#------------------------------------------------------------------------------ #$Date: 2019-12-03 12:50:33 +0200 (Tue, 03 Dec 2019) $ #$Revision: 244887 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/64/1556420.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556420 loop_ _publ_author_name 'Goldsworthy, J.' 'Thomas, S.D.' 'Tizzard, G.J.' 'Coles, S.J.' 'Owen, G.R.' _publ_section_title ; Adding to the Family of Copper Complexes Featuring Borohydride Ligands Based on 2-Mercaptopyridyl Units ; _journal_name_full Inorganics _journal_page_first 93 _journal_paper_doi 10.3390/inorganics7080093 _journal_volume 7 _journal_year 2019 _chemical_formula_moiety 'C23 H40 B Cu N P S' _chemical_formula_sum 'C23 H40 B Cu N P S' _chemical_formula_weight 467.94 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _cell_angle_alpha 96.9390(10) _cell_angle_beta 95.6170(10) _cell_angle_gamma 112.3730(10) _cell_formula_units_Z 2 _cell_length_a 8.16720(10) _cell_length_b 9.38370(10) _cell_length_c 17.2612(2) _cell_measurement_reflns_used 26623 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 70.1570 _cell_measurement_theta_min 2.5930 _cell_volume 1199.33(3) _computing_cell_refinement 'CrysAlisPro 1.171.40.40a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.40a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.40a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100(2) _diffrn_detector 'hybrid pixel detector' _diffrn_detector_area_resol_mean 10 _diffrn_detector_dtime 0.000 _diffrn_detector_type 'Rigaku, HyPix 6000' _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -83.00 -21.00 0.50 0.50 -- 5.00 49.00 90.00 124 2 \w 49.00 92.00 0.50 0.50 -- 5.00 49.00 90.00 86 3 \w -16.00 45.00 0.50 0.50 -- 5.00 49.00 90.00 122 4 \w 12.00 46.00 0.50 0.50 -- -42.00 53.00 111.68 68 5 \w -71.00 -45.00 0.50 0.50 -- -42.00 53.00 111.68 52 6 \w -99.00 -73.00 0.50 0.50 -- -52.30 59.00-150.00 52 7 \w 0.00 34.00 0.50 0.50 -- -52.30 59.00 -30.00 68 8 \w 6.00 37.00 0.50 0.50 -- -52.30 59.00 0.00 62 9 \w -121.00 -96.00 0.50 0.50 -- -52.30 59.00 -90.00 50 10 \w 10.00 36.00 0.50 0.50 -- -52.30 59.00 120.00 52 11 \w -93.00 -54.00 0.50 0.50 -- -52.30 59.00 60.00 78 12 \w -140.00-112.00 0.50 0.50 -- -52.30 59.00-150.00 56 13 \w -30.00 36.00 0.50 0.50 -- -52.30 59.00 -90.00 132 14 \w 4.00 32.00 0.50 0.50 -- -52.30 59.00-150.00 56 15 \w -88.00 -63.00 0.50 0.50 -- -52.30 59.00 -30.00 50 16 \w -137.00-111.00 0.50 0.50 -- -52.30 59.00 -30.00 52 17 \w -123.00 -97.00 0.50 0.50 -- -52.30 59.00 60.00 52 18 \w -10.00 37.00 0.50 0.50 -- -52.30 59.00 60.00 94 19 \w -60.00 -34.00 0.50 0.50 -- -52.30 59.00 -90.00 52 20 \w -150.00-125.00 0.50 0.50 -- -66.00 57.00 172.02 50 21 \w -12.00 23.00 0.50 0.50 -- -66.00 57.00 172.02 70 22 \w -23.00 11.00 0.50 0.50 -- -78.00 56.00 122.68 68 23 \w -110.00 -59.00 0.50 0.50 -- -90.00 57.00 -58.75 102 24 \w -159.00-114.00 0.50 0.50 -- -90.00 57.00 -58.75 90 25 \w -91.00 -1.00 0.50 0.50 -- -90.00 59.00 -20.28 180 26 \w -27.00 -1.00 0.50 0.50 -- -90.00 57.00 -13.81 52 27 \w -97.00 -44.00 0.50 0.50 -- -90.00 59.00 13.94 106 28 \w -39.00 -1.00 0.50 0.50 -- -90.00 59.00 13.94 76 29 \w -109.00 -47.00 0.50 0.50 -- -90.00 57.00 -13.81 124 30 \w -102.00 -1.00 0.50 0.50 -- -90.00 59.00-103.36 202 31 \w -31.00 -2.00 0.50 0.50 -- -90.00 59.00 116.61 58 32 \w -119.00 -45.00 0.50 0.50 -- -90.00 59.00 116.61 148 33 \w -165.00-122.00 0.50 0.50 -- -90.00 59.00-103.36 86 34 \w -156.00-130.00 0.50 0.50 -- -90.00 59.00 -20.28 52 35 \w -168.00-134.00 0.50 0.50 -- -90.00 59.00 116.61 68 36 \w -116.00 -3.00 0.50 0.50 -- -90.00 58.00-165.39 226 37 \w -30.00 -1.00 0.50 0.50 -- -90.00 57.00 59.54 58 38 \w -105.00 -71.00 0.50 0.50 -- -90.00 55.00-139.67 68 39 \w -175.00 -1.00 0.50 0.50 -- -90.00 58.00-123.71 348 40 \w -53.00 -3.00 0.50 0.50 -- -90.00 58.00 126.70 100 41 \w -178.00 -1.00 0.50 0.50 -- -90.00 57.00 69.81 354 42 \w -60.00 -1.00 0.50 0.50 -- -90.00 55.00-139.67 118 43 \w -75.00 -49.00 0.50 0.50 -- -90.00 57.00 59.54 52 44 \w -122.00 -60.00 0.50 0.50 -- -90.00 55.00 -89.23 124 45 \w -45.00 -1.00 0.50 0.50 -- -90.00 55.00 -89.23 88 46 \w -154.00 -2.00 0.50 0.50 -- -90.00 49.00 30.00 304 47 \w -109.00 -69.00 0.50 0.50 -- -90.00 58.00 126.70 80 48 \w -34.00 -1.00 0.50 0.50 -- -90.00 59.00-175.16 66 49 \w -115.00 -40.00 0.50 0.50 -- -90.00 59.00-175.16 150 50 \w -116.00 -90.00 0.50 0.50 -- -90.00 59.00 107.23 52 51 \w -79.00 -1.00 0.50 0.50 -- -90.00 59.00 107.23 156 52 \w -176.00 -1.00 0.50 0.50 -- -90.00 59.00 -42.19 350 53 \w -114.00 -1.00 0.50 0.50 -- -90.00 57.00 87.79 226 54 \w -28.00 -1.00 0.50 0.50 -- -90.00 58.00 159.07 54 55 \w -177.00 -39.00 0.50 0.50 -- -90.00 58.00 159.07 276 56 \w -164.00-128.00 0.50 0.50 -- -90.00 59.00-175.16 72 57 \w -26.00 -1.00 0.50 0.50 -- -90.00 57.00 -58.75 50 58 \w -175.00-124.00 0.50 0.50 -- -90.00 57.00 87.79 102 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_details 'Rigaku, AFC11 quarter \c goniometer' _diffrn_measurement_method 'profile data from \w-scans' _diffrn_measurement_specimen_support 'MiTeGen MicroLoop' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0187269000 _diffrn_orient_matrix_UB_12 0.1570367000 _diffrn_orient_matrix_UB_13 -0.0011538000 _diffrn_orient_matrix_UB_21 -0.0398669000 _diffrn_orient_matrix_UB_22 -0.0360546000 _diffrn_orient_matrix_UB_23 -0.0909594000 _diffrn_orient_matrix_UB_31 -0.2017832000 _diffrn_orient_matrix_UB_32 -0.0807292000 _diffrn_orient_matrix_UB_33 0.0034761000 _diffrn_radiation_collimation 'Varimax focusing mirrors' _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0278 _diffrn_reflns_av_unetI/netI 0.0131 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 30937 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 70.033 _diffrn_reflns_theta_min 2.611 _diffrn_source 'Rotating anode' _diffrn_source_current 30.0 _diffrn_source_power 1.2 _diffrn_source_target Cu _diffrn_source_type 'Rigaku 007 HF' _diffrn_source_voltage 40.0 _exptl_absorpt_coefficient_mu 2.773 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.69591 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.40a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.296 _exptl_crystal_description block _exptl_crystal_F_000 500 _exptl_crystal_recrystallization_method 'The material was recrystallised from ether and hexane' _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.04 _refine_diff_density_max 0.330 _refine_diff_density_min -0.364 _refine_diff_density_rms 0.046 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.052 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 285 _refine_ls_number_reflns 4471 _refine_ls_number_restraints 37 _refine_ls_restrained_S_all 1.050 _refine_ls_R_factor_all 0.0239 _refine_ls_R_factor_gt 0.0236 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0289P)^2^+0.7424P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0625 _refine_ls_wR_factor_ref 0.0628 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 4402 _reflns_number_total 4471 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file Inorganics-2019-7-93-2.cif _cod_data_source_block 2 _cod_database_code 1556420 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.897 _shelx_estimated_absorpt_t_min 0.635 _reflns_odcompleteness_completeness 98.63 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 69.95 _shelx_res_file ; TITL 2019ncs0140z_a.res in P-1 2019ncs0140z.res created by SHELXL-2018/3 at 10:41:32 on 27-Feb-2019 REM Old TITL 2019ncs0140z in P-1 REM SHELXT solution in P-1: R1 0.086, Rweak 0.006, Alpha 0.025 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C23 N2 S2 Cu CELL 1.54178 8.1672 9.3837 17.2612 96.939 95.617 112.373 ZERR 2 0.0001 0.0001 0.0002 0.001 0.001 0.001 LATT 1 SFAC C H B N P S Cu UNIT 46 80 2 2 2 2 2 SADI N1A C1A N1B C1B SADI 0.04 Cu1 C1A Cu1 C1B SADI Cu1 S1A Cu1 S1B SADI S1A C1A S1B C1B SADI 0.04 S1A N1A S1B N1B SADI 0.04 H1Bc H1Ba H1Bc H1Bb H1Ba H1Bb H1Aa H1Ab H1Aa H1Ac H1Ab H1Ac SADI B1B H1Bc B1B H1Ba B1B H1Bb B1A H1Aa B1A H1Ab B1A H1Ac SADI B1A N1A B1B N1B SADI 0.04 B1A C1A B1B C1B EADP C1B N1A EADP C1A N1B EXYZ C1B N1A EXYZ C1A N1B L.S. 7 PLAN 20 SIZE 0.04 0.12 0.18 TEMP -173(2) BIND N1B B1B BIND N1A B1A BIND C1B S1B BIND C1B N1B BIND C1A S1A BIND C1A N1A FREE Cu1 B1A FREE Cu1 B1B BOND $H CONF MORE -1 list 4 fmap 2 53 acta REM REM REM WGHT 0.028900 0.742400 FVAR 0.62695 0.79463 CU1 7 0.598896 0.309341 0.317374 11.00000 0.01697 0.01839 = 0.01553 0.00267 -0.00022 0.00881 PART 1 S1A 6 0.900814 0.410677 0.338448 21.00000 0.01440 0.02832 = 0.02191 0.00887 0.00393 0.00838 PART 0 PART 2 S1B 6 0.573563 0.194158 0.428139 -21.00000 0.02404 0.02451 = 0.01626 0.00664 0.00107 0.00925 PART 0 P1 5 0.412704 0.326035 0.222294 11.00000 0.01354 0.01336 = 0.01377 0.00229 0.00099 0.00549 PART 1 C1A 1 0.936795 0.326087 0.418195 21.00000 0.02411 0.02373 = 0.01589 -0.00150 0.00006 0.01333 PART 0 PART 2 C1B 1 0.801867 0.234871 0.452729 -21.00000 0.02506 0.01968 = 0.01521 0.00013 -0.00046 0.01245 PART 0 PART 1 N1A 4 0.801867 0.234871 0.452729 21.00000 0.02506 0.01968 = 0.01521 0.00013 -0.00046 0.01245 PART 0 PART 2 N1B 4 0.936795 0.326087 0.418195 -21.00000 0.02411 0.02373 = 0.01589 -0.00150 0.00006 0.01333 PART 0 C2 1 1.114245 0.350185 0.447123 11.00000 0.02576 0.03917 = 0.02328 -0.00185 0.00011 0.01575 PART 1 AFIX 43 H2A 2 1.209874 0.417206 0.424533 21.00000 -1.20000 AFIX 43 PART 0 PART 2 H2B 2 1.209874 0.417206 0.424533 -21.00000 -1.20000 AFIX 0 PART 0 C3 1 1.151641 0.279297 0.506896 11.00000 0.03257 0.05003 = 0.02424 -0.00630 -0.00901 0.02662 AFIX 43 H3 2 1.271771 0.294748 0.525068 11.00000 -1.20000 AFIX 0 C4 1 1.010850 0.183696 0.540999 11.00000 0.04868 0.04201 = 0.01920 0.00166 -0.00566 0.03051 AFIX 43 H4 2 1.033650 0.132749 0.582565 11.00000 -1.20000 AFIX 0 C5 1 0.840149 0.164564 0.513744 11.00000 0.03873 0.02795 = 0.01881 0.00386 0.00188 0.01868 PART 1 AFIX 43 H5A 2 0.744538 0.100805 0.537517 21.00000 -1.20000 AFIX 43 PART 0 PART 2 H5B 2 0.744538 0.100805 0.537517 -21.00000 -1.20000 AFIX 0 PART 0 C6 1 0.505992 0.355090 0.129241 11.00000 0.01468 0.01551 = 0.01510 0.00257 0.00186 0.00622 AFIX 13 H6 2 0.422879 0.380673 0.092362 11.00000 -1.20000 AFIX 0 C7 1 0.690062 0.493409 0.145188 11.00000 0.01703 0.01732 = 0.01852 0.00217 0.00265 0.00454 AFIX 23 H7A 2 0.677235 0.588918 0.169554 11.00000 -1.20000 H7B 2 0.773194 0.471455 0.182928 11.00000 -1.20000 AFIX 0 C8 1 0.768713 0.521727 0.068800 11.00000 0.01777 0.02105 = 0.02086 0.00681 0.00397 0.00616 AFIX 23 H8A 2 0.690745 0.552281 0.032718 11.00000 -1.20000 H8B 2 0.888706 0.608706 0.081050 11.00000 -1.20000 AFIX 0 C9 1 0.784513 0.374855 0.028152 11.00000 0.02022 0.02744 = 0.02014 0.00722 0.00657 0.01206 AFIX 23 H9A 2 0.828790 0.393757 -0.022590 11.00000 -1.20000 H9B 2 0.872486 0.350798 0.061914 11.00000 -1.20000 AFIX 0 C10 1 0.603792 0.235677 0.012747 11.00000 0.02592 0.02156 = 0.02043 0.00024 0.00696 0.00986 AFIX 23 H10A 2 0.619222 0.140817 -0.010675 11.00000 -1.20000 H10B 2 0.519887 0.255092 -0.025778 11.00000 -1.20000 AFIX 0 C11 1 0.523438 0.207418 0.088967 11.00000 0.02238 0.01604 = 0.02141 0.00294 0.00657 0.00816 AFIX 23 H11A 2 0.601106 0.177467 0.125540 11.00000 -1.20000 H11B 2 0.403745 0.120060 0.076441 11.00000 -1.20000 AFIX 0 C12 1 0.201189 0.149463 0.193291 11.00000 0.01563 0.01366 = 0.01724 0.00296 0.00160 0.00490 AFIX 13 H12 2 0.235283 0.061021 0.174509 11.00000 -1.20000 AFIX 0 C13 1 0.106415 0.107168 0.265096 11.00000 0.01764 0.01864 = 0.01833 0.00601 0.00304 0.00677 AFIX 23 H13A 2 0.190746 0.097601 0.307399 11.00000 -1.20000 H13B 2 0.070220 0.192044 0.285753 11.00000 -1.20000 AFIX 0 C14 1 -0.059639 -0.047005 0.242998 11.00000 0.01891 0.02065 = 0.02713 0.01026 0.00335 0.00521 AFIX 23 H14A 2 -0.021908 -0.133880 0.228357 11.00000 -1.20000 H14B 2 -0.122153 -0.067473 0.289348 11.00000 -1.20000 AFIX 0 C15 1 -0.188434 -0.041808 0.174062 11.00000 0.01693 0.02053 = 0.03309 0.00933 -0.00078 0.00162 AFIX 23 H15A 2 -0.289825 -0.145191 0.158860 11.00000 -1.20000 H15B 2 -0.237526 0.036492 0.190844 11.00000 -1.20000 AFIX 0 C16 1 -0.094542 0.000448 0.102940 11.00000 0.02197 0.02189 = 0.02443 0.00459 -0.00542 0.00046 AFIX 23 H16A 2 -0.179294 0.008443 0.060279 11.00000 -1.20000 H16B 2 -0.055889 -0.083141 0.082776 11.00000 -1.20000 AFIX 0 C17 1 0.068798 0.156114 0.125616 11.00000 0.01932 0.01878 = 0.01901 0.00536 -0.00219 0.00274 AFIX 23 H17A 2 0.029021 0.240910 0.142138 11.00000 -1.20000 H17B 2 0.129650 0.180179 0.079069 11.00000 -1.20000 AFIX 0 C18 1 0.343330 0.490965 0.247129 11.00000 0.01502 0.01511 = 0.01574 0.00188 0.00162 0.00627 AFIX 13 H18 2 0.230084 0.446779 0.269875 11.00000 -1.20000 AFIX 0 C19 1 0.480622 0.617308 0.313096 11.00000 0.02073 0.01842 = 0.01805 -0.00140 -0.00135 0.00796 AFIX 23 H19A 2 0.503919 0.567984 0.358144 11.00000 -1.20000 H19B 2 0.595064 0.667136 0.293142 11.00000 -1.20000 AFIX 0 C20 1 0.411784 0.742014 0.341223 11.00000 0.02661 0.02086 = 0.02226 -0.00356 0.00072 0.01076 AFIX 23 H20A 2 0.304652 0.694045 0.366458 11.00000 -1.20000 H20B 2 0.505181 0.824723 0.381358 11.00000 -1.20000 AFIX 0 C21 1 0.363285 0.815342 0.272920 11.00000 0.02581 0.01664 = 0.02881 -0.00051 0.00205 0.01056 AFIX 23 H21A 2 0.473315 0.874858 0.251997 11.00000 -1.20000 H21B 2 0.310742 0.889428 0.292468 11.00000 -1.20000 AFIX 0 C22 1 0.229434 0.690386 0.206628 11.00000 0.02238 0.01894 = 0.02521 0.00329 0.00082 0.01107 AFIX 23 H22A 2 0.206719 0.740501 0.161816 11.00000 -1.20000 H22B 2 0.114372 0.639300 0.225885 11.00000 -1.20000 AFIX 0 C23 1 0.299616 0.566628 0.178099 11.00000 0.01853 0.01535 = 0.01810 0.00233 0.00007 0.00670 AFIX 23 H23A 2 0.408926 0.615857 0.154445 11.00000 -1.20000 H23B 2 0.208111 0.485060 0.136846 11.00000 -1.20000 AFIX 0 PART 1 B1A 3 0.597696 0.201753 0.420742 21.00000 0.03609 0.02372 = 0.02207 0.01059 0.00494 0.01002 PART 0 PART 2 B1B 3 0.878338 0.382376 0.339566 -21.00000 0.03573 PART 0 PART 1 H1AA 2 0.562370 0.137806 0.355886 21.00000 -1.50000 H1AB 2 0.585808 0.321887 0.422068 21.00000 -1.50000 PART 0 PART 2 H1BA 2 0.797814 0.457631 0.353815 -21.00000 -1.50000 H1BB 2 0.793599 0.275038 0.291983 -21.00000 -1.50000 PART 0 PART 1 H1AC 2 0.516347 0.130207 0.463121 21.00000 -1.50000 PART 0 PART 2 H1BC 2 1.015719 0.454826 0.323416 -21.00000 -1.50000 HKLF 4 REM 2019ncs0140z_a.res in P-1 REM wR2 = 0.0628, GooF = S = 1.052, Restrained GooF = 1.050 for all data REM R1 = 0.0236 for 4402 Fo > 4sig(Fo) and 0.0239 for all 4471 data REM 285 parameters refined using 37 restraints END WGHT 0.0289 0.7424 REM Highest difference peak 0.330, deepest hole -0.364, 1-sigma level 0.046 Q1 1 0.5990 0.4248 0.1367 11.00000 0.05 0.33 Q2 1 0.4949 0.3197 0.2599 11.00000 0.05 0.31 Q3 1 0.4151 0.5591 0.2803 11.00000 0.05 0.27 Q4 1 0.2773 0.2260 0.2038 11.00000 0.05 0.27 Q5 1 0.1388 0.1553 0.1595 11.00000 0.05 0.27 Q6 1 -0.1268 -0.0440 0.2093 11.00000 0.05 0.26 Q7 1 0.6861 0.3028 0.0225 11.00000 0.05 0.26 Q8 1 0.3672 0.4189 0.2341 11.00000 0.05 0.25 Q9 1 -0.0089 0.0821 0.1159 11.00000 0.05 0.25 Q10 1 0.5084 0.2722 0.1081 11.00000 0.05 0.24 Q11 1 0.0198 0.0288 0.2525 11.00000 0.05 0.24 Q12 1 0.7184 0.5040 0.1064 11.00000 0.05 0.24 Q13 1 0.3209 0.5243 0.2138 11.00000 0.05 0.24 Q14 1 0.4648 0.3368 0.1654 11.00000 0.05 0.23 Q15 1 0.5653 0.2249 0.0504 11.00000 0.05 0.23 Q16 1 0.1537 0.1356 0.2284 11.00000 0.05 0.23 Q17 1 0.3032 0.7537 0.2377 11.00000 0.05 0.22 Q18 1 1.0246 0.3375 0.4381 11.00000 0.05 0.21 Q19 1 0.3806 0.7675 0.3043 11.00000 0.05 0.21 Q20 1 -0.1392 -0.0206 0.1391 11.00000 0.05 0.20 ; _shelx_res_checksum 90327 _shelx_hkl_file ; 0 0 1 159.68 3.43 0 0 -2 1698.55 32.50 0 0 2 1646.01 32.50 0 0 -3 9.05 0.63 0 0 3 10.15 0.70 0 0 3 9.40 0.46 0 0 -4 187.68 4.56 0 0 4 178.42 3.99 0 0 4 172.83 4.16 0 0 4 182.00 4.61 0 0 5 722.29 14.69 0 0 5 714.94 15.56 0 0 5 678.32 14.58 0 0 5 713.63 14.95 0 0 -6 639.95 13.48 0 0 6 594.18 12.68 0 0 6 596.60 12.57 0 0 6 603.58 13.03 0 0 -6 619.95 13.65 0 0 6 598.64 13.75 0 0 7 0.63 0.39 0 0 -7 0.90 0.50 0 0 7 0.45 0.20 0 0 7 0.51 0.41 0 0 7 -0.07 0.59 0 0 8 798.62 16.74 0 0 -8 783.14 16.78 0 0 -8 772.61 16.98 0 0 8 771.89 16.30 0 0 8 787.00 16.72 0 0 8 769.56 18.10 0 0 -8 845.99 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6.06 0 -4 -7 189.89 5.21 0 -4 -7 193.56 5.13 0 -4 -8 21.79 1.38 0 -4 -8 17.83 1.34 0 4 8 21.78 1.67 0 4 8 19.96 1.42 0 4 8 20.79 1.26 0 4 8 21.91 1.58 0 4 8 20.06 1.50 0 -4 -8 20.13 1.30 0 -4 -8 22.29 1.49 0 -4 -8 22.14 1.22 0 -4 -8 19.06 1.16 0 -4 -9 48.61 2.23 0 -4 -9 50.94 2.45 0 -4 -9 55.66 2.59 0 4 9 50.84 2.35 0 4 9 49.27 2.59 0 -4 -9 47.55 2.20 0 -4 -9 47.59 1.99 0 4 9 51.15 2.57 0 4 9 50.28 2.41 0 -4 -9 49.93 2.46 0 4 9 52.64 2.51 0 4 10 163.43 5.40 0 4 10 163.08 5.12 0 4 10 171.18 5.20 0 4 10 152.90 4.92 0 -4 -10 153.60 4.87 0 -4 -10 166.95 5.27 0 -4 -10 171.26 5.90 0 -4 -10 158.72 4.85 0 -4 -11 3.17 0.65 0 -4 -11 2.96 0.58 0 4 11 2.62 0.60 0 4 11 5.75 0.83 0 -4 -11 3.50 0.77 0 4 11 3.17 0.76 0 -4 -11 3.81 0.89 0 4 11 5.93 0.86 0 -4 -12 735.20 17.86 0 -4 -12 686.76 16.48 0 -4 -12 767.15 17.13 0 4 12 750.73 16.52 0 -4 -12 695.24 16.22 0 4 12 741.97 16.77 0 4 12 717.79 16.41 0 4 12 735.36 17.05 0 -4 -13 20.66 1.46 0 4 13 22.71 1.58 0 4 13 21.00 1.63 0 -4 -13 21.43 1.66 0 -4 -13 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3.10 0 -5 8 95.42 3.27 0 -5 8 94.70 2.98 0 -5 7 13.46 0.97 0 -5 7 12.39 0.90 0 -5 7 13.37 0.95 0 -5 7 13.06 0.90 0 -5 7 12.97 0.95 0 -5 7 12.89 0.99 0 -5 7 12.52 1.00 0 5 -7 12.86 1.28 0 5 -7 13.20 1.49 0 -5 6 128.63 3.79 0 -5 6 135.04 3.84 0 -5 6 132.07 3.77 0 -5 6 129.55 3.90 0 5 -6 144.36 4.73 0 5 -6 127.62 4.48 0 5 -6 138.94 5.08 0 -5 6 134.46 3.97 0 -5 6 136.66 3.82 0 -5 6 130.59 3.87 0 -5 6 129.26 3.70 0 -5 6 138.28 3.98 0 5 -5 49.42 2.77 0 -5 5 50.00 1.89 0 -5 5 50.23 1.98 0 -5 5 48.86 1.98 0 -5 5 45.84 1.69 0 -5 5 46.84 1.89 0 -5 5 47.44 1.83 0 5 -5 54.93 2.52 0 -5 5 48.98 2.01 0 -5 5 47.84 1.85 0 5 -5 47.63 2.38 0 -5 5 45.69 1.84 0 -5 4 57.81 2.02 0 -5 4 60.03 2.23 0 -5 4 54.74 2.03 0 5 -4 55.59 3.00 0 -5 4 58.22 2.14 0 -5 4 59.09 2.07 0 -5 4 53.62 2.01 0 -5 4 56.43 2.04 0 -5 4 61.04 2.25 0 5 -4 55.20 2.55 0 -5 4 62.37 2.19 0 5 -4 62.52 2.57 0 -5 3 6.24 0.63 0 5 -3 6.02 0.82 0 -5 3 5.32 0.64 0 -5 3 5.10 0.57 0 -5 3 5.25 0.55 0 5 -3 4.72 0.69 0 -5 3 4.97 0.56 0 -5 3 5.20 0.56 0 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79.38 2.94 0 -6 -5 85.46 3.34 0 -6 -5 80.74 3.06 0 -6 -5 84.20 3.04 0 -6 -5 79.42 2.99 0 -6 -5 76.32 3.15 0 -6 -5 75.56 2.82 0 6 5 88.12 3.89 0 6 5 80.96 3.50 0 6 5 78.33 3.31 0 -6 -6 298.35 8.00 0 6 6 329.26 8.69 0 6 6 369.04 9.69 0 -6 -6 312.94 8.75 0 -6 -6 348.20 8.85 0 6 6 346.48 9.19 0 6 6 334.17 9.08 0 -6 -6 321.05 8.43 0 -6 -6 334.35 8.44 0 -6 -6 346.08 8.41 0 -6 -7 28.67 1.73 0 6 7 35.22 2.20 0 -6 -7 29.92 2.00 0 -6 -7 31.41 1.71 0 6 7 33.28 2.22 0 -6 -7 33.13 1.79 0 6 7 32.59 1.86 0 -6 -7 34.37 2.03 0 6 7 34.52 2.22 0 -6 -7 32.98 1.89 0 -6 -8 5.24 0.75 0 6 8 8.36 0.96 0 -6 -8 6.38 0.98 0 6 8 7.73 0.88 0 6 8 7.51 1.10 0 6 8 8.07 1.20 0 6 8 9.39 1.19 0 6 8 8.08 1.02 0 -6 -8 7.14 0.84 0 -6 -8 6.72 0.93 0 -6 -8 8.20 0.99 0 -6 -8 8.10 0.86 0 -6 -9 4.33 0.68 0 6 9 4.09 0.84 0 6 9 4.02 0.68 0 -6 -9 4.66 0.77 0 -6 -9 4.78 0.78 0 6 9 4.60 0.80 0 6 9 4.63 0.84 0 -6 -9 4.03 0.59 0 6 10 164.23 4.99 0 6 10 190.90 5.56 0 6 10 185.68 5.73 0 -6 -10 195.17 5.67 0 -6 -10 178.31 5.34 0 6 10 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210.81 5.83 0 7 -12 203.15 6.48 0 -7 12 225.40 6.05 0 -7 12 208.67 5.65 0 7 -12 238.61 7.23 0 -7 11 0.14 0.47 0 7 -11 0.72 0.66 0 7 -11 0.98 0.69 0 7 -11 -0.39 0.62 0 -7 11 0.49 0.43 0 -7 11 1.13 0.45 0 -7 11 0.42 0.34 0 7 -11 0.05 0.56 0 -7 10 1011.71 22.10 0 -7 10 972.58 21.67 0 -7 10 981.90 21.97 0 -7 10 1011.39 21.98 0 7 -10 1050.65 23.60 0 -7 10 1043.19 22.52 0 7 -10 1015.77 24.03 0 -7 10 991.65 22.06 0 -7 10 1019.56 21.79 0 -7 9 194.67 5.37 0 -7 9 203.00 5.81 0 -7 9 194.67 5.53 0 -7 9 197.79 5.65 0 7 -9 196.76 6.67 0 7 -9 193.37 7.16 0 -7 9 197.57 5.99 0 7 -9 210.06 6.73 0 -7 9 206.12 5.97 0 -7 9 195.97 5.57 0 -7 9 196.15 5.59 0 -7 9 206.41 5.58 0 -7 8 182.46 5.51 0 -7 8 183.15 5.12 0 7 -8 184.26 6.04 0 7 -8 175.18 6.07 0 -7 8 165.46 5.06 0 -7 8 166.76 4.97 0 -7 8 167.16 4.99 0 7 -8 169.72 6.63 0 -7 8 167.75 4.86 0 -7 8 172.16 5.32 0 -7 8 174.49 5.27 0 -7 7 54.04 2.31 0 -7 7 51.77 2.50 0 -7 7 56.71 2.65 0 -7 7 54.05 2.45 0 7 -7 54.82 2.86 0 7 -7 53.43 3.45 0 -7 7 53.67 2.31 0 7 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1 52.66 2.54 0 -7 1 50.83 2.40 0 7 -1 52.04 2.87 0 7 -1 49.59 2.92 0 7 -1 47.80 2.76 0 -7 1 55.27 2.28 0 -7 1 52.04 2.35 0 7 -1 52.16 2.48 0 -7 1 55.61 2.54 0 7 0 3.60 0.88 0 -7 0 3.33 0.61 0 -7 0 3.22 0.56 0 -7 0 3.69 0.71 0 -7 0 3.49 0.71 0 7 0 3.48 0.91 0 -7 0 3.63 0.69 0 -7 0 3.33 0.67 0 -7 0 3.98 0.59 0 7 0 3.40 0.93 0 -7 -1 357.11 8.98 0 -7 -1 358.38 8.79 0 -7 -1 370.37 9.35 0 -7 -1 380.07 9.45 0 7 1 375.61 10.17 0 7 1 354.18 9.87 0 -7 -1 361.31 9.35 0 -7 -1 372.87 9.31 0 -7 -1 348.97 8.73 0 7 1 357.24 9.85 0 -7 -2 3.02 0.68 0 -7 -2 3.22 0.66 0 -7 -2 2.58 0.51 0 -7 -2 2.81 0.69 0 -7 -2 2.74 0.54 0 7 2 2.40 0.74 0 7 2 2.63 0.84 0 -7 -2 3.60 0.66 0 -7 -3 129.02 4.06 0 7 3 134.03 4.86 0 7 3 133.57 4.88 0 -7 -3 141.91 4.48 0 -7 -3 132.58 4.02 0 7 3 127.40 4.83 0 -7 -3 135.93 4.52 0 -7 -4 83.07 3.19 0 7 4 79.44 3.48 0 7 4 76.27 3.44 0 7 4 84.07 3.99 0 -7 -4 83.51 3.27 0 -7 -5 1.26 0.49 0 7 5 2.39 0.90 0 7 5 2.20 0.67 0 7 5 1.90 0.75 0 -7 -5 1.77 0.54 0 -7 -5 1.67 0.64 0 -7 -6 296.42 7.88 0 7 6 363.63 9.39 0 7 6 304.56 8.01 0 -7 -6 338.03 8.38 0 -7 -6 302.98 8.32 0 7 6 339.13 8.60 0 7 6 315.93 8.67 0 -7 -6 350.35 8.87 0 7 7 110.08 4.21 0 -7 -7 99.55 3.39 0 -7 -7 115.66 4.03 0 7 7 88.36 3.15 0 -7 -7 92.16 3.39 0 7 7 102.25 3.65 0 -7 -7 107.64 3.60 0 7 7 103.18 3.56 0 7 7 103.14 3.84 0 -7 -8 1.64 0.47 0 -7 -8 0.53 0.47 0 7 8 0.48 0.45 0 7 8 -0.12 0.49 0 -7 -8 0.32 0.34 0 7 9 195.49 5.70 0 -7 -9 176.93 5.14 0 -7 -9 195.17 5.62 0 7 9 181.67 5.25 0 -7 -9 192.08 5.59 0 -7 -10 126.09 3.86 0 -7 -10 133.93 4.20 0 7 10 124.69 3.83 0 7 10 130.78 4.14 0 -7 -10 133.91 4.14 0 -7 -11 15.02 1.06 0 -7 -11 12.50 0.91 0 7 11 13.32 0.90 0 7 11 11.47 0.96 0 -7 -11 13.89 1.06 0 -7 -12 288.28 6.84 0 7 12 279.79 6.52 0 -7 -12 287.11 6.61 0 -8 16 7.34 0.65 0 8 -16 12.95 0.91 0 -8 15 0.47 0.27 0 8 -15 0.66 0.41 0 8 -15 1.08 0.43 0 -8 15 0.47 0.31 0 -8 14 40.37 1.87 0 -8 14 45.49 1.90 0 8 -14 41.48 2.09 0 8 -14 45.36 2.21 0 8 -14 37.71 1.69 0 8 -13 26.23 1.58 0 -8 13 29.73 1.61 0 -8 13 27.52 1.56 0 8 -13 28.01 1.80 0 8 -12 5.15 0.90 0 8 -12 4.60 0.77 0 8 -12 4.12 0.81 0 -8 12 5.44 0.76 0 8 -12 4.31 0.78 0 -8 12 5.04 0.73 0 -8 12 4.35 0.56 0 8 -11 114.10 4.19 0 8 -11 109.39 4.24 0 -8 11 104.43 3.36 0 8 -11 101.91 4.02 0 8 -11 93.94 3.78 0 -8 11 95.29 3.57 0 8 -10 79.77 3.68 0 -8 10 76.85 2.69 0 8 -10 73.03 3.39 0 -8 10 87.15 3.24 0 -8 10 82.48 3.02 0 -8 10 83.33 3.25 0 8 -10 84.43 3.54 0 8 -10 77.04 3.54 0 -8 9 155.32 4.89 0 -8 9 146.84 4.71 0 -8 9 143.04 4.36 0 8 -9 153.80 5.41 0 -8 9 143.03 4.58 0 8 -9 133.67 5.10 0 -8 9 151.30 5.06 0 8 -9 147.14 5.08 0 8 -9 147.29 5.37 0 8 -8 183.11 6.26 0 -8 8 172.24 5.37 0 -8 8 178.77 5.29 0 8 -8 189.61 5.87 0 8 -8 161.39 5.98 0 -8 8 186.97 5.63 0 -8 8 180.85 5.42 0 8 -8 191.42 6.25 0 -8 7 127.67 4.60 0 8 -7 125.81 4.79 0 8 -7 120.88 4.34 0 -8 7 123.69 4.15 0 -8 7 125.70 4.18 0 8 -7 108.11 4.72 0 -8 7 120.93 4.25 0 -8 7 129.22 4.37 0 8 -6 3.51 0.69 0 -8 6 4.25 0.77 0 -8 6 3.56 0.69 0 8 -6 4.78 0.99 0 -8 6 5.05 0.82 0 -8 6 4.26 0.82 0 8 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269.66 7.27 0 -8 -1 249.58 6.59 0 8 1 265.32 7.87 0 -8 -1 267.97 7.36 0 -8 -1 270.60 7.32 0 8 2 302.60 8.90 0 8 2 333.30 9.61 0 -8 -2 337.54 8.64 0 -8 -2 325.49 8.70 0 -8 -2 337.77 8.74 0 8 2 326.48 9.12 0 -8 -3 20.74 1.58 0 -8 -3 22.50 1.53 0 8 3 23.39 1.97 0 8 3 21.61 1.75 0 8 3 19.61 1.64 0 -8 -3 20.80 1.54 0 -8 -4 217.46 6.23 0 8 4 223.48 6.97 0 8 4 214.43 6.60 0 8 4 211.40 6.40 0 -8 -4 222.14 6.17 0 8 5 125.11 4.21 0 -8 -5 133.92 4.22 0 8 5 115.82 3.90 0 8 5 123.46 3.90 0 8 5 127.89 4.52 0 8 5 133.41 4.76 0 -8 -5 128.79 4.13 0 8 6 11.70 1.25 0 -8 -6 9.01 0.90 0 -8 -6 10.67 0.98 0 8 6 10.99 0.99 0 -8 -6 13.15 1.20 0 8 6 10.65 0.95 0 -8 -6 9.76 0.86 0 -8 -7 0.19 0.30 0 -8 -7 0.38 0.29 0 8 7 0.24 0.36 0 8 7 0.20 0.42 0 -8 -8 137.19 3.98 0 8 8 139.23 3.89 0 -8 -8 137.38 3.90 0 -8 -8 154.06 4.50 0 8 8 155.58 4.52 0 8 9 4.44 0.63 0 -8 -9 5.73 0.68 0 8 9 5.04 0.50 0 -8 -9 4.69 0.53 0 8 10 35.02 1.50 0 -8 -10 37.65 1.58 0 9 -13 26.51 1.44 0 -9 13 24.97 1.21 0 -9 12 40.73 1.79 0 9 -12 54.86 2.32 0 9 -12 51.19 2.07 0 9 -12 45.41 1.93 0 -9 11 98.98 3.21 0 9 -11 102.16 3.36 0 9 -11 94.89 3.25 0 -9 11 101.66 3.00 0 -9 10 28.76 1.44 0 9 -10 31.53 1.88 0 9 -10 24.55 1.44 0 9 -10 30.75 1.86 0 -9 10 27.06 1.47 0 -9 10 30.51 1.65 0 9 -10 27.82 1.67 0 -9 9 371.46 9.17 0 -9 9 385.63 9.23 0 -9 9 371.30 8.85 0 9 -9 389.06 9.99 0 -9 9 413.00 9.55 0 9 -9 364.72 9.74 0 9 -9 409.15 9.99 0 9 -8 23.02 1.67 0 -9 8 22.47 1.33 0 -9 8 24.37 1.48 0 -9 8 25.02 1.55 0 9 -8 22.45 1.72 0 -9 8 22.72 1.41 0 9 -7 89.96 3.52 0 -9 7 89.05 3.25 0 -9 7 88.83 3.26 0 9 -7 82.38 3.60 0 -9 7 80.55 2.98 0 -9 7 85.47 3.08 0 -9 6 61.17 2.59 0 9 -6 58.52 3.00 0 -9 6 58.47 2.58 0 9 -6 60.81 2.77 0 9 -6 53.18 2.88 0 -9 6 56.17 2.34 0 -9 6 56.94 2.49 0 -9 5 143.94 4.61 0 -9 5 146.38 4.56 0 -9 5 140.77 4.29 0 9 -5 149.48 5.27 0 -9 4 161.43 4.92 0 9 -4 172.19 5.70 0 -9 4 156.62 5.01 0 -9 4 160.36 4.65 0 9 -4 161.91 5.63 0 -9 3 0.62 0.44 0 -9 3 1.06 0.50 0 -9 3 0.38 0.28 0 -9 3 0.82 0.47 0 9 -3 0.63 0.62 0 9 -3 0.68 0.38 0 9 -3 0.77 0.61 0 -9 3 1.08 0.39 0 9 -3 0.64 0.52 0 9 -2 141.24 5.01 0 -9 2 146.90 4.59 0 -9 2 125.05 3.91 0 9 -2 128.13 4.43 0 -9 2 136.62 4.11 0 9 -1 105.64 3.92 0 -9 1 121.02 4.00 0 -9 1 109.38 3.66 0 -9 1 116.59 4.00 0 9 -1 95.15 4.15 0 9 -1 108.23 4.28 0 -9 0 10.24 1.01 0 -9 0 12.08 1.12 0 9 0 10.23 1.20 0 -9 0 11.06 1.11 0 9 0 11.01 1.16 0 9 0 9.62 1.26 0 -9 -1 156.45 4.69 0 -9 -1 148.72 4.68 0 -9 -1 139.98 4.50 0 9 1 137.91 4.67 0 9 1 147.52 4.93 0 -9 -2 239.82 6.47 0 -9 -2 226.39 6.37 0 9 2 221.62 6.50 0 9 2 230.77 6.62 0 -9 -2 248.76 6.44 0 -9 -3 7.63 0.84 0 9 3 8.27 1.04 0 -9 -3 8.05 0.88 0 9 3 8.44 0.93 0 9 3 6.36 0.73 0 -9 -3 8.83 0.91 0 9 3 6.78 0.67 0 9 3 7.71 0.94 0 9 4 249.64 6.51 0 9 4 257.44 6.80 0 -9 -4 259.22 6.57 0 -9 -4 250.14 6.65 0 9 4 262.51 6.99 0 -9 -4 232.06 6.37 0 9 5 0.24 0.29 0 -9 -5 0.02 0.26 0 9 5 0.03 0.39 0 -9 -6 51.55 1.92 0 9 6 56.12 2.24 0 -9 -7 22.98 1.23 0 9 7 21.50 1.23 0 -10 10 80.21 2.46 0 -10 9 0.34 0.24 0 10 -9 0.87 0.32 0 10 -9 0.26 0.27 0 10 -8 290.13 7.21 0 -10 8 289.33 6.87 0 -10 8 310.26 7.02 0 -10 7 19.57 1.02 0 10 -7 18.62 1.25 0 -10 7 19.23 1.12 0 10 -7 18.82 1.07 0 10 -6 0.27 0.31 0 10 -6 1.12 0.49 0 -10 6 0.70 0.32 0 -10 6 0.97 0.37 0 10 -5 17.64 1.22 0 -10 5 34.66 1.53 0 10 -4 14.90 1.21 0 -10 4 13.74 1.00 0 10 -3 80.78 2.97 0 10 -3 64.34 2.27 0 -10 3 74.63 2.63 0 -10 3 85.79 2.81 0 10 -3 60.26 2.58 0 10 -2 194.25 5.32 0 -10 2 206.09 5.11 0 -10 1 50.68 2.04 0 10 -1 44.46 1.79 0 -10 1 48.61 2.01 0 10 -1 46.15 2.10 0 10 0 67.66 2.35 0 10 0 69.48 2.60 0 -10 0 71.57 2.52 0 10 0 63.90 2.58 0 -10 0 74.01 2.56 0 10 1 233.91 5.58 0 -10 -1 240.64 5.78 0 10 1 199.11 5.72 0 -10 -1 242.97 5.76 0 10 1 196.13 5.36 0 10 1 227.33 5.75 0 -10 -2 4.96 0.57 0 10 2 5.35 0.57 0 -10 -2 5.73 0.57 1 -10 -5 169.29 4.44 1 -10 -4 5.46 0.61 1 -10 -4 6.39 0.59 -1 10 4 6.24 0.69 -1 10 4 5.82 0.61 1 -10 -3 205.72 5.28 -1 10 3 194.22 5.36 1 -10 -3 190.40 5.00 -1 10 3 195.66 5.08 1 -10 -3 211.79 5.25 -1 10 3 202.74 5.34 -1 10 2 19.41 1.29 1 -10 -2 20.55 1.23 -1 10 2 20.59 1.33 -1 10 2 19.89 1.23 1 -10 -2 21.14 1.24 1 -10 -2 21.32 1.19 -1 10 1 59.90 2.51 -1 10 1 54.56 2.39 1 -10 -1 57.42 2.22 1 -10 -1 57.13 2.31 1 -10 -1 55.33 2.22 1 -10 0 95.35 3.12 -1 10 0 95.81 3.37 1 -10 0 86.78 2.90 -1 10 0 81.76 2.76 -1 10 0 79.03 3.10 1 -10 0 90.95 3.14 -1 10 -1 5.85 0.65 -1 10 -1 5.53 0.79 -1 10 -1 7.39 0.93 1 -10 1 6.88 0.80 1 -10 1 6.61 0.68 1 -10 1 6.73 0.78 -1 10 -2 6.98 0.92 -1 10 -2 4.99 0.74 1 -10 2 6.18 0.76 1 -10 2 5.68 0.62 1 -10 2 6.78 0.79 1 -10 3 54.16 2.26 -1 10 -3 43.58 2.13 -1 10 -4 6.77 0.74 1 -10 4 7.30 0.74 -1 10 -4 6.40 0.78 1 -10 4 8.14 0.86 1 -10 4 8.18 0.87 1 -10 5 1.80 0.45 1 -10 5 2.15 0.49 -1 10 -5 1.86 0.58 -1 10 -5 1.49 0.44 -1 10 -5 0.82 0.39 1 -10 6 60.34 2.31 1 -10 6 58.56 2.33 -1 10 -6 58.38 2.39 -1 10 -6 58.87 2.57 1 -10 7 1.24 0.38 -1 10 -7 2.28 0.56 1 -10 7 1.45 0.40 1 -10 7 1.73 0.44 -1 10 -7 1.37 0.50 -1 10 -8 174.49 4.70 1 -10 8 169.81 4.53 1 -10 8 188.37 4.64 1 -10 8 176.92 4.37 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296.59 8.22 1 -9 8 288.45 7.61 -1 9 -8 294.62 7.77 -1 9 -8 286.57 8.00 -1 9 -8 291.30 8.17 1 -9 8 285.46 7.43 1 -9 8 302.40 7.68 1 -9 8 267.97 7.22 1 -9 9 279.87 7.41 -1 9 -9 311.04 8.21 -1 9 -9 297.36 7.78 1 -9 9 258.01 7.12 1 -9 9 290.51 7.19 1 -9 9 296.59 7.59 -1 9 -9 274.34 7.67 -1 9 -9 294.41 7.98 1 -9 10 72.06 2.66 -1 9 -10 66.42 2.71 -1 9 -10 71.36 3.14 1 -9 10 69.58 2.40 1 -9 10 73.19 2.82 -1 9 -10 72.33 2.97 1 -9 10 64.56 2.54 -1 9 -10 73.24 3.01 -1 9 -11 86.21 3.20 1 -9 11 71.41 2.70 -1 9 -11 81.30 3.01 1 -9 11 84.34 2.77 -1 9 -11 86.62 3.36 1 -9 11 85.41 3.01 -1 9 -11 74.23 2.66 1 -9 12 1.87 0.44 1 -9 12 2.37 0.51 -1 9 -12 2.09 0.59 1 -9 12 2.21 0.37 -1 9 -12 2.56 0.62 -1 9 -13 10.80 0.95 1 -9 13 7.60 0.71 -1 9 -14 0.97 0.37 1 -9 14 0.93 0.30 1 -9 14 0.76 0.28 1 -8 -11 47.60 1.81 -1 8 11 48.79 1.88 1 -8 -11 45.46 1.75 1 -8 -10 29.75 1.52 -1 8 10 32.25 1.61 1 -8 -10 31.87 1.54 -1 8 9 13.73 1.13 1 -8 -9 12.26 1.01 1 -8 -9 13.34 1.07 -1 8 8 3.56 0.57 1 -8 -8 5.31 0.77 -1 8 8 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-9 1.06 0.45 -1 3 9 0.63 0.28 1 -3 -9 2.30 0.52 1 -3 -9 2.06 0.47 -1 3 9 0.94 0.42 -1 3 8 3.21 0.50 -1 3 8 3.28 0.58 -1 3 8 3.17 0.84 -1 3 8 3.30 0.67 1 -3 -8 4.66 0.62 -1 3 8 3.00 0.45 1 -3 -8 2.99 0.55 -1 3 8 2.92 0.57 1 -3 -8 2.75 0.50 -1 3 8 4.28 0.61 1 -3 -8 2.83 0.52 1 -3 -8 2.01 0.50 1 -3 -8 2.81 0.45 1 -3 -7 106.05 3.36 -1 3 7 110.51 3.50 1 -3 -7 106.82 3.28 -1 3 7 101.79 3.20 -1 3 7 98.00 3.05 -1 3 7 103.92 3.94 -1 3 7 104.52 3.42 -1 3 7 107.90 3.40 -1 3 7 101.19 3.14 1 -3 -7 108.82 3.30 1 -3 -7 100.26 3.04 1 -3 -7 99.93 3.32 -1 3 7 101.98 3.04 -1 3 6 268.04 6.17 -1 3 6 236.87 6.60 -1 3 6 217.59 5.76 1 -3 -6 234.61 5.97 -1 3 6 228.55 5.71 -1 3 6 232.49 5.88 1 -3 -6 251.06 6.06 1 -3 -6 243.75 6.74 1 -3 -6 252.67 5.98 -1 3 6 239.95 6.13 1 -3 -6 219.83 5.89 1 -3 -6 240.47 5.30 -1 3 6 232.51 6.22 1 -3 -6 237.05 5.91 1 -3 -6 224.21 5.73 1 -3 -5 819.18 17.96 -1 3 5 822.29 18.56 -1 3 5 866.07 18.10 1 -3 -5 820.26 17.99 1 -3 -5 882.94 18.82 1 -3 -5 894.11 17.99 -1 3 5 821.88 18.00 -1 3 5 857.29 18.40 -1 3 4 1370.85 28.30 1 -3 -4 1297.39 27.64 -1 3 4 1392.98 28.36 1 -3 -4 1428.93 28.56 1 -3 -4 1313.55 27.30 -1 3 4 1382.54 27.91 1 -3 -3 23.04 0.88 1 -3 -3 24.97 1.38 -1 3 3 24.28 1.17 1 -3 -3 25.19 1.19 -1 3 3 26.93 1.32 -1 3 2 1897.02 40.50 1 -3 -2 2061.36 40.89 1 -3 -2 1910.00 40.50 -1 3 2 2057.50 40.64 -1 3 2 2034.52 40.04 -1 3 1 1104.17 22.86 -1 3 1 1081.18 22.45 -1 3 0 6.46 0.42 1 -3 0 5.95 0.53 1 -3 0 6.14 0.52 -1 3 -1 1821.64 37.98 1 -3 1 1896.24 37.32 1 -3 1 1902.43 37.38 -1 3 -1 1752.77 37.19 1 -3 1 1782.87 36.93 1 -3 1 1883.07 37.27 1 -3 1 1929.77 37.31 -1 3 -2 50.86 2.01 1 -3 2 50.42 1.65 1 -3 2 52.91 1.75 1 -3 2 50.74 1.54 -1 3 -3 306.88 7.46 1 -3 3 308.86 7.08 1 -3 3 321.21 7.29 -1 3 -3 325.34 7.21 -1 3 -4 1402.63 30.06 1 -3 4 1442.45 29.67 -1 3 -4 1508.73 30.02 1 -3 5 12.00 0.94 -1 3 -5 10.94 0.87 -1 3 -5 9.91 0.86 1 -3 5 12.87 0.79 -1 3 -6 3110.80 63.00 1 -3 6 3170.28 62.73 -1 3 -6 3101.39 63.03 1 -3 6 3013.80 62.48 1 -3 6 3170.19 63.56 1 -3 6 3046.29 62.55 -1 3 -6 3248.34 63.45 1 -3 7 2047.03 42.04 1 -3 7 2077.66 43.13 1 -3 7 2074.39 41.84 1 -3 7 2113.23 41.92 -1 3 -7 2150.27 43.03 -1 3 -7 1973.78 42.04 -1 3 -7 2099.49 42.38 -1 3 -7 1981.07 42.23 -1 3 -7 2238.41 43.09 1 -3 7 1990.19 41.96 1 -3 7 2068.02 42.17 -1 3 -7 2040.23 42.46 1 -3 8 6.80 0.71 -1 3 -8 6.48 0.66 -1 3 -8 5.97 0.68 1 -3 8 6.22 0.62 1 -3 8 10.03 0.79 -1 3 -8 6.98 0.77 1 -3 8 6.38 0.63 1 -3 8 6.51 0.69 -1 3 -8 5.62 0.74 -1 3 -8 9.46 1.01 -1 3 -8 5.47 0.72 1 -3 8 6.86 0.62 1 -3 8 6.22 0.90 1 -3 8 7.47 0.66 1 -3 9 660.92 14.33 1 -3 9 671.25 16.03 1 -3 9 649.89 13.96 -1 3 -9 614.15 14.76 -1 3 -9 644.46 14.58 -1 3 -9 604.48 14.35 1 -3 9 682.48 14.60 1 -3 9 686.43 14.67 1 -3 9 673.99 14.42 -1 3 -9 676.62 14.95 1 -3 9 662.55 14.15 -1 3 -9 688.77 15.09 1 -3 9 671.39 14.46 1 -3 10 5.10 0.64 -1 3 -10 4.56 0.65 1 -3 10 5.28 0.67 -1 3 -10 4.37 0.56 1 -3 10 4.37 0.65 -1 3 -10 4.80 0.72 1 -3 10 4.82 0.66 -1 3 -10 6.71 0.86 1 -3 10 5.06 0.60 -1 3 -10 5.25 0.79 1 -3 10 5.55 1.05 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118.16 4.12 1 -3 17 126.75 3.97 1 -3 18 273.52 6.64 -1 3 -18 269.31 7.03 -1 3 -18 263.83 6.75 1 -3 18 265.22 6.42 1 -3 18 274.10 6.46 1 -3 19 13.79 0.96 1 -3 19 13.73 0.93 -1 3 -19 12.47 1.01 -1 3 -19 14.77 1.16 -1 3 -19 13.71 1.12 1 -3 19 13.05 0.98 1 -3 20 130.48 3.57 1 -3 20 127.43 3.43 -1 3 -20 127.58 3.70 -1 3 -20 128.31 3.59 -1 3 -20 130.16 3.80 -1 2 19 4.62 0.50 1 -2 -19 4.69 0.63 -1 2 19 4.85 0.57 1 -2 -19 4.61 0.61 1 -2 -19 4.95 0.54 -1 2 18 0.18 0.29 1 -2 -18 0.29 0.37 -1 2 18 0.41 0.27 1 -2 -18 0.62 0.34 1 -2 -18 0.22 0.28 1 -2 -18 0.86 0.43 1 -2 -17 3.23 0.70 1 -2 -17 2.73 0.59 -1 2 17 4.19 0.60 1 -2 -17 3.49 0.64 1 -2 -17 4.21 0.74 1 -2 -17 3.80 0.59 -1 2 17 3.58 0.63 -1 2 16 0.37 0.36 1 -2 -16 0.16 0.50 1 -2 -16 0.62 0.43 -1 2 16 0.50 0.43 -1 2 16 0.37 0.40 1 -2 -16 0.57 0.50 1 -2 -16 0.66 0.45 -1 2 16 0.92 0.38 1 -2 -15 1.77 0.51 1 -2 -15 1.36 0.61 -1 2 15 0.98 0.42 1 -2 -15 0.51 0.46 -1 2 15 1.13 0.51 1 -2 -15 1.00 0.50 -1 2 15 1.17 0.47 1 -2 -15 1.16 0.58 -1 2 15 0.78 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2 -6 2090.93 42.39 1 -2 7 581.14 12.45 1 -2 7 549.91 12.19 -1 2 -7 582.17 13.45 -1 2 -7 563.85 12.80 1 -2 7 564.87 12.50 -1 2 -7 592.54 12.81 -1 2 -7 548.15 12.56 1 -2 7 599.04 12.45 1 -2 7 576.14 13.50 -1 2 -7 572.00 13.07 1 -2 7 572.53 11.84 -1 2 -7 579.81 12.60 1 -2 7 594.75 12.65 -1 2 -7 599.54 12.84 -1 2 -8 993.91 20.78 1 -2 8 985.25 20.21 -1 2 -8 952.70 20.52 -1 2 -8 990.02 21.57 1 -2 8 1002.11 20.39 -1 2 -8 902.86 20.17 1 -2 8 947.19 19.97 1 -2 8 938.77 20.38 -1 2 -8 965.05 20.80 -1 2 -8 953.61 20.59 -1 2 -8 976.51 21.13 1 -2 8 956.91 19.58 -1 2 -8 972.64 20.52 1 -2 8 973.40 21.72 1 -2 8 1001.50 20.39 -1 2 -9 705.07 16.13 1 -2 9 767.78 16.23 1 -2 9 730.58 15.64 1 -2 9 790.87 16.24 1 -2 9 746.89 16.01 -1 2 -9 755.37 16.43 1 -2 9 737.06 17.73 -1 2 -9 791.10 16.69 -1 2 -9 718.06 15.82 1 -2 9 772.84 16.23 -1 2 -9 722.92 16.00 -1 2 -9 735.21 16.35 1 -2 10 181.43 4.89 1 -2 10 175.26 4.55 -1 2 -10 178.10 5.09 1 -2 10 185.33 4.91 -1 2 -10 166.60 4.53 -1 2 -10 178.09 5.09 1 -2 10 183.59 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2 -8 -12 0.90 0.31 2 -8 -11 0.53 0.26 2 -8 -11 0.28 0.26 -2 8 11 0.28 0.35 -2 8 10 3.26 0.64 2 -8 -10 2.95 0.48 -2 8 10 4.05 0.53 2 -8 -10 3.29 0.55 -2 8 9 1.27 0.55 2 -8 -9 0.59 0.41 2 -8 -9 1.37 0.40 -2 8 9 0.81 0.38 -2 8 8 22.83 1.38 -2 8 8 23.97 1.67 2 -8 -8 22.72 1.34 -2 8 8 23.95 1.52 2 -8 -8 22.56 1.54 2 -8 -7 290.19 7.35 -2 8 7 317.93 8.37 2 -8 -7 326.88 8.17 2 -8 -7 279.84 7.41 -2 8 7 298.20 8.03 -2 8 7 306.60 7.83 2 -8 -6 217.20 6.06 2 -8 -6 191.52 5.40 -2 8 6 198.73 5.82 -2 8 6 197.91 6.00 2 -8 -6 176.80 5.19 2 -8 -6 198.37 5.66 2 -8 -5 264.71 7.06 -2 8 5 278.89 7.70 2 -8 -5 274.95 7.51 2 -8 -5 258.93 6.72 -2 8 5 251.58 7.29 2 -8 -5 259.90 7.00 -2 8 4 232.20 7.02 2 -8 -4 227.73 6.32 -2 8 4 231.12 6.64 -2 8 4 226.77 6.89 2 -8 -4 221.71 6.05 2 -8 -4 214.02 6.12 2 -8 -4 233.24 6.70 -2 8 3 234.25 7.11 -2 8 3 232.33 7.06 -2 8 3 228.79 6.62 2 -8 -3 232.98 6.24 2 -8 -3 234.61 6.44 2 -8 -3 210.89 6.05 -2 8 2 44.51 2.61 2 -8 -2 41.08 1.90 2 -8 -2 44.67 2.24 -2 8 2 44.86 2.12 -2 8 2 42.19 2.25 -2 8 2 44.96 2.64 2 -8 -2 44.27 2.13 -2 8 1 29.67 1.84 2 -8 -1 32.77 1.78 -2 8 1 33.39 2.26 -2 8 1 32.20 2.23 -2 8 1 30.71 1.81 2 -8 -1 33.13 1.93 2 -8 -1 31.03 1.79 2 -8 -1 30.00 1.52 2 -8 -1 34.84 2.06 -2 8 0 36.15 2.44 2 -8 0 38.34 1.98 -2 8 0 33.85 1.95 2 -8 0 37.38 1.76 2 -8 0 38.51 2.16 2 -8 0 36.29 1.99 -2 8 0 35.14 2.27 2 -8 0 38.91 2.12 -2 8 0 38.72 2.11 2 -8 1 56.98 2.33 -2 8 -1 55.81 2.70 -2 8 -1 58.34 2.52 2 -8 1 57.11 2.67 2 -8 1 55.98 2.55 2 -8 1 59.67 2.68 -2 8 -1 57.52 2.95 -2 8 -1 51.38 2.41 2 -8 1 56.30 2.57 -2 8 -2 674.31 15.83 2 -8 2 638.24 14.83 2 -8 2 625.14 14.37 -2 8 -2 632.95 15.62 2 -8 2 674.44 15.04 2 -8 2 668.57 14.90 -2 8 -2 643.53 14.84 -2 8 -3 23.45 1.69 -2 8 -3 21.53 1.39 2 -8 3 25.98 1.55 2 -8 3 24.51 1.59 2 -8 3 23.35 1.64 -2 8 -3 22.82 1.86 2 -8 3 26.32 1.74 -2 8 -4 361.00 10.03 2 -8 4 347.53 8.61 -2 8 -4 349.64 9.90 2 -8 4 362.02 9.04 2 -8 4 366.06 9.08 -2 8 -4 368.15 9.59 2 -8 4 368.72 9.40 -2 8 -4 378.58 10.02 2 -8 5 66.27 2.55 -2 8 -5 67.33 3.25 2 -8 5 67.88 2.97 2 -8 5 69.12 3.00 2 -8 5 67.88 2.81 2 -8 5 65.92 2.62 -2 8 -5 67.04 3.31 -2 8 -5 65.65 3.29 -2 8 -5 68.58 3.17 2 -8 6 217.46 5.83 -2 8 -6 222.54 6.84 -2 8 -6 206.15 6.56 -2 8 -6 228.76 6.81 -2 8 -6 224.60 6.93 2 -8 6 219.58 6.32 -2 8 -7 194.32 6.38 2 -8 7 198.82 5.63 -2 8 -7 191.99 6.21 2 -8 7 205.91 6.04 -2 8 -7 213.47 6.62 -2 8 -7 210.87 6.70 -2 8 -8 2.20 0.76 -2 8 -8 2.51 0.73 2 -8 8 1.98 0.56 2 -8 8 2.61 0.57 -2 8 -8 2.19 0.82 -2 8 -8 1.83 0.66 2 -8 8 1.99 0.61 2 -8 9 148.15 4.52 2 -8 9 141.95 4.52 2 -8 9 140.12 4.65 -2 8 -9 142.98 4.91 -2 8 -9 149.89 5.34 -2 8 -9 134.09 4.55 -2 8 -9 147.97 5.30 -2 8 -10 225.19 6.40 2 -8 10 216.99 6.05 -2 8 -10 235.59 7.07 2 -8 10 220.03 5.97 2 -8 10 216.85 6.18 -2 8 -11 0.70 0.51 -2 8 -11 1.57 0.74 2 -8 11 0.51 0.36 -2 8 -11 0.61 0.43 2 -8 11 0.41 0.34 2 -8 11 0.77 0.44 2 -8 12 116.83 3.96 -2 8 -12 127.85 4.53 2 -8 12 122.83 3.88 -2 8 -12 134.88 4.79 2 -8 13 140.33 4.43 2 -8 13 149.81 4.17 -2 8 -13 145.47 4.31 -2 8 -13 156.94 5.17 -2 8 -13 153.99 4.87 2 -8 14 1.38 0.41 -2 8 -14 1.06 0.39 -2 8 -14 1.01 0.53 2 -8 15 287.99 7.02 -2 8 -15 271.84 6.95 2 -8 16 30.59 1.37 2 -8 16 34.81 1.46 2 -7 -14 141.42 3.78 -2 7 14 132.06 3.67 2 -7 -13 16.20 1.09 -2 7 13 16.50 1.09 2 -7 -13 14.36 0.91 2 -7 -12 0.78 0.35 2 -7 -12 0.54 0.37 2 -7 -12 0.75 0.33 -2 7 12 0.97 0.46 -2 7 11 0.97 0.48 -2 7 11 0.43 0.30 2 -7 -11 0.49 0.33 2 -7 -11 0.30 0.37 2 -7 -11 0.60 0.35 -2 7 10 155.15 4.97 2 -7 -10 158.42 4.84 -2 7 10 151.09 4.55 2 -7 -10 151.19 4.64 -2 7 10 145.74 4.27 2 -7 -10 148.91 4.52 2 -7 -10 148.30 4.81 2 -7 -9 69.34 2.92 -2 7 9 78.74 3.30 -2 7 9 73.27 2.95 2 -7 -9 71.30 2.99 2 -7 -9 69.06 2.75 -2 7 9 67.26 2.70 2 -7 -9 75.84 3.12 -2 7 8 121.36 4.29 -2 7 8 124.18 4.14 -2 7 8 135.33 4.69 2 -7 -8 131.74 4.35 2 -7 -8 117.10 3.95 2 -7 -8 129.12 4.39 2 -7 -7 53.71 2.35 -2 7 7 60.31 2.96 2 -7 -7 55.70 2.27 -2 7 7 58.00 2.61 -2 7 7 60.18 2.80 2 -7 -7 56.41 2.66 2 -7 -7 58.27 2.69 2 -7 -6 147.26 4.75 -2 7 6 146.59 4.94 2 -7 -6 150.42 4.84 2 -7 -6 141.07 4.33 2 -7 -6 135.16 4.24 -2 7 6 147.68 4.79 -2 7 5 347.03 9.29 2 -7 -5 336.16 8.78 -2 7 5 344.70 9.12 2 -7 -5 333.50 8.25 2 -7 -5 338.75 8.52 2 -7 -5 359.65 9.09 2 -7 -4 120.75 3.82 -2 7 4 128.44 4.71 2 -7 -4 122.59 4.09 2 -7 -4 118.25 3.94 2 -7 -4 128.01 4.37 -2 7 4 124.66 4.38 -2 7 4 126.21 4.58 2 -7 -3 127.30 3.97 2 -7 -3 134.15 4.50 -2 7 3 141.27 4.89 2 -7 -3 126.54 4.10 -2 7 3 125.02 4.37 -2 7 3 130.83 4.72 -2 7 3 125.86 4.01 2 -7 -3 119.79 4.03 -2 7 2 10.25 1.11 -2 7 2 10.10 1.00 -2 7 2 11.05 1.28 2 -7 -2 9.93 0.98 2 -7 -2 9.87 0.93 -2 7 2 10.72 1.27 2 -7 -2 11.48 0.93 2 -7 -2 8.92 0.87 -2 7 1 186.87 6.07 2 -7 -1 184.09 4.93 2 -7 -1 189.74 5.32 2 -7 -1 179.56 5.08 -2 7 1 176.59 5.45 2 -7 -1 191.86 5.46 2 -7 -1 194.05 5.28 -2 7 1 203.68 6.22 -2 7 1 190.67 5.34 -2 7 1 183.68 5.51 2 -7 0 75.02 2.58 2 -7 0 76.79 2.62 2 -7 0 77.73 2.90 -2 7 0 73.07 3.03 -2 7 0 70.61 2.88 2 -7 0 80.04 3.02 -2 7 0 72.47 2.93 -2 7 -1 2.92 0.60 -2 7 -1 3.02 0.80 2 -7 1 3.24 0.62 2 -7 1 2.96 0.51 2 -7 1 4.18 0.68 -2 7 -1 2.41 0.59 2 -7 2 10.68 1.03 2 -7 2 10.33 1.04 -2 7 -2 10.90 1.26 2 -7 2 9.86 0.89 -2 7 -2 10.43 1.09 -2 7 -2 11.84 1.25 -2 7 -3 1302.43 28.83 2 -7 3 1260.12 27.29 -2 7 -3 1230.37 28.73 2 -7 3 1333.60 28.07 -2 7 -3 1359.81 28.46 2 -7 3 1332.88 28.15 -2 7 -3 1366.97 28.75 2 -7 4 302.38 7.43 -2 7 -4 294.73 8.46 2 -7 4 299.35 7.97 -2 7 -4 311.69 8.39 -2 7 -4 313.93 8.59 -2 7 -4 307.95 8.60 2 -7 5 494.75 11.61 2 -7 5 526.14 12.28 -2 7 -5 526.56 12.82 2 -7 5 521.89 12.25 -2 7 -5 526.20 12.90 -2 7 -5 506.08 12.81 -2 7 -6 387.11 10.35 2 -7 6 384.87 9.48 -2 7 -6 422.76 10.77 2 -7 6 397.59 9.75 -2 7 -6 418.74 10.76 -2 7 -6 395.03 10.50 2 -7 7 231.61 6.21 -2 7 -7 215.09 6.70 2 -7 7 219.79 6.49 -2 7 -7 223.86 6.19 2 -7 7 239.64 6.43 -2 7 -7 239.27 7.27 -2 7 -7 228.57 6.94 -2 7 -7 242.90 7.24 2 -7 8 387.92 9.38 -2 7 -8 354.65 9.69 2 -7 8 374.51 9.65 -2 7 -8 376.16 9.75 2 -7 8 383.83 9.61 -2 7 -8 380.47 9.47 2 -7 8 386.94 9.58 -2 7 -8 374.35 10.00 -2 7 -9 1.37 0.54 -2 7 -9 2.01 0.59 2 -7 9 1.82 0.57 2 -7 9 2.56 0.63 -2 7 -9 1.47 0.61 -2 7 -9 1.60 0.53 -2 7 -9 3.00 0.86 2 -7 9 1.61 0.54 2 -7 9 2.81 0.48 2 -7 9 2.47 0.57 2 -7 10 6.37 0.86 -2 7 -10 5.36 0.85 2 -7 10 7.23 0.90 2 -7 10 6.54 0.80 2 -7 10 6.53 0.89 -2 7 -10 5.96 1.12 2 -7 10 5.85 0.67 -2 7 -10 5.00 0.86 -2 7 -10 6.35 0.86 -2 7 -10 5.65 1.02 2 -7 11 62.97 2.74 2 -7 11 61.85 2.52 -2 7 -11 64.05 3.11 -2 7 -11 63.07 2.86 2 -7 11 65.40 2.46 2 -7 11 68.10 2.91 -2 7 -11 73.58 3.58 2 -7 11 67.01 2.77 -2 7 -11 63.21 2.69 -2 7 -11 64.93 3.19 2 -7 12 139.45 4.45 2 -7 12 117.73 3.81 -2 7 -12 131.74 4.87 2 -7 12 140.51 4.55 2 -7 12 142.79 4.34 2 -7 12 130.83 4.00 -2 7 -12 141.27 4.67 -2 7 -12 157.77 5.53 -2 7 -12 144.18 4.98 2 -7 13 0.73 0.45 -2 7 -13 1.36 0.76 2 -7 13 0.76 0.35 -2 7 -13 0.97 0.51 2 -7 13 0.18 0.30 -2 7 -13 0.75 0.51 -2 7 -13 0.67 0.41 2 -7 14 265.58 6.92 2 -7 14 252.53 6.43 -2 7 -14 250.47 6.65 -2 7 -14 277.29 7.19 -2 7 -14 262.33 7.11 2 -7 14 243.59 6.26 2 -7 15 224.37 5.76 -2 7 -15 233.98 6.40 -2 7 -15 219.86 5.93 2 -7 16 32.40 1.59 -2 7 -16 32.43 1.68 2 -7 16 30.62 1.34 2 -7 17 114.42 3.20 -2 7 -17 116.19 3.32 2 -6 -16 1.73 0.36 -2 6 16 1.81 0.35 -2 6 15 377.94 8.64 2 -6 -15 375.58 8.63 -2 6 14 6.87 0.76 2 -6 -14 5.59 0.75 2 -6 -14 6.70 0.77 2 -6 -13 77.29 3.02 -2 6 13 82.65 3.06 2 -6 -13 78.46 3.13 2 -6 -12 211.23 6.09 -2 6 12 214.59 6.16 -2 6 12 195.30 5.34 2 -6 -12 205.98 5.60 -2 6 12 205.84 5.50 2 -6 -12 223.91 6.31 2 -6 -12 219.07 6.19 -2 6 11 2.16 0.48 -2 6 11 2.34 0.67 2 -6 -11 2.46 0.64 2 -6 -11 2.97 0.57 2 -6 -11 1.63 0.58 -2 6 11 2.41 0.53 2 -6 -10 36.58 1.93 -2 6 10 37.41 2.21 -2 6 10 37.42 1.98 2 -6 -10 35.91 2.06 -2 6 10 35.90 1.74 -2 6 10 35.77 1.82 -2 6 9 1.75 0.48 2 -6 -9 2.72 0.60 -2 6 9 2.09 0.69 2 -6 -9 2.59 0.62 -2 6 9 2.28 0.61 -2 6 9 2.50 0.58 -2 6 8 10.11 0.94 -2 6 8 11.02 1.14 2 -6 -8 10.36 1.07 -2 6 8 9.82 0.91 2 -6 -8 11.62 1.17 2 -6 -8 10.37 1.04 -2 6 8 11.46 1.09 -2 6 8 10.80 1.24 -2 6 7 1514.13 32.80 2 -6 -7 1593.87 33.39 2 -6 -7 1649.87 33.51 -2 6 7 1595.27 33.42 2 -6 -7 1528.61 32.70 -2 6 7 1623.55 33.73 -2 6 7 1471.23 32.79 -2 6 7 1678.52 34.26 2 -6 -7 1642.78 33.65 2 -6 -6 1240.27 25.99 2 -6 -6 1198.93 25.72 -2 6 6 1123.28 25.26 -2 6 6 1266.40 26.30 2 -6 -6 1296.04 26.03 -2 6 6 1293.48 26.67 2 -6 -6 1155.51 25.25 -2 6 6 1210.22 26.22 -2 6 6 1126.06 25.18 -2 6 6 1181.95 25.90 2 -6 -6 1202.31 25.79 -2 6 5 0.80 0.53 -2 6 5 0.87 0.41 -2 6 5 0.76 0.58 2 -6 -5 0.61 0.39 2 -6 -5 2.65 0.48 2 -6 -5 2.73 0.58 -2 6 5 0.46 0.34 2 -6 -5 0.22 0.25 2 -6 -5 0.34 0.32 2 -6 -4 397.60 9.27 -2 6 4 377.28 9.19 -2 6 4 429.98 10.56 2 -6 -4 396.34 9.45 2 -6 -4 405.12 9.47 2 -6 -4 400.57 9.59 -2 6 4 409.39 10.28 -2 6 4 396.95 9.97 -2 6 4 401.86 9.44 2 -6 -4 412.75 9.78 2 -6 -3 203.36 5.46 2 -6 -3 223.09 5.73 -2 6 3 208.50 5.99 -2 6 3 198.57 5.33 2 -6 -3 212.93 5.88 2 -6 -3 208.60 5.61 -2 6 3 220.46 6.37 -2 6 3 214.38 5.73 2 -6 -3 219.93 5.42 2 -6 -3 216.86 5.82 2 -6 -3 212.95 5.51 -2 6 2 230.25 6.48 2 -6 -2 236.66 6.09 2 -6 -2 241.72 6.16 -2 6 2 276.97 7.27 2 -6 -2 255.30 6.12 2 -6 -2 253.30 6.35 -2 6 2 218.98 5.81 -2 6 2 259.13 7.06 2 -6 -2 249.08 6.38 -2 6 2 243.71 6.42 -2 6 2 237.14 6.25 2 -6 -2 247.48 6.33 2 -6 -1 249.61 6.19 2 -6 -1 254.10 6.12 -2 6 1 263.21 7.25 2 -6 -1 270.78 6.65 -2 6 1 256.60 6.74 2 -6 -1 262.71 6.54 -2 6 1 264.57 6.66 -2 6 1 238.79 6.05 -2 6 1 241.05 6.61 2 -6 -1 256.87 6.45 2 -6 -1 261.75 6.47 -2 6 0 6.19 0.90 2 -6 0 7.62 0.80 -2 6 0 5.23 0.56 2 -6 0 6.16 0.69 2 -6 0 6.12 0.65 2 -6 0 6.06 0.65 2 -6 0 5.11 0.60 2 -6 0 6.47 0.60 -2 6 0 5.97 0.74 -2 6 -1 286.99 7.72 2 -6 1 267.71 6.86 2 -6 1 289.31 7.09 -2 6 -1 295.48 7.35 -2 6 -1 251.86 6.53 -2 6 -1 299.40 7.59 2 -6 1 282.64 6.77 2 -6 1 279.80 6.72 2 -6 1 301.21 7.28 2 -6 2 982.83 20.77 -2 6 -2 976.14 22.03 2 -6 2 968.31 20.83 2 -6 2 1025.67 21.46 -2 6 -2 1064.49 21.88 -2 6 -2 1037.16 22.01 2 -6 2 927.08 21.10 2 -6 2 1035.89 21.53 2 -6 3 746.10 16.56 -2 6 -3 740.66 17.68 2 -6 3 817.59 17.21 2 -6 3 791.74 17.12 2 -6 3 773.58 17.17 -2 6 -3 791.76 17.70 -2 6 -3 825.03 17.68 2 -6 3 761.58 16.77 -2 6 -3 770.57 16.79 -2 6 -3 785.66 17.77 2 -6 4 170.27 4.54 -2 6 -4 157.08 5.26 -2 6 -4 184.78 5.52 2 -6 4 180.54 5.05 2 -6 4 170.31 4.85 2 -6 4 172.46 4.74 -2 6 -4 172.23 4.83 -2 6 -4 181.95 5.49 -2 6 -4 173.82 5.40 2 -6 5 1220.47 26.11 -2 6 -5 1198.52 27.06 2 -6 5 1196.62 26.29 -2 6 -5 1246.49 27.17 2 -6 5 1272.77 26.38 -2 6 -5 1244.90 26.33 -2 6 -5 1267.74 26.63 -2 6 -5 1256.86 27.30 2 -6 5 1259.20 26.64 -2 6 -5 1343.06 27.52 -2 6 -6 80.81 3.31 -2 6 -6 85.79 3.07 2 -6 6 85.03 2.89 -2 6 -6 91.88 3.35 2 -6 6 88.81 3.20 2 -6 6 86.99 3.07 -2 6 -6 93.50 3.78 -2 6 -6 88.65 3.60 -2 6 -6 82.44 3.39 2 -6 6 89.94 2.94 -2 6 -7 754.51 17.76 2 -6 7 793.71 17.54 -2 6 -7 812.03 17.99 -2 6 -7 858.67 18.69 2 -6 7 762.39 16.80 2 -6 7 819.11 17.53 2 -6 7 809.19 17.62 2 -6 7 771.70 16.96 -2 6 -7 783.15 17.24 -2 6 -7 772.53 17.55 -2 6 -7 764.73 17.90 2 -6 7 790.37 17.26 2 -6 8 279.92 7.19 -2 6 -8 293.95 8.18 2 -6 8 274.62 7.07 -2 6 -8 262.63 7.20 2 -6 8 255.42 6.49 2 -6 8 275.73 7.11 -2 6 -8 266.22 6.94 -2 6 -8 277.43 7.78 -2 6 -8 246.80 7.25 -2 6 -8 242.54 7.06 2 -6 8 263.47 6.89 -2 6 -9 72.49 2.89 -2 6 -9 76.28 3.17 -2 6 -9 84.41 3.79 2 -6 9 80.63 2.99 2 -6 9 80.56 3.08 2 -6 9 74.91 2.64 -2 6 -9 75.72 2.97 -2 6 -9 76.42 3.43 2 -6 9 81.80 3.11 -2 6 -9 72.82 3.07 2 -6 9 75.59 2.91 -2 6 -10 151.98 5.51 2 -6 10 141.56 4.52 2 -6 10 135.21 4.10 -2 6 -10 147.22 4.86 -2 6 -10 141.09 4.56 2 -6 10 142.87 4.58 -2 6 -10 141.11 5.04 -2 6 -10 128.59 4.39 2 -6 10 142.83 4.51 -2 6 -11 80.38 3.38 2 -6 11 75.60 2.95 2 -6 11 72.19 2.73 2 -6 11 74.05 3.06 -2 6 -11 74.27 3.10 -2 6 -11 68.38 3.29 2 -6 11 76.79 3.05 2 -6 12 10.26 1.00 2 -6 12 10.48 0.95 2 -6 12 8.02 0.78 -2 6 -12 9.67 1.16 -2 6 -12 10.59 1.12 -2 6 -12 9.91 1.18 2 -6 12 11.40 1.13 2 -6 13 42.27 1.97 -2 6 -13 43.01 2.31 2 -6 13 43.83 2.25 -2 6 -13 44.49 2.74 -2 6 -13 43.37 2.46 2 -6 13 41.38 1.99 -2 6 -13 43.30 2.37 2 -6 14 123.53 3.80 -2 6 -14 131.40 4.68 -2 6 -14 128.90 5.00 2 -6 14 127.96 4.06 -2 6 -14 137.18 4.55 2 -6 14 142.27 4.46 -2 6 -14 130.96 4.40 2 -6 14 135.99 4.40 -2 6 -15 12.27 1.39 -2 6 -15 13.54 1.31 2 -6 15 12.91 1.03 -2 6 -15 12.90 1.19 2 -6 15 13.66 1.16 2 -6 15 14.65 1.22 2 -6 16 222.41 5.79 -2 6 -16 212.30 5.88 2 -6 16 204.07 5.42 2 -6 16 208.46 5.61 -2 6 -16 212.40 6.09 -2 6 -17 21.68 1.43 2 -6 17 19.75 1.16 2 -6 17 19.79 1.11 -2 6 -17 20.54 1.29 2 -6 17 23.58 1.33 -2 6 -18 33.04 1.48 -2 6 -18 32.92 1.61 2 -6 18 31.15 1.28 2 -5 -17 12.39 0.85 2 -5 -17 14.88 0.97 -2 5 17 14.82 0.91 2 -5 -17 14.88 0.96 -2 5 16 294.43 7.27 -2 5 16 338.56 7.65 2 -5 -16 324.56 7.74 2 -5 -16 327.60 7.78 2 -5 -16 277.53 7.08 2 -5 -15 126.69 3.88 -2 5 15 125.10 3.95 -2 5 15 132.68 4.15 2 -5 -15 133.29 4.26 2 -5 -15 137.91 4.31 2 -5 -14 158.68 4.78 2 -5 -14 166.09 5.16 2 -5 -14 161.20 5.13 -2 5 14 160.18 4.91 -2 5 13 195.07 5.83 -2 5 13 203.78 5.99 -2 5 13 200.68 5.50 2 -5 -13 211.42 6.22 2 -5 -13 199.21 6.11 2 -5 -13 199.66 5.81 2 -5 -13 208.68 6.07 -2 5 12 4.03 0.74 2 -5 -12 6.06 0.82 2 -5 -12 3.41 0.56 2 -5 -12 3.51 0.74 -2 5 12 3.76 0.63 -2 5 12 3.66 0.63 -2 5 12 2.84 0.55 -2 5 12 4.16 0.79 2 -5 -12 3.91 0.76 2 -5 -11 7.30 0.81 -2 5 11 7.14 1.02 -2 5 11 5.62 0.76 2 -5 -11 6.29 0.92 -2 5 11 6.95 0.84 -2 5 11 7.07 0.81 -2 5 11 6.32 0.74 2 -5 -11 7.79 0.94 2 -5 -11 7.06 0.96 -2 5 10 52.74 2.41 2 -5 -10 56.22 2.36 2 -5 -10 53.96 2.64 -2 5 10 54.92 2.32 2 -5 -10 50.66 2.43 -2 5 10 52.52 2.29 -2 5 10 58.58 2.78 2 -5 -10 53.33 2.58 2 -5 -9 96.68 3.49 -2 5 9 99.05 3.54 -2 5 9 98.05 3.80 2 -5 -9 96.81 3.66 -2 5 9 95.80 3.38 -2 5 9 96.97 3.39 2 -5 -9 94.25 3.57 2 -5 -9 100.84 3.67 -2 5 9 94.42 3.26 2 -5 -9 100.92 3.40 2 -5 -8 62.74 2.52 -2 5 8 58.53 2.36 -2 5 8 61.28 2.47 -2 5 8 63.87 2.89 2 -5 -8 61.48 2.70 -2 5 8 61.75 2.63 -2 5 8 60.83 2.52 2 -5 -8 59.95 2.64 2 -5 -8 60.20 2.54 -2 5 7 1884.20 39.00 -2 5 7 1778.40 38.79 -2 5 7 2018.87 39.96 2 -5 -7 1886.16 39.43 -2 5 7 1885.40 39.47 2 -5 -7 1930.68 39.41 2 -5 -7 1808.57 39.11 2 -5 -7 1978.12 39.25 -2 5 7 1840.36 39.23 -2 5 6 34.35 1.89 -2 5 6 32.46 1.62 2 -5 -6 34.54 1.49 2 -5 -6 34.40 1.69 2 -5 -6 34.13 1.79 2 -5 -6 34.73 1.89 -2 5 6 33.62 1.80 -2 5 6 33.26 1.58 2 -5 -6 39.14 1.90 -2 5 6 38.41 2.01 2 -5 -6 36.43 1.85 -2 5 5 942.47 20.86 -2 5 5 970.21 20.59 2 -5 -5 907.69 19.52 2 -5 -5 943.61 20.23 -2 5 5 959.27 19.88 2 -5 -5 931.80 19.73 2 -5 -5 968.29 20.34 -2 5 5 983.51 20.54 2 -5 -5 888.06 19.90 2 -5 -5 978.44 20.49 -2 5 5 880.87 19.67 2 -5 -5 955.30 20.25 -2 5 5 898.55 19.76 -2 5 4 954.51 20.38 2 -5 -4 926.22 20.13 2 -5 -4 1018.95 20.86 2 -5 -4 949.04 20.62 2 -5 -4 999.76 20.74 2 -5 -4 963.93 21.58 2 -5 -4 1003.69 20.93 2 -5 -4 946.90 20.32 -2 5 4 991.61 21.18 2 -5 -4 961.56 20.00 -2 5 4 942.66 20.86 -2 5 4 933.72 20.46 -2 5 4 947.61 21.15 -2 5 4 980.06 20.33 -2 5 3 77.90 2.64 -2 5 3 78.51 2.86 2 -5 -3 78.49 2.48 2 -5 -3 89.29 2.84 2 -5 -3 83.89 3.27 2 -5 -3 81.18 2.40 2 -5 -3 78.29 2.59 -2 5 3 78.89 2.47 2 -5 -3 77.47 2.66 -2 5 3 84.58 3.12 2 -5 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0.96 -2 5 -10 7.87 1.02 2 -5 10 10.45 0.99 -2 5 -10 7.05 0.79 2 -5 10 6.64 0.66 -2 5 -11 6.08 0.75 2 -5 11 6.80 0.70 2 -5 11 6.08 0.80 -2 5 -11 6.51 1.13 2 -5 11 5.39 0.70 -2 5 -11 5.98 0.90 -2 5 -11 5.10 0.85 2 -5 11 6.22 0.83 2 -5 11 6.92 0.78 2 -5 12 67.12 2.65 -2 5 -12 62.61 2.64 -2 5 -12 69.57 3.09 2 -5 12 60.61 2.33 -2 5 -12 63.89 3.33 2 -5 12 64.25 2.60 2 -5 12 62.08 2.40 -2 5 -12 65.32 2.93 2 -5 12 69.04 2.86 -2 5 -13 423.50 10.63 -2 5 -13 452.84 11.30 2 -5 13 431.54 10.33 2 -5 13 456.83 10.92 2 -5 13 419.81 10.21 -2 5 -13 447.51 11.81 -2 5 -13 442.64 10.90 2 -5 13 457.20 10.92 2 -5 13 429.29 10.55 -2 5 -14 121.75 4.78 2 -5 14 113.53 3.60 2 -5 14 130.10 4.26 -2 5 -14 120.09 4.06 2 -5 14 115.66 3.71 2 -5 14 126.73 4.04 -2 5 -14 127.00 4.54 -2 5 -14 118.42 4.00 2 -5 14 126.23 4.27 -2 5 -15 387.76 9.64 -2 5 -15 386.43 10.49 2 -5 15 388.38 9.56 2 -5 15 368.74 9.19 -2 5 -15 390.99 10.36 2 -5 15 398.52 9.75 -2 5 -15 402.12 10.25 2 -5 15 409.02 9.89 2 -5 16 30.88 1.52 -2 5 -16 32.27 1.71 2 -5 16 31.96 1.73 -2 5 -16 30.95 2.01 2 -5 16 30.52 1.68 -2 5 -16 33.09 2.00 -2 5 -16 32.33 2.03 2 -5 16 33.84 1.86 2 -5 17 18.00 1.17 -2 5 -17 16.27 1.28 2 -5 17 18.42 1.19 2 -5 17 17.88 1.03 -2 5 -17 20.63 1.51 -2 5 -17 20.56 1.45 -2 5 -18 43.79 2.01 2 -5 18 38.82 1.64 2 -5 18 38.09 1.53 -2 5 -18 39.30 1.88 2 -5 19 25.27 1.18 -2 5 -19 24.66 1.28 2 -5 19 20.95 1.05 -2 5 -19 24.93 1.34 2 -4 -18 0.31 0.29 -2 4 18 0.17 0.24 2 -4 -18 0.17 0.25 2 -4 -17 98.08 3.30 2 -4 -17 96.03 3.20 2 -4 -17 95.83 3.13 -2 4 17 97.96 3.12 -2 4 16 36.30 1.78 2 -4 -16 39.87 2.00 -2 4 16 40.55 1.99 2 -4 -16 41.01 2.12 2 -4 -16 42.57 2.09 2 -4 -15 120.97 4.27 2 -4 -15 128.61 4.46 -2 4 15 122.66 4.06 2 -4 -15 129.49 4.38 -2 4 15 130.23 4.27 -2 4 14 417.14 9.95 2 -4 -14 416.71 10.51 -2 4 14 433.15 10.33 2 -4 -14 419.72 10.32 -2 4 13 9.46 1.01 2 -4 -13 10.74 1.17 2 -4 -13 10.28 1.00 -2 4 13 8.28 0.82 -2 4 13 10.65 1.02 -2 4 13 11.06 1.14 -2 4 13 11.02 1.04 2 -4 -13 11.54 1.16 -2 4 12 279.09 7.68 -2 4 12 288.55 7.37 2 -4 -12 285.18 7.86 -2 4 12 281.46 7.46 -2 4 12 270.09 6.95 -2 4 12 272.56 7.14 2 -4 -12 271.67 7.37 -2 4 12 292.77 7.79 2 -4 -12 287.81 7.69 -2 4 11 109.76 3.99 2 -4 -11 105.05 3.39 -2 4 11 108.34 3.63 -2 4 11 113.97 4.05 -2 4 11 114.67 3.70 -2 4 11 108.51 3.49 2 -4 -11 103.78 3.70 2 -4 -11 109.85 4.04 2 -4 -11 112.21 3.93 -2 4 10 33.75 1.78 2 -4 -10 32.01 1.59 -2 4 10 32.17 1.95 -2 4 10 33.91 1.71 -2 4 10 35.52 1.77 2 -4 -10 33.32 1.97 2 -4 -10 33.60 1.93 2 -4 -10 31.29 1.75 2 -4 -10 34.28 1.99 2 -4 -10 34.56 1.91 -2 4 9 6.42 0.74 2 -4 -9 7.45 0.74 -2 4 9 7.09 0.83 2 -4 -9 6.73 0.86 -2 4 9 6.04 0.88 2 -4 -9 5.51 0.81 2 -4 -9 6.18 0.76 2 -4 -9 8.56 0.91 -2 4 9 6.68 0.78 2 -4 -9 5.99 0.79 -2 4 9 7.26 0.77 2 -4 -8 16.94 1.11 -2 4 8 18.41 1.38 2 -4 -8 16.68 1.27 -2 4 8 16.66 1.11 -2 4 8 16.72 1.17 -2 4 8 16.15 1.14 -2 4 8 16.39 1.18 2 -4 -8 19.84 1.34 2 -4 -8 16.98 1.31 2 -4 -8 16.78 1.28 2 -4 -8 17.65 1.29 -2 4 7 62.75 2.47 -2 4 7 63.36 2.32 -2 4 7 62.06 2.39 -2 4 7 57.46 2.07 -2 4 7 65.26 2.66 2 -4 -7 63.02 2.47 2 -4 -7 63.72 2.54 -2 4 7 55.53 2.88 2 -4 -7 63.43 2.54 2 -4 -7 63.82 2.56 -2 4 7 57.96 2.19 -2 4 6 2172.07 42.53 2 -4 -6 2062.51 42.32 -2 4 6 2000.34 41.86 -2 4 6 2014.74 41.72 2 -4 -6 2108.77 42.31 -2 4 6 2023.22 42.15 -2 4 6 1975.97 41.76 2 -4 -6 2065.31 42.27 -2 4 6 1968.50 43.04 -2 4 6 2177.36 42.60 -2 4 6 2085.11 42.31 2 -4 -6 2039.23 42.28 -2 4 6 1994.45 41.66 2 -4 -5 1262.99 26.59 -2 4 5 1279.09 25.69 -2 4 5 1201.31 26.16 -2 4 5 1161.92 25.05 2 -4 -5 1178.57 24.85 -2 4 5 1234.09 25.49 2 -4 -5 1188.72 25.47 2 -4 -5 1188.22 25.45 -2 4 5 1259.78 25.62 -2 4 5 1216.78 25.08 -2 4 5 1191.79 25.05 2 -4 -5 1192.04 25.44 -2 4 4 417.42 9.95 -2 4 4 407.73 9.62 -2 4 4 404.72 9.20 2 -4 -4 422.31 10.29 -2 4 4 409.29 9.04 -2 4 4 410.22 9.17 2 -4 -4 408.95 9.00 2 -4 -4 393.75 9.55 2 -4 -4 401.69 8.67 2 -4 -4 408.36 9.34 -2 4 4 412.97 9.49 -2 4 3 2122.22 42.74 -2 4 3 2077.34 42.28 2 -4 -3 2136.58 43.18 -2 4 3 2066.56 42.53 2 -4 -3 1955.53 42.38 2 -4 -3 2110.14 42.24 -2 4 3 2273.82 42.85 -2 4 3 2007.03 42.11 -2 4 3 2026.34 42.14 -2 4 3 2008.88 41.76 2 -4 -2 46.97 2.23 -2 4 2 49.85 2.06 -2 4 2 52.30 2.14 2 -4 -2 46.67 1.85 -2 4 2 46.67 1.53 2 -4 -2 48.18 1.72 -2 4 2 49.17 2.06 2 -4 -2 52.54 2.23 -2 4 2 47.54 1.64 -2 4 2 48.92 1.86 -2 4 1 1258.04 25.06 2 -4 -1 1189.70 24.69 2 -4 -1 1203.83 24.51 2 -4 -1 1225.59 24.98 2 -4 -1 1250.32 25.05 2 -4 -1 1191.44 24.98 2 -4 0 9.12 0.91 -2 4 0 8.17 0.80 -2 4 0 7.39 0.46 -2 4 0 8.70 0.64 2 -4 0 9.35 0.81 2 -4 0 8.30 0.83 2 -4 0 9.49 0.72 -2 4 0 8.57 0.77 2 -4 0 9.68 0.92 -2 4 -1 3.03 0.54 -2 4 -1 1.86 0.45 2 -4 1 3.00 0.63 2 -4 1 3.40 0.47 2 -4 1 3.04 0.57 2 -4 1 2.92 0.47 2 -4 1 2.55 0.57 -2 4 -1 1.87 0.39 2 -4 1 2.05 0.63 2 -4 1 2.34 0.53 2 -4 1 2.07 0.46 2 -4 2 71.36 2.49 2 -4 2 76.76 2.38 2 -4 2 72.98 1.75 -2 4 -2 76.20 2.62 2 -4 2 73.94 2.61 2 -4 2 73.40 2.39 -2 4 -2 74.37 2.39 -2 4 -2 73.18 2.58 2 -4 2 72.67 2.45 2 -4 2 74.25 2.38 2 -4 3 959.91 20.36 2 -4 3 963.72 19.88 2 -4 3 937.19 19.65 -2 4 -3 960.01 20.04 2 -4 3 952.09 19.97 2 -4 3 941.26 20.12 2 -4 3 918.25 19.70 2 -4 3 923.52 19.08 -2 4 -3 987.19 20.39 -2 4 -4 362.57 8.69 2 -4 4 346.47 8.19 -2 4 -4 345.20 8.17 2 -4 4 357.56 8.23 2 -4 4 360.45 8.02 2 -4 4 351.05 8.15 2 -4 4 360.99 8.72 2 -4 4 336.39 7.83 -2 4 -5 200.64 5.23 2 -4 5 209.21 5.89 2 -4 5 203.10 5.17 2 -4 5 213.68 5.33 -2 4 -5 215.22 5.83 2 -4 5 194.82 5.24 -2 4 -5 203.60 5.56 -2 4 -5 207.84 5.74 2 -4 5 203.64 5.05 -2 4 -6 689.70 15.34 -2 4 -6 748.32 16.06 2 -4 6 694.94 15.09 2 -4 6 748.05 15.62 2 -4 6 731.72 15.65 2 -4 6 710.09 15.59 -2 4 -6 693.98 15.93 2 -4 6 733.81 15.56 -2 4 -6 709.18 15.67 -2 4 -6 732.33 16.35 2 -4 6 738.05 15.46 -2 4 -6 685.47 15.54 2 -4 7 11.67 0.94 2 -4 7 10.97 0.70 2 -4 7 13.10 0.98 -2 4 -7 10.80 0.85 2 -4 7 11.25 0.77 2 -4 7 13.99 1.04 2 -4 7 12.92 0.94 -2 4 -7 11.44 1.04 2 -4 7 11.72 1.20 -2 4 -7 11.82 0.97 2 -4 7 11.77 0.96 -2 4 -7 12.03 0.90 2 -4 8 559.43 12.34 2 -4 8 512.44 11.68 2 -4 8 545.72 12.11 2 -4 8 552.42 12.27 2 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1.87 -2 4 -13 24.99 1.52 2 -4 13 25.16 1.69 -2 4 -14 598.61 14.23 2 -4 14 621.69 13.98 -2 4 -14 611.72 14.86 2 -4 14 628.33 14.10 2 -4 14 589.35 13.62 -2 4 -14 650.18 14.86 2 -4 14 642.60 14.25 -2 4 -15 165.31 5.22 2 -4 15 163.13 4.97 2 -4 15 156.74 4.69 2 -4 15 169.62 5.04 -2 4 -15 166.49 5.55 2 -4 16 104.64 3.60 -2 4 -16 104.79 3.79 2 -4 16 107.49 3.56 2 -4 16 102.33 3.37 -2 4 -16 105.56 4.04 -2 4 -17 122.40 4.00 2 -4 17 120.54 3.68 2 -4 17 124.32 3.62 2 -4 17 123.91 3.85 -2 4 -17 130.59 4.35 -2 4 -18 57.55 2.34 2 -4 18 56.38 2.05 2 -4 18 60.65 2.30 2 -4 18 57.81 2.08 -2 4 -18 64.04 2.64 2 -4 18 59.35 2.30 -2 4 -19 2.83 0.47 -2 4 -19 3.33 0.55 -2 4 -19 3.24 0.55 2 -4 19 2.83 0.45 2 -4 19 3.39 0.48 2 -3 -19 15.33 0.97 2 -3 -19 14.53 0.86 -2 3 19 14.26 0.85 2 -3 -19 15.61 0.96 2 -3 -18 149.72 4.42 -2 3 18 144.19 4.03 -2 3 18 151.85 4.22 2 -3 -18 143.39 4.20 2 -3 -18 153.81 4.46 -2 3 17 247.90 6.25 2 -3 -17 235.08 6.43 2 -3 -17 246.57 6.49 2 -3 -17 241.64 6.27 -2 3 16 295.33 7.49 -2 3 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-12 1.32 0.78 -2 -6 12 0.94 0.46 -2 -6 11 345.85 9.01 2 6 -11 351.77 11.03 -2 -6 11 354.42 9.21 -2 -6 11 355.08 9.12 2 6 -11 364.05 10.07 -2 -6 11 340.28 8.89 -2 -6 11 362.47 9.21 2 6 -11 346.68 10.10 -2 -6 11 369.96 8.98 -2 -6 11 346.53 9.22 -2 -6 10 25.85 1.46 2 6 -10 26.96 2.57 -2 -6 10 27.77 1.83 -2 -6 10 25.85 1.66 -2 -6 10 26.94 1.77 2 6 -10 27.53 2.12 -2 -6 10 29.30 1.81 -2 -6 10 26.70 1.72 2 6 -10 26.63 2.18 -2 -6 10 29.41 1.73 -2 -6 9 31.32 1.95 -2 -6 9 30.09 1.87 -2 -6 9 30.34 1.80 2 6 -9 32.61 2.84 -2 -6 9 31.96 1.86 -2 -6 9 36.39 2.11 2 6 -9 33.09 2.28 -2 -6 9 29.46 1.65 -2 -6 9 32.09 1.91 2 6 -9 30.24 2.32 -2 -6 9 30.49 1.90 -2 -6 8 131.08 4.44 -2 -6 8 130.10 4.30 -2 -6 8 124.99 4.34 -2 -6 8 124.70 4.10 -2 -6 8 126.34 4.21 2 6 -8 129.62 5.95 -2 -6 8 117.55 3.82 2 6 -8 120.14 4.68 -2 -6 8 130.49 4.61 -2 -6 8 129.51 4.32 2 6 -8 122.21 5.00 -2 -6 8 126.85 4.37 -2 -6 7 339.49 8.58 -2 -6 7 331.88 8.52 -2 -6 7 325.43 8.27 -2 -6 7 326.69 8.34 -2 -6 7 311.88 8.03 -2 -6 7 333.25 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4.51 0.60 2 7 -13 3.03 0.71 -2 -7 13 4.17 0.63 2 7 -13 4.94 0.87 -2 -7 12 328.41 8.09 -2 -7 12 323.23 7.86 -2 -7 12 307.29 7.80 2 7 -12 306.59 8.51 -2 -7 12 336.94 8.18 2 7 -12 329.66 9.00 -2 -7 11 37.24 2.02 -2 -7 11 39.10 1.99 -2 -7 11 38.88 1.87 -2 -7 11 40.48 1.93 2 7 -11 35.26 2.11 2 7 -11 38.24 2.43 -2 -7 10 23.08 1.60 -2 -7 10 21.94 1.53 -2 -7 10 22.51 1.45 -2 -7 10 23.39 1.51 2 7 -10 23.24 1.66 -2 -7 10 21.97 1.29 2 7 -10 21.97 1.86 -2 -7 9 122.25 4.19 -2 -7 9 112.49 4.02 -2 -7 9 112.88 3.74 -2 -7 9 116.39 3.91 -2 -7 9 120.51 4.01 -2 -7 9 117.87 4.28 2 7 -9 116.36 4.63 2 7 -9 111.67 5.37 -2 -7 8 149.95 4.83 -2 -7 8 144.94 4.76 -2 -7 8 143.28 4.54 -2 -7 8 140.96 4.55 2 7 -8 141.43 6.24 -2 -7 8 156.44 4.79 -2 -7 8 134.62 4.19 -2 -7 8 146.63 5.02 2 7 -8 141.20 5.27 -2 -7 7 1.07 0.47 -2 -7 7 0.54 0.48 -2 -7 7 1.12 0.50 2 7 -7 1.30 0.96 -2 -7 7 1.38 0.44 -2 -7 7 0.86 0.48 2 7 -7 1.13 0.66 -2 -7 7 0.81 0.46 -2 -7 6 76.81 3.17 -2 -7 6 75.44 3.10 -2 -7 6 73.37 3.01 -2 -7 6 78.67 3.17 -2 -7 6 70.23 2.92 -2 -7 6 73.86 3.33 2 7 -6 67.72 3.30 -2 -7 5 202.93 5.88 -2 -7 5 195.19 5.72 -2 -7 5 192.61 5.83 2 7 -5 198.84 7.74 -2 -7 5 189.66 5.70 -2 -7 5 184.34 5.66 -2 -7 5 189.48 5.82 -2 -7 5 190.14 5.82 2 7 -5 185.14 5.99 2 7 -5 178.71 6.50 -2 -7 4 152.32 4.86 -2 -7 4 147.47 4.90 -2 -7 4 153.46 5.20 -2 -7 4 151.22 4.95 -2 -7 4 148.76 4.88 2 7 -4 160.19 6.76 -2 -7 4 143.51 4.70 -2 -7 4 140.55 4.78 2 7 -4 138.92 4.81 2 7 -4 141.74 5.48 2 7 -3 162.66 6.12 -2 -7 3 187.88 5.49 -2 -7 3 184.27 5.66 -2 -7 3 186.24 5.59 -2 -7 3 174.02 5.32 -2 -7 3 170.01 5.46 -2 -7 3 185.86 5.58 2 7 -3 175.74 7.27 -2 -7 3 155.40 4.89 2 7 -3 170.25 6.08 2 7 -2 6.71 1.17 -2 -7 2 6.78 0.91 -2 -7 2 5.73 0.77 2 7 -2 6.49 1.18 -2 -7 2 6.59 0.93 2 7 -2 6.05 1.31 -2 -7 2 5.94 0.83 -2 -7 2 7.45 0.97 2 7 -1 320.78 9.53 -2 -7 1 345.88 8.74 -2 -7 1 315.80 8.51 -2 -7 1 362.00 9.13 -2 -7 1 333.01 8.62 2 7 -1 315.05 9.99 2 7 -1 329.88 9.28 2 7 0 78.28 3.43 2 7 0 77.23 3.62 -2 -7 0 70.32 3.04 -2 -7 0 82.27 3.39 -2 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87.52 2.93 4 -9 11 80.84 2.72 -4 9 -11 91.98 3.40 -4 9 -11 84.19 3.05 4 -9 12 25.26 1.29 -4 9 -12 25.20 1.34 -4 9 -12 27.87 1.61 4 -9 13 69.05 2.18 -4 9 -14 1.69 0.39 -4 8 13 26.36 1.22 -4 8 12 6.15 0.57 -4 8 12 5.43 0.52 4 -8 -12 5.78 0.60 4 -8 -11 405.43 9.25 -4 8 11 436.65 9.62 4 -8 -11 378.99 9.19 4 -8 -11 435.20 9.69 -4 8 11 413.39 9.36 -4 8 11 402.14 9.34 4 -8 -11 434.91 9.79 4 -8 -10 83.54 2.81 -4 8 10 82.87 2.76 4 -8 -10 81.94 2.72 -4 8 10 87.78 3.08 -4 8 10 86.07 2.93 4 -8 -10 84.50 3.05 4 -8 -9 197.49 5.48 -4 8 9 211.03 5.85 -4 8 9 204.93 5.80 4 -8 -9 188.06 5.25 -4 8 9 204.72 5.66 4 -8 -9 202.13 5.71 4 -8 -8 112.16 3.83 -4 8 8 123.27 4.15 -4 8 8 118.88 4.05 4 -8 -8 109.43 3.55 -4 8 8 117.76 3.98 4 -8 -8 113.03 3.91 4 -8 -7 26.29 1.68 -4 8 7 27.45 1.82 -4 8 7 27.09 1.74 4 -8 -7 24.03 1.41 -4 8 7 26.83 1.77 4 -8 -7 27.00 1.68 4 -8 -6 70.39 2.94 -4 8 6 71.27 3.14 -4 8 6 69.40 2.95 4 -8 -6 61.54 2.46 4 -8 -6 66.14 2.68 -4 8 6 70.72 3.08 4 -8 -6 69.85 2.89 -4 8 6 66.93 2.55 -4 8 5 16.79 1.50 -4 8 5 17.62 1.40 4 -8 -5 15.60 1.11 4 -8 -5 15.36 1.18 -4 8 5 17.41 1.49 4 -8 -5 16.45 1.32 -4 8 5 17.03 1.24 -4 8 4 1.85 0.58 4 -8 -4 1.60 0.44 4 -8 -4 1.98 0.47 -4 8 4 2.17 0.53 -4 8 4 2.35 0.74 -4 8 4 1.34 0.60 4 -8 -4 2.09 0.57 -4 8 4 2.02 0.55 4 -8 -3 65.97 2.50 -4 8 3 73.27 2.97 4 -8 -3 69.68 2.74 4 -8 -3 67.03 2.87 -4 8 3 71.90 2.90 -4 8 3 70.18 3.19 4 -8 -3 65.67 2.58 4 -8 -3 67.48 2.83 -4 8 3 70.23 2.94 4 -8 -2 146.47 4.41 -4 8 2 157.65 4.83 4 -8 -2 152.08 4.67 4 -8 -2 154.37 4.77 4 -8 -2 139.37 4.28 -4 8 2 157.15 4.90 -4 8 2 150.39 5.19 -4 8 2 150.86 4.95 4 -8 -2 149.32 4.66 -4 8 1 38.58 2.30 4 -8 -1 37.76 1.88 -4 8 1 36.93 1.95 4 -8 -1 37.70 2.00 4 -8 -1 35.39 1.90 -4 8 1 40.60 2.18 -4 8 1 37.03 2.17 4 -8 -1 35.27 1.87 4 -8 0 166.84 4.92 -4 8 0 162.75 4.80 4 -8 0 166.84 5.13 4 -8 0 155.84 4.78 -4 8 0 166.00 5.35 -4 8 0 166.12 5.44 -4 8 0 167.55 5.43 4 -8 0 158.82 4.78 4 -8 1 0.19 0.64 4 -8 1 1.93 0.53 -4 8 -1 0.29 0.31 4 -8 1 0.14 0.48 4 -8 1 0.26 0.35 -4 8 -1 0.25 0.50 4 -8 1 0.03 0.33 -4 8 -1 0.79 0.56 -4 8 -2 211.68 6.39 4 -8 2 220.98 6.35 4 -8 2 210.53 6.07 -4 8 -2 204.59 6.54 -4 8 -2 216.38 6.62 -4 8 -3 112.88 4.12 4 -8 3 115.36 4.03 -4 8 -3 114.47 4.42 4 -8 3 115.58 4.09 -4 8 -3 118.37 4.44 -4 8 -4 24.24 1.65 4 -8 4 24.19 1.67 4 -8 4 25.79 1.73 -4 8 -4 27.23 2.02 -4 8 -4 28.19 1.99 -4 8 -5 184.08 5.53 4 -8 5 197.83 5.72 4 -8 5 196.46 5.86 -4 8 -5 192.30 6.30 -4 8 -5 192.47 6.24 4 -8 6 9.68 1.03 4 -8 6 10.34 1.15 -4 8 -6 10.17 1.29 -4 8 -6 10.17 0.95 4 -8 6 9.37 0.94 4 -8 7 63.30 2.58 4 -8 7 69.01 2.97 -4 8 -7 64.62 3.27 4 -8 7 64.80 2.64 4 -8 8 3.14 0.52 -4 8 -8 4.22 0.92 4 -8 8 4.80 0.73 -4 8 -8 2.90 0.75 4 -8 9 6.83 0.74 -4 8 -9 7.82 1.17 4 -8 9 6.63 0.84 -4 8 -9 7.30 1.00 4 -8 10 2.35 0.63 -4 8 -10 2.45 0.77 4 -8 10 2.74 0.61 4 -8 10 2.57 0.50 -4 8 -10 2.14 0.66 4 -8 11 767.85 16.37 4 -8 11 728.85 16.21 -4 8 -11 729.32 16.43 4 -8 12 23.53 1.31 4 -8 12 28.29 1.54 4 -8 12 21.72 1.29 4 -8 12 27.20 1.54 -4 8 -12 27.44 1.56 4 -8 13 225.08 5.78 4 -8 13 237.30 5.95 -4 8 -13 242.97 6.60 4 -8 13 235.28 6.08 -4 8 -13 226.98 5.85 4 -8 14 8.26 0.68 4 -8 14 9.31 0.69 -4 8 -14 8.42 0.89 4 -8 15 45.11 1.59 -4 8 -15 45.75 1.84 -4 7 14 20.36 1.20 -4 7 14 23.70 1.15 4 -7 -14 22.66 1.17 4 -7 -14 23.18 1.25 -4 7 13 20.39 1.17 4 -7 -13 20.42 1.23 4 -7 -13 18.55 1.25 4 -7 -13 20.56 1.27 -4 7 13 17.95 1.25 -4 7 12 329.62 8.07 4 -7 -12 323.37 8.20 -4 7 12 330.27 8.09 -4 7 12 339.19 8.42 -4 7 12 314.02 7.86 4 -7 -11 32.27 1.56 -4 7 11 34.59 1.85 4 -7 -11 34.08 1.85 -4 7 11 33.86 1.74 4 -7 -11 33.47 1.88 -4 7 10 164.17 5.03 -4 7 10 155.90 5.22 4 -7 -10 152.24 4.55 4 -7 -10 153.79 4.85 -4 7 10 155.64 4.80 4 -7 -9 118.06 3.90 -4 7 9 118.40 4.22 -4 7 9 120.81 4.27 4 -7 -9 117.89 4.07 4 -7 -9 113.15 4.04 -4 7 9 116.68 4.08 4 -7 -8 28.88 1.73 -4 7 8 31.65 2.00 -4 7 8 30.52 1.96 4 -7 -8 29.21 1.79 4 -7 -8 26.37 1.72 -4 7 8 29.24 1.87 4 -7 -8 27.02 1.81 -4 7 7 171.21 5.41 -4 7 7 169.02 5.30 4 -7 -7 160.14 5.01 4 -7 -7 158.88 5.03 -4 7 7 144.65 4.57 -4 7 7 165.49 5.27 4 -7 -7 163.98 5.20 -4 7 7 154.94 4.66 -4 7 6 27.62 1.91 -4 7 6 28.80 1.86 4 -7 -6 25.84 1.67 4 -7 -6 26.68 1.84 4 -7 -6 26.69 1.71 -4 7 6 26.52 1.58 -4 7 6 27.54 1.87 4 -7 -6 28.05 1.81 -4 7 6 26.74 1.61 -4 7 5 22.90 1.75 -4 7 5 22.90 1.62 4 -7 -5 21.73 1.47 4 -7 -5 20.65 1.27 4 -7 -5 21.62 1.63 4 -7 -5 21.82 1.52 -4 7 5 21.16 1.44 -4 7 5 22.62 1.68 4 -7 -5 21.63 1.58 -4 7 5 20.45 1.44 -4 7 4 18.90 1.44 4 -7 -4 18.49 1.33 4 -7 -4 16.68 1.19 4 -7 -4 21.95 1.64 4 -7 -4 19.38 1.41 -4 7 4 19.60 1.42 -4 7 4 20.64 1.62 4 -7 -4 19.67 1.49 -4 7 4 21.58 1.51 4 -7 -3 11.60 1.19 4 -7 -3 9.74 0.83 -4 7 3 12.30 1.14 4 -7 -3 11.34 1.00 4 -7 -3 11.15 1.02 4 -7 -3 12.95 1.13 -4 7 3 11.30 1.12 4 -7 -3 10.95 1.19 -4 7 3 12.01 1.25 4 -7 -3 11.99 1.17 -4 7 3 11.95 1.18 4 -7 -2 5.66 0.69 -4 7 2 6.46 0.83 4 -7 -2 6.05 0.80 4 -7 -2 7.22 0.97 -4 7 2 6.95 1.00 -4 7 2 6.39 0.88 4 -7 -2 7.35 1.01 4 -7 -2 5.33 0.81 -4 7 2 6.87 0.94 -4 7 1 15.06 1.38 4 -7 -1 16.74 1.42 4 -7 -1 15.82 1.15 -4 7 1 16.01 1.21 4 -7 -1 16.27 1.40 -4 7 1 17.13 1.43 -4 7 1 18.73 1.49 4 -7 0 157.02 4.68 -4 7 0 163.39 4.62 4 -7 0 166.26 4.94 4 -7 0 155.26 4.96 -4 7 0 149.27 5.07 -4 7 0 160.30 5.18 -4 7 0 160.03 5.24 -4 7 -1 342.01 8.92 4 -7 1 335.27 9.06 4 -7 1 345.88 8.88 4 -7 1 340.17 8.48 -4 7 -1 327.28 8.03 4 -7 1 328.58 8.63 4 -7 1 353.71 8.73 -4 7 -1 319.76 8.96 -4 7 -1 345.78 9.12 -4 7 -2 0.41 0.48 4 -7 2 0.59 0.59 4 -7 2 -0.04 0.63 4 -7 2 -0.15 0.43 4 -7 2 -0.16 0.50 -4 7 -2 0.62 0.52 -4 7 -2 1.47 0.59 -4 7 -3 65.61 2.76 4 -7 3 66.33 2.85 4 -7 3 66.18 2.75 4 -7 3 61.65 2.58 4 -7 3 64.68 2.81 -4 7 -3 58.14 2.96 -4 7 -3 63.64 2.78 4 -7 3 58.73 2.28 -4 7 -3 65.19 3.03 4 -7 3 62.68 2.84 -4 7 -4 4.55 0.70 4 -7 4 4.74 0.79 4 -7 4 5.87 0.80 4 -7 4 5.23 0.87 -4 7 -4 5.60 0.98 -4 7 -4 4.64 0.77 4 -7 4 5.10 0.66 -4 7 -4 5.20 0.70 4 -7 4 5.95 0.89 -4 7 -4 5.58 0.94 -4 7 -5 36.01 1.85 4 -7 5 40.52 2.12 4 -7 5 38.28 2.11 -4 7 -5 40.17 2.25 4 -7 5 38.32 1.85 -4 7 -5 37.69 2.40 -4 7 -5 37.06 1.92 4 -7 6 0.32 0.55 4 -7 6 0.31 0.30 -4 7 -6 0.28 0.53 -4 7 -6 0.30 0.47 4 -7 6 1.49 0.46 -4 7 -6 0.56 0.40 -4 7 -6 0.17 0.50 4 -7 7 15.52 1.39 4 -7 7 17.34 1.44 -4 7 -7 16.81 1.53 4 -7 7 18.01 1.31 -4 7 -7 16.98 1.35 -4 7 -7 17.21 1.52 4 -7 7 17.86 1.35 -4 7 -7 18.57 1.69 4 -7 7 16.88 1.12 4 -7 8 21.26 1.41 4 -7 8 21.50 1.61 -4 7 -8 20.14 1.72 -4 7 -8 22.67 1.68 -4 7 -8 20.45 1.51 -4 7 -8 19.02 1.59 4 -7 8 19.72 1.26 4 -7 9 49.95 2.43 -4 7 -9 48.66 2.76 -4 7 -9 46.85 2.51 4 -7 9 46.60 2.30 4 -7 9 45.78 2.42 -4 7 -9 46.28 2.37 -4 7 -9 50.38 2.58 4 -7 9 46.19 2.02 4 -7 9 47.06 2.11 4 -7 10 231.58 6.51 4 -7 10 226.47 6.34 -4 7 -10 213.81 7.00 -4 7 -10 228.70 6.74 4 -7 10 222.53 6.31 -4 7 -10 224.24 6.47 -4 7 -10 224.57 6.55 4 -7 10 209.97 5.96 4 -7 11 13.04 1.19 4 -7 11 10.89 1.06 -4 7 -11 10.19 1.28 -4 7 -11 9.98 1.25 -4 7 -11 10.49 1.19 4 -7 11 9.75 1.07 -4 7 -11 13.15 1.23 -4 7 -11 12.41 1.16 4 -7 11 10.65 0.98 -4 7 -12 625.88 14.93 4 -7 12 629.22 14.21 -4 7 -12 617.40 14.71 4 -7 12 627.65 14.28 -4 7 -12 602.64 14.37 -4 7 -12 597.90 14.05 4 -7 12 612.43 13.96 4 -7 13 1.33 0.43 -4 7 -13 1.22 0.57 -4 7 -13 1.15 0.54 4 -7 13 1.18 0.43 4 -7 13 1.22 0.49 -4 7 -13 1.98 0.56 -4 7 -13 1.25 0.39 4 -7 14 198.14 5.22 -4 7 -14 195.92 5.74 -4 7 -14 197.30 5.79 4 -7 14 209.86 5.55 -4 7 -14 200.31 5.61 4 -7 14 197.81 5.32 4 -7 15 83.50 2.62 -4 7 -15 74.92 2.74 4 -7 15 80.60 2.68 -4 7 -15 81.15 2.77 4 -7 16 70.43 2.30 -4 7 -16 75.32 2.44 -4 6 16 42.11 1.54 4 -6 -16 39.64 1.60 4 -6 -16 39.91 1.61 -4 6 15 0.13 0.31 4 -6 -15 0.19 0.31 -4 6 15 0.08 0.25 4 -6 -15 0.49 0.33 -4 6 14 14.84 1.18 4 -6 -14 14.32 1.01 -4 6 14 15.94 1.13 4 -6 -14 15.69 1.18 4 -6 -14 16.61 1.18 -4 6 13 31.37 1.64 4 -6 -13 28.75 1.60 -4 6 13 31.47 1.71 4 -6 -13 30.93 1.81 -4 6 13 29.61 1.52 -4 6 13 31.42 1.81 4 -6 -13 31.49 1.78 -4 6 12 50.52 2.43 -4 6 12 46.24 2.22 4 -6 -12 48.01 2.39 -4 6 12 45.96 2.12 4 -6 -12 47.54 2.24 -4 6 12 46.64 2.23 4 -6 -12 47.43 2.32 -4 6 11 3.23 0.74 4 -6 -11 2.04 0.44 4 -6 -11 1.54 0.52 -4 6 11 2.21 0.66 4 -6 -11 2.35 0.63 -4 6 11 2.21 0.60 -4 6 11 3.23 0.68 4 -6 -11 2.44 0.64 -4 6 10 59.08 2.94 4 -6 -10 53.83 2.32 4 -6 -10 57.44 2.64 4 -6 -10 55.21 2.70 -4 6 10 60.52 2.77 -4 6 10 54.05 2.55 4 -6 -10 55.54 2.66 4 -6 -9 0.26 0.36 -4 6 9 0.38 0.51 4 -6 -9 0.43 0.43 4 -6 -9 0.27 0.43 4 -6 -9 0.30 0.47 -4 6 9 0.17 0.36 -4 6 9 0.25 0.44 4 -6 -9 0.33 0.51 -4 6 8 105.54 3.91 4 -6 -8 92.26 3.60 -4 6 8 104.07 3.88 4 -6 -8 98.98 3.77 4 -6 -8 98.65 3.74 -4 6 8 91.37 3.35 -4 6 8 101.29 3.81 4 -6 -8 98.64 3.76 -4 6 7 -0.26 0.52 4 -6 -7 0.11 0.41 -4 6 7 0.15 0.38 -4 6 7 0.22 0.44 -4 6 7 -0.08 0.49 -4 6 7 0.63 0.37 -4 6 6 111.41 3.87 -4 6 6 106.16 3.96 -4 6 6 105.22 3.83 4 -6 -6 98.69 3.74 4 -6 -6 105.04 3.98 4 -6 -6 97.78 3.75 -4 6 6 102.18 3.58 -4 6 6 106.08 3.90 -4 6 6 101.44 3.57 -4 6 5 5.81 0.85 4 -6 -5 5.10 0.80 -4 6 5 4.75 0.77 4 -6 -5 5.32 0.61 4 -6 -5 5.32 0.91 -4 6 5 5.17 0.76 -4 6 5 4.84 0.82 -4 6 5 5.36 0.88 -4 6 5 5.37 0.78 4 -6 -5 5.22 0.87 4 -6 -4 118.19 3.96 -4 6 4 116.31 3.95 4 -6 -4 112.64 3.54 4 -6 -4 111.36 4.13 -4 6 4 117.24 3.95 -4 6 4 118.78 4.16 -4 6 4 122.17 3.96 -4 6 4 116.37 3.93 -4 6 3 0.66 0.50 4 -6 -3 0.28 0.50 4 -6 -3 0.36 0.27 -4 6 3 1.19 0.45 4 -6 -3 2.09 0.75 -4 6 3 0.89 0.48 -4 6 3 0.11 0.43 -4 6 3 0.83 0.47 -4 6 2 5.40 0.71 4 -6 -2 7.95 0.97 -4 6 2 4.73 0.77 4 -6 -2 6.62 0.68 4 -6 -2 6.82 1.13 -4 6 2 5.28 0.70 4 -6 -2 5.18 0.69 -4 6 2 4.96 0.77 -4 6 2 4.79 0.65 -4 6 2 5.32 0.69 -4 6 2 5.50 0.81 -4 6 1 81.70 2.79 -4 6 1 76.85 3.13 4 -6 -1 73.62 3.11 4 -6 -1 79.56 3.06 4 -6 -1 78.66 3.45 4 -6 -1 75.47 2.81 4 -6 -1 78.64 2.71 -4 6 1 76.71 3.10 -4 6 1 75.36 2.70 -4 6 1 74.51 2.77 -4 6 1 78.27 2.91 -4 6 1 81.71 3.18 -4 6 0 19.69 1.23 -4 6 0 16.15 1.30 -4 6 0 20.87 1.52 4 -6 0 19.81 1.24 -4 6 0 20.06 1.16 4 -6 0 16.79 1.56 4 -6 0 19.47 1.32 -4 6 0 16.69 1.39 4 -6 0 19.46 1.64 -4 6 0 18.31 1.19 -4 6 0 17.85 1.29 -4 6 0 18.82 1.43 4 -6 0 16.89 1.34 4 -6 1 487.68 11.69 -4 6 -1 440.72 10.99 4 -6 1 474.43 10.82 -4 6 -1 478.37 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15.98 1.25 -4 -5 -8 15.12 1.08 4 5 8 15.56 1.24 4 5 8 15.67 1.20 -4 -5 -9 0.60 0.35 4 5 9 0.07 0.35 4 5 9 0.57 0.40 -4 -5 -10 -0.08 0.27 4 5 10 0.04 0.28 4 5 10 0.28 0.29 -4 -6 14 17.12 0.95 4 6 -14 17.52 1.24 -4 -6 13 1.05 0.35 -4 -6 13 0.60 0.33 -4 -6 13 0.58 0.30 4 6 -13 0.99 0.51 -4 -6 12 0.98 0.39 -4 -6 12 0.37 0.35 -4 -6 12 0.30 0.31 4 6 -12 0.54 0.54 -4 -6 11 1.33 0.43 -4 -6 11 0.98 0.45 -4 -6 11 1.04 0.43 4 6 -11 1.29 0.64 -4 -6 10 1.11 0.45 -4 -6 10 1.29 0.48 -4 -6 10 0.98 0.45 4 6 -10 1.02 0.61 -4 -6 9 29.40 1.77 -4 -6 9 31.66 1.80 -4 -6 9 36.87 1.94 -4 -6 9 34.45 1.91 4 6 -9 32.29 2.08 -4 -6 8 0.50 0.44 -4 -6 8 1.37 0.51 -4 -6 8 0.36 0.44 -4 -6 8 0.33 0.45 4 6 -8 0.41 0.52 -4 -6 7 16.26 1.32 -4 -6 7 18.28 1.40 -4 -6 7 17.40 1.38 4 6 -7 15.31 1.39 -4 -6 6 13.66 1.17 -4 -6 6 16.03 1.32 -4 -6 6 17.10 1.38 -4 -6 6 16.32 1.34 -4 -6 5 134.68 4.55 -4 -6 5 138.00 4.51 -4 -6 5 142.46 4.60 -4 -6 5 130.04 4.23 -4 -6 4 180.30 5.40 -4 -6 4 172.35 5.40 -4 -6 4 180.01 5.38 -4 -6 4 157.79 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45.83 1.71 4 7 -11 39.95 1.93 4 7 -10 38.99 2.07 -4 -7 10 38.03 1.68 -4 -7 10 43.15 1.80 4 7 -10 41.21 2.09 4 7 -9 0.40 0.48 -4 -7 9 0.30 0.33 4 7 -9 0.29 0.46 -4 -7 9 0.49 0.32 -4 -7 9 0.02 0.30 4 7 -8 122.66 4.44 -4 -7 8 131.01 3.92 -4 -7 8 127.48 3.92 4 7 -8 124.05 4.33 4 7 -7 15.42 1.41 -4 -7 7 18.88 1.26 -4 -7 7 16.41 1.19 4 7 -7 16.86 1.41 -4 -7 6 206.26 5.57 -4 -7 6 199.84 5.50 -4 -7 6 201.07 5.52 4 7 -6 192.84 5.84 4 7 -5 180.84 5.79 -4 -7 5 196.76 5.45 -4 -7 5 193.64 5.41 4 7 -5 184.89 5.61 4 7 -4 144.58 4.90 -4 -7 4 160.71 4.64 -4 -7 4 150.56 4.53 4 7 -4 144.88 4.60 4 7 -3 181.48 5.56 -4 -7 3 196.76 5.43 -4 -7 3 185.14 5.32 -4 -7 2 0.14 0.34 -4 -7 2 0.25 0.36 4 7 -2 0.14 0.39 -4 -7 1 1.19 0.44 -4 -7 1 2.11 0.52 -4 -7 0 21.90 1.37 4 7 0 19.64 1.46 -4 -7 0 19.60 1.30 -4 -7 -1 76.57 2.63 4 7 1 71.60 2.74 -4 -7 -1 67.68 2.47 -4 -7 -2 4.74 0.64 4 7 2 4.79 0.69 4 7 2 2.69 0.57 -4 -7 -2 3.66 0.51 -4 -7 -3 59.60 2.30 4 7 3 65.66 2.39 -4 -7 -4 59.81 2.23 4 7 4 53.86 2.04 5 -11 -2 217.57 5.35 -5 11 2 220.58 5.33 5 -11 -1 12.56 0.82 -5 11 1 13.45 0.83 -5 11 1 12.75 0.86 5 -11 0 194.02 4.91 -5 11 0 190.92 4.81 5 -11 0 198.09 4.83 -5 11 0 195.85 4.98 5 -11 1 0.12 0.22 -5 11 -1 0.20 0.25 5 -11 1 0.08 0.22 -5 11 -1 0.27 0.25 5 -11 2 5.28 0.52 5 -11 2 4.69 0.48 5 -11 2 5.49 0.57 -5 11 -2 5.29 0.55 -5 11 -2 5.13 0.58 5 -11 3 42.53 1.61 5 -11 3 46.17 1.76 -5 11 -3 42.81 1.61 -5 11 -3 48.52 1.85 5 -11 4 0.63 0.27 5 -11 4 0.60 0.29 -5 11 -4 0.85 0.33 5 -11 5 19.05 1.00 5 -11 5 20.28 1.07 -5 11 -5 21.04 1.14 5 -11 6 60.59 2.03 -5 11 -6 66.07 2.20 5 -10 -7 4.17 0.48 -5 10 7 5.60 0.58 -5 10 7 5.26 0.54 5 -10 -6 13.05 0.89 -5 10 6 13.29 0.95 -5 10 6 13.71 0.94 5 -10 -5 24.79 1.35 -5 10 5 25.28 1.39 5 -10 -4 11.89 0.97 -5 10 4 13.22 1.05 5 -10 -3 36.32 1.78 -5 10 3 37.10 1.81 5 -10 -3 33.47 1.46 -5 10 3 35.28 1.57 -5 10 2 27.87 1.60 5 -10 -2 28.72 1.42 -5 10 2 29.31 1.51 -5 10 1 226.60 6.00 5 -10 -1 217.76 5.72 -5 10 1 204.90 5.57 -5 10 1 224.56 6.09 -5 10 1 224.30 5.92 5 -10 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0.48 5 -8 -3 1.01 0.43 -5 8 3 0.69 0.53 5 -8 -3 0.68 0.47 -5 8 3 1.40 0.55 -5 8 2 69.24 3.09 5 -8 -2 65.14 2.47 -5 8 2 62.31 2.50 5 -8 -2 68.82 2.74 5 -8 -2 66.72 2.96 5 -8 -2 67.29 2.68 -5 8 2 70.58 3.09 -5 8 2 73.12 3.21 5 -8 -2 73.32 2.99 -5 8 2 70.83 3.11 -5 8 1 61.26 2.84 5 -8 -1 61.76 2.89 5 -8 -1 55.33 2.37 5 -8 -1 64.18 2.68 5 -8 -1 58.50 2.73 5 -8 -1 60.70 2.49 -5 8 1 61.42 2.90 -5 8 1 62.29 2.91 5 -8 -1 60.34 2.67 -5 8 1 61.50 2.95 -5 8 0 309.55 8.16 5 -8 0 296.75 7.65 5 -8 0 290.63 7.98 -5 8 0 308.44 8.40 -5 8 0 303.09 8.23 5 -8 0 283.36 7.78 -5 8 0 311.90 8.46 -5 8 -1 5.48 0.81 5 -8 1 5.01 0.73 5 -8 1 4.99 0.80 -5 8 -1 4.25 0.89 -5 8 -1 4.42 0.80 -5 8 -1 4.83 0.93 -5 8 -2 813.95 18.06 5 -8 2 829.25 18.50 5 -8 2 827.18 18.07 5 -8 2 820.20 18.32 -5 8 -2 771.13 18.70 -5 8 -2 807.29 18.29 -5 8 -2 844.81 18.89 -5 8 -3 63.22 2.64 5 -8 3 66.28 2.96 5 -8 3 66.26 2.82 5 -8 3 66.84 2.96 -5 8 -3 64.54 3.19 -5 8 -3 64.05 2.81 -5 8 -3 70.21 3.24 -5 8 -4 5.74 0.70 5 -8 4 5.80 0.93 5 -8 4 7.01 0.96 5 -8 4 5.92 0.95 -5 8 -4 7.57 1.16 -5 8 -4 6.74 0.83 5 -8 5 163.46 5.04 5 -8 5 159.44 5.12 -5 8 -5 164.20 5.55 -5 8 -5 149.17 4.58 5 -8 5 148.47 4.37 5 -8 5 155.95 4.97 5 -8 6 19.48 1.47 5 -8 6 20.73 1.55 -5 8 -6 22.87 1.83 5 -8 6 19.90 1.27 -5 8 -6 18.91 1.34 -5 8 -6 19.63 1.63 5 -8 7 4.48 0.74 5 -8 7 3.97 0.77 -5 8 -7 3.84 0.88 -5 8 -7 3.81 0.77 5 -8 7 3.40 0.59 -5 8 -7 3.43 0.64 -5 8 -7 4.52 0.86 5 -8 8 265.14 6.87 5 -8 8 289.78 7.47 5 -8 8 265.77 7.37 -5 8 -8 265.32 7.72 5 -8 8 262.03 6.92 -5 8 -8 261.37 7.07 -5 8 -8 276.40 7.57 5 -8 9 188.56 5.47 5 -8 9 178.51 5.15 -5 8 -9 180.28 5.27 -5 8 -9 182.84 5.52 5 -8 10 177.29 5.11 -5 8 -10 180.07 5.65 5 -8 10 171.77 4.95 -5 8 -10 167.01 4.98 -5 8 -10 178.07 5.17 5 -8 11 514.20 11.70 -5 8 -11 522.04 12.21 5 -8 11 495.50 11.47 -5 8 -11 479.60 11.48 -5 8 -11 490.76 11.42 5 -8 12 2.03 0.47 -5 8 -12 1.37 0.55 5 -8 12 1.65 0.45 -5 8 -12 1.94 0.46 -5 8 -12 1.70 0.35 5 -8 13 236.26 5.70 -5 8 -13 240.88 6.06 5 -8 13 229.28 5.72 5 -8 14 10.98 0.76 5 -7 -14 0.56 0.28 5 -7 -14 0.49 0.26 -5 7 13 14.38 0.87 5 -7 -13 15.99 1.06 -5 7 13 15.67 0.94 5 -7 -13 16.71 1.09 -5 7 12 54.66 2.22 -5 7 12 46.32 2.16 -5 7 12 49.41 1.92 5 -7 -12 53.66 2.23 -5 7 12 51.00 2.08 5 -7 -12 55.27 2.27 -5 7 11 32.11 1.77 5 -7 -11 26.65 1.44 -5 7 11 32.07 1.77 -5 7 11 29.25 1.47 5 -7 -11 31.08 1.73 -5 7 11 31.93 1.70 5 -7 -11 29.36 1.71 5 -7 -10 132.96 4.10 -5 7 10 157.63 4.80 5 -7 -10 136.89 4.29 -5 7 10 154.83 4.74 -5 7 10 141.20 4.17 5 -7 -10 149.97 4.69 5 -7 -10 145.34 4.63 -5 7 10 154.02 4.70 5 -7 -10 155.73 4.74 5 -7 -9 43.47 2.03 -5 7 9 48.96 2.42 5 -7 -9 43.03 2.09 -5 7 9 50.07 2.38 -5 7 9 43.49 1.92 5 -7 -9 49.53 2.37 5 -7 -9 44.67 2.26 -5 7 9 35.83 1.87 -5 7 9 50.32 2.41 -5 7 8 132.30 4.73 -5 7 8 146.47 4.73 5 -7 -8 120.88 4.14 -5 7 8 126.13 4.35 -5 7 8 122.67 3.81 5 -7 -8 132.18 4.44 5 -7 -8 130.07 4.38 -5 7 8 119.97 4.05 -5 7 8 138.23 4.59 -5 7 7 106.38 4.15 -5 7 7 112.13 4.11 -5 7 7 106.85 3.84 -5 7 7 94.18 3.18 5 -7 -7 105.13 3.86 5 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351.53 9.13 5 -7 4 327.03 9.16 5 -7 5 865.40 18.79 5 -7 5 820.05 18.71 5 -7 5 856.99 18.90 -5 7 -5 850.90 19.44 -5 7 -5 849.89 19.38 -5 7 -5 794.73 17.95 5 -7 5 800.98 17.99 -5 7 -5 826.87 18.67 -5 7 -5 831.56 19.10 5 -7 5 780.47 19.04 5 -7 6 53.41 2.57 5 -7 6 52.91 2.58 -5 7 -6 50.20 2.80 5 -7 6 52.63 2.28 -5 7 -6 51.33 2.53 -5 7 -6 52.25 2.69 5 -7 7 47.57 2.35 5 -7 7 49.74 2.49 -5 7 -7 46.36 2.72 5 -7 7 48.57 2.21 -5 7 -7 46.30 2.43 -5 7 -7 49.72 2.56 5 -7 8 111.44 3.81 5 -7 8 115.75 4.11 5 -7 8 111.13 4.05 -5 7 -8 111.86 4.45 -5 7 -8 110.41 4.50 5 -7 8 108.20 3.74 -5 7 -8 107.09 4.03 -5 7 -8 112.13 4.09 5 -7 9 85.15 3.13 5 -7 9 95.08 3.57 -5 7 -9 101.19 4.02 -5 7 -9 93.72 4.07 5 -7 9 93.55 3.38 -5 7 -9 92.21 3.64 -5 7 -9 91.43 3.50 5 -7 9 91.04 3.03 5 -7 10 372.65 9.38 5 -7 10 373.52 9.29 -5 7 -10 378.91 9.88 -5 7 -10 356.72 10.04 5 -7 10 360.99 9.11 -5 7 -10 376.83 9.52 -5 7 -10 363.07 9.10 5 -7 10 343.20 8.61 5 -7 11 175.30 5.13 5 -7 11 170.13 4.98 -5 7 -11 175.24 5.50 5 -7 11 166.69 4.97 -5 7 -11 166.71 5.26 -5 7 -11 158.90 4.67 5 -7 11 161.19 4.61 5 -7 12 293.03 7.25 5 -7 12 273.27 6.96 -5 7 -12 277.80 7.47 5 -7 12 275.83 7.14 -5 7 -12 272.98 7.41 5 -7 12 264.64 6.76 5 -7 13 197.59 5.24 -5 7 -13 196.88 5.49 5 -7 13 191.21 5.27 -5 7 -13 194.25 5.52 5 -7 13 184.69 4.97 5 -7 14 4.99 0.55 -5 7 -14 4.08 0.57 5 -7 14 5.38 0.63 -5 7 -14 4.27 0.65 5 -7 14 4.46 0.51 5 -7 15 12.46 0.75 5 -7 15 13.53 0.87 -5 7 -15 13.05 0.91 -5 6 15 17.40 1.11 -5 6 15 19.46 1.02 5 -6 -15 20.44 1.19 5 -6 -15 20.56 1.11 5 -6 -14 0.74 0.35 -5 6 14 0.82 0.42 5 -6 -14 0.74 0.41 -5 6 14 0.98 0.35 -5 6 14 0.92 0.34 5 -6 -14 1.22 0.40 5 -6 -13 0.39 0.35 5 -6 -13 0.67 0.43 -5 6 13 0.63 0.36 -5 6 13 0.65 0.38 5 -6 -13 0.94 0.41 -5 6 12 18.49 1.38 5 -6 -12 17.22 1.33 -5 6 12 17.16 1.20 5 -6 -12 18.51 1.40 5 -6 -12 16.53 1.33 -5 6 12 17.16 1.27 5 -6 -12 19.33 1.38 -5 6 11 36.75 2.16 5 -6 -11 35.93 2.01 -5 6 11 36.40 2.03 -5 6 11 34.12 1.75 5 -6 -11 37.91 2.10 -5 6 11 35.06 1.97 5 -6 -11 35.95 1.99 5 -6 -11 31.36 1.71 -5 6 11 33.85 1.89 5 -6 -11 34.68 1.95 -5 6 10 141.99 4.98 5 -6 -10 127.72 4.01 -5 6 10 151.32 4.83 5 -6 -10 138.47 4.72 -5 6 10 146.99 4.76 -5 6 10 141.30 4.32 5 -6 -10 141.94 4.79 5 -6 -10 147.57 4.90 -5 6 10 150.52 4.75 5 -6 -10 145.67 4.71 -5 6 9 10.71 1.19 -5 6 9 10.11 1.14 -5 6 9 9.39 0.91 5 -6 -9 9.17 1.09 5 -6 -9 9.03 1.14 -5 6 9 9.07 1.00 -5 6 9 9.84 1.11 -5 6 9 7.67 0.99 5 -6 -9 11.23 1.18 -5 6 8 388.08 9.58 -5 6 8 400.13 9.86 -5 6 8 353.80 8.88 5 -6 -8 365.09 9.67 5 -6 -8 381.30 9.87 -5 6 8 376.57 9.39 -5 6 8 376.47 9.73 5 -6 -8 381.03 9.71 -5 6 7 35.09 2.20 -5 6 7 35.10 2.20 -5 6 7 36.23 2.17 -5 6 7 36.89 2.04 -5 6 7 33.56 1.67 -5 6 7 35.44 2.01 -5 6 7 35.55 2.12 5 -6 -7 32.37 2.30 -5 6 7 33.32 1.94 5 -6 -7 37.52 2.21 -5 6 7 34.75 1.96 -5 6 6 73.68 3.29 -5 6 6 73.18 2.98 -5 6 6 66.54 2.48 -5 6 6 76.55 3.12 -5 6 6 73.58 3.19 5 -6 -6 71.00 2.93 -5 6 6 76.90 3.26 -5 6 6 78.51 3.04 -5 6 6 74.05 3.05 5 -6 -5 329.80 8.56 -5 6 5 315.59 8.39 -5 6 5 342.81 8.86 -5 6 5 340.23 8.74 -5 6 5 318.83 8.39 -5 6 5 334.98 8.69 -5 6 4 442.69 10.86 -5 6 4 435.54 10.91 5 -6 -4 425.53 10.69 -5 6 4 424.54 10.36 5 -6 -4 435.77 11.18 -5 6 4 433.96 10.91 -5 6 4 431.20 10.50 -5 6 4 443.71 10.88 5 -6 -3 1.62 0.68 -5 6 3 0.70 0.49 5 -6 -3 1.07 0.89 -5 6 3 0.56 0.38 5 -6 -3 0.81 0.42 5 -6 -3 2.05 0.84 -5 6 3 0.74 0.50 -5 6 3 0.61 0.49 -5 6 3 0.54 0.42 -5 6 3 1.09 0.52 -5 6 3 1.43 0.55 -5 6 2 577.63 13.52 5 -6 -2 587.02 14.63 -5 6 2 600.34 13.63 5 -6 -2 579.68 13.60 5 -6 -2 561.32 12.78 -5 6 2 583.76 14.21 5 -6 -2 568.91 13.11 -5 6 2 581.35 13.77 -5 6 2 587.06 13.64 5 -6 -2 579.89 14.41 -5 6 2 586.64 13.35 -5 6 2 593.90 13.74 -5 6 2 603.00 13.82 5 -6 -1 1.30 0.69 -5 6 1 1.05 0.47 5 -6 -1 0.85 0.84 5 -6 -1 0.31 0.34 -5 6 1 0.55 0.61 5 -6 -1 0.50 0.48 -5 6 1 0.08 0.49 -5 6 1 0.50 0.45 5 -6 -1 0.60 0.93 -5 6 1 0.76 0.47 -5 6 1 0.48 0.41 -5 6 1 0.25 0.41 -5 6 1 1.02 0.54 5 -6 0 420.23 11.32 -5 6 0 421.07 10.25 -5 6 0 414.02 10.31 5 -6 0 419.61 10.53 5 -6 0 420.73 10.00 -5 6 0 438.17 10.92 5 -6 0 415.84 10.21 5 -6 0 441.06 10.66 -5 6 0 426.59 10.38 5 -6 0 451.14 11.22 -5 6 0 427.31 10.29 -5 6 0 427.34 10.67 -5 6 0 430.26 10.71 -5 6 -1 674.63 15.19 5 -6 1 695.10 15.27 -5 6 -1 696.45 15.94 5 -6 1 670.47 15.42 5 -6 1 716.77 15.85 -5 6 -1 666.71 15.33 5 -6 1 687.74 16.18 -5 6 -1 676.31 15.44 -5 6 -1 696.20 15.47 5 -6 1 687.55 16.48 -5 6 -2 898.90 19.54 5 -6 2 914.42 19.86 -5 6 -2 940.85 20.39 5 -6 2 912.04 20.06 5 -6 2 928.68 20.41 -5 6 -2 894.63 20.57 -5 6 -2 894.10 19.75 5 -6 2 911.87 20.65 -5 6 -2 918.67 20.07 5 -6 2 921.89 20.99 -5 6 -3 397.56 9.56 5 -6 3 421.03 10.23 -5 6 -3 427.18 10.50 5 -6 3 416.98 10.36 5 -6 3 427.50 10.68 -5 6 -3 428.49 10.88 -5 6 -3 399.97 9.81 5 -6 3 404.60 9.52 5 -6 3 418.10 10.77 -5 6 -3 423.35 10.38 -5 6 -3 415.48 10.60 5 -6 3 421.60 11.09 -5 6 -4 61.53 3.46 5 -6 4 65.74 2.79 -5 6 -4 62.09 2.73 -5 6 -4 63.35 2.80 5 -6 4 66.10 2.87 -5 6 -4 63.64 3.10 5 -6 4 62.03 3.00 -5 6 -4 60.30 2.33 5 -6 4 61.24 2.35 -5 6 -4 62.81 2.81 5 -6 4 63.51 3.22 -5 6 -4 61.31 2.87 -5 6 -5 286.32 8.84 5 -6 5 294.39 7.81 -5 6 -5 286.04 7.73 -5 6 -5 290.43 7.73 5 -6 5 282.20 7.82 -5 6 -5 306.88 8.38 -5 6 -5 290.90 8.40 5 -6 5 276.90 7.94 5 -6 5 275.66 7.21 -5 6 -5 289.07 7.90 -5 6 -5 287.44 7.94 -5 6 -6 106.16 4.63 5 -6 6 109.62 3.98 -5 6 -6 105.91 3.85 -5 6 -6 104.35 3.73 -5 6 -6 112.25 4.31 5 -6 6 107.80 4.11 -5 6 -6 106.91 4.38 5 -6 6 99.30 3.93 5 -6 6 103.52 3.54 -5 6 -6 100.41 3.93 -5 6 -6 107.05 3.95 -5 6 -7 752.59 17.50 -5 6 -7 773.20 18.66 5 -6 7 799.79 17.69 -5 6 -7 786.95 18.14 5 -6 7 780.23 17.82 -5 6 -7 789.32 18.52 5 -6 7 759.29 17.14 -5 6 -7 772.59 17.80 -5 6 -7 767.03 17.55 5 -6 7 720.54 16.59 -5 6 -8 3.67 0.96 -5 6 -8 3.13 0.70 5 -6 8 4.74 0.92 5 -6 8 3.52 0.82 -5 6 -8 4.02 0.88 5 -6 8 3.29 0.84 -5 6 -8 2.65 0.80 5 -6 8 3.78 0.71 -5 6 -8 3.54 0.81 -5 6 -8 3.64 0.68 5 -6 8 5.42 0.68 -5 6 -9 286.94 7.97 5 -6 9 295.35 8.00 -5 6 -9 294.39 8.36 5 -6 9 297.94 8.07 -5 6 -9 292.88 8.84 5 -6 9 294.33 7.80 -5 6 -9 303.91 8.31 -5 6 -9 287.09 7.67 5 -6 9 282.93 7.36 5 -6 10 33.80 2.02 5 -6 10 30.75 1.89 -5 6 -10 30.03 2.03 5 -6 10 31.70 1.95 -5 6 -10 31.77 2.31 -5 6 -10 28.93 2.05 5 -6 10 29.99 1.82 -5 6 -10 32.99 2.10 -5 6 -10 30.48 1.90 -5 6 -10 28.73 1.62 5 -6 10 31.52 1.68 5 -6 11 273.26 7.33 -5 6 -11 261.21 7.31 5 -6 11 264.38 7.14 -5 6 -11 268.52 7.52 5 -6 11 255.44 7.07 -5 6 -11 262.79 8.12 -5 6 -11 270.02 7.75 5 -6 11 263.66 7.20 -5 6 -11 271.69 7.66 5 -6 11 258.43 6.86 5 -6 12 288.09 7.47 -5 6 -12 273.99 7.51 5 -6 12 279.40 7.26 -5 6 -12 277.73 7.54 5 -6 12 285.19 7.47 -5 6 -12 285.51 7.87 5 -6 12 274.23 7.14 5 -6 13 2.09 0.50 -5 6 -13 1.82 0.52 5 -6 13 1.41 0.49 5 -6 13 1.61 0.45 -5 6 -13 1.67 0.51 5 -6 13 2.13 0.55 -5 6 -13 1.51 0.57 5 -6 14 91.14 3.01 -5 6 -14 93.08 3.17 5 -6 14 96.86 3.22 -5 6 -14 102.48 3.53 5 -6 14 92.22 3.03 -5 6 -15 127.56 3.58 5 -6 15 132.81 3.70 -5 6 -15 139.10 4.01 5 -6 15 133.96 3.56 5 -6 16 29.46 1.29 -5 6 -16 29.90 1.43 5 -6 16 28.19 1.21 -5 5 17 8.46 0.63 5 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107.67 3.50 -6 10 -1 19.47 1.05 6 -10 1 18.77 1.04 6 -10 1 19.87 1.20 -6 10 -1 20.95 1.34 -6 10 -1 19.59 1.17 -6 10 -1 20.63 1.35 6 -10 2 0.15 0.25 6 -10 2 0.50 0.34 -6 10 -2 0.33 0.37 -6 10 -2 0.60 0.31 -6 10 -2 0.58 0.42 6 -10 3 9.50 0.80 6 -10 3 9.84 0.87 -6 10 -3 11.08 1.00 -6 10 -3 8.63 0.68 -6 10 -3 10.23 0.97 6 -10 4 46.48 1.91 6 -10 4 47.46 2.02 -6 10 -4 49.08 2.21 -6 10 -4 48.65 2.17 6 -10 5 36.06 1.63 6 -10 5 35.74 1.70 -6 10 -5 39.09 1.88 6 -10 6 191.11 5.01 6 -10 6 184.22 5.08 -6 10 -6 201.97 5.38 -6 10 -6 192.65 5.21 6 -10 7 4.40 0.53 -6 10 -7 4.06 0.61 -6 10 -7 4.10 0.56 6 -10 8 337.64 7.96 6 -10 8 346.59 7.98 -6 10 -8 360.13 8.29 -6 10 -8 344.25 8.00 6 -10 9 62.27 2.05 -6 10 -9 65.90 2.24 -6 9 9 13.45 0.89 -6 9 9 12.62 0.85 6 -9 -9 12.42 0.83 6 -9 -8 1.04 0.28 -6 9 8 1.40 0.40 -6 9 8 0.97 0.37 6 -9 -8 1.12 0.35 6 -9 -7 32.05 1.51 -6 9 7 27.73 1.26 6 -9 -7 31.05 1.51 -6 9 6 97.78 3.20 -6 9 6 100.24 3.25 6 -9 -6 95.69 3.03 -6 9 5 1.76 0.51 6 -9 -5 1.39 0.36 -6 9 5 1.85 0.47 6 -9 -5 2.25 0.50 -6 9 5 2.03 0.50 -6 9 4 181.59 5.11 6 -9 -4 157.13 4.44 -6 9 4 171.31 4.89 -6 9 4 172.21 5.11 6 -9 -4 169.23 4.80 -6 9 4 169.96 4.97 -6 9 3 53.23 2.33 6 -9 -3 48.54 1.91 6 -9 -3 49.23 2.18 6 -9 -3 44.71 1.84 -6 9 3 48.05 2.26 -6 9 3 52.12 2.37 6 -9 -3 50.01 2.14 -6 9 3 53.23 2.36 -6 9 2 108.15 3.62 6 -9 -2 99.16 3.24 6 -9 -2 99.04 3.40 -6 9 2 105.88 3.70 -6 9 2 103.34 3.66 6 -9 -2 101.01 3.37 -6 9 2 107.42 3.76 -6 9 1 313.88 7.77 6 -9 -1 303.18 7.57 6 -9 -1 285.86 7.50 -6 9 1 301.27 8.08 -6 9 1 307.51 7.90 6 -9 -1 294.02 7.46 -6 9 1 309.54 8.08 -6 9 0 67.74 2.58 6 -9 0 60.51 2.30 6 -9 0 63.81 2.56 6 -9 0 60.85 2.42 -6 9 0 66.34 2.87 -6 9 0 65.97 2.69 6 -9 0 62.66 2.41 -6 9 0 68.46 2.92 -6 9 -1 564.23 12.80 6 -9 1 553.75 12.79 6 -9 1 574.90 13.16 -6 9 -1 603.51 13.67 -6 9 -1 569.07 13.09 6 -9 1 532.91 12.57 -6 9 -1 607.95 13.70 -6 9 -2 309.85 7.65 6 -9 2 326.61 8.41 6 -9 2 319.48 7.99 6 -9 2 323.93 8.27 -6 9 -2 327.94 8.70 -6 9 -2 320.43 8.02 -6 9 -2 340.14 8.68 6 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534.53 12.45 6 -8 0 533.51 12.92 6 -8 0 519.70 12.14 6 -8 0 501.03 12.80 -6 8 0 535.78 13.13 -6 8 0 535.16 12.66 -6 8 0 555.35 13.17 -6 8 -1 303.68 7.71 6 -8 1 294.04 7.70 6 -8 1 289.83 8.15 6 -8 1 304.76 8.01 -6 8 -1 314.23 8.63 -6 8 -1 307.68 7.97 -6 8 -1 320.27 8.55 -6 8 -2 206.05 5.54 6 -8 2 204.35 6.23 6 -8 2 218.70 5.94 6 -8 2 200.66 6.10 6 -8 2 218.44 6.19 -6 8 -2 208.97 6.54 -6 8 -2 211.07 5.86 -6 8 -2 207.38 5.82 6 -8 3 2.33 0.78 6 -8 3 2.25 0.60 6 -8 3 2.33 0.68 -6 8 -3 1.99 0.71 -6 8 -3 2.39 0.51 -6 8 -3 2.77 0.58 6 -8 4 58.60 2.71 6 -8 4 58.75 2.58 6 -8 4 51.25 2.38 6 -8 4 54.58 2.61 -6 8 -4 55.43 2.95 -6 8 -4 55.13 2.45 -6 8 -4 55.17 2.73 6 -8 5 503.48 12.05 6 -8 5 528.93 12.04 6 -8 5 507.00 12.14 -6 8 -5 479.79 11.80 -6 8 -5 460.53 12.25 -6 8 -5 511.19 12.31 6 -8 6 282.57 7.54 6 -8 6 297.51 7.66 6 -8 6 288.57 7.75 -6 8 -6 267.79 7.43 -6 8 -6 290.98 7.80 6 -8 7 69.04 2.75 6 -8 7 74.62 2.95 -6 8 -7 70.76 3.24 6 -8 7 67.24 2.43 -6 8 -7 68.82 2.81 -6 8 -7 69.97 2.90 6 -8 8 56.20 2.30 6 -8 8 61.38 2.59 -6 8 -8 66.15 2.94 6 -8 8 55.94 2.18 -6 8 -8 58.53 2.51 -6 8 -8 59.98 2.51 6 -8 9 291.60 7.28 6 -8 9 332.58 8.00 6 -8 9 314.68 7.91 -6 8 -9 330.01 8.28 6 -8 9 300.13 7.42 -6 8 -9 303.72 7.81 -6 8 -9 309.67 7.64 6 -8 10 1.06 0.42 -6 8 -10 0.12 0.38 6 -8 10 0.48 0.31 -6 8 -10 0.10 0.33 -6 8 -10 1.37 0.34 6 -8 11 114.35 3.46 -6 8 -11 118.92 3.62 6 -8 11 105.14 3.19 -6 8 -11 106.67 3.41 6 -8 12 89.39 2.71 -6 8 -12 87.59 2.71 6 -8 12 84.43 2.55 6 -7 -13 14.49 0.94 -6 7 13 14.16 0.86 6 -7 -13 14.12 0.92 -6 7 12 40.31 1.77 6 -7 -12 43.86 1.89 -6 7 12 44.65 1.84 6 -7 -12 44.49 1.88 -6 7 11 210.03 5.64 6 -7 -11 187.17 5.27 -6 7 11 194.85 5.41 6 -7 -11 203.47 5.59 -6 7 11 213.65 5.57 6 -7 -11 205.06 5.57 -6 7 10 106.52 3.53 6 -7 -10 93.06 3.22 -6 7 10 99.23 3.28 6 -7 -10 99.45 3.43 6 -7 -10 97.59 3.37 -6 7 10 104.51 3.49 6 -7 -10 101.34 3.44 6 -7 -9 176.60 5.29 -6 7 9 228.70 6.15 6 -7 -9 194.66 5.77 -6 7 9 203.44 5.76 6 -7 -9 214.86 6.05 6 -7 -9 216.93 6.17 6 -7 -9 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156.99 5.26 6 -7 7 155.71 5.11 -6 7 -7 145.38 5.40 6 -7 7 139.32 4.30 -6 7 -7 146.46 4.95 -6 7 -7 145.99 4.72 6 -7 8 365.31 9.32 6 -7 8 390.76 9.65 -6 7 -8 384.69 9.96 6 -7 8 381.21 9.75 -6 7 -8 376.63 10.35 6 -7 8 362.90 9.05 -6 7 -8 379.41 9.78 -6 7 -8 370.01 9.28 6 -7 9 80.93 2.97 6 -7 9 86.76 3.30 6 -7 9 82.58 3.23 -6 7 -9 88.90 3.50 6 -7 9 81.64 2.98 -6 7 -9 85.64 3.41 -6 7 -9 81.55 2.88 6 -7 10 196.96 5.35 6 -7 10 215.97 5.92 6 -7 10 205.44 5.66 -6 7 -10 211.23 6.13 6 -7 11 36.53 1.82 6 -7 11 36.91 1.78 -6 7 -11 33.94 1.79 6 -7 11 34.37 1.68 -6 7 -11 34.87 1.90 6 -7 12 1.82 0.47 6 -7 12 1.51 0.41 -6 7 -12 1.32 0.40 6 -7 12 1.45 0.41 -6 7 -12 1.75 0.51 6 -7 13 2.80 0.46 6 -7 13 3.03 0.46 -6 7 -13 3.20 0.54 6 -7 14 28.97 1.24 -6 7 -14 30.22 1.38 6 -6 -14 24.04 1.27 6 -6 -14 27.63 1.29 6 -6 -13 139.79 4.17 -6 6 13 125.50 3.98 -6 6 13 129.53 3.60 -6 6 13 142.79 4.05 6 -6 -13 144.82 4.08 6 -6 -12 527.51 12.31 -6 6 12 522.64 12.12 6 -6 -12 548.74 12.22 -6 6 12 553.71 12.16 6 -6 -12 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0.86 0.34 6 -5 1 0.40 0.92 -6 5 -1 1.01 0.58 -6 5 -1 2.13 0.72 -6 5 -1 1.91 0.57 -6 5 -2 134.64 5.44 6 -5 2 131.99 4.31 -6 5 -2 132.51 4.79 6 -5 2 134.63 4.70 -6 5 -2 134.44 4.65 -6 5 -2 135.39 4.68 6 -5 2 129.09 5.28 -6 5 -2 129.18 4.45 -6 5 -3 36.53 2.66 6 -5 3 41.65 2.16 -6 5 -3 40.23 2.31 -6 5 -3 39.75 2.35 6 -5 3 36.75 2.27 -6 5 -3 36.72 2.19 6 -5 3 34.92 1.65 -6 5 -3 35.28 2.18 -6 5 -3 37.30 2.07 -6 5 -4 97.15 4.56 -6 5 -4 104.77 4.05 -6 5 -4 105.38 4.10 6 -5 4 99.60 4.00 -6 5 -4 105.98 3.99 -6 5 -4 99.43 4.30 6 -5 4 94.85 3.25 -6 5 -4 105.28 4.08 -6 5 -4 100.55 3.66 -6 5 -5 72.64 3.86 -6 5 -5 75.66 3.35 -6 5 -5 74.45 3.27 -6 5 -5 79.05 3.77 6 -5 5 72.54 2.79 -6 5 -5 76.10 3.40 -6 5 -5 73.22 2.95 -6 5 -6 49.47 3.04 -6 5 -6 46.00 2.57 -6 5 -6 44.07 2.43 -6 5 -6 44.36 2.81 6 -5 6 45.63 2.16 -6 5 -6 45.32 2.58 -6 5 -6 46.80 2.17 -6 5 -7 14.40 1.65 6 -5 7 14.18 1.42 -6 5 -7 12.90 1.35 6 -5 7 15.07 1.52 -6 5 -7 14.53 1.32 -6 5 -7 14.73 1.60 6 -5 7 12.85 1.16 -6 5 -7 15.96 1.52 -6 5 -7 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22.61 1.81 -7 7 -2 25.03 1.73 -7 7 -3 2.94 0.71 7 -7 3 2.41 0.60 -7 7 -3 2.59 0.73 7 -7 3 2.48 0.73 -7 7 -3 2.78 0.72 7 -7 3 1.22 0.63 7 -7 3 2.54 0.95 -7 7 -3 3.04 0.72 -7 7 -3 2.00 0.65 -7 7 -3 2.72 0.66 -7 7 -4 6.46 0.93 7 -7 4 7.89 1.10 7 -7 4 9.24 0.99 -7 7 -4 8.73 1.06 7 -7 4 7.62 0.99 -7 7 -4 7.78 1.08 7 -7 4 7.43 1.12 -7 7 -4 7.43 0.99 -7 7 -4 6.47 1.04 -7 7 -4 8.01 0.96 -7 7 -5 20.21 1.49 7 -7 5 20.05 1.56 7 -7 5 19.88 1.43 -7 7 -5 18.78 1.45 7 -7 5 17.99 1.46 -7 7 -5 18.42 1.52 -7 7 -5 19.80 1.53 -7 7 -5 19.05 1.38 -7 7 -6 279.56 7.60 7 -7 6 278.27 7.63 7 -7 6 289.16 7.62 7 -7 6 284.56 7.71 -7 7 -6 288.66 7.84 -7 7 -6 290.46 7.88 -7 7 -6 291.99 7.37 7 -7 7 25.10 1.60 7 -7 7 24.83 1.58 7 -7 7 24.91 1.65 -7 7 -7 27.09 1.67 7 -7 7 23.00 1.67 -7 7 -7 24.92 1.68 -7 7 -7 25.05 1.36 7 -7 8 53.39 2.30 7 -7 8 55.50 2.39 -7 7 -8 55.02 2.34 7 -7 8 50.55 1.95 -7 7 -8 51.69 2.46 7 -7 9 20.83 1.25 7 -7 9 22.71 1.40 7 -7 9 21.20 1.37 -7 7 -9 20.30 1.25 7 -7 9 20.65 1.12 -7 7 -9 22.41 1.48 7 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43.46 2.19 -7 6 -5 132.83 5.46 7 -6 5 134.28 4.47 -7 6 -5 131.51 4.71 7 -6 5 129.86 4.55 -7 6 -5 131.18 4.63 7 -6 5 134.54 4.79 7 -6 5 129.33 5.02 -7 6 -5 130.70 4.72 -7 6 -5 127.26 5.02 -7 6 -5 132.81 4.21 -7 6 -6 8.84 1.41 7 -6 6 8.92 1.07 -7 6 -6 7.97 1.03 7 -6 6 8.40 1.12 -7 6 -6 7.67 0.98 7 -6 6 7.91 0.77 7 -6 6 7.36 1.24 -7 6 -6 9.31 1.16 -7 6 -6 8.66 0.84 -7 6 -7 96.15 4.31 7 -6 7 104.44 3.76 -7 6 -7 97.20 3.71 7 -6 7 100.64 3.77 -7 6 -7 98.99 3.57 7 -6 7 103.37 3.93 7 -6 7 98.22 3.22 -7 6 -7 105.59 3.99 -7 6 -8 38.59 2.47 7 -6 8 42.68 2.17 -7 6 -8 39.00 2.05 -7 6 -8 40.43 1.92 7 -6 8 40.91 2.25 7 -6 8 37.55 1.77 -7 6 -8 39.74 2.25 7 -6 9 53.66 2.39 7 -6 9 48.33 2.30 -7 6 -9 49.10 1.98 7 -6 9 49.52 2.39 7 -6 9 49.37 2.05 -7 6 -9 54.65 2.56 7 -6 10 85.76 2.87 7 -6 10 90.21 3.14 7 -6 10 86.32 2.86 -7 6 -10 90.56 3.37 7 -6 11 15.11 1.05 7 -6 11 14.21 0.94 -7 6 -11 15.90 1.20 7 -6 12 29.39 1.41 7 -6 12 31.14 1.34 7 -6 12 29.24 1.31 -7 6 -12 31.88 1.59 -7 6 -13 0.46 0.30 7 -5 -14 7.05 0.74 -7 5 14 6.58 0.64 7 -5 -14 8.03 0.75 7 -5 -14 6.24 0.66 7 -5 -13 74.08 2.93 -7 5 13 76.75 2.66 7 -5 -13 84.86 2.96 7 -5 -13 84.62 2.81 7 -5 -13 79.27 2.59 7 -5 -12 74.02 3.06 -7 5 12 66.65 2.61 7 -5 -12 78.72 3.00 7 -5 -12 79.51 2.87 -7 5 12 80.78 2.92 -7 5 12 70.31 2.95 7 -5 -12 77.27 2.70 -7 5 11 0.13 0.31 7 -5 -11 0.07 0.42 7 -5 -11 0.28 0.40 7 -5 -11 0.12 0.42 -7 5 11 0.07 0.42 -7 5 11 0.15 0.38 -7 5 11 0.18 0.56 7 -5 -11 -0.08 0.40 -7 5 10 4.82 1.06 -7 5 10 4.63 0.69 7 -5 -10 3.39 0.75 7 -5 -10 3.81 0.75 7 -5 -10 4.31 0.78 -7 5 10 4.93 0.88 -7 5 10 4.40 0.76 -7 5 10 4.24 0.89 7 -5 -10 4.18 0.72 -7 5 9 22.26 1.87 -7 5 9 17.51 1.34 7 -5 -9 20.77 1.63 -7 5 9 22.69 1.65 -7 5 9 20.62 1.67 7 -5 -9 19.40 1.50 -7 5 8 9.00 1.27 -7 5 8 9.44 0.93 7 -5 -8 10.28 1.25 -7 5 8 10.19 1.18 -7 5 8 9.41 1.08 7 -5 -8 8.74 1.60 -7 5 8 9.10 1.16 -7 5 7 13.09 1.48 7 -5 -7 11.86 1.04 -7 5 7 14.10 1.08 7 -5 -7 13.81 1.49 -7 5 7 14.16 1.37 -7 5 7 14.00 1.28 -7 5 7 15.96 1.47 -7 5 6 11.39 1.41 7 -5 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3.10 8 -6 -6 89.51 3.69 -8 6 6 99.93 3.62 -8 6 6 91.39 3.24 -8 6 6 98.47 3.62 -8 6 5 17.01 1.51 8 -6 -5 14.85 1.16 8 -6 -5 16.17 1.56 -8 6 5 14.09 1.10 -8 6 5 15.21 1.36 -8 6 4 52.80 2.70 8 -6 -4 50.25 2.32 8 -6 -4 51.15 2.76 -8 6 4 49.49 2.16 -8 6 4 53.22 2.59 -8 6 3 110.51 4.13 8 -6 -3 101.64 3.69 -8 6 3 104.81 4.35 8 -6 -3 105.91 4.20 -8 6 3 105.69 3.93 -8 6 3 101.54 3.32 -8 6 3 108.18 3.98 -8 6 2 2.08 0.71 8 -6 -2 2.33 0.74 -8 6 2 1.69 0.80 -8 6 2 1.54 0.62 -8 6 2 1.89 0.42 -8 6 2 1.85 0.64 -8 6 1 122.65 4.49 8 -6 -1 122.91 4.27 -8 6 1 126.54 4.82 8 -6 -1 118.30 3.78 -8 6 1 126.98 4.36 -8 6 1 122.32 4.40 -8 6 0 129.05 4.65 8 -6 0 129.61 4.51 -8 6 0 129.50 4.90 8 -6 0 126.77 4.11 -8 6 0 139.89 4.58 8 -6 0 131.03 4.48 -8 6 0 136.93 4.67 -8 6 -1 61.99 2.91 8 -6 1 55.94 2.26 -8 6 -1 56.58 2.97 8 -6 1 58.74 2.52 -8 6 -1 58.45 2.67 8 -6 1 57.44 2.74 -8 6 -1 61.83 2.85 -8 6 -2 128.36 4.50 8 -6 2 118.16 3.84 -8 6 -2 120.37 4.59 8 -6 2 123.66 4.12 -8 6 -2 126.66 4.24 8 -6 2 127.05 4.42 -8 6 -2 126.99 4.45 -8 6 -3 246.90 7.10 8 -6 3 241.09 6.53 -8 6 -3 248.73 7.27 8 -6 3 243.55 6.74 -8 6 -3 247.06 6.74 8 -6 3 249.36 7.09 -8 6 -3 249.59 7.10 -8 6 -4 10.75 1.16 8 -6 4 10.19 0.98 -8 6 -4 10.17 1.20 8 -6 4 11.76 1.14 -8 6 -4 11.96 1.04 8 -6 4 11.39 1.24 -8 6 -4 12.06 1.23 -8 6 -5 752.18 16.86 8 -6 5 743.61 16.38 -8 6 -5 733.93 16.88 8 -6 5 725.08 16.54 -8 6 -5 712.18 16.08 8 -6 5 731.78 16.87 -8 6 -5 735.11 16.88 -8 6 -6 20.32 1.48 8 -6 6 22.38 1.41 -8 6 -6 20.60 1.48 8 -6 6 21.76 1.47 -8 6 -6 18.85 1.12 -8 6 -6 22.53 1.56 -8 6 -7 145.21 4.61 8 -6 7 157.06 4.48 -8 6 -7 142.29 4.46 8 -6 7 149.94 4.50 -8 6 -7 153.16 4.69 8 -6 8 211.15 5.51 -8 6 -8 192.39 5.38 8 -6 8 209.48 5.57 -8 6 -8 211.95 5.77 -8 6 -9 1.11 0.41 8 -6 9 2.13 0.46 8 -6 9 2.31 0.48 -8 6 -9 1.67 0.46 -8 6 -10 0.88 0.32 8 -6 10 1.96 0.39 8 -6 10 2.10 0.41 -8 6 -10 1.45 0.38 8 -5 -13 31.58 1.38 8 -5 -12 0.54 0.34 8 -5 -12 0.11 0.26 -8 5 12 0.37 0.44 -8 5 11 4.76 0.52 8 -5 -11 5.59 0.70 8 -5 -11 5.57 0.66 -8 5 11 5.78 0.83 8 -5 -11 5.64 0.61 -8 5 10 4.47 0.53 8 -5 -10 6.23 0.81 8 -5 -10 5.64 0.73 8 -5 -10 6.40 0.77 -8 5 10 5.96 0.91 8 -5 -10 6.44 0.72 -8 5 9 1.41 0.68 -8 5 9 0.71 0.29 8 -5 -9 0.68 0.44 -8 5 9 0.46 0.50 -8 5 9 0.54 0.59 8 -5 -9 1.24 0.47 -8 5 8 30.72 2.02 8 -5 -8 26.36 1.77 -8 5 8 29.54 1.84 -8 5 8 27.10 1.84 -8 5 7 193.00 6.05 8 -5 -7 176.42 5.79 -8 5 7 186.11 5.40 -8 5 7 201.51 5.95 -8 5 6 88.67 3.71 8 -5 -6 86.62 2.96 8 -5 -6 83.24 3.62 -8 5 6 81.57 3.09 -8 5 6 89.80 3.58 -8 5 5 306.00 8.59 8 -5 -5 288.56 7.65 8 -5 -5 301.15 8.55 -8 5 5 315.71 8.29 -8 5 5 291.48 7.67 -8 5 5 324.56 8.49 -8 5 4 183.67 5.93 8 -5 -4 168.15 5.18 -8 5 4 184.54 6.20 -8 5 4 177.88 5.56 -8 5 4 167.44 4.95 8 -5 -4 177.81 6.42 -8 5 4 186.34 5.77 -8 5 3 20.81 1.75 8 -5 -3 20.73 1.52 -8 5 3 19.96 1.86 -8 5 3 21.32 1.60 8 -5 -3 22.45 2.15 -8 5 3 21.15 1.27 -8 5 3 21.84 1.72 -8 5 2 63.00 3.10 -8 5 2 67.72 3.38 8 -5 -2 59.29 2.37 -8 5 2 62.51 2.85 8 -5 -2 61.20 2.70 8 -5 -2 65.95 3.61 -8 5 2 66.17 3.06 -8 5 1 0.88 0.67 -8 5 1 1.00 0.76 8 -5 -1 1.89 0.55 -8 5 1 0.90 0.54 8 -5 -1 0.57 0.56 -8 5 1 1.77 0.70 -8 5 1 0.77 0.53 -8 5 0 1.36 0.68 -8 5 0 2.36 0.94 8 -5 0 1.83 0.50 -8 5 0 1.13 0.72 8 -5 0 1.77 0.57 -8 5 0 1.47 0.56 8 -5 0 1.64 0.68 -8 5 0 1.60 0.68 -8 5 0 1.65 0.71 -8 5 -1 172.13 5.61 8 -5 1 151.91 4.69 -8 5 -1 167.78 5.79 8 -5 1 163.98 5.03 8 -5 1 164.89 5.35 -8 5 -1 163.43 5.07 8 -5 1 170.11 6.25 -8 5 -1 166.68 5.52 -8 5 -1 170.88 5.93 -8 5 -2 198.32 6.22 8 -5 2 188.48 5.55 -8 5 -2 205.77 6.49 8 -5 2 191.70 5.74 8 -5 2 202.21 6.14 -8 5 -2 192.32 5.61 8 -5 2 193.63 6.80 -8 5 -2 204.68 6.28 -8 5 -3 11.19 1.26 -8 5 -3 11.21 1.51 8 -5 3 11.33 1.08 -8 5 -3 12.96 1.41 8 -5 3 11.92 1.20 8 -5 3 12.17 1.32 -8 5 -3 11.50 1.01 -8 5 -3 10.65 1.21 -8 5 -4 642.59 14.92 -8 5 -4 601.99 15.61 8 -5 4 612.50 14.28 -8 5 -4 635.40 15.05 8 -5 4 619.80 14.44 8 -5 4 623.45 14.77 -8 5 -4 594.56 13.75 -8 5 -4 626.01 14.86 8 -5 5 5.96 0.86 -8 5 -5 5.58 1.09 -8 5 -5 4.65 0.89 8 -5 5 5.24 0.87 8 -5 5 4.70 0.90 -8 5 -5 5.06 0.88 -8 5 -6 270.44 8.24 8 -5 6 285.59 7.40 -8 5 -6 279.56 7.74 8 -5 6 274.36 7.45 8 -5 6 284.48 7.70 -8 5 -7 74.49 3.46 8 -5 7 81.78 3.02 -8 5 -7 79.99 3.19 8 -5 7 82.73 3.10 -8 5 -8 35.17 2.13 8 -5 8 37.46 1.84 -8 5 -8 37.64 1.92 8 -5 8 35.11 1.84 -8 5 -9 0.41 0.49 8 -5 9 0.82 0.42 -8 5 -9 -0.22 0.38 8 -5 9 0.20 0.23 8 -5 10 16.79 1.05 8 -5 10 19.72 1.10 -8 5 -10 19.95 1.17 8 -4 -13 22.13 1.32 8 -4 -13 26.49 1.28 8 -4 -12 16.44 1.23 -8 4 12 14.66 0.91 8 -4 -12 17.46 1.14 8 -4 -12 19.79 1.09 -8 4 12 17.36 1.29 -8 4 11 0.91 0.32 8 -4 -11 0.30 0.38 8 -4 -11 0.42 0.34 -8 4 11 0.71 0.57 8 -4 -11 0.28 0.28 -8 4 10 8.86 1.11 -8 4 10 7.47 0.69 8 -4 -10 8.31 0.95 8 -4 -10 7.86 0.84 8 -4 -10 7.98 0.88 -8 4 10 7.84 1.06 8 -4 -10 7.70 0.78 -8 4 9 210.94 6.32 -8 4 9 192.81 5.14 8 -4 -9 201.73 5.80 -8 4 9 219.53 6.22 8 -4 -9 194.61 5.60 -8 4 8 83.63 3.52 -8 4 8 72.71 2.50 8 -4 -8 77.01 3.20 -8 4 8 83.38 3.33 -8 4 8 80.46 3.40 -8 4 7 212.08 6.69 8 -4 -7 210.18 6.52 -8 4 7 224.82 6.49 -8 4 7 230.77 6.71 -8 4 6 135.60 4.91 8 -4 -6 126.22 4.71 -8 4 6 140.46 4.65 -8 4 6 132.07 4.72 -8 4 5 433.13 11.40 8 -4 -5 416.97 10.35 -8 4 5 452.47 11.04 8 -4 -5 429.06 11.98 -8 4 5 467.36 11.39 -8 4 4 87.61 3.78 -8 4 4 86.69 3.46 8 -4 -4 84.54 4.19 -8 4 4 89.33 3.70 -8 4 3 335.07 9.16 -8 4 3 327.62 8.62 8 -4 -3 304.77 9.61 -8 4 3 331.66 8.99 -8 4 2 80.24 3.60 -8 4 2 72.65 3.74 -8 4 2 76.05 3.69 8 -4 -2 77.03 2.84 8 -4 -2 78.06 3.14 -8 4 2 80.49 3.20 8 -4 -2 84.95 4.16 -8 4 2 84.02 3.54 -8 4 1 21.66 1.80 -8 4 1 20.02 1.95 -8 4 1 21.87 1.91 8 -4 -1 20.33 1.39 8 -4 -1 20.90 1.59 -8 4 1 20.72 1.49 8 -4 -1 22.03 2.19 -8 4 0 77.55 3.49 -8 4 0 73.26 3.77 8 -4 0 69.10 2.71 -8 4 0 78.98 3.68 8 -4 0 73.55 3.20 -8 4 0 75.09 2.94 8 -4 0 79.26 4.02 -8 4 0 75.59 3.64 -8 4 -1 324.54 8.85 -8 4 -1 295.27 9.27 -8 4 -1 314.85 8.99 8 -4 1 303.52 8.44 -8 4 -1 302.79 7.82 8 -4 1 311.77 9.48 -8 4 -1 314.61 9.09 -8 4 -2 6.55 1.07 -8 4 -2 6.83 1.14 -8 4 -2 7.18 0.78 8 -4 2 5.30 0.99 -8 4 -2 6.83 1.09 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9 436.56 10.93 -8 3 9 429.61 9.82 8 -3 -9 438.42 10.26 -8 3 8 42.75 2.45 -8 3 8 37.97 1.70 8 -3 -8 42.68 2.20 -8 3 8 42.14 2.25 -8 3 7 92.76 3.84 -8 3 7 85.30 2.79 8 -3 -7 96.68 3.68 -8 3 7 93.66 3.60 -8 3 6 951.33 21.71 -8 3 6 937.20 21.88 8 -3 -6 932.80 21.46 -8 3 6 972.51 21.26 -8 3 5 3.00 0.88 -8 3 5 3.19 0.92 -8 3 5 2.87 0.66 8 -3 -5 2.90 1.14 -8 3 4 390.03 10.42 -8 3 4 408.63 10.78 -8 3 4 416.55 9.98 8 -3 -4 401.87 11.16 -8 3 4 407.36 10.39 -8 3 3 159.83 5.45 -8 3 3 142.59 5.47 -8 3 3 149.58 5.52 -8 3 3 158.15 4.87 8 -3 -3 164.46 6.10 -8 3 3 167.52 5.43 -8 3 2 37.59 2.35 -8 3 2 35.95 2.49 -8 3 2 37.30 2.46 8 -3 -2 35.71 2.01 -8 3 2 38.57 1.98 8 -3 -2 37.79 2.76 -8 3 2 39.21 2.32 -8 3 1 63.38 3.10 -8 3 1 57.03 3.25 8 -3 -1 62.29 2.82 -8 3 1 62.76 2.52 8 -3 -1 59.40 3.51 -8 3 1 60.21 2.96 -8 3 0 117.79 4.50 -8 3 0 108.38 4.70 8 -3 0 117.91 4.24 -8 3 0 111.38 3.60 8 -3 0 123.18 5.17 -8 3 0 123.70 4.44 -8 3 0 118.79 4.71 -8 3 -1 0.75 0.66 -8 3 -1 1.55 0.81 8 -3 1 1.71 0.72 -8 3 -1 1.43 0.63 -8 3 -1 0.99 0.57 -8 3 -2 174.43 5.70 -8 3 -2 155.99 5.96 -8 3 -2 181.00 5.96 8 -3 2 172.20 5.61 -8 3 -2 171.88 5.55 -8 3 -2 166.12 5.80 -8 3 -3 304.05 8.63 -8 3 -3 321.55 8.96 8 -3 3 309.08 8.60 -8 3 -3 315.72 8.50 -8 3 -4 21.67 1.96 -8 3 -4 23.62 1.86 8 -3 4 22.78 1.77 -8 3 -4 20.69 1.59 -8 3 -5 234.03 7.24 8 -3 5 222.93 6.66 8 -3 5 219.01 5.72 -8 3 -5 217.23 6.36 -8 3 -6 78.81 3.57 8 -3 6 77.68 3.26 8 -3 6 73.22 2.60 -8 3 -6 75.01 3.00 -8 3 -7 343.54 9.33 8 -3 7 342.46 8.15 -8 3 -7 344.83 8.58 8 -3 8 47.19 1.86 -8 3 -8 44.96 1.97 -8 3 -9 36.42 1.94 8 -3 9 30.55 1.59 -8 3 -9 37.20 1.85 8 -3 9 33.74 1.44 -8 3 -9 31.55 1.48 -8 3 -10 25.46 1.37 8 -3 10 25.84 1.27 8 -2 -14 76.82 2.63 8 -2 -13 48.51 1.95 -8 2 13 44.55 1.71 8 -2 -12 6.29 0.77 -8 2 12 7.52 0.68 -8 2 12 6.34 0.86 -8 2 11 13.92 0.96 8 -2 -11 15.38 1.05 -8 2 11 14.16 1.28 -8 2 10 37.74 2.12 -8 2 10 36.60 1.67 8 -2 -10 38.15 1.88 -8 2 10 39.76 2.17 -8 2 9 96.66 3.73 -8 2 9 94.41 3.08 -8 2 9 98.74 3.76 -8 2 8 55.84 2.74 -8 2 8 53.04 2.08 -8 2 8 55.39 2.70 -8 2 7 492.54 11.90 -8 2 7 493.32 11.80 -8 2 6 235.90 7.08 -8 2 6 236.19 7.16 8 -2 -6 243.73 6.86 -8 2 6 247.13 7.08 -8 2 5 408.33 10.55 -8 2 5 386.14 10.57 -8 2 5 414.90 10.49 -8 2 4 37.21 2.24 -8 2 4 32.44 2.07 -8 2 4 36.54 2.31 -8 2 4 31.93 1.54 -8 2 4 33.21 1.82 8 -2 -4 37.78 2.60 -8 2 4 36.89 2.19 -8 2 3 156.57 5.23 -8 2 3 139.46 5.18 -8 2 3 157.50 5.40 -8 2 3 138.83 4.39 8 -2 -3 159.85 5.82 -8 2 3 157.58 5.12 -8 2 2 3.51 0.82 -8 2 2 2.52 0.84 -8 2 2 3.03 0.84 8 -2 -2 2.48 1.16 -8 2 2 3.90 0.80 -8 2 1 10.54 1.25 -8 2 1 11.50 1.37 -8 2 1 10.88 1.34 8 -2 -1 11.78 1.22 8 -2 -1 10.86 1.60 -8 2 1 12.32 1.25 -8 2 0 123.97 4.55 -8 2 0 123.75 4.91 -8 2 0 125.55 4.77 8 -2 0 126.88 4.44 -8 2 0 127.33 4.43 -8 2 -1 145.98 5.07 -8 2 -1 152.43 5.54 -8 2 -1 151.74 5.34 8 -2 1 152.07 5.07 -8 2 -1 150.83 4.94 -8 2 -2 181.92 5.79 -8 2 -2 178.97 6.26 -8 2 -2 190.90 6.15 8 -2 2 186.55 5.89 -8 2 -2 180.38 5.58 -8 2 -3 6.44 0.96 -8 2 -3 7.22 1.15 8 -2 3 7.60 1.10 -8 2 -3 7.39 0.91 -8 2 -4 208.13 6.23 8 -2 4 204.77 6.34 8 -2 4 213.29 5.54 -8 2 -4 205.44 5.91 -8 2 -5 27.70 2.06 8 -2 5 27.25 1.87 8 -2 5 27.12 1.46 -8 2 -5 26.72 1.56 -8 2 -6 52.24 2.73 8 -2 6 50.39 2.05 -8 2 -6 47.47 2.06 8 -2 7 87.86 2.85 -8 2 -7 80.35 2.72 -8 2 -8 51.00 2.43 8 -2 8 47.84 1.87 -8 2 -9 21.95 1.41 8 -2 9 21.25 1.07 -8 1 13 4.06 0.47 -8 1 13 3.82 0.50 8 -1 -13 3.94 0.57 -8 1 12 76.14 2.54 -8 1 12 89.94 2.84 8 -1 -11 65.47 2.51 -8 1 11 63.12 2.31 -8 1 11 72.88 2.58 -8 1 11 70.75 2.75 -8 1 10 10.56 0.84 -8 1 10 10.96 0.95 -8 1 10 11.16 1.12 -8 1 9 36.35 1.98 -8 1 9 35.73 1.65 -8 1 9 37.55 1.83 -8 1 9 36.62 2.02 -8 1 8 147.38 4.66 -8 1 8 135.23 4.01 -8 1 8 143.00 4.29 -8 1 8 146.94 4.71 -8 1 7 123.73 4.26 -8 1 7 120.39 3.59 -8 1 7 125.12 3.88 -8 1 7 134.78 4.41 -8 1 6 255.82 7.18 -8 1 6 254.77 6.58 -8 1 6 265.84 7.24 -8 1 5 243.93 6.91 -8 1 5 246.36 7.03 -8 1 5 232.49 6.11 -8 1 5 255.69 6.93 -8 1 4 1.01 0.60 -8 1 4 0.51 0.47 -8 1 4 0.95 0.60 -8 1 4 0.45 0.49 -8 1 3 124.83 4.27 -8 1 3 112.12 4.22 -8 1 3 117.51 4.37 -8 1 3 119.58 4.12 -8 1 2 1.19 0.56 -8 1 2 0.69 0.54 -8 1 2 1.37 0.62 -8 1 2 1.16 0.52 -8 1 1 5.45 0.83 -8 1 1 5.03 0.90 -8 1 1 5.05 0.98 -8 1 1 5.10 0.95 8 -1 -1 4.91 0.85 -8 1 1 5.33 0.80 -8 1 0 23.50 1.62 -8 1 0 22.41 1.78 -8 1 0 24.60 1.92 -8 1 0 26.78 1.90 8 -1 0 23.09 1.66 -8 1 0 22.59 1.50 -8 1 -1 54.98 2.55 -8 1 -1 52.81 2.83 -8 1 -1 55.68 2.91 -8 1 -1 53.82 2.76 -8 1 -1 51.48 2.29 -8 1 -2 1.56 0.56 -8 1 -2 1.43 0.67 -8 1 -2 1.52 0.67 -8 1 -2 1.62 0.64 -8 1 -2 1.16 0.44 -8 1 -3 125.49 4.15 -8 1 -3 123.07 4.70 -8 1 -3 134.43 4.81 -8 1 -3 134.11 4.60 -8 1 -3 114.87 3.68 -8 1 -4 112.25 3.80 -8 1 -4 112.82 4.40 -8 1 -4 116.77 4.41 -8 1 -5 17.03 1.20 8 -1 5 17.18 1.13 -8 1 -6 10.49 0.89 -8 1 -6 11.91 1.21 8 -1 6 11.16 0.89 -8 1 -7 14.73 0.97 8 -1 7 17.07 1.05 8 -1 7 16.43 0.94 -8 1 -8 67.11 2.63 8 -1 8 61.96 2.11 -8 0 12 8.39 0.69 -8 0 12 12.05 0.83 -8 0 11 2.15 0.41 -8 0 11 2.78 0.48 -8 0 10 0.21 0.26 -8 0 10 1.13 0.37 -8 0 9 74.16 2.60 -8 0 9 79.29 2.75 -8 0 8 146.89 4.13 -8 0 8 156.13 4.35 -8 0 8 152.96 4.48 -8 0 7 28.67 1.37 -8 0 7 28.46 1.46 -8 0 7 29.85 1.61 -8 0 6 182.25 5.19 -8 0 6 195.24 5.07 -8 0 6 199.65 5.40 -8 0 5 79.62 2.91 -8 0 5 83.79 2.65 -8 0 5 88.09 3.02 -8 0 4 12.80 1.04 -8 0 4 13.76 1.15 -8 0 4 14.01 1.09 -8 0 3 219.40 6.01 -8 0 3 238.12 6.42 -8 0 2 77.41 2.84 -8 0 2 75.94 3.11 -8 0 2 80.04 3.21 -8 0 1 13.08 1.03 -8 0 1 11.03 1.17 -8 0 1 14.47 1.31 -8 0 1 13.40 1.22 -8 0 0 1.13 0.40 -8 0 0 1.07 0.55 -8 0 0 1.43 0.59 -8 0 0 1.27 0.55 -8 0 -1 0.04 0.49 -8 0 -1 0.36 0.47 -8 0 -1 0.38 0.45 -8 0 -2 46.93 2.55 -8 0 -2 50.13 2.57 -8 0 -2 50.28 2.39 -8 0 -3 22.28 1.69 -8 0 -3 23.61 1.71 -8 0 -3 24.83 1.61 -8 0 -4 20.88 1.59 -8 0 -4 19.82 1.53 -8 0 -4 21.61 1.44 8 0 4 17.01 1.10 -8 0 -5 80.46 3.31 -8 0 -5 93.33 3.46 -8 0 -5 89.14 3.12 8 0 5 79.85 2.64 -8 0 -6 82.69 2.84 8 0 6 74.38 2.47 -8 0 -7 23.47 1.41 -8 -1 11 0.65 0.26 -8 -1 10 2.76 0.41 -8 -1 10 3.41 0.47 -8 -1 9 42.55 1.65 -8 -1 9 45.97 1.77 -8 -1 8 3.98 0.48 -8 -1 7 101.01 2.92 -8 -1 1 44.09 2.12 -8 -1 1 39.79 1.97 -8 -1 0 12.41 1.14 -8 -1 0 12.20 1.09 -8 -1 -1 0.26 0.40 -8 -1 -1 0.18 0.40 -8 -1 -2 6.55 0.87 -8 -1 -2 5.96 0.79 -8 -1 -2 5.00 0.61 -8 -1 -3 42.24 2.12 -8 -1 -3 41.09 2.02 -8 -1 -4 96.89 3.44 -8 -1 -4 101.00 3.39 -8 -1 -5 0.42 0.38 -8 -1 -5 0.64 0.37 -9 8 4 40.03 1.63 9 -8 -4 42.22 1.61 9 -8 -3 27.77 1.30 -9 8 2 0.19 0.28 9 -8 -2 0.25 0.27 9 -8 -1 44.17 1.73 -9 8 1 47.22 1.81 9 -8 -1 41.28 1.69 9 -8 0 155.72 4.09 -9 8 0 144.13 4.02 9 -8 1 3.80 0.53 -9 8 -1 4.61 0.53 9 -8 2 292.92 6.95 9 -7 -7 136.10 3.71 9 -7 -7 141.59 3.71 -9 7 6 0.51 0.41 9 -7 -6 0.77 0.31 9 -7 -6 0.47 0.31 -9 7 5 70.03 2.55 -9 7 5 65.58 2.40 -9 7 4 51.99 2.18 9 -7 -4 52.67 1.89 -9 7 4 54.93 2.16 -9 7 4 53.87 2.11 -9 7 3 30.13 1.61 9 -7 -3 26.54 1.34 -9 7 3 28.66 1.50 -9 7 3 27.65 1.47 -9 7 2 53.40 2.22 9 -7 -2 50.23 2.02 -9 7 2 50.48 2.09 -9 7 2 50.31 2.12 -9 7 1 113.05 3.65 9 -7 -1 114.25 3.52 9 -7 -1 110.05 3.78 -9 7 1 116.50 3.55 -9 7 1 120.07 3.68 -9 7 0 52.17 2.22 9 -7 0 54.16 2.17 9 -7 0 51.47 2.32 -9 7 0 54.71 2.11 -9 7 0 52.44 2.19 -9 7 -1 139.97 4.14 9 -7 1 141.77 4.10 9 -7 1 128.84 3.60 -9 7 -1 142.02 3.92 -9 7 -1 142.42 4.14 -9 7 -2 115.69 3.58 9 -7 2 118.99 3.59 9 -7 2 111.35 3.23 -9 7 -2 115.24 3.31 -9 7 -2 119.14 3.64 -9 7 -3 43.48 1.87 9 -7 3 43.23 1.86 9 -7 3 41.82 1.66 -9 7 -3 43.65 1.88 -9 7 -4 543.11 11.85 9 -7 4 544.28 11.65 9 -7 5 1.34 0.41 9 -7 5 1.09 0.34 -9 7 -5 1.20 0.38 9 -6 -9 0.98 0.32 9 -6 -9 1.41 0.33 9 -6 -8 239.55 6.07 9 -6 -8 253.98 6.04 9 -6 -8 253.95 5.93 -9 6 7 46.45 2.07 9 -6 -7 46.45 1.93 -9 6 7 41.66 1.91 9 -6 -7 46.95 1.90 -9 6 6 285.93 7.23 9 -6 -6 275.38 7.08 -9 6 6 255.40 6.87 -9 6 6 292.97 7.11 9 -6 -6 269.79 6.91 -9 6 5 141.30 4.41 9 -6 -5 133.62 4.34 -9 6 5 138.08 4.16 -9 6 5 141.71 4.28 -9 6 4 34.34 1.90 9 -6 -4 34.34 1.55 9 -6 -4 36.98 1.99 -9 6 4 35.26 1.76 -9 6 4 36.33 1.87 -9 6 3 59.02 2.59 9 -6 -3 54.34 2.17 9 -6 -3 57.03 2.63 -9 6 3 60.26 2.37 -9 6 3 55.92 2.44 -9 6 2 129.82 4.27 9 -6 -2 124.95 3.87 9 -6 -2 129.57 4.38 -9 6 2 125.50 3.91 -9 6 2 133.38 4.19 -9 6 1 12.24 1.14 9 -6 -1 10.97 1.01 -9 6 1 13.03 1.27 -9 6 1 12.38 0.98 -9 6 1 10.90 1.05 -9 6 0 131.71 4.26 9 -6 0 125.59 3.99 -9 6 0 128.65 4.43 -9 6 0 128.53 3.81 -9 6 0 129.23 4.16 -9 6 -1 189.90 5.39 9 -6 1 183.47 5.18 -9 6 -1 183.66 5.54 9 -6 1 176.48 4.71 -9 6 -1 175.22 4.76 -9 6 -1 182.99 5.28 -9 6 -2 49.04 2.25 9 -6 2 49.61 2.17 -9 6 -2 52.28 2.41 9 -6 2 44.71 1.87 -9 6 -2 45.41 1.75 -9 6 -2 49.27 2.21 -9 6 -3 206.86 5.58 9 -6 3 208.24 5.47 -9 6 -3 204.84 5.69 9 -6 3 199.71 5.15 -9 6 -3 206.88 5.54 -9 6 -4 62.67 2.44 9 -6 4 61.85 2.36 9 -6 4 52.64 1.92 -9 6 -4 59.81 2.45 9 -6 4 60.51 2.19 -9 6 -4 60.24 2.38 -9 6 -5 251.04 6.38 -9 6 -5 250.15 6.35 9 -6 5 255.70 6.15 -9 6 -5 258.85 6.39 -9 6 -6 14.85 1.01 9 -6 6 16.28 1.01 9 -6 6 16.32 0.97 -9 6 -6 14.51 0.99 9 -5 -10 6.34 0.66 -9 5 10 7.85 0.76 9 -5 -9 247.61 6.42 -9 5 9 256.65 6.56 -9 5 8 50.10 2.23 9 -5 -8 46.26 1.95 -9 5 8 46.83 2.11 9 -5 -8 47.34 1.87 -9 5 7 50.53 2.32 -9 5 7 47.39 2.08 -9 5 7 49.45 2.21 9 -5 -7 44.00 1.97 -9 5 6 306.25 7.93 9 -5 -6 290.60 7.69 -9 5 6 281.07 7.45 -9 5 6 318.71 7.82 -9 5 5 39.00 2.14 9 -5 -5 40.99 2.15 -9 5 5 39.66 1.92 -9 5 5 43.09 2.12 -9 5 4 19.08 1.49 9 -5 -4 18.43 1.13 9 -5 -4 19.25 1.53 -9 5 4 20.48 1.32 -9 5 4 19.00 1.41 -9 5 3 40.87 2.21 9 -5 -3 41.39 1.87 -9 5 3 43.73 2.43 9 -5 -3 43.03 2.31 -9 5 3 41.31 1.92 -9 5 3 41.94 2.15 -9 5 2 43.65 2.27 9 -5 -2 42.64 1.98 -9 5 2 40.58 2.35 -9 5 2 40.79 1.87 -9 5 2 45.17 2.23 -9 5 1 131.13 4.39 9 -5 -1 124.97 4.00 -9 5 1 130.89 4.58 -9 5 1 121.33 3.75 -9 5 1 132.02 4.31 -9 5 0 317.57 8.09 -9 5 0 308.20 8.29 9 -5 0 287.77 7.11 -9 5 0 285.20 7.16 -9 5 0 315.80 7.98 -9 5 -1 1.65 0.60 -9 5 -1 2.48 0.71 9 -5 1 1.22 0.43 -9 5 -2 41.14 2.11 -9 5 -2 39.49 2.18 9 -5 2 38.14 1.75 -9 5 -3 18.92 1.37 9 -5 3 14.57 0.95 -9 5 -3 16.35 1.34 9 -5 3 17.56 1.15 -9 5 -4 3.75 0.67 9 -5 4 2.88 0.49 -9 5 -4 3.57 0.69 9 -5 4 3.96 0.60 -9 5 -5 157.02 4.52 -9 5 -5 155.24 4.56 9 -5 5 154.84 4.25 -9 5 -5 158.18 4.43 -9 5 -6 7.94 0.80 9 -5 6 7.62 0.65 -9 5 -6 8.93 0.84 9 -5 6 9.18 0.77 -9 5 -6 8.97 0.79 -9 5 -7 18.56 1.10 9 -5 7 20.62 1.07 9 -4 -10 233.20 5.96 -9 4 10 260.85 6.32 9 -4 -9 117.77 3.40 -9 4 9 124.76 3.78 -9 4 8 19.04 1.35 9 -4 -8 19.52 1.11 9 -4 -6 8.04 0.93 9 -4 -5 353.17 8.80 -9 4 5 328.81 8.29 -9 4 4 62.97 2.94 9 -4 -4 64.80 2.84 -9 4 4 59.19 2.37 9 -4 -3 9.96 0.89 -9 4 3 10.46 1.23 -9 4 3 7.59 0.77 -9 4 2 0.36 0.32 -9 4 2 0.47 0.49 -9 4 1 208.16 6.01 -9 4 0 25.87 1.92 -9 4 0 29.18 1.96 9 -4 0 29.52 1.45 -9 4 0 30.48 1.79 -9 4 -1 181.95 5.66 9 -4 1 175.23 4.83 -9 4 -1 186.59 5.34 -9 4 -2 12.58 1.35 9 -4 2 14.32 0.94 -9 4 -2 12.71 1.27 9 -4 2 13.66 1.05 -9 4 -2 14.04 1.17 -9 4 -3 52.30 2.47 9 -4 3 52.22 2.11 -9 4 -3 50.71 2.22 9 -4 4 17.10 1.07 -9 4 -4 21.18 1.48 9 -4 4 20.93 1.28 -9 4 -4 19.89 1.29 -9 4 -5 73.98 3.06 9 -4 5 64.93 2.33 -9 4 -5 73.36 2.82 9 -4 5 71.38 2.53 -9 4 -5 72.57 2.54 -9 4 -6 0.49 0.47 9 -4 6 0.23 0.29 -9 4 -6 0.42 0.38 9 -4 6 0.29 0.35 -9 4 -6 0.42 0.30 -9 3 10 67.72 2.49 9 -3 -9 108.52 3.37 -9 3 9 125.53 3.75 -9 3 8 91.67 3.15 -9 3 8 93.01 3.13 -9 3 7 8.19 0.97 -9 3 7 7.75 0.92 -9 3 6 60.73 2.66 -9 3 6 62.55 2.64 -9 3 5 2.20 0.65 9 -3 -5 2.41 0.68 -9 3 5 2.89 0.65 -9 3 4 2.92 0.73 -9 3 4 3.35 0.77 -9 3 4 3.37 0.70 -9 3 3 13.85 1.26 -9 3 3 12.26 1.26 -9 3 3 14.24 1.22 -9 3 2 93.34 3.53 -9 3 2 92.60 3.69 -9 3 2 96.29 3.45 -9 3 1 5.22 0.82 -9 3 1 4.40 0.87 -9 3 1 3.97 0.83 -9 3 1 4.90 0.76 -9 3 0 140.80 4.54 -9 3 0 135.16 4.83 -9 3 0 142.30 4.77 9 -3 0 133.90 3.91 -9 3 0 147.88 4.44 -9 3 -1 216.95 6.18 -9 3 -1 209.54 6.59 -9 3 -1 217.21 6.42 -9 3 -1 233.11 6.08 -9 3 -2 16.12 1.24 -9 3 -2 14.69 1.42 9 -3 2 11.55 0.88 -9 3 -2 15.51 1.13 -9 3 -3 147.58 4.30 -9 3 -3 135.28 4.70 -9 3 -3 141.07 4.01 9 -3 4 25.42 1.32 -9 3 -4 28.20 1.40 -9 3 -5 120.57 3.55 -9 3 -5 124.18 3.82 -9 3 -6 8.97 0.92 9 -3 6 8.30 0.68 -9 3 -6 10.70 0.90 9 -3 6 8.77 0.75 -9 2 9 254.44 6.39 -9 2 8 13.83 1.06 -9 2 7 25.32 1.48 -9 2 7 27.95 1.54 -9 2 6 7.00 0.84 -9 2 6 8.75 0.91 -9 2 5 14.40 1.17 -9 2 5 15.23 1.17 -9 2 4 1.45 0.54 -9 2 4 1.90 0.61 -9 2 4 1.53 0.51 -9 2 3 27.07 1.61 -9 2 3 26.73 1.69 -9 2 3 25.64 1.50 -9 2 2 17.57 1.28 -9 2 2 15.44 1.25 -9 2 2 17.36 1.38 -9 2 2 18.04 1.22 -9 2 1 1.54 0.50 -9 2 1 2.35 0.62 -9 2 1 1.73 0.58 -9 2 1 1.42 0.46 -9 2 0 30.47 1.63 -9 2 0 27.91 1.78 -9 2 0 28.04 1.75 -9 2 0 26.29 1.42 -9 2 -1 3.59 0.61 -9 2 -1 3.38 0.74 -9 2 -1 4.06 0.75 -9 2 -1 3.19 0.52 -9 2 -2 45.81 1.93 -9 2 -2 44.01 2.26 -9 2 -2 46.92 2.19 -9 2 -3 1.80 0.43 -9 2 -3 1.84 0.59 -9 2 -3 2.10 0.57 -9 2 -4 28.04 1.69 -9 2 -4 28.93 1.59 -9 2 -5 4.91 0.65 -9 1 3 36.30 1.69 -9 1 2 96.87 3.20 -9 1 1 31.53 1.62 -9 1 0 1.76 0.51 -9 1 0 1.12 0.43 -9 1 -1 121.02 3.93 -9 1 -1 127.60 3.81 -9 1 -2 0.93 0.44 -9 1 -2 0.41 0.36 -9 1 -3 64.41 2.52 0 0 0 0.00 0.00 TITL 2019ncs0140z in P-1 REM P-1 (#2 in standard setting) CELL 1.54178 8.167202 9.383742 17.261236 96.9387 95.6166 112.3730 ZERR 2.00 0.000093 0.000102 0.000174 0.0009 0.0009 0.0011 LATT 1 SFAC C H B N P S Cu UNIT 46.00 80.00 2.00 2.00 2.00 2.00 2.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 19064 _olex2_date_sample_data_collection 2019-02-25 _olex2_date_sample_submission 2019-02-20 _olex2_diffrn_ambient_temperature_device 'Oxford Cryosystems' _olex2_exptl_crystal_mounting_method 'The crystal was mounted on a MITIGEN holder in perfluoroether oil' _olex2_submission_original_sample_id JG11 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.133 _oxdiff_exptl_absorpt_empirical_full_min 0.705 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.59890(3) 0.30934(2) 0.31737(2) 0.01664(7) Uani 1 1 d D . . . . S1A S 0.90081(16) 0.41068(18) 0.33845(6) 0.0211(2) Uani 0.795(2) 1 d D . P A 1 S1B S 0.5736(17) 0.1942(16) 0.4281(7) 0.0216(15) Uani 0.205(2) 1 d D . P A 2 P1 P 0.41270(4) 0.32604(4) 0.22229(2) 0.01360(8) Uani 1 1 d . . . . . C1A C 0.93680(19) 0.32609(16) 0.41820(8) 0.0207(3) Uani 0.795(2) 1 d D . P A 1 C1B C 0.80187(17) 0.23487(14) 0.45273(7) 0.0194(3) Uani 0.205(2) 1 d D . P A 2 N1A N 0.80187(17) 0.23487(14) 0.45273(7) 0.0194(3) Uani 0.795(2) 1 d D . P A 1 N1B N 0.93680(19) 0.32609(16) 0.41820(8) 0.0207(3) Uani 0.205(2) 1 d D . P A 2 C2 C 1.1142(2) 0.3502(2) 0.44712(9) 0.0295(3) Uani 1 1 d . . . . . H2A H 1.209874 0.417206 0.424533 0.035 Uiso 0.795(2) 1 calc R . P A 1 H2B H 1.209874 0.417206 0.424533 0.035 Uiso 0.205(2) 1 calc R . P A 2 C3 C 1.1516(2) 0.2793(2) 0.50690(10) 0.0346(4) Uani 1 1 d . . . . . H3 H 1.271771 0.294748 0.525068 0.042 Uiso 1 1 calc R . . . . C4 C 1.0109(3) 0.1837(2) 0.54100(9) 0.0339(4) Uani 1 1 d . . . . . H4 H 1.033650 0.132749 0.582565 0.041 Uiso 1 1 calc R . . . . C5 C 0.8401(2) 0.16456(18) 0.51374(9) 0.0270(3) Uani 1 1 d . . . . . H5A H 0.744538 0.100805 0.537517 0.032 Uiso 0.795(2) 1 calc R . P A 1 H5B H 0.744538 0.100805 0.537517 0.032 Uiso 0.205(2) 1 calc R . P A 2 C6 C 0.50599(17) 0.35509(15) 0.12924(8) 0.0151(3) Uani 1 1 d . . . . . H6 H 0.422879 0.380673 0.092362 0.018 Uiso 1 1 calc R . . . . C7 C 0.69006(18) 0.49341(16) 0.14519(8) 0.0184(3) Uani 1 1 d . . . . . H7A H 0.677235 0.588918 0.169554 0.022 Uiso 1 1 calc R . . . . H7B H 0.773194 0.471455 0.182928 0.022 Uiso 1 1 calc R . . . . C8 C 0.76871(19) 0.52173(16) 0.06880(8) 0.0200(3) Uani 1 1 d . . . . . H8A H 0.690745 0.552281 0.032718 0.024 Uiso 1 1 calc R . . . . H8B H 0.888706 0.608706 0.081050 0.024 Uiso 1 1 calc R . . . . C9 C 0.78451(19) 0.37485(17) 0.02815(8) 0.0213(3) Uani 1 1 d . . . . . H9A H 0.828790 0.393757 -0.022590 0.026 Uiso 1 1 calc R . . . . H9B H 0.872486 0.350798 0.061914 0.026 Uiso 1 1 calc R . . . . C10 C 0.6038(2) 0.23568(17) 0.01275(8) 0.0226(3) Uani 1 1 d . . . . . H10A H 0.619222 0.140817 -0.010675 0.027 Uiso 1 1 calc R . . . . H10B H 0.519887 0.255092 -0.025778 0.027 Uiso 1 1 calc R . . . . C11 C 0.52344(19) 0.20742(16) 0.08897(8) 0.0196(3) Uani 1 1 d . . . . . H11A H 0.601106 0.177467 0.125540 0.023 Uiso 1 1 calc R . . . . H11B H 0.403745 0.120060 0.076441 0.023 Uiso 1 1 calc R . . . . C12 C 0.20119(18) 0.14946(15) 0.19329(8) 0.0158(3) Uani 1 1 d . . . . . H12 H 0.235283 0.061021 0.174509 0.019 Uiso 1 1 calc R . . . . C13 C 0.10641(18) 0.10717(16) 0.26510(8) 0.0181(3) Uani 1 1 d . . . . . H13A H 0.190746 0.097601 0.307399 0.022 Uiso 1 1 calc R . . . . H13B H 0.070220 0.192044 0.285753 0.022 Uiso 1 1 calc R . . . . C14 C -0.05964(19) -0.04700(17) 0.24300(9) 0.0225(3) Uani 1 1 d . . . . . H14A H -0.021908 -0.133880 0.228357 0.027 Uiso 1 1 calc R . . . . H14B H -0.122153 -0.067473 0.289348 0.027 Uiso 1 1 calc R . . . . C15 C -0.18843(19) -0.04181(17) 0.17406(9) 0.0252(3) Uani 1 1 d . . . . . H15A H -0.289825 -0.145191 0.158860 0.030 Uiso 1 1 calc R . . . . H15B H -0.237526 0.036492 0.190844 0.030 Uiso 1 1 calc R . . . . C16 C -0.0945(2) 0.00045(17) 0.10294(9) 0.0259(3) Uani 1 1 d . . . . . H16A H -0.179294 0.008443 0.060279 0.031 Uiso 1 1 calc R . . . . H16B H -0.055889 -0.083141 0.082776 0.031 Uiso 1 1 calc R . . . . C17 C 0.06880(19) 0.15611(16) 0.12562(8) 0.0207(3) Uani 1 1 d . . . . . H17A H 0.029021 0.240910 0.142138 0.025 Uiso 1 1 calc R . . . . H17B H 0.129650 0.180179 0.079069 0.025 Uiso 1 1 calc R . . . . C18 C 0.34333(18) 0.49096(15) 0.24713(8) 0.0153(3) Uani 1 1 d . . . . . H18 H 0.230084 0.446779 0.269875 0.018 Uiso 1 1 calc R . . . . C19 C 0.48062(19) 0.61731(16) 0.31310(8) 0.0197(3) Uani 1 1 d . . . . . H19A H 0.503919 0.567984 0.358144 0.024 Uiso 1 1 calc R . . . . H19B H 0.595064 0.667136 0.293142 0.024 Uiso 1 1 calc R . . . . C20 C 0.4118(2) 0.74201(17) 0.34122(9) 0.0237(3) Uani 1 1 d . . . . . H20A H 0.304652 0.694045 0.366458 0.028 Uiso 1 1 calc R . . . . H20B H 0.505181 0.824723 0.381358 0.028 Uiso 1 1 calc R . . . . C21 C 0.3633(2) 0.81534(16) 0.27292(9) 0.0237(3) Uani 1 1 d . . . . . H21A H 0.473315 0.874858 0.251997 0.028 Uiso 1 1 calc R . . . . H21B H 0.310742 0.889428 0.292468 0.028 Uiso 1 1 calc R . . . . C22 C 0.2294(2) 0.69039(16) 0.20663(9) 0.0216(3) Uani 1 1 d . . . . . H22A H 0.206719 0.740501 0.161816 0.026 Uiso 1 1 calc R . . . . H22B H 0.114372 0.639300 0.225885 0.026 Uiso 1 1 calc R . . . . C23 C 0.29962(18) 0.56663(15) 0.17810(8) 0.0176(3) Uani 1 1 d . . . . . H23A H 0.408926 0.615857 0.154445 0.021 Uiso 1 1 calc R . . . . H23B H 0.208111 0.485060 0.136846 0.021 Uiso 1 1 calc R . . . . B1A B 0.598(2) 0.202(2) 0.4207(10) 0.027(2) Uani 0.795(2) 1 d D . P A 1 B1B B 0.878(4) 0.382(3) 0.3396(15) 0.036(9) Uiso 0.205(2) 1 d D . P A 2 H1AA H 0.562(4) 0.138(3) 0.3559(14) 0.054 Uiso 0.795(2) 1 d DR . P A 1 H1AB H 0.586(4) 0.322(3) 0.4221(15) 0.054 Uiso 0.795(2) 1 d DR . P A 1 H1BA H 0.798(9) 0.458(8) 0.354(6) 0.054 Uiso 0.205(2) 1 d DR . P A 2 H1BB H 0.794(9) 0.275(7) 0.292(5) 0.054 Uiso 0.205(2) 1 d DR . P A 2 H1AC H 0.516(4) 0.130(3) 0.4631(15) 0.054 Uiso 0.795(2) 1 d DR . P A 1 H1BC H 1.016(7) 0.455(8) 0.323(5) 0.054 Uiso 0.205(2) 1 d DR . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.01697(12) 0.01839(11) 0.01553(11) 0.00267(8) -0.00022(8) 0.00881(9) S1A 0.0144(4) 0.0283(5) 0.0219(4) 0.0089(3) 0.0039(2) 0.0084(4) S1B 0.024(2) 0.025(2) 0.016(2) 0.0066(16) 0.0011(19) 0.0092(18) P1 0.01354(17) 0.01336(16) 0.01377(16) 0.00229(12) 0.00099(12) 0.00549(13) C1A 0.0241(7) 0.0237(7) 0.0159(6) -0.0015(5) 0.0001(5) 0.0133(6) C1B 0.0251(7) 0.0197(6) 0.0152(6) 0.0001(5) -0.0005(5) 0.0125(5) N1A 0.0251(7) 0.0197(6) 0.0152(6) 0.0001(5) -0.0005(5) 0.0125(5) N1B 0.0241(7) 0.0237(7) 0.0159(6) -0.0015(5) 0.0001(5) 0.0133(6) C2 0.0258(8) 0.0392(9) 0.0233(7) -0.0019(7) 0.0001(6) 0.0158(7) C3 0.0326(9) 0.0500(10) 0.0242(8) -0.0063(7) -0.0090(7) 0.0266(8) C4 0.0487(10) 0.0420(9) 0.0192(7) 0.0017(7) -0.0057(7) 0.0305(9) C5 0.0387(9) 0.0279(8) 0.0188(7) 0.0039(6) 0.0019(6) 0.0187(7) C6 0.0147(6) 0.0155(6) 0.0151(6) 0.0026(5) 0.0019(5) 0.0062(5) C7 0.0170(7) 0.0173(6) 0.0185(7) 0.0022(5) 0.0026(5) 0.0045(5) C8 0.0178(7) 0.0211(7) 0.0209(7) 0.0068(5) 0.0040(5) 0.0062(6) C9 0.0202(7) 0.0274(7) 0.0201(7) 0.0072(6) 0.0066(5) 0.0121(6) C10 0.0259(8) 0.0216(7) 0.0204(7) 0.0002(6) 0.0070(6) 0.0099(6) C11 0.0224(7) 0.0160(6) 0.0214(7) 0.0029(5) 0.0066(5) 0.0082(6) C12 0.0156(6) 0.0137(6) 0.0172(6) 0.0030(5) 0.0016(5) 0.0049(5) C13 0.0176(7) 0.0186(7) 0.0183(7) 0.0060(5) 0.0030(5) 0.0068(6) C14 0.0189(7) 0.0207(7) 0.0271(7) 0.0103(6) 0.0033(6) 0.0052(6) C15 0.0169(7) 0.0205(7) 0.0331(8) 0.0093(6) -0.0008(6) 0.0016(6) C16 0.0220(8) 0.0219(7) 0.0244(7) 0.0046(6) -0.0054(6) 0.0005(6) C17 0.0193(7) 0.0188(7) 0.0190(7) 0.0054(5) -0.0022(5) 0.0027(6) C18 0.0150(6) 0.0151(6) 0.0157(6) 0.0019(5) 0.0016(5) 0.0063(5) C19 0.0207(7) 0.0184(7) 0.0181(7) -0.0014(5) -0.0014(5) 0.0080(6) C20 0.0266(8) 0.0209(7) 0.0223(7) -0.0036(6) 0.0007(6) 0.0108(6) C21 0.0258(8) 0.0166(7) 0.0288(8) -0.0005(6) 0.0021(6) 0.0106(6) C22 0.0224(7) 0.0189(7) 0.0252(7) 0.0033(6) 0.0008(6) 0.0111(6) C23 0.0185(7) 0.0153(6) 0.0181(6) 0.0023(5) 0.0001(5) 0.0067(5) B1A 0.036(5) 0.024(2) 0.022(3) 0.0106(18) 0.005(2) 0.010(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 S1A Cu1 H1AA 98.2(9) . . S1A Cu1 H1AB 93.0(9) . . S1B Cu1 H1BA 96(3) . . S1B Cu1 H1BB 97(3) . . P1 Cu1 S1A 129.93(3) . . P1 Cu1 S1B 135.9(3) . . P1 Cu1 H1AA 123.0(9) . . P1 Cu1 H1AB 128.5(8) . . P1 Cu1 H1BA 122(3) . . P1 Cu1 H1BB 118(3) . . H1AA Cu1 H1AB 63.9(11) . . H1BA Cu1 H1BB 65.2(17) . . C1A S1A Cu1 99.53(8) . . C1B S1B Cu1 96.2(5) . . C6 P1 Cu1 113.30(4) . . C6 P1 C12 104.25(6) . . C6 P1 C18 105.57(6) . . C12 P1 Cu1 114.21(4) . . C12 P1 C18 105.42(6) . . C18 P1 Cu1 113.20(4) . . N1A C1A S1A 122.92(11) . . N1A C1A C2 118.87(13) . . C2 C1A S1A 118.19(12) . . N1B C1B S1B 126.4(4) . . N1B C1B C5 119.66(13) . . C5 C1B S1B 114.0(4) . . C1A N1A C5 119.66(13) . . C1A N1A B1A 120.6(6) . . C5 N1A B1A 119.7(6) . . C1B N1B C2 118.87(13) . . C1B N1B B1B 116.3(10) . . C2 N1B B1B 124.4(10) . . C1A C2 H2A 119.3 . . N1B C2 H2B 119.3 . . C3 C2 C1A 121.35(16) . . C3 C2 N1B 121.35(16) . . C3 C2 H2A 119.3 . . C3 C2 H2B 119.3 . . C2 C3 H3 120.5 . . C2 C3 C4 119.04(15) . . C4 C3 H3 120.5 . . C3 C4 H4 120.5 . . C5 C4 C3 118.98(15) . . C5 C4 H4 120.5 . . C1B C5 H5B 119.0 . . N1A C5 H5A 119.0 . . C4 C5 C1B 122.07(16) . . C4 C5 N1A 122.07(16) . . C4 C5 H5A 119.0 . . C4 C5 H5B 119.0 . . P1 C6 H6 108.3 . . C7 C6 P1 110.21(9) . . C7 C6 H6 108.3 . . C11 C6 P1 111.96(9) . . C11 C6 H6 108.3 . . C11 C6 C7 109.77(11) . . C6 C7 H7A 109.4 . . C6 C7 H7B 109.4 . . H7A C7 H7B 108.0 . . C8 C7 C6 111.23(11) . . C8 C7 H7A 109.4 . . C8 C7 H7B 109.4 . . C7 C8 H8A 109.5 . . C7 C8 H8B 109.5 . . H8A C8 H8B 108.1 . . C9 C8 C7 110.81(11) . . C9 C8 H8A 109.5 . . C9 C8 H8B 109.5 . . C8 C9 H9A 109.4 . . C8 C9 H9B 109.4 . . H9A C9 H9B 108.0 . . C10 C9 C8 110.97(11) . . C10 C9 H9A 109.4 . . C10 C9 H9B 109.4 . . C9 C10 H10A 109.3 . . C9 C10 H10B 109.3 . . C9 C10 C11 111.62(12) . . H10A C10 H10B 108.0 . . C11 C10 H10A 109.3 . . C11 C10 H10B 109.3 . . C6 C11 H11A 109.5 . . C6 C11 H11B 109.5 . . C10 C11 C6 110.81(11) . . C10 C11 H11A 109.5 . . C10 C11 H11B 109.5 . . H11A C11 H11B 108.1 . . P1 C12 H12 106.6 . . C13 C12 P1 111.00(9) . . C13 C12 H12 106.6 . . C17 C12 P1 115.56(9) . . C17 C12 H12 106.6 . . C17 C12 C13 109.88(11) . . C12 C13 H13A 109.4 . . C12 C13 H13B 109.4 . . H13A C13 H13B 108.0 . . C14 C13 C12 111.24(11) . . C14 C13 H13A 109.4 . . C14 C13 H13B 109.4 . . C13 C14 H14A 109.4 . . C13 C14 H14B 109.4 . . H14A C14 H14B 108.0 . . C15 C14 C13 111.36(11) . . C15 C14 H14A 109.4 . . C15 C14 H14B 109.4 . . C14 C15 H15A 109.4 . . C14 C15 H15B 109.4 . . H15A C15 H15B 108.0 . . C16 C15 C14 111.29(12) . . C16 C15 H15A 109.4 . . C16 C15 H15B 109.4 . . C15 C16 H16A 109.5 . . C15 C16 H16B 109.5 . . C15 C16 C17 110.65(12) . . H16A C16 H16B 108.1 . . C17 C16 H16A 109.5 . . C17 C16 H16B 109.5 . . C12 C17 H17A 109.4 . . C12 C17 H17B 109.4 . . C16 C17 C12 110.98(11) . . C16 C17 H17A 109.4 . . C16 C17 H17B 109.4 . . H17A C17 H17B 108.0 . . P1 C18 H18 106.1 . . C19 C18 P1 110.98(9) . . C19 C18 H18 106.1 . . C23 C18 P1 116.80(9) . . C23 C18 H18 106.1 . . C23 C18 C19 110.09(11) . . C18 C19 H19A 109.4 . . C18 C19 H19B 109.4 . . H19A C19 H19B 108.0 . . C20 C19 C18 110.98(11) . . C20 C19 H19A 109.4 . . C20 C19 H19B 109.4 . . C19 C20 H20A 109.3 . . C19 C20 H20B 109.3 . . H20A C20 H20B 108.0 . . C21 C20 C19 111.59(12) . . C21 C20 H20A 109.3 . . C21 C20 H20B 109.3 . . C20 C21 H21A 109.4 . . C20 C21 H21B 109.4 . . C20 C21 C22 111.16(12) . . H21A C21 H21B 108.0 . . C22 C21 H21A 109.4 . . C22 C21 H21B 109.4 . . C21 C22 H22A 109.4 . . C21 C22 H22B 109.4 . . C21 C22 C23 111.37(12) . . H22A C22 H22B 108.0 . . C23 C22 H22A 109.4 . . C23 C22 H22B 109.4 . . C18 C23 H23A 109.5 . . C18 C23 H23B 109.5 . . C22 C23 C18 110.65(11) . . C22 C23 H23A 109.5 . . C22 C23 H23B 109.5 . . H23A C23 H23B 108.1 . . N1A B1A H1AA 108.6(19) . . N1A B1A H1AB 108.0(19) . . N1A B1A H1AC 105.0(19) . . H1AA B1A H1AB 108.5(19) . . H1AA B1A H1AC 114(2) . . H1AB B1A H1AC 112(2) . . N1B B1B H1BA 110(5) . . N1B B1B H1BB 110(5) . . N1B B1B H1BC 101(5) . . H1BA B1B H1BB 110(3) . . H1BA B1B H1BC 112(3) . . H1BB B1B H1BC 113(3) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Cu1 S1A 2.2523(12) . Cu1 S1B 2.296(12) . Cu1 P1 2.1876(4) . Cu1 H1AA 1.75(2) . Cu1 H1AB 1.81(2) . Cu1 H1BA 1.68(8) . Cu1 H1BB 1.82(8) . S1A C1A 1.7244(17) . S1B C1B 1.751(13) . P1 C6 1.8499(13) . P1 C12 1.8524(13) . P1 C18 1.8587(13) . C1A N1A 1.3550(19) . C1A C2 1.408(2) . C1B N1B 1.3550(19) . C1B C5 1.3794(19) . N1A C5 1.3794(19) . N1A B1A 1.602(16) . N1B C2 1.408(2) . N1B B1B 1.61(2) . C2 H2A 0.9500 . C2 H2B 0.9500 . C2 C3 1.363(2) . C3 H3 0.9500 . C3 C4 1.396(3) . C4 H4 0.9500 . C4 C5 1.363(2) . C5 H5A 0.9500 . C5 H5B 0.9500 . C6 H6 1.0000 . C6 C7 1.5387(18) . C6 C11 1.5365(18) . C7 H7A 0.9900 . C7 H7B 0.9900 . C7 C8 1.5305(18) . C8 H8A 0.9900 . C8 H8B 0.9900 . C8 C9 1.526(2) . C9 H9A 0.9900 . C9 H9B 0.9900 . C9 C10 1.525(2) . C10 H10A 0.9900 . C10 H10B 0.9900 . C10 C11 1.5339(19) . C11 H11A 0.9900 . C11 H11B 0.9900 . C12 H12 1.0000 . C12 C13 1.5381(18) . C12 C17 1.5360(18) . C13 H13A 0.9900 . C13 H13B 0.9900 . C13 C14 1.5328(19) . C14 H14A 0.9900 . C14 H14B 0.9900 . C14 C15 1.527(2) . C15 H15A 0.9900 . C15 H15B 0.9900 . C15 C16 1.524(2) . C16 H16A 0.9900 . C16 H16B 0.9900 . C16 C17 1.5306(19) . C17 H17A 0.9900 . C17 H17B 0.9900 . C18 H18 1.0000 . C18 C19 1.5399(18) . C18 C23 1.5380(18) . C19 H19A 0.9900 . C19 H19B 0.9900 . C19 C20 1.5291(19) . C20 H20A 0.9900 . C20 H20B 0.9900 . C20 C21 1.527(2) . C21 H21A 0.9900 . C21 H21B 0.9900 . C21 C22 1.528(2) . C22 H22A 0.9900 . C22 H22B 0.9900 . C22 C23 1.5308(18) . C23 H23A 0.9900 . C23 H23B 0.9900 . B1A H1AA 1.16(2) . B1A H1AB 1.17(2) . B1A H1AC 1.14(2) . B1B H1BA 1.16(2) . B1B H1BB 1.15(2) . B1B H1BC 1.15(2) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 Cu1 S1A C1A N1A -3.34(14) . . . . Cu1 S1A C1A C2 175.02(11) . . . . Cu1 S1B C1B N1B 7.9(8) . . . . Cu1 S1B C1B C5 -172.3(2) . . . . Cu1 P1 C6 C7 -51.70(10) . . . . Cu1 P1 C6 C11 70.78(10) . . . . Cu1 P1 C12 C13 55.10(10) . . . . Cu1 P1 C12 C17 -178.94(8) . . . . Cu1 P1 C18 C19 21.99(10) . . . . Cu1 P1 C18 C23 149.28(9) . . . . S1A C1A N1A C5 176.67(12) . . . . S1A C1A N1A B1A -0.5(8) . . . . S1A C1A C2 C3 -176.03(13) . . . . S1B C1B N1B C2 178.1(6) . . . . S1B C1B N1B B1B -9.1(14) . . . . S1B C1B C5 C4 -179.7(5) . . . . P1 C6 C7 C8 -179.00(9) . . . . P1 C6 C11 C10 -179.10(9) . . . . P1 C12 C13 C14 -174.85(9) . . . . P1 C12 C17 C16 176.08(10) . . . . P1 C18 C19 C20 -172.41(10) . . . . P1 C18 C23 C22 175.11(9) . . . . C1A N1A C5 C4 0.0(2) . . . . C1A C2 C3 C4 -1.4(2) . . . . C1B N1B C2 C3 2.4(2) . . . . N1A C1A C2 C3 2.4(2) . . . . N1B C1B C5 C4 0.0(2) . . . . N1B C2 C3 C4 -1.4(2) . . . . C2 C1A N1A C5 -1.7(2) . . . . C2 C1A N1A B1A -178.9(8) . . . . C2 C3 C4 C5 -0.3(2) . . . . C3 C4 C5 C1B 1.0(2) . . . . C3 C4 C5 N1A 1.0(2) . . . . C5 C1B N1B C2 -1.7(2) . . . . C5 C1B N1B B1B 171.2(12) . . . . C6 P1 C12 C13 179.26(9) . . . . C6 P1 C12 C17 -54.77(11) . . . . C6 P1 C18 C19 -102.49(10) . . . . C6 P1 C18 C23 24.80(11) . . . . C6 C7 C8 C9 -57.15(15) . . . . C7 C6 C11 C10 -56.37(15) . . . . C7 C8 C9 C10 55.78(15) . . . . C8 C9 C10 C11 -55.62(15) . . . . C9 C10 C11 C6 56.22(15) . . . . C11 C6 C7 C8 57.24(14) . . . . C12 P1 C6 C7 -176.45(9) . . . . C12 P1 C6 C11 -53.97(10) . . . . C12 P1 C18 C19 147.52(9) . . . . C12 P1 C18 C23 -85.19(11) . . . . C12 C13 C14 C15 -55.28(16) . . . . C13 C12 C17 C16 -57.39(15) . . . . C13 C14 C15 C16 55.16(17) . . . . C14 C15 C16 C17 -56.20(17) . . . . C15 C16 C17 C12 57.69(16) . . . . C17 C12 C13 C14 56.08(14) . . . . C18 P1 C6 C7 72.72(10) . . . . C18 P1 C6 C11 -164.80(9) . . . . C18 P1 C12 C13 -69.80(10) . . . . C18 P1 C12 C17 56.17(11) . . . . C18 C19 C20 C21 -55.79(16) . . . . C19 C18 C23 C22 -57.17(15) . . . . C19 C20 C21 C22 54.79(17) . . . . C20 C21 C22 C23 -55.30(16) . . . . C21 C22 C23 C18 56.80(15) . . . . C23 C18 C19 C20 56.72(15) . . . . B1A N1A C5 C4 177.3(8) . . . . B1B N1B C2 C3 -169.9(13) . . . .