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#$Date: 2024-05-02 13:48:35 +0300 (Thu, 02 May 2024) $
#$Revision: 291455 $
#$URL: file:///home/coder/svn-repositories/cod/cif/9/00/80/9008075.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the American Mineralogist Crystal Structure Database,
# http://rruff.geo.arizona.edu/AMS/amcsd.php
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_9008075
loop_
_publ_author_name
'Euler, R.'
'Hellner, E.'
_publ_section_title
;
 Uber komplex zusammengesetzte sulfidische erze VI.
 Zur kristallstruktur des meneghinits, CuPb13Sb7S24
;
_journal_name_full               'Zeitschrift fur Kristallographie'
_journal_page_first              345
_journal_page_last               372
_journal_volume                  113
_journal_year                    1960
_chemical_formula_sum            'Cu0.25 Pb3.25 S6 Sb1.75'
_chemical_name_mineral           Meneghinite
_space_group_IT_number           62
_symmetry_space_group_name_Hall  '-P 2c 2ab'
_symmetry_space_group_name_H-M   'P b n m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   11.363
_cell_length_b                   24.057
_cell_length_c                   4.128
_cell_formula_units_Z            4
_cell_volume                     1128.429
_database_code_amcsd             0010585
_exptl_crystal_density_diffrn    6.444
_cod_original_formula_sum        'Cu.25 Pb3.25 Sb1.75 S6'
_cod_database_code               9008075
loop_
_space_group_symop_operation_xyz
x,y,z
x,y,1/2-z
-x,-y,1/2+z
1/2+x,1/2-y,1/2+z
1/2-x,1/2+y,1/2-z
1/2-x,1/2+y,z
1/2+x,1/2-y,-z
-x,-y,-z
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
Cu 0.24000 0.25600 0.25000 0.25000 ?
Pb1 0.15000 0.02600 0.25000 0.50000 0.01064
Sb1 0.15000 0.02600 0.25000 0.50000 0.01064
Pb2 0.34200 0.37400 0.75000 1.00000 0.00747
Pb3 0.03600 0.43600 0.25000 0.50000 0.00887
Sb3 0.03600 0.43600 0.25000 0.50000 0.00887
Pb4 0.01500 0.28400 0.75000 1.00000 0.01013
Pb5 0.22000 0.15100 0.75000 0.25000 0.00519
Sb5 0.22000 0.15100 0.75000 0.75000 0.00519
S1 0.47400 0.43700 0.25000 1.00000 0.00469
S2 0.40600 0.11000 0.25000 1.00000 0.00519
S3 0.08900 0.18300 0.25000 1.00000 0.00608
S4 0.33600 0.23700 0.75000 1.00000 0.00177
S5 0.16000 0.34800 0.25000 1.00000 0.00545
S6 0.21700 0.47900 0.75000 1.00000 0.00355
loop_
_cod_related_entry_id
_cod_related_entry_database
_cod_related_entry_code
1 AMCSD 0010585
