#------------------------------------------------------------------------------ #$Date: 2016-04-06 15:35:39 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181862 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/52/93/1529387.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1529387 _cell_angle_alpha 90.000 _cell_angle_beta 110.680 _cell_angle_gamma 90.000 _cell_length_a 3.5510 _cell_length_b 21.8340 _cell_length_c 9.0750 _exptl_crystal_F_000 316.00 _reflns_d_resolution_high 0.8199 _cod_data_source_file C3H8FN4O2.fcf _cod_data_source_block m #BEGIN Tags that were not found in dictionaries: _shelx_title ' MSS-5-NATZ in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 150.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10.40 1.65 0.08 o 2 0 0 242.51 324.90 1.84 o 3 0 0 22.66 26.33 0.63 o 4 0 0 56.51 49.03 0.63 o 1 1 0 464.24 406.68 3.78 o 2 1 0 196.11 221.65 1.51 o 3 1 0 184.94 199.78 1.82 o 4 1 0 38.67 30.56 0.47 o 0 2 0 31.75 13.68 0.16 o 1 2 0 602.74 411.77 3.93 o 2 2 0 181.25 265.78 1.67 o 3 2 0 0.34 1.17 0.08 o 4 2 0 1.59 2.11 0.08 o 1 3 0 1384.49 1179.64 7.10 o 2 3 0 61.01 53.09 0.79 o 3 3 0 75.19 80.24 1.18 o 4 3 0 23.65 30.20 0.47 o 0 4 0 5.59 10.34 0.16 o 1 4 0 1679.16 1526.15 8.49 o 2 4 0 156.96 192.48 1.43 o 3 4 0 117.27 120.02 1.42 o 4 4 0 30.78 31.40 0.47 o 1 5 0 9.87 8.30 0.23 o 2 5 0 0.98 0.31 0.08 o 3 5 0 170.40 179.91 1.74 o 0 6 0 875.09 537.19 4.22 o 1 6 0 901.42 740.87 6.16 o 2 6 0 39.87 31.24 0.63 o 3 6 0 7.09 7.83 0.23 o 1 7 0 531.80 483.02 5.15 o 2 7 0 7.33 8.77 0.31 o 3 7 0 48.58 45.85 0.86 o 0 8 0 1692.60 1245.54 7.88 o 1 8 0 116.20 107.59 0.87 o 2 8 0 260.40 246.07 1.76 o 3 8 0 56.43 53.81 0.94 o 1 9 0 362.79 344.74 1.62 o 2 9 0 17.13 18.33 0.55 o 3 9 0 26.69 25.16 0.63 o 0 10 0 43.81 65.41 0.63 o 1 10 0 2264.79 2190.37 13.65 o 2 10 0 14.08 11.43 0.39 o 3 10 0 8.11 7.28 0.23 o 1 11 0 100.87 83.62 0.87 o 2 11 0 29.77 30.73 0.71 o 3 11 0 45.17 47.65 0.86 o 0 12 0 113.60 132.00 1.11 o 1 12 0 95.86 83.23 0.95 o 2 12 0 33.20 39.68 0.78 o 3 12 0 31.39 30.03 0.63 o 1 13 0 308.06 291.34 1.85 o 2 13 0 111.85 118.72 1.42 o 3 13 0 247.60 257.65 1.84 o 0 14 0 1771.53 1601.78 12.90 o 1 14 0 55.20 78.42 1.02 o 2 14 0 179.58 190.11 1.82 o 3 14 0 4.57 4.46 0.16 o 1 15 0 108.36 111.25 1.26 o 2 15 0 11.39 14.17 0.47 o 3 15 0 22.39 20.22 0.47 o 0 16 0 601.85 596.11 2.87 o 1 16 0 242.24 219.22 1.83 o 2 16 0 43.63 52.19 0.94 o 3 16 0 12.53 12.77 0.39 o 1 17 0 72.30 66.70 1.02 o 2 17 0 30.34 35.52 0.78 o 3 17 0 87.01 87.37 0.87 o 0 18 0 30.15 25.87 0.63 o 1 18 0 6.79 5.79 0.23 o 2 18 0 6.85 6.97 0.23 o 1 19 0 14.89 14.10 0.47 o 2 19 0 22.99 22.10 0.55 o 0 20 0 22.11 22.41 0.63 o 1 20 0 14.65 15.43 0.55 o 2 20 0 6.94 9.78 0.31 o 1 21 0 334.20 352.54 2.41 o 2 21 0 0.00 0.78 0.08 o 0 22 0 74.95 73.56 1.10 o 1 22 0 52.63 46.81 0.86 o 2 22 0 25.35 18.74 0.39 o 1 23 0 0.01 0.16 0.08 o 2 23 0 4.39 7.04 0.23 o 0 24 0 104.98 104.87 1.10 o 1 24 0 9.31 10.41 0.31 o 1 25 0 0.52 0.39 0.78 o 0 26 0 0.51 3.68 0.16 o -4 1 1 73.03 55.30 0.71 o -3 1 1 2.50 2.74 0.08 o -2 1 1 123.87 127.49 1.11 o -1 1 1 825.15 753.41 5.07 o 0 1 1 502.22 485.04 2.68 o 1 1 1 196.67 149.07 0.88 o 2 1 1 401.80 481.45 2.43 o 3 1 1 7.56 9.39 0.31 o -4 2 1 13.47 12.85 0.31 o -3 2 1 60.55 59.25 1.02 o -2 2 1 445.79 543.65 2.28 o -1 2 1 2706.64 3323.17 12.03 o 0 2 1 1718.64 1531.19 5.72 o 1 2 1 478.36 515.05 4.74 o 2 2 1 955.95 1089.11 10.72 o 3 2 1 4.93 6.42 0.23 o -4 3 1 13.35 9.16 0.31 o -3 3 1 17.30 17.86 0.55 o -2 3 1 2.02 1.88 0.08 o -1 3 1 1383.81 1656.02 8.18 o 0 3 1 863.17 767.08 4.08 o 1 3 1 6.35 17.77 0.31 o 2 3 1 1068.71 1167.72 11.32 o 3 3 1 102.96 103.03 1.34 o -4 4 1 24.33 19.52 0.39 o -3 4 1 205.88 235.28 1.99 o -2 4 1 180.93 208.97 1.43 o -1 4 1 1750.35 2126.55 9.87 o 0 4 1 502.74 571.12 3.73 o 1 4 1 18.68 28.38 0.39 o 2 4 1 40.68 49.84 0.78 o 3 4 1 83.28 84.30 1.18 o -4 5 1 2.98 3.36 0.08 o -3 5 1 94.65 86.58 1.18 o -2 5 1 9.25 9.00 0.31 o -1 5 1 180.28 176.64 0.96 o 0 5 1 2348.08 1725.47 8.01 o 1 5 1 149.92 151.31 0.96 o 2 5 1 153.95 156.07 1.43 o 3 5 1 82.88 80.21 1.18 o -4 6 1 39.36 30.95 0.47 o -3 6 1 140.98 155.65 1.66 o -2 6 1 455.86 370.42 2.03 o -1 6 1 2343.56 2508.51 11.92 o 0 6 1 12.99 13.48 0.24 o 1 6 1 4143.11 4097.02 17.51 o 2 6 1 2.39 2.03 0.08 o 3 6 1 35.54 36.08 0.78 o -4 7 1 10.93 9.24 0.23 o -3 7 1 38.17 41.34 0.86 o -2 7 1 48.05 42.57 0.71 o -1 7 1 180.72 159.05 0.96 o 0 7 1 16.67 14.90 0.24 o 1 7 1 51.22 68.20 0.71 o 2 7 1 4.71 3.36 0.08 o 3 7 1 1.68 1.88 0.08 o -3 8 1 101.14 114.44 1.42 o -2 8 1 173.82 227.54 1.67 o -1 8 1 738.29 805.45 6.93 o 0 8 1 415.29 346.76 3.96 o 1 8 1 65.64 37.25 0.55 o 2 8 1 4.02 8.37 0.31 o 3 8 1 101.92 98.07 1.26 o -3 9 1 27.93 31.67 0.71 o -2 9 1 99.28 102.21 1.18 o -1 9 1 2.00 2.82 0.08 o 0 9 1 1.28 1.25 0.78 o 1 9 1 26.94 35.14 0.55 o 2 9 1 447.53 512.76 2.83 o 3 9 1 28.31 25.56 0.63 o -3 10 1 0.96 0.78 0.08 o -2 10 1 41.81 51.17 0.86 o -1 10 1 561.25 552.86 6.35 o 0 10 1 123.41 120.04 0.95 o 1 10 1 3.22 0.08 0.08 o 2 10 1 65.81 72.88 1.10 o 3 10 1 48.41 48.84 0.86 o -3 11 1 142.52 141.94 1.50 o -2 11 1 120.94 126.75 1.34 o -1 11 1 399.21 359.00 1.87 o 0 11 1 1421.85 1230.79 9.52 o 1 11 1 3.56 7.75 0.23 o 2 11 1 35.77 29.88 0.71 o 3 11 1 193.30 169.45 1.51 o -3 12 1 3.20 2.50 0.08 o -2 12 1 35.49 37.57 0.78 o -1 12 1 2.93 7.98 0.23 o 0 12 1 1.15 1.41 0.08 o 1 12 1 101.31 74.96 0.95 o 2 12 1 115.10 112.83 1.42 o 3 12 1 20.97 25.70 0.55 o -3 13 1 0.37 0.63 0.08 o -2 13 1 1.07 3.13 0.08 o -1 13 1 54.27 55.01 0.79 o 0 13 1 814.21 769.35 8.22 o 1 13 1 105.55 116.70 1.18 o 2 13 1 182.39 189.04 1.82 o 3 13 1 44.70 40.75 0.71 o -3 14 1 1.89 0.70 0.08 o -2 14 1 224.90 216.30 1.91 o -1 14 1 7.89 6.18 0.23 o 0 14 1 265.86 244.27 1.68 o 1 14 1 123.88 117.32 1.26 o 2 14 1 4.89 5.48 0.16 o 3 14 1 2.43 2.43 0.08 o -3 15 1 14.06 14.96 0.47 o -2 15 1 58.90 57.67 1.02 o -1 15 1 479.43 476.97 2.60 o 0 15 1 22.47 22.02 0.55 o 1 15 1 98.36 74.10 1.02 o 2 15 1 119.81 132.91 1.50 o 3 15 1 48.82 64.52 0.79 o -3 16 1 9.56 21.06 0.47 o -2 16 1 42.15 40.57 0.86 o -1 16 1 83.06 64.95 1.02 o 0 16 1 419.28 385.11 2.34 o 1 16 1 15.41 14.64 0.47 o 2 16 1 196.87 224.75 1.98 o 3 16 1 1.28 2.35 0.08 o -3 17 1 53.29 62.27 0.79 o -2 17 1 79.49 73.97 1.10 o -1 17 1 0.05 0.16 0.16 o 0 17 1 238.56 228.33 1.83 o 1 17 1 125.77 121.69 1.42 o 2 17 1 220.52 255.99 2.07 o -3 18 1 31.37 27.31 0.47 o -2 18 1 117.39 111.13 1.34 o -1 18 1 548.33 558.34 3.09 o 0 18 1 132.60 129.03 1.42 o 1 18 1 25.20 27.74 0.71 o 2 18 1 51.96 51.76 0.86 o -2 19 1 195.48 224.04 1.83 o -1 19 1 91.40 90.97 1.26 o 0 19 1 74.89 70.01 1.10 o 1 19 1 591.75 574.16 3.10 o 2 19 1 73.58 83.26 1.10 o -2 20 1 82.01 104.10 1.18 o -1 20 1 149.88 151.80 1.58 o 0 20 1 10.19 10.02 0.31 o 1 20 1 167.72 161.21 1.58 o 2 20 1 0.99 2.27 0.08 o -2 21 1 30.43 28.31 0.55 o -1 21 1 16.92 19.89 0.55 o 0 21 1 35.77 37.65 0.78 o 1 21 1 12.34 11.82 0.39 o 2 21 1 8.49 6.65 0.23 o -2 22 1 2.40 5.79 0.16 o -1 22 1 206.68 213.43 1.75 o 0 22 1 82.34 88.72 1.18 o 1 22 1 6.71 5.63 0.16 o 2 22 1 0.03 0.31 0.78 o -2 23 1 1.91 1.72 0.08 o -1 23 1 0.08 0.16 0.16 o 0 23 1 27.25 27.75 0.63 o 1 23 1 1.39 1.25 0.08 o -1 24 1 48.10 58.21 0.79 o 0 24 1 59.02 70.91 0.94 o 1 24 1 0.11 1.02 0.08 o -1 25 1 7.79 7.98 0.23 o 0 25 1 21.10 17.09 0.39 o 1 25 1 7.62 13.23 0.31 o 0 26 1 0.36 0.39 0.78 o -4 0 2 112.69 106.35 1.03 o -3 0 2 32.96 50.11 0.94 o -2 0 2 974.38 1080.09 9.29 o -1 0 2 22556.27 31417.29 54.95 o 0 0 2 910.62 836.09 4.88 o 1 0 2 18.33 20.93 0.39 o 2 0 2 268.42 317.29 2.08 o 3 0 2 178.03 188.79 1.74 o -4 1 2 35.99 34.29 0.63 o -3 1 2 10.56 11.59 0.39 o -2 1 2 93.95 88.40 0.87 o -1 1 2 3274.36 3851.42 13.69 o 0 1 2 1098.13 993.44 5.38 o 1 1 2 392.05 418.75 4.82 o 2 1 2 59.07 60.91 0.94 o 3 1 2 18.93 18.41 0.55 o -4 2 2 56.19 50.71 0.71 o -3 2 2 1.05 4.69 0.16 o -2 2 2 2086.32 2209.89 13.97 o -1 2 2 4596.73 6479.64 18.82 o 0 2 2 727.43 833.12 4.97 o 1 2 2 258.80 288.05 1.37 o 2 2 2 0.17 0.86 0.08 o 3 2 2 35.66 37.96 0.78 o -4 3 2 0.25 0.31 0.16 o -3 3 2 85.92 88.73 1.18 o -2 3 2 58.51 60.64 0.79 o -1 3 2 1057.05 1221.02 7.18 o 0 3 2 1468.96 1088.48 6.21 o 1 3 2 490.41 535.53 5.61 o 2 3 2 118.19 147.67 1.42 o 3 3 2 303.16 318.89 2.24 o -4 4 2 7.08 7.04 0.23 o -3 4 2 2.68 6.88 0.23 o -2 4 2 2.91 0.16 0.08 o -1 4 2 1225.67 1450.14 8.17 o 0 4 2 1243.86 1122.47 6.53 o 1 4 2 9.77 6.11 0.23 o 2 4 2 171.79 180.40 1.59 o 3 4 2 22.78 23.12 0.63 o -4 5 2 0.09 0.55 0.78 o -3 5 2 1.61 1.80 0.08 o -2 5 2 188.72 175.58 1.35 o -1 5 2 551.27 614.40 5.36 o 0 5 2 141.13 169.88 0.88 o 1 5 2 1844.18 1931.70 11.82 o 2 5 2 26.75 32.92 0.71 o 3 5 2 0.24 3.68 0.16 o -4 6 2 2.88 2.27 0.08 o -3 6 2 12.03 18.48 0.55 o -2 6 2 67.80 53.75 0.79 o -1 6 2 1121.97 1155.55 7.88 o 0 6 2 1800.34 1581.80 8.74 o 1 6 2 26.87 22.90 0.47 o 2 6 2 0.53 1.80 0.08 o 3 6 2 0.85 1.17 0.08 o -4 7 2 3.11 2.19 0.08 o -3 7 2 4.70 3.83 0.16 o -2 7 2 79.44 87.74 1.02 o -1 7 2 180.84 208.20 1.20 o 0 7 2 0.09 0.08 0.08 o 1 7 2 1159.46 1229.68 9.80 o 2 7 2 155.25 179.63 1.66 o 3 7 2 0.29 3.99 0.16 o -4 8 2 0.13 0.16 0.08 o -3 8 2 0.31 0.47 0.16 o -2 8 2 19.16 18.33 0.47 o -1 8 2 1401.38 1286.10 9.31 o 0 8 2 108.72 91.04 0.71 o 1 8 2 51.10 43.78 0.63 o 2 8 2 189.73 171.19 1.67 o 3 8 2 23.86 27.51 0.63 o -4 9 2 0.60 0.23 0.08 o -3 9 2 39.78 44.01 0.86 o -2 9 2 89.68 96.46 1.10 o -1 9 2 129.89 151.64 1.11 o 0 9 2 0.91 0.47 0.78 o 1 9 2 217.41 215.84 1.44 o 2 9 2 36.84 40.87 0.86 o 3 9 2 0.31 0.63 0.08 o -3 10 2 106.38 105.34 1.34 o -2 10 2 24.44 20.93 0.55 o -1 10 2 188.45 178.03 1.27 o 0 10 2 1079.96 876.53 7.88 o 1 10 2 846.57 802.05 8.72 o 2 10 2 2.96 2.50 0.08 o 3 10 2 82.33 73.96 0.95 o -3 11 2 4.99 4.15 0.16 o -2 11 2 0.09 0.23 0.16 o -1 11 2 20.09 17.48 0.39 o 0 11 2 446.24 359.59 1.79 o 1 11 2 46.15 39.50 0.71 o 2 11 2 403.57 394.76 2.66 o 3 11 2 27.85 23.92 0.55 o -3 12 2 55.98 49.41 0.86 o -2 12 2 851.28 868.41 3.66 o -1 12 2 257.30 253.65 1.68 o 0 12 2 543.42 525.08 2.30 o 1 12 2 96.64 91.22 1.10 o 2 12 2 22.89 19.90 0.63 o 3 12 2 32.03 36.32 0.63 o -3 13 2 10.64 12.92 0.39 o -2 13 2 75.55 74.98 1.10 o -1 13 2 47.27 40.37 0.71 o 0 13 2 47.39 36.21 0.63 o 1 13 2 93.16 79.04 1.02 o 2 13 2 532.92 524.79 3.09 o 3 13 2 2.55 2.50 0.08 o -3 14 2 1.23 2.03 0.08 o -2 14 2 50.27 49.47 0.94 o -1 14 2 153.33 134.88 1.35 o 0 14 2 68.25 60.66 0.87 o 1 14 2 2.40 3.76 0.08 o 2 14 2 62.93 63.58 1.02 o 3 14 2 53.27 52.70 0.63 o -3 15 2 3.23 3.68 0.16 o -2 15 2 122.79 129.39 1.50 o -1 15 2 6.86 10.02 0.31 o 0 15 2 178.99 176.17 1.51 o 1 15 2 25.42 30.10 0.71 o 2 15 2 22.94 28.05 0.71 o -3 16 2 0.94 2.35 0.08 o -2 16 2 128.01 126.83 1.50 o -1 16 2 62.42 56.28 0.94 o 0 16 2 703.62 668.94 3.13 o 1 16 2 15.65 13.94 0.47 o 2 16 2 99.70 98.53 1.26 o -3 17 2 0.32 0.16 0.16 o -2 17 2 68.09 67.07 1.02 o -1 17 2 225.85 232.41 1.91 o 0 17 2 337.26 328.41 2.25 o 1 17 2 11.12 16.75 0.55 o 2 17 2 11.51 9.94 0.31 o -3 18 2 1.04 1.17 0.08 o -2 18 2 27.53 26.81 0.63 o -1 18 2 26.38 26.96 0.71 o 0 18 2 31.08 27.99 0.71 o 1 18 2 173.64 184.95 1.74 o 2 18 2 2.07 1.88 0.08 o -3 19 2 16.80 16.93 0.31 o -2 19 2 25.16 26.26 0.63 o -1 19 2 142.51 148.24 1.58 o 0 19 2 0.30 0.08 0.16 o 1 19 2 213.36 207.13 1.83 o 2 19 2 1.72 0.70 0.08 o -2 20 2 13.10 10.73 0.39 o -1 20 2 8.90 12.21 0.39 o 0 20 2 198.18 190.61 1.75 o 1 20 2 13.43 9.24 0.31 o 2 20 2 0.02 0.23 0.08 o -2 21 2 58.82 65.33 0.86 o -1 21 2 81.71 88.00 1.18 o 0 21 2 172.95 172.37 1.66 o 1 21 2 84.40 84.50 1.10 o 2 21 2 6.91 4.70 0.16 o -2 22 2 24.59 21.17 0.47 o -1 22 2 8.61 8.53 0.31 o 0 22 2 35.87 36.00 0.71 o 1 22 2 0.23 0.70 0.08 o -2 23 2 6.23 5.56 0.16 o -1 23 2 5.46 6.34 0.23 o 0 23 2 2.31 2.74 0.08 o 1 23 2 9.46 14.95 0.39 o -1 24 2 0.24 0.31 0.08 o 0 24 2 0.08 1.10 0.08 o 1 24 2 29.91 25.42 0.47 o -1 25 2 13.53 13.86 0.31 o 0 25 2 0.46 0.94 0.08 o 0 26 2 0.02 0.70 0.78 o -4 1 3 1.84 1.80 0.08 o -3 1 3 6.80 6.26 0.23 o -2 1 3 2046.15 2110.60 13.81 o -1 1 3 1066.78 985.75 6.84 o 0 1 3 2809.24 3096.05 12.71 o 1 1 3 1043.50 1125.22 9.29 o 2 1 3 422.54 507.06 2.83 o 3 1 3 2.61 2.58 0.08 o -4 2 3 25.18 23.21 0.47 o -3 2 3 0.25 1.88 0.08 o -2 2 3 35.54 45.68 0.71 o -1 2 3 762.83 778.41 6.09 o 0 2 3 1302.60 1350.49 7.95 o 1 2 3 1267.97 1245.71 9.89 o 2 2 3 7.63 9.71 0.31 o 3 2 3 115.76 111.02 1.18 o -4 3 3 0.14 0.23 0.08 o -3 3 3 6.14 5.01 0.16 o -2 3 3 97.39 97.15 0.95 o -1 3 3 0.22 2.97 0.08 o 0 3 3 684.26 728.43 5.79 o 1 3 3 184.74 154.70 1.19 o 2 3 3 91.30 76.02 1.10 o 3 3 3 5.68 7.59 0.23 o -4 4 3 3.09 4.38 0.16 o -3 4 3 54.09 57.49 0.94 o -2 4 3 16.01 31.49 0.55 o -1 4 3 349.18 274.48 1.30 o 0 4 3 377.97 401.61 4.34 o 1 4 3 546.64 505.48 2.22 o 2 4 3 103.26 101.71 1.26 o 3 4 3 5.24 4.38 0.16 o -4 5 3 10.07 7.75 0.23 o -3 5 3 0.01 0.00 0.23 o -2 5 3 8.96 18.40 0.47 o -1 5 3 1279.97 1193.88 8.40 o 0 5 3 405.53 410.10 4.59 o 1 5 3 855.61 783.46 8.09 o 2 5 3 77.10 64.91 1.02 o 3 5 3 193.36 199.36 1.59 o -4 6 3 20.23 13.01 0.39 o -3 6 3 511.08 565.83 3.09 o -2 6 3 37.88 66.24 0.86 o -1 6 3 387.34 425.42 4.98 o 0 6 3 909.08 850.49 6.98 o 1 6 3 0.68 2.66 0.08 o 2 6 3 0.14 1.41 0.08 o 3 6 3 55.48 54.39 0.79 o -4 7 3 14.46 14.96 0.39 o -3 7 3 41.80 41.27 0.86 o -2 7 3 171.58 175.88 1.43 o -1 7 3 153.28 165.84 1.11 o 0 7 3 342.57 261.64 1.38 o 1 7 3 43.34 53.71 0.79 o 2 7 3 21.51 24.21 0.63 o 3 7 3 0.05 0.16 0.08 o -4 8 3 1.16 0.08 0.08 o -3 8 3 63.21 67.75 1.10 o -2 8 3 33.84 56.56 0.86 o -1 8 3 2.98 14.87 0.39 o 0 8 3 936.72 944.61 8.04 o 1 8 3 22.11 23.51 0.55 o 2 8 3 424.98 430.71 2.74 o 3 8 3 20.86 27.12 0.55 o -4 9 3 12.65 13.24 0.31 o -3 9 3 34.35 39.37 0.78 o -2 9 3 26.93 33.71 0.63 o -1 9 3 1166.83 1273.99 10.14 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