#------------------------------------------------------------------------------
#$Date: 2025-04-05 06:24:55 +0300 (Sat, 05 Apr 2025) $
#$Revision: 298948 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/71/75/7717587.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7717587
loop_
_publ_author_name
'Kim, Soyeon'
'You, Dong Kyun'
'Kim, Namkyun'
'Shin, Ilsup'
'Kim, Dongwook'
'Lee, Kang Mun'
_publ_section_title
;
 Modulating radiative efficiency in ortho-carboranyl luminophores
 through electron-donating substituents: insights from
 intramolecular-charge-transfer-based emissions.
;
_journal_issue                   3
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1164
_journal_page_last               1172
_journal_paper_doi               10.1039/d4dt02897j
_journal_volume                  54
_journal_year                    2025
_chemical_formula_sum            'C35 H38 B10 Si'
_chemical_formula_weight         594.84
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_audit_block_doi                 10.5517/ccdc.csd.cc2l61xs
_audit_creation_method           SHELXL-2019/3
_audit_update_record
;
2024-10-07 deposited with the CCDC.	2024-11-25 downloaded from the CCDC.
;
_cell_angle_alpha                103.837(2)
_cell_angle_beta                 95.280(2)
_cell_angle_gamma                99.771(2)
_cell_formula_units_Z            4
_cell_length_a                   11.5149(7)
_cell_length_b                   14.8401(10)
_cell_length_c                   21.6004(15)
_cell_measurement_reflns_used    9609
_cell_measurement_temperature    203(2)
_cell_measurement_theta_max      25.97
_cell_measurement_theta_min      2.72
_cell_volume                     3497.9(4)
_computing_cell_refinement       'Bruker APEX5 software'
_computing_data_collection       'Bruker APEX5 software'
_computing_data_reduction        'Bruker APEX5 software'
_computing_molecular_graphics    ORTEP
_computing_publication_material  CIFTAB
_computing_structure_refinement  'SHELXL-2019/2 (Sheldrick, 2019)'
_computing_structure_solution    'SHELXS-2013/1 (Sheldrick, 2013)'
_diffrn_ambient_temperature      203(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'PHOTON II 14 CPAD detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1092
_diffrn_reflns_av_unetI/netI     0.0656
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.994
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            101254
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.994
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.983
_diffrn_reflns_theta_min         2.477
_diffrn_source                   'IuS 3.0 Microfocus'
_exptl_absorpt_coefficient_mu    0.092
_exptl_absorpt_correction_T_max  0.7453
_exptl_absorpt_correction_T_min  0.6532
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.130
_exptl_crystal_description       plate
_exptl_crystal_F_000             1248
_exptl_crystal_size_max          0.159
_exptl_crystal_size_mid          0.132
_exptl_crystal_size_min          0.039
_refine_diff_density_max         0.275
_refine_diff_density_min         -0.290
_refine_diff_density_rms         0.049
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.084
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     978
_refine_ls_number_reflns         13635
_refine_ls_number_restraints     954
_refine_ls_restrained_S_all      1.050
_refine_ls_R_factor_all          0.1139
_refine_ls_R_factor_gt           0.0680
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0282P)²+2.7221P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1155
_refine_ls_wR_factor_ref         0.1368
_reflns_Friedel_coverage         0.000
_reflns_number_gt                8887
_reflns_number_total             13635
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d4dt02897j2.cif
_cod_data_source_block           6CP
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'MULTI-SCAN' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 

 Adding full bibliography for 7717582--7717587.cif.
;
_cod_database_code               7717587
_shelx_shelxl_version_number     2019/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.986
_shelx_estimated_absorpt_t_max   0.996
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
B1 B 0.5301(3) 0.4215(2) 0.57848(15) 0.0352(7) Uani 1 1 d . . . . .
H1 H 0.475953 0.401111 0.529678 0.042 Uiso 1 1 calc R U . . .
B2 B 0.6382(3) 0.5292(2) 0.60628(15) 0.0376(7) Uani 1 1 d . . . . .
H2 H 0.653802 0.580905 0.576281 0.045 Uiso 1 1 calc R U . . .
B3 B 0.7566(3) 0.5069(2) 0.65594(15) 0.0362(7) Uani 1 1 d . . . . .
H3 H 0.850982 0.543847 0.658966 0.043 Uiso 1 1 calc R U . . .
B4 B 0.7190(3) 0.3864(2) 0.65808(14) 0.0335(7) Uani 1 1 d . . . . .
H4 H 0.788656 0.342849 0.661563 0.040 Uiso 1 1 calc R U . . .
B5 B 0.5887(3) 0.3710(2) 0.69526(14) 0.0351(7) Uani 1 1 d . . . . .
H5 H 0.572648 0.318141 0.724441 0.042 Uiso 1 1 calc R U . . .
B6 B 0.6986(3) 0.4772(2) 0.72344(15) 0.0365(7) Uani 1 1 d . . . . .
H6 H 0.754973 0.495019 0.771461 0.044 Uiso 1 1 calc R U . . .
B7 B 0.6478(3) 0.5660(2) 0.69165(16) 0.0401(8) Uani 1 1 d . . . . .
H7 H 0.670001 0.642613 0.718611 0.048 Uiso 1 1 calc R U . . .
B8 B 0.5080(3) 0.5134(2) 0.64324(16) 0.0409(8) Uani 1 1 d . . . . .
H8 H 0.437502 0.555661 0.637880 0.049 Uiso 1 1 calc R U . . .
B9 B 0.4708(3) 0.3936(2) 0.64615(15) 0.0370(7) Uani 1 1 d . . . . .
H9 H 0.376274 0.356673 0.642615 0.044 Uiso 1 1 calc R U . . .
B10 B 0.5447(3) 0.4822(2) 0.71641(15) 0.0382(7) Uani 1 1 d . . . . .
H10 H 0.499282 0.503618 0.759736 0.046 Uiso 1 1 calc R U . . .
C1 C 0.8546(2) 0.36591(18) 0.54041(13) 0.0341(6) Uani 1 1 d . . . . .
H1A H 0.890232 0.366276 0.581945 0.041 Uiso 1 1 calc R U . . .
C2 C 0.7445(2) 0.39255(18) 0.53265(12) 0.0318(6) Uani 1 1 d . . . . .
C3 C 0.6967(2) 0.39673(19) 0.47192(13) 0.0368(6) Uani 1 1 d . . . . .
H3A H 0.623153 0.416823 0.466905 0.044 Uiso 1 1 calc R U . . .
C4 C 0.7546(2) 0.37209(19) 0.41882(13) 0.0369(6) Uani 1 1 d . . . . .
H4A H 0.721647 0.375744 0.377743 0.044 Uiso 1 1 calc R U . . .
C5 C 0.9279(3) 0.2977(2) 0.31321(15) 0.0510(8) Uani 1 1 d . . . . .
H5A H 0.864308 0.316830 0.291728 0.061 Uiso 1 1 calc R U . . .
C6 C 1.0125(3) 0.2595(2) 0.27945(17) 0.0601(9) Uani 1 1 d . . . . .
H6A H 1.006841 0.252173 0.234295 0.072 Uiso 1 1 calc R U . . .
C7 C 1.1049(3) 0.2320(2) 0.31091(18) 0.0616(10) Uani 1 1 d . . . . .
H7A H 1.161497 0.205202 0.286932 0.074 Uiso 1 1 calc R U . . .
C8 C 1.1165(3) 0.2429(2) 0.37696(17) 0.0538(8) Uani 1 1 d . . . . .
H8A H 1.180476 0.223905 0.398249 0.065 Uiso 1 1 calc R U . . .
C9 C 1.0270(2) 0.3021(2) 0.48320(14) 0.0402(7) Uani 1 1 d . . . . .
C10 C 0.9115(2) 0.33893(18) 0.48707(13) 0.0350(6) Uani 1 1 d . . . . .
C11 C 0.8613(2) 0.34205(18) 0.42636(13) 0.0354(6) Uani 1 1 d . . . . .
C12 C 0.9382(2) 0.30738(19) 0.37895(14) 0.0407(7) Uani 1 1 d . . . . .
C13 C 1.0330(2) 0.28193(19) 0.41132(14) 0.0421(7) Uani 1 1 d . . . . .
C14 C 0.6813(2) 0.42200(18) 0.58995(12) 0.0307(6) Uani 1 1 d . . . . .
C15 C 0.5790(2) 0.33904(18) 0.61379(12) 0.0310(6) Uani 1 1 d . . . . .
C16 C 1.0206(3) 0.2127(2) 0.50722(18) 0.0618(9) Uani 1 1 d . . . . .
H16A H 1.092541 0.187017 0.499790 0.093 Uiso 1 1 calc R U . . .
H16B H 0.950526 0.165494 0.483885 0.093 Uiso 1 1 calc R U . . .
H16C H 1.014585 0.228369 0.553386 0.093 Uiso 1 1 calc R U . . .
C17 C 1.1330(2) 0.3789(2) 0.52144(15) 0.0564(9) Uani 1 1 d . . . . .
H17A H 1.206837 0.355088 0.516422 0.085 Uiso 1 1 calc R U . . .
H17B H 1.122967 0.395076 0.567091 0.085 Uiso 1 1 calc R U . . .
H17C H 1.136695 0.435406 0.505182 0.085 Uiso 1 1 calc R U . . .
Si1 Si 0.54054(6) 0.20501(5) 0.56942(3) 0.03297(18) Uani 1 1 d . . . . .
C18 C 0.5485(2) 0.18886(19) 0.48144(12) 0.0352(6) Uani 1 1 d . . . . .
C19 C 0.4663(2) 0.2188(2) 0.44272(13) 0.0429(7) Uani 1 1 d . . . . .
H19 H 0.405953 0.247768 0.461553 0.051 Uiso 1 1 calc R U . . .
C20 C 0.4714(3) 0.2068(2) 0.37739(14) 0.0519(8) Uani 1 1 d . . . . .
H20 H 0.415880 0.228190 0.351864 0.062 Uiso 1 1 calc R U . . .
C21 C 0.5583(3) 0.1633(2) 0.34969(15) 0.0572(9) Uani 1 1 d . . . . .
H21 H 0.562754 0.155426 0.305079 0.069 Uiso 1 1 calc R U . . .
C22 C 0.6378(3) 0.1315(2) 0.38642(15) 0.0538(8) Uani 1 1 d . . . . .
H22 H 0.695952 0.100496 0.366905 0.065 Uiso 1 1 calc R U . . .
C23 C 0.6337(2) 0.14439(19) 0.45175(14) 0.0419(7) Uani 1 1 d . . . . .
H23 H 0.689804 0.122618 0.476709 0.050 Uiso 1 1 calc R U . . .
C24 C 0.6470(2) 0.14506(18) 0.60752(12) 0.0348(6) Uani 1 1 d . . . . .
C25 C 0.7693(2) 0.1629(2) 0.60383(13) 0.0403(7) Uani 1 1 d . . . . .
H25 H 0.799538 0.206110 0.580345 0.048 Uiso 1 1 calc R U . . .
C26 C 0.8476(3) 0.1195(2) 0.63337(14) 0.0466(7) Uani 1 1 d . . . . .
H26 H 0.930168 0.133878 0.630528 0.056 Uiso 1 1 calc R U . . .
C27 C 0.8054(3) 0.0552(2) 0.66694(15) 0.0537(8) Uani 1 1 d . . . . .
H27 H 0.858630 0.025398 0.687389 0.064 Uiso 1 1 calc R U . . .
C28 C 0.6853(3) 0.0348(2) 0.67045(15) 0.0536(8) Uani 1 1 d . . . . .
H28 H 0.655707 -0.009952 0.692964 0.064 Uiso 1 1 calc R U . . .
C29 C 0.6072(3) 0.0790(2) 0.64146(13) 0.0439(7) Uani 1 1 d . . . . .
H29 H 0.524770 0.064125 0.644704 0.053 Uiso 1 1 calc R U . . .
C30 C 0.3849(2) 0.15239(18) 0.57910(13) 0.0351(6) Uani 1 1 d . . . . .
C31 C 0.3407(2) 0.1658(2) 0.63824(13) 0.0420(7) Uani 1 1 d . . . . .
H31 H 0.388583 0.207981 0.675434 0.050 Uiso 1 1 calc R U . . .
C32 C 0.2284(2) 0.1187(2) 0.64386(15) 0.0455(7) Uani 1 1 d . . . . .
H32 H 0.200115 0.129585 0.684409 0.055 Uiso 1 1 calc R U . . .
C33 C 0.1584(2) 0.0563(2) 0.59052(15) 0.0426(7) Uani 1 1 d . . . . .
H33 H 0.082143 0.023499 0.594367 0.051 Uiso 1 1 calc R U . . .
C34 C 0.1992(2) 0.04167(19) 0.53155(14) 0.0410(7) Uani 1 1 d . . . . .
H34 H 0.150536 -0.000621 0.494651 0.049 Uiso 1 1 calc R U . . .
C35 C 0.3117(2) 0.08873(19) 0.52595(13) 0.0374(6) Uani 1 1 d . . . . .
H35 H 0.339181 0.077311 0.485179 0.045 Uiso 1 1 calc R U . . .
B1B B 0.1551(3) 0.4555(2) 0.89401(16) 0.0391(7) Uani 1 1 d . . . . .
H1B H 0.180786 0.481495 0.947455 0.047 Uiso 1 1 calc R U . . .
B2B B 0.0190(3) 0.4702(3) 0.85488(17) 0.0438(8) Uani 1 1 d . . . . .
H2B H -0.044983 0.507216 0.882227 0.053 Uiso 1 1 calc R U . . .
B3B B -0.0302(3) 0.3708(3) 0.78749(15) 0.0418(8) Uani 1 1 d . . . . .
H3B H -0.127078 0.341648 0.769944 0.050 Uiso 1 1 calc R U . . .
B4B B 0.0755(3) 0.2963(2) 0.78655(14) 0.0376(7) Uani 1 1 d . . . . .
H4B H 0.048755 0.217301 0.769226 0.045 Uiso 1 1 calc R U . . .
B5B B 0.2136(3) 0.3580(2) 0.77389(15) 0.0387(7) Uani 1 1 d . . . . .
H5B H 0.278067 0.320437 0.747388 0.046 Uiso 1 1 calc R U . . .
B6B B 0.0770(3) 0.3710(3) 0.73387(16) 0.0434(8) Uani 1 1 d . . . . .
H6B H 0.050805 0.341959 0.680620 0.052 Uiso 1 1 calc R U . . .
B7B B 0.0435(3) 0.4798(3) 0.77610(17) 0.0473(9) Uani 1 1 d . . . . .
H7B H -0.004221 0.523607 0.750951 0.057 Uiso 1 1 calc R U . . .
B8B B 0.1574(3) 0.5322(3) 0.84256(17) 0.0433(8) Uani 1 1 d . . . . .
H8B H 0.184783 0.610843 0.861753 0.052 Uiso 1 1 calc R U . . .
B9B B 0.2623(3) 0.4574(2) 0.84057(15) 0.0388(7) Uani 1 1 d . . . . .
H9B H 0.359121 0.486240 0.858334 0.047 Uiso 1 1 calc R U . . .
B10B B 0.1930(3) 0.4718(3) 0.76720(17) 0.0443(8) Uani 1 1 d . . . . .
H10B H 0.243548 0.509917 0.736050 0.053 Uiso 1 1 calc R U . . .
C1B C -0.1072(17) 0.2133(12) 0.8662(9) 0.031(2) Uani 0.586(17) 1 d . U P A 1
H1BA H -0.119137 0.188382 0.820796 0.037 Uiso 0.586(17) 1 calc R U P A 1
C2B C -0.0293(19) 0.3004(13) 0.8942(7) 0.027(3) Uani 0.586(17) 1 d . U P A 1
C3B C -0.0232(16) 0.3371(10) 0.9621(10) 0.035(3) Uani 0.586(17) 1 d . U P A 1
H3BA H 0.023458 0.398168 0.982199 0.042 Uiso 0.586(17) 1 calc R U P A 1
C4B C -0.0843(13) 0.2853(9) 1.0000(7) 0.036(3) Uani 0.586(17) 1 d . U P A 1
H4BA H -0.078381 0.310998 1.045123 0.043 Uiso 0.586(17) 1 calc R U P A 1
C5B C -0.2305(8) 0.1249(7) 1.0613(4) 0.058(2) Uani 0.586(17) 1 d G U P A 1
H5BA H -0.190141 0.176198 1.096080 0.069 Uiso 0.586(17) 1 calc R U P A 1
C6B C -0.3016(8) 0.0472(7) 1.0734(4) 0.057(2) Uani 0.586(17) 1 d G U P A 1
H6BA H -0.309911 0.045365 1.116424 0.069 Uiso 0.586(17) 1 calc R U P A 1
C7B C -0.3607(7) -0.0279(6) 1.0224(4) 0.057(2) Uani 0.586(17) 1 d G U P A 1
H7BA H -0.409295 -0.080990 1.030697 0.069 Uiso 0.586(17) 1 calc R U P A 1
C8B C -0.3486(8) -0.0252(6) 0.9594(4) 0.0537(19) Uani 0.586(17) 1 d G U P A 1
H8BA H -0.388911 -0.076514 0.924625 0.064 Uiso 0.586(17) 1 calc R U P A 1
C13B C -0.2774(9) 0.0525(7) 0.9473(4) 0.0452(19) Uani 0.586(17) 1 d G U P A 1
C12B C -0.2184(8) 0.1276(7) 0.9983(4) 0.0403(19) Uani 0.586(17) 1 d G U P A 1
C9B C -0.2540(17) 0.0692(12) 0.8835(8) 0.045(3) Uani 0.586(17) 1 d . U P A 1
C10B C -0.1662(17) 0.1639(12) 0.9040(7) 0.034(3) Uani 0.586(17) 1 d . U P A 1
C11B C -0.1523(14) 0.1979(9) 0.9712(8) 0.039(3) Uani 0.586(17) 1 d . U P A 1
C16B C -0.2016(14) -0.0060(12) 0.8419(7) 0.050(3) Uani 0.586(17) 1 d . U P A 1
H16D H -0.184107 0.012083 0.802507 0.074 Uiso 0.586(17) 1 calc R U P A 1
H16E H -0.258697 -0.066407 0.830695 0.074 Uiso 0.586(17) 1 calc R U P A 1
H16F H -0.128055 -0.012731 0.865480 0.074 Uiso 0.586(17) 1 calc R U P A 1
C17B C -0.3643(15) 0.0916(19) 0.8499(12) 0.065(5) Uani 0.586(17) 1 d . U P A 1
H17D H -0.346396 0.106311 0.809460 0.097 Uiso 0.586(17) 1 calc R U P A 1
H17E H -0.387262 0.146148 0.877904 0.097 Uiso 0.586(17) 1 calc R U P A 1
H17F H -0.429838 0.036627 0.840638 0.097 Uiso 0.586(17) 1 calc R U P A 1
C18B C 0.2301(13) 0.2816(9) 0.9747(4) 0.033(2) Uani 0.58(3) 1 d G U P B 1
C19B C 0.1747(12) 0.2000(8) 0.9893(4) 0.044(2) Uani 0.58(3) 1 d G U P B 1
H19B H 0.152331 0.142220 0.956629 0.053 Uiso 0.58(3) 1 calc R U P B 1
C20B C 0.1520(11) 0.2029(9) 1.0518(5) 0.049(2) Uani 0.58(3) 1 d G U P B 1
H20B H 0.114139 0.147141 1.061806 0.059 Uiso 0.58(3) 1 calc R U P B 1
C21B C 0.1847(10) 0.2875(10) 1.0997(4) 0.047(2) Uani 0.58(3) 1 d G U P B 1
H21B H 0.169171 0.289485 1.142351 0.056 Uiso 0.58(3) 1 calc R U P B 1
C22B C 0.2401(11) 0.3691(9) 1.0850(4) 0.044(2) Uani 0.58(3) 1 d G U P B 1
H22B H 0.262396 0.426908 1.117719 0.052 Uiso 0.58(3) 1 calc R U P B 1
C23B C 0.2627(12) 0.3662(8) 1.0225(5) 0.0375(18) Uani 0.58(3) 1 d G U P B 1
H23B H 0.300590 0.421988 1.012542 0.045 Uiso 0.58(3) 1 calc R U P B 1
Si1B Si 0.27041(6) 0.27406(6) 0.89210(3) 0.03460(18) Uani 1 1 d . . . . .
C14B C 0.0407(2) 0.3605(2) 0.85766(13) 0.0360(6) Uani 1 1 d . . . . .
C15B C 0.1878(2) 0.35219(19) 0.84980(12) 0.0332(6) Uani 1 1 d . . . . .
C24B C 0.2419(2) 0.1516(2) 0.83733(13) 0.0378(6) Uani 1 1 d . . . . .
C25B C 0.3347(2) 0.1165(2) 0.80853(13) 0.0419(7) Uani 1 1 d . . . . .
H25B H 0.411689 0.155687 0.816518 0.050 Uiso 1 1 calc R U . . .
C26B C 0.3166(3) 0.0256(2) 0.76855(14) 0.0490(8) Uani 1 1 d . . . . .
H26B H 0.381210 0.003442 0.749706 0.059 Uiso 1 1 calc R U . . .
C27B C 0.2062(3) -0.0328(2) 0.75583(14) 0.0512(8) Uani 1 1 d . . . . .
H27B H 0.194112 -0.094814 0.728095 0.061 Uiso 1 1 calc R U . . .
C28B C 0.1130(3) 0.0000(2) 0.78399(15) 0.0524(8) Uani 1 1 d . . . . .
H28B H 0.036445 -0.039847 0.775873 0.063 Uiso 1 1 calc R U . . .
C29B C 0.1310(3) 0.0907(2) 0.82393(14) 0.0455(7) Uani 1 1 d . . . . .
H29B H 0.065936 0.112051 0.842770 0.055 Uiso 1 1 calc R U . . .
C30B C 0.4347(2) 0.3222(2) 0.90489(13) 0.0376(6) Uani 1 1 d . . . . .
C31B C 0.4990(2) 0.3476(2) 0.85779(14) 0.0445(7) Uani 1 1 d . . . . .
H31B H 0.457678 0.347058 0.817521 0.053 Uiso 1 1 calc R U . . .
C32B C 0.6218(2) 0.3735(2) 0.86876(15) 0.0486(8) Uani 1 1 d . . . . .
H32B H 0.663569 0.390204 0.835914 0.058 Uiso 1 1 calc R U . . .
C33B C 0.6841(3) 0.3754(2) 0.92670(15) 0.0520(8) Uani 1 1 d . . . . .
H33B H 0.768335 0.394142 0.934117 0.062 Uiso 1 1 calc R U . . .
C34B C 0.6233(3) 0.3499(2) 0.97383(15) 0.0544(9) Uani 1 1 d . . . . .
H34B H 0.665834 0.350478 1.013813 0.065 Uiso 1 1 calc R U . . .
C35B C 0.5007(2) 0.3234(2) 0.96318(14) 0.0475(8) Uani 1 1 d . . . . .
H35B H 0.460143 0.305650 0.996086 0.057 Uiso 1 1 calc R U . . .
C1C C -0.095(3) 0.2323(19) 0.8764(13) 0.036(4) Uani 0.414(17) 1 d . U P A 2
H1C H -0.104681 0.207219 0.831060 0.043 Uiso 0.414(17) 1 calc R U P A 2
C2C C -0.022(3) 0.3192(18) 0.9066(12) 0.030(4) Uani 0.414(17) 1 d . U P A 2
C3C C -0.008(2) 0.3605(15) 0.9697(14) 0.031(3) Uani 0.414(17) 1 d . U P A 2
H3C H 0.039818 0.421808 0.986883 0.037 Uiso 0.414(17) 1 calc R U P A 2
C4C C -0.0644(18) 0.3133(12) 1.0090(10) 0.032(3) Uani 0.414(17) 1 d . U P A 2
H4C H -0.054570 0.340772 1.054115 0.038 Uiso 0.414(17) 1 calc R U P A 2
C5C C -0.2119(12) 0.1592(9) 1.0758(5) 0.051(2) Uani 0.414(17) 1 d G U P A 2
H5C H -0.171427 0.213316 1.108513 0.061 Uiso 0.414(17) 1 calc R U P A 2
C6C C -0.2792(11) 0.0836(10) 1.0924(5) 0.062(3) Uani 0.414(17) 1 d G U P A 2
H6C H -0.284758 0.086177 1.136346 0.074 Uiso 0.414(17) 1 calc R U P A 2
C7C C -0.3385(11) 0.0044(9) 1.0446(6) 0.057(3) Uani 0.414(17) 1 d G U P A 2
H7C H -0.384489 -0.047237 1.055862 0.068 Uiso 0.414(17) 1 calc R U P A 2
C8C C -0.3304(12) 0.0007(8) 0.9802(6) 0.063(3) Uani 0.414(17) 1 d G U P A 2
H8C H -0.370891 -0.053513 0.947545 0.076 Uiso 0.414(17) 1 calc R U P A 2
C13C C -0.2631(13) 0.0762(9) 0.9637(5) 0.045(3) Uani 0.414(17) 1 d G U P A 2
C12C C -0.2038(13) 0.1554(8) 1.0115(5) 0.045(3) Uani 0.414(17) 1 d G U P A 2
C9C C -0.242(2) 0.0881(17) 0.8964(11) 0.043(3) Uani 0.414(17) 1 d . U P A 2
C10C C -0.155(2) 0.1830(16) 0.9167(11) 0.035(3) Uani 0.414(17) 1 d . U P A 2
C11C C -0.1368(18) 0.2237(13) 0.9820(9) 0.031(3) Uani 0.414(17) 1 d . U P A 2
C14C C -0.182(2) 0.005(2) 0.8615(10) 0.067(5) Uani 0.414(17) 1 d . U P A 2
H14A H -0.168082 0.011278 0.818608 0.100 Uiso 0.414(17) 1 calc R U P A 2
H14B H -0.234599 -0.056311 0.857539 0.100 Uiso 0.414(17) 1 calc R U P A 2
H14C H -0.105665 0.007199 0.886940 0.100 Uiso 0.414(17) 1 calc R U P A 2
C15C C -0.363(2) 0.079(3) 0.8529(16) 0.059(6) Uani 0.414(17) 1 d . U P A 2
H15A H -0.346888 0.093484 0.812240 0.089 Uiso 0.414(17) 1 calc R U P A 2
H15B H -0.408618 0.123554 0.875408 0.089 Uiso 0.414(17) 1 calc R U P A 2
H15C H -0.408934 0.014245 0.844141 0.089 Uiso 0.414(17) 1 calc R U P A 2
C18C C 0.2181(17) 0.2623(12) 0.9731(6) 0.033(3) Uani 0.42(3) 1 d G U P B 2
C19C C 0.1580(16) 0.1777(11) 0.9817(6) 0.039(2) Uani 0.42(3) 1 d G U P B 2
H19C H 0.137758 0.122825 0.946486 0.047 Uiso 0.42(3) 1 calc R U P B 2
C20C C 0.1275(14) 0.1733(11) 1.0418(7) 0.053(3) Uani 0.42(3) 1 d G U P B 2
H20C H 0.086431 0.115474 1.047747 0.064 Uiso 0.42(3) 1 calc R U P B 2
C21C C 0.1571(13) 0.2536(13) 1.0934(6) 0.049(3) Uani 0.42(3) 1 d G U P B 2
H21C H 0.136252 0.250618 1.134478 0.059 Uiso 0.42(3) 1 calc R U P B 2
C22C C 0.2172(14) 0.3382(12) 1.0847(6) 0.042(3) Uani 0.42(3) 1 d G U P B 2
H22C H 0.237399 0.393113 1.119947 0.050 Uiso 0.42(3) 1 calc R U P B 2
C23C C 0.2477(16) 0.3426(11) 1.0246(6) 0.034(2) Uani 0.42(3) 1 d G U P B 2
H23C H 0.288728 0.400466 1.018686 0.041 Uiso 0.42(3) 1 calc R U P B 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C15 B1 C14 60.96(15) . . ?
C15 B1 B9 58.42(16) . . ?
C14 B1 B9 107.1(2) . . ?
C15 B1 B8 105.5(2) . . ?
C14 B1 B8 104.9(2) . . ?
B9 B1 B8 59.96(18) . . ?
C15 B1 B2 107.4(2) . . ?
C14 B1 B2 58.17(16) . . ?
B9 B1 B2 108.2(2) . . ?
B8 B1 B2 59.58(18) . . ?
C15 B1 H1 122.4 . . ?
C14 B1 H1 122.9 . . ?
B9 B1 H1 121.9 . . ?
B8 B1 H1 123.4 . . ?
B2 B1 H1 122.0 . . ?
C14 B2 B8 106.1(2) . . ?
C14 B2 B3 58.48(16) . . ?
B8 B2 B3 107.9(2) . . ?
C14 B2 B7 105.5(2) . . ?
B8 B2 B7 60.18(18) . . ?
B3 B2 B7 59.88(17) . . ?
C14 B2 B1 59.38(16) . . ?
B8 B2 B1 59.92(18) . . ?
B3 B2 B1 107.4(2) . . ?
B7 B2 B1 107.8(2) . . ?
C14 B2 H2 123.8 . . ?
B8 B2 H2 121.9 . . ?
B3 B2 H2 122.0 . . ?
B7 B2 H2 122.2 . . ?
B1 B2 H2 121.7 . . ?
C14 B3 B6 106.0(2) . . ?
C14 B3 B7 105.9(2) . . ?
B6 B3 B7 60.12(18) . . ?
C14 B3 B4 59.16(16) . . ?
B6 B3 B4 59.63(17) . . ?
B7 B3 B4 107.5(2) . . ?
C14 B3 B2 58.74(16) . . ?
B6 B3 B2 108.0(2) . . ?
B7 B3 B2 60.07(18) . . ?
B4 B3 B2 107.2(2) . . ?
C14 B3 H3 123.7 . . ?
B6 B3 H3 122.0 . . ?
B7 B3 H3 122.1 . . ?
B4 B3 H3 122.1 . . ?
B2 B3 H3 121.9 . . ?
C14 B4 C15 61.08(15) . . ?
C14 B4 B6 105.6(2) . . ?
C15 B4 B6 106.0(2) . . ?
C14 B4 B5 106.9(2) . . ?
C15 B4 B5 57.86(15) . . ?
B6 B4 B5 60.50(17) . . ?
C14 B4 B3 58.30(16) . . ?
C15 B4 B3 107.6(2) . . ?
B6 B4 B3 60.05(17) . . ?
B5 B4 B3 108.6(2) . . ?
C14 B4 H4 122.8 . . ?
C15 B4 H4 122.5 . . ?
B6 B4 H4 122.8 . . ?
B5 B4 H4 121.9 . . ?
B3 B4 H4 121.6 . . ?
C15 B5 B4 60.03(16) . . ?
C15 B5 B9 59.06(16) . . ?
B4 B5 B9 108.0(2) . . ?
C15 B5 B10 106.8(2) . . ?
B4 B5 B10 107.7(2) . . ?
B9 B5 B10 60.34(18) . . ?
C15 B5 B6 107.0(2) . . ?
B4 B5 B6 59.65(17) . . ?
B9 B5 B6 108.2(2) . . ?
B10 B5 B6 59.99(17) . . ?
C15 B5 H5 122.8 . . ?
B4 B5 H5 121.7 . . ?
B9 B5 H5 121.6 . . ?
B10 B5 H5 122.0 . . ?
B6 B5 H5 121.9 . . ?
B4 B6 B3 60.32(17) . . ?
B4 B6 B7 107.9(2) . . ?
B3 B6 B7 60.00(18) . . ?
B4 B6 B10 107.8(2) . . ?
B3 B6 B10 108.3(2) . . ?
B7 B6 B10 60.10(18) . . ?
B4 B6 B5 59.85(17) . . ?
B3 B6 B5 108.3(2) . . ?
B7 B6 B5 107.9(2) . . ?
B10 B6 B5 59.84(17) . . ?
B4 B6 H6 121.8 . . ?
B3 B6 H6 121.3 . . ?
B7 B6 H6 121.8 . . ?
B10 B6 H6 121.7 . . ?
B5 B6 H6 121.8 . . ?
B3 B7 B6 59.88(17) . . ?
B3 B7 B8 107.6(2) . . ?
B6 B7 B8 107.6(2) . . ?
B3 B7 B2 60.05(17) . . ?
B6 B7 B2 107.8(2) . . ?
B8 B7 B2 59.60(18) . . ?
B3 B7 B10 108.1(2) . . ?
B6 B7 B10 59.95(17) . . ?
B8 B7 B10 60.13(18) . . ?
B2 B7 B10 108.0(2) . . ?
B3 B7 H7 121.8 . . ?
B6 B7 H7 122.0 . . ?
B8 B7 H7 122.1 . . ?
B2 B7 H7 121.8 . . ?
B10 B7 H7 121.5 . . ?
B2 B8 B9 109.0(2) . . ?
B2 B8 B1 60.50(18) . . ?
B9 B8 B1 60.00(18) . . ?
B2 B8 B7 60.22(18) . . ?
B9 B8 B7 108.5(2) . . ?
B1 B8 B7 108.3(2) . . ?
B2 B8 B10 108.4(2) . . ?
B9 B8 B10 60.17(18) . . ?
B1 B8 B10 107.9(2) . . ?
B7 B8 B10 59.99(18) . . ?
B2 B8 H8 121.1 . . ?
B9 B8 H8 121.3 . . ?
B1 B8 H8 121.7 . . ?
B7 B8 H8 121.5 . . ?
B10 B8 H8 121.8 . . ?
C15 B9 B5 58.27(16) . . ?
C15 B9 B8 106.5(2) . . ?
B5 B9 B8 107.8(2) . . ?
C15 B9 B1 59.52(16) . . ?
B5 B9 B1 107.1(2) . . ?
B8 B9 B1 60.05(18) . . ?
C15 B9 B10 105.8(2) . . ?
B5 B9 B10 59.94(17) . . ?
B8 B9 B10 60.21(18) . . ?
B1 B9 B10 108.0(2) . . ?
C15 B9 H9 123.6 . . ?
B5 B9 H9 122.3 . . ?
B8 B9 H9 121.8 . . ?
B1 B9 H9 121.7 . . ?
B10 B9 H9 122.0 . . ?
B5 B10 B6 60.18(17) . . ?
B5 B10 B7 108.0(2) . . ?
B6 B10 B7 59.95(18) . . ?
B5 B10 B9 59.72(17) . . ?
B6 B10 B9 107.9(2) . . ?
B7 B10 B9 108.0(2) . . ?
B5 B10 B8 107.1(2) . . ?
B6 B10 B8 107.4(2) . . ?
B7 B10 B8 59.87(18) . . ?
B9 B10 B8 59.62(18) . . ?
B5 B10 H10 121.9 . . ?
B6 B10 H10 121.8 . . ?
B7 B10 H10 121.6 . . ?
B9 B10 H10 121.8 . . ?
B8 B10 H10 122.4 . . ?
C10 C1 C2 119.6(2) . . ?
C10 C1 H1A 120.2 . . ?
C2 C1 H1A 120.2 . . ?
C3 C2 C1 119.4(2) . . ?
C3 C2 C14 120.1(2) . . ?
C1 C2 C14 120.4(2) . . ?
C4 C3 C2 121.1(2) . . ?
C4 C3 H3A 119.4 . . ?
C2 C3 H3A 119.4 . . ?
C11 C4 C3 119.1(2) . . ?
C11 C4 H4A 120.4 . . ?
C3 C4 H4A 120.4 . . ?
C12 C5 C6 118.5(3) . . ?
C12 C5 H5A 120.8 . . ?
C6 C5 H5A 120.8 . . ?
C7 C6 C5 120.6(3) . . ?
C7 C6 H6A 119.7 . . ?
C5 C6 H6A 119.7 . . ?
C6 C7 C8 121.1(3) . . ?
C6 C7 H7A 119.4 . . ?
C8 C7 H7A 119.4 . . ?
C7 C8 C13 118.8(3) . . ?
C7 C8 H8A 120.6 . . ?
C13 C8 H8A 120.6 . . ?
C13 C9 C10 101.0(2) . . ?
C13 C9 C16 112.0(3) . . ?
C10 C9 C16 111.5(2) . . ?
C13 C9 C17 111.1(2) . . ?
C10 C9 C17 110.7(2) . . ?
C16 C9 C17 110.3(3) . . ?
C1 C10 C11 120.2(2) . . ?
C1 C10 C9 128.8(2) . . ?
C11 C10 C9 111.0(2) . . ?
C4 C11 C10 120.5(2) . . ?
C4 C11 C12 131.0(3) . . ?
C10 C11 C12 108.5(2) . . ?
C5 C12 C13 121.3(3) . . ?
C5 C12 C11 130.7(3) . . ?
C13 C12 C11 108.0(2) . . ?
C8 C13 C12 119.8(3) . . ?
C8 C13 C9 128.8(3) . . ?
C12 C13 C9 111.4(2) . . ?
C2 C14 B3 119.1(2) . . ?
C2 C14 B2 120.2(2) . . ?
B3 C14 B2 62.78(17) . . ?
C2 C14 B4 118.3(2) . . ?
B3 C14 B4 62.54(17) . . ?
B2 C14 B4 113.2(2) . . ?
C2 C14 B1 119.7(2) . . ?
B3 C14 B1 113.4(2) . . ?
B2 C14 B1 62.45(17) . . ?
B4 C14 B1 110.7(2) . . ?
C2 C14 C15 121.2(2) . . ?
B3 C14 C15 110.01(19) . . ?
B2 C14 C15 109.60(19) . . ?
B4 C14 C15 59.85(15) . . ?
B1 C14 C15 59.46(15) . . ?
B5 C15 B9 62.68(17) . . ?
B5 C15 B1 112.7(2) . . ?
B9 C15 B1 62.06(17) . . ?
B5 C15 B4 62.11(16) . . ?
B9 C15 B4 112.6(2) . . ?
B1 C15 B4 110.1(2) . . ?
B5 C15 C14 108.66(19) . . ?
B9 C15 C14 108.83(19) . . ?
B1 C15 C14 59.58(15) . . ?
B4 C15 C14 59.07(15) . . ?
B5 C15 Si1 118.56(18) . . ?
B9 C15 Si1 119.76(17) . . ?
B1 C15 Si1 120.61(17) . . ?
B4 C15 Si1 118.94(17) . . ?
C14 C15 Si1 123.10(16) . . ?
C9 C16 H16A 109.5 . . ?
C9 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C9 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C9 C17 H17A 109.5 . . ?
C9 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C9 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C18 Si1 C24 112.23(12) . . ?
C18 Si1 C30 108.09(12) . . ?
C24 Si1 C30 108.67(12) . . ?
C18 Si1 C15 109.97(11) . . ?
C24 Si1 C15 107.80(11) . . ?
C30 Si1 C15 110.06(11) . . ?
C23 C18 C19 117.7(3) . . ?
C23 C18 Si1 121.4(2) . . ?
C19 C18 Si1 120.9(2) . . ?
C20 C19 C18 121.2(3) . . ?
C20 C19 H19 119.4 . . ?
C18 C19 H19 119.4 . . ?
C21 C20 C19 119.5(3) . . ?
C21 C20 H20 120.3 . . ?
C19 C20 H20 120.3 . . ?
C22 C21 C20 120.3(3) . . ?
C22 C21 H21 119.9 . . ?
C20 C21 H21 119.9 . . ?
C21 C22 C23 120.4(3) . . ?
C21 C22 H22 119.8 . . ?
C23 C22 H22 119.8 . . ?
C22 C23 C18 120.9(3) . . ?
C22 C23 H23 119.5 . . ?
C18 C23 H23 119.5 . . ?
C29 C24 C25 116.4(2) . . ?
C29 C24 Si1 121.0(2) . . ?
C25 C24 Si1 122.7(2) . . ?
C26 C25 C24 122.1(3) . . ?
C26 C25 H25 118.9 . . ?
C24 C25 H25 118.9 . . ?
C27 C26 C25 120.0(3) . . ?
C27 C26 H26 120.0 . . ?
C25 C26 H26 120.0 . . ?
C28 C27 C26 119.3(3) . . ?
C28 C27 H27 120.3 . . ?
C26 C27 H27 120.3 . . ?
C27 C28 C29 120.7(3) . . ?
C27 C28 H28 119.7 . . ?
C29 C28 H28 119.7 . . ?
C28 C29 C24 121.5(3) . . ?
C28 C29 H29 119.2 . . ?
C24 C29 H29 119.2 . . ?
C35 C30 C31 117.0(2) . . ?
C35 C30 Si1 118.9(2) . . ?
C31 C30 Si1 123.8(2) . . ?
C32 C31 C30 121.6(3) . . ?
C32 C31 H31 119.2 . . ?
C30 C31 H31 119.2 . . ?
C33 C32 C31 119.9(3) . . ?
C33 C32 H32 120.0 . . ?
C31 C32 H32 120.0 . . ?
C32 C33 C34 119.9(3) . . ?
C32 C33 H33 120.1 . . ?
C34 C33 H33 120.1 . . ?
C33 C34 C35 120.2(3) . . ?
C33 C34 H34 119.9 . . ?
C35 C34 H34 119.9 . . ?
C34 C35 C30 121.3(3) . . ?
C34 C35 H35 119.3 . . ?
C30 C35 H35 119.3 . . ?
C15B B1B C14B 60.56(16) . . ?
C15B B1B B9B 58.82(17) . . ?
C14B B1B B9B 107.0(2) . . ?
C15B B1B B8B 106.1(2) . . ?
C14B B1B B8B 105.1(2) . . ?
B9B B1B B8B 60.08(18) . . ?
C15B B1B B2B 107.2(2) . . ?
C14B B1B B2B 57.99(17) . . ?
B9B B1B B2B 108.4(2) . . ?
B8B B1B B2B 59.97(18) . . ?
C15B B1B H1B 122.4 . . ?
C14B B1B H1B 123.2 . . ?
B9B B1B H1B 121.7 . . ?
B8B B1B H1B 123.0 . . ?
B2B B1B H1B 121.9 . . ?
C14B B2B B8B 106.0(2) . . ?
C14B B2B B3B 58.70(18) . . ?
B8B B2B B3B 107.7(2) . . ?
C14B B2B B1B 59.41(17) . . ?
B8B B2B B1B 59.62(18) . . ?
B3B B2B B1B 107.4(2) . . ?
C14B B2B B7B 105.6(2) . . ?
B8B B2B B7B 59.89(19) . . ?
B3B B2B B7B 59.90(19) . . ?
B1B B2B B7B 107.3(2) . . ?
C14B B2B H2B 123.6 . . ?
B8B B2B H2B 122.2 . . ?
B3B B2B H2B 121.9 . . ?
B1B B2B H2B 121.9 . . ?
B7B B2B H2B 122.4 . . ?
C14B B3B B6B 106.3(2) . . ?
C14B B3B B2B 58.51(17) . . ?
B6B B3B B2B 108.3(2) . . ?
C14B B3B B4B 59.28(16) . . ?
B6B B3B B4B 59.83(18) . . ?
B2B B3B B4B 107.3(2) . . ?
C14B B3B B7B 105.8(2) . . ?
B6B B3B B7B 60.2(2) . . ?
B2B B3B B7B 60.3(2) . . ?
B4B B3B B7B 107.6(2) . . ?
C14B B3B H3B 123.7 . . ?
B6B B3B H3B 121.8 . . ?
B2B B3B H3B 121.8 . . ?
B4B B3B H3B 122.0 . . ?
B7B B3B H3B 122.1 . . ?
C14B B4B C15B 60.50(15) . . ?
C14B B4B B6B 105.6(2) . . ?
C15B B4B B6B 106.3(2) . . ?
C14B B4B B5B 106.9(2) . . ?
C15B B4B B5B 58.47(16) . . ?
B6B B4B B5B 60.59(18) . . ?
C14B B4B B3B 58.34(17) . . ?
C15B B4B B3B 107.3(2) . . ?
B6B B4B B3B 59.86(18) . . ?
B5B B4B B3B 108.6(2) . . ?
C14B B4B H4B 123.0 . . ?
C15B B4B H4B 122.5 . . ?
B6B B4B H4B 122.7 . . ?
B5B B4B H4B 121.7 . . ?
B3B B4B H4B 121.8 . . ?
C15B B5B B9B 59.02(17) . . ?
C15B B5B B4B 59.50(16) . . ?
B9B B5B B4B 107.6(2) . . ?
C15B B5B B10B 106.4(2) . . ?
B9B B5B B10B 60.33(19) . . ?
B4B B5B B10B 107.4(2) . . ?
C15B B5B B6B 106.3(2) . . ?
B9B B5B B6B 108.0(2) . . ?
B4B B5B B6B 59.53(17) . . ?
B10B B5B B6B 59.85(19) . . ?
C15B B5B H5B 123.2 . . ?
B9B B5B H5B 121.7 . . ?
B4B B5B H5B 122.0 . . ?
B10B B5B H5B 122.1 . . ?
B6B B5B H5B 122.2 . . ?
B4B B6B B3B 60.31(18) . . ?
B4B B6B B7B 108.0(2) . . ?
B3B B6B B7B 60.18(19) . . ?
B4B B6B B10B 107.8(2) . . ?
B3B B6B B10B 108.1(2) . . ?
B7B B6B B10B 59.69(19) . . ?
B4B B6B B5B 59.88(17) . . ?
B3B B6B B5B 108.4(2) . . ?
B7B B6B B5B 107.7(2) . . ?
B10B B6B B5B 59.93(18) . . ?
B4B B6B H6B 121.8 . . ?
B3B B6B H6B 121.3 . . ?
B7B B6B H6B 121.9 . . ?
B10B B6B H6B 121.9 . . ?
B5B B6B H6B 121.8 . . ?
B10B B7B B8B 60.26(19) . . ?
B10B B7B B6B 60.23(19) . . ?
B8B B7B B6B 107.8(2) . . ?
B10B B7B B3B 108.2(2) . . ?
B8B B7B B3B 107.5(2) . . ?
B6B B7B B3B 59.66(19) . . ?
B10B B7B B2B 108.3(2) . . ?
B8B B7B B2B 59.80(19) . . ?
B6B B7B B2B 107.6(2) . . ?
B3B B7B B2B 59.81(19) . . ?
B10B B7B H7B 121.3 . . ?
B8B B7B H7B 121.9 . . ?
B6B B7B H7B 121.9 . . ?
B3B B7B H7B 122.0 . . ?
B2B B7B H7B 121.9 . . ?
B1B B8B B9B 59.91(18) . . ?
B1B B8B B2B 60.41(18) . . ?
B9B B8B B2B 108.6(2) . . ?
B1B B8B B7B 108.3(2) . . ?
B9B B8B B7B 108.2(2) . . ?
B2B B8B B7B 60.32(19) . . ?
B1B B8B B10B 108.0(2) . . ?
B9B B8B B10B 60.28(18) . . ?
B2B B8B B10B 108.3(2) . . ?
B7B B8B B10B 59.70(19) . . ?
B1B B8B H8B 121.6 . . ?
B9B B8B H8B 121.5 . . ?
B2B B8B H8B 121.2 . . ?
B7B B8B H8B 121.7 . . ?
B10B B8B H8B 121.8 . . ?
C15B B9B B5B 58.92(17) . . ?
C15B B9B B1B 59.28(17) . . ?
B5B B9B B1B 107.7(2) . . ?
C15B B9B B8B 106.4(2) . . ?
B5B B9B B8B 108.3(2) . . ?
B1B B9B B8B 60.01(18) . . ?
C15B B9B B10B 106.3(2) . . ?
B5B B9B B10B 60.26(18) . . ?
B1B B9B B10B 108.0(2) . . ?
B8B B9B B10B 60.15(18) . . ?
C15B B9B H9B 123.4 . . ?
B5B B9B H9B 121.7 . . ?
B1B B9B H9B 121.7 . . ?
B8B B9B H9B 121.8 . . ?
B10B B9B H9B 121.9 . . ?
B7B B10B B6B 60.1(2) . . ?
B7B B10B B8B 60.05(19) . . ?
B6B B10B B8B 107.5(2) . . ?
B7B B10B B5B 108.3(2) . . ?
B6B B10B B5B 60.22(18) . . ?
B8B B10B B5B 107.1(2) . . ?
B7B B10B B9B 107.9(2) . . ?
B6B B10B B9B 107.5(2) . . ?
B8B B10B B9B 59.56(18) . . ?
B5B B10B B9B 59.40(18) . . ?
B7B B10B H10B 121.4 . . ?
B6B B10B H10B 121.8 . . ?
B8B B10B H10B 122.3 . . ?
B5B B10B H10B 121.9 . . ?
B9B B10B H10B 122.2 . . ?
C10B C1B C2B 120.5(13) . . ?
C10B C1B H1BA 119.8 . . ?
C2B C1B H1BA 119.8 . . ?
C1B C2B C3B 116.7(15) . . ?
C1B C2B C14B 125.1(12) . . ?
C3B C2B C14B 118.1(12) . . ?
C4B C3B C2B 121.8(10) . . ?
C4B C3B H3BA 119.1 . . ?
C2B C3B H3BA 119.1 . . ?
C11B C4B C3B 119.3(12) . . ?
C11B C4B H4BA 120.3 . . ?
C3B C4B H4BA 120.3 . . ?
C6B C5B C12B 120.0 . . ?
C6B C5B H5BA 120.0 . . ?
C12B C5B H5BA 120.0 . . ?
C5B C6B C7B 120.0 . . ?
C5B C6B H6BA 120.0 . . ?
C7B C6B H6BA 120.0 . . ?
C8B C7B C6B 120.0 . . ?
C8B C7B H7BA 120.0 . . ?
C6B C7B H7BA 120.0 . . ?
C7B C8B C13B 120.0 . . ?
C7B C8B H8BA 120.0 . . ?
C13B C8B H8BA 120.0 . . ?
C12B C13B C8B 120.0 . . ?
C12B C13B C9B 111.9(6) . . ?
C8B C13B C9B 128.1(6) . . ?
C13B C12B C5B 120.0 . . ?
C13B C12B C11B 107.7(6) . . ?
C5B C12B C11B 132.3(6) . . ?
C13B C9B C16B 114.5(14) . . ?
C13B C9B C10B 101.5(9) . . ?
C16B C9B C10B 111.2(14) . . ?
C13B C9B C17B 110.1(16) . . ?
C16B C9B C17B 114.2(13) . . ?
C10B C9B C17B 104.0(15) . . ?
C1B C10B C11B 121.9(11) . . ?
C1B C10B C9B 128.7(11) . . ?
C11B C10B C9B 109.3(13) . . ?
C4B C11B C10B 119.5(13) . . ?
C4B C11B C12B 131.1(12) . . ?
C10B C11B C12B 109.4(9) . . ?
C9B C16B H16D 109.5 . . ?
C9B C16B H16E 109.5 . . ?
H16D C16B H16E 109.5 . . ?
C9B C16B H16F 109.5 . . ?
H16D C16B H16F 109.5 . . ?
H16E C16B H16F 109.5 . . ?
C9B C17B H17D 109.5 . . ?
C9B C17B H17E 109.5 . . ?
H17D C17B H17E 109.5 . . ?
C9B C17B H17F 109.5 . . ?
H17D C17B H17F 109.5 . . ?
H17E C17B H17F 109.5 . . ?
C19B C18B C23B 120.0 . . ?
C19B C18B Si1B 119.2(5) . . ?
C23B C18B Si1B 120.6(5) . . ?
C18B C19B C20B 120.0 . . ?
C18B C19B H19B 120.0 . . ?
C20B C19B H19B 120.0 . . ?
C21B C20B C19B 120.0 . . ?
C21B C20B H20B 120.0 . . ?
C19B C20B H20B 120.0 . . ?
C20B C21B C22B 120.0 . . ?
C20B C21B H21B 120.0 . . ?
C22B C21B H21B 120.0 . . ?
C23B C22B C21B 120.0 . . ?
C23B C22B H22B 120.0 . . ?
C21B C22B H22B 120.0 . . ?
C22B C23B C18B 120.0 . . ?
C22B C23B H23B 120.0 . . ?
C18B C23B H23B 120.0 . . ?
C18B Si1B C24B 115.2(4) . . ?
C18B Si1B C30B 104.8(4) . . ?
C24B Si1B C30B 108.01(12) . . ?
C24B Si1B C18C 106.9(5) . . ?
C30B Si1B C18C 109.8(6) . . ?
C18B Si1B C15B 110.9(5) . . ?
C24B Si1B C15B 108.24(12) . . ?
C30B Si1B C15B 109.44(12) . . ?
C18C Si1B C15B 114.3(6) . . ?
C2B C14B B2B 123.5(8) . . ?
C2C C14B B2B 115.4(11) . . ?
C2B C14B B3B 117.3(7) . . ?
C2C C14B B3B 124.2(11) . . ?
B2B C14B B3B 62.79(19) . . ?
C2B C14B B4B 113.7(6) . . ?
C2C C14B B4B 125.7(9) . . ?
B2B C14B B4B 113.3(2) . . ?
B3B C14B B4B 62.38(18) . . ?
C2B C14B B1B 123.6(6) . . ?
C2C C14B B1B 112.1(9) . . ?
B2B C14B B1B 62.59(18) . . ?
B3B C14B B1B 113.2(2) . . ?
B4B C14B B1B 110.6(2) . . ?
C2B C14B C15B 119.6(9) . . ?
C2C C14B C15B 120.2(12) . . ?
B2B C14B C15B 110.1(2) . . ?
B3B C14B C15B 110.1(2) . . ?
B4B C14B C15B 59.96(15) . . ?
B1B C14B C15B 59.53(16) . . ?
B5B C15B B9B 62.06(18) . . ?
B5B C15B B1B 112.3(2) . . ?
B9B C15B B1B 61.89(18) . . ?
B5B C15B B4B 62.04(17) . . ?
B9B C15B B4B 112.1(2) . . ?
B1B C15B B4B 110.6(2) . . ?
B5B C15B C14B 108.96(19) . . ?
B9B C15B C14B 108.9(2) . . ?
B1B C15B C14B 59.91(16) . . ?
B4B C15B C14B 59.54(15) . . ?
B5B C15B Si1B 119.12(18) . . ?
B9B C15B Si1B 120.78(17) . . ?
B1B C15B Si1B 120.53(18) . . ?
B4B C15B Si1B 118.40(19) . . ?
C14B C15B Si1B 122.11(17) . . ?
C29B C24B C25B 116.8(3) . . ?
C29B C24B Si1B 123.2(2) . . ?
C25B C24B Si1B 120.1(2) . . ?
C26B C25B C24B 121.3(3) . . ?
C26B C25B H25B 119.4 . . ?
C24B C25B H25B 119.4 . . ?
C27B C26B C25B 120.8(3) . . ?
C27B C26B H26B 119.6 . . ?
C25B C26B H26B 119.6 . . ?
C26B C27B C28B 119.1(3) . . ?
C26B C27B H27B 120.5 . . ?
C28B C27B H27B 120.5 . . ?
C29B C28B C27B 120.2(3) . . ?
C29B C28B H28B 119.9 . . ?
C27B C28B H28B 119.9 . . ?
C28B C29B C24B 121.9(3) . . ?
C28B C29B H29B 119.1 . . ?
C24B C29B H29B 119.1 . . ?
C31B C30B C35B 116.8(2) . . ?
C31B C30B Si1B 124.6(2) . . ?
C35B C30B Si1B 118.3(2) . . ?
C32B C31B C30B 121.2(3) . . ?
C32B C31B H31B 119.4 . . ?
C30B C31B H31B 119.4 . . ?
C33B C32B C31B 120.7(3) . . ?
C33B C32B H32B 119.6 . . ?
C31B C32B H32B 119.6 . . ?
C32B C33B C34B 119.4(3) . . ?
C32B C33B H33B 120.3 . . ?
C34B C33B H33B 120.3 . . ?
C33B C34B C35B 120.2(3) . . ?
C33B C34B H34B 119.9 . . ?
C35B C34B H34B 119.9 . . ?
C34B C35B C30B 121.6(3) . . ?
C34B C35B H35B 119.2 . . ?
C30B C35B H35B 119.2 . . ?
C2C C1C C10C 117(2) . . ?
C2C C1C H1C 121.7 . . ?
C10C C1C H1C 121.7 . . ?
C3C C2C C1C 125(2) . . ?
C3C C2C C14B 124.9(19) . . ?
C1C C2C C14B 110.3(18) . . ?
C2C C3C C4C 119.1(17) . . ?
C2C C3C H3C 120.5 . . ?
C4C C3C H3C 120.5 . . ?
C3C C4C C11C 119.2(17) . . ?
C3C C4C H4C 120.4 . . ?
C11C C4C H4C 120.4 . . ?
C6C C5C C12C 120.0 . . ?
C6C C5C H5C 120.0 . . ?
C12C C5C H5C 120.0 . . ?
C5C C6C C7C 120.0 . . ?
C5C C6C H6C 120.0 . . ?
C7C C6C H6C 120.0 . . ?
C8C C7C C6C 120.0 . . ?
C8C C7C H7C 120.0 . . ?
C6C C7C H7C 120.0 . . ?
C7C C8C C13C 120.0 . . ?
C7C C8C H8C 120.0 . . ?
C13C C8C H8C 120.0 . . ?
C12C C13C C8C 120.0 . . ?
C12C C13C C9C 110.8(9) . . ?
C8C C13C C9C 129.2(9) . . ?
C13C C12C C5C 120.0 . . ?
C13C C12C C11C 109.6(8) . . ?
C5C C12C C11C 130.4(8) . . ?
C10C C9C C13C 99.0(14) . . ?
C10C C9C C15C 119(2) . . ?
C13C C9C C15C 111(2) . . ?
C10C C9C C14C 112(2) . . ?
C13C C9C C14C 108.8(18) . . ?
C15C C9C C14C 106.4(18) . . ?
C11C C10C C1C 118.6(16) . . ?
C11C C10C C9C 114(2) . . ?
C1C C10C C9C 127.6(17) . . ?
C10C C11C C4C 121.7(18) . . ?
C10C C11C C12C 106.6(14) . . ?
C4C C11C C12C 131.7(15) . . ?
C9C C14C H14A 109.5 . . ?
C9C C14C H14B 109.5 . . ?
H14A C14C H14B 109.5 . . ?
C9C C14C H14C 109.5 . . ?
H14A C14C H14C 109.5 . . ?
H14B C14C H14C 109.5 . . ?
C9C C15C H15A 109.5 . . ?
C9C C15C H15B 109.5 . . ?
H15A C15C H15B 109.5 . . ?
C9C C15C H15C 109.5 . . ?
H15A C15C H15C 109.5 . . ?
H15B C15C H15C 109.5 . . ?
C19C C18C C23C 120.0 . . ?
C19C C18C Si1B 123.0(7) . . ?
C23C C18C Si1B 116.9(7) . . ?
C18C C19C C20C 120.0 . . ?
C18C C19C H19C 120.0 . . ?
C20C C19C H19C 120.0 . . ?
C21C C20C C19C 120.0 . . ?
C21C C20C H20C 120.0 . . ?
C19C C20C H20C 120.0 . . ?
C22C C21C C20C 120.0 . . ?
C22C C21C H21C 120.0 . . ?
C20C C21C H21C 120.0 . . ?
C21C C22C C23C 120.0 . . ?
C21C C22C H22C 120.0 . . ?
C23C C22C H22C 120.0 . . ?
C22C C23C C18C 120.0 . . ?
C22C C23C H23C 120.0 . . ?
C18C C23C H23C 120.0 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
B1 C15 1.732(4) . ?
B1 C14 1.734(4) . ?
B1 B9 1.775(4) . ?
B1 B8 1.776(4) . ?
B1 B2 1.786(4) . ?
B1 H1 1.1200 . ?
B2 C14 1.712(4) . ?
B2 B8 1.770(4) . ?
B2 B3 1.780(4) . ?
B2 B7 1.781(4) . ?
B2 H2 1.1200 . ?
B3 C14 1.707(4) . ?
B3 B6 1.775(4) . ?
B3 B7 1.777(4) . ?
B3 B4 1.780(4) . ?
B3 H3 1.1200 . ?
B4 C14 1.723(4) . ?
B4 C15 1.736(4) . ?
B4 B6 1.768(4) . ?
B4 B5 1.772(4) . ?
B4 H4 1.1200 . ?
B5 C15 1.697(4) . ?
B5 B9 1.773(4) . ?
B5 B10 1.777(4) . ?
B5 B6 1.783(4) . ?
B5 H5 1.1200 . ?
B6 B7 1.780(4) . ?
B6 B10 1.780(4) . ?
B6 H6 1.1200 . ?
B7 B8 1.780(5) . ?
B7 B10 1.782(4) . ?
B7 H7 1.1200 . ?
B8 B9 1.774(5) . ?
B8 B10 1.785(4) . ?
B8 H8 1.1200 . ?
B9 C15 1.712(4) . ?
B9 B10 1.784(4) . ?
B9 H9 1.1200 . ?
B10 H10 1.1200 . ?
C1 C10 1.387(4) . ?
C1 C2 1.398(3) . ?
C1 H1A 0.9500 . ?
C2 C3 1.395(3) . ?
C2 C14 1.506(3) . ?
C3 C4 1.385(4) . ?
C3 H3A 0.9500 . ?
C4 C11 1.384(4) . ?
C4 H4A 0.9500 . ?
C5 C12 1.384(4) . ?
C5 C6 1.387(4) . ?
C5 H5A 0.9500 . ?
C6 C7 1.381(5) . ?
C6 H6A 0.9500 . ?
C7 C8 1.388(5) . ?
C7 H7A 0.9500 . ?
C8 C13 1.389(4) . ?
C8 H8A 0.9500 . ?
C9 C13 1.520(4) . ?
C9 C10 1.523(4) . ?
C9 C16 1.529(4) . ?
C9 C17 1.537(4) . ?
C10 C11 1.398(4) . ?
C11 C12 1.472(4) . ?
C12 C13 1.396(4) . ?
C14 C15 1.758(3) . ?
C15 Si1 1.945(3) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
Si1 C18 1.870(3) . ?
Si1 C24 1.872(3) . ?
Si1 C30 1.881(3) . ?
C18 C23 1.394(4) . ?
C18 C19 1.402(4) . ?
C19 C20 1.388(4) . ?
C19 H19 0.9500 . ?
C20 C21 1.385(4) . ?
C20 H20 0.9500 . ?
C21 C22 1.372(4) . ?
C21 H21 0.9500 . ?
C22 C23 1.384(4) . ?
C22 H22 0.9500 . ?
C23 H23 0.9500 . ?
C24 C29 1.400(4) . ?
C24 C25 1.401(4) . ?
C25 C26 1.387(4) . ?
C25 H25 0.9500 . ?
C26 C27 1.382(4) . ?
C26 H26 0.9500 . ?
C27 C28 1.377(4) . ?
C27 H27 0.9500 . ?
C28 C29 1.387(4) . ?
C28 H28 0.9500 . ?
C29 H29 0.9500 . ?
C30 C35 1.398(4) . ?
C30 C31 1.401(4) . ?
C31 C32 1.391(4) . ?
C31 H31 0.9500 . ?
C32 C33 1.379(4) . ?
C32 H32 0.9500 . ?
C33 C34 1.380(4) . ?
C33 H33 0.9500 . ?
C34 C35 1.393(4) . ?
C34 H34 0.9500 . ?
C35 H35 0.9500 . ?
B1B C15B 1.722(4) . ?
B1B C14B 1.729(4) . ?
B1B B9B 1.767(4) . ?
B1B B8B 1.769(5) . ?
B1B B2B 1.783(4) . ?
B1B H1B 1.1200 . ?
B2B C14B 1.703(4) . ?
B2B B8B 1.776(5) . ?
B2B B3B 1.776(5) . ?
B2B B7B 1.785(5) . ?
B2B H2B 1.1200 . ?
B3B C14B 1.707(4) . ?
B3B B6B 1.769(4) . ?
B3B B4B 1.777(4) . ?
B3B B7B 1.778(5) . ?
B3B H3B 1.1200 . ?
B4B C14B 1.724(4) . ?
B4B C15B 1.731(4) . ?
B4B B6B 1.768(5) . ?
B4B B5B 1.774(4) . ?
B4B H4B 1.1200 . ?
B5B C15B 1.712(4) . ?
B5B B9B 1.766(5) . ?
B5B B10B 1.782(5) . ?
B5B B6B 1.787(4) . ?
B5B H5B 1.1200 . ?
B6B B7B 1.778(5) . ?
B6B B10B 1.781(5) . ?
B6B H6B 1.1200 . ?
B7B B10B 1.771(5) . ?
B7B B8B 1.777(5) . ?
B7B H7B 1.1200 . ?
B8B B9B 1.770(4) . ?
B8B B10B 1.781(5) . ?
B8B H8B 1.1200 . ?
B9B C15B 1.714(4) . ?
B9B B10B 1.783(4) . ?
B9B H9B 1.1200 . ?
B10B H10B 1.1200 . ?
C1B C10B 1.37(2) . ?
C1B C2B 1.405(18) . ?
C1B H1BA 0.9500 . ?
C2B C3B 1.43(2) . ?
C2B C14B 1.51(2) . ?
C3B C4B 1.41(2) . ?
C3B H3BA 0.9500 . ?
C4B C11B 1.364(12) . ?
C4B H4BA 0.9500 . ?
C5B C6B 1.3900 . ?
C5B C12B 1.3900 . ?
C5B H5BA 0.9500 . ?
C6B C7B 1.3900 . ?
C6B H6BA 0.9500 . ?
C7B C8B 1.3900 . ?
C7B H7BA 0.9500 . ?
C8B C13B 1.3900 . ?
C8B H8BA 0.9500 . ?
C13B C12B 1.3900 . ?
C13B C9B 1.498(18) . ?
C12B C11B 1.455(16) . ?
C9B C16B 1.50(2) . ?
C9B C10B 1.526(17) . ?
C9B C17B 1.53(3) . ?
C10B C11B 1.402(18) . ?
C16B H16D 0.9800 . ?
C16B H16E 0.9800 . ?
C16B H16F 0.9800 . ?
C17B H17D 0.9800 . ?
C17B H17E 0.9800 . ?
C17B H17F 0.9800 . ?
C18B C19B 1.3900 . ?
C18B C23B 1.3900 . ?
C18B Si1B 1.867(8) . ?
C19B C20B 1.3900 . ?
C19B H19B 0.9500 . ?
C20B C21B 1.3900 . ?
C20B H20B 0.9500 . ?
C21B C22B 1.3900 . ?
C21B H21B 0.9500 . ?
C22B C23B 1.3900 . ?
C22B H22B 0.9500 . ?
C23B H23B 0.9500 . ?
Si1B C24B 1.873(3) . ?
Si1B C30B 1.875(3) . ?
Si1B C18C 1.938(11) . ?
Si1B C15B 1.951(3) . ?
C14B C2C 1.52(3) . ?
C14B C15B 1.740(3) . ?
C24B C29B 1.396(4) . ?
C24B C25B 1.398(4) . ?
C25B C26B 1.386(4) . ?
C25B H25B 0.9500 . ?
C26B C27B 1.375(4) . ?
C26B H26B 0.9500 . ?
C27B C28B 1.384(4) . ?
C27B H27B 0.9500 . ?
C28B C29B 1.384(4) . ?
C28B H28B 0.9500 . ?
C29B H29B 0.9500 . ?
C30B C31B 1.398(4) . ?
C30B C35B 1.404(4) . ?
C31B C32B 1.383(4) . ?
C31B H31B 0.9500 . ?
C32B C33B 1.376(4) . ?
C32B H32B 0.9500 . ?
C33B C34B 1.376(4) . ?
C33B H33B 0.9500 . ?
C34B C35B 1.382(4) . ?
C34B H34B 0.9500 . ?
C35B H35B 0.9500 . ?
C1C C2C 1.39(3) . ?
C1C C10C 1.42(4) . ?
C1C H1C 0.9500 . ?
C2C C3C 1.34(3) . ?
C3C C4C 1.37(3) . ?
C3C H3C 0.9500 . ?
C4C C11C 1.402(17) . ?
C4C H4C 0.9500 . ?
C5C C6C 1.3900 . ?
C5C C12C 1.3900 . ?
C5C H5C 0.9500 . ?
C6C C7C 1.3900 . ?
C6C H6C 0.9500 . ?
C7C C8C 1.3900 . ?
C7C H7C 0.9500 . ?
C8C C13C 1.3900 . ?
C8C H8C 0.9500 . ?
C13C C12C 1.3900 . ?
C13C C9C 1.54(3) . ?
C12C C11C 1.47(2) . ?
C9C C10C 1.52(3) . ?
C9C C15C 1.58(4) . ?
C9C C14C 1.59(4) . ?
C10C C11C 1.38(2) . ?
C14C H14A 0.9800 . ?
C14C H14B 0.9800 . ?
C14C H14C 0.9800 . ?
C15C H15A 0.9800 . ?
C15C H15B 0.9800 . ?
C15C H15C 0.9800 . ?
C18C C19C 1.3900 . ?
C18C C23C 1.3900 . ?
C19C C20C 1.3900 . ?
C19C H19C 0.9500 . ?
C20C C21C 1.3900 . ?
C20C H20C 0.9500 . ?
C21C C22C 1.3900 . ?
C21C H21C 0.9500 . ?
C22C C23C 1.3900 . ?
C22C H22C 0.9500 . ?
C23C H23C 0.9500 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C15 B1 B2 C14 37.53(18) . . . . ?
B9 B1 B2 C14 99.2(2) . . . . ?
B8 B1 B2 C14 135.7(2) . . . . ?
C15 B1 B2 B8 -98.1(2) . . . . ?
C14 B1 B2 B8 -135.7(2) . . . . ?
B9 B1 B2 B8 -36.5(2) . . . . ?
C15 B1 B2 B3 2.9(3) . . . . ?
C14 B1 B2 B3 -34.67(19) . . . . ?
B9 B1 B2 B3 64.5(3) . . . . ?
B8 B1 B2 B3 101.0(2) . . . . ?
C15 B1 B2 B7 -60.3(3) . . . . ?
C14 B1 B2 B7 -97.8(2) . . . . ?
B9 B1 B2 B7 1.4(3) . . . . ?
B8 B1 B2 B7 37.9(2) . . . . ?
B8 B2 B3 C14 98.3(2) . . . . ?
B7 B2 B3 C14 135.9(2) . . . . ?
B1 B2 B3 C14 35.04(19) . . . . ?
C14 B2 B3 B6 -98.2(2) . . . . ?
B8 B2 B3 B6 0.1(3) . . . . ?
B7 B2 B3 B6 37.7(2) . . . . ?
B1 B2 B3 B6 -63.1(3) . . . . ?
C14 B2 B3 B7 -135.9(2) . . . . ?
B8 B2 B3 B7 -37.6(2) . . . . ?
B1 B2 B3 B7 -100.9(2) . . . . ?
C14 B2 B3 B4 -35.28(19) . . . . ?
B8 B2 B3 B4 63.0(3) . . . . ?
B7 B2 B3 B4 100.6(2) . . . . ?
B1 B2 B3 B4 -0.2(3) . . . . ?
B6 B3 B4 C14 136.2(2) . . . . ?
B7 B3 B4 C14 98.4(2) . . . . ?
B2 B3 B4 C14 35.10(19) . . . . ?
C14 B3 B4 C15 -37.57(18) . . . . ?
B6 B3 B4 C15 98.6(2) . . . . ?
B7 B3 B4 C15 60.8(3) . . . . ?
B2 B3 B4 C15 -2.5(3) . . . . ?
C14 B3 B4 B6 -136.2(2) . . . . ?
B7 B3 B4 B6 -37.8(2) . . . . ?
B2 B3 B4 B6 -101.1(2) . . . . ?
C14 B3 B4 B5 -98.8(2) . . . . ?
B6 B3 B4 B5 37.4(2) . . . . ?
B7 B3 B4 B5 -0.4(3) . . . . ?
B2 B3 B4 B5 -63.7(3) . . . . ?
C14 B4 B5 C15 38.03(19) . . . . ?
B6 B4 B5 C15 136.8(2) . . . . ?
B3 B4 B5 C15 99.5(2) . . . . ?
C14 B4 B5 B9 2.3(3) . . . . ?
C15 B4 B5 B9 -35.75(19) . . . . ?
B6 B4 B5 B9 101.0(2) . . . . ?
B3 B4 B5 B9 63.8(3) . . . . ?
C14 B4 B5 B10 -61.5(3) . . . . ?
C15 B4 B5 B10 -99.5(2) . . . . ?
B6 B4 B5 B10 37.3(2) . . . . ?
B3 B4 B5 B10 0.0(3) . . . . ?
C14 B4 B5 B6 -98.7(2) . . . . ?
C15 B4 B5 B6 -136.8(2) . . . . ?
B3 B4 B5 B6 -37.2(2) . . . . ?
C14 B4 B6 B3 -37.71(19) . . . . ?
C15 B4 B6 B3 -101.5(2) . . . . ?
B5 B4 B6 B3 -138.6(2) . . . . ?
C14 B4 B6 B7 0.2(3) . . . . ?
C15 B4 B6 B7 -63.6(3) . . . . ?
B5 B4 B6 B7 -100.7(2) . . . . ?
B3 B4 B6 B7 37.9(2) . . . . ?
C14 B4 B6 B10 63.7(3) . . . . ?
C15 B4 B6 B10 -0.1(3) . . . . ?
B5 B4 B6 B10 -37.2(2) . . . . ?
B3 B4 B6 B10 101.4(2) . . . . ?
C14 B4 B6 B5 100.9(2) . . . . ?
C15 B4 B6 B5 37.11(19) . . . . ?
B3 B4 B6 B5 138.6(2) . . . . ?
C14 B3 B6 B4 38.19(19) . . . . ?
B7 B3 B6 B4 137.6(2) . . . . ?
B2 B3 B6 B4 99.9(2) . . . . ?
C14 B3 B6 B7 -99.4(2) . . . . ?
B4 B3 B6 B7 -137.6(2) . . . . ?
B2 B3 B6 B7 -37.7(2) . . . . ?
C14 B3 B6 B10 -62.3(3) . . . . ?
B7 B3 B6 B10 37.1(2) . . . . ?
B4 B3 B6 B10 -100.5(2) . . . . ?
B2 B3 B6 B10 -0.6(3) . . . . ?
C14 B3 B6 B5 1.1(3) . . . . ?
B7 B3 B6 B5 100.5(2) . . . . ?
B4 B3 B6 B5 -37.1(2) . . . . ?
B2 B3 B6 B5 62.8(3) . . . . ?
C15 B5 B6 B4 -38.36(19) . . . . ?
B9 B5 B6 B4 -100.6(2) . . . . ?
B10 B5 B6 B4 -138.2(2) . . . . ?
C15 B5 B6 B3 -1.1(3) . . . . ?
B4 B5 B6 B3 37.3(2) . . . . ?
B9 B5 B6 B3 -63.3(3) . . . . ?
B10 B5 B6 B3 -101.0(2) . . . . ?
C15 B5 B6 B7 62.4(3) . . . . ?
B4 B5 B6 B7 100.8(2) . . . . ?
B9 B5 B6 B7 0.1(3) . . . . ?
B10 B5 B6 B7 -37.5(2) . . . . ?
C15 B5 B6 B10 99.9(2) . . . . ?
B4 B5 B6 B10 138.2(2) . . . . ?
B9 B5 B6 B10 37.6(2) . . . . ?
C14 B3 B7 B6 99.6(2) . . . . ?
B4 B3 B7 B6 37.6(2) . . . . ?
B2 B3 B7 B6 137.8(2) . . . . ?
C14 B3 B7 B8 -0.9(3) . . . . ?
B6 B3 B7 B8 -100.5(2) . . . . ?
B4 B3 B7 B8 -62.9(3) . . . . ?
B2 B3 B7 B8 37.3(2) . . . . ?
C14 B3 B7 B2 -38.2(2) . . . . ?
B6 B3 B7 B2 -137.8(2) . . . . ?
B4 B3 B7 B2 -100.2(2) . . . . ?
C14 B3 B7 B10 62.6(3) . . . . ?
B6 B3 B7 B10 -37.0(2) . . . . ?
B4 B3 B7 B10 0.6(3) . . . . ?
B2 B3 B7 B10 100.8(2) . . . . ?
B4 B6 B7 B3 -38.0(2) . . . . ?
B10 B6 B7 B3 -138.6(2) . . . . ?
B5 B6 B7 B3 -101.3(2) . . . . ?
B4 B6 B7 B8 62.5(3) . . . . ?
B3 B6 B7 B8 100.5(2) . . . . ?
B10 B6 B7 B8 -38.1(2) . . . . ?
B5 B6 B7 B8 -0.7(3) . . . . ?
B4 B6 B7 B2 -0.4(3) . . . . ?
B3 B6 B7 B2 37.7(2) . . . . ?
B10 B6 B7 B2 -101.0(2) . . . . ?
B5 B6 B7 B2 -63.6(3) . . . . ?
B4 B6 B7 B10 100.6(2) . . . . ?
B3 B6 B7 B10 138.6(2) . . . . ?
B5 B6 B7 B10 37.4(2) . . . . ?
C14 B2 B7 B3 38.00(19) . . . . ?
B8 B2 B7 B3 138.0(2) . . . . ?
B1 B2 B7 B3 100.2(2) . . . . ?
C14 B2 B7 B6 0.4(3) . . . . ?
B8 B2 B7 B6 100.4(2) . . . . ?
B3 B2 B7 B6 -37.6(2) . . . . ?
B1 B2 B7 B6 62.6(3) . . . . ?
C14 B2 B7 B8 -100.0(2) . . . . ?
B3 B2 B7 B8 -138.0(2) . . . . ?
B1 B2 B7 B8 -37.7(2) . . . . ?
C14 B2 B7 B10 -62.9(3) . . . . ?
B8 B2 B7 B10 37.0(2) . . . . ?
B3 B2 B7 B10 -100.9(2) . . . . ?
B1 B2 B7 B10 -0.7(3) . . . . ?
C14 B2 B8 B9 -2.0(3) . . . . ?
B3 B2 B8 B9 -63.5(3) . . . . ?
B7 B2 B8 B9 -101.0(2) . . . . ?
B1 B2 B8 B9 36.7(2) . . . . ?
C14 B2 B8 B1 -38.74(19) . . . . ?
B3 B2 B8 B1 -100.2(2) . . . . ?
B7 B2 B8 B1 -137.7(2) . . . . ?
C14 B2 B8 B7 98.9(2) . . . . ?
B3 B2 B8 B7 37.5(2) . . . . ?
B1 B2 B8 B7 137.7(2) . . . . ?
C14 B2 B8 B10 61.9(3) . . . . ?
B3 B2 B8 B10 0.4(3) . . . . ?
B7 B2 B8 B10 -37.1(2) . . . . ?
B1 B2 B8 B10 100.6(2) . . . . ?
C15 B1 B8 B2 101.3(2) . . . . ?
C14 B1 B8 B2 37.90(19) . . . . ?
B9 B1 B8 B2 139.3(2) . . . . ?
C15 B1 B8 B9 -37.92(19) . . . . ?
C14 B1 B8 B9 -101.4(2) . . . . ?
B2 B1 B8 B9 -139.3(2) . . . . ?
C15 B1 B8 B7 63.3(3) . . . . ?
C14 B1 B8 B7 -0.1(3) . . . . ?
B9 B1 B8 B7 101.3(2) . . . . ?
B2 B1 B8 B7 -38.0(2) . . . . ?
C15 B1 B8 B10 -0.1(3) . . . . ?
C14 B1 B8 B10 -63.6(3) . . . . ?
B9 B1 B8 B10 37.8(2) . . . . ?
B2 B1 B8 B10 -101.5(2) . . . . ?
B3 B7 B8 B2 -37.5(2) . . . . ?
B6 B7 B8 B2 -100.7(2) . . . . ?
B10 B7 B8 B2 -138.7(2) . . . . ?
B3 B7 B8 B9 64.2(3) . . . . ?
B6 B7 B8 B9 1.1(3) . . . . ?
B2 B7 B8 B9 101.7(2) . . . . ?
B10 B7 B8 B9 -37.0(2) . . . . ?
B3 B7 B8 B1 0.6(3) . . . . ?
B6 B7 B8 B1 -62.5(3) . . . . ?
B2 B7 B8 B1 38.1(2) . . . . ?
B10 B7 B8 B1 -100.6(2) . . . . ?
B3 B7 B8 B10 101.2(2) . . . . ?
B6 B7 B8 B10 38.0(2) . . . . ?
B2 B7 B8 B10 138.7(2) . . . . ?
B4 B5 B9 C15 36.2(2) . . . . ?
B10 B5 B9 C15 136.7(2) . . . . ?
B6 B5 B9 C15 99.3(2) . . . . ?
C15 B5 B9 B8 -98.7(2) . . . . ?
B4 B5 B9 B8 -62.6(3) . . . . ?
B10 B5 B9 B8 38.0(2) . . . . ?
B6 B5 B9 B8 0.5(3) . . . . ?
C15 B5 B9 B1 -35.5(2) . . . . ?
B4 B5 B9 B1 0.7(3) . . . . ?
B10 B5 B9 B1 101.3(2) . . . . ?
B6 B5 B9 B1 63.8(3) . . . . ?
C15 B5 B9 B10 -136.7(2) . . . . ?
B4 B5 B9 B10 -100.6(2) . . . . ?
B6 B5 B9 B10 -37.5(2) . . . . ?
B2 B8 B9 C15 1.7(3) . . . . ?
B1 B8 B9 C15 38.66(19) . . . . ?
B7 B8 B9 C15 -62.2(3) . . . . ?
B10 B8 B9 C15 -99.1(2) . . . . ?
B2 B8 B9 B5 63.0(3) . . . . ?
B1 B8 B9 B5 99.9(2) . . . . ?
B7 B8 B9 B5 -1.0(3) . . . . ?
B10 B8 B9 B5 -37.9(2) . . . . ?
B2 B8 B9 B1 -36.9(2) . . . . ?
B7 B8 B9 B1 -100.9(2) . . . . ?
B10 B8 B9 B1 -137.8(2) . . . . ?
B2 B8 B9 B10 100.9(2) . . . . ?
B1 B8 B9 B10 137.8(2) . . . . ?
B7 B8 B9 B10 36.9(2) . . . . ?
C14 B1 B9 C15 -38.31(19) . . . . ?
B8 B1 B9 C15 -136.0(2) . . . . ?
B2 B1 B9 C15 -99.6(2) . . . . ?
C15 B1 B9 B5 34.95(19) . . . . ?
C14 B1 B9 B5 -3.4(3) . . . . ?
B8 B1 B9 B5 -101.0(2) . . . . ?
B2 B1 B9 B5 -64.7(3) . . . . ?
C15 B1 B9 B8 136.0(2) . . . . ?
C14 B1 B9 B8 97.7(2) . . . . ?
B2 B1 B9 B8 36.3(2) . . . . ?
C15 B1 B9 B10 98.1(2) . . . . ?
C14 B1 B9 B10 59.8(3) . . . . ?
B8 B1 B9 B10 -37.8(2) . . . . ?
B2 B1 B9 B10 -1.5(3) . . . . ?
C15 B5 B10 B6 -100.3(2) . . . . ?
B4 B5 B10 B6 -37.1(2) . . . . ?
B9 B5 B10 B6 -138.2(2) . . . . ?
C15 B5 B10 B7 -62.8(3) . . . . ?
B4 B5 B10 B7 0.3(3) . . . . ?
B9 B5 B10 B7 -100.7(2) . . . . ?
B6 B5 B10 B7 37.5(2) . . . . ?
C15 B5 B10 B9 37.87(19) . . . . ?
B4 B5 B10 B9 101.0(2) . . . . ?
B6 B5 B10 B9 138.2(2) . . . . ?
C15 B5 B10 B8 0.3(3) . . . . ?
B4 B5 B10 B8 63.5(3) . . . . ?
B9 B5 B10 B8 -37.6(2) . . . . ?
B6 B5 B10 B8 100.6(2) . . . . ?
B4 B6 B10 B5 37.2(2) . . . . ?
B3 B6 B10 B5 101.0(2) . . . . ?
B7 B6 B10 B5 138.1(2) . . . . ?
B4 B6 B10 B7 -100.9(2) . . . . ?
B3 B6 B10 B7 -37.1(2) . . . . ?
B5 B6 B10 B7 -138.1(2) . . . . ?
B4 B6 B10 B9 0.0(3) . . . . ?
B3 B6 B10 B9 63.7(3) . . . . ?
B7 B6 B10 B9 100.8(2) . . . . ?
B5 B6 B10 B9 -37.3(2) . . . . ?
B4 B6 B10 B8 -62.9(3) . . . . ?
B3 B6 B10 B8 0.9(3) . . . . ?
B7 B6 B10 B8 37.9(2) . . . . ?
B5 B6 B10 B8 -100.1(2) . . . . ?
B3 B7 B10 B5 -0.6(3) . . . . ?
B6 B7 B10 B5 -37.6(2) . . . . ?
B8 B7 B10 B5 99.7(2) . . . . ?
B2 B7 B10 B5 62.9(3) . . . . ?
B3 B7 B10 B6 37.0(2) . . . . ?
B8 B7 B10 B6 137.3(2) . . . . ?
B2 B7 B10 B6 100.5(2) . . . . ?
B3 B7 B10 B9 -63.7(3) . . . . ?
B6 B7 B10 B9 -100.7(2) . . . . ?
B8 B7 B10 B9 36.6(2) . . . . ?
B2 B7 B10 B9 -0.2(3) . . . . ?
B3 B7 B10 B8 -100.3(2) . . . . ?
B6 B7 B10 B8 -137.3(2) . . . . ?
B2 B7 B10 B8 -36.8(2) . . . . ?
C15 B9 B10 B5 -37.3(2) . . . . ?
B8 B9 B10 B5 -137.5(2) . . . . ?
B1 B9 B10 B5 -99.8(2) . . . . ?
C15 B9 B10 B6 0.2(3) . . . . ?
B5 B9 B10 B6 37.5(2) . . . . ?
B8 B9 B10 B6 -100.1(2) . . . . ?
B1 B9 B10 B6 -62.3(3) . . . . ?
C15 B9 B10 B7 63.5(3) . . . . ?
B5 B9 B10 B7 100.8(2) . . . . ?
B8 B9 B10 B7 -36.7(2) . . . . ?
B1 B9 B10 B7 1.1(3) . . . . ?
C15 B9 B10 B8 100.2(2) . . . . ?
B5 B9 B10 B8 137.5(2) . . . . ?
B1 B9 B10 B8 37.8(2) . . . . ?
B2 B8 B10 B5 -64.1(3) . . . . ?
B9 B8 B10 B5 37.6(2) . . . . ?
B1 B8 B10 B5 -0.1(3) . . . . ?
B7 B8 B10 B5 -101.3(2) . . . . ?
B2 B8 B10 B6 -0.8(3) . . . . ?
B9 B8 B10 B6 100.9(2) . . . . ?
B1 B8 B10 B6 63.2(3) . . . . ?
B7 B8 B10 B6 -38.0(2) . . . . ?
B2 B8 B10 B7 37.2(2) . . . . ?
B9 B8 B10 B7 138.9(2) . . . . ?
B1 B8 B10 B7 101.2(2) . . . . ?
B2 B8 B10 B9 -101.7(2) . . . . ?
B1 B8 B10 B9 -37.7(2) . . . . ?
B7 B8 B10 B9 -138.9(2) . . . . ?
C10 C1 C2 C3 -3.6(4) . . . . ?
C10 C1 C2 C14 180.0(2) . . . . ?
C1 C2 C3 C4 2.0(4) . . . . ?
C14 C2 C3 C4 178.5(2) . . . . ?
C2 C3 C4 C11 0.6(4) . . . . ?
C12 C5 C6 C7 -0.1(5) . . . . ?
C5 C6 C7 C8 -0.8(5) . . . . ?
C6 C7 C8 C13 0.2(5) . . . . ?
C2 C1 C10 C11 2.6(4) . . . . ?
C2 C1 C10 C9 -176.1(2) . . . . ?
C13 C9 C10 C1 177.1(3) . . . . ?
C16 C9 C10 C1 58.0(4) . . . . ?
C17 C9 C10 C1 -65.2(4) . . . . ?
C13 C9 C10 C11 -1.7(3) . . . . ?
C16 C9 C10 C11 -120.8(3) . . . . ?
C17 C9 C10 C11 116.0(3) . . . . ?
C3 C4 C11 C10 -1.6(4) . . . . ?
C3 C4 C11 C12 176.5(3) . . . . ?
C1 C10 C11 C4 0.1(4) . . . . ?
C9 C10 C11 C4 179.0(2) . . . . ?
C1 C10 C11 C12 -178.5(2) . . . . ?
C9 C10 C11 C12 0.5(3) . . . . ?
C6 C5 C12 C13 1.8(4) . . . . ?
C6 C5 C12 C11 -177.8(3) . . . . ?
C4 C11 C12 C5 2.4(5) . . . . ?
C10 C11 C12 C5 -179.3(3) . . . . ?
C4 C11 C12 C13 -177.2(3) . . . . ?
C10 C11 C12 C13 1.1(3) . . . . ?
C7 C8 C13 C12 1.4(4) . . . . ?
C7 C8 C13 C9 -179.2(3) . . . . ?
C5 C12 C13 C8 -2.4(4) . . . . ?
C11 C12 C13 C8 177.2(2) . . . . ?
C5 C12 C13 C9 178.1(3) . . . . ?
C11 C12 C13 C9 -2.3(3) . . . . ?
C10 C9 C13 C8 -177.0(3) . . . . ?
C16 C9 C13 C8 -58.3(4) . . . . ?
C17 C9 C13 C8 65.6(4) . . . . ?
C10 C9 C13 C12 2.4(3) . . . . ?
C16 C9 C13 C12 121.2(3) . . . . ?
C17 C9 C13 C12 -115.0(3) . . . . ?
C3 C2 C14 B3 -124.9(3) . . . . ?
C1 C2 C14 B3 51.5(3) . . . . ?
C3 C2 C14 B2 -51.2(3) . . . . ?
C1 C2 C14 B2 125.2(3) . . . . ?
C3 C2 C14 B4 162.6(2) . . . . ?
C1 C2 C14 B4 -21.0(3) . . . . ?
C3 C2 C14 B1 22.3(4) . . . . ?
C1 C2 C14 B1 -161.3(2) . . . . ?
C3 C2 C14 C15 92.5(3) . . . . ?
C1 C2 C14 C15 -91.1(3) . . . . ?
B6 B3 C14 C2 -147.2(2) . . . . ?
B7 B3 C14 C2 150.0(2) . . . . ?
B4 B3 C14 C2 -108.8(2) . . . . ?
B2 B3 C14 C2 111.2(3) . . . . ?
B6 B3 C14 B2 101.6(2) . . . . ?
B7 B3 C14 B2 38.8(2) . . . . ?
B4 B3 C14 B2 140.0(2) . . . . ?
B6 B3 C14 B4 -38.41(19) . . . . ?
B7 B3 C14 B4 -101.2(2) . . . . ?
B2 B3 C14 B4 -140.0(2) . . . . ?
B6 B3 C14 B1 63.7(3) . . . . ?
B7 B3 C14 B1 0.9(3) . . . . ?
B4 B3 C14 B1 102.1(2) . . . . ?
B2 B3 C14 B1 -37.9(2) . . . . ?
B6 B3 C14 C15 -0.8(3) . . . . ?
B7 B3 C14 C15 -63.5(2) . . . . ?
B4 B3 C14 C15 37.66(19) . . . . ?
B2 B3 C14 C15 -102.4(2) . . . . ?
B8 B2 C14 C2 149.1(2) . . . . ?
B3 B2 C14 C2 -109.4(2) . . . . ?
B7 B2 C14 C2 -148.1(2) . . . . ?
B1 B2 C14 C2 110.1(2) . . . . ?
B8 B2 C14 B3 -101.5(2) . . . . ?
B7 B2 C14 B3 -38.7(2) . . . . ?
B1 B2 C14 B3 -140.5(2) . . . . ?
B8 B2 C14 B4 -63.1(3) . . . . ?
B3 B2 C14 B4 38.3(2) . . . . ?
B7 B2 C14 B4 -0.3(3) . . . . ?
B1 B2 C14 B4 -102.1(2) . . . . ?
B8 B2 C14 B1 39.0(2) . . . . ?
B3 B2 C14 B1 140.5(2) . . . . ?
B7 B2 C14 B1 101.8(2) . . . . ?
B8 B2 C14 C15 1.6(3) . . . . ?
B3 B2 C14 C15 103.0(2) . . . . ?
B7 B2 C14 C15 64.4(2) . . . . ?
B1 B2 C14 C15 -37.43(19) . . . . ?
C15 B4 C14 C2 -111.6(2) . . . . ?
B6 B4 C14 C2 148.6(2) . . . . ?
B5 B4 C14 C2 -148.1(2) . . . . ?
B3 B4 C14 C2 110.0(2) . . . . ?
C15 B4 C14 B3 138.4(2) . . . . ?
B6 B4 C14 B3 38.53(19) . . . . ?
B5 B4 C14 B3 101.8(2) . . . . ?
C15 B4 C14 B2 100.0(2) . . . . ?
B6 B4 C14 B2 0.1(3) . . . . ?
B5 B4 C14 B2 63.4(3) . . . . ?
B3 B4 C14 B2 -38.4(2) . . . . ?
C15 B4 C14 B1 32.1(2) . . . . ?
B6 B4 C14 B1 -67.8(2) . . . . ?
B5 B4 C14 B1 -4.5(3) . . . . ?
B3 B4 C14 B1 -106.3(2) . . . . ?
B6 B4 C14 C15 -99.9(2) . . . . ?
B5 B4 C14 C15 -36.58(18) . . . . ?
B3 B4 C14 C15 -138.4(2) . . . . ?
C15 B1 C14 C2 110.8(2) . . . . ?
B9 B1 C14 C2 148.0(2) . . . . ?
B8 B1 C14 C2 -149.4(2) . . . . ?
B2 B1 C14 C2 -110.9(3) . . . . ?
C15 B1 C14 B3 -100.3(2) . . . . ?
B9 B1 C14 B3 -63.1(3) . . . . ?
B8 B1 C14 B3 -0.5(3) . . . . ?
B2 B1 C14 B3 38.1(2) . . . . ?
C15 B1 C14 B2 -138.3(2) . . . . ?
B9 B1 C14 B2 -101.2(2) . . . . ?
B8 B1 C14 B2 -38.6(2) . . . . ?
C15 B1 C14 B4 -32.2(2) . . . . ?
B9 B1 C14 B4 5.0(3) . . . . ?
B8 B1 C14 B4 67.6(3) . . . . ?
B2 B1 C14 B4 106.1(2) . . . . ?
B9 B1 C14 C15 37.16(19) . . . . ?
B8 B1 C14 C15 99.8(2) . . . . ?
B2 B1 C14 C15 138.3(2) . . . . ?
B4 B5 C15 B9 -139.6(2) . . . . ?
B10 B5 C15 B9 -38.5(2) . . . . ?
B6 B5 C15 B9 -101.4(2) . . . . ?
B4 B5 C15 B1 -101.6(2) . . . . ?
B9 B5 C15 B1 38.0(2) . . . . ?
B10 B5 C15 B1 -0.4(3) . . . . ?
B6 B5 C15 B1 -63.4(3) . . . . ?
B9 B5 C15 B4 139.6(2) . . . . ?
B10 B5 C15 B4 101.2(2) . . . . ?
B6 B5 C15 B4 38.2(2) . . . . ?
B4 B5 C15 C14 -37.57(19) . . . . ?
B9 B5 C15 C14 102.1(2) . . . . ?
B10 B5 C15 C14 63.6(2) . . . . ?
B6 B5 C15 C14 0.6(3) . . . . ?
B4 B5 C15 Si1 109.6(2) . . . . ?
B9 B5 C15 Si1 -110.8(2) . . . . ?
B10 B5 C15 Si1 -149.25(18) . . . . ?
B6 B5 C15 Si1 147.77(18) . . . . ?
B8 B9 C15 B5 101.0(2) . . . . ?
B1 B9 C15 B5 139.9(2) . . . . ?
B10 B9 C15 B5 38.1(2) . . . . ?
B5 B9 C15 B1 -139.9(2) . . . . ?
B8 B9 C15 B1 -38.9(2) . . . . ?
B10 B9 C15 B1 -101.9(2) . . . . ?
B5 B9 C15 B4 -38.3(2) . . . . ?
B8 B9 C15 B4 62.7(3) . . . . ?
B1 B9 C15 B4 101.6(2) . . . . ?
B10 B9 C15 B4 -0.2(3) . . . . ?
B5 B9 C15 C14 -101.8(2) . . . . ?
B8 B9 C15 C14 -0.8(3) . . . . ?
B1 B9 C15 C14 38.14(19) . . . . ?
B10 B9 C15 C14 -63.7(2) . . . . ?
B5 B9 C15 Si1 108.9(2) . . . . ?
B8 B9 C15 Si1 -150.05(18) . . . . ?
B1 B9 C15 Si1 -111.1(2) . . . . ?
B10 B9 C15 Si1 146.99(18) . . . . ?
C14 B1 C15 B5 99.0(2) . . . . ?
B9 B1 C15 B5 -38.3(2) . . . . ?
B8 B1 C15 B5 0.3(3) . . . . ?
B2 B1 C15 B5 62.7(3) . . . . ?
C14 B1 C15 B9 137.3(2) . . . . ?
B8 B1 C15 B9 38.6(2) . . . . ?
B2 B1 C15 B9 101.0(2) . . . . ?
C14 B1 C15 B4 31.78(19) . . . . ?
B9 B1 C15 B4 -105.5(2) . . . . ?
B8 B1 C15 B4 -66.9(2) . . . . ?
B2 B1 C15 B4 -4.5(3) . . . . ?
B9 B1 C15 C14 -137.3(2) . . . . ?
B8 B1 C15 C14 -98.7(2) . . . . ?
B2 B1 C15 C14 -36.29(18) . . . . ?
C14 B1 C15 Si1 -112.9(2) . . . . ?
B9 B1 C15 Si1 109.8(2) . . . . ?
B8 B1 C15 Si1 148.47(18) . . . . ?
B2 B1 C15 Si1 -149.15(18) . . . . ?
C14 B4 C15 B5 -137.7(2) . . . . ?
B6 B4 C15 B5 -38.3(2) . . . . ?
B3 B4 C15 B5 -101.3(2) . . . . ?
C14 B4 C15 B9 -99.1(2) . . . . ?
B6 B4 C15 B9 0.2(3) . . . . ?
B5 B4 C15 B9 38.5(2) . . . . ?
B3 B4 C15 B9 -62.8(3) . . . . ?
C14 B4 C15 B1 -31.97(19) . . . . ?
B6 B4 C15 B1 67.4(2) . . . . ?
B5 B4 C15 B1 105.7(2) . . . . ?
B3 B4 C15 B1 4.4(3) . . . . ?
B6 B4 C15 C14 99.3(2) . . . . ?
B5 B4 C15 C14 137.7(2) . . . . ?
B3 B4 C15 C14 36.35(18) . . . . ?
C14 B4 C15 Si1 113.34(19) . . . . ?
B6 B4 C15 Si1 -147.32(18) . . . . ?
B5 B4 C15 Si1 -109.0(2) . . . . ?
B3 B4 C15 Si1 149.69(18) . . . . ?
C2 C14 C15 B5 145.7(2) . . . . ?
B3 C14 C15 B5 0.1(3) . . . . ?
B2 C14 C15 B5 -67.1(2) . . . . ?
B4 C14 C15 B5 38.9(2) . . . . ?
B1 C14 C15 B5 -105.9(2) . . . . ?
C2 C14 C15 B9 -147.7(2) . . . . ?
B3 C14 C15 B9 66.7(2) . . . . ?
B2 C14 C15 B9 -0.5(3) . . . . ?
B4 C14 C15 B9 105.5(2) . . . . ?
B1 C14 C15 B9 -39.2(2) . . . . ?
C2 C14 C15 B1 -108.4(2) . . . . ?
B3 C14 C15 B1 106.0(2) . . . . ?
B2 C14 C15 B1 38.7(2) . . . . ?
B4 C14 C15 B1 144.8(2) . . . . ?
C2 C14 C15 B4 106.8(2) . . . . ?
B3 C14 C15 B4 -38.8(2) . . . . ?
B2 C14 C15 B4 -106.1(2) . . . . ?
B1 C14 C15 B4 -144.8(2) . . . . ?
C2 C14 C15 Si1 0.4(3) . . . . ?
B3 C14 C15 Si1 -145.25(18) . . . . ?
B2 C14 C15 Si1 147.52(18) . . . . ?
B4 C14 C15 Si1 -106.4(2) . . . . ?
B1 C14 C15 Si1 108.8(2) . . . . ?
C24 Si1 C18 C23 -5.7(3) . . . . ?
C30 Si1 C18 C23 -125.5(2) . . . . ?
C15 Si1 C18 C23 114.3(2) . . . . ?
C24 Si1 C18 C19 172.4(2) . . . . ?
C30 Si1 C18 C19 52.6(2) . . . . ?
C15 Si1 C18 C19 -67.6(2) . . . . ?
C23 C18 C19 C20 -1.6(4) . . . . ?
Si1 C18 C19 C20 -179.8(2) . . . . ?
C18 C19 C20 C21 0.9(4) . . . . ?
C19 C20 C21 C22 0.6(5) . . . . ?
C20 C21 C22 C23 -1.4(5) . . . . ?
C21 C22 C23 C18 0.6(5) . . . . ?
C19 C18 C23 C22 0.9(4) . . . . ?
Si1 C18 C23 C22 179.0(2) . . . . ?
C18 Si1 C24 C29 -124.7(2) . . . . ?
C30 Si1 C24 C29 -5.2(3) . . . . ?
C15 Si1 C24 C29 114.1(2) . . . . ?
C18 Si1 C24 C25 55.1(3) . . . . ?
C30 Si1 C24 C25 174.6(2) . . . . ?
C15 Si1 C24 C25 -66.1(2) . . . . ?
C29 C24 C25 C26 -1.5(4) . . . . ?
Si1 C24 C25 C26 178.7(2) . . . . ?
C24 C25 C26 C27 1.0(5) . . . . ?
C25 C26 C27 C28 0.2(5) . . . . ?
C26 C27 C28 C29 -0.9(5) . . . . ?
C27 C28 C29 C24 0.3(5) . . . . ?
C25 C24 C29 C28 0.8(4) . . . . ?
Si1 C24 C29 C28 -179.3(2) . . . . ?
C18 Si1 C30 C35 17.9(3) . . . . ?
C24 Si1 C30 C35 -104.1(2) . . . . ?
C15 Si1 C30 C35 138.1(2) . . . . ?
C18 Si1 C30 C31 -168.6(2) . . . . ?
C24 Si1 C30 C31 69.4(3) . . . . ?
C15 Si1 C30 C31 -48.5(3) . . . . ?
C35 C30 C31 C32 -0.7(4) . . . . ?
Si1 C30 C31 C32 -174.3(2) . . . . ?
C30 C31 C32 C33 0.8(5) . . . . ?
C31 C32 C33 C34 -0.8(4) . . . . ?
C32 C33 C34 C35 0.9(4) . . . . ?
C33 C34 C35 C30 -0.9(4) . . . . ?
C31 C30 C35 C34 0.8(4) . . . . ?
Si1 C30 C35 C34 174.7(2) . . . . ?
C15B B1B B2B C14B 36.8(2) . . . . ?
B9B B1B B2B C14B 98.9(2) . . . . ?
B8B B1B B2B C14B 135.8(2) . . . . ?
C15B B1B B2B B8B -99.0(2) . . . . ?
C14B B1B B2B B8B -135.8(2) . . . . ?
B9B B1B B2B B8B -36.9(2) . . . . ?
C15B B1B B2B B3B 1.7(3) . . . . ?
C14B B1B B2B B3B -35.1(2) . . . . ?
B9B B1B B2B B3B 63.8(3) . . . . ?
B8B B1B B2B B3B 100.7(3) . . . . ?
C15B B1B B2B B7B -61.4(3) . . . . ?
C14B B1B B2B B7B -98.2(3) . . . . ?
B9B B1B B2B B7B 0.7(3) . . . . ?
B8B B1B B2B B7B 37.6(2) . . . . ?
B8B B2B B3B C14B 98.3(2) . . . . ?
B1B B2B B3B C14B 35.4(2) . . . . ?
B7B B2B B3B C14B 135.8(2) . . . . ?
C14B B2B B3B B6B -98.2(2) . . . . ?
B8B B2B B3B B6B 0.1(3) . . . . ?
B1B B2B B3B B6B -62.8(3) . . . . ?
B7B B2B B3B B6B 37.6(2) . . . . ?
C14B B2B B3B B4B -35.0(2) . . . . ?
B8B B2B B3B B4B 63.3(3) . . . . ?
B1B B2B B3B B4B 0.4(3) . . . . ?
B7B B2B B3B B4B 100.7(2) . . . . ?
C14B B2B B3B B7B -135.8(2) . . . . ?
B8B B2B B3B B7B -37.5(2) . . . . ?
B1B B2B B3B B7B -100.3(2) . . . . ?
B6B B3B B4B C14B 136.2(2) . . . . ?
B2B B3B B4B C14B 34.7(2) . . . . ?
B7B B3B B4B C14B 98.2(2) . . . . ?
C14B B3B B4B C15B -37.0(2) . . . . ?
B6B B3B B4B C15B 99.2(2) . . . . ?
B2B B3B B4B C15B -2.3(3) . . . . ?
B7B B3B B4B C15B 61.2(3) . . . . ?
C14B B3B B4B B6B -136.2(2) . . . . ?
B2B B3B B4B B6B -101.5(3) . . . . ?
B7B B3B B4B B6B -38.0(2) . . . . ?
C14B B3B B4B B5B -98.8(2) . . . . ?
B6B B3B B4B B5B 37.4(2) . . . . ?
B2B B3B B4B B5B -64.1(3) . . . . ?
B7B B3B B4B B5B -0.6(3) . . . . ?
C14B B4B B5B C15B 37.80(19) . . . . ?
B6B B4B B5B C15B 136.5(2) . . . . ?
B3B B4B B5B C15B 99.3(2) . . . . ?
C14B B4B B5B B9B 2.2(3) . . . . ?
C15B B4B B5B B9B -35.6(2) . . . . ?
B6B B4B B5B B9B 100.9(3) . . . . ?
B3B B4B B5B B9B 63.8(3) . . . . ?
C14B B4B B5B B10B -61.4(3) . . . . ?
C15B B4B B5B B10B -99.1(2) . . . . ?
B6B B4B B5B B10B 37.3(2) . . . . ?
B3B B4B B5B B10B 0.2(3) . . . . ?
C14B B4B B5B B6B -98.7(2) . . . . ?
C15B B4B B5B B6B -136.5(2) . . . . ?
B3B B4B B5B B6B -37.1(2) . . . . ?
C14B B4B B6B B3B -37.7(2) . . . . ?
C15B B4B B6B B3B -100.9(2) . . . . ?
B5B B4B B6B B3B -138.6(2) . . . . ?
C14B B4B B6B B7B 0.4(3) . . . . ?
C15B B4B B6B B7B -62.7(3) . . . . ?
B5B B4B B6B B7B -100.5(2) . . . . ?
B3B B4B B6B B7B 38.1(2) . . . . ?
C14B B4B B6B B10B 63.5(3) . . . . ?
C15B B4B B6B B10B 0.3(3) . . . . ?
B5B B4B B6B B10B -37.4(2) . . . . ?
B3B B4B B6B B10B 101.2(3) . . . . ?
C14B B4B B6B B5B 100.9(2) . . . . ?
C15B B4B B6B B5B 37.7(2) . . . . ?
B3B B4B B6B B5B 138.6(2) . . . . ?
C14B B3B B6B B4B 38.3(2) . . . . ?
B2B B3B B6B B4B 99.8(2) . . . . ?
B7B B3B B6B B4B 137.4(2) . . . . ?
C14B B3B B6B B7B -99.2(2) . . . . ?
B2B B3B B6B B7B -37.6(2) . . . . ?
B4B B3B B6B B7B -137.4(2) . . . . ?
C14B B3B B6B B10B -62.3(3) . . . . ?
B2B B3B B6B B10B -0.7(3) . . . . ?
B4B B3B B6B B10B -100.5(2) . . . . ?
B7B B3B B6B B10B 36.9(2) . . . . ?
C14B B3B B6B B5B 1.2(3) . . . . ?
B2B B3B B6B B5B 62.7(3) . . . . ?
B4B B3B B6B B5B -37.1(2) . . . . ?
B7B B3B B6B B5B 100.3(3) . . . . ?
C15B B5B B6B B4B -38.2(2) . . . . ?
B9B B5B B6B B4B -100.2(2) . . . . ?
B10B B5B B6B B4B -138.0(2) . . . . ?
C15B B5B B6B B3B -0.9(3) . . . . ?
B9B B5B B6B B3B -63.0(3) . . . . ?
B4B B5B B6B B3B 37.3(2) . . . . ?
B10B B5B B6B B3B -100.8(3) . . . . ?
C15B B5B B6B B7B 62.7(3) . . . . ?
B9B B5B B6B B7B 0.7(3) . . . . ?
B4B B5B B6B B7B 100.9(2) . . . . ?
B10B B5B B6B B7B -37.1(2) . . . . ?
C15B B5B B6B B10B 99.8(2) . . . . ?
B9B B5B B6B B10B 37.8(2) . . . . ?
B4B B5B B6B B10B 138.0(2) . . . . ?
B4B B6B B7B B10B 100.5(2) . . . . ?
B3B B6B B7B B10B 138.7(2) . . . . ?
B5B B6B B7B B10B 37.2(2) . . . . ?
B4B B6B B7B B8B 62.1(3) . . . . ?
B3B B6B B7B B8B 100.3(2) . . . . ?
B10B B6B B7B B8B -38.4(2) . . . . ?
B5B B6B B7B B8B -1.1(3) . . . . ?
B4B B6B B7B B3B -38.2(2) . . . . ?
B10B B6B B7B B3B -138.7(2) . . . . ?
B5B B6B B7B B3B -101.4(2) . . . . ?
B4B B6B B7B B2B -1.0(3) . . . . ?
B3B B6B B7B B2B 37.2(2) . . . . ?
B10B B6B B7B B2B -101.4(2) . . . . ?
B5B B6B B7B B2B -64.2(3) . . . . ?
C14B B3B B7B B10B 62.9(3) . . . . ?
B6B B3B B7B B10B -37.1(2) . . . . ?
B2B B3B B7B B10B 101.1(3) . . . . ?
B4B B3B B7B B10B 0.7(3) . . . . ?
C14B B3B B7B B8B -0.8(3) . . . . ?
B6B B3B B7B B8B -100.8(2) . . . . ?
B2B B3B B7B B8B 37.4(2) . . . . ?
B4B B3B B7B B8B -62.9(3) . . . . ?
C14B B3B B7B B6B 100.0(2) . . . . ?
B2B B3B B7B B6B 138.2(2) . . . . ?
B4B B3B B7B B6B 37.9(2) . . . . ?
C14B B3B B7B B2B -38.2(2) . . . . ?
B6B B3B B7B B2B -138.2(2) . . . . ?
B4B B3B B7B B2B -100.3(2) . . . . ?
C14B B2B B7B B10B -62.6(3) . . . . ?
B8B B2B B7B B10B 37.1(2) . . . . ?
B3B B2B B7B B10B -100.8(3) . . . . ?
B1B B2B B7B B10B -0.3(3) . . . . ?
C14B B2B B7B B8B -99.7(2) . . . . ?
B3B B2B B7B B8B -137.9(2) . . . . ?
B1B B2B B7B B8B -37.5(2) . . . . ?
C14B B2B B7B B6B 1.1(3) . . . . ?
B8B B2B B7B B6B 100.8(2) . . . . ?
B3B B2B B7B B6B -37.1(2) . . . . ?
B1B B2B B7B B6B 63.3(3) . . . . ?
C14B B2B B7B B3B 38.2(2) . . . . ?
B8B B2B B7B B3B 137.9(2) . . . . ?
B1B B2B B7B B3B 100.4(3) . . . . ?
C15B B1B B8B B9B -38.0(2) . . . . ?
C14B B1B B8B B9B -101.2(2) . . . . ?
B2B B1B B8B B9B -138.9(2) . . . . ?
C15B B1B B8B B2B 100.9(2) . . . . ?
C14B B1B B8B B2B 37.8(2) . . . . ?
B9B B1B B8B B2B 138.9(2) . . . . ?
C15B B1B B8B B7B 62.9(3) . . . . ?
C14B B1B B8B B7B -0.3(3) . . . . ?
B9B B1B B8B B7B 100.9(3) . . . . ?
B2B B1B B8B B7B -38.0(2) . . . . ?
C15B B1B B8B B10B -0.3(3) . . . . ?
C14B B1B B8B B10B -63.5(3) . . . . ?
B9B B1B B8B B10B 37.7(2) . . . . ?
B2B B1B B8B B10B -101.2(3) . . . . ?
C14B B2B B8B B1B -38.6(2) . . . . ?
B3B B2B B8B B1B -100.2(2) . . . . ?
B7B B2B B8B B1B -137.7(3) . . . . ?
C14B B2B B8B B9B -1.7(3) . . . . ?
B3B B2B B8B B9B -63.3(3) . . . . ?
B1B B2B B8B B9B 36.9(2) . . . . ?
B7B B2B B8B B9B -100.8(3) . . . . ?
C14B B2B B8B B7B 99.1(3) . . . . ?
B3B B2B B8B B7B 37.5(2) . . . . ?
B1B B2B B8B B7B 137.7(3) . . . . ?
C14B B2B B8B B10B 62.2(3) . . . . ?
B3B B2B B8B B10B 0.6(3) . . . . ?
B1B B2B B8B B10B 100.8(3) . . . . ?
B7B B2B B8B B10B -36.9(2) . . . . ?
B10B B7B B8B B1B -100.6(3) . . . . ?
B6B B7B B8B B1B -62.3(3) . . . . ?
B3B B7B B8B B1B 0.7(3) . . . . ?
B2B B7B B8B B1B 38.1(2) . . . . ?
B10B B7B B8B B9B -37.2(2) . . . . ?
B6B B7B B8B B9B 1.2(3) . . . . ?
B3B B7B B8B B9B 64.1(3) . . . . ?
B2B B7B B8B B9B 101.5(3) . . . . ?
B10B B7B B8B B2B -138.7(3) . . . . ?
B6B B7B B8B B2B -100.4(3) . . . . ?
B3B B7B B8B B2B -37.4(2) . . . . ?
B6B B7B B8B B10B 38.3(2) . . . . ?
B3B B7B B8B B10B 101.3(3) . . . . ?
B2B B7B B8B B10B 138.7(3) . . . . ?
B4B B5B B9B C15B 35.8(2) . . . . ?
B10B B5B B9B C15B 136.2(2) . . . . ?
B6B B5B B9B C15B 98.6(2) . . . . ?
C15B B5B B9B B1B -35.1(2) . . . . ?
B4B B5B B9B B1B 0.6(3) . . . . ?
B10B B5B B9B B1B 101.1(2) . . . . ?
B6B B5B B9B B1B 63.5(3) . . . . ?
C15B B5B B9B B8B -98.5(2) . . . . ?
B4B B5B B9B B8B -62.8(3) . . . . ?
B10B B5B B9B B8B 37.6(2) . . . . ?
B6B B5B B9B B8B 0.1(3) . . . . ?
C15B B5B B9B B10B -136.2(2) . . . . ?
B4B B5B B9B B10B -100.4(2) . . . . ?
B6B B5B B9B B10B -37.6(2) . . . . ?
C14B B1B B9B C15B -38.23(19) . . . . ?
B8B B1B B9B C15B -136.3(2) . . . . ?
B2B B1B B9B C15B -99.4(2) . . . . ?
C15B B1B B9B B5B 35.0(2) . . . . ?
C14B B1B B9B B5B -3.3(3) . . . . ?
B8B B1B B9B B5B -101.3(2) . . . . ?
B2B B1B B9B B5B -64.4(3) . . . . ?
C15B B1B B9B B8B 136.3(2) . . . . ?
C14B B1B B9B B8B 98.0(2) . . . . ?
B2B B1B B9B B8B 36.9(2) . . . . ?
C15B B1B B9B B10B 98.6(2) . . . . ?
C14B B1B B9B B10B 60.4(3) . . . . ?
B8B B1B B9B B10B -37.6(2) . . . . ?
B2B B1B B9B B10B -0.8(3) . . . . ?
B1B B8B B9B C15B 38.3(2) . . . . ?
B2B B8B B9B C15B 1.2(3) . . . . ?
B7B B8B B9B C15B -62.7(3) . . . . ?
B10B B8B B9B C15B -99.7(2) . . . . ?
B1B B8B B9B B5B 100.3(2) . . . . ?
B2B B8B B9B B5B 63.2(3) . . . . ?
B7B B8B B9B B5B -0.7(3) . . . . ?
B10B B8B B9B B5B -37.7(2) . . . . ?
B2B B8B B9B B1B -37.1(2) . . . . ?
B7B B8B B9B B1B -101.0(3) . . . . ?
B10B B8B B9B B1B -138.0(2) . . . . ?
B1B B8B B9B B10B 138.0(2) . . . . ?
B2B B8B B9B B10B 100.9(3) . . . . ?
B7B B8B B9B B10B 36.9(2) . . . . ?
B8B B7B B10B B6B 137.1(2) . . . . ?
B3B B7B B10B B6B 36.9(2) . . . . ?
B2B B7B B10B B6B 100.2(3) . . . . ?
B6B B7B B10B B8B -137.1(2) . . . . ?
B3B B7B B10B B8B -100.3(3) . . . . ?
B2B B7B B10B B8B -36.9(2) . . . . ?
B8B B7B B10B B5B 99.6(3) . . . . ?
B6B B7B B10B B5B -37.5(2) . . . . ?
B3B B7B B10B B5B -0.6(3) . . . . ?
B2B B7B B10B B5B 62.7(3) . . . . ?
B8B B7B B10B B9B 36.8(2) . . . . ?
B6B B7B B10B B9B -100.3(3) . . . . ?
B3B B7B B10B B9B -63.5(3) . . . . ?
B2B B7B B10B B9B -0.1(3) . . . . ?
B4B B6B B10B B7B -100.8(3) . . . . ?
B3B B6B B10B B7B -37.1(2) . . . . ?
B5B B6B B10B B7B -138.2(2) . . . . ?
B4B B6B B10B B8B -62.7(3) . . . . ?
B3B B6B B10B B8B 1.1(3) . . . . ?
B7B B6B B10B B8B 38.2(2) . . . . ?
B5B B6B B10B B8B -100.1(2) . . . . ?
B4B B6B B10B B5B 37.4(2) . . . . ?
B3B B6B B10B B5B 101.1(2) . . . . ?
B7B B6B B10B B5B 138.2(2) . . . . ?
B4B B6B B10B B9B 0.1(3) . . . . ?
B3B B6B B10B B9B 63.9(3) . . . . ?
B7B B6B B10B B9B 101.0(3) . . . . ?
B5B B6B B10B B9B -37.3(2) . . . . ?
B1B B8B B10B B7B 101.1(3) . . . . ?
B9B B8B B10B B7B 138.6(3) . . . . ?
B2B B8B B10B B7B 37.1(2) . . . . ?
B1B B8B B10B B6B 62.9(3) . . . . ?
B9B B8B B10B B6B 100.4(2) . . . . ?
B2B B8B B10B B6B -1.1(3) . . . . ?
B7B B8B B10B B6B -38.2(2) . . . . ?
B1B B8B B10B B5B -0.5(3) . . . . ?
B9B B8B B10B B5B 37.0(2) . . . . ?
B2B B8B B10B B5B -64.4(3) . . . . ?
B7B B8B B10B B5B -101.6(3) . . . . ?
B1B B8B B10B B9B -37.5(2) . . . . ?
B2B B8B B10B B9B -101.5(3) . . . . ?
B7B B8B B10B B9B -138.6(3) . . . . ?
C15B B5B B10B B7B -62.2(3) . . . . ?
B9B B5B B10B B7B -100.4(3) . . . . ?
B4B B5B B10B B7B 0.3(3) . . . . ?
B6B B5B B10B B7B 37.4(2) . . . . ?
C15B B5B B10B B6B -99.6(2) . . . . ?
B9B B5B B10B B6B -137.9(2) . . . . ?
B4B B5B B10B B6B -37.2(2) . . . . ?
C15B B5B B10B B8B 1.1(3) . . . . ?
B9B B5B B10B B8B -37.1(2) . . . . ?
B4B B5B B10B B8B 63.6(3) . . . . ?
B6B B5B B10B B8B 100.8(2) . . . . ?
C15B B5B B10B B9B 38.23(19) . . . . ?
B4B B5B B10B B9B 100.7(2) . . . . ?
B6B B5B B10B B9B 137.9(2) . . . . ?
C15B B9B B10B B7B 62.9(3) . . . . ?
B5B B9B B10B B7B 101.0(3) . . . . ?
B1B B9B B10B B7B 0.6(3) . . . . ?
B8B B9B B10B B7B -37.0(2) . . . . ?
C15B B9B B10B B6B -0.5(3) . . . . ?
B5B B9B B10B B6B 37.6(2) . . . . ?
B1B B9B B10B B6B -62.8(3) . . . . ?
B8B B9B B10B B6B -100.4(3) . . . . ?
C15B B9B B10B B8B 99.9(2) . . . . ?
B5B B9B B10B B8B 138.0(2) . . . . ?
B1B B9B B10B B8B 37.6(2) . . . . ?
C15B B9B B10B B5B -38.2(2) . . . . ?
B1B B9B B10B B5B -100.5(2) . . . . ?
B8B B9B B10B B5B -138.0(2) . . . . ?
C10B C1B C2B C3B -5(3) . . . . ?
C10B C1B C2B C14B 179.6(17) . . . . ?
C1B C2B C3B C4B 5(2) . . . . ?
C14B C2B C3B C4B -179.2(15) . . . . ?
C2B C3B C4B C11B -1(2) . . . . ?
C12B C5B C6B C7B 0.0 . . . . ?
C5B C6B C7B C8B 0.0 . . . . ?
C6B C7B C8B C13B 0.0 . . . . ?
C7B C8B C13B C12B 0.0 . . . . ?
C7B C8B C13B C9B -179.4(12) . . . . ?
C8B C13B C12B C5B 0.0 . . . . ?
C9B C13B C12B C5B 179.5(10) . . . . ?
C8B C13B C12B C11B -179.7(9) . . . . ?
C9B C13B C12B C11B -0.2(12) . . . . ?
C6B C5B C12B C13B 0.0 . . . . ?
C6B C5B C12B C11B 179.6(11) . . . . ?
C12B C13B C9B C16B 122.8(10) . . . . ?
C8B C13B C9B C16B -57.8(17) . . . . ?
C12B C13B C9B C10B 2.8(14) . . . . ?
C8B C13B C9B C10B -177.8(9) . . . . ?
C12B C13B C9B C17B -106.9(13) . . . . ?
C8B C13B C9B C17B 72.5(16) . . . . ?
C2B C1B C10B C11B 0(3) . . . . ?
C2B C1B C10B C9B 179.8(18) . . . . ?
C13B C9B C10B C1B 176.0(17) . . . . ?
C16B C9B C10B C1B 54(2) . . . . ?
C17B C9B C10B C1B -70(2) . . . . ?
C13B C9B C10B C11B -4.5(17) . . . . ?
C16B C9B C10B C11B -126.7(15) . . . . ?
C17B C9B C10B C11B 109.9(17) . . . . ?
C3B C4B C11B C10B -4(2) . . . . ?
C3B C4B C11B C12B 176.0(14) . . . . ?
C1B C10B C11B C4B 4(2) . . . . ?
C9B C10B C11B C4B -175.2(14) . . . . ?
C1B C10B C11B C12B -175.8(15) . . . . ?
C9B C10B C11B C12B 4.7(17) . . . . ?
C13B C12B C11B C4B 177.0(14) . . . . ?
C5B C12B C11B C4B -3(2) . . . . ?
C13B C12B C11B C10B -2.8(13) . . . . ?
C5B C12B C11B C10B 177.5(10) . . . . ?
C23B C18B C19B C20B 0.0 . . . . ?
Si1B C18B C19B C20B 175.2(10) . . . . ?
C18B C19B C20B C21B 0.0 . . . . ?
C19B C20B C21B C22B 0.0 . . . . ?
C20B C21B C22B C23B 0.0 . . . . ?
C21B C22B C23B C18B 0.0 . . . . ?
C19B C18B C23B C22B 0.0 . . . . ?
Si1B C18B C23B C22B -175.2(10) . . . . ?
C19B C18B Si1B C24B -4.7(8) . . . . ?
C23B C18B Si1B C24B 170.5(5) . . . . ?
C19B C18B Si1B C30B -123.2(6) . . . . ?
C23B C18B Si1B C30B 52.0(7) . . . . ?
C19B C18B Si1B C15B 118.7(6) . . . . ?
C23B C18B Si1B C15B -66.1(7) . . . . ?
C1B C2B C14B B2B 115.1(16) . . . . ?
C3B C2B C14B B2B -60.2(18) . . . . ?
C1B C2B C14B B3B 41(2) . . . . ?
C3B C2B C14B B3B -134.3(13) . . . . ?
C1B C2B C14B B4B -29(2) . . . . ?
C3B C2B C14B B4B 155.8(13) . . . . ?
C1B C2B C14B B1B -167.7(14) . . . . ?
C3B C2B C14B B1B 17(2) . . . . ?
C1B C2B C14B C15B -96.6(18) . . . . ?
C3B C2B C14B C15B 88.1(16) . . . . ?
B8B B2B C14B C2B 152.5(8) . . . . ?
B3B B2B C14B C2B -106.2(8) . . . . ?
B1B B2B C14B C2B 113.8(8) . . . . ?
B7B B2B C14B C2B -145.0(8) . . . . ?
B8B B2B C14B C2C 141.6(11) . . . . ?
B3B B2B C14B C2C -117.1(11) . . . . ?
B1B B2B C14B C2C 102.9(11) . . . . ?
B7B B2B C14B C2C -155.9(11) . . . . ?
B8B B2B C14B B3B -101.3(2) . . . . ?
B1B B2B C14B B3B -140.0(2) . . . . ?
B7B B2B C14B B3B -38.8(2) . . . . ?
B8B B2B C14B B4B -63.4(3) . . . . ?
B3B B2B C14B B4B 37.9(2) . . . . ?
B1B B2B C14B B4B -102.1(2) . . . . ?
B7B B2B C14B B4B -0.9(3) . . . . ?
B8B B2B C14B B1B 38.7(2) . . . . ?
B3B B2B C14B B1B 140.0(2) . . . . ?
B7B B2B C14B B1B 101.2(2) . . . . ?
B8B B2B C14B C15B 1.6(3) . . . . ?
B3B B2B C14B C15B 102.9(2) . . . . ?
B1B B2B C14B C15B -37.1(2) . . . . ?
B7B B2B C14B C15B 64.1(3) . . . . ?
B6B B3B C14B C2B -142.4(8) . . . . ?
B2B B3B C14B C2B 115.7(8) . . . . ?
B4B B3B C14B C2B -103.9(8) . . . . ?
B7B B3B C14B C2B 154.7(8) . . . . ?
B6B B3B C14B C2C -154.6(12) . . . . ?
B2B B3B C14B C2C 103.5(12) . . . . ?
B4B B3B C14B C2C -116.1(12) . . . . ?
B7B B3B C14B C2C 142.5(12) . . . . ?
B6B B3B C14B B2B 101.9(3) . . . . ?
B4B B3B C14B B2B 140.4(2) . . . . ?
B7B B3B C14B B2B 39.0(2) . . . . ?
B6B B3B C14B B4B -38.5(2) . . . . ?
B2B B3B C14B B4B -140.4(2) . . . . ?
B7B B3B C14B B4B -101.4(2) . . . . ?
B6B B3B C14B B1B 63.5(3) . . . . ?
B2B B3B C14B B1B -38.4(2) . . . . ?
B4B B3B C14B B1B 102.0(2) . . . . ?
B7B B3B C14B B1B 0.6(3) . . . . ?
B6B B3B C14B C15B -1.0(3) . . . . ?
B2B B3B C14B C15B -102.9(2) . . . . ?
B4B B3B C14B C15B 37.5(2) . . . . ?
B7B B3B C14B C15B -63.9(3) . . . . ?
C15B B4B C14B C2B -111.7(9) . . . . ?
B6B B4B C14B C2B 148.0(9) . . . . ?
B5B B4B C14B C2B -148.6(9) . . . . ?
B3B B4B C14B C2B 109.7(9) . . . . ?
C15B B4B C14B C2C -107.5(15) . . . . ?
B6B B4B C14B C2C 152.3(15) . . . . ?
B5B B4B C14B C2C -144.3(15) . . . . ?
B3B B4B C14B C2C 113.9(15) . . . . ?
C15B B4B C14B B2B 100.5(2) . . . . ?
B6B B4B C14B B2B 0.3(3) . . . . ?
B5B B4B C14B B2B 63.7(3) . . . . ?
B3B B4B C14B B2B -38.1(2) . . . . ?
C15B B4B C14B B3B 138.6(2) . . . . ?
B6B B4B C14B B3B 38.4(2) . . . . ?
B5B B4B C14B B3B 101.8(2) . . . . ?
C15B B4B C14B B1B 32.5(2) . . . . ?
B6B B4B C14B B1B -67.8(3) . . . . ?
B5B B4B C14B B1B -4.4(3) . . . . ?
B3B B4B C14B B1B -106.2(2) . . . . ?
B6B B4B C14B C15B -100.3(2) . . . . ?
B5B B4B C14B C15B -36.88(19) . . . . ?
B3B B4B C14B C15B -138.6(2) . . . . ?
C15B B1B C14B C2B 107.3(10) . . . . ?
B9B B1B C14B C2B 144.8(10) . . . . ?
B8B B1B C14B C2B -152.4(10) . . . . ?
B2B B1B C14B C2B -113.8(10) . . . . ?
C15B B1B C14B C2C 113.0(13) . . . . ?
B9B B1B C14B C2C 150.5(13) . . . . ?
B8B B1B C14B C2C -146.8(13) . . . . ?
B2B B1B C14B C2C -108.1(13) . . . . ?
C15B B1B C14B B2B -138.9(2) . . . . ?
B9B B1B C14B B2B -101.5(2) . . . . ?
B8B B1B C14B B2B -38.7(2) . . . . ?
C15B B1B C14B B3B -100.4(2) . . . . ?
B9B B1B C14B B3B -63.0(3) . . . . ?
B8B B1B C14B B3B -0.2(3) . . . . ?
B2B B1B C14B B3B 38.5(2) . . . . ?
C15B B1B C14B B4B -32.6(2) . . . . ?
B9B B1B C14B B4B 4.8(3) . . . . ?
B8B B1B C14B B4B 67.6(3) . . . . ?
B2B B1B C14B B4B 106.3(2) . . . . ?
B9B B1B C14B C15B 37.45(19) . . . . ?
B8B B1B C14B C15B 100.2(2) . . . . ?
B2B B1B C14B C15B 138.9(2) . . . . ?
B4B B5B C15B B9B -139.7(2) . . . . ?
B10B B5B C15B B9B -38.8(2) . . . . ?
B6B B5B C15B B9B -101.5(2) . . . . ?
B9B B5B C15B B1B 37.4(2) . . . . ?
B4B B5B C15B B1B -102.3(2) . . . . ?
B10B B5B C15B B1B -1.4(3) . . . . ?
B6B B5B C15B B1B -64.1(3) . . . . ?
B9B B5B C15B B4B 139.7(2) . . . . ?
B10B B5B C15B B4B 100.9(2) . . . . ?
B6B B5B C15B B4B 38.2(2) . . . . ?
B9B B5B C15B C14B 101.8(2) . . . . ?
B4B B5B C15B C14B -37.9(2) . . . . ?
B10B B5B C15B C14B 63.0(3) . . . . ?
B6B B5B C15B C14B 0.3(3) . . . . ?
B9B B5B C15B Si1B -111.6(2) . . . . ?
B4B B5B C15B Si1B 108.7(2) . . . . ?
B10B B5B C15B Si1B -150.42(18) . . . . ?
B6B B5B C15B Si1B 146.9(2) . . . . ?
B1B B9B C15B B5B 140.4(2) . . . . ?
B8B B9B C15B B5B 101.8(2) . . . . ?
B10B B9B C15B B5B 38.8(2) . . . . ?
B5B B9B C15B B1B -140.4(2) . . . . ?
B8B B9B C15B B1B -38.6(2) . . . . ?
B10B B9B C15B B1B -101.6(2) . . . . ?
B5B B9B C15B B4B -38.0(2) . . . . ?
B1B B9B C15B B4B 102.4(2) . . . . ?
B8B B9B C15B B4B 63.7(3) . . . . ?
B10B B9B C15B B4B 0.8(3) . . . . ?
B5B B9B C15B C14B -102.0(2) . . . . ?
B1B B9B C15B C14B 38.43(19) . . . . ?
B8B B9B C15B C14B -0.2(3) . . . . ?
B10B B9B C15B C14B -63.2(3) . . . . ?
B5B B9B C15B Si1B 109.0(2) . . . . ?
B1B B9B C15B Si1B -110.6(2) . . . . ?
B8B B9B C15B Si1B -149.26(19) . . . . ?
B10B B9B C15B Si1B 147.77(19) . . . . ?
C14B B1B C15B B5B 99.7(2) . . . . ?
B9B B1B C15B B5B -37.5(2) . . . . ?
B8B B1B C15B B5B 1.1(3) . . . . ?
B2B B1B C15B B5B 64.0(3) . . . . ?
C14B B1B C15B B9B 137.2(2) . . . . ?
B8B B1B C15B B9B 38.6(2) . . . . ?
B2B B1B C15B B9B 101.5(2) . . . . ?
C14B B1B C15B B4B 32.5(2) . . . . ?
B9B B1B C15B B4B -104.7(2) . . . . ?
B8B B1B C15B B4B -66.1(3) . . . . ?
B2B B1B C15B B4B -3.2(3) . . . . ?
B9B B1B C15B C14B -137.2(2) . . . . ?
B8B B1B C15B C14B -98.6(2) . . . . ?
B2B B1B C15B C14B -35.70(19) . . . . ?
C14B B1B C15B Si1B -111.8(2) . . . . ?
B9B B1B C15B Si1B 111.0(2) . . . . ?
B8B B1B C15B Si1B 149.61(18) . . . . ?
B2B B1B C15B Si1B -147.50(19) . . . . ?
C14B B4B C15B B5B -137.6(2) . . . . ?
B6B B4B C15B B5B -38.7(2) . . . . ?
B3B B4B C15B B5B -101.5(2) . . . . ?
C14B B4B C15B B9B -99.6(2) . . . . ?
B6B B4B C15B B9B -0.7(3) . . . . ?
B5B B4B C15B B9B 38.0(2) . . . . ?
B3B B4B C15B B9B -63.5(3) . . . . ?
C14B B4B C15B B1B -32.6(2) . . . . ?
B6B B4B C15B B1B 66.3(3) . . . . ?
B5B B4B C15B B1B 105.0(2) . . . . ?
B3B B4B C15B B1B 3.5(3) . . . . ?
B6B B4B C15B C14B 98.9(2) . . . . ?
B5B B4B C15B C14B 137.6(2) . . . . ?
B3B B4B C15B C14B 36.10(19) . . . . ?
C14B B4B C15B Si1B 112.5(2) . . . . ?
B6B B4B C15B Si1B -148.55(19) . . . . ?
B5B B4B C15B Si1B -109.8(2) . . . . ?
B3B B4B C15B Si1B 148.62(18) . . . . ?
C2B C14B C15B B5B 140.9(6) . . . . ?
C2C C14B C15B B5B 155.3(9) . . . . ?
B2B C14B C15B B5B -67.0(3) . . . . ?
B3B C14B C15B B5B 0.4(3) . . . . ?
B4B C14B C15B B5B 39.0(2) . . . . ?
B1B C14B C15B B5B -105.4(2) . . . . ?
C2B C14B C15B B9B -153.1(6) . . . . ?
C2C C14B C15B B9B -138.7(9) . . . . ?
B2B C14B C15B B9B -0.9(3) . . . . ?
B3B C14B C15B B9B 66.5(3) . . . . ?
B4B C14B C15B B9B 105.0(2) . . . . ?
B1B C14B C15B B9B -39.3(2) . . . . ?
C2B C14B C15B B1B -113.8(6) . . . . ?
C2C C14B C15B B1B -99.4(9) . . . . ?
B2B C14B C15B B1B 38.4(2) . . . . ?
B3B C14B C15B B1B 105.8(2) . . . . ?
B4B C14B C15B B1B 144.4(2) . . . . ?
C2B C14B C15B B4B 101.9(6) . . . . ?
C2C C14B C15B B4B 116.3(10) . . . . ?
B2B C14B C15B B4B -105.9(2) . . . . ?
B3B C14B C15B B4B -38.6(2) . . . . ?
B1B C14B C15B B4B -144.4(2) . . . . ?
C2B C14B C15B Si1B -4.5(7) . . . . ?
C2C C14B C15B Si1B 9.9(10) . . . . ?
B2B C14B C15B Si1B 147.66(19) . . . . ?
B3B C14B C15B Si1B -145.0(2) . . . . ?
B4B C14B C15B Si1B -106.4(2) . . . . ?
B1B C14B C15B Si1B 109.2(2) . . . . ?
C18B Si1B C24B C29B 55.2(6) . . . . ?
C30B Si1B C24B C29B 172.0(2) . . . . ?
C18C Si1B C24B C29B 53.9(7) . . . . ?
C15B Si1B C24B C29B -69.6(3) . . . . ?
C18B Si1B C24B C25B -123.6(6) . . . . ?
C30B Si1B C24B C25B -6.9(3) . . . . ?
C18C Si1B C24B C25B -124.9(6) . . . . ?
C15B Si1B C24B C25B 111.5(2) . . . . ?
C29B C24B C25B C26B 0.1(4) . . . . ?
Si1B C24B C25B C26B 179.0(2) . . . . ?
C24B C25B C26B C27B 0.2(5) . . . . ?
C25B C26B C27B C28B -0.5(5) . . . . ?
C26B C27B C28B C29B 0.5(5) . . . . ?
C27B C28B C29B C24B -0.2(5) . . . . ?
C25B C24B C29B C28B -0.2(4) . . . . ?
Si1B C24B C29B C28B -179.0(2) . . . . ?
C18B Si1B C30B C31B -166.6(5) . . . . ?
C24B Si1B C30B C31B 70.1(3) . . . . ?
C18C Si1B C30B C31B -173.8(6) . . . . ?
C15B Si1B C30B C31B -47.5(3) . . . . ?
C18B Si1B C30B C35B 20.8(5) . . . . ?
C24B Si1B C30B C35B -102.5(2) . . . . ?
C18C Si1B C30B C35B 13.6(6) . . . . ?
C15B Si1B C30B C35B 139.8(2) . . . . ?
C35B C30B C31B C32B -0.6(4) . . . . ?
Si1B C30B C31B C32B -173.3(2) . . . . ?
C30B C31B C32B C33B -0.3(5) . . . . ?
C31B C32B C33B C34B 0.9(5) . . . . ?
C32B C33B C34B C35B -0.6(5) . . . . ?
C33B C34B C35B C30B -0.4(5) . . . . ?
C31B C30B C35B C34B 1.0(5) . . . . ?
Si1B C30B C35B C34B 174.2(3) . . . . ?
C10C C1C C2C C3C -3(4) . . . . ?
C10C C1C C2C C14B 177(2) . . . . ?
B2B C14B C2C C3C -57(3) . . . . ?
B3B C14B C2C C3C -130(2) . . . . ?
B4B C14B C2C C3C 152(2) . . . . ?
B1B C14B C2C C3C 13(3) . . . . ?
C15B C14B C2C C3C 79(3) . . . . ?
B2B C14B C2C C1C 123.4(19) . . . . ?
B3B C14B C2C C1C 50(3) . . . . ?
B4B C14B C2C C1C -28(3) . . . . ?
B1B C14B C2C C1C -167.5(18) . . . . ?
C15B C14B C2C C1C -101(2) . . . . ?
C1C C2C C3C C4C 4(4) . . . . ?
C14B C2C C3C C4C -176(2) . . . . ?
C2C C3C C4C C11C -1(3) . . . . ?
C12C C5C C6C C7C 0.0 . . . . ?
C5C C6C C7C C8C 0.0 . . . . ?
C6C C7C C8C C13C 0.0 . . . . ?
C7C C8C C13C C12C 0.0 . . . . ?
C7C C8C C13C C9C -179.8(17) . . . . ?
C8C C13C C12C C5C 0.0 . . . . ?
C9C C13C C12C C5C 179.8(14) . . . . ?
C8C C13C C12C C11C 178.4(12) . . . . ?
C9C C13C C12C C11C -1.8(15) . . . . ?
C6C C5C C12C C13C 0.0 . . . . ?
C6C C5C C12C C11C -178.1(15) . . . . ?
C12C C13C C9C C10C 3.8(18) . . . . ?
C8C C13C C9C C10C -176.4(13) . . . . ?
C12C C13C C9C C15C -122.2(19) . . . . ?
C8C C13C C9C C15C 58(2) . . . . ?
C12C C13C C9C C14C 121.1(14) . . . . ?
C8C C13C C9C C14C -59(2) . . . . ?
C2C C1C C10C C11C 0(4) . . . . ?
C2C C1C C10C C9C 179(3) . . . . ?
C13C C9C C10C C11C -5(2) . . . . ?
C15C C9C C10C C11C 115(3) . . . . ?
C14C C9C C10C C11C -120(2) . . . . ?
C13C C9C C10C C1C 177(2) . . . . ?
C15C C9C C10C C1C -63(3) . . . . ?
C14C C9C C10C C1C 62(3) . . . . ?
C1C C10C C11C C4C 2(3) . . . . ?
C9C C10C C11C C4C -177(2) . . . . ?
C1C C10C C11C C12C -177(2) . . . . ?
C9C C10C C11C C12C 4(2) . . . . ?
C3C C4C C11C C10C -1(3) . . . . ?
C3C C4C C11C C12C 177(2) . . . . ?
C13C C12C C11C C10C -1.4(18) . . . . ?
C5C C12C C11C C10C 176.8(15) . . . . ?
C13C C12C C11C C4C 179.6(18) . . . . ?
C5C C12C C11C C4C -2(3) . . . . ?
C23C C18C C19C C20C 0.0 . . . . ?
Si1B C18C C19C C20C 177.2(13) . . . . ?
C18C C19C C20C C21C 0.0 . . . . ?
C19C C20C C21C C22C 0.0 . . . . ?
C20C C21C C22C C23C 0.0 . . . . ?
C21C C22C C23C C18C 0.0 . . . . ?
C19C C18C C23C C22C 0.0 . . . . ?
Si1B C18C C23C C22C -177.4(12) . . . . ?
