#------------------------------------------------------------------------------
#$Date: 2018-06-14 06:45:12 +0300 (Thu, 14 Jun 2018) $
#$Revision: 208362 $
#$URL: file:///home/coder/svn-repositories/cod/cif/8/10/12/8101230.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8101230
loop_
_publ_author_name
'Klepp, O. Kurt'
'Zeitlinger, Martin'
_publ_section_title
;
Crystal structure of tetracesium decasulfidotetragermanate, Cs₄Ge₄S₁₀
;
_journal_issue                   1
_journal_name_full
'Zeitschrift für Kristallographie - New Crystal Structures'
_journal_page_first              7
_journal_page_last               8
_journal_volume                  215
_journal_year                    2000
_chemical_formula_sum            'Cs4 Ge4 S10'
_chemical_formula_weight         1142.62
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 106.74(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   15.714(3)
_cell_length_b                   15.858(2)
_cell_length_c                   9.491(2)
_cell_measurement_temperature    294
_cell_volume                     2265(1)
_diffrn_ambient_temperature      294
_exptl_crystal_density_diffrn    3.35
_refine_ls_R_factor_obs          0.027
_refine_ls_wR_factor_obs         0.025
_cod_depositor_comments
;
 Updating space group information and adding the symmetry operation list.

 Antanas Vaitkus,
 2018-06-14
;
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               8101230
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x,y,-z+1/2
3 -x,-y,-z
4 x,-y,z+1/2
5 x+1/2,y+1/2,z
6 -x+1/2,y+1/2,-z+1/2
7 -x+1/2,-y+1/2,-z
8 x+1/2,-y+1/2,z+1/2
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_Wyckoff_symbol
Cs1 0.15335(3) 0.36379(3) 0.87171(5) 0.0347(1) Uani ? 1 8 f
Cs2 0.13530(3) 0.07036(3) 0.64501(5) 0.0348(1) Uani ? 1 8 f
Ge1 0.10476(4) 0.36854(4) 0.39799(7) 0.0224(2) Uani ? 1 8 f
Ge2 0.43581(4) 0.29524(4) 0.87865(7) 0.0208(2) Uani ? 1 8 f
S1 0.1694(1) 0.2855(1) 0.2654(2) 0.0281(4) Uani ? 1 8 f
S2 0.4580(1) 0.2169(1) 0.4718(2) 0.0272(4) Uani ? 1 8 f
S3 0.2030(1) 0.4424(1) 0.5452(2) 0.0300(4) Uani ? 1 8 f
S4 0.1157(1) 0.1304(1) 0.9794(2) 0.0307(4) Uani ? 1 8 f
S5 0.0000 0.1197(1) 0.2500 0.0256(6) Uani ? 1 4 e
S6 0.0000 0.4495(2) 0.2500 0.0346(7) Uani ? 1 4 e
