#------------------------------------------------------------------------------ #$Date: 2019-01-11 06:21:43 +0200 (Fri, 11 Jan 2019) $ #$Revision: 213004 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/04/1550438.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1550438 loop_ _publ_author_name 'Gajarushi, Ashwini' 'Wasim, Mohd' 'Nabi, Rizwan' 'Srinivasu, Kancharlapalli' 'Rao, Ramgopal' 'Rajaraman, Gopalan' 'Subramaniam, Chandramouli' 'Shanmugam, Maheswaran' _publ_section_title ; Lanthanide complexes as molecular dopants for realizing air-stable n-type graphene logic inverters with symmetric transconductance ; _journal_name_full 'Materials Horizons' _journal_paper_doi 10.1039/C8MH01241E _journal_year 2019 _chemical_formula_sum 'C26 H18 Ce N9 O9' _chemical_formula_weight 740.61 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _audit_update_record ; 2018-06-13 deposited with the CCDC. 2019-01-02 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 118.320(13) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 15.0921(16) _cell_length_b 10.8118(8) _cell_length_c 19.5232(17) _cell_measurement_reflns_used 3916 _cell_measurement_temperature 150 _cell_measurement_theta_max 30.3400 _cell_measurement_theta_min 2.3560 _cell_volume 2804.4(6) _computing_cell_refinement 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.41 (Rigaku OD, 2015)' _computing_molecular_graphics 'BRUKER SHELXTL' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXL-2014/7 (Sheldrick, 2014)' _diffrn_ambient_temperature 150 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'dtrek-CrysAlisPro-abstract goniometer imported rigaku-d*trek images' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0887 _diffrn_reflns_av_unetI/netI 0.0989 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 6863 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.000 _diffrn_reflns_theta_max 25.000 _diffrn_reflns_theta_min 2.362 _exptl_absorpt_coefficient_mu 1.694 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.68195 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.41 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.754 _exptl_crystal_description 'block shaped' _exptl_crystal_F_000 1468 _refine_diff_density_max 0.980 _refine_diff_density_min -1.404 _refine_diff_density_rms 0.247 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.081 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 207 _refine_ls_number_reflns 2463 _refine_ls_number_restraints 18 _refine_ls_restrained_S_all 1.083 _refine_ls_R_factor_all 0.0708 _refine_ls_R_factor_gt 0.0503 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0510P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1067 _refine_ls_wR_factor_ref 0.1187 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2078 _reflns_number_total 2463 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file c8mh01241e2.cif _cod_data_source_block cel1 _cod_original_cell_volume 2804.4(5) _cod_database_code 1550438 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; cel1.res created by SHELXL-2014/7 TITL ms-mw-01-149-cel1_mo_a.res in C2/c REM Old TITL MS-MW-01-149-CeL1_Mo in C2/c #15 REM SHELXT solution in C2/c REM R1 0.144, Rweak 0.011, Alpha 0.039, Orientation as input REM Formula found by SHELXT: C29 N6 O9 Ce CELL 0.71073 15.092105 10.811831 19.523203 90 118.3195 90 ZERR 4 0.001622 0.00082 0.001696 0 0.0127 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H Ce N O UNIT 104 72 4 36 36 L.S. 100 PLAN 10 BOND $H LIST 6 MORE -1 CONF fmap 2 53 acta 52 OMIT -3 50 OMIT 2 0 0 REM REM REM EQIV $1 1-x, +y, 1.5-z DFIX 1.261 0.01 N61 O61 N61 O61_$1 N61 O63 DANG 2.170 0.01 O61 O63 O63 O61_$1 O61 O61_$1 FLAT 0.001 N61 O61 O61_$1 O63 SIMU 0.01 N61 O61 O63 DFIX 1.261 0.01 N61A O61A N61A O61A_$1 N61A O63A DANG 2.170 0.01 O61A O63A O63A O61A_$1 O61A O61A_$1 FLAT 0.001 N61A O61A O61A_$1 O63A SIMU 0.01 N61A O61A O63A WGHT 0.051000 FVAR 0.23774 0.08038 O53 5 0.648333 -0.014302 0.875544 11.00000 0.03720 0.04844 = 0.03546 -0.01037 0.01313 -0.00967 O51 5 0.521885 -0.143348 0.830847 11.00000 0.01932 0.04000 = 0.02827 0.00120 0.01290 0.00246 CE01 3 0.500000 -0.349182 0.750000 10.50000 0.02259 0.03879 = 0.01905 0.00000 0.00891 0.00000 O52 5 0.653312 -0.185992 0.817489 11.00000 0.01926 0.04767 = 0.02798 -0.00436 0.01176 0.00459 N51 4 0.609385 -0.113248 0.841668 11.00000 0.02223 0.04396 = 0.01548 0.00584 0.00370 -0.00216 N11 4 0.309015 -0.437555 0.674903 11.00000 0.03492 0.03977 = 0.02121 -0.00124 0.01103 -0.00923 C11 1 0.256401 -0.458329 0.712365 11.00000 0.03467 0.04691 = 0.03022 -0.00396 0.01804 -0.01325 N12 4 0.406441 -0.378306 0.590801 11.00000 0.02719 0.03921 = 0.02102 0.00004 0.01097 -0.00397 C12 1 0.158409 -0.503503 0.676251 11.00000 0.03087 0.05702 = 0.03492 -0.00138 0.00994 -0.01164 AFIX 43 H12A 2 0.123340 -0.515773 0.704054 11.00000 -1.20000 AFIX 0 N13 4 0.607753 -0.374907 0.670931 11.00000 0.02524 0.04106 = 0.02065 0.00129 0.01324 0.00552 C13 1 0.114636 -0.529707 0.597152 11.00000 0.02916 0.04598 = 0.03744 0.00172 0.00938 -0.01427 AFIX 43 H13A 2 0.050130 -0.562907 0.571450 11.00000 -1.20000 AFIX 0 C14 1 0.166197 -0.506738 0.557800 11.00000 0.03049 0.03998 = 0.02831 -0.00081 0.01253 -0.01145 AFIX 43 H14A 2 0.136499 -0.521300 0.504534 11.00000 -1.20000 AFIX 0 C15 1 0.265137 -0.460635 0.597866 11.00000 0.03380 0.03344 = 0.02687 -0.00150 0.01252 -0.01249 C16 1 0.320761 -0.431214 0.556659 11.00000 0.03399 0.03885 = 0.02023 -0.00284 0.00834 -0.00199 AFIX 43 H16A 2 0.293469 -0.451298 0.504218 11.00000 -1.20000 AFIX 0 C17 1 0.458756 -0.349849 0.548584 11.00000 0.03060 0.03205 = 0.02265 -0.00072 0.01341 0.00026 C18 1 0.409443 -0.320441 0.468491 11.00000 0.03021 0.04367 = 0.02351 -0.00056 0.00970 0.00356 AFIX 43 H18A 2 0.339533 -0.317757 0.440950 11.00000 -1.20000 AFIX 0 C19 1 0.465143 -0.296077 0.432000 11.00000 0.06054 0.03973 = 0.02063 0.00506 0.01940 0.00937 AFIX 43 H19A 2 0.432557 -0.277742 0.379132 11.00000 -1.20000 AFIX 0 C20 1 0.568949 -0.298007 0.471794 11.00000 0.04687 0.04342 = 0.02563 -0.00514 0.01882 0.00402 AFIX 43 H20A 2 0.605863 -0.282676 0.445758 11.00000 -1.20000 AFIX 0 C21 1 0.618124 -0.323168 0.551482 11.00000 0.02518 0.04471 = 0.03206 0.00209 0.01363 0.00906 AFIX 43 H21A 2 0.688067 -0.322182 0.578962 11.00000 -1.20000 AFIX 0 C22 1 0.563650 -0.349310 0.589327 11.00000 0.03366 0.02796 = 0.02454 0.00249 0.01608 -0.00092 C23 1 0.692587 -0.431409 0.703289 11.00000 0.03029 0.05728 = 0.02440 0.00161 0.01203 0.00900 AFIX 43 H23 2 0.722427 -0.455779 0.673309 11.00000 -1.20000 AFIX 0 PART 1 N61 4 0.500000 -0.628638 0.750000 10.25000 0.07661 O61 5 0.479371 -0.569874 0.796183 10.50000 0.06085 O63 5 0.500000 -0.745444 0.750000 10.25000 0.06301 PART 2 N61A 4 0.478959 -0.632110 0.743603 10.25000 0.02087 O61A 5 0.507735 -0.577244 0.807782 10.50000 0.03022 O63A 5 0.438571 -0.737085 0.730380 10.25000 0.04190 PART 0 HKLF 4 REM ms-mw-01-149-cel1_mo_a.res in C2/c REM R1 = 0.0503 for 2078 Fo > 4sig(Fo) and 0.0708 for all 2463 data REM 207 parameters refined using 18 restraints END WGHT 0.0510 0.0000 REM Highest difference peak 0.980, deepest hole -1.404, 1-sigma level 0.247 Q1 1 0.3770 -0.7435 0.6991 11.00000 0.05 0.98 Q2 1 0.5000 -0.5384 0.7500 10.50000 0.05 0.78 Q3 1 0.2496 -0.4092 0.4744 11.00000 0.05 0.66 Q4 1 0.3863 -0.4218 0.4433 11.00000 0.05 0.65 Q5 1 0.4022 -0.3325 0.3982 11.00000 0.05 0.64 Q6 1 0.5259 -0.0564 0.8346 11.00000 0.05 0.64 Q7 1 0.0101 -0.4207 0.5655 11.00000 0.05 0.62 Q8 1 0.2949 -0.3949 0.5217 11.00000 0.05 0.60 Q9 1 0.6258 0.0969 0.8513 11.00000 0.05 0.59 Q10 1 0.4430 -0.4042 0.4259 11.00000 0.05 0.59 ; _shelx_res_checksum 84607 _shelx_hkl_file ; -21 -1 9 79.05 35.01 -21 -1 10 35.48 26.19 -21 -1 11 74.71 37.09 -21 -1 12 20.33 24.13 -21 -1 13 55.93 37.72 -21 -1 14 60.13 41.13 -21 -3 9 23.09 27.71 -21 -3 10 114.58 48.90 -21 -3 11 -1.01 20.40 -21 -3 12 134.03 53.47 -20 0 10 121.94 40.85 -20 0 11 14.81 21.63 -20 0 12 186.46 56.63 -20 0 13 28.33 28.55 -20 0 14 170.47 55.24 -20 0 15 8.75 20.00 -20 0 16 84.58 37.08 -20 -2 8 -8.38 18.23 -20 -2 9 162.13 55.72 -20 -2 10 -10.07 14.41 -20 -2 11 200.19 59.74 -20 -2 12 31.00 30.65 -20 -2 13 137.80 49.61 -20 -2 14 42.90 34.25 -20 -2 15 46.41 32.69 -20 -2 16 61.23 38.72 -20 -2 17 71.75 33.89 -20 -4 8 2.58 21.01 -20 -4 9 124.29 48.12 -20 -4 10 118.57 48.51 -20 -4 11 -9.97 20.78 -20 -4 12 113.01 43.40 -20 -4 13 85.33 43.99 -20 -4 14 39.36 14.54 -20 -6 9 5.75 19.21 -19 -1 6 32.62 24.43 -19 -1 7 77.50 36.15 -19 -1 8 107.88 45.07 -19 -1 9 136.58 45.61 -19 -1 10 81.23 44.51 -19 -1 11 93.48 38.66 -19 -1 12 51.28 33.32 -19 -1 13 180.50 54.86 -19 1 13 239.50 59.42 -19 -1 14 9.59 31.16 -19 1 14 3.58 11.56 -19 -1 15 51.40 33.57 -19 1 15 61.73 30.48 -19 -1 16 61.32 34.83 -19 1 16 12.22 19.89 -19 1 17 89.84 39.60 -19 -1 17 144.93 50.77 -19 -1 18 61.68 37.05 -19 1 18 80.57 37.15 -19 -1 19 43.69 37.69 -19 1 19 28.46 26.20 -19 -1 20 84.43 39.19 -19 1 20 -23.01 23.85 -19 -3 6 148.18 48.69 -19 -3 7 57.33 40.32 -19 -3 8 -5.02 17.61 -19 -3 9 -11.45 10.93 -19 -3 10 172.19 53.94 -19 -3 11 64.64 32.80 -19 -3 12 48.18 27.50 -19 -3 13 6.41 23.38 -19 -3 14 171.12 60.11 -19 -3 15 6.84 15.23 -19 -3 16 60.72 38.58 -19 -3 17 -5.86 13.68 -19 -3 18 102.36 57.60 -19 -3 19 25.46 30.70 -19 -5 7 40.95 31.98 -19 -5 8 -9.13 16.81 -19 -5 9 69.01 39.49 -19 -5 10 -1.52 13.19 -19 -5 12 7.22 13.49 -19 -5 13 114.64 51.07 -19 -5 14 14.37 25.89 -19 -5 16 14.72 21.77 -19 -7 8 55.55 46.03 -19 -7 9 -8.89 24.81 -19 -7 10 143.70 62.21 -18 0 7 -9.69 12.46 -18 0 8 101.08 36.96 -18 0 9 18.81 23.49 -18 0 10 322.76 71.22 -18 0 11 10.01 20.97 -18 0 12 206.42 57.63 -18 0 13 -8.83 14.35 -18 0 14 371.25 81.61 -18 0 15 20.33 25.06 -18 0 16 142.74 53.45 -18 0 17 9.75 24.96 -18 0 18 153.68 54.24 -18 0 19 20.80 35.93 -18 0 20 178.93 60.71 -18 0 21 -23.19 15.55 -18 0 22 -1.48 21.92 -18 -2 4 18.67 19.82 -18 -2 5 188.97 48.32 -18 -2 6 6.04 14.85 -18 -2 7 83.96 38.38 -18 -2 8 12.08 20.17 -18 -2 9 150.83 50.23 -18 -2 10 33.27 29.69 -18 -2 11 164.97 51.25 -18 -2 12 13.25 24.61 -18 -2 13 211.84 60.49 -18 -2 14 52.33 36.56 -18 -2 15 80.63 37.78 -18 -2 16 -13.45 22.13 -18 -2 17 197.05 59.93 -18 -2 18 37.10 39.05 -18 -2 19 84.51 42.31 -18 -2 20 30.09 29.96 -18 -2 21 37.24 34.79 -18 -4 5 46.47 25.10 -18 -4 6 97.11 39.03 -18 -4 7 15.81 22.54 -18 -4 8 53.24 30.72 -18 -4 9 59.77 31.66 -18 -4 10 111.59 48.23 -18 -4 11 22.61 26.09 -18 -4 12 94.75 41.58 -18 -4 13 85.81 41.22 -18 -4 14 35.45 32.50 -18 -4 15 21.00 26.04 -18 -4 16 39.12 32.66 -18 -4 17 45.90 35.54 -18 -4 18 172.10 64.45 -18 -4 19 22.78 34.33 -18 -4 20 18.08 32.45 -18 -6 5 6.78 20.92 -18 -6 6 13.15 13.08 -18 -6 7 -7.65 14.54 -18 -6 8 72.05 39.65 -18 -6 9 2.97 16.97 -18 -6 10 42.71 37.52 -18 -6 11 27.77 26.06 -18 -6 12 40.58 32.61 -18 -6 13 55.74 41.89 -18 -6 14 58.23 46.85 -18 -6 15 48.99 46.61 -18 -6 16 63.66 51.64 -18 -6 17 -18.85 25.29 -18 -8 7 42.24 42.16 -18 -8 8 -27.30 28.91 -18 -8 9 21.65 19.39 -18 -8 10 -9.83 19.07 -18 -8 11 -25.81 30.09 -17 -1 3 102.39 33.38 -17 -1 4 88.53 34.94 -17 -1 5 307.02 68.77 -17 -1 6 25.52 19.17 -17 -1 7 110.65 39.97 -17 -1 8 32.80 23.58 -17 -1 9 125.09 41.94 -17 1 9 171.27 46.35 -17 -1 10 53.37 27.47 -17 1 10 90.26 31.27 -17 -1 11 192.20 54.01 -17 1 11 106.26 36.35 -17 -1 12 142.37 46.54 -17 1 12 96.24 38.21 -17 -1 13 164.59 50.20 -17 1 13 148.90 48.48 -17 1 14 141.20 48.80 -17 -1 14 189.34 54.32 -17 1 15 197.79 56.21 -17 -1 15 128.31 46.89 -17 1 16 213.57 63.58 -17 -1 16 176.88 55.29 -17 -1 17 128.35 47.86 -17 1 17 222.50 61.78 -17 1 18 108.74 44.83 -17 -1 18 17.47 25.49 -17 1 19 71.52 40.88 -17 -1 19 162.57 58.71 -17 1 20 18.29 24.56 -17 -1 20 46.91 31.85 -17 1 21 32.05 21.85 -17 -1 21 47.77 35.94 -17 -1 22 4.88 18.24 -17 1 22 59.75 34.27 -17 1 23 45.11 29.45 -17 -1 23 -1.03 17.21 -17 -1 24 126.02 51.76 -17 1 24 47.53 34.27 -17 -3 3 23.05 23.28 -17 -3 4 151.10 44.06 -17 -3 5 9.44 12.41 -17 -3 6 141.93 43.39 -17 -3 7 84.31 40.00 -17 -3 8 75.39 34.30 -17 -3 9 9.04 18.87 -17 -3 10 160.90 54.67 -17 -3 11 10.19 9.63 -17 -3 12 242.19 63.90 -17 -3 13 61.27 36.16 -17 -3 14 174.47 56.63 -17 -3 15 26.77 24.13 -17 -3 16 203.91 70.99 -17 -3 17 5.38 17.45 -17 -3 18 124.48 50.05 -17 -3 19 10.55 19.59 -17 -3 20 132.99 51.43 -17 -3 21 -13.18 20.72 -17 -3 22 45.30 41.09 -17 -3 23 -20.95 26.92 -17 -5 4 0.12 13.93 -17 -5 5 130.57 46.90 -17 -5 6 11.49 19.02 -17 -5 7 80.05 35.40 -17 -5 8 -16.99 19.86 -17 -5 9 270.33 70.51 -17 -5 10 23.16 30.27 -17 -5 11 156.22 52.30 -17 -5 12 -16.20 19.65 -17 -5 13 161.69 61.22 -17 -5 14 25.28 27.03 -17 -5 15 79.10 47.78 -17 -5 16 36.12 31.57 -17 -5 17 166.73 65.49 -17 -5 18 37.53 30.05 -17 -5 19 81.01 48.66 -17 -5 20 17.81 15.96 -17 -7 5 15.39 17.49 -17 -7 6 54.50 39.71 -17 -7 7 -16.91 25.10 -17 -7 8 99.12 46.91 -17 -7 9 -3.95 23.10 -17 -7 10 220.51 75.19 -17 -7 11 3.59 19.88 -17 -7 12 194.68 65.04 -17 -7 13 61.09 40.38 -17 -7 14 69.88 55.21 -17 -7 15 5.92 26.96 -17 -7 16 22.28 33.62 -17 -7 17 11.72 26.23 -17 -9 6 35.44 42.30 -17 -9 7 -12.87 27.57 -17 -9 8 -27.12 28.56 -17 -9 10 27.84 26.54 -16 0 4 436.70 63.27 -16 0 5 8.20 19.50 -16 0 6 434.50 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33.47 2 4 4 507.95 30.96 2 -4 5 535.95 37.29 2 4 5 523.25 28.30 2 -4 6 347.71 31.13 2 4 6 271.26 30.01 2 4 6 362.10 22.30 2 4 7 479.20 26.40 2 4 7 458.94 42.77 2 -4 7 439.83 34.78 2 -4 7 430.64 24.59 2 -4 7 407.93 36.26 2 -4 8 308.12 22.20 2 4 8 284.04 20.08 2 -4 8 280.39 29.37 2 -4 8 289.42 32.39 2 -4 9 12.43 8.58 2 4 9 13.23 4.18 2 -4 9 15.38 5.75 2 -4 9 21.91 8.90 2 4 10 859.63 38.01 2 -4 10 846.24 54.31 2 -4 10 852.93 38.71 2 -4 10 858.43 61.48 2 -4 11 11.63 7.68 2 -4 11 7.69 9.58 2 4 11 4.24 3.13 2 4 12 445.70 31.83 2 -4 12 421.00 42.16 2 -4 12 418.28 44.92 2 -4 13 116.58 28.47 2 4 13 82.91 13.72 2 -4 13 92.89 20.44 2 -4 14 239.78 37.17 2 -4 14 215.74 31.04 2 4 14 246.45 23.68 2 -4 15 234.38 34.00 2 4 15 212.27 24.13 2 -4 16 108.76 23.50 2 4 16 69.53 14.46 2 -4 17 121.83 25.37 2 -4 18 143.81 27.60 2 -4 19 122.36 27.05 2 -4 20 126.27 29.51 2 -4 21 139.22 32.41 2 -6 -21 127.95 29.80 2 -6 -20 96.85 25.69 2 -6 -19 150.60 29.81 2 -6 -18 173.21 30.19 2 -6 -17 24.68 10.55 2 -6 -16 45.68 15.86 2 -6 -15 4.85 5.70 2 -6 -14 310.77 37.34 2 -6 -5 266.16 11.64 2 -6 -4 1262.94 30.13 2 6 -3 8.58 5.47 2 -6 -3 6.69 2.60 2 -6 -2 85.06 10.88 2 6 -2 103.15 14.53 2 -6 -1 564.90 29.90 2 6 -1 466.93 28.02 2 -6 0 848.73 38.08 2 6 0 883.88 35.71 2 -6 1 892.87 41.74 2 6 1 946.78 34.83 2 -6 2 537.23 34.11 2 6 2 530.46 24.47 2 -6 3 163.83 19.78 2 6 3 155.37 12.28 2 -6 4 123.31 17.71 2 6 4 81.28 8.36 2 6 5 413.34 17.73 2 6 5 320.59 21.88 2 6 6 330.18 16.71 2 6 6 472.08 20.17 2 6 7 87.10 7.89 2 6 7 36.06 6.34 2 6 8 135.11 9.50 2 -6 8 171.75 25.18 2 6 8 169.02 28.94 2 -6 8 213.37 32.81 2 -6 9 6.46 11.25 2 6 9 1.03 1.49 2 -6 9 4.22 5.47 2 6 9 2.38 2.03 2 6 9 7.42 7.34 2 -6 9 5.42 2.13 2 -6 10 261.68 31.95 2 6 10 153.85 11.87 2 -6 10 217.72 35.85 2 -6 11 9.05 12.02 2 6 11 4.02 1.51 2 -6 12 420.21 43.78 2 -6 12 335.08 48.67 2 -6 13 172.49 37.07 2 -6 13 144.49 26.40 2 -6 14 329.49 40.44 2 -6 14 308.87 50.32 2 -6 15 122.62 27.47 2 -6 16 133.23 28.67 2 -6 17 39.82 16.87 2 -6 18 43.10 18.16 2 -6 19 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9 23.83 9.23 8 -6 9 10.20 7.20 8 -6 10 162.70 34.75 8 -6 11 51.15 18.98 8 -6 12 118.18 30.28 8 -6 13 93.23 27.77 8 -6 14 86.32 26.38 8 -8 -10 128.43 19.37 8 -8 -9 192.68 24.94 8 -8 -8 44.64 12.95 8 -8 -7 277.72 32.56 8 -8 -6 56.04 14.86 8 -8 -5 323.25 36.67 8 -8 -4 23.15 10.09 8 -8 -3 292.81 38.04 8 -8 -2 21.79 11.56 8 -8 -1 237.68 34.71 8 -8 0 86.39 21.56 8 -8 1 432.06 46.14 8 -8 2 80.67 20.64 8 -8 3 524.07 53.45 8 -8 4 3.93 5.69 8 8 4 -3.76 10.57 8 8 5 156.69 33.00 8 -8 5 246.57 38.86 8 -8 6 18.96 11.91 8 8 7 99.70 29.91 8 -8 7 61.68 19.73 8 8 8 29.56 21.52 8 -8 8 -2.00 7.45 8 -8 9 203.15 37.83 8 -8 10 44.28 20.60 8 -8 11 97.02 27.59 8 -8 12 16.62 13.01 8 -10 -6 333.64 34.14 8 -10 -5 10.44 5.96 8 -10 -4 226.03 30.16 8 -10 -3 7.74 9.08 8 -10 -2 312.35 37.82 8 -10 -1 3.75 6.43 8 -10 0 133.09 26.10 8 -10 1 11.08 7.54 8 -10 2 50.21 16.62 8 -10 3 8.79 10.60 8 -10 4 205.79 35.55 8 -10 5 26.18 10.10 8 -10 6 111.16 27.83 8 -10 7 6.58 8.30 8 10 7 26.71 20.01 8 -10 8 145.75 32.57 8 10 8 156.30 42.98 8 10 9 18.89 15.67 8 -10 10 116.55 32.19 8 -12 0 0.59 5.77 8 -12 1 20.59 12.09 8 -12 2 -11.83 11.27 8 -12 3 88.06 24.11 8 -12 4 33.40 15.94 8 -12 5 54.91 21.10 8 -12 6 12.45 12.77 8 -12 7 44.72 18.56 9 -1 -25 104.22 25.47 9 -1 -2 297.90 30.35 9 -1 -2 334.52 55.34 9 -1 -1 1061.65 96.14 9 1 0 600.99 73.93 9 -1 0 719.88 72.92 9 1 1 437.94 44.90 9 1 1 464.33 63.47 9 -1 1 524.81 65.78 9 1 1 410.10 53.02 9 -1 2 764.71 74.24 9 1 2 641.55 56.03 9 1 2 649.62 70.90 9 -1 2 763.14 76.45 9 1 2 646.52 58.35 9 1 3 125.41 25.75 9 -1 3 124.36 29.50 9 1 3 131.77 35.44 9 -1 3 164.20 34.66 9 -1 4 216.26 37.65 9 1 4 298.27 48.53 9 -1 4 193.39 35.65 9 1 4 224.42 29.87 9 -1 5 108.92 22.70 9 1 5 182.68 35.65 9 -1 5 143.02 33.20 9 1 6 78.61 23.78 9 -1 6 109.98 27.65 9 1 7 221.07 37.89 9 -1 7 227.18 40.65 9 1 8 13.89 9.89 9 -1 8 28.04 17.34 9 -1 9 362.33 50.97 9 1 9 361.17 51.57 9 1 10 36.49 18.00 9 -1 10 28.61 13.51 9 1 11 317.90 47.14 9 -1 11 315.47 47.19 9 1 12 52.16 19.83 9 -1 12 72.71 23.72 9 1 13 155.69 33.68 9 -1 13 171.94 36.27 9 1 14 73.53 21.93 9 -1 14 60.88 19.97 9 1 15 44.70 19.28 9 -1 15 81.06 26.51 9 1 16 73.44 25.65 9 -1 16 121.34 29.95 9 -3 -27 19.96 14.84 9 -3 -26 184.52 35.21 9 -3 -5 4.52 11.96 9 -3 -4 589.98 68.34 9 -3 -3 133.11 32.22 9 -3 -2 642.09 69.07 9 -3 -1 114.30 31.52 9 -3 0 490.13 59.86 9 -3 1 200.01 37.68 9 3 2 896.14 90.08 9 -3 2 897.98 76.64 9 3 3 24.57 15.56 9 3 3 10.67 9.46 9 -3 3 10.06 8.64 9 3 3 8.82 11.03 9 3 4 882.22 75.98 9 3 4 939.16 90.59 9 -3 4 949.71 78.85 9 3 5 11.95 10.43 9 -3 5 30.93 18.88 9 3 6 469.63 55.80 9 -3 6 633.28 65.81 9 3 7 50.85 18.51 9 -3 7 23.99 13.09 9 -3 8 432.37 56.05 9 3 8 373.05 48.73 9 3 9 -0.26 7.09 9 -3 9 -0.46 6.06 9 3 10 31.05 12.80 9 -3 10 80.48 25.43 9 3 11 6.80 6.72 9 -3 11 19.22 14.00 9 3 12 141.51 31.73 9 -3 12 174.90 35.82 9 3 13 74.29 21.81 9 -3 13 96.89 28.52 9 3 14 214.91 37.44 9 -3 14 268.73 46.28 9 -3 15 7.50 12.78 9 -5 -26 5.75 11.28 9 -5 -9 160.01 33.33 9 -5 -8 38.31 19.82 9 -5 -7 123.98 29.42 9 -5 -6 29.56 18.41 9 -5 -5 639.61 67.87 9 -5 -4 13.31 11.40 9 -5 -3 936.26 76.65 9 -5 -2 -4.75 3.83 9 -5 -1 804.27 69.84 9 -5 0 73.42 22.68 9 -5 1 634.03 62.92 9 -5 2 6.78 11.45 9 5 3 341.72 57.25 9 -5 3 407.97 51.84 9 5 4 -7.73 12.71 9 -5 4 7.29 8.98 9 -5 5 217.03 39.02 9 5 5 183.29 37.66 9 5 5 210.10 41.61 9 5 6 13.63 9.55 9 -5 6 14.33 13.82 9 5 6 34.05 18.76 9 -5 7 271.45 43.52 9 5 7 195.42 33.56 9 5 8 5.76 4.62 9 -5 8 7.79 8.65 9 -5 9 656.89 67.49 9 5 9 578.98 59.69 9 5 10 28.47 13.13 9 -5 10 34.32 14.66 9 -5 11 300.18 47.16 9 -5 12 13.19 14.71 9 -5 13 51.66 20.50 9 -5 14 6.49 16.49 9 -7 -13 20.29 11.42 9 -7 -12 252.58 37.66 9 -7 -11 -0.51 6.20 9 -7 -10 486.14 49.58 9 -7 -9 83.05 19.83 9 -7 -8 184.97 30.71 9 -7 -7 298.90 37.85 9 -7 -6 556.91 53.58 9 -7 -5 155.37 28.13 9 -7 -4 257.89 36.45 9 -7 -3 99.08 24.95 9 -7 -2 265.56 38.56 9 -7 -1 23.65 13.78 9 -7 0 426.23 50.00 9 -7 1 -3.72 6.24 9 -7 2 202.99 35.61 9 -7 3 20.80 18.30 9 7 3 -8.56 12.02 9 -7 4 446.06 52.81 9 7 4 278.50 45.74 9 7 5 88.89 27.18 9 -7 5 113.46 28.08 9 7 6 84.09 24.79 9 -7 6 68.08 21.84 9 7 6 77.40 25.35 9 7 7 33.67 17.26 9 -7 7 52.17 20.75 9 -7 8 174.76 34.99 9 -7 9 5.82 6.41 9 -7 10 224.37 42.21 9 -7 11 2.06 11.55 9 -7 12 106.37 30.64 9 -9 -9 4.36 4.06 9 -9 -8 288.94 34.95 9 -9 -7 99.98 21.34 9 -9 -6 75.11 19.68 9 -9 -5 44.14 14.26 9 -9 -4 8.26 7.25 9 -9 -3 213.33 32.96 9 -9 -2 166.58 29.73 9 -9 -1 301.84 40.18 9 -9 0 41.16 16.18 9 -9 1 81.64 21.68 9 -9 2 40.16 17.95 9 -9 3 130.67 28.42 9 -9 4 169.38 33.68 9 -9 5 34.69 15.29 9 9 6 49.10 22.04 9 -9 6 47.71 18.83 9 9 7 88.17 30.86 9 -9 7 128.68 30.94 9 9 8 39.69 23.56 9 -9 8 27.65 14.96 9 -9 9 71.56 23.18 9 -9 10 1.07 8.97 9 -11 -3 129.44 25.03 9 -11 -2 40.95 14.81 9 -11 -1 28.74 13.52 9 -11 0 4.90 9.16 9 -11 1 45.69 15.54 9 -11 2 15.33 10.24 9 -11 4 44.66 17.10 9 -11 5 29.87 17.32 9 -11 6 31.32 16.96 9 -11 7 57.74 25.03 10 0 -1 4.86 8.58 10 0 -1 -1.32 8.63 10 0 0 882.17 63.35 10 0 0 844.92 89.41 10 0 1 -4.71 8.04 10 0 2 781.34 84.96 10 0 3 6.93 15.00 10 0 4 287.01 48.71 10 0 5 -5.11 7.84 10 0 6 319.31 49.74 10 0 7 24.06 17.28 10 0 8 331.36 51.13 10 0 9 1.03 9.71 10 0 10 310.66 52.45 10 0 11 3.67 11.33 10 0 12 306.08 47.83 10 0 13 20.47 18.58 10 0 14 136.92 34.88 10 0 15 3.30 7.18 10 -2 -5 292.06 25.42 10 -2 -3 445.86 65.07 10 -2 -2 12.07 14.70 10 -2 -1 574.70 71.07 10 -2 0 73.64 27.89 10 2 1 895.75 94.91 10 -2 1 882.90 84.60 10 2 2 22.41 18.63 10 -2 2 64.68 19.80 10 2 2 73.88 23.43 10 2 3 849.50 73.32 10 2 3 791.86 85.46 10 -2 3 714.07 71.12 10 2 4 5.98 10.93 10 -2 4 46.64 19.92 10 2 5 456.87 63.55 10 -2 5 485.05 59.83 10 2 6 118.64 29.98 10 -2 6 161.55 36.40 10 2 7 112.65 28.79 10 -2 7 198.08 38.99 10 2 8 35.89 15.78 10 -2 8 107.96 30.37 10 2 9 9.95 5.24 10 -2 9 33.30 18.64 10 2 10 46.75 20.48 10 -2 10 13.71 8.95 10 2 11 266.57 45.54 10 -2 11 210.75 41.61 10 2 12 -2.64 5.38 10 -2 12 -6.24 10.18 10 -2 13 190.96 38.64 10 2 13 144.15 33.12 10 2 14 16.97 16.54 10 -2 14 19.54 11.27 10 2 15 132.02 32.50 10 -4 -27 29.72 16.23 10 -4 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21.23 10 6 2 54.21 24.84 10 -6 3 180.07 36.75 10 6 3 146.01 37.20 10 -6 4 376.60 54.30 10 6 4 346.17 53.47 10 -6 5 168.40 36.28 10 6 5 157.86 37.81 10 6 5 105.17 30.63 10 -6 6 195.83 37.82 10 6 6 161.98 35.17 10 6 6 210.47 44.38 10 6 7 87.21 23.06 10 -6 7 107.18 29.25 10 -6 8 342.05 51.20 10 6 8 237.70 39.37 10 -6 9 32.20 17.63 10 -6 10 129.15 32.60 10 -6 11 -4.51 11.27 10 -8 -11 212.79 31.42 10 -8 -10 2.60 7.34 10 -8 -9 502.20 50.22 10 -8 -8 -1.58 4.86 10 -8 -7 266.21 38.25 10 -8 -6 88.39 21.86 10 -8 -5 57.32 17.84 10 -8 -4 -0.34 7.11 10 -8 -3 429.08 51.66 10 -8 -2 116.24 28.06 10 -8 -1 168.18 33.16 10 -8 0 13.66 10.38 10 -8 1 126.91 29.93 10 -8 2 14.19 11.53 10 -8 3 242.70 40.90 10 8 3 110.21 35.30 10 -8 4 1.42 6.84 10 -8 5 158.14 33.09 10 8 6 18.56 18.42 10 -8 6 -0.54 8.81 10 8 7 99.13 33.61 10 -8 7 95.31 28.86 10 -8 8 74.80 22.86 10 -8 9 49.24 23.42 10 -10 -6 90.92 21.98 10 -10 -5 5.74 5.48 10 -10 -4 103.26 22.76 10 -10 -3 31.13 13.85 10 -10 -2 201.13 34.13 10 -10 -1 2.72 6.59 10 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23.94 11 1 14 42.44 18.33 11 -3 -8 982.79 35.20 11 -3 -6 1012.08 101.35 11 -3 -5 69.49 28.61 11 -3 -4 587.22 74.97 11 -3 -3 51.11 23.43 11 -3 -2 614.87 79.02 11 -3 -1 139.63 35.05 11 -3 0 475.30 64.86 11 -3 1 51.57 18.95 11 3 1 108.86 32.66 11 3 2 451.07 54.54 11 3 2 577.73 77.64 11 -3 2 489.48 62.75 11 3 3 13.93 16.79 11 -3 3 9.28 6.88 11 3 3 15.02 15.15 11 3 4 308.27 57.58 11 -3 4 347.37 51.47 11 3 5 18.14 18.03 11 -3 5 4.61 9.77 11 3 6 169.32 37.21 11 -3 6 132.61 34.27 11 3 7 48.97 20.26 11 -3 7 20.35 11.43 11 3 8 97.75 31.41 11 -3 8 136.66 37.57 11 3 9 44.78 19.04 11 -3 9 72.14 26.65 11 3 10 73.14 24.89 11 -3 10 104.14 30.04 11 3 11 31.35 19.42 11 -3 11 62.55 24.66 11 3 12 140.32 33.95 11 -3 12 156.73 37.23 11 -5 -10 13.81 16.59 11 -5 -9 712.76 83.04 11 -5 -8 38.28 20.51 11 -5 -7 1135.29 98.71 11 -5 -6 99.30 29.89 11 -5 -5 156.52 38.77 11 -5 -4 102.87 31.29 11 -5 -3 724.39 76.17 11 -5 -2 31.18 17.52 11 -5 -1 655.75 70.48 11 -5 0 7.03 8.16 11 -5 1 235.11 43.82 11 -5 2 -15.91 13.89 11 5 2 -0.92 7.38 11 5 3 193.28 42.23 11 -5 3 263.67 46.17 11 5 4 50.56 29.84 11 -5 4 19.68 15.00 11 5 4 32.89 16.46 11 -5 5 226.58 43.79 11 5 5 240.35 47.67 11 5 5 249.54 48.72 11 5 6 -22.65 19.55 11 -5 6 13.04 15.30 11 -5 7 279.13 51.24 11 5 7 284.69 46.03 11 5 8 11.10 12.87 11 -5 8 11.35 10.12 11 5 9 45.45 21.82 11 -5 9 78.70 26.73 11 -5 10 -6.00 6.06 11 -5 11 159.59 38.55 11 -7 -14 94.00 24.45 11 -7 -13 5.46 7.81 11 -7 -12 290.22 44.54 11 -7 -11 84.37 25.40 11 -7 -10 546.40 63.04 11 -7 -9 39.53 19.95 11 -7 -8 966.77 81.86 11 -7 -7 13.97 15.52 11 -7 -6 385.78 49.99 11 -7 -5 28.33 13.76 11 -7 -4 34.48 15.88 11 -7 -3 44.98 20.65 11 -7 -2 187.89 37.14 11 -7 -1 2.55 11.03 11 -7 0 92.17 25.50 11 -7 1 56.31 23.79 11 -7 2 280.66 47.77 11 7 2 127.31 37.78 11 -7 3 159.79 36.45 11 7 3 91.36 30.68 11 7 4 200.41 45.64 11 -7 4 262.85 45.68 11 7 5 8.51 12.94 11 -7 5 4.79 6.46 11 7 5 8.96 13.63 11 -7 6 242.93 43.77 11 7 6 181.50 45.03 11 -7 7 11.74 8.76 11 -7 8 116.77 32.72 11 -7 9 7.28 10.23 11 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476.32 75.91 12 -2 -1 513.82 77.51 12 -2 0 -3.10 9.83 12 2 0 6.52 8.21 12 2 0 -1.29 9.72 12 2 1 284.05 44.12 12 2 1 246.61 54.67 12 -2 1 328.62 56.57 12 2 2 20.13 22.48 12 -2 2 36.04 23.34 12 2 2 41.02 17.35 12 2 3 364.54 65.20 12 -2 3 511.71 67.85 12 2 4 63.38 26.59 12 -2 4 42.31 20.07 12 2 5 380.31 61.74 12 -2 5 340.93 57.19 12 2 6 26.64 19.76 12 -2 6 54.78 22.30 12 2 7 336.30 56.32 12 -2 7 285.99 54.65 12 2 8 -4.21 8.66 12 -2 8 7.78 11.85 12 2 9 76.76 28.87 12 -2 9 105.84 36.99 12 2 10 0.78 6.41 12 -2 10 4.72 6.67 12 2 11 199.42 42.93 12 -2 11 174.56 39.14 12 2 12 21.51 15.81 12 -4 -8 675.91 88.77 12 -4 -7 486.96 76.45 12 -4 -6 216.86 47.90 12 -4 -5 158.92 41.35 12 -4 -4 197.17 45.27 12 -4 -3 391.17 62.23 12 -4 -2 583.56 77.21 12 -4 -1 121.54 36.30 12 -4 0 136.59 36.80 12 -4 1 58.16 24.11 12 4 1 27.97 11.38 12 4 2 22.34 15.29 12 -4 2 5.35 10.90 12 4 2 31.58 14.07 12 4 3 159.83 46.61 12 4 3 154.00 37.41 12 -4 3 178.69 39.55 12 4 4 88.58 31.69 12 4 4 199.50 40.26 12 -4 4 222.24 46.11 12 4 5 39.70 14.66 12 -4 5 35.29 23.44 12 -4 6 286.63 50.87 12 4 6 265.36 48.01 12 4 7 83.40 26.82 12 -4 7 129.44 38.36 12 4 8 13.23 12.20 12 -4 8 126.76 35.10 12 4 9 22.39 13.85 12 -4 9 21.75 18.29 12 4 10 27.12 16.54 12 -4 10 24.80 17.86 12 -6 -14 257.63 52.74 12 -6 -13 188.37 44.71 12 -6 -12 252.16 48.42 12 -6 -11 129.02 36.13 12 -6 -10 145.77 35.33 12 -6 -9 561.20 70.52 12 -6 -8 336.44 56.99 12 -6 -7 154.46 39.38 12 -6 -6 107.55 34.26 12 -6 -5 7.69 13.44 12 -6 -4 278.49 48.61 12 -6 -3 4.20 7.69 12 -6 -2 156.92 36.42 12 -6 -1 51.52 21.24 12 -6 0 237.31 44.21 12 -6 1 224.82 44.69 12 6 1 82.65 35.91 12 -6 2 393.08 57.88 12 6 2 149.53 44.06 12 6 3 107.01 33.64 12 -6 3 179.26 40.79 12 6 4 72.91 31.96 12 -6 4 94.22 29.44 12 6 4 81.30 33.62 12 6 5 101.69 33.53 12 -6 5 155.44 38.10 12 6 5 84.56 29.62 12 6 6 42.26 23.41 12 -6 6 86.71 29.86 12 -6 7 -4.91 9.97 12 -6 8 47.82 25.93 12 -6 9 8.85 14.20 12 -8 -12 19.39 11.02 12 -8 -11 76.43 22.98 12 -8 -10 -5.31 8.77 12 -8 -9 231.64 40.29 12 -8 -8 10.72 7.51 12 -8 -7 233.89 40.49 12 -8 -6 129.83 29.15 12 -8 -5 86.74 25.57 12 -8 -4 17.54 15.26 12 -8 -3 297.94 49.16 12 -8 -2 22.76 17.13 12 -8 -1 222.20 42.01 12 -8 0 2.25 7.08 12 -8 1 115.45 32.18 12 8 1 29.47 22.12 12 -8 2 17.71 16.22 12 8 2 9.30 24.36 12 -8 3 185.00 40.87 12 -8 4 -6.13 8.62 12 8 4 0.77 6.35 12 -8 5 126.56 32.46 12 8 5 88.96 33.99 12 -8 6 65.42 26.40 12 8 6 16.40 14.27 12 -8 7 121.30 33.18 12 -10 -7 -1.39 7.96 12 -10 -6 162.83 34.38 12 -10 -5 24.35 14.50 12 -10 -4 96.26 26.65 12 -10 -3 16.12 10.99 12 -10 -2 139.09 33.23 12 -10 -1 8.47 10.92 12 -10 0 82.09 25.92 12 -10 1 9.78 12.20 12 -10 2 54.93 21.70 12 -10 3 -3.42 6.57 12 -10 4 57.76 23.50 12 -12 0 25.81 16.10 13 -1 -5 248.88 30.59 13 -1 -4 39.87 16.19 13 -1 -4 6.83 10.13 13 -1 -3 412.22 76.93 13 1 -2 189.41 31.17 13 -1 -2 213.61 50.97 13 1 -2 215.13 54.91 13 1 -1 478.06 55.34 13 1 -1 448.26 76.53 13 -1 -1 507.99 78.41 13 1 0 53.80 24.54 13 -1 0 46.06 23.16 13 1 0 52.61 19.75 13 1 1 107.87 38.11 13 -1 1 40.60 24.89 13 1 2 48.88 21.15 13 -1 2 -0.85 9.30 13 1 3 177.48 46.41 13 -1 3 212.58 48.79 13 1 4 121.76 38.70 13 -1 4 223.85 48.13 13 1 5 130.53 39.45 13 -1 5 158.83 40.30 13 1 6 138.83 37.16 13 -1 6 148.73 39.72 13 1 7 208.92 46.84 13 -1 7 291.84 54.58 13 1 8 40.37 20.31 13 -1 8 84.21 31.75 13 -1 9 62.34 26.14 13 1 10 29.59 18.06 13 -1 10 4.16 12.68 13 1 11 53.77 25.27 13 -3 -10 400.78 25.69 13 -3 -7 324.91 63.50 13 -3 -6 137.21 42.96 13 -3 -5 31.81 18.07 13 -3 -4 244.62 52.63 13 -3 -3 69.40 27.58 13 -3 -2 343.67 63.48 13 -3 -1 31.97 22.26 13 3 -1 4.35 17.69 13 3 0 288.49 62.26 13 -3 0 274.44 53.57 13 3 1 33.60 22.08 13 -3 1 21.83 14.49 13 3 1 10.62 7.93 13 3 2 426.74 58.07 13 3 2 448.60 78.96 13 -3 2 483.96 69.78 13 3 3 10.18 19.48 13 -3 3 -2.24 7.14 13 3 4 217.53 48.92 13 -3 4 306.75 55.88 13 3 5 8.27 13.56 13 -3 5 65.29 31.22 13 3 6 156.27 41.70 13 -3 6 255.61 52.07 13 3 7 52.44 21.54 13 -3 7 43.18 16.74 13 3 8 61.91 26.17 13 -3 8 90.33 32.23 13 3 9 18.88 12.81 13 -3 9 6.21 14.73 13 3 10 99.27 32.64 13 3 11 15.09 14.19 13 -5 -11 192.15 49.25 13 -5 -10 26.65 20.67 13 -5 -9 68.25 29.70 13 -5 -8 -4.19 11.06 13 -5 -7 271.09 55.03 13 -5 -6 22.80 19.73 13 -5 -5 291.37 56.30 13 -5 -4 86.93 28.28 13 -5 -3 481.61 68.49 13 -5 -2 -8.60 9.66 13 -5 -1 437.44 65.32 13 -5 0 8.35 8.16 13 5 0 51.39 32.84 13 -5 1 178.80 41.20 13 5 1 95.98 35.25 13 5 2 -3.79 10.38 13 -5 2 -7.09 10.60 13 5 2 3.67 7.68 13 5 3 193.10 43.80 13 5 3 325.63 63.51 13 -5 3 204.64 44.70 13 5 4 8.01 17.56 13 -5 4 8.13 9.41 13 5 4 -9.03 10.75 13 -5 5 277.64 53.43 13 5 5 164.21 43.21 13 5 6 21.00 16.18 13 -5 6 15.01 15.45 13 -5 7 203.66 46.89 13 5 7 219.48 44.57 13 -5 8 11.15 11.87 13 -7 -14 76.95 27.75 13 -7 -13 -5.29 19.76 13 -7 -12 276.53 53.02 13 -7 -11 40.12 22.78 13 -7 -10 214.36 47.35 13 -7 -9 52.11 26.43 13 -7 -8 241.24 46.52 13 -7 -7 36.38 18.97 13 -7 -6 133.48 35.23 13 -7 -5 13.52 14.20 13 -7 -4 55.42 21.72 13 -7 -3 48.76 21.52 13 -7 -2 302.82 51.17 13 -7 -1 83.10 27.12 13 -7 0 140.50 36.55 13 -7 1 39.08 23.74 13 7 1 51.12 29.66 13 -7 2 198.38 43.55 13 7 2 59.35 29.92 13 7 3 32.21 20.90 13 -7 3 67.26 28.65 13 7 3 24.32 18.13 13 -7 4 201.17 44.10 13 7 4 144.48 41.29 13 -7 5 9.97 12.17 13 7 5 49.29 27.62 13 -7 6 184.23 41.45 13 -9 -9 128.83 31.03 13 -9 -8 79.50 25.20 13 -9 -7 92.31 27.59 13 -9 -6 79.07 26.04 13 -9 -5 78.08 28.10 13 -9 -4 36.40 18.86 13 -9 -3 123.16 32.30 13 -9 -2 64.72 24.61 13 -9 -1 55.59 23.51 13 -9 0 105.37 31.50 13 -9 1 33.28 17.33 13 -9 2 24.63 19.26 13 -9 4 26.09 16.99 13 -11 -3 20.93 14.23 13 -11 -2 17.81 14.56 13 -11 -1 28.47 20.45 13 -11 0 66.89 25.79 13 -11 1 26.33 16.62 14 0 -4 590.09 54.97 14 0 -4 499.64 82.60 14 0 -3 3.27 9.12 14 0 -3 -2.69 15.59 14 0 -2 706.80 97.74 14 0 -1 14.66 17.90 14 0 0 102.92 45.74 14 0 1 16.48 16.83 14 0 2 712.01 113.04 14 0 3 17.66 24.16 14 0 4 239.32 49.50 14 0 5 7.90 8.98 14 0 6 183.83 45.64 14 0 7 12.02 10.69 14 0 8 105.85 35.13 14 0 9 5.30 13.36 14 -2 -8 8.42 6.64 14 -2 -7 841.58 54.38 14 -2 -6 144.38 49.28 14 -2 -5 89.16 32.82 14 -2 -4 88.34 34.26 14 -2 -3 212.69 50.51 14 -2 -2 55.42 29.33 14 2 -2 66.69 36.62 14 2 -1 232.71 42.10 14 2 -1 260.01 61.55 14 -2 -1 318.54 64.28 14 2 0 17.30 21.96 14 -2 0 109.82 36.54 14 2 0 91.94 26.94 14 2 1 86.78 35.19 14 -2 1 210.33 52.00 14 2 2 9.88 12.39 14 -2 2 13.78 15.51 14 2 3 316.27 62.68 14 -2 3 257.87 53.96 14 2 4 18.51 17.24 14 -2 4 38.71 23.10 14 2 5 146.54 40.38 14 -2 5 142.61 41.16 14 2 6 6.99 10.42 14 -2 6 6.39 10.91 14 2 7 123.86 35.45 14 -2 7 191.03 47.70 14 2 8 46.22 24.51 14 -2 8 32.27 22.41 14 2 9 31.38 20.75 14 2 10 38.39 21.83 14 -4 -10 21.83 22.68 14 -4 -9 15.88 18.83 14 -4 -8 87.63 33.94 14 -4 -7 112.20 37.45 14 -4 -6 533.20 78.85 14 -4 -5 125.96 42.92 14 -4 -4 304.15 63.15 14 -4 -3 28.73 16.20 14 -4 -2 228.25 50.00 14 -4 -1 161.70 41.21 14 4 -1 152.21 53.45 14 -4 0 39.33 22.59 14 4 0 63.06 35.41 14 4 1 66.87 30.47 14 -4 1 60.63 27.06 14 4 1 52.74 18.63 14 -4 2 95.08 31.80 14 4 2 101.10 33.08 14 4 3 125.08 41.37 14 -4 3 187.68 46.57 14 4 4 99.05 37.21 14 -4 4 151.26 41.61 14 4 5 51.35 27.21 14 -4 5 74.68 26.71 14 4 6 146.05 42.53 14 -4 6 177.61 45.88 14 4 7 67.46 29.88 14 -4 7 77.72 31.28 14 4 8 78.37 30.93 14 -6 -15 20.09 24.58 14 -6 -14 81.87 31.85 14 -6 -13 103.42 38.87 14 -6 -12 152.31 44.37 14 -6 -11 0.98 18.15 14 -6 -10 66.02 29.33 14 -6 -9 75.94 35.05 14 -6 -8 180.08 49.58 14 -6 -7 8.26 11.64 14 -6 -6 45.81 22.63 14 -6 -5 11.74 10.78 14 -6 -4 179.92 43.78 14 -6 -3 121.85 35.27 14 -6 -2 279.90 53.12 14 -6 -1 118.95 34.26 14 -6 0 149.40 41.17 14 6 0 97.32 35.41 14 -6 1 106.36 35.15 14 6 1 35.86 23.37 14 6 2 24.07 17.04 14 6 2 81.28 33.25 14 6 3 29.40 12.23 14 -6 3 20.43 18.18 14 -6 4 25.44 19.11 14 6 4 32.30 19.21 14 6 5 34.62 20.23 14 -6 5 78.81 30.67 14 -8 -12 21.20 16.77 14 -8 -11 110.13 30.31 14 -8 -10 -0.07 10.51 14 -8 -9 150.82 35.86 14 -8 -8 28.48 17.32 14 -8 -7 184.48 41.79 14 -8 -6 7.34 6.36 14 -8 -5 104.78 34.01 14 -8 -4 26.92 20.14 14 -8 -3 122.73 36.44 14 -8 -2 4.35 14.61 14 -8 -1 126.24 34.18 14 -8 0 45.39 25.62 14 8 0 16.46 27.63 14 -8 1 56.46 26.52 14 8 1 48.77 30.98 14 -8 2 2.16 9.24 14 -8 3 93.06 32.83 14 -10 -6 78.14 29.54 14 -10 -5 5.37 12.60 14 -10 -4 42.12 22.49 14 -10 -3 15.41 15.10 14 -10 -2 69.87 26.42 14 -10 0 52.09 26.84 15 -1 -7 303.30 34.82 15 -1 -6 37.90 13.93 15 -1 -6 35.53 30.75 15 -1 -5 312.79 63.81 15 1 -4 182.17 54.03 15 -1 -4 64.85 30.67 15 1 -3 348.63 49.20 15 1 -3 308.85 76.76 15 -1 -3 288.09 64.95 15 -1 -2 87.06 36.25 15 1 -2 63.87 21.63 15 1 -2 82.84 41.53 15 1 -1 134.89 47.17 15 -1 -1 162.00 49.79 15 1 0 177.52 53.39 15 -1 0 120.23 41.98 15 1 1 63.56 31.26 15 -1 1 36.95 23.70 15 1 2 176.33 50.67 15 -1 2 177.66 47.35 15 1 3 34.31 27.14 15 -1 3 107.31 36.87 15 1 4 52.16 27.97 15 -1 4 54.07 23.72 15 -1 5 90.40 37.45 15 1 6 35.34 23.80 15 -1 6 12.66 12.40 15 1 7 139.92 46.18 15 -1 7 77.59 33.32 15 -3 -9 101.34 38.33 15 -3 -8 585.85 96.78 15 -3 -7 40.17 24.26 15 -3 -6 71.34 29.73 15 -3 -5 18.39 23.38 15 -3 -4 153.84 49.18 15 -3 -3 64.52 32.34 15 -3 -2 347.32 68.13 15 3 -2 325.70 73.50 15 -3 -1 10.34 14.41 15 3 -1 16.37 12.10 15 3 -1 -2.03 13.76 15 3 0 112.60 40.72 15 -3 0 186.78 48.40 15 3 0 128.21 35.21 15 3 1 24.03 22.41 15 -3 1 0.46 10.10 15 3 1 21.26 17.48 15 3 2 170.08 49.75 15 -3 2 255.19 55.44 15 3 3 28.43 18.93 15 -3 3 56.28 28.47 15 3 4 151.91 46.69 15 -3 4 189.35 48.52 15 3 5 34.43 27.08 15 -3 5 17.92 15.31 15 3 6 125.04 38.91 15 3 7 14.49 19.84 15 3 8 80.43 30.02 15 -5 -13 233.99 60.63 15 -5 -12 57.34 35.57 15 -5 -11 80.98 36.98 15 -5 -10 485.28 76.68 15 -5 -9 97.87 36.59 15 -5 -8 -6.53 13.84 15 -5 -7 352.44 71.14 15 -5 -6 18.32 19.21 15 -5 -5 535.52 83.74 15 -5 -4 -19.78 22.14 15 -5 -3 233.35 51.25 15 -5 -2 11.54 14.56 15 -5 -1 226.72 51.81 15 5 -1 133.94 47.74 15 -5 0 -12.52 14.73 15 5 0 35.45 37.80 15 5 1 78.28 37.70 15 -5 1 33.93 23.96 15 5 1 42.04 24.23 15 -5 2 -4.67 10.24 15 5 2 -2.87 13.43 15 5 3 82.51 36.25 15 -5 3 99.70 37.48 15 5 4 16.87 23.17 15 -5 4 10.34 20.56 15 5 5 70.01 28.76 15 5 6 28.70 25.56 15 -7 -14 69.97 31.43 15 -7 -13 37.35 19.82 15 -7 -12 169.53 45.46 15 -7 -11 48.82 24.90 15 -7 -10 134.94 38.99 15 -7 -9 35.58 21.06 15 -7 -8 185.55 46.03 15 -7 -7 14.69 21.14 15 -7 -6 223.04 49.86 15 -7 -5 21.38 19.10 15 -7 -4 154.97 41.69 15 -7 -3 18.72 16.37 15 -7 -2 187.73 46.25 15 -7 -1 91.31 34.03 15 7 -1 91.52 50.26 15 -7 0 160.85 43.72 15 7 0 22.54 26.47 15 7 1 -17.32 22.23 15 -7 1 -7.90 13.37 15 7 2 -11.61 18.04 15 -7 2 36.26 25.74 15 7 2 63.08 36.67 15 -9 -9 67.42 24.13 15 -9 -8 38.71 23.29 15 -9 -7 76.88 29.40 15 -9 -6 18.16 13.54 15 -9 -5 32.53 22.06 15 -9 -4 18.54 16.04 15 -9 -3 74.36 28.83 15 -9 -2 17.10 18.93 15 -9 -1 34.27 23.06 15 -9 0 -15.45 16.54 16 0 -6 290.47 39.61 16 0 -5 0.52 8.07 16 0 -5 -5.16 16.58 16 0 -4 454.22 86.34 16 0 -3 -20.34 23.20 16 0 -2 297.06 69.31 16 0 -1 -18.14 18.14 16 0 0 135.33 50.14 16 0 1 2.56 16.77 16 0 2 94.70 39.31 16 0 3 4.35 12.13 16 0 4 135.31 44.65 16 0 5 -5.47 10.19 16 -2 -8 29.26 18.90 16 -2 -7 12.09 13.83 16 -2 -6 117.21 43.53 16 -2 -5 176.80 51.30 16 -2 -4 42.71 22.20 16 2 -4 41.04 32.33 16 2 -3 243.31 43.37 16 -2 -3 359.34 78.22 16 2 -3 297.94 75.15 16 -2 -2 -16.41 23.18 16 2 -2 -9.76 15.58 16 2 -2 16.16 24.24 16 2 -1 153.61 53.36 16 -2 -1 285.32 63.10 16 2 -1 204.66 42.59 16 2 0 243.59 68.99 16 -2 0 -14.38 11.18 16 2 1 269.15 69.36 16 -2 1 375.25 69.38 16 2 2 23.81 21.35 16 -2 2 10.67 15.55 16 2 3 99.92 38.84 16 -2 3 102.85 41.21 16 2 4 -9.60 11.12 16 -2 4 90.87 42.55 16 2 5 58.56 30.81 16 2 6 -0.49 15.60 16 -4 -11 88.41 43.51 16 -4 -10 126.63 45.97 16 -4 -9 75.15 36.00 16 -4 -8 97.24 37.35 16 -4 -7 103.29 43.39 16 -4 -6 183.93 55.30 16 -4 -5 58.00 33.29 16 -4 -4 168.03 49.03 16 -4 -3 36.71 26.00 16 -4 -2 90.00 37.93 16 4 -2 19.59 18.05 16 4 -1 109.62 33.57 16 4 -1 70.72 36.91 16 4 0 75.70 35.09 16 -4 0 120.41 41.42 16 4 0 69.94 26.34 16 4 1 18.56 19.21 16 -4 1 16.58 20.62 16 4 1 24.30 18.13 16 4 2 79.35 39.59 16 -4 2 54.97 24.88 16 4 3 56.11 30.27 16 -4 3 25.71 24.29 16 4 4 27.52 25.98 16 4 5 71.53 30.80 16 4 6 37.13 28.46 16 -6 -17 12.60 15.10 16 -6 -16 40.77 30.37 16 -6 -15 21.65 27.37 16 -6 -14 21.93 21.63 16 -6 -13 63.03 28.91 16 -6 -12 124.07 43.61 16 -6 -11 2.86 10.85 16 -6 -10 107.03 38.90 16 -6 -9 166.86 54.51 16 -6 -8 236.79 57.41 16 -6 -7 61.39 33.83 16 -6 -6 293.71 60.76 16 -6 -5 19.81 22.76 16 -6 -4 74.65 32.41 16 -6 -3 122.04 37.94 16 -6 -2 91.97 33.14 16 6 -2 67.31 36.65 16 -6 -1 64.34 30.49 16 6 -1 22.84 15.14 16 6 0 -4.02 18.99 16 -6 0 24.84 21.50 16 6 0 14.41 13.33 16 6 1 -12.30 22.36 16 -6 1 -10.56 16.42 16 6 1 2.87 10.16 16 6 2 31.93 22.27 16 6 2 -1.71 10.99 16 6 3 -28.56 28.21 16 -8 -12 24.00 20.86 16 -8 -11 50.26 23.40 16 -8 -10 -0.08 13.68 16 -8 -9 46.53 27.48 16 -8 -8 16.49 15.41 16 -8 -7 83.17 31.70 16 -8 -6 -14.25 16.39 16 -8 -5 73.93 31.36 16 -8 -4 32.69 21.20 16 -8 -3 47.86 27.97 16 -8 -2 10.48 15.93 16 8 -2 -12.11 25.51 16 -8 -1 46.48 27.68 16 8 -1 25.72 28.65 16 -10 -6 20.20 15.97 16 -10 -5 6.72 16.59 16 -10 -4 119.42 34.62 17 -1 -8 18.69 22.52 17 -1 -7 61.07 41.70 17 -1 -6 7.98 17.23 17 1 -5 257.40 43.94 17 1 -5 132.30 53.16 17 -1 -5 212.62 60.82 17 -1 -4 41.48 26.20 17 1 -4 102.75 28.89 17 1 -4 110.08 47.90 17 1 -3 88.07 46.09 17 -1 -3 198.94 58.73 17 1 -2 116.73 41.80 17 -1 -2 130.31 50.25 17 1 -1 50.19 38.36 17 -1 -1 79.84 42.33 17 1 0 72.74 40.23 17 -1 0 162.99 53.46 17 1 1 118.38 47.91 17 -1 1 136.11 46.86 17 1 2 -10.69 11.83 17 -1 2 97.96 40.08 17 1 3 3.99 12.72 17 -3 -11 3.11 17.73 17 -3 -10 98.17 43.48 17 -3 -9 16.26 28.51 17 -3 -8 71.41 33.85 17 -3 -7 14.09 17.15 17 -3 -6 152.41 54.30 17 -3 -5 3.40 16.65 17 -3 -4 83.05 38.82 17 3 -4 42.65 34.50 17 -3 -3 9.87 17.73 17 3 -3 8.18 13.06 17 3 -3 6.13 21.04 17 -3 -2 138.87 45.29 17 3 -2 153.28 40.45 17 3 -2 146.51 52.63 17 3 -1 62.69 38.04 17 -3 -1 41.38 26.34 17 3 -1 57.03 25.09 17 3 0 119.77 50.24 17 -3 0 140.67 47.74 17 3 1 17.30 21.83 17 -3 1 52.75 32.31 17 3 2 91.87 38.94 17 3 3 -7.59 14.65 17 -5 -15 46.11 39.35 17 -5 -14 26.79 25.15 17 -5 -13 105.42 42.36 17 -5 -12 17.81 23.11 17 -5 -11 60.41 27.47 17 -5 -10 41.32 28.31 17 -5 -9 250.49 66.04 17 -5 -8 28.01 26.52 17 -5 -7 123.64 46.22 17 -5 -6 -11.59 19.48 17 -5 -5 213.77 54.58 17 -5 -4 0.64 11.58 17 -5 -3 141.33 44.53 17 5 -3 144.95 49.51 17 -5 -2 128.71 59.77 17 5 -2 -4.78 20.91 17 5 -1 8.93 12.95 17 -5 -1 38.13 29.76 17 5 -1 19.95 19.26 17 5 0 13.65 20.60 17 -5 0 4.21 14.72 17 5 0 14.89 17.14 17 5 1 32.63 24.97 17 5 1 79.20 29.51 17 5 2 35.59 27.76 17 5 3 3.44 13.62 17 -7 -14 64.72 34.34 17 -7 -13 -15.91 20.63 17 -7 -12 105.17 39.21 17 -7 -11 -13.91 14.93 17 -7 -10 172.31 51.26 17 -7 -9 11.65 17.72 17 -7 -8 109.53 41.03 17 -7 -7 55.50 26.98 17 -7 -6 36.96 21.52 17 -7 -5 5.76 11.80 17 -7 -4 101.34 37.18 17 -7 -3 14.72 22.58 17 7 -3 10.16 37.51 17 -7 -2 46.35 26.01 17 7 -2 0.83 18.24 17 7 -1 42.18 35.47 17 7 0 775.61 105.79 17 -9 -9 -5.27 14.77 17 -9 -8 -7.73 12.46 17 -9 -7 2.92 16.30 17 -9 -6 40.78 25.53 17 -9 -5 74.25 32.43 18 0 -7 35.65 22.57 18 0 -6 235.59 68.97 18 0 -5 -22.22 24.76 18 0 -4 105.49 42.68 18 0 -3 -21.02 33.10 18 0 -2 75.42 45.24 18 0 -1 -3.28 22.22 18 0 0 37.93 31.05 18 -2 -10 89.06 46.93 18 -2 -9 160.26 56.39 18 -2 -8 12.97 58.11 18 -2 -7 54.76 33.82 18 -2 -6 64.43 35.17 18 2 -6 6.74 16.58 18 -2 -5 195.99 58.78 18 2 -5 123.34 34.17 18 2 -5 91.26 51.03 18 -2 -4 -4.97 16.03 18 2 -4 22.91 18.29 18 2 -4 57.91 36.32 18 2 -3 94.93 46.84 18 2 -3 112.03 32.16 18 2 -2 -10.08 16.61 18 -2 -2 26.90 21.01 18 2 -1 41.68 30.72 18 -2 -1 46.57 30.27 18 2 0 -26.11 30.14 18 -4 -14 2.25 22.64 18 -4 -13 45.21 37.18 18 -4 -12 49.29 31.39 18 -4 -11 11.96 11.85 18 -4 -10 120.53 48.59 18 -4 -9 15.09 21.24 18 -4 -8 111.32 43.73 18 -4 -7 96.31 50.26 18 -4 -6 36.58 29.85 18 -4 -5 88.33 42.90 18 -4 -4 122.84 46.95 18 4 -4 53.95 42.26 18 -4 -3 60.62 33.64 18 4 -3 55.55 23.70 18 4 -3 87.91 45.83 18 4 -2 16.07 23.81 18 -4 -2 55.31 28.94 18 4 -2 83.18 29.37 18 4 -1 20.28 25.60 18 4 -1 27.47 25.25 18 4 0 38.37 39.90 18 -6 -16 18.74 26.44 18 -6 -15 43.34 34.45 18 -6 -14 118.74 41.12 18 -6 -13 47.10 31.66 18 -6 -12 75.36 42.76 18 -6 -11 54.21 38.21 18 -6 -10 38.70 28.41 18 -6 -9 15.54 14.82 18 -6 -8 48.53 22.94 18 -6 -7 4.36 16.77 18 -6 -6 104.89 39.77 18 -6 -5 40.70 27.25 18 -6 -4 75.77 35.72 18 6 -4 15.15 17.32 18 6 -3 -17.78 19.90 18 6 -2 -11.56 33.47 18 6 -1 42.43 32.68 18 -8 -11 61.78 27.30 18 -8 -10 -0.10 11.26 18 -8 -8 17.22 18.86 18 -8 -7 35.23 24.48 19 -1 -10 81.20 46.47 19 -1 -9 122.77 52.74 19 -1 -8 -33.24 39.46 19 1 -7 -32.33 27.42 19 -1 -7 37.49 28.39 19 -1 -6 -19.06 27.71 19 1 -6 1.18 26.31 19 -1 -5 22.29 17.10 19 1 -5 44.42 28.60 19 1 -4 13.71 22.85 19 -1 -4 58.56 36.36 19 1 -3 118.48 51.11 19 -1 -3 20.54 23.79 19 -3 -13 10.08 18.99 19 -3 -12 69.84 38.80 19 -3 -11 3.89 30.64 19 -3 -10 78.69 37.50 19 -3 -9 42.82 32.03 19 -3 -8 80.50 41.52 19 -3 -7 6.49 13.95 19 -3 -6 246.97 72.77 19 3 -6 -49.56 44.57 19 3 -5 31.31 18.86 19 3 -5 -2.16 31.18 19 -3 -4 72.11 39.45 19 3 -4 107.80 35.82 19 3 -4 31.94 37.01 19 3 -3 37.74 34.06 19 3 -3 -0.92 8.80 19 -5 -18 -7.14 29.70 19 -5 -17 -5.58 34.54 19 -5 -16 -38.09 29.95 19 -5 -15 128.21 56.71 19 -5 -14 24.73 26.25 19 -5 -13 66.73 35.61 19 -5 -12 -4.16 21.90 19 -5 -10 26.10 34.53 19 -5 -9 68.85 38.60 19 -5 -8 5.03 20.15 19 -5 -7 87.90 42.31 19 -5 -6 6.49 14.95 19 5 -5 15.53 27.55 19 -7 -14 38.67 30.07 19 -7 -13 3.03 17.37 19 -7 -12 86.73 44.97 19 -7 -11 -9.89 12.58 19 -7 -10 47.80 26.34 19 -7 -9 22.52 24.98 20 0 -10 61.73 39.71 20 0 -9 17.43 28.10 20 0 -8 6.42 17.31 20 0 -7 18.61 24.31 20 -2 -12 3.13 18.35 20 -2 -11 143.42 61.73 20 -2 -10 21.57 33.76 20 -2 -9 72.30 35.20 20 -2 -8 -33.19 29.35 20 2 -8 -33.89 35.83 20 -4 -17 10.84 22.71 20 -4 -16 1.24 28.18 20 -4 -15 59.10 39.99 20 -4 -14 30.29 37.91 20 -4 -13 31.44 29.33 20 -4 -12 2.08 22.49 20 -4 -11 6.37 15.31 20 4 -5 42.69 21.04 20 -6 -15 27.83 34.09 20 -6 -14 98.19 51.19 20 -6 -13 55.09 32.79 20 -6 -12 37.33 24.84 TITL MS-MW-01-149-CeL1_Mo in Cc REM Cc (#9 in standard setting) CELL 0.71073 15.092105 10.811831 19.523203 90.0000 118.3195 90.0000 ZERR 12.00 0.001622 0.000820 0.001696 0.0000 0.0127 0.0000 LATT -7 SYMM x,-y, z+1/2 SFAC C H N O UNIT 132.00 120.00 12.00 12.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 93726 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O53 O 0.6483(3) -0.0143(4) 0.8755(2) 0.0420(12) Uani 1 1 d . . . . . O51 O 0.5219(3) -0.1433(3) 0.8308(2) 0.0285(10) Uani 1 1 d . . . . . Ce01 Ce 0.5000 -0.34918(4) 0.7500 0.0272(2) Uani 1 2 d S T P . . O52 O 0.6533(3) -0.1860(4) 0.8175(2) 0.0314(10) Uani 1 1 d . . . . . N51 N 0.6094(4) -0.1132(4) 0.8417(2) 0.0294(12) Uani 1 1 d . . . . . N11 N 0.3090(4) -0.4376(4) 0.6749(2) 0.0329(13) Uani 1 1 d . . . . . C11 C 0.2564(5) -0.4583(6) 0.7124(3) 0.0362(16) Uani 1 1 d . . . . . N12 N 0.4064(4) -0.3783(4) 0.5908(2) 0.0293(12) Uani 1 1 d . . . . . C12 C 0.1584(5) -0.5035(6) 0.6763(3) 0.0432(18) Uani 1 1 d . . . . . H12A H 0.1233 -0.5158 0.7041 0.052 Uiso 1 1 calc R U . . . N13 N 0.6078(4) -0.3749(4) 0.6709(2) 0.0280(12) Uani 1 1 d . . . . . C13 C 0.1146(5) -0.5297(6) 0.5972(3) 0.0401(17) Uani 1 1 d . . . . . H13A H 0.0501 -0.5629 0.5714 0.048 Uiso 1 1 calc R U . . . C14 C 0.1662(5) -0.5067(5) 0.5578(3) 0.0335(15) Uani 1 1 d . . . . . H14A H 0.1365 -0.5213 0.5045 0.040 Uiso 1 1 calc R U . . . C15 C 0.2651(5) -0.4606(5) 0.5979(3) 0.0321(15) Uani 1 1 d . . . . . C16 C 0.3208(5) -0.4312(5) 0.5567(3) 0.0329(15) Uani 1 1 d . . . . . H16A H 0.2935 -0.4513 0.5042 0.039 Uiso 1 1 calc R U . . . C17 C 0.4588(5) -0.3498(5) 0.5486(3) 0.0281(14) Uani 1 1 d . . . . . C18 C 0.4094(5) -0.3204(5) 0.4685(3) 0.0337(15) Uani 1 1 d . . . . . H18A H 0.3395 -0.3178 0.4409 0.040 Uiso 1 1 calc R U . . . C19 C 0.4651(6) -0.2961(6) 0.4320(3) 0.0402(18) Uani 1 1 d . . . . . H19A H 0.4326 -0.2777 0.3791 0.048 Uiso 1 1 calc R U . . . C20 C 0.5689(5) -0.2980(5) 0.4718(3) 0.0380(16) Uani 1 1 d . . . . . H20A H 0.6059 -0.2827 0.4458 0.046 Uiso 1 1 calc R U . . . C21 C 0.6181(5) -0.3232(5) 0.5515(3) 0.0340(15) Uani 1 1 d . . . . . H21A H 0.6881 -0.3222 0.5790 0.041 Uiso 1 1 calc R U . . . C22 C 0.5637(5) -0.3493(5) 0.5893(3) 0.0278(14) Uani 1 1 d . . . . . C23 C 0.6926(5) -0.4314(6) 0.7033(3) 0.0377(16) Uani 1 1 d . . . . . H23 H 0.7224 -0.4558 0.6733 0.045 Uiso 1 1 calc R U . . . N61 N 0.5000 -0.6286(13) 0.7500 0.077(8) Uiso 0.5 2 d DS U P A 1 O61 O 0.4794(10) -0.5699(10) 0.7962(6) 0.061(4) Uiso 0.5 1 d D U P A 1 O63 O 0.5000 -0.7454(11) 0.7500 0.063(4) Uiso 0.5 2 d DS U P A 1 N61A N 0.4790(4) -0.6321(8) 0.7436(5) 0.021(4) Uiso 0.25 1 d D U P A 2 O61A O 0.5077(8) -0.5772(8) 0.8078(3) 0.030(3) Uiso 0.5 1 d D U P A 2 O63A O 0.4386(10) -0.7371(9) 0.7304(6) 0.042(4) Uiso 0.25 1 d D U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O53 0.037(3) 0.048(3) 0.035(2) -0.0104(19) 0.013(2) -0.010(2) O51 0.019(2) 0.040(2) 0.0283(18) 0.0012(16) 0.0129(18) 0.0025(19) Ce01 0.0226(3) 0.0388(3) 0.0191(2) 0.000 0.0089(2) 0.000 O52 0.019(2) 0.048(2) 0.0280(18) -0.0044(17) 0.0118(18) 0.005(2) N51 0.022(3) 0.044(3) 0.015(2) 0.006(2) 0.004(2) -0.002(3) N11 0.035(3) 0.040(3) 0.021(2) -0.001(2) 0.011(2) -0.009(2) C11 0.035(4) 0.047(4) 0.030(3) -0.004(3) 0.018(3) -0.013(3) N12 0.027(3) 0.039(3) 0.021(2) 0.0000(19) 0.011(2) -0.004(2) C12 0.031(4) 0.057(4) 0.035(3) -0.001(3) 0.010(3) -0.012(3) N13 0.025(3) 0.041(3) 0.021(2) 0.0013(19) 0.013(2) 0.006(2) C13 0.029(4) 0.046(4) 0.037(3) 0.002(3) 0.009(3) -0.014(3) C14 0.030(4) 0.040(3) 0.028(3) -0.001(2) 0.013(3) -0.011(3) C15 0.034(4) 0.033(3) 0.027(3) -0.001(2) 0.013(3) -0.012(3) C16 0.034(4) 0.039(3) 0.020(2) -0.003(2) 0.008(3) -0.002(3) C17 0.031(4) 0.032(3) 0.023(3) -0.001(2) 0.013(3) 0.000(3) C18 0.030(4) 0.044(3) 0.024(3) -0.001(2) 0.010(3) 0.004(3) C19 0.061(5) 0.040(3) 0.021(3) 0.005(2) 0.019(3) 0.009(3) C20 0.047(5) 0.043(3) 0.026(3) -0.005(3) 0.019(3) 0.004(3) C21 0.025(4) 0.045(3) 0.032(3) 0.002(3) 0.014(3) 0.009(3) C22 0.034(4) 0.028(3) 0.025(3) 0.002(2) 0.016(3) -0.001(3) C23 0.030(4) 0.057(4) 0.024(3) 0.002(3) 0.012(3) 0.009(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ce Ce -0.2486 2.6331 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 N51 O51 Ce01 98.0(3) . . O61 Ce01 O61 48.9(3) 2_656 . O61 Ce01 O51 164.9(3) 2_656 . O61 Ce01 O51 124.04(17) . . O61 Ce01 O51 124.04(17) 2_656 2_656 O61 Ce01 O51 164.9(3) . 2_656 O51 Ce01 O51 66.21(16) . 2_656 O51 Ce01 O61A 170.08(14) . 2_656 O51 Ce01 O61A 123.37(13) 2_656 2_656 O51 Ce01 O61A 123.37(13) . . O51 Ce01 O61A 170.08(14) 2_656 . O61A Ce01 O61A 47.2(2) 2_656 . O61 Ce01 O52 123.2(3) 2_656 . O61 Ce01 O52 129.8(3) . . O51 Ce01 O52 47.73(13) . . O51 Ce01 O52 65.12(11) 2_656 . O61A Ce01 O52 131.2(2) 2_656 . O61A Ce01 O52 122.5(2) . . O61 Ce01 O52 129.8(3) 2_656 2_656 O61 Ce01 O52 123.2(3) . 2_656 O51 Ce01 O52 65.13(11) . 2_656 O51 Ce01 O52 47.73(13) 2_656 2_656 O61A Ce01 O52 122.5(2) 2_656 2_656 O61A Ce01 O52 131.2(2) . 2_656 O52 Ce01 O52 98.53(17) . 2_656 O61 Ce01 N11 76.3(3) 2_656 . O61 Ce01 N11 66.2(3) . . O51 Ce01 N11 114.63(14) . . O51 Ce01 N11 99.97(13) 2_656 . O61A Ce01 N11 68.1(3) 2_656 . O61A Ce01 N11 74.2(2) . . O52 Ce01 N11 159.61(14) . . O52 Ce01 N11 61.46(13) 2_656 . O61 Ce01 N11 66.2(3) 2_656 2_656 O61 Ce01 N11 76.3(3) . 2_656 O51 Ce01 N11 99.97(13) . 2_656 O51 Ce01 N11 114.64(14) 2_656 2_656 O61A Ce01 N11 74.2(2) 2_656 2_656 O61A Ce01 N11 68.1(3) . 2_656 O52 Ce01 N11 61.46(13) . 2_656 O52 Ce01 N11 159.61(14) 2_656 2_656 N11 Ce01 N11 138.8(2) . 2_656 O61 Ce01 N13 107.51(19) 2_656 2_656 O61 Ce01 N13 60.92(18) . 2_656 O51 Ce01 N13 71.92(13) . 2_656 O51 Ce01 N13 118.73(13) 2_656 2_656 O61A Ce01 N13 102.95(19) 2_656 2_656 O61A Ce01 N13 65.8(2) . 2_656 O52 Ce01 N13 113.06(13) . 2_656 O52 Ce01 N13 74.99(13) 2_656 2_656 N11 Ce01 N13 60.38(13) . 2_656 N11 Ce01 N13 115.00(14) 2_656 2_656 O61 Ce01 N13 60.92(18) 2_656 . O61 Ce01 N13 107.51(19) . . O51 Ce01 N13 118.73(14) . . O51 Ce01 N13 71.92(13) 2_656 . O61A Ce01 N13 65.8(2) 2_656 . O61A Ce01 N13 102.95(19) . . O52 Ce01 N13 74.99(13) . . O52 Ce01 N13 113.06(13) 2_656 . N11 Ce01 N13 115.01(14) . . N11 Ce01 N13 60.38(13) 2_656 . N13 Ce01 N13 168.33(19) 2_656 . N51 O52 Ce01 96.3(3) . . O53 N51 O52 122.4(5) . . O53 N51 O51 119.8(5) . . O52 N51 O51 117.8(5) . . C11 N11 C15 118.5(5) . . C11 N11 Ce01 121.4(3) . . C15 N11 Ce01 120.1(4) . . N11 C11 C12 123.3(5) . . N11 C11 C23 116.6(6) . 2_656 C12 C11 C23 120.0(6) . 2_656 C16 N12 C17 119.9(5) . . C16 N12 Ce01 119.4(4) . . C17 N12 Ce01 120.1(3) . . C11 C12 C13 117.7(7) . . C11 C12 H12A 121.1 . . C13 C12 H12A 121.1 . . C23 N13 C22 117.9(5) . . C23 N13 Ce01 119.5(4) . . C22 N13 Ce01 121.4(4) . . C14 C13 C12 119.7(6) . . C14 C13 H13A 120.1 . . C12 C13 H13A 120.1 . . C13 C14 C15 119.6(5) . . C13 C14 H14A 120.2 . . C15 C14 H14A 120.2 . . N11 C15 C14 121.0(6) . . N11 C15 C16 118.2(5) . . C14 C15 C16 120.7(5) . . N12 C16 C15 121.3(5) . . N12 C16 H16A 119.3 . . C15 C16 H16A 119.3 . . C22 C17 C18 119.3(6) . . C22 C17 N12 117.6(5) . . C18 C17 N12 123.1(6) . . C19 C18 C17 119.4(6) . . C19 C18 H18A 120.3 . . C17 C18 H18A 120.3 . . C18 C19 C20 121.4(5) . . C18 C19 H19A 119.3 . . C20 C19 H19A 119.3 . . C19 C20 C21 119.5(6) . . C19 C20 H20A 120.3 . . C21 C20 H20A 120.3 . . C22 C21 C20 120.2(6) . . C22 C21 H21A 119.9 . . C20 C21 H21A 119.9 . . C21 C22 C17 120.2(5) . . C21 C22 N13 123.9(6) . . C17 C22 N13 115.9(6) . . N13 C23 C11 120.9(6) . 2_656 N13 C23 H23 119.6 . . C11 C23 H23 119.6 2_656 . O61 N61 O61 119.3(9) . 2_656 O61 N61 O63 120.4(5) . . O61 N61 O63 120.4(5) 2_656 . O61 N61 Ce01 59.6(5) . . O61 N61 Ce01 59.6(5) 2_656 . O63 N61 Ce01 180.0 . . N61 O61 Ce01 95.9(5) . . N61A N61A O63A 115.3(4) 2_656 . N61A N61A O61A 77.3(14) 2_656 2_656 O63A N61A O61A 120.4(8) . 2_656 N61A N61A O61A 77.0(14) 2_656 . O63A N61A O61A 122.2(9) . . O61A N61A O61A 117.3(7) 2_656 . N61A N61A O63A 45.9(6) 2_656 2_656 O63A N61A O63A 69.4(10) . 2_656 O61A N61A O63A 101.3(7) 2_656 2_656 O61A N61A O63A 99.8(7) . 2_656 N61A O61A N61A 25.7(5) 2_656 . N61A O61A Ce01 95.1(4) 2_656 . N61A O61A Ce01 95.1(4) . . N61A O63A N61A 18.7(3) . 2_656 N61A O63A O63A 64.7(4) . 2_656 N61A O63A O63A 45.9(6) 2_656 2_656 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 O53 N51 1.248(6) . O51 N51 1.277(7) . O51 Ce01 2.657(4) . Ce01 O61 2.621(10) 2_656 Ce01 O61 2.621(10) . Ce01 O51 2.657(4) 2_656 Ce01 O61A 2.691(8) 2_656 Ce01 O61A 2.691(8) . Ce01 O52 2.704(4) . Ce01 O52 2.704(4) 2_656 Ce01 N11 2.713(5) . Ce01 N11 2.713(5) 2_656 Ce01 N13 2.736(5) 2_656 Ce01 N13 2.736(5) . O52 N51 1.256(6) . N11 C11 1.329(8) . N11 C15 1.348(6) . C11 C12 1.391(9) . C11 C23 1.479(7) 2_656 N12 C16 1.275(8) . N12 C17 1.419(8) . C12 C13 1.391(8) . C12 H12A 0.9300 . N13 C23 1.282(8) . N13 C22 1.432(6) . C13 C14 1.351(9) . C13 H13A 0.9300 . C14 C15 1.408(8) . C14 H14A 0.9300 . C15 C16 1.447(9) . C16 H16A 0.9300 . C17 C22 1.394(9) . C17 C18 1.413(7) . C18 C19 1.361(9) . C18 H18A 0.9300 . C19 C20 1.380(9) . C19 H19A 0.9300 . C20 C21 1.396(7) . C20 H20A 0.9300 . C21 C22 1.370(9) . C21 H21A 0.9300 . C23 C11 1.479(7) 2_656 C23 H23 0.9300 . N61 O61 1.257(5) . N61 O61 1.257(5) 2_656 N61 O63 1.263(8) . N61A N61A 0.561(11) 2_656 N61A O63A 1.256(8) . N61A O61A 1.261(8) 2_656 N61A O61A 1.263(8) . N61A O63A 1.580(11) 2_656 O61A N61A 1.261(8) 2_656 O63A N61A 1.580(11) 2_656 O63A O63A 1.64(3) 2_656 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_4 Ce01 O52 N51 O53 -176.5(4) . . Ce01 O52 N51 O51 3.7(4) . . Ce01 O51 N51 O53 176.4(4) . . Ce01 O51 N51 O52 -3.7(4) . . C15 N11 C11 C12 0.4(9) . . Ce01 N11 C11 C12 180.0(5) . . C15 N11 C11 C23 -179.8(5) . 2_656 Ce01 N11 C11 C23 -0.3(7) . 2_656 N11 C11 C12 C13 1.0(10) . . C23 C11 C12 C13 -178.7(6) 2_656 . C11 C12 C13 C14 -2.4(10) . . C12 C13 C14 C15 2.3(10) . . C11 N11 C15 C14 -0.6(9) . . Ce01 N11 C15 C14 179.9(4) . . C11 N11 C15 C16 176.6(6) . . Ce01 N11 C15 C16 -3.0(7) . . C13 C14 C15 N11 -0.8(9) . . C13 C14 C15 C16 -177.8(6) . . C17 N12 C16 C15 -179.5(5) . . Ce01 N12 C16 C15 8.8(8) . . N11 C15 C16 N12 -4.0(9) . . C14 C15 C16 N12 173.1(6) . . C16 N12 C17 C22 -149.9(5) . . Ce01 N12 C17 C22 21.7(6) . . C16 N12 C17 C18 31.2(8) . . Ce01 N12 C17 C18 -157.2(4) . . C22 C17 C18 C19 2.1(8) . . N12 C17 C18 C19 -179.0(5) . . C17 C18 C19 C20 -0.8(9) . . C18 C19 C20 C21 -1.2(9) . . C19 C20 C21 C22 1.9(9) . . C20 C21 C22 C17 -0.6(8) . . C20 C21 C22 N13 -179.3(5) . . C18 C17 C22 C21 -1.4(8) . . N12 C17 C22 C21 179.6(5) . . C18 C17 C22 N13 177.4(5) . . N12 C17 C22 N13 -1.5(7) . . C23 N13 C22 C21 -33.4(8) . . Ce01 N13 C22 C21 159.1(4) . . C23 N13 C22 C17 147.8(6) . . Ce01 N13 C22 C17 -19.7(6) . . C22 N13 C23 C11 178.6(5) . 2_656 Ce01 N13 C23 C11 -13.6(8) . 2_656 O61 N61 O61 Ce01 0.000(3) 2_656 . O63 N61 O61 Ce01 180.000(2) . . O63A N61A O61A N61A 111.9(9) . 2_656 O61A N61A O61A N61A -68.1(9) 2_656 2_656 O63A N61A O61A N61A 40.1(8) 2_656 2_656 N61A N61A O61A Ce01 91.3(8) 2_656 . O63A N61A O61A Ce01 -156.8(4) . . O61A N61A O61A Ce01 23.2(4) 2_656 . O63A N61A O61A Ce01 131.4(6) 2_656 . O61A N61A O63A N61A 90(2) 2_656 2_656 O61A N61A O63A N61A -90(2) . 2_656 O63A N61A O63A N61A -1(2) 2_656 2_656 N61A N61A O63A O63A 1(2) 2_656 2_656 O61A N61A O63A O63A 91.2(7) 2_656 2_656 O61A N61A O63A O63A -88.8(7) . 2_656