122.28(8) . . . yes
F41 K2 O19 132.09(9) . . . yes
F41 K2 O20 92.74(8) . . . yes
F41 K2 O15A 77.5(2) . . . yes
O19A K2 O20A 61.8(4) . . . yes
O18A K2 O20A 122.3(4) . . . yes
Ge1 F1 K1 148.04(9) . . . yes
K1 F4 C5 108.42(19) 1_455 . . yes
K1 F19 C10 149.09(19) . . . yes
Ge1 O1 C1 115.82(17) . . . yes
Ge1 O2 C2 114.88(18) . . . yes
Ge1 O3 C3 115.50(17) . . . yes
Ge1 O4 C4 114.82(18) . . . yes
C13 O9 C24 111.7(2) . . . yes
K1 O9 C13 116.38(18) . . . yes
K1 O9 C24 119.65(18) . . . yes
K1 O10 C14 107.30(17) . . . yes
K1 O10 C15 111.88(18) . . . yes
C14 O10 C15 111.5(3) . . . yes
K1 O11 C16 116.75(18) . . . yes
C16 O11 C17 112.6(2) . . . yes
K1 O11 C17 117.78(18) . . . yes
C18 O12 C19 113.8(3) . . . yes
K1 O12 C19 109.72(18) . . . yes
K1 O12 C18 113.47(18) . . . yes
K1 O13 C20 115.87(17) . . . yes
K1 O13 C21 117.34(17) . . . yes
C20 O13 C21 112.2(2) . . . yes
K1 O14 C22 116.74(18) . . . yes
C22 O14 C23 111.9(2) . . . yes
K1 O14 C23 113.95(17) . . . yes
K2 F41 C35 153.74(17) . . . yes
Ge2 F42 K2 147.96(9) . . . yes
C2 C1 C6 117.2(2) . . . no
O1 C1 C6 107.8(2) . . . yes
C2 C1 C5 112.3(2) . . . no
O1 C1 C2 105.7(2) . . . yes
O1 C1 C5 105.5(2) . . . yes
C5 C1 C6 107.6(2) . . . no
C1 C2 C7 115.8(3) . . . no
C7 C2 C8 107.2(2) . . . no
O2 C2 C7 107.4(2) . . . yes
C1 C2 C8 112.7(2) . . . no
O2 C2 C1 106.1(2) . . . yes
O2 C2 C8 107.2(3) . . . yes
O3 C3 C4 105.9(2) . . . yes
C9 C3 C10 107.4(2) . . . no
O3 C3 C10 105.9(2) . . . yes
C4 C3 C9 116.5(2) . . . no
O3 C3 C9 107.1(2) . . . yes
C4 C3 C10 113.4(2) . . . no
O4 C4 C3 106.1(2) . . . yes
O4 C4 C11 105.6(2) . . . yes
C11 C4 C12 107.9(3) . . . no
C3 C4 C12 115.7(2) . . . no
C3 C4 C11 112.5(2) . . . no
O4 C4 C12 108.5(2) . . . yes
F2 C5 C1 110.6(3) . . . yes
F2 C5 F4 107.5(3) . . . yes
F4 C5 C1 113.0(3) . . . yes
F3 C5 F4 107.3(3) . . . yes
F3 C5 C1 111.7(3) . . . yes
F2 C5 F3 106.4(3) . . . yes
Ge2 O5 C30 114.74(16) . . . yes
F6 C6 C1 112.4(3) . . . yes
F7 C6 C1 111.9(3) . . . yes
F5 C6 C1 110.8(3) . . . yes
F5 C6 F6 106.3(3) . . . yes
F5 C6 F7 106.8(3) . . . yes
F6 C6 F7 108.3(3) . . . yes
Ge2 O6 C28 115.49(17) . . . yes
F8 C7 F9 107.8(3) . . . yes
Ge2 O7 C36 113.93(16) . . . yes
F8 C7 C2 112.4(3) . . . yes
F9 C7 F10 107.1(3) . . . yes
F8 C7 F10 106.1(3) . . . yes
F10 C7 C2 110.7(3) . . . yes
F9 C7 C2 112.5(2) . . . yes
F11 C8 C2 112.9(3) . . . yes
F11 C8 F13 108.4(3) . . . yes
F11 C8 F12 107.1(3) . . . yes
Ge2 O8 C38 115.25(16) . . . yes
F12 C8 F13 105.8(3) . . . yes
F12 C8 C2 111.0(3) . . . yes
F13 C8 C2 111.3(3) . . . yes
F14 C9 F15 106.9(2) . . . yes
F14 C9 F16 108.5(3) . . . yes
F14 C9 C3 111.9(3) . . . yes
F15 C9 F16 106.4(3) . . . yes
F16 C9 C3 112.0(2) . . . yes
F15 C9 C3 110.9(3) . . . yes
F18 C10 C3 111.1(3) . . . yes
F19 C10 C3 111.6(2) . . . yes
F17 C10 F18 107.6(2) . . . yes
F17 C10 F19 106.9(3) . . . yes
F17 C10 C3 112.8(3) . . . yes
F18 C10 F19 106.6(3) . . . yes
F20 C11 F21 107.3(3) . . . yes
F20 C11 F22 107.8(3) . . . yes
F20 C11 C4 113.3(3) . . . yes
F21 C11 F22 106.2(3) . . . yes
F21 C11 C4 111.1(3) . . . yes
F22 C11 C4 110.8(3) . . . yes
F23 C12 F24 110.9(9) . . . yes
F23 C12 F25 101.6(3) . . . yes
F25A C12 C4 115.3(10) . . . yes
F23 C12 F24A 98.0(15) . . . yes
F23 C12 F25A 124.8(9) . . . yes
F23 C12 C4 111.5(3) . . . yes
F24 C12 C4 114.3(9) . . . yes
F25 C12 C4 111.6(4) . . . yes
F24A C12 C4 110.0(15) . . . yes
O9 C13 C14 108.7(3) . . . yes
O10 C14 C13 109.3(3) . . . yes
O10 C15 C16 108.9(3) . . . yes
C39 O15 C46 112.5(6) . . . yes
K2 O15 C39 117.2(5) . . . yes
K2 O15 C46 112.4(3) . . . yes
C23A O15A C25A 113.6(13) . . . yes
K2 O15A C25A 114.8(8) . . . yes
K2 O15A C23A 112.5(11) . . . yes
O11 C16 C15 107.9(3) . . . yes
K2 O16 C26 115.5(3) . . . yes
C26 O16 C29 112.5(5) . . . yes
K2 O16 C29 115.8(4) . . . yes
C26A O16A C29A 111.6(17) . . . yes
K2 O16A C26A 116.6(14) . . . yes
K2 O16A C29A 113.4(8) . . . yes
K2 O17 C48 111.5(3) . . . yes
K2 O17 C31 112.0(2) . . . yes
O11 C17 C18 107.7(3) . . . yes
C31 O17 C48 113.6(4) . . . yes
K2 O17A C13A 107.6(9) . . . yes
K2 O17A C31A 117.4(12) . . . yes
C13A O17A C31A 111.3(16) . . . yes
O12 C18 C17 108.1(3) . . . yes
C32 O18 C37 111.9(4) . . . yes
K2 O18 C32 116.9(3) . . . yes
K2 O18 C37 118.5(3) . . . yes
C14A O18A C16A 112.4(12) . . . yes
K2 O18A C16A 116.4(8) . . . yes
K2 O18A C14A 118.4(10) . . . yes
O12 C19 C20 107.4(3) . . . yes
C40 O19 C42 110.8(4) . . . yes
K2 O19 C40 113.0(3) . . . yes
K2 O19 C42 112.4(4) . . . yes
K2 O19A C17A 115.2(12) . . . yes
C17A O19A C19A 113.6(15) . . . yes
K2 O19A C19A 108.4(9) . . . yes
O13 C20 C19 108.3(3) . . . yes
K2 O20 C43 117.0(2) . . . yes
K2 O20 C45 117.4(3) . . . yes
C43 O20 C45 110.9(4) . . . yes
K2 O20A C20A 117.1(12) . . . yes
K2 O20A C22A 118.5(10) . . . yes
C20A O20A C22A 111.8(14) . . . yes
O13 C21 C22 108.0(3) . . . yes
O14 C22 C21 109.1(2) . . . yes
O14 C23 C24 109.3(3) . . . yes
O9 C24 C23 109.3(3) . . . yes
C14 C13 H13C 110.00 . . . no
O9 C13 H13C 110.00 . . . no
O9 C13 H13D 110.00 . . . no
H13C C13 H13D 108.00 . . . no
C14 C13 H13D 110.00 . . . no
C13 C14 H14D 110.00 . . . no
C13 C14 H14C 110.00 . . . no
O10 C14 H14C 110.00 . . . no
H14C C14 H14D 108.00 . . . no
O10 C14 H14D 110.00 . . . no
O10 C15 H15A 110.00 . . . no
O10 C15 H15B 110.00 . . . no
H15A C15 H15B 108.00 . . . no
C16 C15 H15A 110.00 . . . no
C16 C15 H15B 110.00 . . . no
O11 C16 H16B 110.00 . . . no
O11 C16 H16C 110.00 . . . no
C15 C16 H16B 110.00 . . . no
C15 C16 H16C 110.00 . . . no
H16B C16 H16C 108.00 . . . no
C18 C17 H17D 110.00 . . . no
O11 C17 H17C 110.00 . . . no
O11 C17 H17D 110.00 . . . no
H17C C17 H17D 108.00 . . . no
C18 C17 H17C 110.00 . . . no
O12 C18 H18A 110.00 . . . no
O12 C18 H18B 110.00 . . . no
H18A C18 H18B 108.00 . . . no
C17 C18 H18A 110.00 . . . no
C17 C18 H18B 110.00 . . . no
O12 C19 H19C 110.00 . . . no
C20 C19 H19D 110.00 . . . no
O12 C19 H19D 110.00 . . . no
C20 C19 H19C 110.00 . . . no
H19C C19 H19D 108.00 . . . no
H20C C20 H20D 108.00 . . . no
C19 C20 H20D 110.00 . . . no
O13 C20 H20C 110.00 . . . no
O13 C20 H20D 110.00 . . . no
C19 C20 H20C 110.00 . . . no
C22 C21 H21B 110.00 . . . no
H21A C21 H21B 108.00 . . . no
C22 C21 H21A 110.00 . . . no
O13 C21 H21B 110.00 . . . no
O13 C21 H21A 110.00 . . . no
O14 C22 H22D 110.00 . . . no
C21 C22 H22C 110.00 . . . no
O14 C22 H22C 110.00 . . . no
H22C C22 H22D 108.00 . . . no
C21 C22 H22D 110.00 . . . no
O14 C23 H23C 110.00 . . . no
O14 C23 H23B 110.00 . . . no
C24 C23 H23C 110.00 . . . no
H23B C23 H23C 108.00 . . . no
C24 C23 H23B 110.00 . . . no
C23 C24 H24B 110.00 . . . no
H24A C24 H24B 108.00 . . . no
O9 C24 H24A 110.00 . . . no
O9 C24 H24B 110.00 . . . no
C23 C24 H24A 110.00 . . . no
O17A C13A C14A 106.8(14) . . . yes
O18A C14A C13A 108.6(13) . . . yes
O18A C16A C17A 110.2(15) . . . yes
O19A C17A C16A 113(2) . . . yes
O19A C19A C20A 109.8(15) . . . yes
O20A C20A C19A 107.5(17) . . . yes
O20A C22A C23A 110.1(15) . . . yes
O15A C23A C22A 108.8(15) . . . yes
F27 C25 F29 107.1(2) . . . yes
F27 C25 C28 111.5(2) . . . yes
F27 C25 F28 106.4(2) . . . yes
F28 C25 C28 112.0(2) . . . yes
F29 C25 C28 111.6(2) . . . yes
F28 C25 F29 108.1(2) . . . yes
O15A C25A C26A 107.8(16) . . . yes
O16 C26 C39 109.0(6) . . . yes
O16A C26A C25A 110(3) . . . yes
F31 C27 F50 106.3(3) . . . yes
F31 C27 C36 111.5(3) . . . yes
F49 C27 C36 112.1(3) . . . yes
F50 C27 C36 111.7(2) . . . yes
F49 C27 F50 107.5(3) . . . yes
F31 C27 F49 107.4(2) . . . yes
C25 C28 C30 116.6(2) . . . no
C25 C28 C35 107.3(2) . . . no
C30 C28 C35 113.2(2) . . . no
O6 C28 C30 105.9(2) . . . yes
O6 C28 C35 105.4(2) . . . yes
O6 C28 C25 107.8(2) . . . yes
O16 C29 C31 108.3(7) . . . yes
O16A C29A C31A 106.6(15) . . . yes
O5 C30 C28 106.3(2) . . . yes
O5 C30 C34 106.1(2) . . . yes
C28 C30 C33 115.7(2) . . . no
C28 C30 C34 112.8(2) . . . no
C33 C30 C34 107.9(2) . . . no
O5 C30 C33 107.4(2) . . . yes
O17 C31 C29 107.9(5) . . . yes
O17A C31A C29A 108.3(19) . . . yes
O18 C32 C40 108.6(5) . . . yes
F40 C33 C30 112.2(2) . . . yes
F35 C33 C30 112.2(3) . . . yes
F33 C33 F35 106.5(2) . . . yes
F33 C33 F40 106.3(3) . . . yes
F33 C33 C30 111.1(3) . . . yes
F35 C33 F40 108.4(3) . . . yes
F44 C34 C30 111.1(2) . . . yes
F45 C34 F46 106.6(2) . . . yes
F44 C34 F46 105.9(3) . . . yes
F44 C34 F45 108.2(3) . . . yes
F45 C34 C30 113.5(3) . . . yes
F46 C34 C30 111.2(3) . . . yes
F41 C35 C28 111.2(3) . . . yes
F26 C35 C28 110.6(2) . . . yes
F41 C35 F43 108.1(2) . . . yes
F26 C35 F41 106.1(2) . . . yes
F26 C35 F43 107.6(3) . . . yes
F43 C35 C28 112.9(2) . . . yes
C38 C36 C47 116.0(2) . . . no
O7 C36 C38 105.8(2) . . . yes
C27 C36 C47 106.9(2) . . . no
O7 C36 C27 107.1(2) . . . yes
O7 C36 C47 107.6(2) . . . yes
C27 C36 C38 113.0(2) . . . no
O18 C37 C48 107.9(4) . . . yes
C36 C38 C41 112.2(2) . . . no
C36 C38 C44 117.6(2) . . . no
C41 C38 C44 107.7(2) . . . no
O8 C38 C44 106.8(2) . . . yes
O8 C38 C36 106.23(19) . . . yes
O8 C38 C41 105.5(2) . . . yes
O15 C39 C26 108.7(7) . . . yes
O19 C40 C32 108.8(5) . . . yes
F32 C41 C38 113.6(2) . . . yes
F30 C41 F32 106.6(3) . . . yes
F30 C41 F36 106.2(2) . . . yes
F36 C41 C38 110.6(3) . . . yes
F32 C41 F36 107.6(2) . . . yes
F30 C41 C38 111.9(2) . . . yes
O19 C42 C43 109.8(6) . . . yes
O20 C43 C42 109.1(4) . . . yes
F37 C44 C38 111.0(2) . . . yes
F38 C44 C38 111.6(2) . . . yes
F34 C44 C38 112.4(3) . . . yes
F34 C44 F37 106.4(3) . . . yes
F34 C44 F38 107.6(3) . . . yes
F37 C44 F38 107.5(3) . . . yes
O20 C45 C46 109.9(5) . . . yes
O15 C46 C45 109.6(5) . . . yes
F48 C47 C36 110.8(3) . . . yes
F39 C47 F48 107.1(2) . . . yes
F47 C47 C36 112.3(2) . . . yes
F39 C47 F47 107.7(3) . . . yes
F39 C47 C36 112.2(3) . . . yes
F47 C47 F48 106.5(2) . . . yes
O17 C48 C37 107.7(4) . . . yes
H13A C13A H13B 109.00 . . . no
O17A C13A H13A 110.00 . . . no
O17A C13A H13B 110.00 . . . no
C14A C13A H13A 110.00 . . . no
C14A C13A H13B 110.00 . . . no
C13A C14A H14B 110.00 . . . no
H14A C14A H14B 108.00 . . . no
C13A C14A H14A 110.00 . . . no
O18A C14A H14B 110.00 . . . no
O18A C14A H14A 110.00 . . . no
O18A C16A H16A 125.00 . . . no
C17A C16A H16A 125.00 . . . no
H17A C17A H17B 108.00 . . . no
O19A C17A H17A 109.00 . . . no
O19A C17A H17B 109.00 . . . no
C16A C17A H17A 109.00 . . . no
C16A C17A H17B 109.00 . . . no
O19A C19A H19B 110.00 . . . no
C20A C19A H19A 110.00 . . . no
O19A C19A H19A 110.00 . . . no
H19A C19A H19B 108.00 . . . no
C20A C19A H19B 110.00 . . . no
C19A C20A H20A 110.00 . . . no
O20A C20A H20B 110.00 . . . no
O20A C20A H20A 110.00 . . . no
C19A C20A H20B 110.00 . . . no
H20A C20A H20B 108.00 . . . no
H22A C22A H22B 108.00 . . . no
O20A C22A H22A 110.00 . . . no
O20A C22A H22B 110.00 . . . no
C23A C22A H22A 110.00 . . . no
C23A C22A H22B 110.00 . . . no
O15A C23A H23A 126.00 . . . no
C22A C23A H23A 126.00 . . . no
O15A C25A H25A 110.00 . . . no
H25A C25A H25B 108.00 . . . no
C26A C25A H25B 110.00 . . . no
O15A C25A H25B 110.00 . . . no
C26A C25A H25A 110.00 . . . no
C39 C26 H26A 110.00 . . . no
O16 C26 H26B 110.00 . . . no
O16 C26 H26A 110.00 . . . no
C39 C26 H26B 110.00 . . . no
H26A C26 H26B 108.00 . . . no
H26C C26A H26D 108.00 . . . no
C25A C26A H26D 110.00 . . . no
O16A C26A H26C 110.00 . . . no
O16A C26A H26D 109.00 . . . no
C25A C26A H26C 110.00 . . . no
C31 C29 H29A 110.00 . . . no
C31 C29 H29B 110.00 . . . no
H29A C29 H29B 108.00 . . . no
O16 C29 H29B 110.00 . . . no
O16 C29 H29A 110.00 . . . no
O16A C29A H29C 110.00 . . . no
O16A C29A H29D 110.00 . . . no
C31A C29A H29C 110.00 . . . no
H29C C29A H29D 109.00 . . . no
C31A C29A H29D 110.00 . . . no
C29 C31 H31A 110.00 . . . no
C29 C31 H31B 110.00 . . . no
H31A C31 H31B 108.00 . . . no
O17 C31 H31B 110.00 . . . no
O17 C31 H31A 110.00 . . . no
O17A C31A H31C 110.00 . . . no
H31C C31A H31D 108.00 . . . no
C29A C31A H31D 110.00 . . . no
O17A C31A H31D 110.00 . . . no
C29A C31A H31C 110.00 . . . no
O18 C32 H32 126.00 . . . no
C40 C32 H32 126.00 . . . no
O18 C37 H37A 110.00 . . . no
O18 C37 H37B 110.00 . . . no
C48 C37 H37A 110.00 . . . no
C48 C37 H37B 110.00 . . . no
H37A C37 H37B 108.00 . . . no
O15 C39 H39A 110.00 . . . no
O15 C39 H39B 110.00 . . . no
C26 C39 H39A 110.00 . . . no
H39A C39 H39B 108.00 . . . no
C26 C39 H39B 110.00 . . . no
O19 C40 H40A 110.00 . . . no
H40A C40 H40B 108.00 . . . no
C32 C40 H40B 110.00 . . . no
O19 C40 H40B 110.00 . . . no
C32 C40 H40A 110.00 . . . no
O19 C42 H42A 110.00 . . . no
C43 C42 H42B 110.00 . . . no
O19 C42 H42B 110.00 . . . no
C43 C42 H42A 110.00 . . . no
H42A C42 H42B 108.00 . . . no
C42 C43 H43A 110.00 . . . no
O20 C43 H43A 110.00 . . . no
O20 C43 H43B 110.00 . . . no
H43A C43 H43B 108.00 . . . no
C42 C43 H43B 110.00 . . . no
O20 C45 H45A 110.00 . . . no
H45A C45 H45B 108.00 . . . no
C46 C45 H45B 110.00 . . . no
O20 C45 H45B 110.00 . . . no
C46 C45 H45A 110.00 . . . no
C45 C46 H46A 110.00 . . . no
O15 C46 H46B 110.00 . . . no
C45 C46 H46B 110.00 . . . no
H46A C46 H46B 108.00 . . . no
O15 C46 H46A 110.00 . . . no
O17 C48 H48A 110.00 . . . no
O17 C48 H48B 110.00 . . . no
C37 C48 H48B 110.00 . . . no
H48A C48 H48B 108.00 . . . no
C37 C48 H48A 110.00 . . . no
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ge1 F1 1.7274(18) . . yes
Ge1 O1 1.812(2) . . yes
Ge1 O2 1.841(2) . . yes
Ge1 O3 1.8100(19) . . yes
Ge1 O4 1.847(2) . . yes
Ge2 O7 1.8539(19) . . yes
Ge2 O8 1.815(2) . . yes
Ge2 O6 1.814(2) . . yes
Ge2 F42 1.7274(17) . . yes
Ge2 O5 1.8511(19) . . yes
K1 O9 2.766(2) . . yes
K1 O10 2.800(2) . . yes
K1 O11 2.778(2) . . yes
K1 O12 2.801(2) . . yes
K1 F1 2.8188(18) . . yes
K1 F19 2.7794(18) . . yes
K1 O14 2.844(2) . . yes
K1 F4 2.969(2) . 1_655 yes
K1 O13 2.826(2) . . yes
K2 O16A 2.912(10) . . yes
K2 O17A 2.815(9) . . yes
K2 O20 2.796(3) . . yes
K2 O15A 2.874(12) . . yes
K2 F41 2.8333(18) . . yes
K2 F42 2.8254(18) . . yes
K2 O15 2.805(4) . . yes
K2 O16 2.843(3) . . yes
K2 O17 2.820(3) . . yes
K2 O18 2.790(3) . . yes
K2 O19 2.800(3) . . yes
K2 O18A 2.765(11) . . yes
K2 O19A 2.760(12) . . yes
K2 O20A 2.746(12) . . yes
F2 C5 1.338(4) . . yes
F3 C5 1.321(4) . . yes
F4 C5 1.344(4) . . yes
F5 C6 1.337(4) . . yes
F6 C6 1.319(4) . . yes
F7 C6 1.335(4) . . yes
F8 C7 1.329(4) . . yes
F9 C7 1.332(4) . . yes
F10 C7 1.340(4) . . yes
F11 C8 1.340(4) . . yes
F12 C8 1.332(4) . . yes
F13 C8 1.329(4) . . yes
F14 C9 1.329(4) . . yes
F15 C9 1.339(4) . . yes
F16 C9 1.325(4) . . yes
F17 C10 1.339(4) . . yes
F18 C10 1.316(4) . . yes
F19 C10 1.333(4) . . yes
F20 C11 1.342(4) . . yes
F21 C11 1.331(4) . . yes
F22 C11 1.325(4) . . yes
F23 C12 1.329(4) . . yes
F24 C12 1.323(11) . . yes
F24A C12 1.33(3) . . yes
F25 C12 1.356(4) . . yes
F25A C12 1.321(19) . . yes
O1 C1 1.392(3) . . yes
O2 C2 1.375(4) . . yes
O3 C3 1.389(4) . . yes
O4 C4 1.377(3) . . yes
O9 C24 1.428(4) . . yes
O9 C13 1.426(4) . . yes
O10 C14 1.425(4) . . yes
O10 C15 1.424(4) . . yes
O11 C17 1.409(4) . . yes
O11 C16 1.421(4) . . yes
O12 C19 1.425(4) . . yes
O12 C18 1.419(4) . . yes
O13 C20 1.430(4) . . yes
O13 C21 1.428(4) . . yes
O14 C23 1.425(4) . . yes
O14 C22 1.423(4) . . yes
F26 C35 1.330(4) . . yes
F27 C25 1.334(4) . . yes
F28 C25 1.331(4) . . yes
F29 C25 1.334(3) . . yes
F30 C41 1.329(3) . . yes
F31 C27 1.326(4) . . yes
F32 C41 1.344(4) . . yes
F33 C33 1.339(4) . . yes
F34 C44 1.326(4) . . yes
F35 C33 1.338(4) . . yes
F36 C41 1.342(4) . . yes
F37 C44 1.324(4) . . yes
F38 C44 1.334(4) . . yes
F39 C47 1.336(4) . . yes
F40 C33 1.321(4) . . yes
F41 C35 1.335(4) . . yes
F43 C35 1.339(4) . . yes
F44 C34 1.327(4) . . yes
F45 C34 1.347(4) . . yes
F46 C34 1.338(4) . . yes
F47 C47 1.329(4) . . yes
F48 C47 1.335(4) . . yes
F49 C27 1.348(4) . . yes
F50 C27 1.335(4) . . yes
C1 C6 1.555(4) . . no
C1 C2 1.623(4) . . no
C1 C5 1.561(4) . . no
C2 C8 1.564(5) . . no
C2 C7 1.564(5) . . no
C3 C9 1.555(4) . . no
C3 C10 1.565(4) . . no
C3 C4 1.627(4) . . no
C4 C12 1.557(5) . . no
C4 C11 1.566(5) . . no
O5 C30 1.378(4) . . yes
O6 C28 1.391(3) . . yes
O7 C36 1.384(4) . . yes
O8 C38 1.394(3) . . yes
C13 C14 1.497(5) . . no
O15 C39 1.435(13) . . yes
C15 C16 1.489(5) . . no
O15 C46 1.415(7) . . yes
O15A C23A 1.41(2) . . yes
O15A C25A 1.42(2) . . yes
O16 C26 1.421(6) . . yes
O16 C29 1.434(9) . . yes
O16A C26A 1.41(4) . . yes
O16A C29A 1.436(18) . . yes
O17 C48 1.422(7) . . yes
C17 C18 1.495(5) . . no
O17 C31 1.419(6) . . yes
O17A C31A 1.41(3) . . yes
O17A C13A 1.429(19) . . yes
O18 C32 1.407(9) . . yes
O18 C37 1.416(5) . . yes
O18A C16A 1.41(2) . . yes
O18A C14A 1.42(2) . . yes
O19 C40 1.429(6) . . yes
O19 C42 1.421(9) . . yes
C19 C20 1.494(5) . . no
O19A C17A 1.41(3) . . yes
O19A C19A 1.416(19) . . yes
O20 C45 1.431(7) . . yes
O20 C43 1.425(6) . . yes
O20A C22A 1.42(2) . . yes
O20A C20A 1.43(3) . . yes
C21 C22 1.494(5) . . no
C23 C24 1.488(5) . . no
C13 H13D 0.9900 . . no
C13 H13C 0.9900 . . no
C14 H14D 0.9900 . . no
C14 H14C 0.9900 . . no
C15 H15A 0.9900 . . no
C15 H15B 0.9900 . . no
C16 H16C 0.9900 . . no
C16 H16B 0.9900 . . no
C17 H17C 0.9900 . . no
C17 H17D 0.9900 . . no
C18 H18A 0.9900 . . no
C18 H18B 0.9900 . . no
C19 H19C 0.9900 . . no
C19 H19D 0.9900 . . no
C20 H20C 0.9900 . . no
C20 H20D 0.9900 . . no
C21 H21B 0.9900 . . no
C21 H21A 0.9900 . . no
C22 H22D 0.9900 . . no
C22 H22C 0.9900 . . no
C23 H23B 0.9900 . . no
C23 H23C 0.9900 . . no
C24 H24A 0.9900 . . no
C24 H24B 0.9900 . . no
C13A C14A 1.50(3) . . no
C16A C17A 1.47(3) . . no
C19A C20A 1.51(3) . . no
C22A C23A 1.50(3) . . no
C25 C28 1.555(4) . . no
C25A C26A 1.49(3) . . no
C26 C39 1.488(12) . . no
C27 C36 1.561(4) . . no
C28 C30 1.628(4) . . no
C28 C35 1.568(4) . . no
C29 C31 1.491(11) . . no
C29A C31A 1.48(3) . . no
C30 C33 1.560(4) . . no
C30 C34 1.558(4) . . no
C32 C40 1.489(8) . . no
C36 C38 1.621(4) . . no
C36 C47 1.560(4) . . no
C37 C48 1.496(8) . . no
C38 C41 1.557(4) . . no
C38 C44 1.564(4) . . no
C42 C43 1.494(9) . . no
C45 C46 1.497(10) . . no
C13A H13A 0.9900 . . no
C13A H13B 0.9900 . . no
C14A H14A 0.9900 . . no
C14A H14B 0.9900 . . no
C16A H16A 0.9500 . . no
C17A H17B 0.9900 . . no
C17A H17A 0.9900 . . no
C19A H19B 0.9900 . . no
C19A H19A 0.9900 . . no
C20A H20B 0.9900 . . no
C20A H20A 0.9900 . . no
C22A H22A 0.9900 . . no
C22A H22B 0.9900 . . no
C23A H23A 0.9500 . . no
C25A H25A 0.9900 . . no
C25A H25B 0.9900 . . no
C26 H26A 0.9900 . . no
C26 H26B 0.9900 . . no
C26A H26D 0.9900 . . no
C26A H26C 0.9900 . . no
C29 H29B 0.9900 . . no
C29 H29A 0.9900 . . no
C29A H29C 0.9900 . . no
C29A H29D 0.9900 . . no
C31 H31B 0.9900 . . no
C31 H31A 0.9900 . . no
C31A H31D 0.9900 . . no
C31A H31C 0.9900 . . no
C32 H32 0.9500 . . no
C37 H37B 0.9900 . . no
C37 H37A 0.9900 . . no
C39 H39A 0.9900 . . no
C39 H39B 0.9900 . . no
C40 H40B 0.9900 . . no
C40 H40A 0.9900 . . no
C42 H42A 0.9900 . . no
C42 H42B 0.9900 . . no
C43 H43A 0.9900 . . no
C43 H43B 0.9900 . . no
C45 H45A 0.9900 . . no
C45 H45B 0.9900 . . no
C46 H46A 0.9900 . . no
C46 H46B 0.9900 . . no
C48 H48A 0.9900 . . no
C48 H48B 0.9900 . . no
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
_geom_hbond_publ_flag
C15 H15B F23 0.9900 2.4500 3.409(4) 162.00 2_777 yes
C23 H23B F24 0.9900 2.5000 3.394(11) 150.00 . yes
C31 H31A O2 0.9900 2.4900 3.421(5) 156.00 2_666 yes
C40 H40A F20 0.9900 2.4900 3.226(5) 131.00 2_676 yes
C46 H46B F40 0.9900 2.5100 3.486(5) 167.00 . yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 Ge1 F1 K1 -151.42(18) . . . . no
O2 Ge1 F1 K1 119.1(2) . . . . no
O3 Ge1 F1 K1 28.6(2) . . . . no
O4 Ge1 F1 K1 -59.4(2) . . . . no
F1 Ge1 O1 C1 -107.10(18) . . . . no
O2 Ge1 O1 C1 -10.33(18) . . . . no
O3 Ge1 O1 C1 72.9(2) . . . . no
O4 Ge1 O1 C1 159.01(18) . . . . no
F1 Ge1 O2 C2 98.9(2) . . . . no
O1 Ge1 O2 C2 -13.1(2) . . . . no
O3 Ge1 O2 C2 -148.9(2) . . . . no
F1 Ge1 O3 C3 -80.00(19) . . . . no
O1 Ge1 O3 C3 100.1(2) . . . . no
O2 Ge1 O3 C3 -177.12(18) . . . . no
O4 Ge1 O3 C3 12.38(17) . . . . no
F1 Ge1 O4 C4 123.4(2) . . . . no
O1 Ge1 O4 C4 -124.3(2) . . . . no
O3 Ge1 O4 C4 11.2(2) . . . . no
F42 Ge2 O7 C36 -99.20(17) . . . . no
O6 Ge2 O7 C36 145.97(17) . . . . no
O8 Ge2 O7 C36 14.48(17) . . . . no
F42 Ge2 O8 C38 104.49(18) . . . . no
O5 Ge2 O8 C38 -162.78(18) . . . . no
O6 Ge2 O8 C38 -76.6(2) . . . . no
O7 Ge2 O8 C38 9.71(18) . . . . no
O8 Ge2 O5 C30 120.54(17) . . . . no
O5 Ge2 F42 K2 69.57(17) . . . . no
O6 Ge2 F42 K2 -18.12(19) . . . . no
O7 Ge2 F42 K2 -109.81(16) . . . . no
O8 Ge2 F42 K2 161.00(15) . . . . no
F42 Ge2 O5 C30 -125.57(17) . . . . no
O6 Ge2 O5 C30 -10.86(17) . . . . no
O7 Ge2 O6 C28 174.51(17) . . . . no
F42 Ge2 O6 C28 78.74(17) . . . . no
O5 Ge2 O6 C28 -12.43(17) . . . . no
O8 Ge2 O6 C28 -100.19(18) . . . . no
F4 K1 F1 Ge1 -165.96(17) 1_655 . . . no
O10 K1 O9 C13 3.66(19) . . . . no
O10 K1 O9 C24 142.9(2) . . . . no
O11 K1 O9 C13 8.2(2) . . . . no
O11 K1 O9 C24 147.42(19) . . . . no
F1 K1 F19 C10 -90.7(3) . . . . no
O9 K1 F19 C10 164.2(3) . . . . no
O10 K1 F19 C10 -146.0(3) . . . . no
O11 K1 F19 C10 -73.0(3) . . . . no
O12 K1 F19 C10 -8.7(4) . . . . no
O13 K1 F19 C10 42.3(3) . . . . no
O14 K1 F19 C10 103.7(3) . . . . no
F1 K1 O9 C13 77.3(2) . . . . no
F1 K1 O9 C24 -143.5(2) . . . . no
F19 K1 O9 C13 134.8(2) . . . . no
F19 K1 O9 C24 -86.0(2) . . . . no
O9 K1 O10 C15 152.4(2) . . . . no
O11 K1 O10 C14 -145.8(2) . . . . no
O11 K1 O10 C15 -23.2(2) . . . . no
O12 K1 O10 C14 -162.35(18) . . . . no
O12 K1 O10 C15 -39.7(2) . . . . no
O14 K1 O10 C14 55.0(2) . . . . no
O14 K1 O10 C15 177.6(2) . . . . no
F4 K1 O10 C14 140.5(2) 1_655 . . . no
F4 K1 O10 C15 -96.9(2) 1_655 . . . no
F1 K1 O11 C16 -102.4(2) . . . . no
F1 K1 O11 C17 118.9(2) . . . . no
F19 K1 O11 C16 -118.9(2) . . . . no
F19 K1 O11 C17 102.4(2) . . . . no
O9 K1 O11 C16 -16.3(2) . . . . no
O9 K1 O11 C17 -155.0(2) . . . . no
O10 K1 O11 C16 -11.62(19) . . . . no
O10 K1 O11 C17 -150.3(2) . . . . no
O12 K1 O11 C16 151.4(2) . . . . no
O12 K1 O11 C17 12.7(2) . . . . no
O13 K1 O11 C16 150.14(19) . . . . no
O13 K1 O9 C13 -158.44(19) . . . . no
O13 K1 O9 C24 -19.3(2) . . . . no
O14 K1 O9 C13 -149.8(2) . . . . no
O14 K1 O9 C24 -10.58(19) . . . . no
F4 K1 O9 C13 -62.3(2) 1_655 . . . no
F4 K1 O9 C24 76.9(2) 1_655 . . . no
F1 K1 O10 C14 -75.57(19) . . . . no
F1 K1 O10 C15 47.1(2) . . . . no
F19 K1 O10 C14 -29.4(2) . . . . no
F19 K1 O10 C15 93.3(2) . . . . no
O9 K1 O10 C14 29.70(18) . . . . no
O13 K1 O12 C18 -158.7(2) . . . . no
O13 K1 O12 C19 -30.17(18) . . . . no
O14 K1 O12 C18 -178.1(2) . . . . no
O14 K1 O12 C19 -49.6(2) . . . . no
F4 K1 O12 C18 98.4(2) 1_655 . . . no
F4 K1 O12 C19 -133.1(2) 1_655 . . . no
F1 K1 O13 C20 -81.5(2) . . . . no
F1 K1 O13 C21 142.08(19) . . . . no
F19 K1 O13 C20 -125.9(2) . . . . no
F19 K1 O13 C21 97.7(2) . . . . no
O9 K1 O13 C20 163.35(19) . . . . no
O9 K1 O13 C21 27.0(2) . . . . no
O11 K1 O13 C20 -3.6(2) . . . . no
O11 K1 O13 C21 -140.02(19) . . . . no
O12 K1 O13 C20 -4.88(19) . . . . no
O12 K1 O13 C21 -141.3(2) . . . . no
O14 K1 O13 C20 154.6(2) . . . . no
O14 K1 O13 C21 18.21(19) . . . . no
F4 K1 O13 C20 61.8(2) 1_655 . . . no
F4 K1 O13 C21 -74.6(2) 1_655 . . . no
F1 K1 O14 C22 -81.8(2) . . . . no
F1 K1 O14 C23 51.2(2) . . . . no
F19 K1 O14 C22 -65.30(19) . . . . no
F19 K1 O14 C23 67.61(19) . . . . no
O9 K1 O14 C22 -154.9(2) . . . . no
O9 K1 O14 C23 -21.98(18) . . . . no
O10 K1 O14 C22 179.23(19) . . . . no
O10 K1 O14 C23 -47.9(2) . . . . no
O12 K1 O14 C22 35.8(2) . . . . no
O12 K1 O14 C23 168.67(18) . . . . no
O13 K1 O14 C22 16.07(19) . . . . no
O13 K1 O14 C23 149.0(2) . . . . no
F4 K1 O14 C22 105.3(2) 1_655 . . . no
F4 K1 O14 C23 -121.77(19) 1_655 . . . no
F1 K1 F4 C5 -155.96(18) . . 1_655 1_655 no
O9 K1 F4 C5 -43.0(2) . . 1_655 1_655 no
O10 K1 F4 C5 -99.6(2) . . 1_655 1_655 no
O11 K1 F4 C5 -163.4(2) . . 1_655 1_655 no
O12 K1 F4 C5 132.6(2) . . 1_655 1_655 no
O13 K1 F4 C5 74.94(19) . . 1_655 1_655 no
O14 K1 F4 C5 16.34(19) . . 1_655 1_655 no
F1 K1 O12 C19 88.22(19) . . . . no
F19 K1 O12 C18 -99.2(2) . . . . no
F19 K1 O12 C19 29.3(2) . . . . no
O10 K1 O12 C18 39.2(2) . . . . no
O10 K1 O12 C19 167.76(18) . . . . no
O11 K1 O12 C18 22.6(2) . . . . no
O11 K1 O12 C19 151.1(2) . . . . no
F19 K1 F1 Ge1 5.96(18) . . . . no
O9 K1 F1 Ge1 80.5(2) . . . . no
O10 K1 F1 Ge1 139.5(2) . . . . no
O11 K1 F1 Ge1 -158.5(2) . . . . no
O13 K1 O11 C17 11.4(2) . . . . no
F4 K1 O11 C16 72.1(2) 1_655 . . . no
F4 K1 O11 C17 -66.6(2) 1_655 . . . no
F1 K1 O12 C18 -40.3(2) . . . . no
O14 K1 F1 Ge1 24.2(2) . . . . no
O12 K1 F1 Ge1 -102.7(2) . . . . no
O13 K1 F1 Ge1 -45.1(2) . . . . no
O18 K2 O16 C26 140.9(3) . . . . no
O18 K2 O16 C29 6.3(6) . . . . no
O19 K2 O16 C26 59.8(5) . . . . no
O19 K2 O16 C29 -74.8(6) . . . . no
F41 K2 O17 C48 96.2(3) . . . . no
F42 K2 O17 C31 -90.1(3) . . . . no
F42 K2 O17 C48 38.4(3) . . . . no
O15 K2 O17 C31 44.2(3) . . . . no
O20 K2 O16 C26 -23.6(3) . . . . no
O20 K2 O16 C29 -158.1(5) . . . . no
F41 K2 O17 C31 -32.3(3) . . . . no
F42 K2 F41 C35 101.4(4) . . . . no
O15 K2 F41 C35 -101.6(4) . . . . no
O16 K2 F41 C35 -39.2(4) . . . . no
O17 K2 F41 C35 13.9(4) . . . . no
O18 K2 F41 C35 71.7(4) . . . . no
O19 K2 F41 C35 148.6(4) . . . . no
O20 K2 F41 C35 -159.8(4) . . . . no
F41 K2 F42 Ge2 -13.36(15) . . . . no
O15 K2 F42 Ge2 -41.9(2) . . . . no
O16 K2 F42 Ge2 26.45(19) . . . . no
O17 K2 F42 Ge2 83.72(18) . . . . no
O18 K2 F42 Ge2 140.21(18) . . . . no
O19 K2 F42 Ge2 -160.24(18) . . . . no
O20 K2 F42 Ge2 -100.99(17) . . . . no
F41 K2 O15 C39 56.6(6) . . . . no
F41 K2 O15 C46 -76.0(3) . . . . no
F42 K2 O15 C39 81.4(6) . . . . no
F42 K2 O15 C46 -51.3(4) . . . . no
O16 K2 O15 C39 -15.8(6) . . . . no
O16 K2 O15 C46 -148.4(4) . . . . no
O17 K2 O15 C39 -33.6(7) . . . . no
O17 K2 O15 C46 -166.2(3) . . . . no
O19 K2 O15 C39 -173.6(6) . . . . no
O19 K2 O15 C46 53.8(3) . . . . no
O20 K2 O15 C39 158.8(7) . . . . no
O20 K2 O15 C46 26.2(3) . . . . no
F41 K2 O16 C26 -103.6(3) . . . . no
F41 K2 O16 C29 121.9(5) . . . . no
F42 K2 O16 C26 -139.5(3) . . . . no
F42 K2 O16 C29 86.0(5) . . . . no
O15 K2 O16 C26 -18.2(3) . . . . no
O15 K2 O16 C29 -152.7(6) . . . . no
O17 K2 O16 C26 143.3(3) . . . . no
O17 K2 O16 C29 8.8(5) . . . . no
F41 K2 O19 C42 40.0(4) . . . . no
F42 K2 O19 C40 -47.6(3) . . . . no
F42 K2 O19 C42 78.6(4) . . . . no
O15 K2 O19 C40 -177.8(3) . . . . no
O15 K2 O19 C42 -51.6(4) . . . . no
O16 K2 O19 C40 114.7(4) . . . . no
O16 K2 O19 C42 -119.1(5) . . . . no
O17 K2 O19 C40 42.1(3) . . . . no
O17 K2 O19 C42 168.4(4) . . . . no
O18 K2 O19 C40 21.9(3) . . . . no
O18 K2 O19 C42 148.1(4) . . . . no
O15 K2 O17 C48 172.7(3) . . . . no
O16 K2 O17 C31 26.5(3) . . . . no
O16 K2 O17 C48 155.0(4) . . . . no
O18 K2 O17 C31 -155.9(3) . . . . no
O18 K2 O17 C48 -27.5(3) . . . . no
O19 K2 O17 C31 -176.3(3) . . . . no
O19 K2 O17 C48 -47.9(3) . . . . no
F41 K2 O18 C32 136.0(4) . . . . no
F41 K2 O18 C37 -85.2(3) . . . . no
F42 K2 O18 C32 109.6(4) . . . . no
F42 K2 O18 C37 -111.6(3) . . . . no
O16 K2 O18 C32 -143.8(4) . . . . no
O16 K2 O18 C37 -5.0(3) . . . . no
O17 K2 O18 C32 -146.2(5) . . . . no
O17 K2 O18 C37 -7.4(3) . . . . no
O19 K2 O18 C32 12.6(4) . . . . no
O19 K2 O18 C37 151.4(3) . . . . no
O20 K2 O18 C32 20.5(5) . . . . no
O20 K2 O18 C37 159.3(3) . . . . no
F41 K2 O19 C40 -86.2(3) . . . . no
F42 K2 O20 C43 -89.5(3) . . . . no
F42 K2 O20 C45 134.9(3) . . . . no
O15 K2 O20 C43 141.8(3) . . . . no
O15 K2 O20 C45 6.2(3) . . . . no
O16 K2 O20 C43 147.1(3) . . . . no
O16 K2 O20 C45 11.5(4) . . . . no
O18 K2 O20 C43 -17.1(3) . . . . no
O18 K2 O20 C45 -152.8(3) . . . . no
O19 K2 O20 C43 -9.2(3) . . . . no
O19 K2 O20 C45 -144.9(4) . . . . no
F41 K2 O20 C43 -147.3(3) . . . . no
O20 K2 O19 C40 -150.2(3) . . . . no
O20 K2 O19 C42 -24.0(4) . . . . no
F41 K2 O20 C45 77.0(3) . . . . no
K1 F4 C5 C1 167.39(19) 1_455 . . . no
K1 F4 C5 F2 -70.3(3) 1_455 . . . no
K1 F4 C5 F3 43.8(3) 1_455 . . . no
K1 F19 C10 C3 119.2(3) . . . . no
K1 F19 C10 F17 -117.2(3) . . . . no
K1 F19 C10 F18 -2.3(5) . . . . no
Ge1 O1 C1 C6 152.66(18) . . . . no
Ge1 O1 C1 C2 26.6(2) . . . . no
Ge1 O1 C1 C5 -92.6(2) . . . . no
Ge1 O2 C2 C7 153.20(19) . . . . no
Ge1 O2 C2 C1 28.8(3) . . . . no
Ge1 O2 C2 C8 -91.9(2) . . . . no
Ge1 O3 C3 C10 92.4(2) . . . . no
Ge1 O3 C3 C4 -28.3(2) . . . . no
Ge1 O3 C3 C9 -153.20(18) . . . . no
Ge1 O4 C4 C3 -27.3(3) . . . . no
Ge1 O4 C4 C11 92.3(2) . . . . no
Ge1 O4 C4 C12 -152.3(2) . . . . no
C13 O9 C24 C23 -178.8(3) . . . . no
K1 O9 C13 C14 -35.2(3) . . . . no
C24 O9 C13 C14 -177.5(3) . . . . no
K1 O9 C24 C23 40.2(3) . . . . no
K1 O10 C15 C16 55.6(3) . . . . no
C14 O10 C15 C16 175.8(3) . . . . no
C15 O10 C14 C13 174.9(3) . . . . no
K1 O10 C14 C13 -62.2(3) . . . . no
K1 O11 C16 C15 43.3(3) . . . . no
C17 O11 C16 C15 -175.9(3) . . . . no
K1 O11 C17 C18 -44.1(3) . . . . no
C16 O11 C17 C18 175.5(3) . . . . no
C19 O12 C18 C17 179.4(3) . . . . no
K1 O12 C19 C20 63.5(3) . . . . no
C18 O12 C19 C20 -168.2(3) . . . . no
K1 O12 C18 C17 -54.3(3) . . . . no
K1 O13 C20 C19 37.6(3) . . . . no
C21 O13 C20 C19 176.1(2) . . . . no
K1 O13 C21 C22 -48.5(3) . . . . no
C20 O13 C21 C22 173.6(2) . . . . no
K1 O14 C23 C24 51.3(3) . . . . no
C22 O14 C23 C24 -173.5(3) . . . . no
C23 O14 C22 C21 179.3(3) . . . . no
K1 O14 C22 C21 -46.8(3) . . . . no
K2 F41 C35 F26 -2.7(5) . . . . no
K2 F41 C35 F43 112.4(3) . . . . no
K2 F41 C35 C28 -123.1(3) . . . . no
C6 C1 C5 F3 64.7(3) . . . . no
C6 C1 C5 F4 -56.4(3) . . . . no
O1 C1 C6 F5 66.9(3) . . . . no
O1 C1 C6 F6 -51.9(3) . . . . no
O1 C1 C6 F7 -174.0(2) . . . . no
C2 C1 C6 F5 -174.1(2) . . . . no
C2 C1 C6 F6 67.1(3) . . . . no
C2 C1 C6 F7 -55.1(3) . . . . no
C5 C1 C6 F5 -46.4(3) . . . . no
C5 C1 C6 F6 -165.3(3) . . . . no
C5 C1 C6 F7 72.6(3) . . . . no
O1 C1 C5 F3 -50.1(3) . . . . no
O1 C1 C5 F4 -171.2(2) . . . . no
C2 C1 C5 F2 -46.5(3) . . . . no
C2 C1 C5 F3 -164.8(2) . . . . no
C2 C1 C5 F4 74.1(3) . . . . no
O1 C1 C2 O2 -34.3(3) . . . . no
O1 C1 C2 C7 -153.3(2) . . . . no
O1 C1 C2 C8 82.7(3) . . . . no
C5 C1 C2 O2 80.3(3) . . . . no
C5 C1 C2 C7 -38.8(3) . . . . no
C5 C1 C2 C8 -162.7(3) . . . . no
C6 C1 C2 O2 -154.4(2) . . . . no
C6 C1 C2 C7 86.6(3) . . . . no
C6 C1 C2 C8 -37.3(4) . . . . no
O1 C1 C5 F2 68.2(3) . . . . no
C6 C1 C5 F2 -177.0(3) . . . . no
O2 C2 C7 F8 -48.5(3) . . . . no
O2 C2 C7 F9 -170.4(2) . . . . no
C1 C2 C7 F8 69.8(3) . . . . no
C1 C2 C7 F9 -52.0(3) . . . . no
O2 C2 C7 F10 69.9(3) . . . . no
O2 C2 C8 F13 68.9(3) . . . . no
C1 C2 C7 F10 -171.8(2) . . . . no
C8 C2 C7 F8 -163.5(3) . . . . no
C8 C2 C7 F9 74.7(3) . . . . no
C8 C2 C7 F10 -45.1(3) . . . . no
O2 C2 C8 F11 -168.9(3) . . . . no
O2 C2 C8 F12 -48.7(3) . . . . no
C1 C2 C8 F13 -47.5(3) . . . . no
C1 C2 C8 F11 74.7(3) . . . . no
C1 C2 C8 F12 -165.1(2) . . . . no
C7 C2 C8 F13 -176.1(2) . . . . no
C7 C2 C8 F11 -53.9(3) . . . . no
C7 C2 C8 F12 66.4(3) . . . . no
O3 C3 C4 C12 155.0(2) . . . . no
C10 C3 C9 F15 43.3(3) . . . . no
C10 C3 C9 F16 162.0(3) . . . . no
C9 C3 C4 O4 153.5(2) . . . . no
C9 C3 C4 C11 38.5(3) . . . . no
C9 C3 C4 C12 -86.2(3) . . . . no
C10 C3 C4 O4 -81.1(3) . . . . no
C10 C3 C4 C11 163.9(2) . . . . no
C10 C3 C4 C12 39.3(3) . . . . no
O3 C3 C9 F14 170.6(2) . . . . no
O3 C3 C9 F15 -70.1(3) . . . . no
O3 C3 C9 F16 48.6(3) . . . . no
C4 C3 C9 F14 52.4(3) . . . . no
C4 C3 C9 F15 171.7(2) . . . . no
C4 C3 C9 F16 -69.6(3) . . . . no
C10 C3 C9 F14 -76.0(3) . . . . no
O3 C3 C4 O4 34.6(3) . . . . no
O3 C3 C4 C11 -80.4(3) . . . . no
C9 C3 C10 F17 51.3(3) . . . . no
O3 C3 C10 F17 165.4(2) . . . . no
O3 C3 C10 F18 44.5(3) . . . . no
O3 C3 C10 F19 -74.3(3) . . . . no
C4 C3 C10 F17 -78.9(3) . . . . no
C4 C3 C10 F18 160.2(2) . . . . no
C4 C3 C10 F19 41.4(3) . . . . no
C9 C3 C10 F18 -69.6(3) . . . . no
C9 C3 C10 F19 171.5(3) . . . . no
C12 C4 C11 F22 177.7(2) . . . . no
O4 C4 C11 F20 172.3(3) . . . . no
O4 C4 C11 F21 51.4(3) . . . . no
O4 C4 C11 F22 -66.4(3) . . . . no
C3 C4 C11 F20 -72.5(3) . . . . no
C3 C4 C11 F21 166.7(2) . . . . no
C3 C4 C11 F22 48.8(3) . . . . no
O4 C4 C12 F23 -75.2(3) . . . . no
O4 C4 C12 F24 51.6(9) . . . . no
O4 C4 C12 F25 172.0(4) . . . . no
C3 C4 C12 F23 165.7(2) . . . . no
C3 C4 C12 F24 -67.5(9) . . . . no
C3 C4 C12 F25 52.9(5) . . . . no
C11 C4 C12 F23 38.8(3) . . . . no
C11 C4 C12 F24 165.6(9) . . . . no
C11 C4 C12 F25 -74.0(4) . . . . no
C12 C4 C11 F21 -64.5(3) . . . . no
C12 C4 C11 F20 56.3(3) . . . . no
Ge2 O5 C30 C28 26.9(2) . . . . no
Ge2 O5 C30 C33 151.35(18) . . . . no
Ge2 O5 C30 C34 -93.4(2) . . . . no
Ge2 O6 C28 C25 153.64(18) . . . . no
Ge2 O6 C28 C30 28.1(2) . . . . no
Ge2 O6 C28 C35 -92.1(2) . . . . no
Ge2 O7 C36 C38 -30.5(2) . . . . no
Ge2 O7 C36 C47 -155.09(18) . . . . no
Ge2 O7 C36 C27 90.3(2) . . . . no
Ge2 O8 C38 C36 -27.1(3) . . . . no
Ge2 O8 C38 C44 -153.36(18) . . . . no
Ge2 O8 C38 C41 92.3(2) . . . . no
O9 C13 C14 O10 67.2(3) . . . . no
K2 O15 C46 C45 -56.1(4) . . . . no
C39 O15 C46 C45 169.0(7) . . . . no
C46 O15 C39 C26 179.1(6) . . . . no
K2 O15 C39 C26 46.6(11) . . . . no
O10 C15 C16 O11 -66.1(4) . . . . no
C26 O16 C29 C31 -177.0(5) . . . . no
K2 O16 C26 C39 49.0(6) . . . . no
C29 O16 C26 C39 -175.0(7) . . . . no
K2 O16 C29 C31 -41.1(7) . . . . no
K2 O17 C31 C29 -59.6(5) . . . . no
C48 O17 C31 C29 173.1(5) . . . . no
K2 O17 C48 C37 59.3(4) . . . . no
O11 C17 C18 O12 64.7(4) . . . . no
C31 O17 C48 C37 -173.1(4) . . . . no
K2 O18 C32 C40 -43.9(7) . . . . no
C37 O18 C32 C40 174.7(5) . . . . no
C32 O18 C37 C48 179.8(5) . . . . no
K2 O18 C37 C48 39.1(5) . . . . no
C42 O19 C40 C32 179.5(6) . . . . no
K2 O19 C42 C43 55.0(6) . . . . no
O12 C19 C20 O13 -68.2(3) . . . . no
K2 O19 C40 C32 -53.4(5) . . . . no
C40 O19 C42 C43 -177.6(5) . . . . no
K2 O20 C43 C42 39.5(5) . . . . no
C45 O20 C43 C42 177.9(5) . . . . no
C43 O20 C45 C46 -174.0(4) . . . . no
K2 O20 C45 C46 -35.8(5) . . . . no
O13 C21 C22 O14 61.9(3) . . . . no
O14 C23 C24 O9 -59.9(3) . . . . no
F27 C25 C28 O6 67.4(3) . . . . no
F27 C25 C28 C30 -173.7(2) . . . . no
F27 C25 C28 C35 -45.7(3) . . . . no
F28 C25 C28 O6 -51.6(3) . . . . no
F28 C25 C28 C30 67.3(3) . . . . no
F28 C25 C28 C35 -164.7(2) . . . . no
F29 C25 C28 O6 -172.9(2) . . . . no
F29 C25 C28 C30 -54.0(3) . . . . no
F29 C25 C28 C35 74.0(3) . . . . no
O16 C26 C39 O15 -62.6(10) . . . . no
F31 C27 C36 O7 48.7(3) . . . . no
F31 C27 C36 C38 164.8(2) . . . . no
F31 C27 C36 C47 -66.4(3) . . . . no
F49 C27 C36 O7 169.1(2) . . . . no
F49 C27 C36 C38 -74.8(3) . . . . no
F49 C27 C36 C47 54.0(3) . . . . no
F50 C27 C36 O7 -70.2(3) . . . . no
F50 C27 C36 C38 45.9(3) . . . . no
F50 C27 C36 C47 174.8(2) . . . . no
O6 C28 C30 O5 -34.3(2) . . . . no
O6 C28 C30 C33 -153.4(2) . . . . no
O6 C28 C30 C34 81.7(3) . . . . no
C25 C28 C30 O5 -154.2(2) . . . . no
C25 C28 C30 C33 86.7(3) . . . . no
C25 C28 C30 C34 -38.2(3) . . . . no
C35 C28 C30 O5 80.7(3) . . . . no
C35 C28 C30 C33 -38.4(3) . . . . no
C35 C28 C30 C34 -163.4(2) . . . . no
O6 C28 C35 F26 -49.4(3) . . . . no
O6 C28 C35 F41 68.3(3) . . . . no
O6 C28 C35 F43 -170.0(2) . . . . no
C25 C28 C35 F26 65.3(3) . . . . no
C25 C28 C35 F41 -177.0(2) . . . . no
C25 C28 C35 F43 -55.3(3) . . . . no
C30 C28 C35 F26 -164.7(2) . . . . no
C30 C28 C35 F41 -47.0(3) . . . . no
C30 C28 C35 F43 74.8(3) . . . . no
O16 C29 C31 O17 67.4(7) . . . . no
O5 C30 C33 F33 68.6(3) . . . . no
O5 C30 C33 F35 -172.4(2) . . . . no
O5 C30 C33 F40 -50.1(3) . . . . no
C28 C30 C33 F33 -172.9(2) . . . . no
C28 C30 C33 F35 -53.8(3) . . . . no
C28 C30 C33 F40 68.4(3) . . . . no
C34 C30 C33 F33 -45.4(3) . . . . no
C34 C30 C33 F35 73.6(3) . . . . no
C34 C30 C33 F40 -164.2(3) . . . . no
O5 C30 C34 F44 67.2(3) . . . . no
O5 C30 C34 F45 -170.7(2) . . . . no
O5 C30 C34 F46 -50.5(3) . . . . no
C28 C30 C34 F44 -48.9(3) . . . . no
C28 C30 C34 F45 73.3(3) . . . . no
C28 C30 C34 F46 -166.5(2) . . . . no
C33 C30 C34 F44 -178.0(2) . . . . no
C33 C30 C34 F45 -55.8(3) . . . . no
C33 C30 C34 F46 64.4(3) . . . . no
O18 C32 C40 O19 64.8(7) . . . . no
O7 C36 C38 O8 36.0(3) . . . . no
O7 C36 C38 C41 -78.8(3) . . . . no
O7 C36 C38 C44 155.5(2) . . . . no
C27 C36 C38 O8 -80.8(3) . . . . no
C27 C36 C38 C41 164.4(2) . . . . no
C27 C36 C38 C44 38.6(3) . . . . no
C47 C36 C38 O8 155.2(2) . . . . no
C47 C36 C38 C41 40.4(3) . . . . no
C47 C36 C38 C44 -85.4(3) . . . . no
O7 C36 C47 F39 171.1(2) . . . . no
O7 C36 C47 F47 49.6(3) . . . . no
O7 C36 C47 F48 -69.3(3) . . . . no
C27 C36 C47 F39 -74.2(3) . . . . no
C27 C36 C47 F47 164.3(3) . . . . no
C27 C36 C47 F48 45.4(3) . . . . no
C38 C36 C47 F39 52.9(3) . . . . no
C38 C36 C47 F47 -68.6(3) . . . . no
C38 C36 C47 F48 172.5(2) . . . . no
O18 C37 C48 O17 -65.2(5) . . . . no
O8 C38 C41 F30 51.5(3) . . . . no
O8 C38 C41 F32 172.2(2) . . . . no
O8 C38 C41 F36 -66.6(3) . . . . no
C36 C38 C41 F30 166.8(2) . . . . no
C36 C38 C41 F32 -72.5(3) . . . . no
C36 C38 C41 F36 48.6(3) . . . . no
C44 C38 C41 F30 -62.2(3) . . . . no
C44 C38 C41 F32 58.5(3) . . . . no
C44 C38 C41 F36 179.6(2) . . . . no
O8 C38 C44 F34 56.2(3) . . . . no
O8 C38 C44 F37 -62.8(3) . . . . no
O8 C38 C44 F38 177.2(2) . . . . no
C36 C38 C44 F34 -63.0(3) . . . . no
C36 C38 C44 F37 178.0(2) . . . . no
C36 C38 C44 F38 58.1(3) . . . . no
C41 C38 C44 F34 169.1(2) . . . . no
C41 C38 C44 F37 50.1(3) . . . . no
C41 C38 C44 F38 -69.9(3) . . . . no
O19 C42 C43 O20 -63.3(6) . . . . no
O20 C45 C46 O15 61.5(5) . . . . no
