#------------------------------------------------------------------------------ #$Date: 2019-05-11 05:27:54 +0300 (Sat, 11 May 2019) $ #$Revision: 215044 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/55/10/1551018.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1551018 _cell_angle_alpha 90.000 _cell_angle_beta 105.876 _cell_angle_gamma 90.000 _cell_length_a 11.3335 _cell_length_b 32.6839 _cell_length_c 15.9743 _exptl_crystal_F_000 3216.00 _reflns_d_resolution_high 0.7705 _cod_data_source_file nr4002Isup2.hkl _cod_data_source_block I _shelx_title ' shelx in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 929.23 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 130.17 -11.87 11.87 o 2 0 0 170581.19 172011.03 2584.95 o 3 0 0 2140.53 1991.13 97.25 o 4 0 0 562447.00 581334.38 8552.96 o 5 0 0 1766.82 1782.82 144.66 o 6 0 0 407.66 124.29 101.77 o 7 0 0 11967.60 11671.70 330.44 o 8 0 0 18032.11 19000.51 824.18 o 9 0 0 8563.22 7950.80 454.54 o 10 0 0 8690.28 8431.63 377.93 o 11 0 0 3.80 -85.94 221.63 o 12 0 0 3314.90 3092.77 813.75 o 13 0 0 5177.31 5375.59 1103.39 o 14 0 0 103.30 -712.03 1149.94 o 2 1 0 951.29 1285.18 230.85 o 3 1 0 1852.21 1769.75 60.92 o 4 1 0 58520.55 59910.93 720.49 o 5 1 0 15001.78 15891.09 252.42 o 6 1 0 1236.85 1233.25 86.17 o 7 1 0 1463.16 1626.52 100.82 o 8 1 0 13578.12 14005.42 315.71 o 9 1 0 7417.48 7825.75 235.13 o 10 1 0 7106.75 7316.27 251.46 o 11 1 0 151.00 107.87 136.00 o 12 1 0 6782.40 6836.92 361.18 o 13 1 0 4251.48 4410.01 663.76 o 14 1 0 2107.86 1379.15 616.02 o 0 2 0 206.84 24.14 24.14 o 2 2 0 29.95 23.18 24.95 o 3 2 0 8404.95 8691.81 155.89 o 4 2 0 1807.16 1969.57 78.55 o 5 2 0 196642.94 197714.61 2173.14 o 6 2 0 2661.92 2452.27 101.47 o 7 2 0 9987.68 10247.39 230.31 o 8 2 0 10546.04 10488.55 253.83 o 9 2 0 24592.77 25385.47 487.09 o 10 2 0 3711.55 3522.39 192.60 o 11 2 0 3792.11 4317.62 260.12 o 12 2 0 12368.86 12236.41 499.54 o 13 2 0 1446.88 3003.66 2119.72 o 14 2 0 290.87 -265.72 508.66 o 1 3 0 874.94 523.91 95.61 o 2 3 0 8636.61 8052.20 147.23 o 3 3 0 197.92 137.93 45.55 o 4 3 0 557.27 547.62 58.98 o 5 3 0 33352.58 33038.98 498.47 o 6 3 0 23830.11 24226.76 341.31 o 7 3 0 1496.63 1649.27 104.80 o 8 3 0 9520.75 10203.97 237.54 o 9 3 0 32701.85 33134.58 642.06 o 10 3 0 378.79 344.73 149.64 o 11 3 0 5212.04 5013.45 317.06 o 12 3 0 1717.74 2145.62 322.82 o 13 3 0 4303.57 5967.85 1487.86 o 14 3 0 20.64 410.32 799.96 o 1 4 0 388.47 432.23 38.54 o 2 4 0 32141.31 32539.59 555.00 o 3 4 0 62.94 41.45 42.41 o 4 4 0 32407.71 31154.16 577.43 o 5 4 0 461.98 628.05 93.26 o 6 4 0 3116.72 3615.42 131.38 o 7 4 0 2892.11 2597.30 116.23 o 8 4 0 8320.83 8297.02 237.45 o 9 4 0 1161.06 1665.71 154.71 o 10 4 0 426.35 525.74 147.07 o 11 4 0 1.87 1339.13 846.03 o 12 4 0 663.41 945.65 258.52 o 13 4 0 3378.76 2458.50 1115.46 o 14 4 0 8.65 365.50 546.52 o 1 5 0 62.16 162.06 38.81 o 2 5 0 557.40 553.14 53.69 o 3 5 0 529.18 467.44 55.43 o 4 5 0 14945.50 14643.07 253.43 o 5 5 0 13621.07 13964.73 250.43 o 6 5 0 444.49 697.21 129.19 o 7 5 0 13284.62 13462.90 474.63 o 8 5 0 249.58 335.36 254.54 o 9 5 0 3181.07 2581.06 162.14 o 10 5 0 4414.23 4315.39 270.40 o 11 5 0 4047.91 3923.94 318.95 o 12 5 0 2451.49 2009.29 537.84 o 13 5 0 7.88 408.60 705.14 o 14 5 0 578.22 363.77 979.26 o 0 6 0 879.64 856.85 167.23 o 1 6 0 685.92 823.16 117.45 o 2 6 0 0.48 0.00 44.12 o 3 6 0 20316.40 19323.14 375.07 o 4 6 0 136.20 277.08 78.07 o 5 6 0 30754.11 32440.89 510.20 o 6 6 0 69.19 183.20 116.11 o 7 6 0 17.78 164.30 116.77 o 8 6 0 3691.51 3449.80 157.78 o 9 6 0 4011.72 4107.03 211.52 o 10 6 0 1102.16 989.57 238.25 o 11 6 0 225.32 527.36 202.43 o 12 6 0 949.70 1247.18 262.89 o 13 6 0 143.65 113.79 658.59 o 14 6 0 1175.62 499.97 977.54 o 1 7 0 1835.10 1772.63 88.69 o 2 7 0 10867.63 9911.77 252.15 o 3 7 0 3251.57 3015.80 105.42 o 4 7 0 4180.95 3981.05 128.04 o 5 7 0 26.25 273.89 102.32 o 6 7 0 863.55 996.96 111.42 o 7 7 0 644.55 624.05 142.38 o 8 7 0 2373.92 2227.01 211.73 o 9 7 0 473.38 513.67 135.86 o 10 7 0 3278.73 3072.33 206.15 o 11 7 0 566.42 726.20 211.62 o 12 7 0 2565.02 2438.39 320.67 o 0 8 0 845946.75 774124.38 25553.87 o 1 8 0 130.67 178.04 68.32 o 2 8 0 187.90 53.88 58.86 o 3 8 0 5234.30 4999.63 162.86 o 4 8 0 118516.39 121070.77 1759.41 o 5 8 0 2561.53 2753.55 129.18 o 6 8 0 270.02 448.55 121.41 o 7 8 0 1049.67 1244.31 125.77 o 8 8 0 1217.91 1107.36 226.77 o 9 8 0 1092.34 1028.54 149.56 o 10 8 0 4409.65 4411.70 350.66 o 11 8 0 59.81 230.89 196.91 o 12 8 0 41.26 638.60 386.19 o 13 8 0 2150.51 1913.51 468.22 o 1 9 0 269.72 289.09 57.82 o 2 9 0 54288.01 52382.81 1006.24 o 3 9 0 1002.30 959.12 114.93 o 4 9 0 37266.43 36885.32 697.18 o 5 9 0 10178.77 11128.24 370.22 o 6 9 0 4947.78 4843.56 204.34 o 7 9 0 146.99 355.31 112.37 o 8 9 0 4932.36 4535.05 260.76 o 9 9 0 10288.80 10485.56 315.88 o 10 9 0 25.84 155.25 171.81 o 11 9 0 8.81 329.03 325.24 o 12 9 0 195.15 270.46 292.89 o 13 9 0 4407.74 3910.15 1068.91 o 1 10 0 34632.49 31316.77 665.67 o 2 10 0 2867.55 2732.82 139.60 o 3 10 0 2738.42 2846.33 154.35 o 4 10 0 4235.47 4108.49 769.30 o 5 10 0 167967.69 172531.02 2666.29 o 6 10 0 64.12 205.55 86.67 o 7 10 0 7864.33 8437.35 273.11 o 8 10 0 9369.30 9150.35 357.14 o 9 10 0 22407.21 22502.81 562.41 o 10 10 0 374.39 298.86 163.62 o 11 10 0 3758.94 3514.04 346.22 o 12 10 0 9299.06 9626.77 1436.13 o 13 10 0 334.59 22.41 455.15 o 1 11 0 25063.54 22921.87 495.06 o 2 11 0 35878.59 33377.11 718.64 o 3 11 0 10018.44 10388.47 440.21 o 4 11 0 18538.97 17160.29 409.40 o 5 11 0 8076.73 8272.46 232.42 o 6 11 0 14930.52 16069.19 572.14 o 7 11 0 650.91 357.04 142.28 o 8 11 0 30046.19 31647.05 770.58 o 9 11 0 20566.29 20186.06 565.09 o 10 11 0 186.66 268.25 175.02 o 11 11 0 9103.59 9145.63 420.42 o 12 11 0 1696.65 1875.72 429.12 o 0 12 0 566302.06 543186.12 17855.99 o 1 12 0 2766.81 3095.54 187.10 o 2 12 0 1390.24 1302.62 104.58 o 3 12 0 413.75 488.11 177.92 o 4 12 0 191238.27 195230.23 3503.02 o 5 12 0 126.96 96.79 91.05 o 6 12 0 3870.91 3853.31 209.54 o 7 12 0 528.59 716.20 132.79 o 8 12 0 25871.13 27665.55 823.55 o 9 12 0 7929.80 7562.18 416.82 o 10 12 0 3520.95 3308.59 259.90 o 11 12 0 2675.11 2777.08 305.45 o 12 12 0 3339.50 4335.29 718.93 o 13 12 0 7743.20 6658.28 980.98 o 1 13 0 712.13 962.83 189.28 o 2 13 0 3846.38 3641.86 178.34 o 3 13 0 436.53 344.05 123.18 o 4 13 0 84993.83 84344.07 2400.86 o 5 13 0 509.87 728.99 178.58 o 6 13 0 4682.35 5414.71 688.53 o 7 13 0 8294.53 8142.01 368.29 o 8 13 0 15696.34 15335.66 445.04 o 9 13 0 1502.31 2154.11 205.73 o 10 13 0 1402.90 1292.95 203.48 o 11 13 0 1483.78 1658.72 216.74 o 12 13 0 3559.52 3567.55 510.78 o 13 13 0 3879.62 3763.60 717.20 o 0 14 0 3775.97 3715.33 405.15 o 1 14 0 78030.34 75438.15 1992.14 o 2 14 0 374.61 277.03 85.91 o 3 14 0 40700.07 36569.35 775.39 o 4 14 0 3099.75 3953.16 229.41 o 5 14 0 23638.36 24659.66 594.18 o 6 14 0 303.80 451.42 174.44 o 7 14 0 11631.37 11869.79 452.84 o 8 14 0 5547.33 5880.90 317.15 o 9 14 0 3074.28 3172.97 324.29 o 10 14 0 3133.49 3747.86 385.99 o 11 14 0 3540.33 3420.42 469.90 o 12 14 0 1834.64 2124.46 474.45 o 1 15 0 2788.15 2868.62 191.03 o 2 15 0 39654.61 37007.48 812.56 o 3 15 0 1362.89 1206.41 154.04 o 4 15 0 6021.54 6440.39 289.91 o 5 15 0 10607.69 10177.78 362.93 o 6 15 0 11899.08 11218.50 385.42 o 7 15 0 258.34 366.68 160.48 o 8 15 0 4821.63 5222.00 277.59 o 9 15 0 12667.50 13060.37 490.47 o 10 15 0 192.93 -55.84 175.88 o 11 15 0 3654.26 3409.26 658.59 o 12 15 0 288.18 136.20 636.17 o 13 15 0 2293.79 1167.18 663.76 o 0 16 0 2735.83 2715.38 453.43 o 1 16 0 78.34 122.55 144.17 o 2 16 0 3232.48 3370.52 306.08 o 3 16 0 237.85 242.06 95.27 o 4 16 0 29344.30 31152.87 724.45 o 5 16 0 368.66 450.71 164.23 o 6 16 0 1007.11 822.78 168.82 o 7 16 0 2370.79 2464.56 790.98 o 8 16 0 14449.39 14240.52 539.50 o 9 16 0 705.86 706.71 311.64 o 10 16 0 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9477.86 9312.44 373.53 o 4 19 0 21054.88 21009.48 660.92 o 5 19 0 82.20 10.45 139.11 o 6 19 0 619.69 601.29 199.80 o 7 19 0 776.41 498.39 192.31 o 8 19 0 19793.24 19749.15 991.15 o 9 19 0 1384.37 1616.44 365.54 o 10 19 0 206.46 309.29 332.49 o 11 19 0 538.01 1534.40 779.27 o 12 19 0 197.63 215.15 544.20 o 0 20 0 84595.42 93805.57 3627.40 o 1 20 0 2036.74 2086.91 250.86 o 2 20 0 18.66 7.55 197.58 o 3 20 0 347.90 396.31 161.47 o 4 20 0 26758.16 27658.45 1748.25 o 5 20 0 483.60 638.02 175.82 o 6 20 0 7009.15 6860.38 461.54 o 7 20 0 2775.48 2656.69 294.19 o 8 20 0 1533.89 1806.65 334.56 o 9 20 0 1624.59 1492.47 278.92 o 10 20 0 11339.90 11860.65 581.90 o 11 20 0 4183.74 3818.77 960.30 o 12 20 0 291.86 243.37 476.25 o 1 21 0 3365.21 3163.46 471.74 o 2 21 0 20791.30 21855.79 1194.77 o 3 21 0 2138.53 1811.69 178.29 o 4 21 0 37182.84 37990.00 1096.29 o 5 21 0 2137.41 2144.31 384.92 o 6 21 0 21683.80 21832.57 1085.29 o 7 21 0 4401.76 4181.62 438.77 o 8 21 0 3112.32 3385.24 388.55 o 9 21 0 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1555.26 1664.97 425.38 o 10 24 0 4.81 -496.53 677.55 o 11 24 0 162.11 -1113.74 1113.74 o 2 25 0 658.01 796.51 398.26 o 3 25 0 9477.60 10092.59 651.69 o 4 25 0 63.45 -68.96 231.02 o 5 25 0 5977.11 6137.62 596.52 o 6 25 0 282.18 539.05 306.80 o 7 25 0 1648.31 1760.26 429.29 o 8 25 0 2478.61 2125.75 470.67 o 9 25 0 1150.91 1032.15 362.79 o 10 25 0 386.85 86.41 406.48 o 11 25 0 7.17 158.61 817.20 o 1 26 0 10110.49 9616.75 777.55 o 2 26 0 1905.79 1662.15 687.90 o 3 26 0 31111.34 30848.12 1206.82 o 4 26 0 36.77 1106.84 599.97 o 5 26 0 24.58 128.61 229.70 o 6 26 0 4793.67 5591.40 715.48 o 7 26 0 9606.33 11070.13 815.48 o 8 26 0 867.03 918.92 560.32 o 9 26 0 53.72 89.65 489.63 o 10 26 0 839.85 901.68 608.59 o 11 26 0 4323.27 4081.71 616.77 o 1 27 0 4656.10 4499.77 565.49 o 2 27 0 4555.79 3978.66 350.45 o 3 27 0 1277.07 348.26 418.94 o 4 27 0 3239.45 3427.16 384.86 o 5 27 0 2551.61 2406.77 481.01 o 6 27 0 5723.56 6065.67 644.79 o 7 27 0 1656.54 1943.18 353.43 o 8 27 0 3202.70 3121.66 399.66 o 10 27 0 2968.62 4796.31 1779.22 o 1 28 0 46.19 -258.61 258.61 o 2 28 0 2969.94 2855.03 515.49 o 3 28 0 488.82 22.41 417.22 o 4 28 0 928.89 715.48 437.91 o 5 28 0 12.49 304.50 424.12 o 6 28 0 5127.84 5499.02 1601.64 o 7 28 0 3342.97 3396.38 634.45 o 8 28 0 1011.70 405.01 357.87 o 9 28 0 0.62 -113.79 479.29 o 10 28 0 5795.95 4585.97 867.20 o 1 29 0 427.16 414.31 294.81 o 2 29 0 18332.56 19080.06 1287.87 o 3 29 0 4041.01 4248.06 510.32 o 4 29 0 248.58 391.36 531.01 o 5 29 0 3713.53 4098.82 415.57 o 6 29 0 14251.72 15826.78 1165.46 o 7 29 0 786.43 998.23 408.60 o 8 29 0 335.53 651.37 381.43 o 9 29 0 183.06 -365.50 662.04 o 1 30 0 3041.17 3478.65 406.22 o 2 30 0 6.18 46.55 374.12 o 3 30 0 773.32 864.82 411.36 o 4 30 0 3684.43 3120.18 408.39 o 5 30 0 8298.75 8987.47 712.03 o 6 30 0 1078.00 615.49 524.11 o 7 30 0 1624.45 1825.35 435.32 o 8 30 0 12445.10 15102.68 1287.87 o 9 30 0 3422.95 2923.99 868.92 o 1 31 0 10578.18 10550.42 632.70 o 2 31 0 660.25 303.43 374.12 o 3 31 0 10084.57 11211.28 1583.54 o 4 31 0 4546.30 4346.08 457.82 o 5 31 0 794.66 756.86 481.01 o 6 31 0 699.43 339.49 302.36 o 7 31 0 5556.14 5610.06 749.96 o 8 31 0 1676.69 2663.66 789.61 o 9 31 0 35.18 960.30 686.17 o 0 32 0 6246.11 7068.61 753.41 o 1 32 0 2377.99 3197.21 435.16 o 2 32 0 768.02 1306.83 560.32 o 3 32 0 18119.30 18003.89 856.83 o 4 32 0 8563.36 9606.41 944.78 o 5 32 0 1648.94 2203.13 480.84 o 6 32 0 1287.38 1227.02 452.16 o 7 32 0 3777.17 3568.78 613.76 o 8 32 0 219.13 360.11 447.00 o 9 32 0 35.51 -434.46 822.37 o 1 33 0 880.15 809.76 543.08 o 2 33 0 22852.66 24551.70 1234.44 o 3 33 0 617.64 862.22 444.95 o 4 33 0 226.16 1036.15 598.25 o 5 33 0 940.24 1257.23 904.26 o 6 33 0 4189.51 5734.19 822.37 o 7 33 0 128.07 33.00 329.93 o 8 33 0 340.37 573.92 684.55 o 0 34 0 1515.97 2163.68 751.69 o 1 34 0 2852.92 2529.25 498.60 o 2 34 0 772.28 1689.16 903.40 o 3 34 0 4622.10 4847.62 648.49 o 4 34 0 1304.14 1025.35 398.89 o 5 34 0 2762.77 2676.03 503.30 o 6 34 0 1047.90 1599.92 617.21 o 7 34 0 41.49 1629.91 1055.12 o 8 34 0 6040.66 1901.63 1191.32 o 1 35 0 520.81 615.01 322.26 o 2 35 0 854.23 1166.67 385.91 o 3 35 0 4269.79 3897.46 536.17 o 4 35 0 356.96 530.92 384.50 o 5 35 0 54.28 -470.78 649.10 o 6 35 0 1481.77 857.45 436.16 o 7 35 0 4475.89 5566.51 676.45 o 0 36 0 539.27 -187.92 375.84 o 1 36 0 1414.97 924.52 663.79 o 2 36 0 546.67 252.38 352.49 o 3 36 0 716.37 270.48 396.05 o 4 36 0 1671.61 1121.09 530.15 o 5 36 0 8.17 -167.94 376.87 o 6 36 0 76.05 526.37 509.00 o 7 36 0 270.18 474.24 580.34 o 1 37 0 2330.75 2539.20 628.54 o 2 37 0 2.97 313.00 444.12 o 3 37 0 4646.79 4566.63 704.05 o 4 37 0 431.68 1317.29 1286.14 o 5 37 0 2333.09 2820.40 536.56 o 6 37 0 190.93 120.83 551.76 o 0 38 0 1142.02 1896.46 982.71 o 1 38 0 98.69 6.52 1017.19 o 2 38 0 1.62 589.26 562.90 o 3 38 0 1792.16 2166.41 889.61 o 4 38 0 39.41 455.33 1172.35 o 5 38 0 1133.41 1552.99 601.85 o 6 38 0 428.98 482.71 588.70 o 1 39 0 3205.54 3291.27 577.28 o 2 39 0 2642.95 2366.77 532.98 o 3 39 0 1186.25 958.59 579.11 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