#------------------------------------------------------------------------------ #$Date: 2019-12-06 11:07:20 +0200 (Fri, 06 Dec 2019) $ #$Revision: 244923 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/64/1556426.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556426 loop_ _publ_author_name 'Rungthanaphatsophon, P.' 'Fajen, O.J.' 'Kelley, S.P.' 'Walensky, J.R.' _publ_section_title ; Thorium(IV) and Uranium(IV) Phosphaazaallenes ; _journal_name_full Inorganics _journal_page_first 105 _journal_paper_doi 10.3390/inorganics7090105 _journal_volume 7 _journal_year 2019 _chemical_absolute_configuration ad _chemical_formula_moiety 'C38 H58 P2 Si2 Th' _chemical_formula_sum 'C38 H58 P2 Si2 Th' _chemical_formula_weight 865.00 _space_group_crystal_system tetragonal _space_group_IT_number 96 _space_group_name_Hall 'P 4nw 2abw' _space_group_name_H-M_alt 'P 43 21 2' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _atom_sites_solution_secondary difmap _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.1642(12) _cell_length_b 12.1642(12) _cell_length_c 26.953(3) _cell_measurement_reflns_used 9987 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 28.7 _cell_measurement_theta_min 2.8 _cell_volume 3988.2(7) _computing_cell_refinement 'SAINT (Bruker, 1998)' _computing_data_collection 'SMART (Bruker, 1998)' _computing_data_reduction 'SAINT (Bruker, 1998)' _computing_molecular_graphics 'ORTEP-III (Burnett & Johnson, 1996)' _computing_publication_material 'CIFTAB (Sheldrick, 1997)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1997)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker SMART CCD area detector' _diffrn_measurement_method 'omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0433 _diffrn_reflns_av_unetI/netI 0.0270 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 36 _diffrn_reflns_limit_l_min -36 _diffrn_reflns_number 32720 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.738 _diffrn_reflns_theta_min 2.486 _diffrn_standards_decay_% 0.0 _exptl_absorpt_coefficient_mu 3.903 _exptl_absorpt_correction_T_max 0.51 _exptl_absorpt_correction_T_min 0.40 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; Data were corrected for decay and absorption using the program SADABS (Sheldrick, G. M. (2003). SADABS. Version 2.10. University of G\"ottingen, Germany). ; _exptl_crystal_colour Red _exptl_crystal_density_diffrn 1.441 _exptl_crystal_description Prism _exptl_crystal_F_000 1736 _exptl_crystal_size_max 0.250 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.200 _refine_diff_density_max 1.658 _refine_diff_density_min -1.569 _refine_diff_density_rms 0.082 _refine_ls_abs_structure_details ; Flack x determined using 1950 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.009(3) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.077 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 203 _refine_ls_number_reflns 5170 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.077 _refine_ls_R_factor_all 0.0229 _refine_ls_R_factor_gt 0.0203 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0178P)^2^+1.6384P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0416 _refine_ls_wR_factor_ref 0.0424 _reflns_Friedel_coverage 0.711 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.998 _reflns_number_gt 4903 _reflns_number_total 5170 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file Complex1_CIF.cif _cod_data_source_block PR5029 _cod_original_cell_volume 3988.1(9) _cod_database_code 1556426 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.442 _shelx_estimated_absorpt_t_max 0.509 _shelx_res_file ; C:\Xtals\Walensky\Ken\PR5029\PR5029.res created by SHELXL-2014/7 TITL PR5029_a.res in P4(3)2(1)2 CELL 0.71073 12.1642 12.1642 26.9528 90.000 90.000 90.000 ZERR 4.0000 0.0012 0.0012 0.0028 0.000 0.000 0.000 LATT -1 SYMM 0.5-Y, 0.5+X, 0.75+Z SYMM -X, -Y, 0.5+Z SYMM 0.5+Y, 0.5-X, 0.25+Z SYMM 0.5+X, 0.5-Y, 0.25-Z SYMM 0.5-X, 0.5+Y, 0.75-Z SYMM Y, X, -Z SYMM -Y, -X, 0.5-Z SFAC C H P SI TH UNIT 152 232 8 8 4 BOND $H CONF OMIT 0 1 1 OMIT 0 1 2 ACTA FMAP 2 1 53 PLAN 20 0 0 LIST 6 1 SIZE 0.20 0.20 0.25 TEMP -173 L.S. 10 WGHT 0.017800 1.638400 FVAR 0.08851 TH1 5 0.523156 0.476844 0.250000 10.50000 0.01154 0.01154 = 0.01742 0.00006 0.00006 0.00091 P1 3 0.291936 0.472173 0.259285 11.00000 0.01217 0.02508 = 0.02634 -0.00885 0.00153 -0.00075 SI1 4 0.179471 0.572591 0.306125 11.00000 0.01582 0.02852 = 0.02861 -0.00645 0.00285 0.00352 C1 1 0.531964 0.442864 0.352501 11.00000 0.02016 0.02151 = 0.02007 0.00392 -0.00351 -0.00102 C2 1 0.592216 0.354702 0.331049 11.00000 0.02709 0.01961 = 0.02763 0.00794 -0.00278 0.00143 C3 1 0.691169 0.398219 0.311815 11.00000 0.02354 0.03242 = 0.02635 0.00942 -0.00516 0.00701 C4 1 0.691492 0.513174 0.320273 11.00000 0.01507 0.03070 = 0.02563 0.01050 -0.00693 -0.00369 C5 1 0.593389 0.540824 0.346305 11.00000 0.02050 0.02056 = 0.01785 0.00454 -0.00662 -0.00499 C6 1 0.430103 0.429981 0.383829 11.00000 0.02690 0.03315 = 0.02462 0.00433 0.00229 -0.00846 AFIX 137 H6A 2 0.449878 0.397188 0.415819 11.00000 -1.50000 H6B 2 0.377582 0.382146 0.366679 11.00000 -1.50000 H6C 2 0.396632 0.502233 0.389354 11.00000 -1.50000 AFIX 0 C7 1 0.556669 0.236468 0.333890 11.00000 0.04889 0.02169 = 0.04297 0.01002 0.00256 0.00449 AFIX 137 H7A 2 0.612561 0.189753 0.318358 11.00000 -1.50000 H7B 2 0.486575 0.227405 0.316438 11.00000 -1.50000 H7C 2 0.547704 0.215194 0.368725 11.00000 -1.50000 AFIX 0 C8 1 0.792860 0.335578 0.295984 11.00000 0.02654 0.04769 = 0.04750 0.01207 -0.00244 0.02187 AFIX 137 H8A 2 0.851404 0.346916 0.320433 11.00000 -1.50000 H8B 2 0.817337 0.362251 0.263502 11.00000 -1.50000 H8C 2 0.775654 0.257025 0.293771 11.00000 -1.50000 AFIX 0 C9 1 0.789241 0.586617 0.310763 11.00000 0.01762 0.04936 = 0.03921 0.01493 -0.01014 -0.00771 AFIX 137 H9A 2 0.849597 0.565742 0.332929 11.00000 -1.50000 H9B 2 0.768693 0.663287 0.316985 11.00000 -1.50000 H9C 2 0.812909 0.578511 0.276201 11.00000 -1.50000 AFIX 0 C10 1 0.567311 0.648681 0.370352 11.00000 0.03059 0.02439 = 0.02477 -0.00145 -0.00607 -0.00650 AFIX 137 H10A 2 0.494645 0.673700 0.359443 11.00000 -1.50000 H10B 2 0.622830 0.703142 0.360861 11.00000 -1.50000 H10C 2 0.567390 0.639794 0.406490 11.00000 -1.50000 AFIX 0 C11 1 0.260222 0.684462 0.336804 11.00000 0.03015 0.03132 = 0.04987 -0.01991 0.00051 0.00801 AFIX 137 H11A 2 0.314176 0.714040 0.313333 11.00000 -1.50000 H11B 2 0.298474 0.654674 0.365843 11.00000 -1.50000 H11C 2 0.210314 0.743269 0.347306 11.00000 -1.50000 AFIX 0 C12 1 0.108421 0.485001 0.353591 11.00000 0.02907 0.04257 = 0.03614 -0.00073 0.01255 0.00775 AFIX 137 H12A 2 0.162907 0.455015 0.376703 11.00000 -1.50000 H12B 2 0.070099 0.424499 0.336937 11.00000 -1.50000 H12C 2 0.055138 0.529729 0.371928 11.00000 -1.50000 AFIX 0 C13 1 0.072110 0.637716 0.265728 11.00000 0.02104 0.04749 = 0.03857 0.00082 0.00352 0.01082 AFIX 137 H13A 2 0.023411 0.683223 0.286153 11.00000 -1.50000 H13B 2 0.028986 0.580207 0.249308 11.00000 -1.50000 H13C 2 0.107841 0.683741 0.240619 11.00000 -1.50000 AFIX 0 C14 1 0.199988 0.356160 0.244659 11.00000 0.01618 0.02633 = 0.02177 -0.00624 0.00209 -0.00045 C15 1 0.204556 0.258968 0.271316 11.00000 0.03151 0.03236 = 0.02376 -0.00035 0.00202 -0.00445 AFIX 43 H15 2 0.255439 0.252338 0.297888 11.00000 -1.20000 AFIX 0 C16 1 0.136013 0.170649 0.259959 11.00000 0.04807 0.02837 = 0.03273 0.00241 0.00891 -0.01047 AFIX 43 H16 2 0.141249 0.104418 0.278487 11.00000 -1.20000 AFIX 0 C17 1 0.060753 0.179029 0.221991 11.00000 0.03548 0.03934 = 0.03730 -0.01623 0.00960 -0.01840 AFIX 43 H17 2 0.014069 0.118790 0.214290 11.00000 -1.20000 AFIX 0 C18 1 0.053466 0.275906 0.195048 11.00000 0.02252 0.04260 = 0.03014 -0.01526 -0.00105 -0.00681 AFIX 43 H18 2 0.001293 0.282125 0.168971 11.00000 -1.20000 AFIX 0 C19 1 0.122108 0.363875 0.206019 11.00000 0.01676 0.03346 = 0.02508 -0.00436 0.00164 -0.00025 AFIX 43 H19 2 0.116563 0.429857 0.187329 11.00000 -1.20000 AFIX 0 HKLF 4 REM PR5029_a.res in P4(3)2(1)2 REM R1 = 0.0203 for 4903 Fo > 4sig(Fo) and 0.0229 for all 5170 data REM 203 parameters refined using 0 restraints END WGHT 0.0178 1.6439 REM Highest difference peak 1.658, deepest hole -1.569, 1-sigma level 0.082 Q1 1 0.5268 0.4725 0.2790 11.00000 0.05 1.66 Q2 1 0.5767 0.4233 0.2500 10.50000 0.05 0.76 Q3 1 0.5613 0.5375 0.2512 11.00000 0.05 0.60 Q4 1 0.3831 0.4687 0.2548 11.00000 0.05 0.54 Q5 1 0.4647 0.5353 0.2500 10.50000 0.05 0.53 Q6 1 0.3987 0.5820 0.2307 11.00000 0.05 0.43 Q7 1 0.6079 0.4862 0.2503 11.00000 0.05 0.40 Q8 1 0.6238 0.5699 0.2492 11.00000 0.05 0.33 Q9 1 0.5435 0.5000 0.3504 11.00000 0.05 0.32 Q10 1 0.6388 0.3638 0.3376 11.00000 0.05 0.32 Q11 1 0.5570 0.4013 0.3404 11.00000 0.05 0.29 Q12 1 0.3158 0.4548 0.2298 11.00000 0.05 0.29 Q13 1 0.3212 0.5124 0.2305 11.00000 0.05 0.29 Q14 1 0.6218 0.3613 0.3138 11.00000 0.05 0.28 Q15 1 0.1623 0.5276 0.3409 11.00000 0.05 0.27 Q16 1 0.5797 0.4204 0.2885 11.00000 0.05 0.27 Q17 1 0.2736 0.4650 0.3004 11.00000 0.05 0.27 Q18 1 0.7375 0.2625 0.2500 10.50000 0.05 0.26 Q19 1 0.2571 0.5125 0.2198 11.00000 0.05 0.26 Q20 1 0.2032 0.6044 0.3390 11.00000 0.05 0.25 ; _shelx_res_checksum 17134 _shelx_hkl_file ; 1 0 0 -0.03 0.05 0 1 0 0.00 0.02 0 1 0 -0.04 0.04 0 -1 0 -0.03 0.04 0 -1 0 0.07 0.05 -1 0 0 -0.01 0.02 0 -1 0 -0.02 0.06 0 1 0 0.03 0.05 1 0 0 0.00 0.07 -1 0 0 -0.07 0.04 -1 2 0 75.76 2.68 -1 2 0 76.94 2.68 -2 -1 0 71.99 2.69 1 -2 0 75.00 2.68 -1 2 0 72.14 2.71 -2 -1 0 71.83 2.79 -2 0 0 568.96 21.02 0 -2 0 626.85 21.03 0 -2 0 601.44 20.98 -1 -2 0 72.37 2.63 -2 1 0 73.09 2.70 1 2 0 73.70 2.63 -1 -2 0 75.61 2.77 2 -2 0 247.75 8.57 -2 2 0 257.85 8.53 -2 2 0 247.49 8.59 -2 -2 0 211.30 8.63 -2 -2 0 240.15 8.49 -2 3 0 9.36 0.54 -3 -2 0 9.94 0.62 -3 -2 0 9.33 0.83 -2 3 0 9.40 0.66 -1 3 0 762.72 26.49 -3 -1 0 710.15 26.48 -1 3 0 790.56 26.48 -3 -1 0 723.93 26.58 1 -3 0 776.34 26.47 1 -3 0 763.19 26.49 -3 0 0 0.39 0.34 0 -3 0 0.13 0.21 0 -3 0 0.49 0.30 0 3 0 0.07 0.19 -3 0 0 0.29 0.29 -1 -3 0 801.93 26.74 -3 1 0 720.38 26.66 -1 -3 0 745.40 26.58 -3 1 0 768.91 26.69 -2 -3 0 10.04 0.52 -3 2 0 9.67 0.63 -3 2 0 10.09 0.73 -2 -3 0 9.02 0.82 -3 3 0 206.69 7.44 -3 -3 0 201.31 7.56 -3 3 0 215.66 7.34 -3 -3 0 198.29 7.29 -4 -3 0 22.07 1.41 -4 -3 0 21.33 1.04 -3 4 0 22.11 1.17 -3 4 0 22.69 1.01 -2 4 0 276.42 9.43 -4 -2 0 242.09 9.63 -2 4 0 270.19 9.50 -4 -2 0 271.69 9.47 1 -4 0 4.28 0.43 -4 -1 0 3.14 0.47 -4 -1 0 3.65 0.61 -1 4 0 3.14 0.38 1 -4 0 3.89 0.42 0 -4 0 410.82 14.22 -4 0 0 392.22 14.35 -4 0 0 385.91 14.29 0 4 0 407.55 14.21 0 -4 0 417.84 14.31 -1 -4 0 3.69 0.34 -4 1 0 3.79 0.52 1 4 0 3.61 0.33 -1 -4 0 4.51 0.55 -4 1 0 3.87 0.49 -4 2 0 276.27 9.82 -4 2 0 266.55 9.74 -2 -4 0 266.40 9.63 -2 -4 0 282.44 9.90 -3 -4 0 22.40 1.37 -3 -4 0 20.86 0.95 -4 3 0 23.62 1.08 -4 3 0 21.85 1.23 -4 4 0 489.67 16.69 -4 -4 0 462.85 16.63 -4 4 0 463.92 16.83 -4 -4 0 471.61 16.99 -5 -4 0 98.90 4.51 -5 -4 0 114.99 4.14 -4 5 0 110.04 4.33 -4 5 0 119.85 4.14 -3 5 0 250.92 8.93 -5 -3 0 225.38 9.09 -5 -3 0 253.69 8.85 -3 5 0 252.72 8.78 2 -5 0 0.97 0.36 -5 -2 0 0.47 0.46 -5 -2 0 0.73 0.62 -2 5 0 1.17 0.35 -2 5 0 0.69 0.37 1 -5 0 319.22 10.83 -5 -1 0 273.14 10.98 -5 -1 0 291.79 10.87 -1 5 0 317.31 10.83 1 -5 0 314.77 10.84 0 -5 0 0.19 0.39 0 5 0 -0.21 0.26 -5 0 0 -0.41 0.43 -5 0 0 -0.29 0.47 0 -5 0 0.67 0.31 -1 -5 0 306.55 10.75 -1 -5 0 324.35 10.97 -5 1 0 291.35 10.92 1 5 0 313.82 10.76 -5 1 0 281.63 10.90 -5 2 0 1.62 0.47 -2 -5 0 0.43 0.27 -2 -5 0 0.70 0.53 -5 2 0 0.30 0.49 -5 3 0 247.42 8.95 -3 -5 0 242.92 8.81 -5 3 0 257.74 9.09 -3 -5 0 247.03 9.18 -5 4 0 109.78 4.40 -4 -5 0 112.91 4.13 -5 4 0 115.94 4.23 -4 -5 0 113.77 4.60 -5 -5 0 322.25 12.09 -5 -5 0 322.89 11.60 -5 5 0 339.80 11.66 -5 5 0 321.45 11.86 -5 6 0 85.84 3.16 -6 -5 0 83.34 3.77 -6 -5 0 80.60 3.17 -5 6 0 79.09 3.43 -6 -4 0 71.73 3.72 -4 6 0 87.60 3.51 -4 6 0 91.96 3.29 -6 -4 0 92.23 3.38 -3 6 0 4.87 0.50 -6 -3 0 3.43 0.64 -3 6 0 3.23 0.61 -6 -3 0 3.90 0.90 2 -6 0 235.34 8.37 -2 6 0 234.11 8.43 -2 6 0 235.37 8.37 -6 -2 0 232.19 8.69 -6 -2 0 224.06 8.45 1 -6 0 -0.41 0.37 -6 -1 0 -0.12 0.51 -6 -1 0 -0.04 0.63 -1 6 0 0.52 0.35 -6 0 0 173.16 6.53 0 6 0 175.72 6.37 -6 0 0 168.93 6.59 0 -6 0 179.31 6.38 0 -6 0 181.40 6.51 -1 -6 0 0.33 0.33 -6 1 0 -0.31 0.54 1 6 0 0.59 0.31 -6 1 0 -0.35 0.53 -1 -6 0 -0.05 0.51 -6 2 0 224.07 8.35 -6 2 0 218.43 8.27 -2 -6 0 239.69 8.43 2 6 0 225.58 8.09 -2 -6 0 226.65 8.09 -3 -6 0 3.23 0.78 -3 -6 0 3.72 0.41 -6 3 0 4.02 0.73 -6 3 0 2.99 0.59 -4 -6 0 87.54 3.77 -6 4 0 86.47 3.37 -6 4 0 88.01 3.59 -4 -6 0 85.61 3.22 -5 -6 0 85.56 3.74 -5 -6 0 79.06 3.06 -6 5 0 82.98 3.18 -6 5 0 79.19 3.44 -6 6 0 4.40 0.86 -6 -6 0 4.59 0.56 -6 -6 0 3.56 1.08 -6 6 0 4.10 0.60 -7 -6 0 61.28 3.26 -7 -6 0 63.15 2.55 -6 7 0 62.43 2.93 -7 -5 0 55.30 3.21 -5 7 0 70.53 2.60 -5 7 0 67.13 2.97 -7 -5 0 64.75 2.69 -4 7 0 274.38 9.73 -4 7 0 277.84 9.50 -7 -4 0 268.27 9.62 -7 -4 0 235.97 9.99 -7 -3 0 12.60 1.39 -3 7 0 10.80 0.80 -7 -3 0 10.65 0.97 -3 7 0 10.96 0.92 -2 7 0 25.28 1.27 -7 -2 0 23.49 1.49 2 -7 0 24.23 1.27 -2 7 0 26.07 1.35 -7 -2 0 22.94 1.74 -7 -1 0 71.49 3.20 -7 -1 0 72.99 3.03 -1 7 0 72.08 2.86 1 -7 0 71.09 2.89 0 -7 0 -0.10 0.41 -7 0 0 0.16 0.62 -7 0 0 -0.81 0.63 0 -7 0 0.74 0.52 0 7 0 0.32 0.37 -1 -7 0 74.87 3.04 -7 1 0 75.96 3.09 1 7 0 70.53 2.73 -1 -7 0 72.48 2.76 -7 1 0 62.43 2.98 -7 2 0 23.15 1.47 -2 -7 0 25.47 1.18 2 7 0 25.02 1.15 -7 2 0 27.22 1.66 -2 -7 0 24.60 1.60 -7 3 0 11.17 1.10 -7 3 0 10.42 0.96 -3 -7 0 13.06 1.23 -3 -7 0 10.72 0.75 3 7 0 10.88 0.70 -7 4 0 263.25 9.68 -4 -7 0 250.67 9.28 -4 -7 0 265.08 9.84 -7 4 0 264.87 9.48 -7 5 0 65.57 2.69 -5 -7 0 71.84 3.29 -7 5 0 65.10 3.01 -5 -7 0 61.27 2.51 -7 6 0 63.98 2.62 -6 -7 0 65.67 2.51 -7 6 0 62.06 2.99 -6 -7 0 61.27 3.27 -7 -7 0 2.36 1.20 -7 7 0 5.14 1.03 -8 -7 0 193.45 7.88 -7 8 0 185.78 7.39 -8 -6 0 24.73 2.24 -6 8 0 22.71 1.79 -8 -5 0 174.21 6.61 -8 -5 0 174.26 7.23 -5 8 0 182.84 6.82 -4 8 0 25.45 1.32 -8 -4 0 26.41 1.62 -4 8 0 26.53 1.64 -8 -4 0 29.74 2.26 -3 8 0 98.23 3.76 -3 8 0 94.83 3.56 -8 -3 0 91.15 3.78 -8 -3 0 83.17 4.10 2 -8 0 22.79 1.32 -2 8 0 24.83 1.33 -8 -2 0 27.11 1.93 -8 -2 0 20.71 1.55 -2 8 0 23.47 1.38 -1 8 0 0.94 0.50 1 -8 0 0.31 0.52 -8 -1 0 -0.08 0.82 -8 -1 0 0.87 0.73 -8 0 0 1.98 0.88 0 8 0 2.50 0.51 -8 0 0 3.35 0.84 0 -8 0 2.28 0.68 -1 -8 0 1.09 0.69 -8 1 0 1.50 0.79 1 8 0 0.27 0.40 -1 -8 0 1.11 0.45 -8 1 0 0.44 0.72 -8 2 0 23.97 1.67 2 8 0 23.70 1.16 -2 -8 0 24.70 1.67 -2 -8 0 23.18 1.20 -8 2 0 20.53 1.52 -3 -8 0 92.19 4.01 -8 3 0 91.33 3.77 3 8 0 93.49 3.49 -8 3 0 94.06 3.95 -3 -8 0 92.76 3.50 -4 -8 0 24.50 1.97 4 8 0 23.79 1.16 -4 -8 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48.48 2.90 -12 3 0 49.42 3.28 -3 -12 0 47.16 2.98 -4 -12 0 13.71 1.89 -12 4 0 13.85 1.91 -12 5 0 71.07 3.86 -5 -12 0 59.91 3.87 -6 -12 0 2.97 1.69 -12 6 0 2.90 1.55 -7 -12 0 83.02 4.83 -12 7 0 77.10 4.35 -12 8 0 8.84 1.89 -8 -12 0 10.30 2.31 -9 -12 0 149.72 7.33 -12 9 0 141.16 6.62 -12 10 0 -0.43 1.66 -10 -12 0 0.73 2.25 -12 11 0 63.96 4.22 -11 -12 0 59.58 5.14 -10 13 0 57.14 3.81 -13 -9 0 6.78 2.59 -9 13 0 2.63 1.58 -8 13 0 82.73 4.30 -13 -8 0 81.32 5.49 -7 13 0 1.60 1.35 -13 -7 0 2.50 2.22 -13 -6 0 77.48 4.97 -6 13 0 73.44 3.86 -13 -5 0 28.78 3.18 -5 13 0 32.74 2.35 -4 13 0 90.25 4.27 -13 -4 0 99.63 5.25 -13 -3 0 8.26 1.97 -3 13 0 10.24 1.36 -13 -2 0 34.34 3.19 -2 13 0 35.53 2.31 -13 -2 0 36.92 2.87 -13 -1 0 19.69 2.05 -13 -1 0 24.96 2.42 -13 0 0 2.86 1.54 -13 0 0 3.66 1.54 -13 1 0 23.86 2.32 -13 1 0 27.34 2.44 -13 2 0 44.18 3.21 -13 2 0 36.26 2.89 -13 3 0 8.24 1.83 -3 -13 0 8.14 1.63 -4 -13 0 84.75 4.48 -13 4 0 85.94 4.66 -13 5 0 32.37 2.83 -5 -13 0 31.74 2.90 -6 -13 0 75.11 4.56 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8.12 1.36 -6 8 -4 6.82 1.10 -6 8 4 9.37 1.18 -8 -6 4 10.80 1.14 -8 -6 4 9.18 1.55 -5 8 -4 89.79 3.67 -8 -5 -4 92.77 4.38 -5 8 -4 89.72 3.89 -8 -5 4 84.32 4.14 -5 8 4 85.21 3.72 -8 -5 4 94.46 3.75 -8 -4 -4 42.35 2.66 -4 8 -4 45.55 2.10 -4 8 -4 43.89 2.24 -8 -4 -4 42.41 2.04 -4 8 4 35.44 1.93 -8 -4 4 39.39 2.05 -8 -4 4 31.94 2.34 -8 -3 -4 85.65 3.59 -3 8 -4 89.69 3.62 -3 8 -4 95.00 3.70 -8 -3 -4 86.24 4.05 3 -8 4 99.09 4.01 -3 8 4 103.09 3.97 -8 -3 4 99.07 4.13 -8 -3 4 94.53 4.38 -2 8 -4 33.35 1.72 -8 -2 -4 32.99 1.75 -8 -2 -4 29.04 2.06 -2 8 -4 31.72 1.74 2 -8 -4 31.99 1.43 -8 -2 4 30.71 1.89 2 -8 4 31.06 1.72 -2 8 4 31.16 1.39 -2 8 4 29.94 1.56 2 -8 4 28.70 1.69 -8 -2 4 27.32 2.06 -8 -1 -4 30.49 2.08 1 -8 -4 31.55 1.51 -1 8 -4 32.12 1.60 -1 8 -4 30.18 1.77 -8 -1 -4 29.02 1.72 -8 -1 4 25.11 1.75 1 -8 4 24.07 1.43 -8 -1 4 23.05 1.76 1 -8 4 22.51 1.51 -1 8 4 20.58 1.24 0 8 -4 46.72 2.28 0 -8 -4 42.72 2.02 -8 0 -4 38.62 2.16 0 8 -4 44.80 2.00 -8 0 -4 46.00 2.43 0 -8 4 41.92 2.20 -8 0 4 43.54 2.33 -8 0 4 40.04 2.24 0 8 4 44.35 1.85 0 -8 4 43.16 1.99 1 8 -4 23.70 1.31 -8 1 -4 24.37 1.78 -8 1 -4 24.10 1.61 -1 -8 -4 25.34 1.53 -1 -8 4 31.57 1.60 -8 1 4 31.93 2.03 -1 -8 4 33.84 1.91 1 8 4 31.41 1.41 -8 1 4 28.36 1.81 -8 2 -4 30.65 1.85 -2 -8 -4 32.90 1.84 -8 2 -4 26.57 1.84 -2 -8 4 30.51 1.97 -8 2 4 31.64 2.03 2 8 4 32.37 1.36 -2 -8 4 32.33 1.59 -8 2 4 31.16 1.79 -3 -8 -4 107.43 4.43 -8 3 -4 105.11 4.36 -8 3 -4 103.39 4.35 -8 3 4 90.73 3.66 -8 3 4 94.85 3.96 -3 -8 4 87.24 4.00 -3 -8 4 88.76 3.53 -8 4 -4 38.87 2.25 -4 -8 -4 38.90 2.40 -8 4 -4 39.44 2.19 -4 -8 4 44.22 2.00 -4 -8 4 42.68 2.59 -8 4 4 44.28 2.47 -8 4 4 43.96 2.03 -8 5 -4 92.05 3.89 -5 -8 -4 92.39 4.25 -8 5 -4 91.55 4.03 -5 -8 4 85.99 4.15 -8 5 4 89.51 3.93 -5 -8 4 87.78 3.49 -8 6 -4 9.93 1.36 -8 6 -4 14.40 1.31 -6 -8 -4 12.25 1.71 -8 6 4 6.50 1.15 -6 -8 4 6.82 0.86 -6 -8 4 8.09 1.50 -8 7 -4 161.88 6.47 -7 -8 -4 157.18 6.83 -8 7 4 149.69 6.17 -7 -8 4 155.25 6.61 -8 8 -4 1.41 1.12 -8 -8 -4 1.04 1.49 -8 -8 4 2.90 1.53 -8 8 4 2.52 1.10 -9 -8 -4 185.28 8.30 -8 9 -4 206.01 7.87 -8 9 4 183.78 7.14 -9 -8 4 170.19 7.63 -9 -7 -4 9.74 1.90 -7 9 -4 6.34 1.25 -9 -7 4 10.57 1.84 -7 9 4 8.11 1.22 -6 9 -4 109.50 4.79 -9 -6 -4 117.15 5.42 -6 9 4 103.25 4.46 -9 -6 4 110.49 5.07 -9 -6 4 102.96 4.36 -5 9 -4 9.13 1.16 -9 -5 -4 8.27 1.56 -9 -5 4 9.98 1.22 -5 9 4 12.08 1.22 -9 -5 4 10.23 1.71 -4 9 -4 75.23 3.24 -9 -4 -4 66.43 3.70 -9 -4 -4 71.42 3.07 -4 9 -4 71.14 3.06 -9 -4 4 69.43 3.65 -4 9 4 65.69 3.05 -9 -4 4 70.47 3.21 -9 -3 -4 49.67 2.52 -3 9 -4 53.52 2.49 -3 9 -4 53.99 2.54 -9 -3 -4 58.59 3.18 -3 9 4 46.70 2.21 -9 -3 4 42.67 2.80 -9 -3 4 46.30 2.51 -9 -2 -4 19.67 1.85 -2 9 -4 17.79 1.38 -2 9 -4 17.00 1.35 -9 -2 -4 15.19 1.31 -9 -2 4 27.19 2.14 -9 -2 4 25.51 1.91 2 -9 4 24.48 1.66 -2 9 4 28.03 1.51 2 -9 4 22.08 1.58 -9 -1 -4 65.10 2.90 -1 9 -4 61.15 2.86 -9 -1 -4 61.82 3.21 1 -9 -4 60.13 2.61 -1 9 -4 62.03 2.71 1 -9 4 61.64 2.72 1 -9 4 60.73 2.86 -9 -1 4 62.82 3.16 -9 -1 4 63.01 3.01 -1 9 4 60.19 2.59 0 -9 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1.94 -9 7 4 7.62 1.35 -7 -9 4 7.02 1.65 -8 -9 -4 182.87 8.06 -9 8 -4 196.39 7.68 -8 -9 4 185.89 8.13 -9 8 4 194.39 7.66 -9 -9 -4 0.37 1.67 -9 9 -4 0.02 1.23 -9 -9 4 0.65 1.71 -9 9 4 2.51 1.28 -9 10 -4 142.63 6.16 -10 -9 -4 139.72 6.81 -10 -9 4 167.26 7.50 -9 10 4 152.61 6.69 -8 10 -4 2.18 1.25 -10 -8 -4 3.94 1.88 -10 -8 4 2.82 1.84 -8 10 4 3.12 1.22 -10 -7 -4 81.66 4.60 -7 10 -4 77.74 3.83 -10 -7 4 79.78 4.44 -7 10 4 70.28 3.58 -6 10 -4 3.47 1.11 -10 -6 -4 3.69 1.72 -10 -6 4 4.22 1.59 -6 10 4 2.37 1.02 -5 10 -4 73.33 3.48 -10 -5 -4 75.66 4.18 -10 -5 4 67.95 3.78 -10 -5 4 62.12 3.10 -5 10 4 58.67 3.00 -10 -4 -4 20.23 2.12 -4 10 -4 19.66 1.67 -4 10 4 19.81 1.64 -10 -4 4 23.56 1.93 -10 -4 4 23.99 2.22 -10 -3 -4 48.22 3.08 -3 10 -4 40.53 2.24 -3 10 -4 45.72 2.35 -10 -3 -4 43.39 2.33 -10 -3 4 47.89 2.66 -3 10 4 47.93 2.37 -10 -3 4 51.15 3.11 -2 10 -4 20.93 1.55 -10 -2 -4 20.57 1.62 -2 10 -4 19.90 1.56 -10 -2 -4 20.95 2.00 2 -10 4 22.27 1.62 -10 -2 4 23.98 2.09 -10 -2 4 20.67 1.77 2 -10 4 23.37 1.68 -2 10 4 21.62 1.46 -10 -1 -4 7.93 1.43 -1 10 -4 9.02 0.97 -1 10 -4 7.45 1.13 -10 -1 -4 9.91 1.22 -10 -1 4 14.09 1.53 -10 -1 4 13.36 1.59 1 -10 4 13.76 1.20 -1 10 4 12.69 1.04 1 -10 4 14.23 1.38 0 10 -4 17.72 1.64 0 -10 -4 18.42 1.43 0 10 -4 15.54 1.29 -10 0 -4 15.04 1.45 -10 0 -4 15.11 1.69 0 10 4 15.65 1.16 -10 0 4 16.34 1.65 -10 0 4 14.60 1.61 0 -10 4 18.57 1.68 0 -10 4 18.15 1.41 -1 -10 -4 14.01 1.33 1 10 -4 14.16 1.10 -10 1 -4 14.49 1.43 -10 1 -4 15.50 1.67 -1 -10 4 10.50 1.01 -10 1 4 9.93 1.41 -10 1 4 8.58 1.25 -1 -10 4 6.58 1.18 -2 -10 -4 22.97 1.83 -10 2 -4 26.54 2.10 2 10 -4 20.46 1.42 -10 2 -4 25.67 2.05 -10 2 4 18.46 1.68 -10 2 4 20.11 1.78 -2 -10 4 19.73 1.80 -2 -10 4 18.89 1.41 -10 3 -4 47.83 2.70 3 10 -4 47.81 2.21 -10 3 -4 47.34 2.74 -3 -10 -4 48.83 2.73 -10 3 4 46.54 2.75 -3 -10 4 41.18 2.62 -10 3 4 43.30 2.32 -3 -10 4 40.30 2.06 -10 4 -4 27.29 2.07 -4 -10 -4 27.56 2.16 -10 4 -4 20.53 2.00 -4 -10 4 18.95 1.93 -10 4 4 21.45 1.94 -4 -10 4 18.59 1.50 -10 5 -4 64.10 3.37 -10 5 -4 65.76 3.17 -5 -10 -4 60.27 3.49 -10 5 4 76.81 3.75 -5 -10 4 69.78 3.88 -10 6 -4 2.83 1.30 -6 -10 -4 4.04 1.47 -10 6 4 3.22 1.29 -6 -10 4 3.96 1.50 -10 7 -4 77.42 4.02 -7 -10 -4 80.54 4.40 -10 7 4 77.71 4.02 -7 -10 4 83.14 4.52 -10 8 -4 0.56 1.33 -8 -10 -4 1.37 1.72 -8 -10 4 1.34 1.67 -10 8 4 2.50 1.38 -10 9 -4 161.51 6.82 -9 -10 -4 155.40 7.44 -10 9 4 141.56 6.28 -9 -10 4 149.56 6.97 -10 10 -4 1.49 1.48 -10 -10 -4 1.12 1.99 -10 -10 4 3.42 2.11 -10 10 4 4.56 1.51 -11 -10 -4 86.90 5.48 -10 11 -4 77.04 4.42 -10 11 4 78.36 4.30 -11 -10 4 75.62 5.06 -9 11 -4 0.70 1.37 -11 -9 -4 1.78 2.08 -11 -9 4 -0.68 2.01 -9 11 4 0.42 1.29 -11 -8 -4 109.23 5.93 -8 11 -4 110.77 5.09 -8 11 4 118.72 5.45 -11 -8 4 131.41 6.38 -7 11 -4 1.95 1.21 -11 -7 -4 -0.27 1.77 -11 -7 4 -0.08 1.77 -7 11 4 -0.45 1.05 -11 -6 -4 54.94 3.88 -6 11 -4 57.66 3.08 -6 11 4 60.72 3.30 -11 -6 4 73.42 4.22 -5 11 -4 6.66 1.24 -11 -5 -4 11.44 2.11 -11 -5 4 9.02 1.85 -5 11 4 8.94 1.23 -11 -5 4 9.37 1.60 -4 11 -4 56.01 3.02 -11 -4 -4 68.50 3.93 -11 -4 4 46.12 3.23 -11 -4 4 50.01 2.82 -4 11 4 49.76 2.56 -11 -3 -4 1.35 1.46 -3 11 -4 0.14 0.78 -3 11 4 0.56 0.77 -11 -3 4 1.81 1.39 -11 -3 4 -0.05 1.04 -11 -2 -4 1.32 1.39 -11 -2 -4 -0.24 0.97 -2 11 -4 -1.29 0.73 -2 11 4 2.52 0.75 -11 -2 4 3.39 1.36 -11 -2 4 2.99 1.20 -1 11 -4 2.07 0.97 -1 11 -4 2.48 0.80 -11 -1 -4 5.68 1.43 -11 -1 -4 3.36 1.09 1 -11 4 0.65 0.78 -11 -1 4 1.29 1.17 -1 11 4 2.29 0.70 1 -11 4 0.48 0.87 -11 -1 4 0.83 1.21 0 11 -4 11.23 1.10 0 11 -4 10.94 1.40 -11 0 -4 9.80 1.39 -11 0 -4 11.71 1.65 -11 0 4 8.82 1.48 0 -11 4 11.54 1.39 0 -11 4 10.17 1.12 -11 0 4 10.77 1.57 -11 1 -4 2.30 1.14 1 11 -4 1.20 0.70 -11 1 -4 2.58 1.24 -1 -11 -4 2.14 0.95 -1 -11 4 1.68 1.01 -11 1 4 1.50 1.07 -1 -11 4 2.11 0.78 -11 1 4 3.88 1.34 -11 2 -4 1.86 1.13 -11 2 -4 1.38 1.18 -2 -11 -4 2.51 1.04 2 11 -4 2.11 0.71 -2 -11 4 0.06 0.70 -2 -11 4 0.54 1.04 -11 2 4 1.16 1.01 -11 2 4 0.61 1.21 -3 -11 -4 0.67 1.08 -11 3 -4 0.63 1.13 -11 3 -4 2.06 1.22 -11 3 4 2.97 1.29 -3 -11 4 0.60 1.12 -4 -11 -4 57.01 3.29 -11 4 -4 56.82 3.26 -11 4 -4 56.15 3.06 -4 -11 4 55.98 3.40 -11 4 4 58.72 3.40 -11 5 -4 9.38 1.60 -5 -11 -4 5.75 1.61 -11 5 4 8.61 1.56 -5 -11 4 5.63 1.61 -11 6 -4 70.38 3.89 -6 -11 -4 70.33 4.01 -6 -11 4 59.46 3.74 -11 6 4 54.01 3.39 -11 7 -4 0.46 1.42 -7 -11 -4 0.86 1.61 -7 -11 4 1.90 1.70 -11 7 4 2.71 1.46 -11 8 -4 127.05 5.91 -8 -11 -4 134.99 6.44 -8 -11 4 111.61 5.75 -11 8 4 108.09 5.24 -9 -11 -4 3.29 2.06 -11 9 -4 2.44 1.58 -9 -11 4 0.76 1.98 -11 9 4 1.14 1.53 -11 10 -4 83.56 4.70 -10 -11 -4 92.46 5.50 -11 10 4 76.53 4.34 -10 -11 4 78.94 5.04 -11 11 -4 2.02 1.77 -11 -11 -4 0.26 2.34 -11 -11 4 0.42 2.38 -11 11 4 -2.05 1.49 -12 -11 -4 94.87 6.38 -11 12 -4 101.60 5.63 -11 12 4 98.86 5.27 -12 -11 4 113.38 8.73 -12 -10 -4 5.38 2.59 -10 12 -4 2.35 1.75 -12 -10 4 0.75 2.40 -10 12 4 -0.84 1.46 -9 12 -4 128.13 6.03 -12 -9 -4 132.72 7.09 -9 12 4 119.94 5.46 -12 -9 4 113.00 6.28 -12 -8 -4 4.57 2.32 -8 12 -4 1.25 1.36 -12 -8 4 3.14 2.14 -8 12 4 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5.59 -1 6 -14 151.45 6.11 -6 -1 -14 164.10 6.26 1 -6 -14 149.90 5.66 1 -6 14 175.34 6.54 -6 -1 14 157.41 6.69 -1 6 14 168.18 6.36 6 1 14 172.12 6.35 -6 -1 14 180.89 6.70 0 -6 -14 32.99 1.75 -6 0 -14 29.49 1.64 0 6 -14 30.53 2.11 -6 0 -14 29.24 2.21 6 0 14 32.70 1.66 0 6 14 30.03 1.51 0 -6 14 30.38 2.18 -6 0 14 30.64 1.97 -6 0 14 26.71 1.90 0 -6 14 32.47 1.82 -6 1 -14 162.78 6.38 1 6 -14 160.19 6.79 -1 -6 -14 172.70 6.52 6 -1 -14 176.35 6.56 -6 1 -14 175.05 6.86 -6 1 14 148.62 5.87 -1 -6 14 149.81 5.73 -6 1 14 148.30 5.79 -1 -6 14 139.31 6.07 6 -1 14 151.04 5.67 1 6 14 148.43 5.42 -2 -6 -14 13.31 1.29 2 6 -14 12.21 1.45 -6 2 -14 12.97 1.13 -6 2 -14 14.33 1.58 6 -2 -14 13.04 1.20 -2 -6 14 10.51 1.09 -6 2 14 11.67 1.12 -6 2 14 12.30 1.31 -2 -6 14 11.58 1.50 6 -2 14 8.85 1.03 2 6 14 10.47 0.76 3 6 -14 92.62 4.27 6 -3 -14 88.19 3.62 -3 -6 -14 89.57 3.96 -6 3 -14 86.60 4.12 -6 3 -14 95.39 3.82 -6 3 14 100.15 4.00 -6 3 14 105.59 4.31 6 -3 14 102.73 4.17 -3 -6 14 95.07 4.12 -3 -6 14 96.02 4.60 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2.03 4 3 -15 29.00 2.05 3 -4 -15 32.57 1.60 -3 4 -15 29.07 2.07 4 3 15 37.56 1.62 -4 -3 15 34.04 2.36 -3 4 15 35.72 1.96 3 -4 15 36.83 1.94 -4 -3 15 36.34 2.04 -2 4 -15 93.45 4.05 -4 -2 -15 85.83 4.01 4 2 -15 92.52 3.99 2 -4 -15 91.66 3.63 -4 -2 15 95.25 3.82 -4 -2 15 86.71 4.02 4 2 15 89.41 3.46 2 -4 15 91.54 3.71 -2 4 15 87.75 3.64 1 -4 -15 10.79 0.99 -1 4 -15 7.50 1.11 -4 -1 -15 9.03 1.21 4 1 -15 8.61 1.11 -1 4 15 11.96 0.95 1 -4 15 11.28 1.04 -4 -1 15 12.17 1.34 4 1 15 11.38 0.87 -4 -1 15 10.56 1.09 4 0 -15 25.18 1.70 0 -4 -15 25.80 1.64 0 4 -15 26.45 1.88 -4 0 -15 27.82 1.98 0 -4 15 26.74 1.57 4 0 15 25.82 1.46 0 4 15 26.52 1.39 -4 0 15 28.57 1.82 -4 0 15 26.54 1.70 4 -1 -15 11.77 1.10 1 4 -15 8.30 1.20 -4 1 -15 10.92 1.27 -1 -4 -15 12.26 1.18 -1 -4 15 10.81 1.03 -4 1 15 9.12 1.08 4 -1 15 10.87 0.97 1 4 15 10.80 0.87 -4 1 15 9.43 1.04 -1 -4 15 9.86 1.29 -4 2 -15 87.03 3.88 4 -2 -15 87.49 3.56 -2 -4 -15 89.40 3.75 2 4 -15 81.48 3.88 -2 -4 15 89.74 4.31 -2 -4 15 97.14 4.02 2 4 15 103.32 3.74 -4 2 15 100.12 4.07 4 -2 15 101.10 3.97 -3 -4 -15 34.94 2.14 4 -3 -15 36.49 1.77 3 4 -15 34.58 2.27 -4 3 -15 33.56 2.19 3 4 15 31.21 1.42 -3 -4 15 38.66 2.39 -3 -4 15 34.13 1.90 4 -3 15 28.85 1.77 -4 3 15 29.51 1.85 -4 4 -15 52.95 2.83 4 -4 -15 51.01 2.27 4 4 -15 52.35 2.89 -4 -4 -15 50.91 2.79 -4 4 -15 54.94 2.50 4 4 15 55.15 2.19 4 -4 15 51.29 2.59 -4 -4 15 60.09 3.16 -4 -4 15 55.47 2.68 -4 4 15 56.23 2.67 -4 5 -15 102.28 4.34 5 4 -15 87.46 4.26 -5 -4 -15 93.13 4.29 -5 -4 -15 99.70 3.67 -4 5 -15 91.28 3.95 -5 -4 15 95.68 4.13 -4 5 15 99.96 4.08 -5 -4 15 89.25 4.45 4 -5 15 100.18 4.08 -3 5 -15 63.01 3.15 3 -5 -15 59.96 2.57 5 3 -15 63.26 3.17 -5 -3 -15 62.39 2.50 -5 -3 -15 64.25 3.25 5 3 15 73.95 2.96 -5 -3 15 71.57 3.65 -5 -3 15 79.91 3.45 -3 5 15 77.97 3.30 3 -5 15 79.20 3.35 -5 -2 -15 37.59 2.36 2 -5 -15 36.40 1.82 -5 -2 -15 39.32 1.76 -2 5 -15 43.40 2.38 5 2 -15 34.30 2.18 5 2 15 44.30 1.93 -2 5 15 40.35 2.09 -5 -2 15 44.78 2.34 2 -5 15 45.06 2.23 -5 -2 15 43.01 2.55 -5 -1 -15 48.93 2.15 -1 5 -15 51.56 2.72 -5 -1 -15 46.34 2.73 5 1 -15 47.24 2.53 1 -5 -15 50.10 2.28 -5 -1 15 46.86 2.46 -1 5 15 47.44 2.19 5 1 15 49.65 2.17 -5 -1 15 50.69 2.64 1 -5 15 51.92 2.39 -5 0 -15 127.46 5.42 0 5 -15 130.12 5.40 -5 0 -15 129.85 4.92 5 0 -15 129.34 5.19 0 -5 -15 127.34 5.03 0 -5 15 131.03 5.62 0 -5 15 130.97 5.24 5 0 15 138.97 5.14 -5 0 15 139.43 5.43 -5 0 15 133.53 5.36 0 5 15 131.37 5.03 5 -1 -15 41.92 2.23 -1 -5 -15 44.37 2.28 -5 1 -15 42.98 2.56 -5 1 -15 46.59 2.14 1 5 -15 50.61 2.65 -5 1 15 52.23 2.51 -1 -5 15 51.09 2.42 1 5 15 49.24 2.13 -1 -5 15 53.18 2.88 -5 1 15 49.96 2.54 5 -1 15 52.17 2.36 2 5 -15 43.77 2.54 -5 2 -15 47.74 2.62 -5 2 -15 40.09 2.12 5 -2 -15 44.93 2.16 -2 -5 -15 44.59 2.33 -5 2 15 37.56 2.08 -5 2 15 43.96 2.28 5 -2 15 38.17 2.04 -2 -5 15 42.02 2.53 -2 -5 15 40.83 2.15 2 5 15 43.85 1.76 5 -3 -15 77.17 3.12 -5 3 -15 72.99 3.59 -5 3 -15 72.48 3.22 3 5 -15 75.80 3.69 -3 -5 -15 76.93 3.48 3 5 15 65.77 2.54 -3 -5 15 68.96 3.52 5 -3 15 66.05 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170.38 7.35 3 -2 -22 175.52 7.08 -2 -3 -22 186.64 7.34 2 3 22 172.03 6.46 3 -2 22 171.29 6.62 -3 2 22 166.50 6.67 -2 -3 22 171.48 6.77 -3 3 -22 1.64 1.21 3 3 -22 1.69 1.16 3 -3 -22 2.92 0.95 -3 -3 -22 5.12 1.34 -3 -3 22 4.38 1.44 3 -3 22 3.39 0.96 -3 3 22 3.06 0.95 -3 -3 22 1.78 1.04 3 3 22 4.35 0.78 3 -4 -22 78.55 3.49 -4 -3 -22 70.37 3.92 -3 4 -22 77.65 4.06 4 3 -22 74.77 3.87 4 3 22 98.96 4.04 3 -4 22 104.04 4.38 -4 -3 22 98.72 4.50 -3 4 22 100.27 4.30 -4 -3 22 101.85 4.88 -4 -2 -22 4.71 1.39 2 -4 -22 3.39 1.00 4 2 -22 4.95 1.27 -2 4 -22 3.33 1.32 2 -4 22 7.52 1.16 4 2 22 6.64 0.89 -4 -2 22 6.32 1.47 -4 -2 22 6.74 1.24 -2 4 22 6.46 1.03 1 -4 -22 140.44 5.62 -4 -1 -22 125.03 5.88 4 1 -22 137.38 5.77 -1 4 -22 141.04 6.03 -4 -1 22 148.80 5.99 -1 4 22 153.44 5.74 1 -4 22 145.92 5.88 4 1 22 136.17 5.62 4 0 -22 0.01 0.89 0 4 -22 1.96 1.15 -4 0 -22 1.55 1.21 0 -4 -22 2.82 1.05 -4 0 22 0.70 0.92 0 -4 22 -0.02 0.88 4 0 22 -0.35 0.70 0 4 22 3.05 0.79 -4 1 -22 144.38 6.15 4 -1 -22 134.06 5.69 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78.29 3.27 5 1 -22 4.17 1.19 -5 -1 -22 4.21 1.48 1 -5 -22 5.40 1.14 -1 5 -22 2.03 1.27 -5 -1 22 2.58 1.25 -1 5 22 2.55 0.85 5 1 22 4.73 0.86 -5 -1 22 4.42 1.17 1 -5 22 4.09 1.06 0 -5 -22 89.46 4.03 0 5 -22 94.22 4.48 5 0 -22 85.98 4.04 -5 0 -22 84.19 4.41 -5 0 22 91.44 4.27 5 0 22 98.63 4.01 0 5 22 95.50 3.93 -5 0 22 93.74 4.39 0 -5 22 97.10 4.24 -5 1 -22 3.10 1.39 1 5 -22 4.63 1.44 5 -1 -22 3.59 1.04 -1 -5 -22 3.97 1.16 1 5 22 4.45 0.82 -5 1 22 3.17 1.09 5 -1 22 4.06 0.94 -1 -5 22 5.98 1.17 -2 -5 -22 74.97 3.61 -5 2 -22 70.47 3.95 2 5 -22 70.23 3.85 5 -2 -22 70.13 3.34 -5 2 22 68.68 3.38 -2 -5 22 66.05 3.85 -2 -5 22 68.56 3.37 5 -2 22 64.77 3.14 -5 3 -22 10.78 1.70 -3 -5 -22 10.24 1.59 5 -3 -22 11.89 1.39 -5 3 -22 12.01 1.34 3 5 -22 10.95 1.68 -5 3 22 7.69 1.30 5 -3 22 7.29 1.19 -3 -5 22 7.73 1.76 -3 -5 22 8.78 1.33 -5 4 -22 83.53 3.90 -5 4 -22 86.78 4.47 4 5 -22 91.56 4.49 -4 -5 -22 78.77 4.18 -4 -5 22 89.37 4.51 5 -4 22 105.88 4.44 -5 4 22 99.79 4.51 -4 -5 22 107.26 5.19 -5 -5 -22 10.76 1.77 -5 5 -22 11.37 1.43 5 5 -22 9.78 1.70 -5 5 -22 12.35 1.89 -5 5 22 13.48 1.59 5 -5 22 13.26 1.56 -5 -5 22 13.59 2.09 -5 -5 22 10.60 1.57 6 5 -22 31.67 2.74 -5 6 -22 23.57 2.41 -6 -5 -22 25.61 2.56 -5 6 -22 21.79 1.93 -5 6 22 24.04 2.06 5 -6 22 23.69 2.00 -6 -5 22 29.23 2.36 -6 -5 22 26.90 2.74 6 4 -22 21.08 2.16 -4 6 -22 18.58 2.19 -6 -4 -22 13.78 2.04 -4 6 -22 18.74 1.69 -6 -4 22 19.37 2.29 4 -6 22 19.65 1.74 -6 -4 22 15.04 1.80 -4 6 22 15.11 1.63 -6 -3 -22 53.26 3.45 6 3 -22 60.53 3.38 -3 6 -22 53.88 3.46 3 -6 22 51.29 2.96 -6 -3 22 52.95 3.41 -6 -3 22 48.83 3.05 -3 6 22 54.41 2.79 -2 6 -22 3.06 1.41 6 2 -22 3.20 1.22 -6 -2 -22 4.27 1.52 -6 -2 22 -0.21 1.07 -6 -2 22 2.67 1.36 -2 6 22 1.27 0.85 2 -6 22 2.95 1.07 -6 -1 -22 43.74 2.36 6 1 -22 49.02 2.92 -1 6 -22 49.75 3.22 -6 -1 -22 49.73 3.26 -6 -1 22 52.29 2.96 -1 6 22 52.76 2.52 6 1 22 49.33 2.48 1 -6 22 47.59 2.78 -6 -1 22 50.78 3.05 -6 0 -22 6.97 1.03 0 -6 -22 3.71 1.13 -6 0 -22 5.64 1.60 0 6 -22 6.24 1.54 6 0 -22 6.47 1.22 0 -6 22 4.24 1.13 -6 0 22 4.30 1.26 0 6 22 6.70 1.38 6 0 22 5.24 0.97 -6 0 22 6.60 1.27 6 -1 -22 52.95 2.82 -1 -6 -22 47.01 2.80 -6 1 -22 52.86 2.64 -6 1 -22 47.51 3.29 1 6 -22 54.43 3.36 6 -1 22 46.21 2.46 -6 1 22 45.05 2.78 -1 -6 22 46.59 2.70 -2 -6 -22 1.68 1.13 -6 2 -22 2.02 1.45 6 -2 -22 1.73 0.89 2 6 -22 1.54 1.35 -6 2 -22 1.43 0.95 -2 -6 22 4.20 1.18 6 -2 22 3.35 1.01 -2 -6 22 3.49 1.65 -6 2 22 2.63 1.17 3 6 -22 48.30 3.34 -6 3 -22 47.58 3.38 -3 -6 -22 49.78 3.06 -6 3 -22 53.03 2.80 6 -3 22 58.82 3.07 -3 -6 22 59.83 3.88 -6 3 22 58.62 3.22 -3 -6 22 57.11 3.18 4 6 -22 19.00 2.17 -4 -6 -22 19.33 2.07 -6 4 -22 17.31 1.67 -6 4 -22 17.15 2.20 -4 -6 22 19.93 1.93 -6 4 22 21.90 2.01 6 -4 22 19.58 1.76 -4 -6 22 24.35 2.62 -5 -6 -22 24.53 2.38 5 6 -22 24.05 2.47 -6 5 -22 21.97 2.37 -6 5 -22 25.75 2.11 -6 5 22 24.89 2.14 -5 -6 22 26.65 2.24 6 -5 22 26.82 2.26 -5 -6 22 28.87 2.83 -6 6 -22 45.52 3.41 -6 -6 -22 49.53 3.41 -6 6 -22 52.50 2.97 6 6 -22 45.42 3.44 -6 -6 22 54.24 3.92 -6 -6 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32.88 2.01 0 7 -22 37.28 2.96 7 0 22 29.07 1.95 -7 0 22 28.41 2.44 -7 0 22 37.99 2.54 0 -7 22 29.82 2.31 -1 -7 -22 2.16 1.09 7 -1 -22 2.78 1.03 -7 1 -22 3.15 1.01 -7 1 -22 -0.79 1.50 1 7 -22 1.95 1.38 -1 -7 22 1.85 1.11 -7 1 22 1.59 1.18 7 -1 22 0.49 0.88 -7 1 22 3.29 1.27 2 7 -22 37.10 2.98 -7 2 -22 34.85 3.09 -2 -7 -22 30.62 2.42 -7 2 -22 37.32 2.29 7 -2 22 24.68 1.93 -7 2 22 24.46 2.17 -2 -7 22 26.67 2.08 -2 -7 22 21.87 2.49 -3 -7 -22 20.52 2.05 3 7 -22 20.73 2.32 -7 3 -22 20.62 2.38 -7 3 -22 18.05 1.70 7 -3 22 19.63 1.72 -3 -7 22 18.07 2.34 -7 3 22 18.14 1.94 -3 -7 22 20.85 1.91 4 7 -22 26.49 2.57 -7 4 -22 21.21 2.42 -7 4 -22 22.40 1.89 -4 -7 -22 21.49 2.17 -4 -7 22 30.95 3.02 -4 -7 22 30.76 2.49 -7 4 22 31.70 2.59 7 -4 22 28.56 2.29 -5 -7 -22 41.96 3.11 -7 5 -22 45.71 3.39 5 7 -22 50.84 3.50 -7 5 -22 42.82 2.79 -5 -7 22 66.00 4.37 -7 5 22 71.82 3.74 7 -5 22 66.45 3.53 -5 -7 22 69.73 3.77 6 7 -22 25.47 2.63 -7 6 -22 23.88 2.07 -7 6 -22 23.20 2.47 -6 -7 -22 26.82 2.58 7 -6 22 19.19 1.92 -6 -7 22 20.08 2.61 -7 6 22 21.86 2.15 -6 -7 22 20.34 2.15 -7 -7 -22 58.57 3.96 7 7 -22 62.06 4.04 -7 7 -22 59.56 3.49 -7 7 -22 55.80 3.83 -7 7 22 60.97 3.69 -7 -7 22 58.11 3.69 7 -7 22 62.23 3.59 -7 -7 22 74.28 4.62 8 7 -22 9.06 2.04 -7 8 -22 9.39 1.95 -7 8 -22 6.59 1.59 -8 -7 -22 5.23 2.01 -7 8 22 11.84 1.85 -8 -7 22 9.55 1.82 7 -8 22 12.72 1.83 -8 -7 22 9.87 2.34 -6 8 -22 72.68 4.24 8 6 -22 71.82 4.34 -8 -6 -22 67.85 4.41 -6 8 -22 73.54 3.81 -6 8 22 89.30 4.39 -8 -6 22 79.63 4.49 6 -8 22 89.18 4.33 -8 -6 22 86.78 5.12 -5 8 -22 11.74 2.02 -8 -5 -22 13.58 2.26 -5 8 -22 15.03 1.74 8 5 -22 14.34 2.07 -5 8 22 15.67 1.79 5 -8 22 12.63 1.71 -8 -5 22 13.01 1.87 -8 -5 22 12.38 2.26 8 4 -22 31.55 2.87 -8 -4 -22 33.31 3.10 -4 8 -22 34.45 2.55 -4 8 -22 32.07 2.96 4 -8 22 37.93 2.72 -4 8 22 41.88 2.64 -8 -4 22 36.40 3.29 -8 -4 22 32.56 2.76 -3 8 -22 10.91 1.57 -8 -3 -22 13.91 2.22 8 3 -22 17.10 2.05 -3 8 -22 18.57 2.18 -3 8 22 18.05 1.80 -8 -3 22 18.28 2.27 3 -8 22 16.80 1.80 -8 -3 22 16.35 1.93 -2 8 -22 17.61 2.21 8 2 -22 18.54 2.07 -8 -2 -22 17.07 2.34 2 -8 22 14.31 1.69 -8 -2 22 10.50 1.67 -8 -2 22 15.54 1.99 8 1 -22 21.22 2.05 -8 -1 -22 20.07 2.41 -1 8 -22 23.65 2.43 -8 -1 22 25.38 2.31 -8 -1 22 30.48 2.65 1 -8 22 29.41 2.38 0 8 -22 -1.20 1.35 -8 0 -22 0.20 0.90 -8 0 -22 0.39 1.54 8 0 -22 1.19 1.08 8 0 22 -0.26 0.83 -8 0 22 2.58 1.33 0 -8 22 0.91 1.09 -8 0 22 1.56 1.25 -8 1 -22 24.34 2.09 -8 1 -22 33.36 3.10 1 8 -22 30.72 2.88 8 -1 -22 30.40 2.81 8 -1 22 22.91 1.77 -8 1 22 21.25 2.08 -1 -8 22 20.62 1.94 2 8 -22 15.57 2.11 -8 2 -22 13.44 2.20 -8 2 -22 13.62 1.51 -2 -8 22 18.93 1.84 -8 2 22 18.78 2.01 -2 -8 22 14.91 2.29 8 -2 22 16.61 1.58 3 8 -22 17.72 2.31 -8 3 -22 16.22 1.64 -3 -8 -22 15.24 1.86 -8 3 -22 12.22 2.13 -8 3 22 10.83 1.70 -3 -8 22 16.02 1.74 -3 -8 22 16.86 2.47 8 -3 22 12.19 1.49 4 8 -22 38.90 3.23 -4 -8 -22 35.01 2.88 -8 4 -22 36.57 3.24 -8 4 -22 33.84 2.49 -4 -8 22 38.61 3.59 8 -4 22 40.66 2.57 -4 -8 22 29.58 2.46 -8 4 22 40.30 2.89 -8 5 -22 14.45 1.81 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9.99 2.34 7 7 -27 12.46 2.31 -7 -7 27 10.48 2.63 -7 7 27 14.86 2.03 7 -7 27 11.15 1.87 -7 -7 27 14.41 2.20 8 7 -27 3.93 1.92 -8 -7 -27 5.84 2.29 -7 8 -27 5.26 2.10 -7 8 -27 3.99 1.77 -7 8 27 8.09 1.87 -8 -7 27 7.72 1.99 7 -8 27 6.00 1.73 -8 -7 27 8.82 2.70 8 6 -27 19.73 2.59 -8 -6 -27 22.66 2.94 -6 8 -27 19.47 2.21 -6 8 -27 18.12 2.65 -8 -6 27 16.30 2.39 -8 -6 27 23.28 3.01 6 -8 27 21.42 2.30 -6 8 27 27.66 2.46 -5 8 -27 19.33 2.65 8 5 -27 22.37 2.54 -8 -5 -27 24.08 2.97 -5 8 -27 21.86 2.28 -8 -5 27 23.86 2.63 -8 -5 27 21.20 2.80 5 -8 27 21.95 2.27 -8 -4 -27 38.33 3.52 -4 8 -27 35.82 2.98 8 4 -27 35.56 3.14 -4 8 -27 34.21 3.29 -8 -4 27 30.19 3.09 -8 -4 27 31.29 2.83 4 -8 27 34.35 2.69 -8 -3 -27 14.97 2.57 -3 8 -27 13.51 2.37 8 3 -27 16.22 2.15 3 -8 27 15.51 1.96 -8 -3 27 17.33 2.38 -8 -3 27 18.59 2.20 -8 -2 -27 63.92 4.40 -2 8 -27 57.72 4.09 8 2 -27 53.34 3.55 -8 -2 27 62.91 3.89 -8 -2 27 51.56 3.65 2 -8 27 59.38 3.53 -8 -1 -27 34.99 3.43 -1 8 -27 34.84 3.24 8 1 -27 36.50 2.92 -8 -1 27 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1.67 -7 -8 27 3.30 2.38 -7 -8 27 6.42 1.93 9 6 -27 13.04 2.33 -9 -6 -27 11.33 2.62 -6 9 -27 11.08 2.36 -6 9 -27 11.10 2.00 -9 -6 27 13.41 2.66 -9 -6 27 14.23 2.39 6 -9 27 12.84 2.05 -5 9 -27 20.62 2.23 -9 -5 -27 19.24 2.98 9 5 -27 26.39 2.80 -5 9 -27 22.05 2.86 -9 -5 27 23.49 2.99 5 -9 27 24.12 2.41 -9 -5 27 23.14 2.68 -4 9 -27 26.52 2.99 -9 -4 -27 34.26 3.45 -4 9 -27 21.82 2.36 9 4 -27 28.19 2.80 -9 -4 27 24.40 2.60 4 -9 27 20.37 2.25 -9 -4 27 22.99 2.84 -9 -3 -27 46.63 4.16 9 3 -27 42.63 3.36 -3 9 -27 47.90 3.28 -3 9 -27 41.28 3.74 -9 -3 27 46.53 3.62 -9 -3 27 39.12 3.17 3 -9 27 42.03 3.12 9 2 -27 32.13 2.99 -2 9 -27 35.34 3.37 -9 -2 -27 31.81 3.44 -9 -2 27 25.55 2.58 -9 -2 27 22.72 2.59 2 -9 27 27.81 2.39 -9 -1 -27 28.53 3.24 -1 9 -27 40.99 3.58 1 -9 27 33.22 2.67 -9 -1 27 27.94 2.83 -9 0 -27 30.63 3.24 0 9 -27 35.64 3.31 -9 0 27 34.16 2.93 0 -9 27 35.07 2.92 1 9 -27 32.64 3.22 -9 1 -27 35.69 3.53 -9 1 27 30.88 2.76 -1 -9 27 30.36 2.57 2 9 -27 27.27 3.07 -9 2 -27 29.48 3.19 -9 2 27 28.28 2.60 -2 -9 27 28.40 2.53 3 9 -27 40.95 3.69 -9 3 -27 43.54 3.97 -9 3 -27 38.12 2.90 -9 3 27 43.99 3.42 9 -3 27 43.80 2.98 -3 -9 27 45.31 3.37 4 9 -27 23.17 2.91 -9 4 -27 14.79 2.64 -9 4 -27 24.86 2.27 -9 4 27 36.15 2.96 9 -4 27 25.22 2.35 -4 -9 27 30.75 2.74 -4 -9 27 32.37 3.53 -9 5 -27 24.90 2.36 -9 5 -27 22.29 2.93 5 9 -27 22.80 2.96 -5 -9 27 21.36 2.41 -9 5 27 22.38 2.49 -5 -9 27 26.19 3.27 9 -5 27 22.64 2.23 6 9 -27 12.98 2.72 -9 6 -27 12.80 2.62 -9 6 -27 10.87 1.95 -6 -9 27 15.46 3.18 -9 6 27 13.83 2.24 -6 -9 27 16.00 2.28 9 -6 27 11.50 1.90 10 4 -27 20.75 2.55 -4 10 -27 15.57 2.67 -4 10 -27 15.23 2.14 -10 -4 -27 19.33 3.05 -10 -4 27 12.18 2.24 4 -10 27 15.92 2.12 -10 -4 27 13.17 2.47 -3 10 -27 16.34 2.19 -3 10 -27 22.76 2.84 10 3 -27 20.78 2.52 -10 -3 -27 17.35 2.92 3 -10 27 18.53 2.26 -10 -3 27 18.82 2.63 -10 -3 27 16.41 2.40 -2 10 -27 48.55 3.45 -2 10 -27 49.56 4.02 -10 -2 -27 48.77 4.42 -10 -2 27 40.37 3.26 2 -10 27 41.66 3.23 -1 10 -27 59.57 4.37 -10 -1 -27 70.96 4.93 1 -10 27 65.64 3.87 -10 -1 27 56.77 4.06 0 10 -27 21.68 2.81 -10 0 -27 19.62 2.95 0 -10 27 20.53 2.28 -10 0 27 18.01 2.42 1 10 -27 63.94 4.56 -10 1 -27 64.71 4.76 -1 -10 27 64.59 3.91 -10 1 27 65.32 4.31 2 10 -27 45.75 4.06 -10 2 -27 45.65 4.21 -10 2 27 43.80 3.55 -2 -10 27 46.02 3.45 -10 3 -27 14.99 2.77 -10 3 -27 14.44 2.70 3 10 -27 18.64 2.69 -3 -10 27 18.65 2.24 -10 3 27 17.56 2.35 -10 4 -27 11.32 2.63 4 10 -27 18.29 2.94 -10 4 -27 20.97 2.25 -4 -10 27 20.78 2.41 -10 4 27 16.71 2.52 -4 -10 27 20.74 3.22 10 -4 27 20.81 2.18 -1 11 -27 26.06 3.30 -1 11 -27 23.06 2.90 0 11 -27 33.93 3.38 0 -11 27 35.45 3.14 1 11 -27 19.87 3.12 0 0 -28 57.71 3.57 0 0 28 67.66 3.48 1 0 -28 1.87 1.31 0 1 -28 0.85 1.34 -1 0 -28 1.28 1.38 0 -1 -28 0.76 1.33 0 1 28 0.12 0.98 1 0 28 2.18 1.07 0 -1 28 2.05 1.10 -1 0 28 1.29 1.10 1 1 -28 135.20 6.33 -1 1 -28 158.01 6.59 -1 -1 -28 130.52 6.28 1 -1 -28 151.57 6.37 -1 1 28 147.17 6.26 -1 -1 28 156.46 6.40 1 -1 28 154.72 6.29 1 1 28 152.67 6.21 -2 -1 -28 0.86 1.42 1 -2 -28 -1.20 1.18 -1 2 -28 0.54 1.41 2 1 -28 1.42 1.27 -2 -1 28 0.69 1.17 1 -2 28 -0.30 1.03 -1 2 28 0.86 1.04 2 1 28 -0.06 0.89 0 2 -28 147.45 6.46 -2 0 -28 140.06 6.40 2 0 -28 142.72 6.24 0 -2 -28 133.60 6.15 -2 0 28 148.56 6.22 0 -2 28 144.40 6.20 0 2 28 152.13 6.07 2 0 28 149.84 6.09 2 -1 -28 -0.09 1.15 1 2 -28 -1.56 1.24 -1 -2 -28 -0.03 1.35 -2 1 -28 0.35 1.40 2 -1 28 0.81 1.00 1 2 28 0.15 0.92 -1 -2 28 2.61 1.20 -2 1 28 1.16 1.10 -2 -2 -28 128.50 5.85 2 -2 -28 118.83 5.57 -2 2 -28 128.98 6.01 2 2 -28 122.95 5.79 -2 -2 28 127.18 5.64 -2 2 28 137.16 5.57 2 2 28 129.49 5.34 2 -2 28 125.15 5.49 2 -3 -28 12.08 1.72 -2 3 -28 10.40 2.02 -3 -2 -28 13.61 2.09 3 2 -28 11.48 1.83 -3 -2 28 11.55 1.69 -2 3 28 11.36 1.49 2 -3 28 13.04 1.58 3 2 28 13.47 1.40 1 -3 -28 91.26 4.45 3 1 -28 87.03 4.50 -3 -1 -28 90.97 4.75 -1 3 -28 89.82 4.84 -3 -1 28 96.66 4.56 3 1 28 97.60 4.25 -1 3 28 92.35 4.30 1 -3 28 98.33 4.48 -3 0 -28 6.66 1.80 0 3 -28 5.34 1.63 3 0 -28 2.04 1.32 0 -3 -28 5.24 1.49 0 -3 28 6.83 1.39 0 3 28 7.42 1.24 -3 0 28 6.34 1.41 3 0 28 5.96 1.20 -1 -3 -28 92.02 4.56 1 3 -28 81.42 4.55 -3 1 -28 88.82 4.79 3 -1 -28 89.87 4.35 1 3 28 88.07 3.92 -3 1 28 89.26 4.18 3 -1 28 85.75 4.03 -1 -3 28 85.07 4.24 -3 2 -28 12.00 2.04 2 3 -28 13.79 1.96 -2 -3 -28 11.13 1.87 3 -2 -28 10.80 1.65 3 -2 28 7.69 1.38 -2 -3 28 13.30 1.71 -3 2 28 11.07 1.55 -3 -3 -28 59.57 3.88 -3 3 -28 72.00 4.26 3 3 -28 69.11 3.97 3 -3 -28 62.71 4.76 -3 -3 28 65.00 3.66 3 -3 28 67.48 3.45 -3 3 28 63.46 3.40 4 3 -28 2.31 1.47 -4 -3 -28 1.90 1.64 -3 4 -28 3.41 1.76 -3 4 28 7.02 1.36 -4 -3 28 4.75 1.48 3 -4 28 5.18 1.34 4 2 -28 79.00 4.26 -2 4 -28 75.80 4.46 -4 -2 -28 77.15 4.45 -2 4 28 84.74 3.96 2 -4 28 83.33 4.09 -4 -2 28 83.45 4.25 -1 4 -28 0.26 1.48 4 1 -28 0.73 1.25 1 -4 -28 -0.51 1.19 -4 -1 -28 1.32 1.59 -4 -1 28 2.04 1.28 4 1 28 1.76 0.96 1 -4 28 -0.34 1.15 -1 4 28 1.98 1.06 0 4 -28 95.86 4.99 -4 0 -28 92.06 4.88 0 -4 -28 92.85 4.52 4 0 -28 90.84 4.53 4 0 28 100.20 4.50 0 -4 28 109.17 4.85 0 4 28 100.68 4.45 -4 0 28 100.06 4.74 -4 1 -28 0.82 1.59 -1 -4 -28 -1.70 1.25 1 4 -28 0.85 1.42 4 -1 -28 0.34 1.18 -4 1 28 -0.48 1.11 4 -1 28 0.24 1.03 -1 -4 28 2.57 1.27 2 4 -28 81.96 4.51 -4 2 -28 78.52 4.53 4 -2 -28 78.48 3.99 -2 -4 -28 77.95 4.24 -2 -4 28 76.65 4.05 -4 2 28 71.24 3.87 4 -2 28 87.01 3.91 -4 3 -28 4.39 1.76 -3 -4 -28 5.13 1.69 3 4 -28 7.87 1.79 4 -3 28 3.14 1.22 -4 3 28 4.23 1.32 -3 -4 28 3.59 1.43 -4 -4 -28 46.00 3.46 4 4 -28 43.58 3.36 -4 4 -28 42.83 3.63 4 -4 28 46.12 3.04 -4 4 28 46.04 2.98 -4 -4 28 45.38 3.25 5 4 -28 9.02 1.85 -4 5 -28 9.70 2.10 -5 -4 -28 15.57 2.25 -5 -4 28 16.13 2.02 -4 5 28 13.37 1.73 4 -5 28 17.01 1.88 -5 -3 -28 69.32 4.34 5 3 -28 76.02 4.20 -3 5 -28 73.67 4.52 -3 5 28 64.38 3.49 -5 -3 28 71.25 3.88 3 -5 28 68.29 3.75 -2 5 -28 14.31 2.25 5 2 -28 13.75 1.92 -5 -2 -28 11.06 2.17 -2 5 28 17.13 1.70 2 -5 28 16.42 1.89 -5 -2 28 16.93 2.01 5 1 -28 72.89 3.92 -1 5 -28 72.29 4.38 -5 -1 -28 71.10 4.41 1 -5 28 89.24 4.31 -1 5 28 84.84 4.72 -5 -1 28 86.87 4.36 -5 0 -28 -0.70 1.55 0 -5 -28 1.51 1.96 5 0 -28 0.81 1.20 0 5 -28 -1.34 1.46 -5 0 28 -0.03 1.21 0 -5 28 -0.82 1.16 5 0 28 -1.42 0.93 1 5 -28 81.53 4.69 5 -1 -28 84.21 4.28 -1 -5 -28 89.46 4.47 -5 1 -28 91.97 5.01 -1 -5 28 74.84 3.99 -5 1 28 81.35 4.02 5 -1 28 74.47 3.71 -2 -5 -28 13.87 2.02 2 5 -28 17.20 2.25 -5 2 -28 18.92 2.48 -5 2 28 15.95 1.82 -2 -5 28 10.40 1.68 5 -2 28 12.39 1.58 -5 3 -28 71.44 4.43 -3 -5 -28 67.66 3.98 3 5 -28 69.21 4.31 -3 -5 28 72.82 4.13 5 -3 28 79.98 3.92 -5 3 28 80.78 4.02 -5 4 -28 13.93 1.74 -5 4 -28 12.59 2.20 4 5 -28 15.66 2.23 -4 -5 -28 10.96 2.02 -4 -5 28 12.75 1.86 5 -4 28 11.20 1.63 -5 4 28 14.87 1.80 -5 5 -28 33.22 3.14 -5 5 -28 26.86 2.33 5 5 -28 33.65 3.14 -5 -5 -28 29.00 2.91 -5 -5 28 25.09 3.01 -5 -5 28 34.03 2.72 5 -5 28 30.25 2.38 -5 5 28 25.90 2.28 -5 6 -28 15.95 1.99 -6 -5 -28 25.73 2.77 6 5 -28 24.74 2.64 -5 6 -28 22.88 2.77 -6 -5 28 30.15 3.19 5 -6 28 25.66 2.29 -5 6 28 26.59 2.29 -6 -5 28 25.77 2.55 6 4 -28 31.35 2.82 -6 -4 -28 27.50 2.86 -4 6 -28 27.02 2.93 -6 -4 28 25.64 2.83 -6 -4 28 21.19 2.39 -4 6 28 25.65 2.17 4 -6 28 23.16 2.20 6 3 -28 20.56 2.30 -3 6 -28 20.88 2.63 -6 -3 -28 18.25 2.49 3 -6 28 25.33 2.22 -3 6 28 23.03 2.04 -6 -3 28 20.17 2.23 -2 6 -28 26.56 2.89 -6 -2 -28 26.59 2.85 6 2 -28 26.22 2.48 2 -6 28 19.44 2.00 -6 -2 28 21.71 2.16 -1 6 -28 1.10 1.64 -6 -1 -28 1.07 1.76 6 1 -28 4.28 1.41 -6 -1 28 1.20 1.37 1 -6 28 1.52 1.28 6 0 -28 66.31 3.65 -6 0 -28 64.04 4.34 -6 0 -28 62.00 3.29 0 6 -28 61.80 4.14 0 -6 28 67.96 3.72 -6 0 28 63.91 3.75 -6 1 -28 0.88 1.12 1 6 -28 0.89 1.57 -6 1 -28 0.24 1.79 6 -1 28 1.24 1.07 -1 -6 28 1.86 1.30 -6 1 28 2.50 1.36 -6 2 -28 21.00 1.93 2 6 -28 24.99 2.71 -2 -6 -28 22.98 2.33 -6 2 -28 14.87 2.42 -6 2 28 27.06 2.40 6 -2 28 31.27 2.44 -2 -6 28 27.98 2.46 -6 3 -28 21.51 2.77 -3 -6 -28 22.13 2.38 -6 3 -28 20.35 2.02 3 6 -28 24.49 2.74 6 -3 28 22.01 2.03 -3 -6 28 22.85 2.30 -6 3 28 22.41 2.21 -6 4 -28 28.63 2.33 4 6 -28 24.35 2.65 -6 4 -28 25.17 2.87 -4 -6 -28 24.57 2.64 6 -4 28 31.20 2.39 -6 4 28 25.95 2.36 -4 -6 28 27.48 2.49 -6 5 -28 24.97 2.96 -6 5 -28 25.36 2.30 5 6 -28 24.35 2.70 -5 -6 -28 26.15 2.74 -5 -6 28 23.77 3.09 -5 -6 28 25.89 2.49 6 -5 28 26.42 2.27 -6 5 28 22.66 2.28 -6 -6 -28 29.05 2.97 -6 6 -28 32.58 3.23 6 6 -28 28.23 2.92 -6 6 -28 29.74 2.53 6 -6 28 33.35 2.64 -6 6 28 32.83 2.68 -6 -6 28 31.35 2.88 -6 -6 28 27.74 3.19 7 6 -28 42.50 3.62 -6 7 -28 34.20 3.44 -6 7 -28 40.15 3.13 -7 -6 -28 40.12 3.57 -6 7 28 39.08 3.14 -7 -6 28 45.23 4.12 -7 -6 28 39.17 3.23 6 -7 28 42.23 3.18 -7 -5 -28 7.96 2.13 7 5 -28 5.34 1.80 -5 7 -28 9.58 2.23 -5 7 -28 9.23 1.81 5 -7 28 9.87 1.82 -7 -5 28 8.20 1.92 -7 -5 28 5.41 2.16 -5 7 28 10.79 1.71 -7 -4 -28 19.41 2.70 7 4 -28 20.48 2.39 -4 7 -28 18.06 2.06 -4 7 -28 15.68 2.51 -7 -4 28 12.42 2.08 4 -7 28 17.56 2.01 -7 -4 28 14.84 2.41 7 3 -28 33.03 2.93 -7 -3 -28 29.04 3.01 -3 7 -28 24.46 2.89 3 -7 28 23.89 2.28 -7 -3 28 24.26 2.78 -7 -3 28 28.41 2.59 -2 7 -28 6.50 2.06 7 2 -28 5.44 1.62 -7 -2 -28 7.53 2.15 2 -7 28 8.47 1.65 -7 -2 28 5.24 1.61 -7 -2 28 5.79 1.87 -7 -1 -28 17.03 2.64 7 1 -28 18.75 2.13 -1 7 -28 16.00 2.38 -7 -1 28 20.61 2.25 1 -7 28 16.33 1.97 -7 0 -28 4.19 2.00 0 7 -28 6.26 1.93 7 0 -28 9.00 1.64 -7 0 28 6.43 1.65 0 -7 28 10.62 1.73 -7 1 -28 18.54 1.80 1 7 -28 20.92 2.62 -7 1 -28 18.57 2.64 -7 1 28 15.95 2.06 7 -1 28 15.06 1.67 -1 -7 28 14.89 1.91 2 7 -28 7.06 1.96 -7 2 -28 6.60 1.43 -7 2 -28 9.29 2.29 7 -2 28 6.44 1.42 -7 2 28 8.64 1.70 -2 -7 28 11.31 1.78 3 7 -28 27.61 2.86 -7 3 -28 23.69 2.14 -7 3 -28 25.94 3.07 7 -3 28 33.23 2.58 -7 3 28 26.90 2.48 -3 -7 28 32.76 2.72 -4 -7 -28 14.74 2.20 -7 4 -28 15.36 1.88 -7 4 -28 17.74 2.71 4 7 -28 13.33 2.34 -7 4 28 18.25 2.09 -4 -7 28 18.46 2.17 7 -4 28 16.07 1.87 -7 5 -28 9.59 1.75 -7 5 -28 8.44 2.28 -5 -7 -28 7.89 2.04 5 7 -28 9.48 2.15 -5 -7 28 5.81 1.85 -5 -7 28 8.21 2.48 -7 5 28 5.62 1.66 7 -5 28 10.44 1.73 -7 6 -28 38.82 3.13 6 7 -28 37.31 3.35 -7 6 -28 36.49 3.43 -6 -7 -28 33.40 3.25 -6 -7 28 45.62 4.22 7 -6 28 43.98 3.24 -7 6 28 44.55 3.34 -6 -7 28 35.78 3.08 -7 7 -28 5.79 2.14 -7 7 -28 6.24 1.75 7 7 -28 5.44 2.08 -7 -7 -28 6.82 2.15 7 -7 28 7.68 1.75 -7 -7 28 5.82 2.44 -7 7 28 6.74 1.89 -7 -7 28 2.90 1.74 -6 8 -28 3.35 1.68 8 6 -28 3.79 1.90 -8 -6 -28 2.00 2.08 -6 8 -28 6.19 2.12 -6 8 28 5.18 2.06 6 -8 28 6.12 1.68 -8 -6 28 1.90 2.15 -8 -6 28 4.34 1.92 -5 8 -28 30.34 3.16 -5 8 -28 24.70 2.47 8 5 -28 33.89 3.12 -8 -5 -28 31.36 3.26 -8 -5 28 32.13 3.03 -8 -5 28 38.80 3.51 5 -8 28 28.80 2.63 -4 8 -28 4.47 2.04 -4 8 -28 4.04 1.64 8 4 -28 5.66 1.82 -8 -4 -28 6.99 2.28 -8 -4 28 4.79 1.84 4 -8 28 9.20 1.76 -8 -4 28 6.55 2.09 -8 -3 -28 14.91 2.53 -3 8 -28 13.53 2.43 8 3 -28 13.74 2.11 -8 -3 28 12.22 2.22 3 -8 28 13.67 1.91 -8 -3 28 13.23 2.09 8 2 -28 4.75 1.64 -2 8 -28 7.54 2.08 -8 -2 -28 2.94 2.08 2 -8 28 8.55 1.67 -8 -2 28 8.74 1.98 -8 -2 28 7.12 1.87 8 1 -28 4.72 1.49 -8 -1 -28 3.12 2.07 -1 8 -28 3.86 1.95 -8 -1 28 2.45 1.55 1 -8 28 2.33 1.49 -8 0 -28 24.52 3.02 0 8 -28 31.23 3.14 -8 0 28 23.02 2.42 0 -8 28 29.79 2.53 1 8 -28 3.11 1.85 -8 1 -28 1.66 1.90 -8 1 28 1.46 1.47 -1 -8 28 2.07 1.48 2 8 -28 6.47 2.09 -8 2 -28 10.29 2.34 -8 2 -28 7.57 1.54 -8 2 28 2.56 1.56 -2 -8 28 5.37 1.61 8 -2 28 5.42 1.38 3 8 -28 16.44 2.50 -8 3 -28 15.30 1.86 -8 3 -28 11.39 2.55 8 -3 28 18.50 1.94 -3 -8 28 13.36 1.98 -8 3 28 13.00 2.04 4 8 -28 6.89 2.06 -8 4 -28 6.56 2.34 -8 4 -28 7.22 1.67 8 -4 28 8.75 1.64 -4 -8 28 7.38 1.81 -8 4 28 7.39 1.80 -8 5 -28 33.72 3.49 5 8 -28 30.79 3.11 -8 5 -28 26.91 2.50 -8 5 28 31.22 2.73 -5 -8 28 27.83 2.69 8 -5 28 33.62 2.66 -5 -8 28 31.63 3.61 -8 6 -28 6.62 1.72 -8 6 -28 4.50 2.25 -6 -8 -28 6.71 2.14 6 8 -28 3.40 2.01 -6 -8 28 2.55 2.28 -8 6 28 1.59 1.66 -6 -8 28 4.76 1.80 8 -6 28 0.37 1.45 -5 9 -28 2.87 1.79 -9 -5 -28 -4.55 2.03 -5 9 -28 0.54 1.87 9 5 -28 5.97 1.94 -9 -5 28 2.49 1.91 5 -9 28 6.27 1.92 -9 -5 28 6.23 2.32 9 4 -28 33.07 3.07 -4 9 -28 32.46 3.28 -4 9 -28 34.98 2.87 -9 -4 -28 30.69 3.40 -9 -4 28 33.11 3.08 -9 -4 28 28.88 3.12 4 -9 28 35.02 2.81 -9 -3 -28 8.20 2.46 -3 9 -28 2.68 1.59 9 3 -28 7.00 1.86 -3 9 -28 3.33 1.98 -9 -3 28 2.90 1.95 -9 -3 28 4.60 1.83 3 -9 28 4.73 1.64 -9 -2 -28 9.00 2.42 9 2 -28 10.98 1.97 -2 9 -28 8.42 2.23 2 -9 28 10.13 1.81 -9 -2 28 7.54 1.98 -9 -2 28 4.38 1.79 -1 9 -28 0.75 1.85 -9 -1 -28 2.81 2.18 1 -9 28 0.49 1.46 -9 -1 28 4.77 1.76 0 9 -28 6.73 2.09 -9 0 -28 0.89 2.08 -9 0 28 2.54 1.61 0 -9 28 -0.57 1.39 -9 1 -28 2.81 2.16 1 9 -28 0.01 1.80 -1 -9 28 3.87 1.63 -9 1 28 3.33 1.67 2 9 -28 8.85 2.28 -9 2 -28 7.18 2.36 -2 -9 28 7.72 1.77 -9 2 28 5.96 1.81 -9 3 -28 2.63 2.15 3 9 -28 3.59 1.95 -9 3 -28 4.44 1.59 -3 -9 28 3.98 1.71 -9 3 28 4.98 1.74 9 -3 28 5.96 1.50 -9 4 -28 27.62 2.52 -9 4 -28 29.45 3.27 4 9 -28 35.56 3.49 9 -4 28 35.22 2.71 -9 4 28 35.76 3.04 -4 -9 28 31.37 2.90 -4 -9 28 41.29 3.91 -9 5 -28 5.45 1.66 5 9 -28 6.83 2.40 -9 5 -28 1.80 2.15 -5 -9 28 4.32 2.72 -5 -9 28 4.77 1.84 9 -5 28 1.46 1.46 -9 5 28 2.75 1.75 -3 10 -28 6.21 2.19 10 3 -28 10.40 2.12 -10 -3 -28 8.51 3.24 -10 -3 28 6.03 2.24 -10 -3 28 10.28 2.27 -10 -2 -28 0.87 2.26 -2 10 -28 0.45 1.81 -2 10 -28 -1.22 1.49 2 -10 28 0.01 1.53 -10 -2 28 -2.40 1.65 -10 -1 -28 1.35 2.25 -1 10 -28 0.30 1.98 1 -10 28 0.81 1.59 -10 -1 28 4.06 1.81 -10 0 -28 2.83 2.18 0 10 -28 3.86 2.00 -10 0 28 2.11 1.69 0 -10 28 1.58 1.58 1 10 -28 1.51 1.91 -10 1 -28 2.92 2.28 -10 1 28 0.36 1.63 -1 -10 28 2.86 1.64 2 10 -28 0.37 2.00 -10 2 -28 -1.70 2.05 -10 2 28 2.09 1.78 -2 -10 28 0.26 1.59 -10 3 -28 4.44 2.52 -3 -10 28 10.19 2.03 -10 3 28 7.64 2.56 0 0 -29 -0.27 1.32 0 0 29 0.70 1.09 0 1 -29 3.02 1.48 -1 0 -29 3.07 1.53 0 -1 -29 4.27 1.54 1 0 -29 3.06 1.46 0 -1 29 3.68 1.24 1 0 29 2.68 1.10 -1 0 29 2.10 1.14 0 1 29 1.69 1.11 1 1 -29 8.33 1.66 -1 -1 -29 6.40 1.66 -1 1 -29 4.59 1.67 1 -1 -29 9.54 1.72 -1 -1 29 7.96 1.47 1 1 29 9.34 1.38 -1 1 29 9.34 1.45 1 -1 29 8.86 1.41 -1 2 -29 1.61 1.50 -2 -1 -29 -0.13 1.40 1 -2 -29 -0.84 1.24 2 1 -29 0.30 1.29 2 1 29 1.57 1.01 -1 2 29 1.53 1.11 -2 -1 29 1.49 1.22 1 -2 29 2.20 1.15 -2 0 -29 10.83 2.02 2 0 -29 13.43 1.91 0 -2 -29 15.09 1.97 0 2 -29 16.73 2.17 2 0 29 14.15 1.53 -2 0 29 17.94 1.82 0 2 29 13.55 1.53 0 -2 29 14.99 1.72 1 2 -29 2.01 1.43 -2 1 -29 -0.08 1.44 -1 -2 -29 -0.45 1.35 2 -1 -29 2.26 1.33 -1 -2 29 2.40 1.29 2 -1 29 1.15 1.12 -2 1 29 0.93 1.16 1 2 29 -1.39 0.96 2 -2 -29 23.76 2.25 -2 -2 -29 23.41 2.41 -2 2 -29 14.52 2.19 2 2 -29 16.09 2.08 2 2 29 21.41 1.72 -2 2 29 18.64 1.84 2 -2 29 16.82 1.77 -2 -2 29 17.44 1.89 -2 3 -29 31.50 2.96 2 -3 -29 31.05 2.63 -3 -2 -29 29.77 2.78 3 2 -29 28.98 2.67 -2 3 29 33.55 2.55 -3 -2 29 34.51 2.78 2 -3 29 37.29 2.74 -3 -1 -29 15.36 2.16 -1 3 -29 14.96 2.23 3 1 -29 12.76 1.89 1 -3 -29 15.53 1.97 3 1 29 9.53 1.35 -1 3 29 10.98 1.45 1 -3 29 11.11 1.59 -3 -1 29 12.20 1.71 -3 0 -29 12.39 2.08 0 3 -29 10.26 1.95 3 0 -29 10.43 1.76 0 -3 -29 11.73 1.84 0 -3 29 11.93 1.65 -3 0 29 11.83 1.67 3 0 29 10.98 1.42 0 3 29 12.09 1.44 -1 -3 -29 10.04 1.82 1 3 -29 9.83 1.86 3 -1 -29 9.71 1.68 -3 1 -29 9.46 1.92 1 3 29 14.48 1.50 -3 1 29 15.03 1.80 -1 -3 29 15.52 1.85 3 -1 29 14.97 1.62 3 -2 -29 34.07 2.75 2 3 -29 32.09 2.88 -2 -3 -29 33.79 2.89 -3 2 -29 33.76 3.08 -3 2 29 34.51 2.53 3 -2 29 34.58 2.55 -2 -3 29 32.19 2.72 -3 3 -29 27.13 2.84 -3 -3 -29 28.88 2.77 3 3 -29 36.67 3.03 3 -3 29 32.31 2.58 -3 -3 29 32.04 2.58 -3 3 29 29.20 2.43 -4 -3 -29 27.65 2.78 4 3 -29 31.91 2.91 -3 4 -29 26.83 2.89 -4 -3 29 25.25 2.36 -3 4 29 25.19 2.09 3 -4 29 25.24 2.20 -4 -2 -29 21.22 2.55 -2 4 -29 21.48 2.63 4 2 -29 23.90 2.36 2 -4 29 15.61 1.81 -4 -2 29 15.42 1.96 -2 4 29 18.58 1.79 4 1 -29 27.54 2.62 1 -4 -29 28.31 2.67 -4 -1 -29 31.80 2.99 -1 4 -29 26.85 2.77 -1 4 29 28.98 2.33 -4 -1 29 29.74 2.45 4 1 29 31.90 2.28 1 -4 29 32.10 2.48 0 -4 -29 12.67 1.86 0 4 -29 13.04 2.11 -4 0 -29 13.40 2.21 4 0 -29 7.29 1.60 0 4 29 10.90 1.84 4 0 29 13.95 1.54 0 -4 29 15.79 1.86 -4 0 29 13.91 1.79 4 -1 -29 28.93 2.54 -4 1 -29 29.22 2.85 -1 -4 -29 27.40 2.58 1 4 -29 28.53 2.82 4 -1 29 30.25 2.39 -1 -4 29 32.53 2.70 -4 1 29 30.98 2.56 -2 -4 -29 17.75 2.26 4 -2 -29 17.95 2.43 2 4 -29 16.19 2.23 -4 2 -29 14.90 2.34 4 -2 29 20.95 1.92 -2 -4 29 21.99 2.20 -4 2 29 20.93 2.01 -3 -4 -29 24.26 2.56 3 4 -29 26.25 2.71 -4 3 -29 27.63 2.85 -4 3 29 23.60 2.13 4 -3 29 25.85 2.13 -3 -4 29 27.49 2.40 -4 4 -29 23.52 2.76 4 4 -29 20.31 2.41 -4 -4 -29 20.90 2.44 4 -4 29 18.60 1.92 -4 4 29 22.59 2.06 -4 -4 29 16.78 2.08 -5 -4 -29 19.07 2.59 5 4 -29 18.78 2.34 -4 5 -29 17.53 2.49 -4 5 29 13.48 1.77 4 -5 29 20.99 2.10 -5 -4 29 14.87 2.10 -3 5 -29 23.13 2.74 -5 -3 -29 20.01 2.51 5 3 -29 21.79 2.39 3 -5 29 26.38 2.29 -3 5 29 28.84 2.26 -5 -3 29 33.15 2.67 5 2 -29 27.15 2.55 -5 -2 -29 29.26 2.90 -2 5 -29 24.97 2.78 2 -5 29 27.79 2.36 -5 -2 29 27.57 2.45 -2 5 29 34.99 2.49 -5 -1 -29 29.45 2.98 5 1 -29 28.33 2.61 -1 5 -29 25.59 2.74 -5 -1 29 28.36 2.45 1 -5 29 26.08 2.26 5 0 -29 9.62 1.70 -5 0 -29 8.08 2.12 0 5 -29 6.48 1.85 0 -5 29 7.87 1.59 -5 0 29 8.57 1.62 5 0 29 9.41 1.38 1 5 -29 29.29 2.79 -1 -5 -29 27.87 2.54 5 -1 -29 25.86 2.35 -5 1 -29 23.33 2.73 5 -1 29 26.36 2.07 -5 1 29 26.10 2.26 -1 -5 29 25.98 2.32 -5 2 -29 26.88 2.90 2 5 -29 28.31 2.85 -2 -5 -29 32.58 2.93 -2 -5 29 28.24 2.41 -5 2 29 29.03 2.42 5 -2 29 30.12 2.44 -5 3 -29 29.47 3.04 3 5 -29 25.18 2.72 -3 -5 -29 28.52 2.68 5 -3 29 22.93 2.04 -3 -5 29 18.97 2.11 -5 3 29 22.71 2.17 4 5 -29 21.27 2.53 -5 4 -29 14.71 2.41 -4 -5 -29 19.29 2.37 -5 4 -29 16.87 1.89 5 -4 29 19.15 1.97 -4 -5 29 21.97 2.32 -5 4 29 16.52 1.96 -5 5 -29 29.90 2.43 -5 5 -29 30.57 3.12 -5 -5 -29 28.53 2.94 5 5 -29 26.28 2.74 -5 -5 29 27.42 2.58 -5 5 29 31.76 2.47 5 -5 29 26.81 2.34 -6 -5 -29 18.84 2.61 -5 6 -29 16.13 2.54 6 5 -29 21.61 2.55 -5 6 -29 13.74 1.94 -6 -5 29 20.64 2.42 -5 6 29 22.86 2.16 5 -6 29 18.94 2.09 -6 -5 29 19.66 2.83 -6 -4 -29 24.09 2.75 6 4 -29 24.92 2.58 -4 6 -29 26.27 2.97 -4 6 29 30.94 2.43 4 -6 29 23.65 2.28 -6 -4 29 28.57 2.67 -6 -3 -29 28.84 2.97 6 3 -29 30.11 2.78 -3 6 -29 31.61 3.16 3 -6 29 28.30 2.39 -6 -3 29 23.57 2.43 -3 6 29 35.10 3.10 -6 -2 -29 31.91 3.19 -2 6 -29 36.10 3.28 6 2 -29 31.95 2.92 2 -6 29 28.93 2.48 -6 -2 29 35.44 2.80 -1 6 -29 26.08 2.83 6 1 -29 26.22 2.46 -6 -1 -29 25.43 2.91 1 -6 29 21.02 2.13 -6 -1 29 18.70 2.10 6 0 -29 54.00 3.39 -6 0 -29 60.86 4.26 0 6 -29 56.11 4.10 0 -6 29 56.83 3.55 -6 0 29 56.19 3.51 1 6 -29 22.93 2.80 -6 1 -29 23.68 2.88 -6 1 -29 24.20 2.01 -6 1 29 25.91 2.35 -1 -6 29 25.50 2.31 6 -1 29 26.61 2.09 -6 2 -29 30.69 3.30 -6 2 -29 32.37 2.53 2 6 -29 35.26 3.19 -6 2 29 38.32 2.94 6 -2 29 30.64 2.37 -2 -6 29 34.99 2.75 -6 3 -29 29.58 2.37 -6 3 -29 37.78 3.41 -3 -6 -29 27.35 2.70 3 6 -29 31.97 3.15 -6 3 29 34.56 2.86 -3 -6 29 32.31 2.69 6 -3 29 31.59 2.55 -6 4 -29 26.51 3.01 4 6 -29 29.81 2.94 -4 -6 -29 23.97 2.64 -6 4 -29 26.00 2.33 6 -4 29 30.16 2.41 -4 -6 29 29.82 2.69 -6 4 29 26.57 2.39 -5 -6 -29 16.52 2.43 5 6 -29 24.03 2.69 -6 5 -29 22.53 2.25 -6 5 -29 22.39 2.89 -5 -6 29 18.43 2.28 -6 5 29 19.87 2.10 6 -5 29 15.37 1.98 -6 6 -29 36.23 2.97 6 6 -29 31.99 3.13 -6 6 -29 38.84 3.55 -6 -6 -29 39.08 3.50 -6 -6 29 28.30 3.29 6 -6 29 31.43 2.58 -6 6 29 29.50 2.56 -6 -6 29 31.03 2.78 -6 7 -29 8.60 2.33 -6 7 -29 12.77 1.95 -7 -6 -29 11.01 2.44 7 6 -29 14.12 2.27 -6 7 29 15.50 2.03 6 -7 29 14.05 2.04 -7 -6 29 12.50 2.21 -7 -6 29 17.64 2.83 -5 7 -29 20.67 2.85 -5 7 -29 19.66 2.29 -7 -5 -29 20.28 2.86 7 5 -29 19.15 2.54 -7 -5 29 21.70 2.90 5 -7 29 22.04 2.31 -7 -5 29 22.88 2.57 -5 7 29 25.82 2.34 -4 7 -29 31.23 2.63 7 4 -29 27.45 2.76 -4 7 -29 27.67 3.07 -7 -4 -29 34.22 3.34 -7 -4 29 27.66 2.72 4 -7 29 31.31 2.60 -7 -4 29 25.69 3.02 -7 -3 -29 26.29 3.01 -3 7 -29 28.57 3.12 7 3 -29 27.03 2.65 -7 -3 29 22.25 2.46 3 -7 29 32.65 2.52 -7 -3 29 23.46 2.75 -7 -2 -29 56.56 4.28 -2 7 -29 60.53 4.25 7 2 -29 56.38 3.71 2 -7 29 61.35 3.68 -7 -2 29 50.94 3.62 -1 7 -29 40.47 3.66 7 1 -29 37.94 3.07 -7 -1 -29 33.77 3.42 1 -7 29 42.10 3.18 -7 -1 29 38.67 3.18 0 7 -29 30.83 3.08 -7 0 -29 30.57 3.26 -7 0 29 28.96 2.55 0 -7 29 27.63 2.40 -7 1 -29 45.84 4.06 1 7 -29 44.27 3.74 -7 1 29 38.45 3.07 -1 -7 29 38.31 3.07 2 7 -29 50.35 3.90 -7 2 -29 56.82 3.23 -7 2 -29 53.49 4.23 7 -2 29 57.41 3.30 -7 2 29 54.62 3.59 -2 -7 29 58.32 3.63 -7 3 -29 29.24 2.38 -7 3 -29 27.99 3.20 3 7 -29 27.54 2.97 -3 -7 29 22.50 2.42 -7 3 29 26.47 2.40 7 -3 29 29.22 2.31 4 7 -29 34.19 3.21 -4 -7 -29 24.64 2.82 -7 4 -29 26.88 2.46 -7 4 -29 27.22 3.14 -4 -7 29 35.92 2.91 7 -4 29 31.20 2.55 -7 4 29 30.88 2.71 -5 -7 -29 22.74 2.72 5 7 -29 23.31 2.82 -7 5 -29 22.23 2.88 -7 5 -29 22.93 2.28 7 -5 29 20.11 2.10 -5 -7 29 18.47 2.93 -5 -7 29 20.30 2.47 -7 5 29 22.09 2.29 6 7 -29 19.39 2.68 -7 6 -29 15.99 2.12 -7 6 -29 16.47 2.74 -6 -7 -29 14.08 2.55 -6 -7 29 10.92 2.66 -7 6 29 14.21 2.09 7 -6 29 13.04 1.96 -6 -7 29 15.07 2.29 7 7 -29 8.31 2.23 -7 7 -29 15.33 2.67 -7 7 -29 8.57 1.91 -7 -7 -29 12.25 2.50 -7 -7 29 12.45 2.28 7 -7 29 7.25 1.82 -7 7 29 9.69 1.99 -7 -7 29 9.70 2.61 -5 8 -29 16.01 2.63 -8 -5 -29 23.69 3.03 -5 8 -29 21.95 2.36 8 5 -29 24.18 2.71 -8 -5 29 21.94 2.68 5 -8 29 26.33 2.46 -8 -5 29 22.95 2.96 -8 -4 -29 13.96 2.61 -4 8 -29 14.24 2.57 8 4 -29 13.16 2.22 -4 8 -29 13.94 2.02 -8 -4 29 22.16 2.68 4 -8 29 17.67 2.21 -8 -4 29 22.37 2.85 -3 8 -29 43.72 3.89 8 3 -29 39.28 3.30 -8 -3 -29 44.28 4.09 3 -8 29 43.18 3.24 -8 -3 29 41.84 3.68 -8 -3 29 44.84 3.42 -2 8 -29 28.95 3.12 -8 -2 -29 27.58 3.19 8 2 -29 23.43 2.51 -8 -2 29 21.74 2.45 -8 -2 29 23.34 2.70 2 -8 29 26.06 2.46 -1 8 -29 32.53 3.28 -8 -1 -29 25.92 3.20 8 1 -29 31.80 3.63 -8 -1 29 27.13 2.63 1 -8 29 26.66 2.47 -8 0 -29 25.40 3.07 0 8 -29 28.15 3.00 0 -8 29 26.61 2.50 -8 0 29 34.20 2.85 -8 1 -29 27.42 3.25 1 8 -29 30.65 3.21 -8 1 29 23.91 2.43 -1 -8 29 21.23 2.25 -8 2 -29 29.54 2.68 2 8 -29 31.14 3.21 -8 2 -29 28.23 3.17 -2 -8 29 22.98 2.39 -8 2 29 22.58 2.38 -8 3 -29 40.64 3.81 -8 3 -29 43.18 3.03 3 8 -29 42.49 3.91 8 -3 29 40.61 2.97 -3 -8 29 39.29 3.27 -8 3 29 43.15 3.31 -8 4 -29 21.69 2.20 -8 4 -29 19.94 3.01 4 8 -29 19.01 2.68 8 -4 29 13.30 1.84 -8 4 29 15.57 2.15 -4 -8 29 11.34 2.03 -8 5 -29 26.04 2.46 5 8 -29 26.35 3.06 -8 5 -29 27.45 3.24 -8 5 29 20.75 2.42 8 -5 29 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89.40 4.52 2 -3 30 103.85 4.76 -3 -2 30 94.70 4.84 -2 3 30 103.83 4.67 3 1 -30 2.24 1.43 1 -3 -30 3.68 1.54 -3 -1 -30 2.66 1.67 -1 3 -30 6.50 1.88 -3 -1 30 5.20 1.48 3 1 30 3.71 1.14 1 -3 30 5.36 1.40 -1 3 30 2.60 1.21 -3 0 -30 108.75 5.42 0 -3 -30 99.16 5.06 0 3 -30 108.91 5.45 3 0 -30 97.78 4.97 0 3 30 109.19 4.74 -3 0 30 102.83 4.97 3 0 30 105.32 4.73 0 -3 30 109.78 4.99 -3 1 -30 5.18 1.84 -1 -3 -30 3.65 1.58 1 3 -30 2.78 1.61 3 -1 -30 2.39 1.37 -1 -3 30 6.56 1.49 1 3 30 3.81 1.51 -3 1 30 5.92 1.47 3 -1 30 4.42 1.26 -2 -3 -30 100.18 4.98 -3 2 -30 89.82 5.04 3 -2 -30 90.31 4.63 2 3 -30 96.07 5.03 -2 -3 30 87.40 4.47 3 -2 30 85.63 4.19 -3 2 30 92.32 4.33 3 3 -30 1.23 1.47 -3 -3 -30 0.51 1.62 -3 3 -30 2.16 1.73 -3 -3 30 0.53 1.36 3 -3 30 1.06 1.23 -3 3 30 2.41 1.26 -4 -3 -30 51.30 3.82 -3 4 -30 48.52 4.03 4 3 -30 62.65 3.78 -3 4 30 48.34 3.13 -4 -3 30 50.76 3.53 3 -4 30 57.54 3.38 -4 -2 -30 2.58 1.73 4 2 -30 4.12 1.57 -2 4 -30 0.72 1.71 -4 -2 30 6.47 1.62 -2 4 30 6.79 1.41 2 -4 30 6.08 1.48 4 1 -30 62.84 3.83 -4 -1 -30 69.17 4.32 -1 4 -30 65.71 4.30 -4 -1 30 88.37 4.50 -1 4 30 87.57 4.17 1 -4 30 92.98 4.47 -4 0 -30 0.06 1.70 0 -4 -30 1.54 1.45 0 4 -30 2.02 1.66 4 0 -30 2.18 1.38 4 0 30 -0.46 1.07 0 -4 30 0.71 1.28 -4 0 30 1.90 1.33 -4 1 -30 78.63 4.87 -1 -4 -30 81.57 4.47 4 -1 -30 87.76 4.37 1 4 -30 85.42 4.80 -1 -4 30 65.27 3.87 4 -1 30 71.65 3.58 -4 1 30 68.56 3.73 -2 -4 -30 7.83 1.86 2 4 -30 5.46 1.81 -4 2 -30 2.85 1.88 -4 2 30 3.03 1.37 4 -2 30 1.85 1.20 -2 -4 30 0.55 1.37 -4 3 -30 58.07 4.09 3 4 -30 54.64 3.78 -3 -4 -30 44.36 3.64 -3 -4 30 49.11 3.41 -4 3 30 52.17 3.19 4 -3 30 55.77 3.26 -4 -4 -30 2.56 1.70 4 4 -30 3.28 1.63 -4 4 -30 4.28 1.93 -4 4 30 2.05 1.31 -4 -4 30 2.97 1.49 4 -4 30 3.62 1.36 -4 5 -30 29.33 3.13 5 4 -30 26.45 2.74 -5 -4 -30 31.98 3.10 4 -5 30 35.70 2.67 -5 -4 30 30.38 2.67 -4 5 30 27.81 2.38 -3 5 -30 5.58 2.03 -5 -3 -30 4.63 1.89 5 3 -30 5.65 1.69 3 -5 30 10.48 1.73 -5 -3 30 11.12 1.89 -3 5 30 10.95 1.62 5 2 -30 46.15 3.39 -2 5 -30 45.52 3.85 -5 -2 -30 46.57 3.79 2 -5 30 45.12 3.14 -2 5 30 44.48 3.23 -5 -2 30 45.17 3.25 5 1 -30 4.95 1.56 -5 -1 -30 3.54 1.89 -1 5 -30 5.09 1.88 -5 -1 30 6.50 1.62 1 -5 30 4.33 1.43 0 5 -30 63.73 4.29 5 0 -30 63.01 3.74 -5 0 -30 65.71 4.43 5 0 30 62.79 3.55 -5 0 30 58.80 3.66 0 -5 30 70.76 3.85 -5 1 -30 6.50 2.07 5 -1 -30 6.48 2.33 -1 -5 -30 5.79 1.90 1 5 -30 7.76 1.98 -5 1 30 4.47 1.51 -1 -5 30 6.03 1.61 5 -1 30 4.44 1.30 -2 -5 -30 45.16 3.28 2 5 -30 49.58 3.73 -5 2 -30 42.05 3.81 5 -2 30 48.73 3.00 -2 -5 30 46.15 3.30 -5 2 30 44.44 3.22 -5 3 -30 8.84 2.24 -3 -5 -30 9.21 1.96 3 5 -30 11.22 2.12 5 -3 30 3.47 1.34 -5 3 30 7.32 1.59 -3 -5 30 5.22 1.66 -4 -5 -30 25.94 2.78 -5 4 -30 32.22 2.46 -5 4 -30 25.96 2.95 4 5 -30 28.95 2.96 -5 4 30 27.08 2.38 -4 -5 30 31.73 2.64 5 -4 30 28.55 2.38 -5 -5 -30 24.89 2.81 -5 5 -30 20.39 2.18 -5 5 -30 20.29 2.79 5 5 -30 20.94 2.59 5 -5 30 17.13 1.99 -5 -5 30 23.95 2.41 -5 5 30 19.46 2.11 6 5 -30 20.72 2.52 -6 -5 -30 22.94 2.87 -5 6 -30 20.65 2.83 -5 6 -30 21.93 2.27 5 -6 30 20.38 2.22 -6 -5 30 23.18 2.56 -5 6 30 24.77 2.31 -6 -4 -30 16.24 2.49 6 4 -30 17.84 2.34 -4 6 -30 16.47 2.61 4 -6 30 14.41 1.97 -6 -4 30 19.38 2.35 -4 6 30 17.87 1.98 -3 6 -30 21.20 2.78 6 3 -30 22.34 2.51 -6 -3 -30 18.84 2.66 -6 -3 30 16.78 2.17 3 -6 30 20.99 2.20 -6 -2 -30 6.53 2.09 6 2 -30 3.64 1.64 -2 6 -30 7.35 2.11 2 -6 30 11.13 1.78 -6 -2 30 11.23 1.95 6 1 -30 25.97 2.48 -6 -1 -30 25.58 2.95 -1 6 -30 23.62 2.84 1 -6 30 31.35 2.62 -6 -1 30 27.19 2.59 6 0 -30 7.98 1.64 -6 0 -30 5.71 2.13 0 6 -30 7.86 2.13 0 -6 30 6.98 1.65 -6 0 30 7.34 1.70 1 6 -30 27.01 2.92 -6 1 -30 28.42 2.22 -6 1 -30 31.09 3.22 6 -1 30 24.33 2.04 -1 -6 30 22.12 2.25 -6 1 30 22.38 2.26 -6 2 -30 8.45 2.32 -6 2 -30 10.30 1.61 2 6 -30 8.69 2.09 -6 2 30 5.65 1.62 6 -2 30 9.25 1.54 -2 -6 30 8.23 1.72 -3 -6 -30 19.97 2.45 3 6 -30 23.47 2.73 -6 3 -30 19.53 2.05 -6 3 -30 16.39 2.60 -6 3 30 25.02 2.34 -3 -6 30 19.79 2.31 6 -3 30 25.06 2.18 -6 4 -30 14.96 2.67 -6 4 -30 18.17 2.05 4 6 -30 14.55 2.42 -4 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2 -4 31 29.01 2.45 -4 -2 31 30.06 2.65 -1 4 -31 11.32 2.23 4 1 -31 8.40 1.76 -4 -1 -31 9.57 2.17 -4 -1 31 6.31 1.63 1 -4 31 6.05 1.54 -1 4 31 7.81 1.53 0 4 -31 13.67 2.26 0 -4 -31 8.85 1.83 -4 0 -31 9.46 2.26 4 0 -31 7.98 1.74 0 -4 31 9.13 1.67 4 0 31 9.54 1.49 -4 0 31 8.54 1.67 4 -1 -31 7.47 1.67 1 4 -31 6.03 1.89 -4 1 -31 4.91 1.99 -1 -4 -31 7.81 1.82 -1 -4 31 9.62 1.71 4 -1 31 8.77 1.48 -4 1 31 10.66 1.73 -2 -4 -31 28.40 2.81 2 4 -31 23.58 2.66 -4 2 -31 28.00 2.92 -2 -4 31 31.52 2.61 4 -2 31 27.30 2.29 -4 2 31 25.34 2.29 -3 -4 -31 19.57 2.52 -4 3 -31 26.51 2.97 3 4 -31 26.22 2.75 4 -3 31 20.74 2.04 -4 3 31 22.39 2.13 -3 -4 31 23.30 2.41 -4 -4 -31 23.81 2.73 -4 4 -31 26.10 2.91 4 4 -31 23.88 2.60 4 -4 31 31.42 2.46 -4 4 31 24.77 2.29 -4 -4 31 26.79 2.53 5 4 -31 16.92 2.39 -5 -4 -31 17.87 2.58 -4 5 -31 17.32 2.66 4 -5 31 17.97 2.08 -5 -4 31 17.85 2.23 -4 5 31 19.19 2.04 -5 -3 -31 20.52 2.72 5 3 -31 22.41 2.53 -3 5 -31 22.84 2.89 3 -5 31 22.24 2.25 -5 -3 31 27.31 2.58 -3 5 31 25.84 2.25 5 2 -31 21.92 2.37 -5 -2 -31 19.91 2.71 -2 5 -31 16.17 2.63 -5 -2 31 16.97 2.15 2 -5 31 15.77 1.99 -5 -1 -31 16.52 2.61 5 1 -31 15.50 2.11 -1 5 -31 13.73 2.40 1 -5 31 21.10 2.18 -5 -1 31 20.63 2.27 0 5 -31 32.47 3.19 5 0 -31 34.03 2.96 -5 0 -31 32.61 3.29 -5 0 31 29.96 2.59 0 -5 31 38.54 3.06 -5 1 -31 19.67 2.77 1 5 -31 14.38 2.40 -1 -5 31 15.67 1.99 -5 1 31 15.08 1.98 5 -1 31 16.98 1.85 -5 2 -31 13.79 2.48 -2 -5 -31 15.61 2.20 2 5 -31 19.65 2.52 -5 2 31 21.17 2.20 -2 -5 31 17.91 2.13 5 -2 31 16.52 1.87 3 5 -31 30.37 3.00 -3 -5 -31 25.84 2.82 -5 3 -31 26.32 3.05 5 -3 31 20.75 2.06 -3 -5 31 24.33 2.40 -5 3 31 19.89 2.16 -5 4 -31 21.99 2.21 -4 -5 -31 18.32 2.53 4 5 -31 21.19 2.63 -5 4 -31 20.02 2.79 5 -4 31 19.60 2.12 -4 -5 31 21.73 2.40 -5 4 31 18.94 2.19 -5 5 -31 17.48 2.72 -5 -5 -31 18.17 2.70 5 5 -31 22.29 2.73 -5 5 -31 24.31 2.34 -5 -5 31 23.73 2.57 -5 5 31 22.29 2.27 5 -5 31 21.74 2.25 -6 -5 -31 21.67 2.85 -5 6 -31 20.75 2.27 6 5 -31 21.32 2.60 -5 6 -31 21.84 2.91 5 -6 31 23.20 2.35 -6 -5 31 23.80 2.68 -5 6 31 28.81 2.51 -4 6 -31 9.64 2.36 -6 -4 -31 9.79 2.29 6 4 -31 17.29 2.38 -6 -4 31 10.73 2.08 -4 6 31 10.18 3.02 4 -6 31 9.10 1.78 6 3 -31 30.98 2.89 -3 6 -31 27.74 3.10 -6 -3 -31 36.64 3.39 3 -6 31 32.68 2.72 -6 -3 31 35.39 2.94 -2 6 -31 27.30 3.06 -6 -2 -31 27.36 3.06 6 2 -31 27.78 2.67 -6 -2 31 28.78 2.66 2 -6 31 29.63 2.58 -1 6 -31 41.93 3.76 -6 -1 -31 28.89 3.17 6 1 -31 35.03 3.05 -6 -1 31 31.35 2.68 1 -6 31 31.43 2.61 -6 0 -31 8.54 2.42 0 6 -31 8.63 2.21 -6 0 31 7.74 1.77 0 -6 31 7.87 1.78 1 6 -31 41.35 3.63 -6 1 -31 32.49 2.76 -6 1 -31 43.42 3.86 -6 1 31 33.65 2.74 -1 -6 31 33.23 2.71 2 6 -31 30.93 3.16 -6 2 -31 29.04 2.37 -6 2 -31 28.59 3.18 -2 -6 31 30.90 2.66 -6 2 31 27.58 2.47 6 -2 31 30.15 2.36 3 6 -31 32.11 3.16 -6 3 -31 27.33 3.18 -6 3 -31 32.36 2.55 -3 -6 31 35.45 2.96 -6 3 31 34.21 2.79 6 -3 31 34.62 2.83 -4 -6 -31 10.78 2.22 -6 4 -31 9.24 1.77 4 6 -31 11.16 2.31 -6 4 -31 12.44 2.56 -4 -6 31 14.48 2.17 -6 4 31 13.39 2.00 6 -4 31 13.72 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2.15 5 4 -33 13.49 2.28 -5 -4 -33 8.90 2.38 -4 5 -33 12.68 2.62 -5 -4 33 15.03 2.25 4 -5 33 14.78 2.08 -4 5 33 14.69 2.02 -3 5 -33 16.07 2.65 -5 -3 -33 16.60 2.60 5 3 -33 17.04 2.37 3 -5 33 16.74 2.08 -5 -3 33 16.97 2.28 -2 5 -33 24.27 3.09 5 2 -33 24.24 2.64 -5 -2 -33 20.25 2.86 -5 -2 33 25.26 2.52 2 -5 33 24.67 2.45 -5 -1 -33 23.50 3.00 -1 5 -33 25.02 3.01 5 1 -33 26.61 2.67 -5 -1 33 23.64 2.48 1 -5 33 22.00 2.36 5 0 -33 6.77 2.21 0 5 -33 3.00 2.01 -5 0 -33 4.11 2.23 0 -5 33 4.34 1.72 -5 0 33 5.73 1.75 -5 1 -33 30.05 3.37 1 5 -33 26.51 3.03 -1 -5 33 29.15 2.69 -5 1 33 28.34 2.56 5 -1 33 23.88 3.40 -5 2 -33 23.41 2.97 2 5 -33 24.71 2.98 5 -2 33 28.38 2.34 -5 2 33 22.72 2.44 -2 -5 33 29.12 2.69 -5 3 -33 11.43 2.58 -3 -5 -33 17.69 2.54 3 5 -33 15.06 2.43 -5 3 33 16.92 2.13 -3 -5 33 16.28 2.25 5 -3 33 15.88 1.96 -5 4 -33 14.05 1.97 -5 4 -33 14.72 2.75 4 5 -33 14.12 2.41 -4 -5 -33 12.46 2.40 5 -4 33 11.01 1.85 -5 4 33 10.00 1.90 -4 -5 33 12.24 2.17 -3 6 -33 17.62 3.52 6 3 -33 11.46 2.18 -6 -3 -33 11.25 2.53 3 -6 33 11.21 2.03 -6 -3 33 13.61 2.81 -6 -2 -33 22.80 2.93 6 2 -33 24.10 2.68 -2 6 -33 17.34 2.86 2 -6 33 21.56 2.35 -6 -2 33 19.11 2.38 -6 -1 -33 16.00 2.81 6 1 -33 19.68 2.39 -1 6 -33 19.97 2.89 1 -6 33 16.17 2.12 -6 -1 33 11.13 2.02 0 6 -33 40.62 3.75 -6 0 -33 43.10 3.94 0 -6 33 38.87 3.24 -6 0 33 39.62 3.14 -6 1 -33 18.49 2.94 1 6 -33 21.21 2.94 -1 -6 33 15.83 2.17 -6 1 33 15.44 2.17 2 6 -33 22.15 2.81 -6 2 -33 23.18 2.28 -6 2 -33 22.53 3.24 -6 2 33 16.61 2.25 6 -2 33 21.03 2.22 -2 -6 33 19.96 2.35 -6 3 -33 14.08 2.01 -6 3 -33 21.43 3.99 3 6 -33 12.12 2.50 -6 3 33 16.32 2.20 6 -3 33 13.46 1.95 -3 -6 33 15.46 3.28 0 0 -34 -1.16 1.51 0 0 34 -1.78 1.18 0 1 -34 56.49 4.06 -1 0 -34 57.43 4.08 1 0 -34 58.41 4.09 0 -1 -34 59.57 4.07 -1 0 34 60.13 3.65 0 -1 34 58.91 3.55 0 1 34 60.45 3.52 1 0 34 58.23 3.42 1 -1 -34 1.82 1.62 -1 1 -34 2.52 1.83 1 1 -34 2.67 1.76 -1 -1 -34 0.45 1.77 -1 1 34 1.52 1.31 -1 -1 34 1.76 1.41 1 1 34 2.95 1.30 1 -1 34 2.75 1.36 -1 2 -34 39.45 3.56 2 1 -34 46.31 3.68 -2 -1 -34 44.82 3.74 1 -2 -34 49.11 3.59 1 -2 34 45.54 3.32 -2 -1 34 50.07 3.38 -1 2 34 51.09 3.15 2 0 -34 0.39 1.56 0 -2 -34 -1.04 1.58 -2 0 -34 0.19 1.78 0 2 -34 0.05 1.69 0 2 34 1.61 1.30 0 -2 34 1.51 1.37 2 0 34 -0.27 1.26 -2 0 34 2.02 1.39 -1 -2 -34 47.42 3.71 -2 1 -34 47.48 3.91 2 -1 -34 49.31 3.66 1 2 -34 47.82 3.79 2 -1 34 42.95 3.09 -1 -2 34 42.24 3.24 -2 1 34 48.45 3.22 -2 -2 -34 0.52 1.73 -2 2 -34 -1.02 1.73 2 2 -34 -1.43 1.56 -2 2 34 -2.37 1.22 -2 -2 34 2.12 1.53 2 -2 34 0.28 1.29 -2 3 -34 62.74 4.56 -3 -2 -34 61.27 4.38 3 2 -34 65.75 4.21 -3 -2 34 72.60 4.14 -2 3 34 71.37 3.89 2 -3 34 62.91 3.90 -1 3 -34 2.95 1.94 3 1 -34 4.85 1.80 -3 -1 -34 5.29 2.04 -1 3 34 2.91 1.69 1 -3 34 1.74 1.45 -3 -1 34 3.73 1.59 3 0 -34 44.78 3.50 0 3 -34 51.15 3.98 -3 0 -34 52.05 4.05 0 -3 -34 46.96 3.64 -3 0 34 55.95 3.56 0 -3 34 57.70 3.68 3 0 34 53.21 3.40 -1 -3 -34 3.52 1.87 -3 1 -34 4.69 2.09 3 -1 -34 2.17 1.61 1 3 -34 3.24 1.90 3 -1 34 4.15 1.46 -1 -3 34 5.11 1.62 -3 1 34 4.49 1.59 2 3 -34 64.50 4.38 -2 -3 -34 70.67 4.48 -3 2 -34 64.08 4.63 3 -2 34 63.94 3.80 -3 2 34 65.78 3.83 -2 -3 34 71.12 4.16 -3 3 -34 5.32 2.18 3 3 -34 1.79 1.76 -3 -3 -34 1.33 1.92 -3 3 34 0.57 1.40 3 -3 34 1.77 1.42 -3 -3 34 2.14 1.61 4 3 -34 40.92 3.60 -3 4 -34 41.89 3.86 -4 -3 -34 42.35 3.75 3 -4 34 39.79 3.21 -3 4 34 36.24 3.01 -4 -3 34 31.52 2.86 4 2 -34 2.51 1.65 -4 -2 -34 1.83 1.94 -2 4 -34 0.09 2.02 2 -4 34 2.11 1.52 -4 -2 34 0.64 1.57 -1 4 -34 37.42 3.59 4 1 -34 42.74 3.37 -4 -1 -34 36.46 3.53 -4 -1 34 45.87 3.55 1 -4 34 42.89 3.37 0 4 -34 -1.91 1.78 -4 0 -34 -0.50 2.01 4 0 -34 -0.13 1.49 0 -4 34 -0.90 1.42 -4 0 34 -2.11 1.42 -4 1 -34 56.29 4.29 1 4 -34 41.78 3.95 4 -1 34 41.84 3.01 -4 1 34 46.89 3.39 -1 -4 34 42.66 3.35 -4 2 -34 4.00 2.21 -2 -4 -34 0.09 1.75 2 4 -34 3.10 1.92 -4 2 34 3.89 1.67 -2 -4 34 1.98 1.61 4 -2 34 1.63 1.35 3 4 -34 33.99 3.34 -3 -4 -34 31.16 3.19 -4 3 -34 42.91 3.83 -4 3 34 46.60 3.25 -3 -4 34 42.69 3.31 4 -3 34 40.57 3.22 -4 4 -34 12.28 3.89 -4 -4 -34 9.71 2.32 4 4 -34 9.23 2.14 -4 4 34 10.41 1.92 4 -4 34 12.27 1.93 -4 -4 34 7.56 2.50 5 3 -34 2.55 1.75 -5 -3 -34 4.42 2.08 3 -5 34 2.11 1.59 -2 5 -34 33.38 3.64 5 2 -34 32.72 3.01 -5 -2 -34 28.45 3.27 2 -5 34 27.99 2.56 -5 -2 34 28.88 2.75 -1 5 -34 -0.64 1.92 5 1 -34 0.71 1.57 -5 -1 -34 1.42 2.07 -5 -1 34 3.17 1.77 1 -5 34 3.14 1.72 -5 0 -34 24.09 3.19 0 5 -34 14.70 2.67 0 -5 34 13.11 2.04 -5 0 34 15.67 2.18 1 5 -34 -0.07 1.92 -5 1 -34 2.41 2.23 -5 1 34 2.49 1.71 -1 -5 34 -0.44 1.48 -5 2 -34 30.14 3.39 2 5 -34 26.46 3.05 -5 2 34 31.45 2.82 -2 -5 34 31.92 2.85 5 -2 34 34.69 2.86 -3 -5 -34 3.65 2.86 -5 3 -34 5.33 1.69 3 5 -34 1.21 1.86 5 -3 34 3.24 1.49 -5 3 34 2.77 1.61 0 0 -35 -1.22 1.65 0 0 35 -1.60 1.25 -1 0 -35 -2.09 1.62 0 -1 -35 1.56 1.72 1 0 -35 -0.46 1.69 0 1 -35 2.93 1.86 0 1 35 0.69 1.30 -1 0 35 0.72 1.41 1 0 35 0.80 1.32 0 -1 35 0.52 1.32 -1 -1 -35 2.30 1.83 1 -1 -35 -0.19 1.63 -1 1 -35 0.88 1.83 1 1 -35 -1.43 1.68 -1 1 35 2.37 1.46 1 -1 35 0.63 1.38 1 1 35 3.92 1.39 -1 -1 35 2.61 1.46 -2 -1 -35 5.54 2.04 1 -2 -35 5.66 1.92 -1 2 -35 4.83 2.14 2 1 -35 8.75 2.02 1 -2 35 7.71 1.70 -1 2 35 5.28 1.48 -2 -1 35 5.27 1.71 0 -2 -35 2.46 1.79 -2 0 -35 2.32 1.95 2 0 -35 2.25 1.70 0 2 -35 7.05 2.04 2 0 35 4.03 1.40 0 2 35 3.05 2.21 0 -2 35 4.25 1.54 -2 0 35 3.53 1.53 -1 -2 -35 4.52 2.00 -2 1 -35 4.19 2.09 2 -1 -35 6.42 1.91 1 2 -35 3.20 1.89 2 -1 35 7.72 1.62 -2 1 35 9.59 1.77 -1 -2 35 4.85 1.72 2 2 -35 8.53 2.10 -2 2 -35 7.31 2.26 -2 -2 -35 6.61 2.16 -2 2 35 7.82 1.76 2 -2 35 8.90 1.69 -2 -2 35 9.94 1.92 -2 3 -35 1.50 2.05 -3 -2 -35 2.52 2.02 3 2 -35 1.98 1.75 2 -3 35 2.43 1.50 -3 -2 35 2.05 1.65 -2 3 35 1.63 1.40 -1 3 -35 15.17 2.69 -3 -1 -35 15.16 2.61 3 1 -35 9.46 2.12 1 -3 35 12.30 1.91 -3 -1 35 12.64 2.03 3 0 -35 1.93 1.63 0 3 -35 1.86 1.94 -3 0 -35 4.32 2.04 -3 0 35 0.08 1.42 0 -3 35 2.37 1.54 -3 1 -35 14.12 2.56 1 3 -35 10.66 2.39 -1 -3 -35 7.82 2.14 -1 -3 35 10.70 1.93 3 -1 35 14.13 1.84 -3 1 35 10.40 1.87 -2 -3 -35 0.23 1.82 -3 2 -35 1.21 2.04 2 3 -35 -0.35 1.77 -3 2 35 1.45 1.55 -2 -3 35 1.85 1.64 3 -2 35 0.78 1.40 -3 3 -35 3.78 2.32 3 3 -35 7.59 2.12 -3 -3 -35 5.55 2.14 -3 3 35 6.67 1.72 3 -3 35 3.90 1.62 -3 -3 35 6.94 1.89 4 2 -35 12.16 2.24 -4 -2 -35 12.30 2.51 -2 4 -35 7.67 3.62 -4 -2 35 11.64 2.11 2 -4 35 14.97 2.07 -1 4 -35 4.15 2.18 -4 -1 -35 4.72 2.25 4 1 -35 3.88 1.83 -4 -1 35 3.59 1.66 1 -4 35 2.70 1.48 -4 0 -35 6.39 2.40 0 4 -35 3.61 2.15 4 0 -35 7.22 2.09 -4 0 35 6.49 1.78 0 -4 35 2.76 1.60 -4 1 -35 4.96 2.28 1 4 -35 3.57 2.08 -4 1 35 6.36 1.80 -1 -4 35 6.33 1.82 4 -1 35 0.82 2.12 2 4 -35 14.40 2.53 -4 2 -35 9.12 2.79 -2 -4 -35 12.54 2.53 4 -2 35 14.18 1.94 -4 2 35 9.44 1.90 -2 -4 35 12.52 2.24 0 0 -36 62.67 4.32 0 0 36 67.87 3.94 0 1 -36 0.46 1.83 1 0 -36 -0.88 1.66 -1 0 -36 0.62 1.86 0 -1 -36 -1.37 1.72 0 1 36 -1.48 1.28 0 -1 36 -0.20 1.41 1 0 36 -0.71 1.36 -1 0 36 -2.21 1.32 -1 -1 -36 46.00 4.03 1 1 -36 47.73 3.91 1 -1 -36 43.88 3.66 -1 1 -36 45.78 4.00 -1 -1 36 44.64 3.41 -1 1 36 44.63 3.31 1 -1 36 47.21 3.33 -2 -1 -36 -0.86 1.84 -1 2 -36 2.11 1.99 2 1 -36 0.76 1.77 1 -2 36 -0.80 1.43 -2 -1 36 1.42 1.62 -1 2 36 3.80 1.48 0 2 -36 47.07 4.03 2 0 -36 43.72 3.79 0 -2 -36 47.90 3.87 -2 0 -36 42.44 4.00 2 0 36 44.72 3.23 -2 0 36 48.56 3.36 0 -2 36 45.55 3.37 -1 -2 -36 2.52 1.89 2 -1 -36 -0.99 1.65 -2 1 -36 1.36 2.04 1 2 -36 2.50 1.96 -1 -2 36 4.73 1.75 2 -1 36 -0.86 1.28 -2 1 36 1.92 1.54 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 40288 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y+1/2, x+1/2, z+3/4' '-x, -y, z+1/2' 'y+1/2, -x+1/2, z+1/4' 'x+1/2, -y+1/2, -z+1/4' '-x+1/2, y+1/2, -z+3/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Th1 Th 0.52316(2) 0.47684(2) 0.2500 0.01350(5) Uani 1 2 d S T P . . P1 P 0.29194(7) 0.47217(9) 0.25929(3) 0.02120(18) Uani 1 1 d . . . . . Si1 Si 0.17947(9) 0.57259(10) 0.30612(4) 0.0243(2) Uani 1 1 d . . . . . C1 C 0.5320(3) 0.4429(3) 0.35250(11) 0.0206(7) Uani 1 1 d . . . . . C2 C 0.5922(3) 0.3547(3) 0.33105(14) 0.0248(8) Uani 1 1 d . . . . . C3 C 0.6912(3) 0.3982(4) 0.31182(14) 0.0274(9) Uani 1 1 d . . . . . C4 C 0.6915(3) 0.5132(4) 0.32027(13) 0.0238(8) Uani 1 1 d . . . . . C5 C 0.5934(3) 0.5408(3) 0.34631(11) 0.0196(8) Uani 1 1 d . . . . . C6 C 0.4301(3) 0.4300(3) 0.38383(12) 0.0282(8) Uani 1 1 d . . . . . H6A H 0.4499 0.3972 0.4158 0.042 Uiso 1 1 calc R U . . . H6B H 0.3776 0.3821 0.3667 0.042 Uiso 1 1 calc R U . . . H6C H 0.3966 0.5022 0.3894 0.042 Uiso 1 1 calc R U . . . C7 C 0.5567(4) 0.2365(3) 0.33389(17) 0.0379(11) Uani 1 1 d . . . . . H7A H 0.6126 0.1898 0.3184 0.057 Uiso 1 1 calc R U . . . H7B H 0.4866 0.2274 0.3164 0.057 Uiso 1 1 calc R U . . . H7C H 0.5477 0.2152 0.3687 0.057 Uiso 1 1 calc R U . . . C8 C 0.7929(4) 0.3356(4) 0.29598(18) 0.0406(12) Uani 1 1 d . . . . . H8A H 0.8514 0.3469 0.3204 0.061 Uiso 1 1 calc R U . . . H8B H 0.8173 0.3623 0.2635 0.061 Uiso 1 1 calc R U . . . H8C H 0.7757 0.2570 0.2938 0.061 Uiso 1 1 calc R U . . . C9 C 0.7892(3) 0.5866(4) 0.31076(16) 0.0354(11) Uani 1 1 d . . . . . H9A H 0.8496 0.5657 0.3329 0.053 Uiso 1 1 calc R U . . . H9B H 0.7687 0.6633 0.3170 0.053 Uiso 1 1 calc R U . . . H9C H 0.8129 0.5785 0.2762 0.053 Uiso 1 1 calc R U . . . C10 C 0.5673(4) 0.6487(3) 0.37035(13) 0.0266(8) Uani 1 1 d . . . . . H10A H 0.4946 0.6737 0.3594 0.040 Uiso 1 1 calc R U . . . H10B H 0.6228 0.7031 0.3609 0.040 Uiso 1 1 calc R U . . . H10C H 0.5674 0.6398 0.4065 0.040 Uiso 1 1 calc R U . . . C11 C 0.2602(4) 0.6845(4) 0.33680(17) 0.0371(11) Uani 1 1 d . . . . . H11A H 0.3142 0.7140 0.3133 0.056 Uiso 1 1 calc R U . . . H11B H 0.2985 0.6547 0.3658 0.056 Uiso 1 1 calc R U . . . H11C H 0.2103 0.7433 0.3473 0.056 Uiso 1 1 calc R U . . . C12 C 0.1084(3) 0.4850(4) 0.35359(15) 0.0359(10) Uani 1 1 d . . . . . H12A H 0.1629 0.4550 0.3767 0.054 Uiso 1 1 calc R U . . . H12B H 0.0701 0.4245 0.3369 0.054 Uiso 1 1 calc R U . . . H12C H 0.0551 0.5297 0.3719 0.054 Uiso 1 1 calc R U . . . C13 C 0.0721(4) 0.6377(4) 0.26573(15) 0.0357(10) Uani 1 1 d . . . . . H13A H 0.0234 0.6832 0.2862 0.054 Uiso 1 1 calc R U . . . H13B H 0.0290 0.5802 0.2493 0.054 Uiso 1 1 calc R U . . . H13C H 0.1078 0.6837 0.2406 0.054 Uiso 1 1 calc R U . . . C14 C 0.2000(3) 0.3562(3) 0.24466(14) 0.0214(7) Uani 1 1 d . . . . . C15 C 0.2046(4) 0.2590(4) 0.27132(14) 0.0292(9) Uani 1 1 d . . . . . H15 H 0.2554 0.2523 0.2979 0.035 Uiso 1 1 calc R U . . . C16 C 0.1360(4) 0.1706(4) 0.25996(15) 0.0364(11) Uani 1 1 d . . . . . H16 H 0.1412 0.1044 0.2785 0.044 Uiso 1 1 calc R U . . . C17 C 0.0608(4) 0.1790(4) 0.22199(15) 0.0374(11) Uani 1 1 d . . . . . H17 H 0.0141 0.1188 0.2143 0.045 Uiso 1 1 calc R U . . . C18 C 0.0535(3) 0.2759(4) 0.19505(15) 0.0318(10) Uani 1 1 d . . . . . H18 H 0.0013 0.2821 0.1690 0.038 Uiso 1 1 calc R U . . . C19 C 0.1221(3) 0.3639(4) 0.20602(14) 0.0251(8) Uani 1 1 d . . . . . H19 H 0.1166 0.4299 0.1873 0.030 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Th1 0.01154(5) 0.01154(5) 0.01742(7) 0.00006(4) 0.00006(4) 0.00091(7) P1 0.0122(4) 0.0251(5) 0.0263(4) -0.0089(4) 0.0015(3) -0.0007(4) Si1 0.0158(5) 0.0285(6) 0.0286(5) -0.0065(5) 0.0029(4) 0.0035(5) C1 0.0202(18) 0.0215(17) 0.0201(14) 0.0039(11) -0.0035(13) -0.0010(15) C2 0.027(2) 0.0196(19) 0.0276(18) 0.0079(14) -0.0028(15) 0.0014(15) C3 0.024(2) 0.032(2) 0.0264(18) 0.0094(16) -0.0052(15) 0.0070(18) C4 0.0151(16) 0.031(2) 0.0256(17) 0.0105(16) -0.0069(12) -0.0037(17) C5 0.0205(18) 0.021(2) 0.0178(14) 0.0045(12) -0.0066(12) -0.0050(14) C6 0.027(2) 0.033(2) 0.0246(16) 0.0043(15) 0.0023(15) -0.0085(17) C7 0.049(3) 0.022(2) 0.043(2) 0.0100(18) 0.003(2) 0.004(2) C8 0.027(2) 0.048(3) 0.048(3) 0.012(2) -0.002(2) 0.022(2) C9 0.018(2) 0.049(3) 0.039(2) 0.015(2) -0.0101(17) -0.008(2) C10 0.031(2) 0.024(2) 0.0248(17) -0.0015(15) -0.0061(16) -0.0065(17) C11 0.030(2) 0.031(2) 0.050(3) -0.020(2) 0.0005(19) 0.0080(19) C12 0.029(2) 0.043(3) 0.036(2) -0.001(2) 0.0125(16) 0.008(2) C13 0.021(2) 0.047(3) 0.039(2) 0.0008(18) 0.0035(17) 0.011(2) C14 0.0162(16) 0.0263(19) 0.0218(17) -0.0062(15) 0.0021(15) -0.0004(14) C15 0.032(2) 0.032(2) 0.0238(17) -0.0003(15) 0.0020(15) -0.0045(18) C16 0.048(3) 0.028(2) 0.033(2) 0.0024(16) 0.0089(18) -0.010(2) C17 0.035(2) 0.039(3) 0.037(2) -0.0162(19) 0.0096(19) -0.018(2) C18 0.023(2) 0.043(3) 0.030(2) -0.0153(18) -0.0011(15) -0.0068(18) C19 0.0168(19) 0.033(2) 0.0251(18) -0.0044(16) 0.0016(14) -0.0003(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Th Th -7.2400 8.8979 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C2 Th1 C2 107.22(16) 8_665 . C2 Th1 C1 135.51(11) 8_665 . C2 Th1 C1 29.59(11) . . C2 Th1 C1 29.59(11) 8_665 8_665 C2 Th1 C1 135.51(11) . 8_665 C1 Th1 C1 164.87(15) . 8_665 C2 Th1 C3 29.35(12) 8_665 8_665 C2 Th1 C3 88.52(12) . 8_665 C1 Th1 C3 117.79(11) . 8_665 C1 Th1 C3 48.29(11) 8_665 8_665 C2 Th1 C3 88.52(12) 8_665 . C2 Th1 C3 29.35(12) . . C1 Th1 C3 48.29(11) . . C1 Th1 C3 117.79(11) 8_665 . C3 Th1 C3 81.72(17) 8_665 . C2 Th1 C4 48.37(12) 8_665 8_665 C2 Th1 C4 100.79(11) . 8_665 C1 Th1 C4 124.16(10) . 8_665 C1 Th1 C4 48.13(10) 8_665 8_665 C3 Th1 C4 29.15(13) 8_665 8_665 C3 Th1 C4 105.38(12) . 8_665 C2 Th1 C4 100.79(11) 8_665 . C2 Th1 C4 48.37(12) . . C1 Th1 C4 48.13(10) . . C1 Th1 C4 124.17(10) 8_665 . C3 Th1 C4 105.38(12) 8_665 . C3 Th1 C4 29.15(13) . . C4 Th1 C4 132.59(18) 8_665 . C2 Th1 P1 126.69(8) 8_665 . C2 Th1 P1 102.78(9) . . C1 Th1 P1 87.00(8) . . C1 Th1 P1 103.53(7) 8_665 . C3 Th1 P1 112.18(9) 8_665 . C3 Th1 P1 131.77(9) . . C4 Th1 P1 83.63(9) 8_665 . C4 Th1 P1 131.74(8) . . C2 Th1 P1 102.78(9) 8_665 8_665 C2 Th1 P1 126.69(8) . 8_665 C1 Th1 P1 103.53(7) . 8_665 C1 Th1 P1 87.00(8) 8_665 8_665 C3 Th1 P1 131.77(9) 8_665 8_665 C3 Th1 P1 112.18(9) . 8_665 C4 Th1 P1 131.75(8) 8_665 8_665 C4 Th1 P1 83.63(9) . 8_665 P1 Th1 P1 92.75(5) . 8_665 C2 Th1 C5 48.38(11) 8_665 8_665 C2 Th1 C5 129.92(11) . 8_665 C1 Th1 C5 150.33(10) . 8_665 C1 Th1 C5 29.09(9) 8_665 8_665 C3 Th1 C5 48.06(11) 8_665 8_665 C3 Th1 C5 129.77(11) . 8_665 C4 Th1 C5 29.13(10) 8_665 8_665 C4 Th1 C5 149.13(11) . 8_665 P1 Th1 C5 78.59(7) . 8_665 P1 Th1 C5 102.95(7) 8_665 8_665 C2 Th1 C5 129.92(11) 8_665 . C2 Th1 C5 48.38(11) . . C1 Th1 C5 29.09(9) . . C1 Th1 C5 150.33(10) 8_665 . C3 Th1 C5 129.77(12) 8_665 . C3 Th1 C5 48.06(11) . . C4 Th1 C5 149.13(11) 8_665 . C4 Th1 C5 29.13(10) . . P1 Th1 C5 102.94(7) . . P1 Th1 C5 78.59(7) 8_665 . C5 Th1 C5 177.83(15) 8_665 . C14 P1 Si1 99.70(12) . . C14 P1 Th1 126.92(12) . . Si1 P1 Th1 130.62(5) . . C11 Si1 C13 108.4(2) . . C11 Si1 C12 110.7(2) . . C13 Si1 C12 108.4(2) . . C11 Si1 P1 109.09(14) . . C13 Si1 P1 109.29(14) . . C12 Si1 P1 110.99(16) . . C5 C1 C2 108.3(3) . . C5 C1 C6 125.9(3) . . C2 C1 C6 125.0(3) . . C5 C1 Th1 77.25(16) . . C2 C1 Th1 74.30(18) . . C6 C1 Th1 122.5(2) . . C3 C2 C1 107.8(3) . . C3 C2 C7 128.4(4) . . C1 C2 C7 123.5(4) . . C3 C2 Th1 76.6(2) . . C1 C2 Th1 76.11(19) . . C7 C2 Th1 117.7(3) . . C2 C3 C4 108.2(3) . . C2 C3 C8 127.6(4) . . C4 C3 C8 122.7(4) . . C2 C3 Th1 74.0(2) . . C4 C3 Th1 76.2(2) . . C8 C3 Th1 126.8(3) . . C3 C4 C5 108.1(3) . . C3 C4 C9 124.0(4) . . C5 C4 C9 127.1(4) . . C3 C4 Th1 74.7(2) . . C5 C4 Th1 76.11(18) . . C9 C4 Th1 123.4(2) . . C1 C5 C4 107.5(3) . . C1 C5 C10 125.1(3) . . C4 C5 C10 126.7(3) . . C1 C5 Th1 73.66(17) . . C4 C5 Th1 74.77(19) . . C10 C5 Th1 124.9(2) . . C1 C6 H6A 109.5 . . C1 C6 H6B 109.5 . . H6A C6 H6B 109.5 . . C1 C6 H6C 109.5 . . H6A C6 H6C 109.5 . . H6B C6 H6C 109.5 . . C2 C7 H7A 109.5 . . C2 C7 H7B 109.5 . . H7A C7 H7B 109.5 . . C2 C7 H7C 109.5 . . H7A C7 H7C 109.5 . . H7B C7 H7C 109.5 . . C3 C8 H8A 109.5 . . C3 C8 H8B 109.5 . . H8A C8 H8B 109.5 . . C3 C8 H8C 109.5 . . H8A C8 H8C 109.5 . . H8B C8 H8C 109.5 . . C4 C9 H9A 109.5 . . C4 C9 H9B 109.5 . . H9A C9 H9B 109.5 . . C4 C9 H9C 109.5 . . H9A C9 H9C 109.5 . . H9B C9 H9C 109.5 . . C5 C10 H10A 109.5 . . C5 C10 H10B 109.5 . . H10A C10 H10B 109.5 . . C5 C10 H10C 109.5 . . H10A C10 H10C 109.5 . . H10B C10 H10C 109.5 . . Si1 C11 H11A 109.5 . . Si1 C11 H11B 109.5 . . H11A C11 H11B 109.5 . . Si1 C11 H11C 109.5 . . H11A C11 H11C 109.5 . . H11B C11 H11C 109.5 . . Si1 C12 H12A 109.5 . . Si1 C12 H12B 109.5 . . H12A C12 H12B 109.5 . . Si1 C12 H12C 109.5 . . H12A C12 H12C 109.5 . . H12B C12 H12C 109.5 . . Si1 C13 H13A 109.5 . . Si1 C13 H13B 109.5 . . H13A C13 H13B 109.5 . . Si1 C13 H13C 109.5 . . H13A C13 H13C 109.5 . . H13B C13 H13C 109.5 . . C15 C14 C19 117.8(4) . . C15 C14 P1 121.2(3) . . C19 C14 P1 121.0(3) . . C14 C15 C16 121.3(4) . . C14 C15 H15 119.3 . . C16 C15 H15 119.3 . . C17 C16 C15 120.3(4) . . C17 C16 H16 119.9 . . C15 C16 H16 119.9 . . C16 C17 C18 119.6(4) . . C16 C17 H17 120.2 . . C18 C17 H17 120.2 . . C17 C18 C19 120.3(4) . . C17 C18 H18 119.8 . . C19 C18 H18 119.8 . . C18 C19 C14 120.6(4) . . C18 C19 H19 119.7 . . C14 C19 H19 119.7 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Th1 C2 2.772(3) 8_665 Th1 C2 2.772(3) . Th1 C1 2.795(3) . Th1 C1 2.796(3) 8_665 Th1 C3 2.805(4) 8_665 Th1 C3 2.805(4) . Th1 C4 2.824(3) 8_665 Th1 C4 2.824(3) . Th1 P1 2.8243(9) . Th1 P1 2.8243(9) 8_665 Th1 C5 2.841(3) 8_665 Th1 C5 2.841(3) . P1 C14 1.843(4) . P1 Si1 2.2265(14) . Si1 C11 1.871(5) . Si1 C13 1.876(4) . Si1 C12 1.876(4) . C1 C5 1.416(5) . C1 C2 1.422(5) . C1 C6 1.508(5) . C2 C3 1.413(6) . C2 C7 1.504(6) . C3 C4 1.417(6) . C3 C8 1.514(6) . C4 C5 1.425(5) . C4 C9 1.509(6) . C5 C10 1.497(5) . C6 H6A 0.9800 . C6 H6B 0.9800 . C6 H6C 0.9800 . C7 H7A 0.9800 . C7 H7B 0.9800 . C7 H7C 0.9800 . C8 H8A 0.9800 . C8 H8B 0.9800 . C8 H8C 0.9800 . C9 H9A 0.9800 . C9 H9B 0.9800 . C9 H9C 0.9800 . C10 H10A 0.9800 . C10 H10B 0.9800 . C10 H10C 0.9800 . C11 H11A 0.9800 . C11 H11B 0.9800 . C11 H11C 0.9800 . C12 H12A 0.9800 . C12 H12B 0.9800 . C12 H12C 0.9800 . C13 H13A 0.9800 . C13 H13B 0.9800 . C13 H13C 0.9800 . C14 C15 1.385(6) . C14 C19 1.411(5) . C15 C16 1.394(6) . C15 H15 0.9500 . C16 C17 1.377(6) . C16 H16 0.9500 . C17 C18 1.387(7) . C17 H17 0.9500 . C18 C19 1.389(6) . C18 H18 0.9500 . C19 H19 0.9500 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C5 C1 C2 C3 0.3(4) . . . . C6 C1 C2 C3 -170.3(3) . . . . Th1 C1 C2 C3 70.7(3) . . . . C5 C1 C2 C7 175.3(3) . . . . C6 C1 C2 C7 4.7(6) . . . . Th1 C1 C2 C7 -114.3(4) . . . . C5 C1 C2 Th1 -70.4(2) . . . . C6 C1 C2 Th1 119.0(3) . . . . C1 C2 C3 C4 -1.2(4) . . . . C7 C2 C3 C4 -175.9(4) . . . . Th1 C2 C3 C4 69.2(3) . . . . C1 C2 C3 C8 165.1(4) . . . . C7 C2 C3 C8 -9.6(7) . . . . Th1 C2 C3 C8 -124.5(4) . . . . C1 C2 C3 Th1 -70.4(2) . . . . C7 C2 C3 Th1 115.0(4) . . . . C2 C3 C4 C5 1.7(4) . . . . C8 C3 C4 C5 -165.4(3) . . . . Th1 C3 C4 C5 69.4(2) . . . . C2 C3 C4 C9 172.1(3) . . . . C8 C3 C4 C9 4.9(6) . . . . Th1 C3 C4 C9 -120.2(3) . . . . C2 C3 C4 Th1 -67.7(3) . . . . C8 C3 C4 Th1 125.1(4) . . . . C2 C1 C5 C4 0.8(3) . . . . C6 C1 C5 C4 171.2(3) . . . . Th1 C1 C5 C4 -67.7(2) . . . . C2 C1 C5 C10 -170.1(3) . . . . C6 C1 C5 C10 0.4(5) . . . . Th1 C1 C5 C10 121.5(3) . . . . C2 C1 C5 Th1 68.5(2) . . . . C6 C1 C5 Th1 -121.1(3) . . . . C3 C4 C5 C1 -1.5(4) . . . . C9 C4 C5 C1 -171.5(3) . . . . Th1 C4 C5 C1 66.9(2) . . . . C3 C4 C5 C10 169.1(3) . . . . C9 C4 C5 C10 -0.9(6) . . . . Th1 C4 C5 C10 -122.4(3) . . . . C3 C4 C5 Th1 -68.5(3) . . . . C9 C4 C5 Th1 121.6(4) . . . . Si1 P1 C14 C15 -97.6(3) . . . . Th1 P1 C14 C15 65.1(3) . . . . Si1 P1 C14 C19 82.0(3) . . . . Th1 P1 C14 C19 -115.3(3) . . . . C19 C14 C15 C16 1.1(6) . . . . P1 C14 C15 C16 -179.2(3) . . . . C14 C15 C16 C17 -0.8(6) . . . . C15 C16 C17 C18 0.0(6) . . . . C16 C17 C18 C19 0.4(6) . . . . C17 C18 C19 C14 -0.1(6) . . . . C15 C14 C19 C18 -0.7(5) . . . . P1 C14 C19 C18 179.7(3) . . . .