#------------------------------------------------------------------------------
#$Date: 2025-04-05 06:24:55 +0300 (Sat, 05 Apr 2025) $
#$Revision: 298948 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/71/75/7717585.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7717585
loop_
_publ_author_name
'Kim, Soyeon'
'You, Dong Kyun'
'Kim, Namkyun'
'Shin, Ilsup'
'Kim, Dongwook'
'Lee, Kang Mun'
_publ_section_title
;
 Modulating radiative efficiency in ortho-carboranyl luminophores
 through electron-donating substituents: insights from
 intramolecular-charge-transfer-based emissions.
;
_journal_issue                   3
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1164
_journal_page_last               1172
_journal_paper_doi               10.1039/d4dt02897j
_journal_volume                  54
_journal_year                    2025
_chemical_formula_moiety         'C23 H38 B10 Si'
_chemical_formula_sum            'C23 H38 B10 Si'
_chemical_formula_weight         450.72
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_audit_block_doi                 10.5517/ccdc.csd.cc2l61yt
_audit_creation_method           SHELXL-2019/3
_audit_update_record
;
2024-10-07 deposited with the CCDC.	2024-11-25 downloaded from the CCDC.
;
_cell_angle_alpha                95.7529(18)
_cell_angle_beta                 90.2216(19)
_cell_angle_gamma                105.5694(16)
_cell_formula_units_Z            4
_cell_length_a                   11.0532(6)
_cell_length_b                   13.0146(6)
_cell_length_c                   19.2255(9)
_cell_measurement_reflns_used    9016
_cell_measurement_temperature    203(2)
_cell_measurement_theta_max      25.53
_cell_measurement_theta_min      2.82
_cell_volume                     2649.4(2)
_computing_cell_refinement       'Bruker APEX5 software'
_computing_data_collection       'Bruker APEX5 software'
_computing_data_reduction        'Bruker APEX5 software'
_computing_molecular_graphics    ORTEP
_computing_publication_material  CIFTAB
_computing_structure_refinement  'SHELXL-2019/2 (Sheldrick, 2019)'
_computing_structure_solution    'SHELXS-2013/1 (Sheldrick, 2013)'
_diffrn_ambient_temperature      203(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'PHOTON II CPAD detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1150
_diffrn_reflns_av_unetI/netI     0.0806
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            49407
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.583
_diffrn_reflns_theta_min         2.452
_diffrn_source                   'Ius 3.0 microfocus source'
_exptl_absorpt_coefficient_mu    0.100
_exptl_absorpt_correction_T_max  0.7452
_exptl_absorpt_correction_T_min  0.6893
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.130
_exptl_crystal_description       block
_exptl_crystal_F_000             960
_exptl_crystal_size_max          0.083
_exptl_crystal_size_mid          0.061
_exptl_crystal_size_min          0.032
_refine_diff_density_max         0.216
_refine_diff_density_min         -0.329
_refine_diff_density_rms         0.047
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.047
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     663
_refine_ls_number_reflns         9913
_refine_ls_number_restraints     128
_refine_ls_restrained_S_all      1.050
_refine_ls_R_factor_all          0.1236
_refine_ls_R_factor_gt           0.0649
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0447P)²+1.1797P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1260
_refine_ls_wR_factor_ref         0.1526
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6003
_reflns_number_total             9913
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d4dt02897j2.cif
_cod_data_source_block           4CE
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'MULTI-SCAN' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 

 Adding full bibliography for 7717582--7717587.cif.
;
_cod_database_code               7717585
_shelx_shelxl_version_number     2019/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.992
_shelx_estimated_absorpt_t_max   0.997
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C2 C 0.3305(3) 0.5999(2) 0.89280(14) 0.0306(6) Uani 1 1 d . . . . .
B2 B 0.4416(3) 0.8186(3) 0.92230(17) 0.0347(7) Uani 1 1 d . . . . .
H2 H 0.360968 0.836396 0.951583 0.042 Uiso 1 1 calc R U . . .
C1 C 0.2104(2) 0.6016(2) 0.87075(14) 0.0311(6) Uani 1 1 d . . . . .
H1A H 0.199019 0.661942 0.850265 0.037 Uiso 1 1 calc R U . . .
B1 B 0.5397(3) 0.7468(3) 0.95740(18) 0.0374(8) Uani 1 1 d . . . . .
H1 H 0.524027 0.716896 1.010153 0.045 Uiso 1 1 calc R U . . .
C3 C 0.3443(3) 0.5126(2) 0.92583(15) 0.0351(7) Uani 1 1 d . . . . .
H3A H 0.425403 0.512022 0.942080 0.042 Uiso 1 1 calc R U . . .
B3 B 0.6008(3) 0.8852(3) 0.94740(18) 0.0414(8) Uani 1 1 d . . . . .
H3 H 0.626172 0.947673 0.993446 0.050 Uiso 1 1 calc R U . . .
C4 C 0.2418(3) 0.4266(2) 0.93536(15) 0.0378(7) Uani 1 1 d . . . . .
H4A H 0.252474 0.367873 0.958020 0.045 Uiso 1 1 calc R U . . .
B4 B 0.6929(3) 0.7932(3) 0.92551(18) 0.0395(8) Uani 1 1 d . . . . .
H4 H 0.778755 0.794191 0.956959 0.047 Uiso 1 1 calc R U . . .
C5 C -0.0355(3) 0.2534(2) 0.94273(15) 0.0420(7) Uani 1 1 d . . . . .
H5A H 0.024961 0.226228 0.964598 0.050 Uiso 1 1 calc R U . . .
B5 B 0.5896(3) 0.6720(3) 0.88643(17) 0.0335(7) Uani 1 1 d . . . . .
H5 H 0.605327 0.591527 0.891490 0.040 Uiso 1 1 calc R U . . .
C6 C -0.1610(3) 0.1970(3) 0.93852(16) 0.0490(9) Uani 1 1 d . . . . .
H6A H -0.186861 0.130068 0.957370 0.059 Uiso 1 1 calc R U . . .
B6 B 0.4335(3) 0.7866(2) 0.82961(16) 0.0318(7) Uani 1 1 d . . . . .
H6 H 0.347173 0.781464 0.797290 0.038 Uiso 1 1 calc R U . . .
C7 C -0.2497(3) 0.2366(3) 0.90727(18) 0.0569(10) Uani 1 1 d . . . . .
H7A H -0.335578 0.196754 0.904943 0.068 Uiso 1 1 calc R U . . .
B7 B 0.5340(3) 0.9098(3) 0.86826(18) 0.0372(8) Uani 1 1 d . . . . .
H7 H 0.514249 0.988424 0.861856 0.045 Uiso 1 1 calc R U . . .
C8 C -0.2140(3) 0.3344(3) 0.87925(18) 0.0521(9) Uani 1 1 d . . . . .
H8A H -0.274930 0.361901 0.858121 0.063 Uiso 1 1 calc R U . . .
B8 B 0.6898(3) 0.8958(3) 0.87073(18) 0.0395(8) Uani 1 1 d . . . . .
H8 H 0.773841 0.965320 0.866243 0.047 Uiso 1 1 calc R U . . .
C9 C -0.0280(3) 0.4989(2) 0.85574(15) 0.0335(6) Uani 1 1 d . . . . .
B9 B 0.6832(3) 0.7636(3) 0.83316(18) 0.0351(7) Uani 1 1 d . . . . .
H9 H 0.762791 0.744795 0.803363 0.042 Uiso 1 1 calc R U . . .
C10 C 0.1087(3) 0.5157(2) 0.87874(14) 0.0311(6) Uani 1 1 d . . . . .
B10 B 0.5869(3) 0.8358(2) 0.79852(18) 0.0340(7) Uani 1 1 d . . . . .
H10 H 0.602838 0.865539 0.745727 0.041 Uiso 1 1 calc R U . . .
C11 C 0.1237(3) 0.4277(2) 0.91135(14) 0.0324(6) Uani 1 1 d . . . . .
C12 C 0.0003(3) 0.3509(2) 0.91414(14) 0.0349(7) Uani 1 1 d . . . . .
C13 C -0.0884(3) 0.3912(2) 0.88261(15) 0.0362(7) Uani 1 1 d . . . . .
C14 C 0.4426(2) 0.6936(2) 0.88588(14) 0.0291(6) Uani 1 1 d . . . . .
C15 C 0.5285(3) 0.7028(2) 0.81084(14) 0.0299(6) Uani 1 1 d . . . . .
C26 C -0.0828(3) 0.5876(2) 0.88847(17) 0.0435(7) Uani 1 1 d . . . . .
H26A H -0.172143 0.570781 0.875065 0.065 Uiso 1 1 calc R U . . .
H26B H -0.038140 0.656033 0.871841 0.065 Uiso 1 1 calc R U . . .
H26C H -0.073271 0.593112 0.939517 0.065 Uiso 1 1 calc R U . . .
C27 C -0.0410(3) 0.4900(2) 0.77545(15) 0.0426(7) Uani 1 1 d . . . . .
H27A H -0.130189 0.469017 0.761216 0.064 Uiso 1 1 calc R U . . .
H27B H -0.001000 0.435887 0.754888 0.064 Uiso 1 1 calc R U . . .
H27C H 0.000025 0.559554 0.759126 0.064 Uiso 1 1 calc R U . . .
Si28 Si 0.49047(8) 0.59680(6) 0.72945(4) 0.0332(2) Uani 1 1 d . . . . .
C29 C 0.5785(3) 0.4943(3) 0.73941(17) 0.0497(8) Uani 1 1 d . . . . .
H29A H 0.603290 0.470152 0.692461 0.060 Uiso 1 1 calc R U . . .
H29B H 0.656587 0.529498 0.767420 0.060 Uiso 1 1 calc R U . . .
C30 C 0.5082(4) 0.3959(3) 0.7735(2) 0.0668(11) Uani 1 1 d . . . . .
H30A H 0.562052 0.347485 0.776066 0.100 Uiso 1 1 calc R U . . .
H30B H 0.431728 0.358762 0.745722 0.100 Uiso 1 1 calc R U . . .
H30C H 0.485698 0.418072 0.820860 0.100 Uiso 1 1 calc R U . . .
C31 C 0.5495(3) 0.6694(3) 0.65165(15) 0.0415(7) Uani 1 1 d . . . . .
H31A H 0.633599 0.718525 0.664266 0.050 Uiso 1 1 calc R U . . .
H31B H 0.560355 0.615942 0.613480 0.050 Uiso 1 1 calc R U . . .
C32 C 0.4678(3) 0.7344(3) 0.62319(17) 0.0514(9) Uani 1 1 d . . . . .
H32A H 0.507820 0.768892 0.582977 0.077 Uiso 1 1 calc R U . . .
H32B H 0.458023 0.789494 0.659777 0.077 Uiso 1 1 calc R U . . .
H32C H 0.384956 0.686710 0.608560 0.077 Uiso 1 1 calc R U . . .
C33 C 0.3180(3) 0.5325(2) 0.71693(16) 0.0428(7) Uani 1 1 d . . . . .
H33A H 0.288149 0.489722 0.756305 0.051 Uiso 1 1 calc R U . . .
H33B H 0.273237 0.589056 0.717462 0.051 Uiso 1 1 calc R U . . .
C34 C 0.2864(4) 0.4594(3) 0.64772(17) 0.0586(10) Uani 1 1 d . . . . .
H34A H 0.195328 0.427513 0.643028 0.088 Uiso 1 1 calc R U . . .
H34B H 0.328999 0.402387 0.647444 0.088 Uiso 1 1 calc R U . . .
H34C H 0.314548 0.501771 0.608563 0.088 Uiso 1 1 calc R U . . .
C41 C 0.8454(3) 1.0730(2) 0.38216(14) 0.0298(6) Uani 1 1 d . . . . .
C42 C 0.9200(3) 1.0831(2) 0.30322(14) 0.0316(6) Uani 1 1 d . . . . .
B43 B 0.9944(3) 1.0565(3) 0.37549(17) 0.0342(7) Uani 1 1 d . . . . .
H43 H 1.015611 0.977733 0.379268 0.041 Uiso 1 1 calc R U . . .
B44 B 0.9506(3) 1.1298(3) 0.44888(17) 0.0374(8) Uani 1 1 d . . . . .
H44 H 0.944190 1.100644 0.501953 0.045 Uiso 1 1 calc R U . . .
B45 B 0.8431(3) 1.1972(3) 0.41940(17) 0.0347(7) Uani 1 1 d . . . . .
H45 H 0.765427 1.212975 0.452413 0.042 Uiso 1 1 calc R U . . .
B46 B 0.8237(3) 1.1634(3) 0.32691(16) 0.0328(7) Uani 1 1 d . . . . .
H46 H 0.732472 1.154866 0.298283 0.039 Uiso 1 1 calc R U . . .
B47 B 0.9696(3) 1.2161(3) 0.28936(18) 0.0366(8) Uani 1 1 d . . . . .
H47 H 0.975995 1.244975 0.236184 0.044 Uiso 1 1 calc R U . . .
B48 B 0.9228(3) 1.2892(3) 0.36206(18) 0.0380(8) Uani 1 1 d . . . . .
H48 H 0.897565 1.366096 0.357486 0.046 Uiso 1 1 calc R U . . .
B49 B 1.0040(3) 1.2680(3) 0.43766(18) 0.0416(8) Uani 1 1 d . . . . .
H49 H 1.033741 1.330993 0.483136 0.050 Uiso 1 1 calc R U . . .
B50 B 1.0972(3) 1.1797(3) 0.41034(18) 0.0396(8) Uani 1 1 d . . . . .
H50 H 1.188369 1.183967 0.437659 0.048 Uiso 1 1 calc R U . . .
B51 B 1.0753(3) 1.1483(3) 0.31848(18) 0.0369(8) Uani 1 1 d . . . . .
H51 H 1.151660 1.131444 0.284798 0.044 Uiso 1 1 calc R U . . .
B52 B 1.0807(3) 1.2804(3) 0.35674(18) 0.0398(8) Uani 1 1 d . . . . .
H52 H 1.160449 1.351838 0.348777 0.048 Uiso 1 1 calc R U . . .
C53 C 0.5160(3) 0.8894(2) 0.38613(14) 0.0324(6) Uani 1 1 d . . . . .
C54 C 0.6141(3) 0.9766(2) 0.37539(14) 0.0317(6) Uani 1 1 d . . . . .
H54 H 0.597988 1.036357 0.356316 0.038 Uiso 1 1 calc R U . . .
C55 C 0.7372(3) 0.9774(2) 0.39243(13) 0.0301(6) Uani 1 1 d . . . . .
C56 C 0.7585(3) 0.8911(2) 0.42329(14) 0.0349(7) Uani 1 1 d . . . . .
H56 H 0.841841 0.892131 0.436276 0.042 Uiso 1 1 calc R U . . .
C57 C 0.6597(3) 0.8035(2) 0.43537(15) 0.0389(7) Uani 1 1 d . . . . .
H57 H 0.675284 0.745101 0.456410 0.047 Uiso 1 1 calc R U . . .
C58 C 0.5387(3) 0.8024(2) 0.41643(14) 0.0344(7) Uani 1 1 d . . . . .
C59 C 0.4186(3) 0.7216(2) 0.42096(14) 0.0387(7) Uani 1 1 d . . . . .
C60 C 0.3909(3) 0.6223(2) 0.44752(16) 0.0485(8) Uani 1 1 d . . . . .
H60 H 0.455656 0.597138 0.466668 0.058 Uiso 1 1 calc R U . . .
C61 C 0.2675(4) 0.5613(3) 0.44536(17) 0.0566(10) Uani 1 1 d . . . . .
H61 H 0.247086 0.493591 0.463338 0.068 Uiso 1 1 calc R U . . .
C62 C 0.1729(4) 0.5978(3) 0.41725(18) 0.0604(10) Uani 1 1 d . . . . .
H62 H 0.088622 0.554313 0.415713 0.072 Uiso 1 1 calc R U . . .
C63 C 0.1997(3) 0.6970(3) 0.39131(18) 0.0524(9) Uani 1 1 d . . . . .
H63 H 0.134448 0.721997 0.372542 0.063 Uiso 1 1 calc R U . . .
C64 C 0.3238(3) 0.7592(2) 0.39334(15) 0.0417(7) Uani 1 1 d . . . . .
C65 C 0.3764(3) 0.8702(2) 0.36925(15) 0.0383(7) Uani 1 1 d . . . . .
C66 C 0.3233(3) 0.9544(3) 0.41053(19) 0.0520(9) Uani 1 1 d . . . . .
H66A H 0.232437 0.936943 0.401375 0.078 Uiso 1 1 calc R U . . .
H66B H 0.363410 1.025341 0.395981 0.078 Uiso 1 1 calc R U . . .
H66C H 0.340280 0.954693 0.460633 0.078 Uiso 1 1 calc R U . . .
C67 C 0.3526(3) 0.8693(3) 0.29014(17) 0.0509(8) Uani 1 1 d . . . . .
H67A H 0.261932 0.849169 0.279707 0.076 Uiso 1 1 calc R U . . .
H67B H 0.390070 0.817169 0.264426 0.076 Uiso 1 1 calc R U . . .
H67C H 0.390726 0.940819 0.275951 0.076 Uiso 1 1 calc R U . . .
Si68 Si 0.87845(9) 0.97505(7) 0.22333(4) 0.0436(2) Uani 1 1 d D . . . .
C69 C 0.7063(3) 0.9115(3) 0.21501(17) 0.0545(9) Uani 1 1 d . . . . .
H69A H 0.679797 0.870421 0.255547 0.065 Uiso 1 1 calc R U . . .
H69B H 0.662000 0.968416 0.216381 0.065 Uiso 1 1 calc R U . . .
C70 C 0.6667(4) 0.8359(3) 0.14725(19) 0.0811(14) Uani 1 1 d . . . . .
H70A H 0.576798 0.799634 0.147778 0.122 Uiso 1 1 calc R U . . .
H70B H 0.714699 0.782357 0.143854 0.122 Uiso 1 1 calc R U . . .
H70C H 0.683516 0.877543 0.106928 0.122 Uiso 1 1 calc R U . . .
C71 C 0.9751(5) 0.8797(3) 0.2306(2) 0.0636(13) Uani 0.870(6) 1 d D U P A 1
H71A H 0.994076 0.853799 0.182783 0.076 Uiso 0.870(6) 1 calc R U P A 1
H71B H 1.055957 0.919420 0.254579 0.076 Uiso 0.870(6) 1 calc R U P A 1
C72 C 0.9171(5) 0.7822(4) 0.2694(3) 0.0801(16) Uani 0.870(6) 1 d D U P A 1
H72A H 0.976987 0.738997 0.271784 0.120 Uiso 0.870(6) 1 calc R U P A 1
H72B H 0.840029 0.738789 0.244357 0.120 Uiso 0.870(6) 1 calc R U P A 1
H72C H 0.897194 0.806197 0.316835 0.120 Uiso 0.870(6) 1 calc R U P A 1
C73 C 0.9444(11) 1.0351(9) 0.1449(6) 0.059(3) Uani 0.600(7) 1 d D U P A 1
H73A H 1.027546 1.086065 0.157053 0.071 Uiso 0.600(7) 1 calc R U P A 1
H73B H 0.956721 0.978066 0.109725 0.071 Uiso 0.600(7) 1 calc R U P A 1
C74 C 0.8584(6) 1.0943(5) 0.1130(3) 0.068(2) Uani 0.600(7) 1 d D U P A 1
H74A H 0.898584 1.128390 0.072684 0.102 Uiso 0.600(7) 1 calc R U P A 1
H74B H 0.843774 1.149281 0.148131 0.102 Uiso 0.600(7) 1 calc R U P A 1
H74C H 0.778008 1.043079 0.097836 0.102 Uiso 0.600(7) 1 calc R U P A 1
C71B C 0.895(3) 0.8446(17) 0.2479(16) 0.057(4) Uani 0.130(6) 1 d D U P A 2
H71C H 0.856895 0.831939 0.293769 0.069 Uiso 0.130(6) 1 calc R U P A 2
H71D H 0.847553 0.786504 0.213013 0.069 Uiso 0.130(6) 1 calc R U P A 2
C72B C 1.032(2) 0.838(3) 0.2524(16) 0.063(6) Uani 0.130(6) 1 d D U P A 2
H72D H 1.033665 0.762890 0.241146 0.095 Uiso 0.130(6) 1 calc R U P A 2
H72E H 1.066579 0.863291 0.299890 0.095 Uiso 0.130(6) 1 calc R U P A 2
H72F H 1.082144 0.882062 0.219039 0.095 Uiso 0.130(6) 1 calc R U P A 2
C73B C 0.9236(17) 1.0625(11) 0.1468(7) 0.046(3) Uani 0.400(7) 1 d D U P A 2
H73C H 0.859723 1.102608 0.142917 0.055 Uiso 0.400(7) 1 calc R U P A 2
H73D H 1.004565 1.116140 0.159983 0.055 Uiso 0.400(7) 1 calc R U P A 2
C74B C 0.9365(9) 1.0077(8) 0.0739(4) 0.061(3) Uani 0.400(7) 1 d D U P A 2
H74D H 0.964476 1.062225 0.041437 0.091 Uiso 0.400(7) 1 calc R U P A 2
H74E H 0.855016 0.959487 0.057313 0.091 Uiso 0.400(7) 1 calc R U P A 2
H74F H 0.998273 0.966311 0.076232 0.091 Uiso 0.400(7) 1 calc R U P A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 C2 C3 119.1(2) . . ?
C1 C2 C14 120.9(2) . . ?
C3 C2 C14 119.9(2) . . ?
C14 B2 B7 106.0(2) . . ?
C14 B2 B1 58.63(17) . . ?
B7 B2 B1 107.9(2) . . ?
C14 B2 B3 105.6(2) . . ?
B7 B2 B3 60.27(19) . . ?
B1 B2 B3 59.86(19) . . ?
C14 B2 B6 59.10(16) . . ?
B7 B2 B6 59.93(18) . . ?
B1 B2 B6 107.3(2) . . ?
B3 B2 B6 107.8(2) . . ?
C14 B2 H2 123.8 . . ?
B7 B2 H2 121.9 . . ?
B1 B2 H2 122.0 . . ?
B3 B2 H2 122.1 . . ?
B6 B2 H2 121.8 . . ?
C10 C1 C2 119.9(2) . . ?
C10 C1 H1A 120.0 . . ?
C2 C1 H1A 120.0 . . ?
C14 B1 B4 106.4(2) . . ?
C14 B1 B5 59.23(17) . . ?
B4 B1 B5 60.03(19) . . ?
C14 B1 B3 105.8(2) . . ?
B4 B1 B3 60.6(2) . . ?
B5 B1 B3 108.1(2) . . ?
C14 B1 B2 58.60(17) . . ?
B4 B1 B2 108.6(2) . . ?
B5 B1 B2 107.5(2) . . ?
B3 B1 B2 60.11(19) . . ?
C14 B1 H1 123.8 . . ?
B4 B1 H1 121.5 . . ?
B5 B1 H1 121.7 . . ?
B3 B1 H1 121.9 . . ?
B2 B1 H1 121.7 . . ?
C4 C3 C2 121.3(3) . . ?
C4 C3 H3A 119.4 . . ?
C2 C3 H3A 119.4 . . ?
B8 B3 B1 107.9(3) . . ?
B8 B3 B2 108.0(2) . . ?
B1 B3 B2 60.03(19) . . ?
B8 B3 B7 60.1(2) . . ?
B1 B3 B7 107.5(2) . . ?
B2 B3 B7 59.58(18) . . ?
B8 B3 B4 60.3(2) . . ?
B1 B3 B4 59.6(2) . . ?
B2 B3 B4 107.8(2) . . ?
B7 B3 B4 108.0(2) . . ?
B8 B3 H3 121.5 . . ?
B1 B3 H3 122.0 . . ?
B2 B3 H3 121.9 . . ?
B7 B3 H3 122.0 . . ?
B4 B3 H3 121.8 . . ?
C11 C4 C3 119.1(3) . . ?
C11 C4 H4A 120.4 . . ?
C3 C4 H4A 120.4 . . ?
B1 B4 B5 59.99(19) . . ?
B1 B4 B9 107.8(2) . . ?
B5 B4 B9 59.83(18) . . ?
B1 B4 B8 107.3(2) . . ?
B5 B4 B8 107.5(2) . . ?
B9 B4 B8 59.94(19) . . ?
B1 B4 B3 59.8(2) . . ?
B5 B4 B3 107.5(2) . . ?
B9 B4 B3 107.3(2) . . ?
B8 B4 B3 59.3(2) . . ?
B1 B4 H4 121.8 . . ?
B5 B4 H4 121.9 . . ?
B9 B4 H4 121.9 . . ?
B8 B4 H4 122.2 . . ?
B3 B4 H4 122.2 . . ?
C6 C5 C12 118.5(3) . . ?
C6 C5 H5A 120.8 . . ?
C12 C5 H5A 120.8 . . ?
C14 B5 C15 60.09(16) . . ?
C14 B5 B9 106.6(2) . . ?
C15 B5 B9 58.63(17) . . ?
C14 B5 B1 58.54(18) . . ?
C15 B5 B1 107.0(2) . . ?
B9 B5 B1 108.0(2) . . ?
C14 B5 B4 105.8(2) . . ?
C15 B5 B4 106.3(2) . . ?
B9 B5 B4 60.13(19) . . ?
B1 B5 B4 59.97(19) . . ?
C14 B5 H5 123.0 . . ?
C15 B5 H5 122.6 . . ?
B9 B5 H5 122.1 . . ?
B1 B5 H5 122.0 . . ?
B4 B5 H5 122.6 . . ?
C5 C6 C7 121.0(3) . . ?
C5 C6 H6A 119.5 . . ?
C7 C6 H6A 119.5 . . ?
C15 B6 C14 60.16(16) . . ?
C15 B6 B10 58.91(17) . . ?
C14 B6 B10 106.5(2) . . ?
C15 B6 B7 106.0(2) . . ?
C14 B6 B7 105.1(2) . . ?
B10 B6 B7 59.66(18) . . ?
C15 B6 B2 106.9(2) . . ?
C14 B6 B2 58.23(17) . . ?
B10 B6 B2 107.5(2) . . ?
B7 B6 B2 59.62(18) . . ?
C15 B6 H6 122.5 . . ?
C14 B6 H6 123.3 . . ?
B10 B6 H6 122.2 . . ?
B7 B6 H6 123.1 . . ?
B2 B6 H6 122.3 . . ?
C6 C7 C8 120.5(3) . . ?
C6 C7 H7A 119.8 . . ?
C8 C7 H7A 119.8 . . ?
B10 B7 B2 108.5(2) . . ?
B10 B7 B6 60.07(18) . . ?
B2 B7 B6 60.44(18) . . ?
B10 B7 B8 59.79(19) . . ?
B2 B7 B8 108.0(2) . . ?
B6 B7 B8 107.8(2) . . ?
B10 B7 B3 107.6(2) . . ?
B2 B7 B3 60.14(19) . . ?
B6 B7 B3 108.1(2) . . ?
B8 B7 B3 59.6(2) . . ?
B10 B7 H7 121.7 . . ?
B2 B7 H7 121.3 . . ?
B6 B7 H7 121.5 . . ?
B8 B7 H7 122.0 . . ?
B3 B7 H7 121.9 . . ?
C13 C8 C7 119.1(3) . . ?
C13 C8 H8A 120.5 . . ?
C7 C8 H8A 120.5 . . ?
B10 B8 B3 108.1(2) . . ?
B10 B8 B9 59.67(18) . . ?
B3 B8 B9 107.9(2) . . ?
B10 B8 B7 59.67(19) . . ?
B3 B8 B7 60.3(2) . . ?
B9 B8 B7 107.3(2) . . ?
B10 B8 B4 107.6(2) . . ?
B3 B8 B4 60.4(2) . . ?
B9 B8 B4 59.64(19) . . ?
B7 B8 B4 108.1(2) . . ?
B10 B8 H8 122.0 . . ?
B3 B8 H8 121.4 . . ?
B9 B8 H8 122.2 . . ?
B7 B8 H8 121.9 . . ?
B4 B8 H8 121.7 . . ?
C13 C9 C10 100.7(2) . . ?
C13 C9 C26 112.2(2) . . ?
C10 C9 C26 112.3(2) . . ?
C13 C9 C27 110.7(2) . . ?
C10 C9 C27 110.5(2) . . ?
C26 C9 C27 110.1(2) . . ?
C15 B9 B10 59.20(17) . . ?
C15 B9 B5 59.45(17) . . ?
B10 B9 B5 107.8(2) . . ?
C15 B9 B4 106.9(2) . . ?
B10 B9 B4 108.3(2) . . ?
B5 B9 B4 60.04(19) . . ?
C15 B9 B8 106.3(2) . . ?
B10 B9 B8 59.80(19) . . ?
B5 B9 B8 108.0(2) . . ?
B4 B9 B8 60.41(19) . . ?
C15 B9 H9 123.1 . . ?
B10 B9 H9 121.7 . . ?
B5 B9 H9 121.7 . . ?
B4 B9 H9 121.6 . . ?
B8 B9 H9 122.0 . . ?
C1 C10 C11 120.6(3) . . ?
C1 C10 C9 128.6(2) . . ?
C11 C10 C9 110.8(2) . . ?
C15 B10 B9 58.86(17) . . ?
C15 B10 B7 106.5(2) . . ?
B9 B10 B7 108.7(2) . . ?
C15 B10 B8 106.6(2) . . ?
B9 B10 B8 60.53(19) . . ?
B7 B10 B8 60.5(2) . . ?
C15 B10 B6 59.04(17) . . ?
B9 B10 B6 107.6(2) . . ?
B7 B10 B6 60.27(18) . . ?
B8 B10 B6 108.6(2) . . ?
C15 B10 H10 123.5 . . ?
B9 B10 H10 121.6 . . ?
B7 B10 H10 121.5 . . ?
B8 B10 H10 121.4 . . ?
B6 B10 H10 121.7 . . ?
C4 C11 C10 119.9(3) . . ?
C4 C11 C12 131.6(3) . . ?
C10 C11 C12 108.4(2) . . ?
C13 C12 C5 120.8(3) . . ?
C13 C12 C11 108.4(2) . . ?
C5 C12 C11 130.8(3) . . ?
C8 C13 C12 120.2(3) . . ?
C8 C13 C9 128.3(3) . . ?
C12 C13 C9 111.6(2) . . ?
C2 C14 B2 119.7(2) . . ?
C2 C14 B1 119.0(2) . . ?
B2 C14 B1 62.76(18) . . ?
C2 C14 B5 118.3(2) . . ?
B2 C14 B5 113.3(2) . . ?
B1 C14 B5 62.24(19) . . ?
C2 C14 B6 119.6(2) . . ?
B2 C14 B6 62.68(17) . . ?
B1 C14 B6 113.5(2) . . ?
B5 C14 B6 111.3(2) . . ?
C2 C14 C15 121.3(2) . . ?
B2 C14 C15 110.1(2) . . ?
B1 C14 C15 110.0(2) . . ?
B5 C14 C15 60.12(16) . . ?
B6 C14 C15 59.82(16) . . ?
B9 C15 B10 61.93(18) . . ?
B9 C15 B6 112.6(2) . . ?
B10 C15 B6 62.05(18) . . ?
B9 C15 C14 108.9(2) . . ?
B10 C15 C14 108.8(2) . . ?
B6 C15 C14 60.02(16) . . ?
B9 C15 B5 61.93(18) . . ?
B10 C15 B5 112.0(2) . . ?
B6 C15 B5 111.1(2) . . ?
C14 C15 B5 59.79(16) . . ?
B9 C15 Si28 118.1(2) . . ?
B10 C15 Si28 118.86(18) . . ?
B6 C15 Si28 120.11(18) . . ?
C14 C15 Si28 124.08(17) . . ?
B5 C15 Si28 119.54(19) . . ?
C9 C26 H26A 109.5 . . ?
C9 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C9 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C9 C27 H27A 109.5 . . ?
C9 C27 H27B 109.5 . . ?
H27A C27 H27B 109.5 . . ?
C9 C27 H27C 109.5 . . ?
H27A C27 H27C 109.5 . . ?
H27B C27 H27C 109.5 . . ?
C33 Si28 C29 111.14(15) . . ?
C33 Si28 C31 109.28(14) . . ?
C29 Si28 C31 108.92(15) . . ?
C33 Si28 C15 111.91(13) . . ?
C29 Si28 C15 108.65(14) . . ?
C31 Si28 C15 106.80(13) . . ?
C30 C29 Si28 115.9(3) . . ?
C30 C29 H29A 108.3 . . ?
Si28 C29 H29A 108.3 . . ?
C30 C29 H29B 108.3 . . ?
Si28 C29 H29B 108.3 . . ?
H29A C29 H29B 107.4 . . ?
C29 C30 H30A 109.5 . . ?
C29 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C29 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C32 C31 Si28 116.7(2) . . ?
C32 C31 H31A 108.1 . . ?
Si28 C31 H31A 108.1 . . ?
C32 C31 H31B 108.1 . . ?
Si28 C31 H31B 108.1 . . ?
H31A C31 H31B 107.3 . . ?
C31 C32 H32A 109.5 . . ?
C31 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C31 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C34 C33 Si28 111.9(2) . . ?
C34 C33 H33A 109.2 . . ?
Si28 C33 H33A 109.2 . . ?
C34 C33 H33B 109.2 . . ?
Si28 C33 H33B 109.2 . . ?
H33A C33 H33B 107.9 . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C55 C41 B44 120.1(2) . . ?
C55 C41 B45 119.6(2) . . ?
B44 C41 B45 62.88(19) . . ?
C55 C41 B43 119.1(2) . . ?
B44 C41 B43 62.21(19) . . ?
B45 C41 B43 113.3(2) . . ?
C55 C41 B46 118.8(2) . . ?
B44 C41 B46 113.3(2) . . ?
B45 C41 B46 62.74(18) . . ?
B43 C41 B46 110.7(2) . . ?
C55 C41 C42 120.7(2) . . ?
B44 C41 C42 109.8(2) . . ?
B45 C41 C42 110.2(2) . . ?
B43 C41 C42 59.87(16) . . ?
B46 C41 C42 59.54(16) . . ?
B51 C42 B46 112.4(2) . . ?
B51 C42 B47 61.90(18) . . ?
B46 C42 B47 61.79(18) . . ?
B51 C42 B43 62.03(18) . . ?
B46 C42 B43 111.0(2) . . ?
B47 C42 B43 111.9(2) . . ?
B51 C42 C41 109.1(2) . . ?
B46 C42 C41 60.04(16) . . ?
B47 C42 C41 108.7(2) . . ?
B43 C42 C41 59.81(16) . . ?
B51 C42 Si68 116.9(2) . . ?
B46 C42 Si68 121.40(19) . . ?
B47 C42 Si68 119.17(18) . . ?
B43 C42 Si68 118.78(19) . . ?
C41 C42 Si68 124.55(18) . . ?
C41 B43 C42 60.31(16) . . ?
C41 B43 B50 105.8(2) . . ?
C42 B43 B50 106.3(2) . . ?
C41 B43 B44 58.24(18) . . ?
C42 B43 B44 107.0(2) . . ?
B50 B43 B44 60.2(2) . . ?
C41 B43 B51 106.8(2) . . ?
C42 B43 B51 58.58(17) . . ?
B50 B43 B51 60.27(19) . . ?
B44 B43 B51 108.4(2) . . ?
C41 B43 H43 123.0 . . ?
C42 B43 H43 122.6 . . ?
B50 B43 H43 122.5 . . ?
B44 B43 H43 121.9 . . ?
B51 B43 H43 121.9 . . ?
C41 B44 B43 59.56(18) . . ?
C41 B44 B49 106.3(2) . . ?
B43 B44 B49 108.1(2) . . ?
C41 B44 B50 106.6(2) . . ?
B43 B44 B50 59.82(19) . . ?
B49 B44 B50 60.4(2) . . ?
C41 B44 B45 58.84(17) . . ?
B43 B44 B45 108.0(2) . . ?
B49 B44 B45 60.41(19) . . ?
B50 B44 B45 108.7(2) . . ?
C41 B44 H44 123.4 . . ?
B43 B44 H44 121.7 . . ?
B49 B44 H44 121.8 . . ?
B50 B44 H44 121.7 . . ?
B45 B44 H44 121.5 . . ?
C41 B45 B48 106.1(2) . . ?
C41 B45 B44 58.28(18) . . ?
B48 B45 B44 107.8(2) . . ?
C41 B45 B49 105.3(2) . . ?
B48 B45 B49 60.39(19) . . ?
B44 B45 B49 59.65(19) . . ?
C41 B45 B46 59.06(17) . . ?
B48 B45 B46 59.86(18) . . ?
B44 B45 B46 106.7(2) . . ?
B49 B45 B46 107.4(2) . . ?
C41 B45 H45 123.9 . . ?
B48 B45 H45 121.7 . . ?
B44 B45 H45 122.4 . . ?
B49 B45 H45 122.3 . . ?
B46 B45 H45 122.2 . . ?
C42 B46 C41 60.42(16) . . ?
C42 B46 B47 59.21(18) . . ?
C41 B46 B47 107.0(2) . . ?
C42 B46 B48 106.6(2) . . ?
C41 B46 B48 105.3(2) . . ?
B47 B46 B48 60.01(19) . . ?
C42 B46 B45 107.2(2) . . ?
C41 B46 B45 58.19(17) . . ?
B47 B46 B45 107.9(2) . . ?
B48 B46 B45 59.61(18) . . ?
C42 B46 H46 122.1 . . ?
C41 B46 H46 123.1 . . ?
B47 B46 H46 121.8 . . ?
B48 B46 H46 122.9 . . ?
B45 B46 H46 122.2 . . ?
C42 B47 B52 106.9(2) . . ?
C42 B47 B51 58.75(17) . . ?
B52 B47 B51 60.94(19) . . ?
C42 B47 B46 59.00(17) . . ?
B52 B47 B46 108.7(2) . . ?
B51 B47 B46 107.6(2) . . ?
C42 B47 B48 106.6(2) . . ?
B52 B47 B48 60.6(2) . . ?
B51 B47 B48 109.0(2) . . ?
B46 B47 B48 60.31(19) . . ?
C42 B47 H47 123.5 . . ?
B52 B47 H47 121.2 . . ?
B51 B47 H47 121.4 . . ?
B46 B47 H47 121.7 . . ?
B48 B47 H47 121.4 . . ?
B47 B48 B45 108.4(2) . . ?
B47 B48 B46 59.68(19) . . ?
B45 B48 B46 60.53(18) . . ?
B47 B48 B52 59.51(19) . . ?
B45 B48 B52 108.3(2) . . ?
B46 B48 B52 107.4(2) . . ?
B47 B48 B49 107.2(2) . . ?
B45 B48 B49 60.22(19) . . ?
B46 B48 B49 107.8(2) . . ?
B52 B48 B49 59.66(19) . . ?
B47 B48 H48 122.1 . . ?
B45 B48 H48 121.1 . . ?
B46 B48 H48 121.9 . . ?
B52 B48 H48 122.1 . . ?
B49 B48 H48 122.1 . . ?
B44 B49 B52 108.2(3) . . ?
B44 B49 B50 59.8(2) . . ?
B52 B49 B50 60.5(2) . . ?
B44 B49 B45 59.94(19) . . ?
B52 B49 B45 107.9(2) . . ?
B50 B49 B45 107.8(2) . . ?
B44 B49 B48 107.3(2) . . ?
B52 B49 B48 59.99(19) . . ?
B50 B49 B48 107.9(2) . . ?
B45 B49 B48 59.40(18) . . ?
B44 B49 H49 121.9 . . ?
B52 B49 H49 121.4 . . ?
B50 B49 H49 121.6 . . ?
B45 B49 H49 122.0 . . ?
B48 B49 H49 122.2 . . ?
B43 B50 B44 59.96(19) . . ?
B43 B50 B51 59.97(18) . . ?
B44 B50 B51 107.9(2) . . ?
B43 B50 B49 107.7(2) . . ?
B44 B50 B49 59.8(2) . . ?
B51 B50 B49 107.8(2) . . ?
B43 B50 B52 107.8(2) . . ?
B44 B50 B52 107.4(2) . . ?
B51 B50 B52 60.17(19) . . ?
B49 B50 B52 59.6(2) . . ?
B43 B50 H50 121.8 . . ?
B44 B50 H50 121.9 . . ?
B51 B50 H50 121.6 . . ?
B49 B50 H50 122.0 . . ?
B52 B50 H50 122.0 . . ?
C42 B51 B47 59.35(18) . . ?
C42 B51 B43 59.39(17) . . ?
B47 B51 B43 107.7(2) . . ?
C42 B51 B50 106.6(2) . . ?
B47 B51 B50 108.0(3) . . ?
B43 B51 B50 59.76(19) . . ?
C42 B51 B52 106.2(2) . . ?
B47 B51 B52 59.52(19) . . ?
B43 B51 B52 107.8(2) . . ?
B50 B51 B52 60.4(2) . . ?
C42 B51 H51 123.1 . . ?
B47 B51 H51 121.9 . . ?
B43 B51 H51 121.8 . . ?
B50 B51 H51 121.8 . . ?
B52 B51 H51 122.1 . . ?
B47 B52 B49 108.1(2) . . ?
B47 B52 B48 59.9(2) . . ?
B49 B52 B48 60.3(2) . . ?
B47 B52 B51 59.54(19) . . ?
B49 B52 B51 107.5(2) . . ?
B48 B52 B51 107.4(2) . . ?
B47 B52 B50 107.1(2) . . ?
B49 B52 B50 59.9(2) . . ?
B48 B52 B50 107.8(2) . . ?
B51 B52 B50 59.39(19) . . ?
B47 B52 H52 122.0 . . ?
B49 B52 H52 121.5 . . ?
B48 B52 H52 121.7 . . ?
B51 B52 H52 122.3 . . ?
B50 B52 H52 122.2 . . ?
C54 C53 C58 120.2(3) . . ?
C54 C53 C65 128.8(3) . . ?
C58 C53 C65 110.9(2) . . ?
C53 C54 C55 120.2(3) . . ?
C53 C54 H54 119.9 . . ?
C55 C54 H54 119.9 . . ?
C56 C55 C54 119.1(3) . . ?
C56 C55 C41 120.0(2) . . ?
C54 C55 C41 120.8(2) . . ?
C57 C56 C55 121.1(3) . . ?
C57 C56 H56 119.5 . . ?
C55 C56 H56 119.5 . . ?
C58 C57 C56 119.2(3) . . ?
C58 C57 H57 120.4 . . ?
C56 C57 H57 120.4 . . ?
C57 C58 C53 120.2(3) . . ?
C57 C58 C59 131.4(3) . . ?
C53 C58 C59 108.4(3) . . ?
C64 C59 C60 120.9(3) . . ?
C64 C59 C58 108.5(3) . . ?
C60 C59 C58 130.6(3) . . ?
C61 C60 C59 118.6(3) . . ?
C61 C60 H60 120.7 . . ?
C59 C60 H60 120.7 . . ?
C60 C61 C62 120.8(3) . . ?
C60 C61 H61 119.6 . . ?
C62 C61 H61 119.6 . . ?
C61 C62 C63 120.9(3) . . ?
C61 C62 H62 119.5 . . ?
C63 C62 H62 119.5 . . ?
C62 C63 C64 118.7(4) . . ?
C62 C63 H63 120.6 . . ?
C64 C63 H63 120.6 . . ?
C63 C64 C59 120.1(3) . . ?
C63 C64 C65 128.6(3) . . ?
C59 C64 C65 111.4(3) . . ?
C53 C65 C64 100.8(2) . . ?
C53 C65 C66 111.3(2) . . ?
C64 C65 C66 111.7(3) . . ?
C53 C65 C67 110.7(3) . . ?
C64 C65 C67 111.5(2) . . ?
C66 C65 C67 110.5(3) . . ?
C65 C66 H66A 109.5 . . ?
C65 C66 H66B 109.5 . . ?
H66A C66 H66B 109.5 . . ?
C65 C66 H66C 109.5 . . ?
H66A C66 H66C 109.5 . . ?
H66B C66 H66C 109.5 . . ?
C65 C67 H67A 109.5 . . ?
C65 C67 H67B 109.5 . . ?
H67A C67 H67B 109.5 . . ?
C65 C67 H67C 109.5 . . ?
H67A C67 H67C 109.5 . . ?
H67B C67 H67C 109.5 . . ?
C73 Si68 C71 99.8(4) . . ?
C73 Si68 C69 113.4(4) . . ?
C71 Si68 C69 114.5(2) . . ?
C69 Si68 C71B 87.3(9) . . ?
C69 Si68 C73B 107.4(6) . . ?
C71B Si68 C73B 137.7(11) . . ?
C73 Si68 C42 109.1(4) . . ?
C71 Si68 C42 108.21(17) . . ?
C69 Si68 C42 111.16(14) . . ?
C71B Si68 C42 110.2(9) . . ?
C73B Si68 C42 101.2(5) . . ?
C70 C69 Si68 113.1(3) . . ?
C70 C69 H69A 109.0 . . ?
Si68 C69 H69A 109.0 . . ?
C70 C69 H69B 109.0 . . ?
Si68 C69 H69B 109.0 . . ?
H69A C69 H69B 107.8 . . ?
C69 C70 H70A 109.5 . . ?
C69 C70 H70B 109.5 . . ?
H70A C70 H70B 109.5 . . ?
C69 C70 H70C 109.5 . . ?
H70A C70 H70C 109.5 . . ?
H70B C70 H70C 109.5 . . ?
C72 C71 Si68 116.2(4) . . ?
C72 C71 H71A 108.2 . . ?
Si68 C71 H71A 108.2 . . ?
C72 C71 H71B 108.2 . . ?
Si68 C71 H71B 108.2 . . ?
H71A C71 H71B 107.4 . . ?
C71 C72 H72A 109.5 . . ?
C71 C72 H72B 109.5 . . ?
H72A C72 H72B 109.5 . . ?
C71 C72 H72C 109.5 . . ?
H72A C72 H72C 109.5 . . ?
H72B C72 H72C 109.5 . . ?
C74 C73 Si68 111.8(6) . . ?
C74 C73 H73A 109.3 . . ?
Si68 C73 H73A 109.3 . . ?
C74 C73 H73B 109.3 . . ?
Si68 C73 H73B 109.3 . . ?
H73A C73 H73B 107.9 . . ?
C73 C74 H74A 109.5 . . ?
C73 C74 H74B 109.5 . . ?
H74A C74 H74B 109.5 . . ?
C73 C74 H74C 109.5 . . ?
H74A C74 H74C 109.5 . . ?
H74B C74 H74C 109.5 . . ?
C72B C71B Si68 114(2) . . ?
C72B C71B H71C 108.7 . . ?
Si68 C71B H71C 108.7 . . ?
C72B C71B H71D 108.7 . . ?
Si68 C71B H71D 108.7 . . ?
H71C C71B H71D 107.6 . . ?
C71B C72B H72D 109.5 . . ?
C71B C72B H72E 109.5 . . ?
H72D C72B H72E 109.5 . . ?
C71B C72B H72F 109.5 . . ?
H72D C72B H72F 109.5 . . ?
H72E C72B H72F 109.5 . . ?
C74B C73B Si68 118.8(9) . . ?
C74B C73B H73C 107.6 . . ?
Si68 C73B H73C 107.6 . . ?
C74B C73B H73D 107.6 . . ?
Si68 C73B H73D 107.6 . . ?
H73C C73B H73D 107.0 . . ?
C73B C74B H74D 109.5 . . ?
C73B C74B H74E 109.5 . . ?
H74D C74B H74E 109.5 . . ?
C73B C74B H74F 109.5 . . ?
H74D C74B H74F 109.5 . . ?
H74E C74B H74F 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C2 C1 1.398(4) . ?
C2 C3 1.398(4) . ?
C2 C14 1.505(4) . ?
B2 C14 1.708(4) . ?
B2 B7 1.771(5) . ?
B2 B1 1.779(5) . ?
B2 B3 1.781(5) . ?
B2 B6 1.785(4) . ?
B2 H2 1.1200 . ?
C1 C10 1.378(4) . ?
C1 H1A 0.9500 . ?
B1 C14 1.709(4) . ?
B1 B4 1.772(5) . ?
B1 B5 1.773(5) . ?
B1 B3 1.776(5) . ?
B1 H1 1.1200 . ?
C3 C4 1.390(4) . ?
C3 H3A 0.9500 . ?
B3 B8 1.771(5) . ?
B3 B7 1.783(5) . ?
B3 B4 1.790(5) . ?
B3 H3 1.1200 . ?
C4 C11 1.387(4) . ?
C4 H4A 0.9500 . ?
B4 B5 1.773(5) . ?
B4 B9 1.775(5) . ?
B4 B8 1.789(5) . ?
B4 H4 1.1200 . ?
C5 C6 1.382(4) . ?
C5 C12 1.394(4) . ?
C5 H5A 0.9500 . ?
B5 C14 1.721(4) . ?
B5 C15 1.727(4) . ?
B5 B9 1.770(4) . ?
B5 H5 1.1200 . ?
C6 C7 1.384(5) . ?
C6 H6A 0.9500 . ?
B6 C15 1.721(4) . ?
B6 C14 1.724(4) . ?
B6 B10 1.773(4) . ?
B6 B7 1.776(5) . ?
B6 H6 1.1200 . ?
C7 C8 1.391(5) . ?
C7 H7A 0.9500 . ?
B7 B10 1.765(5) . ?
B7 B8 1.781(5) . ?
B7 H7 1.1200 . ?
C8 C13 1.385(4) . ?
C8 H8A 0.9500 . ?
B8 B10 1.768(5) . ?
B8 B9 1.780(5) . ?
B8 H8 1.1200 . ?
C9 C13 1.524(4) . ?
C9 C10 1.525(4) . ?
C9 C26 1.527(4) . ?
C9 C27 1.540(4) . ?
B9 C15 1.712(4) . ?
B9 B10 1.765(4) . ?
B9 H9 1.1200 . ?
C10 C11 1.407(4) . ?
B10 C15 1.718(4) . ?
B10 H10 1.1200 . ?
C11 C12 1.463(4) . ?
C12 C13 1.392(4) . ?
C14 C15 1.727(4) . ?
C15 Si28 1.944(3) . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C27 H27A 0.9800 . ?
C27 H27B 0.9800 . ?
C27 H27C 0.9800 . ?
Si28 C33 1.869(3) . ?
Si28 C29 1.873(3) . ?
Si28 C31 1.875(3) . ?
C29 C30 1.520(5) . ?
C29 H29A 0.9900 . ?
C29 H29B 0.9900 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.527(4) . ?
C31 H31A 0.9900 . ?
C31 H31B 0.9900 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?
C33 C34 1.537(4) . ?
C33 H33A 0.9900 . ?
C33 H33B 0.9900 . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C41 C55 1.506(4) . ?
C41 B44 1.698(4) . ?
C41 B45 1.708(4) . ?
C41 B43 1.721(4) . ?
C41 B46 1.724(4) . ?
C41 C42 1.730(4) . ?
C42 B51 1.708(4) . ?
C42 B46 1.715(4) . ?
C42 B47 1.719(4) . ?
C42 B43 1.722(4) . ?
C42 Si68 1.939(3) . ?
B43 B50 1.764(5) . ?
B43 B44 1.766(5) . ?
B43 B51 1.768(4) . ?
B43 H43 1.1200 . ?
B44 B49 1.771(5) . ?
B44 B50 1.771(5) . ?
B44 B45 1.776(5) . ?
B44 H44 1.1200 . ?
B45 B48 1.770(4) . ?
B45 B49 1.785(5) . ?
B45 B46 1.786(4) . ?
B45 H45 1.1200 . ?
B46 B47 1.763(5) . ?
B46 B48 1.774(5) . ?
B46 H46 1.1200 . ?
B47 B52 1.762(5) . ?
B47 B51 1.762(5) . ?
B47 B48 1.769(5) . ?
B47 H47 1.1200 . ?
B48 B52 1.781(5) . ?
B48 B49 1.788(5) . ?
B48 H48 1.1200 . ?
B49 B52 1.775(5) . ?
B49 B50 1.782(5) . ?
B49 H49 1.1200 . ?
B50 B51 1.773(5) . ?
B50 B52 1.792(5) . ?
B50 H50 1.1200 . ?
B51 B52 1.787(5) . ?
B51 H51 1.1200 . ?
B52 H52 1.1200 . ?
C53 C54 1.376(4) . ?
C53 C58 1.403(4) . ?
C53 C65 1.524(4) . ?
C54 C55 1.395(4) . ?
C54 H54 0.9500 . ?
C55 C56 1.394(4) . ?
C56 C57 1.390(4) . ?
C56 H56 0.9500 . ?
C57 C58 1.381(4) . ?
C57 H57 0.9500 . ?
C58 C59 1.464(4) . ?
C59 C64 1.393(4) . ?
C59 C60 1.396(4) . ?
C60 C61 1.380(5) . ?
C60 H60 0.9500 . ?
C61 C62 1.387(5) . ?
C61 H61 0.9500 . ?
C62 C63 1.389(5) . ?
C62 H62 0.9500 . ?
C63 C64 1.392(4) . ?
C63 H63 0.9500 . ?
C64 C65 1.525(4) . ?
C65 C66 1.532(4) . ?
C65 C67 1.541(4) . ?
C66 H66A 0.9800 . ?
C66 H66B 0.9800 . ?
C66 H66C 0.9800 . ?
C67 H67A 0.9800 . ?
C67 H67B 0.9800 . ?
C67 H67C 0.9800 . ?
Si68 C73 1.832(10) . ?
Si68 C71 1.856(5) . ?
Si68 C69 1.859(4) . ?
Si68 C71B 1.863(17) . ?
Si68 C73B 1.936(12) . ?
C69 C70 1.537(4) . ?
C69 H69A 0.9900 . ?
C69 H69B 0.9900 . ?
C70 H70A 0.9800 . ?
C70 H70B 0.9800 . ?
C70 H70C 0.9800 . ?
C71 C72 1.528(7) . ?
C71 H71A 0.9900 . ?
C71 H71B 0.9900 . ?
C72 H72A 0.9800 . ?
C72 H72B 0.9800 . ?
C72 H72C 0.9800 . ?
C73 C74 1.535(11) . ?
C73 H73A 0.9900 . ?
C73 H73B 0.9900 . ?
C74 H74A 0.9800 . ?
C74 H74B 0.9800 . ?
C74 H74C 0.9800 . ?
C71B C72B 1.539(19) . ?
C71B H71C 0.9900 . ?
C71B H71D 0.9900 . ?
C72B H72D 0.9800 . ?
C72B H72E 0.9800 . ?
C72B H72F 0.9800 . ?
C73B C74B 1.534(14) . ?
C73B H73C 0.9900 . ?
C73B H73D 0.9900 . ?
C74B H74D 0.9800 . ?
C74B H74E 0.9800 . ?
C74B H74F 0.9800 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C3 C2 C1 C10 -3.0(4) . . . . ?
C14 C2 C1 C10 -178.8(3) . . . . ?
B7 B2 B1 C14 -98.2(2) . . . . ?
B3 B2 B1 C14 -135.9(2) . . . . ?
B6 B2 B1 C14 -35.0(2) . . . . ?
C14 B2 B1 B4 98.3(3) . . . . ?
B7 B2 B1 B4 0.1(3) . . . . ?
B3 B2 B1 B4 -37.7(2) . . . . ?
B6 B2 B1 B4 63.3(3) . . . . ?
C14 B2 B1 B5 34.8(2) . . . . ?
B7 B2 B1 B5 -63.4(3) . . . . ?
B3 B2 B1 B5 -101.2(3) . . . . ?
B6 B2 B1 B5 -0.2(3) . . . . ?
C14 B2 B1 B3 135.9(2) . . . . ?
B7 B2 B1 B3 37.8(2) . . . . ?
B6 B2 B1 B3 101.0(3) . . . . ?
C1 C2 C3 C4 1.8(4) . . . . ?
C14 C2 C3 C4 177.6(3) . . . . ?
C14 B1 B3 B8 -62.7(3) . . . . ?
B4 B1 B3 B8 37.5(2) . . . . ?
B5 B1 B3 B8 -0.6(3) . . . . ?
B2 B1 B3 B8 -100.8(3) . . . . ?
C14 B1 B3 B2 38.1(2) . . . . ?
B4 B1 B3 B2 138.3(2) . . . . ?
B5 B1 B3 B2 100.2(2) . . . . ?
C14 B1 B3 B7 0.7(3) . . . . ?
B4 B1 B3 B7 100.9(3) . . . . ?
B5 B1 B3 B7 62.9(3) . . . . ?
B2 B1 B3 B7 -37.4(2) . . . . ?
C14 B1 B3 B4 -100.2(3) . . . . ?
B5 B1 B3 B4 -38.1(2) . . . . ?
B2 B1 B3 B4 -138.3(2) . . . . ?
C14 B2 B3 B8 62.7(3) . . . . ?
B7 B2 B3 B8 -37.1(2) . . . . ?
B1 B2 B3 B8 100.8(3) . . . . ?
B6 B2 B3 B8 0.7(3) . . . . ?
C14 B2 B3 B1 -38.1(2) . . . . ?
B7 B2 B3 B1 -137.8(3) . . . . ?
B6 B2 B3 B1 -100.0(2) . . . . ?
C14 B2 B3 B7 99.8(2) . . . . ?
B1 B2 B3 B7 137.8(3) . . . . ?
B6 B2 B3 B7 37.8(2) . . . . ?
C14 B2 B3 B4 -1.0(3) . . . . ?
B7 B2 B3 B4 -100.8(3) . . . . ?
B1 B2 B3 B4 37.0(2) . . . . ?
B6 B2 B3 B4 -63.0(3) . . . . ?
C2 C3 C4 C11 0.2(5) . . . . ?
C14 B1 B4 B5 -38.2(2) . . . . ?
B3 B1 B4 B5 -137.4(2) . . . . ?
B2 B1 B4 B5 -100.0(2) . . . . ?
C14 B1 B4 B9 -0.9(3) . . . . ?
B5 B1 B4 B9 37.3(2) . . . . ?
B3 B1 B4 B9 -100.1(3) . . . . ?
B2 B1 B4 B9 -62.6(3) . . . . ?
C14 B1 B4 B8 62.3(3) . . . . ?
B5 B1 B4 B8 100.5(2) . . . . ?
B3 B1 B4 B8 -36.9(2) . . . . ?
B2 B1 B4 B8 0.6(3) . . . . ?
C14 B1 B4 B3 99.2(2) . . . . ?
B5 B1 B4 B3 137.4(2) . . . . ?
B2 B1 B4 B3 37.5(2) . . . . ?
B8 B3 B4 B1 -138.2(2) . . . . ?
B2 B3 B4 B1 -37.2(2) . . . . ?
B7 B3 B4 B1 -100.2(3) . . . . ?
B8 B3 B4 B5 -100.3(3) . . . . ?
B1 B3 B4 B5 37.9(2) . . . . ?
B2 B3 B4 B5 0.6(3) . . . . ?
B7 B3 B4 B5 -62.3(3) . . . . ?
B8 B3 B4 B9 -37.3(2) . . . . ?
B1 B3 B4 B9 100.9(2) . . . . ?
B2 B3 B4 B9 63.7(3) . . . . ?
B7 B3 B4 B9 0.7(3) . . . . ?
B1 B3 B4 B8 138.2(2) . . . . ?
B2 B3 B4 B8 101.0(3) . . . . ?
B7 B3 B4 B8 38.0(2) . . . . ?
B4 B1 B5 C14 -136.3(2) . . . . ?
B3 B1 B5 C14 -98.0(2) . . . . ?
B2 B1 B5 C14 -34.5(2) . . . . ?
C14 B1 B5 C15 36.98(19) . . . . ?
B4 B1 B5 C15 -99.3(2) . . . . ?
B3 B1 B5 C15 -61.0(3) . . . . ?
B2 B1 B5 C15 2.5(3) . . . . ?
C14 B1 B5 B9 98.8(2) . . . . ?
B4 B1 B5 B9 -37.5(2) . . . . ?
B3 B1 B5 B9 0.8(3) . . . . ?
B2 B1 B5 B9 64.2(3) . . . . ?
C14 B1 B5 B4 136.3(2) . . . . ?
B3 B1 B5 B4 38.3(2) . . . . ?
B2 B1 B5 B4 101.8(3) . . . . ?
B1 B4 B5 C14 37.8(2) . . . . ?
B9 B4 B5 C14 -100.3(2) . . . . ?
B8 B4 B5 C14 -62.5(3) . . . . ?
B3 B4 B5 C14 0.0(3) . . . . ?
B1 B4 B5 C15 100.6(2) . . . . ?
B9 B4 B5 C15 -37.5(2) . . . . ?
B8 B4 B5 C15 0.3(3) . . . . ?
B3 B4 B5 C15 62.8(3) . . . . ?
B1 B4 B5 B9 138.1(2) . . . . ?
B8 B4 B5 B9 37.8(2) . . . . ?
B3 B4 B5 B9 100.3(3) . . . . ?
B9 B4 B5 B1 -138.1(2) . . . . ?
B8 B4 B5 B1 -100.3(3) . . . . ?
B3 B4 B5 B1 -37.8(2) . . . . ?
C12 C5 C6 C7 -0.6(5) . . . . ?
C14 B2 B6 C15 -36.93(19) . . . . ?
B7 B2 B6 C15 98.9(2) . . . . ?
B1 B2 B6 C15 -2.2(3) . . . . ?
B3 B2 B6 C15 61.0(3) . . . . ?
B7 B2 B6 C14 135.9(2) . . . . ?
B1 B2 B6 C14 34.8(2) . . . . ?
B3 B2 B6 C14 97.9(2) . . . . ?
C14 B2 B6 B10 -98.9(2) . . . . ?
B7 B2 B6 B10 37.0(2) . . . . ?
B1 B2 B6 B10 -64.1(3) . . . . ?
B3 B2 B6 B10 -1.0(3) . . . . ?
C14 B2 B6 B7 -135.9(2) . . . . ?
B1 B2 B6 B7 -101.1(3) . . . . ?
B3 B2 B6 B7 -38.0(2) . . . . ?
C5 C6 C7 C8 0.1(5) . . . . ?
C14 B2 B7 B10 1.0(3) . . . . ?
B1 B2 B7 B10 62.6(3) . . . . ?
B3 B2 B7 B10 100.2(3) . . . . ?
B6 B2 B7 B10 -37.4(2) . . . . ?
C14 B2 B7 B6 38.4(2) . . . . ?
B1 B2 B7 B6 100.0(2) . . . . ?
B3 B2 B7 B6 137.6(3) . . . . ?
C14 B2 B7 B8 -62.3(3) . . . . ?
B1 B2 B7 B8 -0.7(3) . . . . ?
B3 B2 B7 B8 36.9(2) . . . . ?
B6 B2 B7 B8 -100.7(3) . . . . ?
C14 B2 B7 B3 -99.1(3) . . . . ?
B1 B2 B7 B3 -37.6(2) . . . . ?
B6 B2 B7 B3 -137.6(3) . . . . ?
C15 B6 B7 B10 37.8(2) . . . . ?
C14 B6 B7 B10 100.5(2) . . . . ?
B2 B6 B7 B10 138.3(2) . . . . ?
C15 B6 B7 B2 -100.5(2) . . . . ?
C14 B6 B7 B2 -37.8(2) . . . . ?
B10 B6 B7 B2 -138.3(2) . . . . ?
C15 B6 B7 B8 0.5(3) . . . . ?
C14 B6 B7 B8 63.2(3) . . . . ?
B10 B6 B7 B8 -37.3(2) . . . . ?
B2 B6 B7 B8 101.0(3) . . . . ?
C15 B6 B7 B3 -62.5(3) . . . . ?
C14 B6 B7 B3 0.2(3) . . . . ?
B10 B6 B7 B3 -100.3(3) . . . . ?
B2 B6 B7 B3 38.0(2) . . . . ?
B8 B3 B7 B10 37.0(2) . . . . ?
B1 B3 B7 B10 -64.0(3) . . . . ?
B2 B3 B7 B10 -101.6(3) . . . . ?
B4 B3 B7 B10 -1.1(3) . . . . ?
B8 B3 B7 B2 138.6(3) . . . . ?
B1 B3 B7 B2 37.6(2) . . . . ?
B4 B3 B7 B2 100.5(3) . . . . ?
B8 B3 B7 B6 100.5(3) . . . . ?
B1 B3 B7 B6 -0.6(3) . . . . ?
B2 B3 B7 B6 -38.1(2) . . . . ?
B4 B3 B7 B6 62.3(3) . . . . ?
B1 B3 B7 B8 -101.0(3) . . . . ?
B2 B3 B7 B8 -138.6(3) . . . . ?
B4 B3 B7 B8 -38.1(2) . . . . ?
C6 C7 C8 C13 0.5(6) . . . . ?
B1 B3 B8 B10 63.2(3) . . . . ?
B2 B3 B8 B10 -0.2(3) . . . . ?
B7 B3 B8 B10 -37.1(2) . . . . ?
B4 B3 B8 B10 100.4(3) . . . . ?
B1 B3 B8 B9 0.2(3) . . . . ?
B2 B3 B8 B9 -63.3(3) . . . . ?
B7 B3 B8 B9 -100.1(3) . . . . ?
B4 B3 B8 B9 37.3(2) . . . . ?
B1 B3 B8 B7 100.3(3) . . . . ?
B2 B3 B8 B7 36.8(2) . . . . ?
B4 B3 B8 B7 137.5(2) . . . . ?
B1 B3 B8 B4 -37.2(2) . . . . ?
B2 B3 B8 B4 -100.6(3) . . . . ?
B7 B3 B8 B4 -137.5(2) . . . . ?
B2 B7 B8 B10 101.3(2) . . . . ?
B6 B7 B8 B10 37.5(2) . . . . ?
B3 B7 B8 B10 138.4(2) . . . . ?
B10 B7 B8 B3 -138.4(2) . . . . ?
B2 B7 B8 B3 -37.1(2) . . . . ?
B6 B7 B8 B3 -101.0(3) . . . . ?
B10 B7 B8 B9 -37.3(2) . . . . ?
B2 B7 B8 B9 64.0(3) . . . . ?
B6 B7 B8 B9 0.1(3) . . . . ?
B3 B7 B8 B9 101.1(3) . . . . ?
B10 B7 B8 B4 -100.2(2) . . . . ?
B2 B7 B8 B4 1.1(3) . . . . ?
B6 B7 B8 B4 -62.8(3) . . . . ?
B3 B7 B8 B4 38.2(2) . . . . ?
B1 B4 B8 B10 -64.1(3) . . . . ?
B5 B4 B8 B10 -0.9(3) . . . . ?
B9 B4 B8 B10 36.9(2) . . . . ?
B3 B4 B8 B10 -101.2(3) . . . . ?
B1 B4 B8 B3 37.1(2) . . . . ?
B5 B4 B8 B3 100.3(3) . . . . ?
B9 B4 B8 B3 138.0(2) . . . . ?
B1 B4 B8 B9 -100.9(3) . . . . ?
B5 B4 B8 B9 -37.7(2) . . . . ?
B3 B4 B8 B9 -138.0(2) . . . . ?
B1 B4 B8 B7 -1.0(3) . . . . ?
B5 B4 B8 B7 62.2(3) . . . . ?
B9 B4 B8 B7 99.9(3) . . . . ?
B3 B4 B8 B7 -38.1(2) . . . . ?
C14 B5 B9 C15 -37.8(2) . . . . ?
B1 B5 B9 C15 -99.3(2) . . . . ?
B4 B5 B9 C15 -136.8(2) . . . . ?
C14 B5 B9 B10 -2.3(3) . . . . ?
C15 B5 B9 B10 35.5(2) . . . . ?
B1 B5 B9 B10 -63.9(3) . . . . ?
B4 B5 B9 B10 -101.3(3) . . . . ?
C14 B5 B9 B4 99.0(3) . . . . ?
C15 B5 B9 B4 136.8(2) . . . . ?
B1 B5 B9 B4 37.5(2) . . . . ?
C14 B5 B9 B8 60.9(3) . . . . ?
C15 B5 B9 B8 98.7(2) . . . . ?
B1 B5 B9 B8 -0.7(3) . . . . ?
B4 B5 B9 B8 -38.1(2) . . . . ?
B1 B4 B9 C15 0.6(3) . . . . ?
B5 B4 B9 C15 38.0(2) . . . . ?
B8 B4 B9 C15 -99.5(2) . . . . ?
B3 B4 B9 C15 -62.5(3) . . . . ?
B1 B4 B9 B10 63.0(3) . . . . ?
B5 B4 B9 B10 100.4(2) . . . . ?
B8 B4 B9 B10 -37.1(2) . . . . ?
B3 B4 B9 B10 0.0(3) . . . . ?
B1 B4 B9 B5 -37.4(2) . . . . ?
B8 B4 B9 B5 -137.5(3) . . . . ?
B3 B4 B9 B5 -100.5(3) . . . . ?
B1 B4 B9 B8 100.1(3) . . . . ?
B5 B4 B9 B8 137.5(3) . . . . ?
B3 B4 B9 B8 37.1(2) . . . . ?
B10 B8 B9 C15 -38.1(2) . . . . ?
B3 B8 B9 C15 62.8(3) . . . . ?
B7 B8 B9 C15 -0.8(3) . . . . ?
B4 B8 B9 C15 100.5(2) . . . . ?
B3 B8 B9 B10 100.9(3) . . . . ?
B7 B8 B9 B10 37.3(2) . . . . ?
B4 B8 B9 B10 138.5(3) . . . . ?
B10 B8 B9 B5 -100.6(2) . . . . ?
B3 B8 B9 B5 0.3(3) . . . . ?
B7 B8 B9 B5 -63.3(3) . . . . ?
B4 B8 B9 B5 38.0(2) . . . . ?
B10 B8 B9 B4 -138.5(3) . . . . ?
B3 B8 B9 B4 -37.6(2) . . . . ?
B7 B8 B9 B4 -101.2(3) . . . . ?
C2 C1 C10 C11 2.4(4) . . . . ?
C2 C1 C10 C9 -177.1(3) . . . . ?
C13 C9 C10 C1 -178.3(3) . . . . ?
C26 C9 C10 C1 -58.8(4) . . . . ?
C27 C9 C10 C1 64.6(4) . . . . ?
C13 C9 C10 C11 2.2(3) . . . . ?
C26 C9 C10 C11 121.7(3) . . . . ?
C27 C9 C10 C11 -114.9(3) . . . . ?
B5 B9 B10 C15 -35.6(2) . . . . ?
B4 B9 B10 C15 -99.1(2) . . . . ?
B8 B9 B10 C15 -136.5(2) . . . . ?
C15 B9 B10 B7 98.4(2) . . . . ?
B5 B9 B10 B7 62.9(3) . . . . ?
B4 B9 B10 B7 -0.7(3) . . . . ?
B8 B9 B10 B7 -38.0(2) . . . . ?
C15 B9 B10 B8 136.5(2) . . . . ?
B5 B9 B10 B8 100.9(3) . . . . ?
B4 B9 B10 B8 37.4(2) . . . . ?
C15 B9 B10 B6 34.7(2) . . . . ?
B5 B9 B10 B6 -0.9(3) . . . . ?
B4 B9 B10 B6 -64.4(3) . . . . ?
B8 B9 B10 B6 -101.8(3) . . . . ?
B2 B7 B10 C15 -0.5(3) . . . . ?
B6 B7 B10 C15 -38.0(2) . . . . ?
B8 B7 B10 C15 100.1(2) . . . . ?
B3 B7 B10 C15 63.1(3) . . . . ?
B2 B7 B10 B9 -62.5(3) . . . . ?
B6 B7 B10 B9 -100.1(2) . . . . ?
B8 B7 B10 B9 38.0(2) . . . . ?
B3 B7 B10 B9 1.1(3) . . . . ?
B2 B7 B10 B8 -100.5(3) . . . . ?
B6 B7 B10 B8 -138.1(2) . . . . ?
B3 B7 B10 B8 -36.9(2) . . . . ?
B2 B7 B10 B6 37.6(2) . . . . ?
B8 B7 B10 B6 138.1(2) . . . . ?
B3 B7 B10 B6 101.2(3) . . . . ?
B3 B8 B10 C15 -62.6(3) . . . . ?
B9 B8 B10 C15 38.0(2) . . . . ?
B7 B8 B10 C15 -99.9(2) . . . . ?
B4 B8 B10 C15 1.1(3) . . . . ?
B3 B8 B10 B9 -100.6(3) . . . . ?
B7 B8 B10 B9 -137.9(2) . . . . ?
B4 B8 B10 B9 -36.9(2) . . . . ?
B3 B8 B10 B7 37.3(2) . . . . ?
B9 B8 B10 B7 137.9(2) . . . . ?
B4 B8 B10 B7 101.1(3) . . . . ?
B3 B8 B10 B6 -0.4(3) . . . . ?
B9 B8 B10 B6 100.2(2) . . . . ?
B7 B8 B10 B6 -37.7(2) . . . . ?
B4 B8 B10 B6 63.3(3) . . . . ?
C14 B6 B10 C15 38.3(2) . . . . ?
B7 B6 B10 C15 136.5(2) . . . . ?
B2 B6 B10 C15 99.5(2) . . . . ?
C15 B6 B10 B9 -34.6(2) . . . . ?
C14 B6 B10 B9 3.8(3) . . . . ?
B7 B6 B10 B9 101.9(3) . . . . ?
B2 B6 B10 B9 64.9(3) . . . . ?
C15 B6 B10 B7 -136.5(2) . . . . ?
C14 B6 B10 B7 -98.1(2) . . . . ?
B2 B6 B10 B7 -37.0(2) . . . . ?
C15 B6 B10 B8 -98.6(2) . . . . ?
C14 B6 B10 B8 -60.3(3) . . . . ?
B7 B6 B10 B8 37.8(2) . . . . ?
B2 B6 B10 B8 0.9(3) . . . . ?
C3 C4 C11 C10 -0.9(4) . . . . ?
C3 C4 C11 C12 -179.4(3) . . . . ?
C1 C10 C11 C4 -0.4(4) . . . . ?
C9 C10 C11 C4 179.1(3) . . . . ?
C1 C10 C11 C12 178.5(3) . . . . ?
C9 C10 C11 C12 -2.0(3) . . . . ?
C6 C5 C12 C13 0.5(5) . . . . ?
C6 C5 C12 C11 179.3(3) . . . . ?
C4 C11 C12 C13 179.6(3) . . . . ?
C10 C11 C12 C13 0.9(3) . . . . ?
C4 C11 C12 C5 0.7(6) . . . . ?
C10 C11 C12 C5 -178.0(3) . . . . ?
C7 C8 C13 C12 -0.5(5) . . . . ?
C7 C8 C13 C9 -180.0(3) . . . . ?
C5 C12 C13 C8 0.0(5) . . . . ?
C11 C12 C13 C8 -179.0(3) . . . . ?
C5 C12 C13 C9 179.6(3) . . . . ?
C11 C12 C13 C9 0.6(3) . . . . ?
C10 C9 C13 C8 177.9(3) . . . . ?
C26 C9 C13 C8 58.2(4) . . . . ?
C27 C9 C13 C8 -65.2(4) . . . . ?
C10 C9 C13 C12 -1.6(3) . . . . ?
C26 C9 C13 C12 -121.3(3) . . . . ?
C27 C9 C13 C12 115.3(3) . . . . ?
C1 C2 C14 B2 55.4(4) . . . . ?
C3 C2 C14 B2 -120.4(3) . . . . ?
C1 C2 C14 B1 128.7(3) . . . . ?
C3 C2 C14 B1 -47.1(4) . . . . ?
C1 C2 C14 B5 -159.2(3) . . . . ?
C3 C2 C14 B5 25.1(4) . . . . ?
C1 C2 C14 B6 -18.1(4) . . . . ?
C3 C2 C14 B6 166.1(3) . . . . ?
C1 C2 C14 C15 -88.8(3) . . . . ?
C3 C2 C14 C15 95.5(3) . . . . ?
B7 B2 C14 C2 -149.0(2) . . . . ?
B1 B2 C14 C2 109.5(3) . . . . ?
B3 B2 C14 C2 148.1(2) . . . . ?
B6 B2 C14 C2 -110.2(3) . . . . ?
B7 B2 C14 B1 101.5(3) . . . . ?
B3 B2 C14 B1 38.6(2) . . . . ?
B6 B2 C14 B1 140.4(2) . . . . ?
B7 B2 C14 B5 64.0(3) . . . . ?
B1 B2 C14 B5 -37.6(2) . . . . ?
B3 B2 C14 B5 1.1(3) . . . . ?
B6 B2 C14 B5 102.8(2) . . . . ?
B7 B2 C14 B6 -38.8(2) . . . . ?
B1 B2 C14 B6 -140.4(2) . . . . ?
B3 B2 C14 B6 -101.7(2) . . . . ?
B7 B2 C14 C15 -1.2(3) . . . . ?
B1 B2 C14 C15 -102.8(2) . . . . ?
B3 B2 C14 C15 -64.1(3) . . . . ?
B6 B2 C14 C15 37.6(2) . . . . ?
B4 B1 C14 C2 147.3(3) . . . . ?
B5 B1 C14 C2 108.7(3) . . . . ?
B3 B1 C14 C2 -149.4(3) . . . . ?
B2 B1 C14 C2 -110.6(3) . . . . ?
B4 B1 C14 B2 -102.1(3) . . . . ?
B5 B1 C14 B2 -140.7(2) . . . . ?
B3 B1 C14 B2 -38.8(2) . . . . ?
B4 B1 C14 B5 38.6(2) . . . . ?
B3 B1 C14 B5 101.9(3) . . . . ?
B2 B1 C14 B5 140.7(2) . . . . ?
B4 B1 C14 B6 -64.0(3) . . . . ?
B5 B1 C14 B6 -102.6(2) . . . . ?
B3 B1 C14 B6 -0.6(3) . . . . ?
B2 B1 C14 B6 38.2(2) . . . . ?
B4 B1 C14 C15 0.9(3) . . . . ?
B5 B1 C14 C15 -37.7(2) . . . . ?
B3 B1 C14 C15 64.2(3) . . . . ?
B2 B1 C14 C15 103.0(2) . . . . ?
C15 B5 C14 C2 111.8(3) . . . . ?
B9 B5 C14 C2 148.9(2) . . . . ?
B1 B5 C14 C2 -109.8(3) . . . . ?
B4 B5 C14 C2 -148.2(2) . . . . ?
C15 B5 C14 B2 -100.6(2) . . . . ?
B9 B5 C14 B2 -63.6(3) . . . . ?
B1 B5 C14 B2 37.8(2) . . . . ?
B4 B5 C14 B2 -0.7(3) . . . . ?
C15 B5 C14 B1 -138.4(2) . . . . ?
B9 B5 C14 B1 -101.3(3) . . . . ?
B4 B5 C14 B1 -38.5(2) . . . . ?
C15 B5 C14 B6 -32.3(2) . . . . ?
B9 B5 C14 B6 4.8(3) . . . . ?
B1 B5 C14 B6 106.2(2) . . . . ?
B4 B5 C14 B6 67.7(3) . . . . ?
B9 B5 C14 C15 37.1(2) . . . . ?
B1 B5 C14 C15 138.4(2) . . . . ?
B4 B5 C14 C15 100.0(2) . . . . ?
C15 B6 C14 C2 -111.2(3) . . . . ?
B10 B6 C14 C2 -148.9(2) . . . . ?
B7 B6 C14 C2 148.8(3) . . . . ?
B2 B6 C14 C2 110.3(3) . . . . ?
C15 B6 C14 B2 138.5(2) . . . . ?
B10 B6 C14 B2 100.7(2) . . . . ?
B7 B6 C14 B2 38.5(2) . . . . ?
C15 B6 C14 B1 100.3(2) . . . . ?
B10 B6 C14 B1 62.5(3) . . . . ?
B7 B6 C14 B1 0.3(3) . . . . ?
B2 B6 C14 B1 -38.2(2) . . . . ?
C15 B6 C14 B5 32.4(2) . . . . ?
B10 B6 C14 B5 -5.4(3) . . . . ?
B7 B6 C14 B5 -67.6(3) . . . . ?
B2 B6 C14 B5 -106.1(2) . . . . ?
B10 B6 C14 C15 -37.8(2) . . . . ?
B7 B6 C14 C15 -100.0(2) . . . . ?
B2 B6 C14 C15 -138.5(2) . . . . ?
B5 B9 C15 B10 140.0(2) . . . . ?
B4 B9 C15 B10 101.7(3) . . . . ?
B8 B9 C15 B10 38.3(2) . . . . ?
B10 B9 C15 B6 -37.2(2) . . . . ?
B5 B9 C15 B6 102.8(2) . . . . ?
B4 B9 C15 B6 64.5(3) . . . . ?
B8 B9 C15 B6 1.1(3) . . . . ?
B10 B9 C15 C14 -101.8(2) . . . . ?
B5 B9 C15 C14 38.2(2) . . . . ?
B4 B9 C15 C14 -0.1(3) . . . . ?
B8 B9 C15 C14 -63.4(3) . . . . ?
B10 B9 C15 B5 -140.0(2) . . . . ?
B4 B9 C15 B5 -38.3(2) . . . . ?
B8 B9 C15 B5 -101.6(3) . . . . ?
B10 B9 C15 Si28 109.6(2) . . . . ?
B5 B9 C15 Si28 -110.4(2) . . . . ?
B4 B9 C15 Si28 -148.73(19) . . . . ?
B8 B9 C15 Si28 147.95(19) . . . . ?
B7 B10 C15 B9 -102.2(3) . . . . ?
B8 B10 C15 B9 -38.7(2) . . . . ?
B6 B10 C15 B9 -140.8(2) . . . . ?
B9 B10 C15 B6 140.8(2) . . . . ?
B7 B10 C15 B6 38.6(2) . . . . ?
B8 B10 C15 B6 102.1(3) . . . . ?
B9 B10 C15 C14 101.9(2) . . . . ?
B7 B10 C15 C14 -0.3(3) . . . . ?
B8 B10 C15 C14 63.2(3) . . . . ?
B6 B10 C15 C14 -38.9(2) . . . . ?
B9 B10 C15 B5 37.7(2) . . . . ?
B7 B10 C15 B5 -64.4(3) . . . . ?
B8 B10 C15 B5 -1.0(3) . . . . ?
B6 B10 C15 B5 -103.1(2) . . . . ?
B9 B10 C15 Si28 -108.3(2) . . . . ?
B7 B10 C15 Si28 149.5(2) . . . . ?
B8 B10 C15 Si28 -147.1(2) . . . . ?
B6 B10 C15 Si28 110.9(2) . . . . ?
C14 B6 C15 B9 -99.5(2) . . . . ?
B10 B6 C15 B9 37.1(2) . . . . ?
B7 B6 C15 B9 -1.0(3) . . . . ?
B2 B6 C15 B9 -63.5(3) . . . . ?
C14 B6 C15 B10 -136.7(2) . . . . ?
B7 B6 C15 B10 -38.2(2) . . . . ?
B2 B6 C15 B10 -100.6(2) . . . . ?
B10 B6 C15 C14 136.7(2) . . . . ?
B7 B6 C15 C14 98.5(2) . . . . ?
B2 B6 C15 C14 36.07(19) . . . . ?
C14 B6 C15 B5 -32.2(2) . . . . ?
B10 B6 C15 B5 104.5(2) . . . . ?
B7 B6 C15 B5 66.3(3) . . . . ?
B2 B6 C15 B5 3.8(3) . . . . ?
C14 B6 C15 Si28 114.4(2) . . . . ?
B10 B6 C15 Si28 -108.9(2) . . . . ?
B7 B6 C15 Si28 -147.09(19) . . . . ?
B2 B6 C15 Si28 150.48(19) . . . . ?
C2 C14 C15 B9 -146.0(2) . . . . ?
B2 C14 C15 B9 66.8(3) . . . . ?
B1 C14 C15 B9 -0.5(3) . . . . ?
B5 C14 C15 B9 -39.2(2) . . . . ?
B6 C14 C15 B9 105.7(2) . . . . ?
C2 C14 C15 B10 148.1(2) . . . . ?
B2 C14 C15 B10 1.0(3) . . . . ?
B1 C14 C15 B10 -66.4(3) . . . . ?
B5 C14 C15 B10 -105.0(2) . . . . ?
B6 C14 C15 B10 39.8(2) . . . . ?
C2 C14 C15 B6 108.3(3) . . . . ?
B2 C14 C15 B6 -38.8(2) . . . . ?
B1 C14 C15 B6 -106.2(2) . . . . ?
B5 C14 C15 B6 -144.8(2) . . . . ?
C2 C14 C15 B5 -106.8(3) . . . . ?
B2 C14 C15 B5 106.0(2) . . . . ?
B1 C14 C15 B5 38.7(2) . . . . ?
B6 C14 C15 B5 144.8(2) . . . . ?
C2 C14 C15 Si28 0.3(3) . . . . ?
B2 C14 C15 Si28 -146.8(2) . . . . ?
B1 C14 C15 Si28 145.8(2) . . . . ?
B5 C14 C15 Si28 107.2(2) . . . . ?
B6 C14 C15 Si28 -108.0(2) . . . . ?
C14 B5 C15 B9 137.4(2) . . . . ?
B1 B5 C15 B9 101.1(3) . . . . ?
B4 B5 C15 B9 38.2(2) . . . . ?
C14 B5 C15 B10 99.6(2) . . . . ?
B9 B5 C15 B10 -37.8(2) . . . . ?
B1 B5 C15 B10 63.3(3) . . . . ?
B4 B5 C15 B10 0.5(3) . . . . ?
C14 B5 C15 B6 32.3(2) . . . . ?
B9 B5 C15 B6 -105.1(2) . . . . ?
B1 B5 C15 B6 -4.0(3) . . . . ?
B4 B5 C15 B6 -66.9(3) . . . . ?
B9 B5 C15 C14 -137.4(2) . . . . ?
B1 B5 C15 C14 -36.3(2) . . . . ?
B4 B5 C15 C14 -99.2(2) . . . . ?
C14 B5 C15 Si28 -114.5(2) . . . . ?
B9 B5 C15 Si28 108.1(2) . . . . ?
B1 B5 C15 Si28 -150.82(19) . . . . ?
B4 B5 C15 Si28 146.3(2) . . . . ?
C33 Si28 C29 C30 -31.1(3) . . . . ?
C31 Si28 C29 C30 -151.6(3) . . . . ?
C15 Si28 C29 C30 92.4(3) . . . . ?
C33 Si28 C31 C32 42.7(3) . . . . ?
C29 Si28 C31 C32 164.3(2) . . . . ?
C15 Si28 C31 C32 -78.5(3) . . . . ?
C29 Si28 C33 C34 -65.6(3) . . . . ?
C31 Si28 C33 C34 54.7(3) . . . . ?
C15 Si28 C33 C34 172.8(2) . . . . ?
C55 C41 C42 B51 -147.1(2) . . . . ?
B44 C41 C42 B51 -0.6(3) . . . . ?
B45 C41 C42 B51 66.9(3) . . . . ?
B43 C41 C42 B51 -39.1(2) . . . . ?
B46 C41 C42 B51 105.4(2) . . . . ?
C55 C41 C42 B46 107.5(3) . . . . ?
B44 C41 C42 B46 -106.0(2) . . . . ?
B45 C41 C42 B46 -38.6(2) . . . . ?
B43 C41 C42 B46 -144.5(2) . . . . ?
C55 C41 C42 B47 147.1(2) . . . . ?
B44 C41 C42 B47 -66.4(3) . . . . ?
B45 C41 C42 B47 1.0(3) . . . . ?
B43 C41 C42 B47 -105.0(2) . . . . ?
B46 C41 C42 B47 39.6(2) . . . . ?
C55 C41 C42 B43 -108.0(3) . . . . ?
B44 C41 C42 B43 38.5(2) . . . . ?
B45 C41 C42 B43 106.0(2) . . . . ?
B46 C41 C42 B43 144.5(2) . . . . ?
C55 C41 C42 Si68 -2.0(3) . . . . ?
B44 C41 C42 Si68 144.5(2) . . . . ?
B45 C41 C42 Si68 -148.0(2) . . . . ?
B43 C41 C42 Si68 106.0(2) . . . . ?
B46 C41 C42 Si68 -109.5(2) . . . . ?
C55 C41 B43 C42 110.7(3) . . . . ?
B44 C41 B43 C42 -138.5(2) . . . . ?
B45 C41 B43 C42 -100.6(2) . . . . ?
B46 C41 B43 C42 -32.3(2) . . . . ?
C55 C41 B43 B50 -149.3(2) . . . . ?
B44 C41 B43 B50 -38.5(2) . . . . ?
B45 C41 B43 B50 -0.5(3) . . . . ?
B46 C41 B43 B50 67.7(3) . . . . ?
C42 C41 B43 B50 100.0(2) . . . . ?
C55 C41 B43 B44 -110.8(3) . . . . ?
B45 C41 B43 B44 37.9(2) . . . . ?
B46 C41 B43 B44 106.2(2) . . . . ?
C42 C41 B43 B44 138.5(2) . . . . ?
C55 C41 B43 B51 147.6(2) . . . . ?
B44 C41 B43 B51 -101.5(3) . . . . ?
B45 C41 B43 B51 -63.6(3) . . . . ?
B46 C41 B43 B51 4.6(3) . . . . ?
C42 C41 B43 B51 37.0(2) . . . . ?
B51 C42 B43 C41 137.6(2) . . . . ?
B46 C42 B43 C41 32.6(2) . . . . ?
B47 C42 B43 C41 99.5(2) . . . . ?
Si68 C42 B43 C41 -115.4(2) . . . . ?
B51 C42 B43 B50 38.3(2) . . . . ?
B46 C42 B43 B50 -66.7(3) . . . . ?
B47 C42 B43 B50 0.3(3) . . . . ?
C41 C42 B43 B50 -99.2(2) . . . . ?
Si68 C42 B43 B50 145.3(2) . . . . ?
B51 C42 B43 B44 101.5(3) . . . . ?
B46 C42 B43 B44 -3.5(3) . . . . ?
B47 C42 B43 B44 63.5(3) . . . . ?
C41 C42 B43 B44 -36.1(2) . . . . ?
Si68 C42 B43 B44 -151.5(2) . . . . ?
B46 C42 B43 B51 -105.0(3) . . . . ?
B47 C42 B43 B51 -38.0(2) . . . . ?
C41 C42 B43 B51 -137.6(2) . . . . ?
Si68 C42 B43 B51 107.0(2) . . . . ?
C55 C41 B44 B43 109.3(3) . . . . ?
B45 C41 B44 B43 -140.6(2) . . . . ?
B46 C41 B44 B43 -102.0(2) . . . . ?
C42 C41 B44 B43 -37.5(2) . . . . ?
C55 C41 B44 B49 -149.0(3) . . . . ?
B45 C41 B44 B49 -38.9(2) . . . . ?
B43 C41 B44 B49 101.7(3) . . . . ?
B46 C41 B44 B49 -0.2(3) . . . . ?
C42 C41 B44 B49 64.2(3) . . . . ?
C55 C41 B44 B50 147.7(3) . . . . ?
B45 C41 B44 B50 -102.2(3) . . . . ?
B43 C41 B44 B50 38.5(2) . . . . ?
B46 C41 B44 B50 -63.5(3) . . . . ?
C42 C41 B44 B50 0.9(3) . . . . ?
C55 C41 B44 B45 -110.1(3) . . . . ?
B43 C41 B44 B45 140.6(2) . . . . ?
B46 C41 B44 B45 38.7(2) . . . . ?
C42 C41 B44 B45 103.1(2) . . . . ?
C42 B43 B44 C41 37.0(2) . . . . ?
B50 B43 B44 C41 136.4(2) . . . . ?
B51 B43 B44 C41 98.8(2) . . . . ?
C41 B43 B44 B49 -98.7(2) . . . . ?
C42 B43 B44 B49 -61.7(3) . . . . ?
B50 B43 B44 B49 37.7(2) . . . . ?
B51 B43 B44 B49 0.1(3) . . . . ?
C41 B43 B44 B50 -136.4(2) . . . . ?
C42 B43 B44 B50 -99.4(2) . . . . ?
B51 B43 B44 B50 -37.6(2) . . . . ?
C41 B43 B44 B45 -34.8(2) . . . . ?
C42 B43 B44 B45 2.2(3) . . . . ?
B50 B43 B44 B45 101.6(3) . . . . ?
B51 B43 B44 B45 64.0(3) . . . . ?
C55 C41 B45 B48 -147.8(2) . . . . ?
B44 C41 B45 B48 101.3(3) . . . . ?
B43 C41 B45 B48 63.6(3) . . . . ?
B46 C41 B45 B48 -38.5(2) . . . . ?
C42 C41 B45 B48 -1.3(3) . . . . ?
C55 C41 B45 B44 110.9(3) . . . . ?
B43 C41 B45 B44 -37.7(2) . . . . ?
B46 C41 B45 B44 -139.8(2) . . . . ?
C42 C41 B45 B44 -102.6(2) . . . . ?
C55 C41 B45 B49 149.2(2) . . . . ?
B44 C41 B45 B49 38.3(2) . . . . ?
B43 C41 B45 B49 0.7(3) . . . . ?
B46 C41 B45 B49 -101.5(2) . . . . ?
C42 C41 B45 B49 -64.3(3) . . . . ?
C55 C41 B45 B46 -109.3(3) . . . . ?
B44 C41 B45 B46 139.8(2) . . . . ?
B43 C41 B45 B46 102.1(2) . . . . ?
C42 C41 B45 B46 37.2(2) . . . . ?
B43 B44 B45 C41 35.1(2) . . . . ?
B49 B44 B45 C41 136.1(2) . . . . ?
B50 B44 B45 C41 98.5(3) . . . . ?
C41 B44 B45 B48 -98.3(2) . . . . ?
B43 B44 B45 B48 -63.2(3) . . . . ?
B49 B44 B45 B48 37.8(2) . . . . ?
B50 B44 B45 B48 0.1(3) . . . . ?
C41 B44 B45 B49 -136.1(2) . . . . ?
B43 B44 B45 B49 -101.0(3) . . . . ?
B50 B44 B45 B49 -37.7(2) . . . . ?
C41 B44 B45 B46 -35.3(2) . . . . ?
B43 B44 B45 B46 -0.2(3) . . . . ?
B49 B44 B45 B46 100.8(3) . . . . ?
B50 B44 B45 B46 63.1(3) . . . . ?
B51 C42 B46 C41 -99.9(2) . . . . ?
B47 C42 B46 C41 -136.8(2) . . . . ?
B43 C42 B46 C41 -32.5(2) . . . . ?
Si68 C42 B46 C41 114.5(2) . . . . ?
B51 C42 B46 B47 36.9(2) . . . . ?
B43 C42 B46 B47 104.3(2) . . . . ?
C41 C42 B46 B47 136.8(2) . . . . ?
Si68 C42 B46 B47 -108.7(2) . . . . ?
B51 C42 B46 B48 -1.4(3) . . . . ?
B47 C42 B46 B48 -38.3(2) . . . . ?
B43 C42 B46 B48 65.9(3) . . . . ?
C41 C42 B46 B48 98.4(2) . . . . ?
Si68 C42 B46 B48 -147.03(19) . . . . ?
B51 C42 B46 B45 -64.0(3) . . . . ?
B47 C42 B46 B45 -100.9(2) . . . . ?
B43 C42 B46 B45 3.4(3) . . . . ?
C41 C42 B46 B45 35.86(19) . . . . ?
Si68 C42 B46 B45 150.38(19) . . . . ?
C55 C41 B46 C42 -110.7(3) . . . . ?
B44 C41 B46 C42 100.1(2) . . . . ?
B45 C41 B46 C42 138.8(2) . . . . ?
B43 C41 B46 C42 32.4(2) . . . . ?
C55 C41 B46 B47 -148.6(2) . . . . ?
B44 C41 B46 B47 62.1(3) . . . . ?
B45 C41 B46 B47 100.9(3) . . . . ?
B43 C41 B46 B47 -5.5(3) . . . . ?
C42 C41 B46 B47 -38.0(2) . . . . ?
C55 C41 B46 B48 148.6(2) . . . . ?
B44 C41 B46 B48 -0.6(3) . . . . ?
B45 C41 B46 B48 38.2(2) . . . . ?
B43 C41 B46 B48 -68.2(3) . . . . ?
C42 C41 B46 B48 -100.7(2) . . . . ?
C55 C41 B46 B45 110.5(3) . . . . ?
B44 C41 B46 B45 -38.7(2) . . . . ?
B43 C41 B46 B45 -106.4(2) . . . . ?
C42 C41 B46 B45 -138.8(2) . . . . ?
C41 B45 B46 C42 -36.8(2) . . . . ?
B48 B45 B46 C42 99.5(2) . . . . ?
B44 B45 B46 C42 -1.8(3) . . . . ?
B49 B45 B46 C42 60.8(3) . . . . ?
B48 B45 B46 C41 136.3(2) . . . . ?
B44 B45 B46 C41 35.0(2) . . . . ?
B49 B45 B46 C41 97.7(3) . . . . ?
C41 B45 B46 B47 -99.2(2) . . . . ?
B48 B45 B46 B47 37.1(2) . . . . ?
B44 B45 B46 B47 -64.2(3) . . . . ?
B49 B45 B46 B47 -1.6(3) . . . . ?
C41 B45 B46 B48 -136.3(2) . . . . ?
B44 B45 B46 B48 -101.3(3) . . . . ?
B49 B45 B46 B48 -38.6(2) . . . . ?
B51 C42 B47 B52 -38.9(2) . . . . ?
B46 C42 B47 B52 102.1(3) . . . . ?
B43 C42 B47 B52 -0.8(3) . . . . ?
C41 C42 B47 B52 63.3(3) . . . . ?
Si68 C42 B47 B52 -145.7(2) . . . . ?
B46 C42 B47 B51 141.0(2) . . . . ?
B43 C42 B47 B51 38.1(2) . . . . ?
C41 C42 B47 B51 102.2(2) . . . . ?
Si68 C42 B47 B51 -106.8(2) . . . . ?
B51 C42 B47 B46 -141.0(2) . . . . ?
B43 C42 B47 B46 -102.9(2) . . . . ?
C41 C42 B47 B46 -38.8(2) . . . . ?
Si68 C42 B47 B46 112.2(2) . . . . ?
B51 C42 B47 B48 -102.5(3) . . . . ?
B46 C42 B47 B48 38.5(2) . . . . ?
B43 C42 B47 B48 -64.4(3) . . . . ?
C41 C42 B47 B48 -0.3(3) . . . . ?
Si68 C42 B47 B48 150.7(2) . . . . ?
C41 B46 B47 C42 38.5(2) . . . . ?
B48 B46 B47 C42 136.7(2) . . . . ?
B45 B46 B47 C42 99.8(2) . . . . ?
C42 B46 B47 B52 -98.9(2) . . . . ?
C41 B46 B47 B52 -60.3(3) . . . . ?
B48 B46 B47 B52 37.8(2) . . . . ?
B45 B46 B47 B52 0.9(3) . . . . ?
C42 B46 B47 B51 -34.4(2) . . . . ?
C41 B46 B47 B51 4.2(3) . . . . ?
B48 B46 B47 B51 102.3(3) . . . . ?
B45 B46 B47 B51 65.4(3) . . . . ?
C42 B46 B47 B48 -136.7(2) . . . . ?
C41 B46 B47 B48 -98.1(2) . . . . ?
B45 B46 B47 B48 -36.9(2) . . . . ?
C42 B47 B48 B45 -0.5(3) . . . . ?
B52 B47 B48 B45 -100.8(3) . . . . ?
B51 B47 B48 B45 -62.5(3) . . . . ?
B46 B47 B48 B45 37.4(2) . . . . ?
C42 B47 B48 B46 -37.9(2) . . . . ?
B52 B47 B48 B46 -138.2(2) . . . . ?
B51 B47 B48 B46 -99.9(2) . . . . ?
C42 B47 B48 B52 100.3(2) . . . . ?
B51 B47 B48 B52 38.3(2) . . . . ?
B46 B47 B48 B52 138.2(2) . . . . ?
C42 B47 B48 B49 63.1(3) . . . . ?
B52 B47 B48 B49 -37.2(2) . . . . ?
B51 B47 B48 B49 1.1(3) . . . . ?
B46 B47 B48 B49 101.0(2) . . . . ?
C41 B45 B48 B47 1.1(3) . . . . ?
B44 B45 B48 B47 62.3(3) . . . . ?
B49 B45 B48 B47 99.8(3) . . . . ?
B46 B45 B48 B47 -37.0(2) . . . . ?
C41 B45 B48 B46 38.1(2) . . . . ?
B44 B45 B48 B46 99.3(2) . . . . ?
B49 B45 B48 B46 136.8(3) . . . . ?
C41 B45 B48 B52 -62.0(3) . . . . ?
B44 B45 B48 B52 -0.8(3) . . . . ?
B49 B45 B48 B52 36.7(2) . . . . ?
B46 B45 B48 B52 -100.1(3) . . . . ?
C41 B45 B48 B49 -98.7(3) . . . . ?
B44 B45 B48 B49 -37.5(2) . . . . ?
B46 B45 B48 B49 -136.8(3) . . . . ?
C42 B46 B48 B47 38.0(2) . . . . ?
C41 B46 B48 B47 101.0(2) . . . . ?
B45 B46 B48 B47 138.5(2) . . . . ?
C42 B46 B48 B45 -100.6(2) . . . . ?
C41 B46 B48 B45 -37.5(2) . . . . ?
B47 B46 B48 B45 -138.5(2) . . . . ?
C42 B46 B48 B52 1.0(3) . . . . ?
C41 B46 B48 B52 64.1(3) . . . . ?
B47 B46 B48 B52 -37.0(2) . . . . ?
B45 B46 B48 B52 101.6(3) . . . . ?
C42 B46 B48 B49 -61.9(3) . . . . ?
C41 B46 B48 B49 1.1(3) . . . . ?
B47 B46 B48 B49 -99.9(3) . . . . ?
B45 B46 B48 B49 38.6(2) . . . . ?
C41 B44 B49 B52 -62.4(3) . . . . ?
B43 B44 B49 B52 0.3(3) . . . . ?
B50 B44 B49 B52 37.7(2) . . . . ?
B45 B44 B49 B52 -100.5(3) . . . . ?
C41 B44 B49 B50 -100.1(3) . . . . ?
B43 B44 B49 B50 -37.5(2) . . . . ?
B45 B44 B49 B50 -138.3(2) . . . . ?
C41 B44 B49 B45 38.2(2) . . . . ?
B43 B44 B49 B45 100.8(2) . . . . ?
B50 B44 B49 B45 138.3(2) . . . . ?
C41 B44 B49 B48 0.9(3) . . . . ?
B43 B44 B49 B48 63.6(3) . . . . ?
B50 B44 B49 B48 101.0(3) . . . . ?
B45 B44 B49 B48 -37.2(2) . . . . ?
C41 B45 B49 B44 -37.7(2) . . . . ?
B48 B45 B49 B44 -137.8(3) . . . . ?
B46 B45 B49 B44 -99.5(2) . . . . ?
C41 B45 B49 B52 63.4(3) . . . . ?
B48 B45 B49 B52 -36.8(2) . . . . ?
B44 B45 B49 B52 101.1(3) . . . . ?
B46 B45 B49 B52 1.6(3) . . . . ?
C41 B45 B49 B50 -0.5(3) . . . . ?
B48 B45 B49 B50 -100.7(3) . . . . ?
B44 B45 B49 B50 37.2(2) . . . . ?
B46 B45 B49 B50 -62.3(3) . . . . ?
C41 B45 B49 B48 100.2(2) . . . . ?
B44 B45 B49 B48 137.8(3) . . . . ?
B46 B45 B49 B48 38.4(2) . . . . ?
B47 B48 B49 B44 -64.2(3) . . . . ?
B45 B48 B49 B44 37.5(2) . . . . ?
B46 B48 B49 B44 -1.3(3) . . . . ?
B52 B48 B49 B44 -101.4(3) . . . . ?
B47 B48 B49 B52 37.2(2) . . . . ?
B45 B48 B49 B52 138.9(3) . . . . ?
B46 B48 B49 B52 100.1(3) . . . . ?
B47 B48 B49 B50 -1.2(3) . . . . ?
B45 B48 B49 B50 100.5(3) . . . . ?
B46 B48 B49 B50 61.8(3) . . . . ?
B52 B48 B49 B50 -38.3(2) . . . . ?
B47 B48 B49 B45 -101.7(3) . . . . ?
B46 B48 B49 B45 -38.8(2) . . . . ?
B52 B48 B49 B45 -138.9(3) . . . . ?
C41 B43 B50 B44 37.5(2) . . . . ?
C42 B43 B50 B44 100.6(2) . . . . ?
B51 B43 B50 B44 138.1(2) . . . . ?
C41 B43 B50 B51 -100.6(2) . . . . ?
C42 B43 B50 B51 -37.6(2) . . . . ?
B44 B43 B50 B51 -138.1(2) . . . . ?
C41 B43 B50 B49 0.2(3) . . . . ?
C42 B43 B50 B49 63.2(3) . . . . ?
B44 B43 B50 B49 -37.4(2) . . . . ?
B51 B43 B50 B49 100.8(3) . . . . ?
C41 B43 B50 B52 -62.7(3) . . . . ?
C42 B43 B50 B52 0.4(3) . . . . ?
B44 B43 B50 B52 -100.2(3) . . . . ?
B51 B43 B50 B52 37.9(2) . . . . ?
C41 B44 B50 B43 -38.3(2) . . . . ?
B49 B44 B50 B43 -138.0(2) . . . . ?
B45 B44 B50 B43 -100.3(2) . . . . ?
C41 B44 B50 B51 -1.0(3) . . . . ?
B43 B44 B50 B51 37.4(2) . . . . ?
B49 B44 B50 B51 -100.6(3) . . . . ?
B45 B44 B50 B51 -63.0(3) . . . . ?
C41 B44 B50 B49 99.7(3) . . . . ?
B43 B44 B50 B49 138.0(2) . . . . ?
B45 B44 B50 B49 37.7(2) . . . . ?
C41 B44 B50 B52 62.5(3) . . . . ?
B43 B44 B50 B52 100.9(3) . . . . ?
B49 B44 B50 B52 -37.1(2) . . . . ?
B45 B44 B50 B52 0.5(3) . . . . ?
B44 B49 B50 B43 37.4(2) . . . . ?
B52 B49 B50 B43 -100.6(2) . . . . ?
B45 B49 B50 B43 0.2(3) . . . . ?
B48 B49 B50 B43 -62.5(3) . . . . ?
B52 B49 B50 B44 -138.1(2) . . . . ?
B45 B49 B50 B44 -37.2(2) . . . . ?
B48 B49 B50 B44 -100.0(3) . . . . ?
B44 B49 B50 B51 100.8(3) . . . . ?
B52 B49 B50 B51 -37.3(2) . . . . ?
B45 B49 B50 B51 63.5(3) . . . . ?
B48 B49 B50 B51 0.8(3) . . . . ?
B44 B49 B50 B52 138.1(2) . . . . ?
B45 B49 B50 B52 100.8(3) . . . . ?
B48 B49 B50 B52 38.1(2) . . . . ?
B46 C42 B51 B47 -36.9(2) . . . . ?
B43 C42 B51 B47 -139.6(2) . . . . ?
C41 C42 B51 B47 -101.5(2) . . . . ?
Si68 C42 B51 B47 110.4(2) . . . . ?
B46 C42 B51 B43 102.7(2) . . . . ?
B47 C42 B51 B43 139.6(2) . . . . ?
C41 C42 B51 B43 38.1(2) . . . . ?
Si68 C42 B51 B43 -110.0(2) . . . . ?
B46 C42 B51 B50 64.6(3) . . . . ?
B47 C42 B51 B50 101.4(3) . . . . ?
B43 C42 B51 B50 -38.2(2) . . . . ?
C41 C42 B51 B50 -0.1(3) . . . . ?
Si68 C42 B51 B50 -148.2(2) . . . . ?
B46 C42 B51 B52 1.3(3) . . . . ?
B47 C42 B51 B52 38.1(2) . . . . ?
B43 C42 B51 B52 -101.5(3) . . . . ?
C41 C42 B51 B52 -63.3(3) . . . . ?
Si68 C42 B51 B52 148.55(19) . . . . ?
B52 B47 B51 C42 136.5(2) . . . . ?
B46 B47 B51 C42 34.5(2) . . . . ?
B48 B47 B51 C42 98.3(2) . . . . ?
C42 B47 B51 B43 -35.8(2) . . . . ?
B52 B47 B51 B43 100.7(3) . . . . ?
B46 B47 B51 B43 -1.4(3) . . . . ?
B48 B47 B51 B43 62.5(3) . . . . ?
C42 B47 B51 B50 -99.0(2) . . . . ?
B52 B47 B51 B50 37.6(2) . . . . ?
B46 B47 B51 B50 -64.5(3) . . . . ?
B48 B47 B51 B50 -0.6(3) . . . . ?
C42 B47 B51 B52 -136.5(2) . . . . ?
B46 B47 B51 B52 -102.1(3) . . . . ?
B48 B47 B51 B52 -38.2(2) . . . . ?
C41 B43 B51 C42 -37.7(2) . . . . ?
B50 B43 B51 C42 -136.7(3) . . . . ?
B44 B43 B51 C42 -99.1(2) . . . . ?
C41 B43 B51 B47 -1.9(3) . . . . ?
C42 B43 B51 B47 35.8(2) . . . . ?
B50 B43 B51 B47 -100.9(3) . . . . ?
B44 B43 B51 B47 -63.3(3) . . . . ?
C41 B43 B51 B50 99.0(3) . . . . ?
C42 B43 B51 B50 136.7(3) . . . . ?
B44 B43 B51 B50 37.6(2) . . . . ?
C41 B43 B51 B52 60.9(3) . . . . ?
C42 B43 B51 B52 98.7(3) . . . . ?
B50 B43 B51 B52 -38.1(2) . . . . ?
B44 B43 B51 B52 -0.5(3) . . . . ?
B43 B50 B51 C42 38.0(2) . . . . ?
B44 B50 B51 C42 0.6(3) . . . . ?
B49 B50 B51 C42 -62.5(3) . . . . ?
B52 B50 B51 C42 -99.6(3) . . . . ?
B43 B50 B51 B47 100.4(2) . . . . ?
B44 B50 B51 B47 63.1(3) . . . . ?
B49 B50 B51 B47 -0.1(3) . . . . ?
B52 B50 B51 B47 -37.2(2) . . . . ?
B44 B50 B51 B43 -37.4(2) . . . . ?
B49 B50 B51 B43 -100.5(3) . . . . ?
B52 B50 B51 B43 -137.6(3) . . . . ?
B43 B50 B51 B52 137.6(3) . . . . ?
B44 B50 B51 B52 100.2(3) . . . . ?
B49 B50 B51 B52 37.1(2) . . . . ?
C42 B47 B52 B49 -62.2(3) . . . . ?
B51 B47 B52 B49 -100.1(3) . . . . ?
B46 B47 B52 B49 0.1(3) . . . . ?
B48 B47 B52 B49 37.8(2) . . . . ?
C42 B47 B52 B48 -99.9(2) . . . . ?
B51 B47 B52 B48 -137.9(2) . . . . ?
B46 B47 B52 B48 -37.7(2) . . . . ?
C42 B47 B52 B51 37.9(2) . . . . ?
B46 B47 B52 B51 100.2(2) . . . . ?
B48 B47 B52 B51 137.9(2) . . . . ?
C42 B47 B52 B50 1.0(3) . . . . ?
B51 B47 B52 B50 -36.9(2) . . . . ?
B46 B47 B52 B50 63.3(3) . . . . ?
B48 B47 B52 B50 101.0(3) . . . . ?
B44 B49 B52 B47 62.3(3) . . . . ?
B50 B49 B52 B47 99.8(3) . . . . ?
B45 B49 B52 B47 -1.0(3) . . . . ?
B48 B49 B52 B47 -37.6(2) . . . . ?
B44 B49 B52 B48 99.9(3) . . . . ?
B50 B49 B52 B48 137.3(3) . . . . ?
B45 B49 B52 B48 36.5(2) . . . . ?
B44 B49 B52 B51 -0.5(3) . . . . ?
B50 B49 B52 B51 36.9(2) . . . . ?
B45 B49 B52 B51 -63.9(3) . . . . ?
B48 B49 B52 B51 -100.4(3) . . . . ?
B44 B49 B52 B50 -37.4(2) . . . . ?
B45 B49 B52 B50 -100.8(3) . . . . ?
B48 B49 B52 B50 -137.3(3) . . . . ?
B45 B48 B52 B47 101.0(3) . . . . ?
B46 B48 B52 B47 37.1(2) . . . . ?
B49 B48 B52 B47 137.9(2) . . . . ?
B47 B48 B52 B49 -137.9(2) . . . . ?
B45 B48 B52 B49 -37.0(2) . . . . ?
B46 B48 B52 B49 -100.9(2) . . . . ?
B47 B48 B52 B51 -37.3(2) . . . . ?
B45 B48 B52 B51 63.7(3) . . . . ?
B46 B48 B52 B51 -0.2(3) . . . . ?
B49 B48 B52 B51 100.7(3) . . . . ?
B47 B48 B52 B50 -99.9(3) . . . . ?
B45 B48 B52 B50 1.1(3) . . . . ?
B46 B48 B52 B50 -62.9(3) . . . . ?
B49 B48 B52 B50 38.0(2) . . . . ?
C42 B51 B52 B47 -38.1(2) . . . . ?
B43 B51 B52 B47 -100.4(3) . . . . ?
B50 B51 B52 B47 -138.2(3) . . . . ?
C42 B51 B52 B49 63.0(3) . . . . ?
B47 B51 B52 B49 101.0(3) . . . . ?
B43 B51 B52 B49 0.6(3) . . . . ?
B50 B51 B52 B49 -37.1(2) . . . . ?
C42 B51 B52 B48 -0.6(3) . . . . ?
B47 B51 B52 B48 37.5(2) . . . . ?
B43 B51 B52 B48 -63.0(3) . . . . ?
B50 B51 B52 B48 -100.7(3) . . . . ?
C42 B51 B52 B50 100.1(2) . . . . ?
B47 B51 B52 B50 138.2(3) . . . . ?
B43 B51 B52 B50 37.8(2) . . . . ?
B43 B50 B52 B47 -0.9(3) . . . . ?
B44 B50 B52 B47 -64.1(3) . . . . ?
B51 B50 B52 B47 37.0(2) . . . . ?
B49 B50 B52 B47 -101.3(3) . . . . ?
B43 B50 B52 B49 100.5(3) . . . . ?
B44 B50 B52 B49 37.2(2) . . . . ?
B51 B50 B52 B49 138.3(3) . . . . ?
B43 B50 B52 B48 62.3(3) . . . . ?
B44 B50 B52 B48 -1.0(3) . . . . ?
B51 B50 B52 B48 100.1(3) . . . . ?
B49 B50 B52 B48 -38.2(2) . . . . ?
B43 B50 B52 B51 -37.8(2) . . . . ?
B44 B50 B52 B51 -101.1(3) . . . . ?
B49 B50 B52 B51 -138.3(3) . . . . ?
C58 C53 C54 C55 2.1(4) . . . . ?
C65 C53 C54 C55 -177.8(3) . . . . ?
C53 C54 C55 C56 -2.9(4) . . . . ?
C53 C54 C55 C41 -178.9(3) . . . . ?
B44 C41 C55 C56 -47.5(4) . . . . ?
B45 C41 C55 C56 -121.4(3) . . . . ?
B43 C41 C55 C56 25.4(4) . . . . ?
B46 C41 C55 C56 165.4(3) . . . . ?
C42 C41 C55 C56 95.6(3) . . . . ?
B44 C41 C55 C54 128.5(3) . . . . ?
B45 C41 C55 C54 54.6(4) . . . . ?
B43 C41 C55 C54 -158.6(3) . . . . ?
B46 C41 C55 C54 -18.6(4) . . . . ?
C42 C41 C55 C54 -88.4(3) . . . . ?
C54 C55 C56 C57 1.8(4) . . . . ?
C41 C55 C56 C57 177.9(3) . . . . ?
C55 C56 C57 C58 0.0(4) . . . . ?
C56 C57 C58 C53 -0.8(4) . . . . ?
C56 C57 C58 C59 178.3(3) . . . . ?
C54 C53 C58 C57 -0.3(4) . . . . ?
C65 C53 C58 C57 179.7(3) . . . . ?
C54 C53 C58 C59 -179.5(3) . . . . ?
C65 C53 C58 C59 0.4(3) . . . . ?
C57 C58 C59 C64 -178.9(3) . . . . ?
C53 C58 C59 C64 0.3(3) . . . . ?
C57 C58 C59 C60 1.7(6) . . . . ?
C53 C58 C59 C60 -179.2(3) . . . . ?
C64 C59 C60 C61 0.5(5) . . . . ?
C58 C59 C60 C61 179.9(3) . . . . ?
C59 C60 C61 C62 0.2(5) . . . . ?
C60 C61 C62 C63 -0.8(5) . . . . ?
C61 C62 C63 C64 0.6(5) . . . . ?
C62 C63 C64 C59 0.0(5) . . . . ?
C62 C63 C64 C65 -179.1(3) . . . . ?
C60 C59 C64 C63 -0.6(5) . . . . ?
C58 C59 C64 C63 179.9(3) . . . . ?
C60 C59 C64 C65 178.7(3) . . . . ?
C58 C59 C64 C65 -0.8(3) . . . . ?
C54 C53 C65 C64 179.1(3) . . . . ?
C58 C53 C65 C64 -0.8(3) . . . . ?
C54 C53 C65 C66 -62.3(4) . . . . ?
C58 C53 C65 C66 117.8(3) . . . . ?
C54 C53 C65 C67 61.0(4) . . . . ?
C58 C53 C65 C67 -118.9(3) . . . . ?
C63 C64 C65 C53 -179.8(3) . . . . ?
C59 C64 C65 C53 1.0(3) . . . . ?
C63 C64 C65 C66 61.9(4) . . . . ?
C59 C64 C65 C66 -117.3(3) . . . . ?
C63 C64 C65 C67 -62.2(4) . . . . ?
C59 C64 C65 C67 118.5(3) . . . . ?
C73 Si68 C69 C70 49.1(5) . . . . ?
C71 Si68 C69 C70 -64.5(3) . . . . ?
C71B Si68 C69 C70 -76.9(10) . . . . ?
C73B Si68 C69 C70 62.7(5) . . . . ?
C42 Si68 C69 C70 172.5(3) . . . . ?
C73 Si68 C71 C72 -155.2(5) . . . . ?
C69 Si68 C71 C72 -33.8(4) . . . . ?
C42 Si68 C71 C72 90.8(4) . . . . ?
C71 Si68 C73 C74 163.5(7) . . . . ?
C69 Si68 C73 C74 41.2(8) . . . . ?
C42 Si68 C73 C74 -83.3(7) . . . . ?
C69 Si68 C71B C72B 171(2) . . . . ?
C73B Si68 C71B C72B 58(3) . . . . ?
C42 Si68 C71B C72B -77(2) . . . . ?
