#------------------------------------------------------------------------------ #$Date: 2019-12-06 11:07:30 +0200 (Fri, 06 Dec 2019) $ #$Revision: 244924 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/64/1556427.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556427 loop_ _publ_author_name 'Rungthanaphatsophon, P.' 'Fajen, O.J.' 'Kelley, S.P.' 'Walensky, J.R.' _publ_section_title ; Thorium(IV) and Uranium(IV) Phosphaazaallenes ; _journal_name_full Inorganics _journal_page_first 105 _journal_paper_doi 10.3390/inorganics7090105 _journal_volume 7 _journal_year 2019 _chemical_formula_sum 'C38 H58 P2 Si2 U' _chemical_formula_weight 870.99 _space_group_crystal_system tetragonal _space_group_IT_number 96 _space_group_name_Hall 'P 4nw 2abw' _space_group_name_H-M_alt 'P 43 21 2' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.0767(11) _cell_length_b 12.0767(11) _cell_length_c 26.931(3) _cell_measurement_reflns_used 9962 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 27.78 _cell_measurement_theta_min 2.27 _cell_volume 3927.8(7) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2017/1 (Sheldrick, 2017)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0615 _diffrn_reflns_av_unetI/netI 0.0280 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 35 _diffrn_reflns_limit_l_min -35 _diffrn_reflns_number 81732 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.888 _diffrn_reflns_theta_min 2.502 _exptl_absorpt_coefficient_mu 4.299 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6885 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'Bruker AXScale' _exptl_crystal_colour brown _exptl_crystal_density_diffrn 1.473 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 1744 _exptl_crystal_size_max 0.110 _exptl_crystal_size_mid 0.090 _exptl_crystal_size_min 0.050 _refine_diff_density_max 0.458 _refine_diff_density_min -0.315 _refine_diff_density_rms 0.059 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.022(5) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.983 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 204 _refine_ls_number_reflns 4691 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.983 _refine_ls_R_factor_all 0.0212 _refine_ls_R_factor_gt 0.0166 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0136P)^2^+0.7178P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0320 _refine_ls_wR_factor_ref 0.0330 _reflns_Friedel_coverage 0.704 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 1.000 _reflns_number_gt 4330 _reflns_number_total 4691 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file Complex2_CIF.cif _cod_data_source_block s1 _cod_original_cell_volume 3927.8(8) _cod_database_code 1556427 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.649 _shelx_estimated_absorpt_t_max 0.814 _shelx_res_file ; TITL s1 in P4(3)2(1)2 s1.res created by SHELXL-2017/1 at 15:55:03 on 09-Jan-2018 CELL 0.71073 12.07670 12.07670 26.93120 90.0000 90.0000 90.0000 ZERR 4.00 0.00110 0.00110 0.00260 0.0000 0.0000 0.0000 LATT -1 SYMM -X, -Y, 0.5+Z SYMM 0.5-Y, 0.5+X, 0.75+Z SYMM 0.5+Y, 0.5-X, 0.25+Z SYMM 0.5-X, 0.5+Y, 0.75-Z SYMM 0.5+X, 0.5-Y, 0.25-Z SYMM Y, X, -Z SYMM -Y, -X, 0.5-Z SFAC C H SI P U UNIT 152 232 8 8 4 TEMP -173 SIZE 0.05 0.09 0.11 L.S. 16 ACTA FMAP 2 PLAN 20 OMIT 1 1 0 TWIN WGHT 0.013600 0.717800 BASF 0.02227 FVAR 0.07827 U1 5 0.470850 0.470850 0.000000 10.50000 0.01107 0.01107 = 0.01293 -0.00042 0.00042 -0.00079 P1 4 0.467510 0.697392 0.009348 11.00000 0.02213 0.01284 = 0.01942 -0.00090 -0.00631 0.00062 SI1 3 0.569448 0.813492 0.054543 11.00000 0.02854 0.01504 = 0.02444 -0.00399 -0.00555 -0.00387 C1 1 0.392197 0.305550 0.060595 11.00000 0.03102 0.02010 = 0.02268 0.00607 0.00952 -0.00783 C2 1 0.348128 0.405878 0.079015 11.00000 0.02074 0.02848 = 0.02038 0.00645 0.01111 -0.00243 C3 1 0.436450 0.467289 0.100098 11.00000 0.02314 0.02081 = 0.01460 0.00529 0.00602 0.00165 C4 1 0.534801 0.405078 0.094682 11.00000 0.02342 0.02024 = 0.01198 0.00718 0.00434 0.00524 C5 1 0.507444 0.306148 0.069543 11.00000 0.02871 0.01498 = 0.02025 0.00970 0.01111 0.00282 C6 1 0.329971 0.202797 0.045972 11.00000 0.05240 0.02835 = 0.04443 0.00459 0.01105 -0.01773 AFIX 137 H6A 2 0.338938 0.146326 0.071793 11.00000 -1.50000 H6B 2 0.359180 0.174644 0.014457 11.00000 -1.50000 H6C 2 0.251226 0.220433 0.042134 11.00000 -1.50000 AFIX 0 C7 1 0.229230 0.441755 0.081909 11.00000 0.02052 0.05348 = 0.03894 0.00235 0.01078 -0.00070 AFIX 137 H7A 2 0.210187 0.458544 0.116471 11.00000 -1.50000 H7B 2 0.181457 0.382105 0.069672 11.00000 -1.50000 H7C 2 0.218461 0.508027 0.061472 11.00000 -1.50000 AFIX 0 C8 1 0.423930 0.569635 0.131287 11.00000 0.03562 0.02907 = 0.01866 -0.00078 0.00602 0.01171 AFIX 137 H8A 2 0.398225 0.548975 0.164535 11.00000 -1.50000 H8B 2 0.369853 0.619337 0.115815 11.00000 -1.50000 H8C 2 0.495542 0.607369 0.133859 11.00000 -1.50000 AFIX 0 C9 1 0.642717 0.431376 0.119216 11.00000 0.02626 0.03242 = 0.01707 0.00487 0.00082 0.00928 AFIX 137 H9A 2 0.633169 0.430282 0.155349 11.00000 -1.50000 H9B 2 0.667614 0.505014 0.108771 11.00000 -1.50000 H9C 2 0.698094 0.376067 0.109606 11.00000 -1.50000 AFIX 0 C10 1 0.581042 0.206986 0.060944 11.00000 0.04427 0.01712 = 0.03195 0.00983 0.01252 0.00898 AFIX 137 H10A 2 0.556549 0.145611 0.082064 11.00000 -1.50000 H10B 2 0.657703 0.226245 0.069177 11.00000 -1.50000 H10C 2 0.576663 0.184713 0.026008 11.00000 -1.50000 AFIX 0 C11 1 0.685376 0.734896 0.084395 11.00000 0.03376 0.02954 = 0.04544 -0.00198 -0.01857 -0.00864 AFIX 137 H11A 2 0.747594 0.785094 0.090641 11.00000 -1.50000 H11B 2 0.709373 0.675118 0.062264 11.00000 -1.50000 H11C 2 0.659822 0.703347 0.115903 11.00000 -1.50000 AFIX 0 C12 1 0.631397 0.922194 0.013467 11.00000 0.04604 0.02173 = 0.03813 -0.00445 0.00185 -0.01218 AFIX 137 H12A 2 0.672702 0.975387 0.033767 11.00000 -1.50000 H12B 2 0.572257 0.960835 -0.004439 11.00000 -1.50000 H12C 2 0.681650 0.887248 -0.010423 11.00000 -1.50000 AFIX 0 C13 1 0.482642 0.884822 0.102621 11.00000 0.04618 0.02536 = 0.03220 -0.01274 -0.00117 -0.00621 AFIX 137 H13A 2 0.528024 0.938998 0.120504 11.00000 -1.50000 H13B 2 0.453799 0.829933 0.126094 11.00000 -1.50000 H13C 2 0.420745 0.922808 0.086385 11.00000 -1.50000 AFIX 0 C14 1 0.351552 0.791031 -0.004981 11.00000 0.02587 0.01442 = 0.01735 -0.00424 -0.00564 0.00097 C15 1 0.358663 0.869893 -0.043102 11.00000 0.03251 0.01858 = 0.01943 -0.00082 -0.00458 0.00188 AFIX 43 H15A 2 0.424850 0.875697 -0.061987 11.00000 -1.20000 AFIX 0 C16 1 0.270279 0.939551 -0.053591 11.00000 0.04482 0.02056 = 0.02689 0.00206 -0.01760 0.00354 AFIX 43 H16A 2 0.276177 0.991779 -0.079836 11.00000 -1.20000 AFIX 0 C17 1 0.174004 0.933527 -0.026218 11.00000 0.03433 0.03193 = 0.03598 -0.00738 -0.01319 0.01601 AFIX 43 H17A 2 0.113632 0.981294 -0.033470 11.00000 -1.20000 AFIX 0 C18 1 0.166273 0.857498 0.011767 11.00000 0.02736 0.04219 = 0.02619 -0.00867 0.00006 0.00991 AFIX 43 H18A 2 0.100570 0.853544 0.031083 11.00000 -1.20000 AFIX 0 C19 1 0.253818 0.786663 0.021999 11.00000 0.03141 0.02731 = 0.01733 -0.00233 -0.00117 0.00503 AFIX 43 H19A 2 0.246662 0.734065 0.048032 11.00000 -1.20000 AFIX 0 HKLF 4 REM s1 in P4(3)2(1)2 REM R1 = 0.0166 for 4330 Fo > 4sig(Fo) and 0.0212 for all 4691 data REM 204 parameters refined using 0 restraints END WGHT 0.0102 0.5888 REM Highest difference peak 0.458, deepest hole -0.315, 1-sigma level 0.059 Q1 1 0.4630 0.4017 0.0025 11.00000 0.05 0.46 Q2 1 0.4737 0.4743 0.0773 11.00000 0.05 0.27 Q3 1 0.4821 0.4359 0.1086 11.00000 0.05 0.27 Q4 1 0.4834 0.6378 0.0185 11.00000 0.05 0.27 Q5 1 0.5886 0.4146 0.1005 11.00000 0.05 0.25 Q6 1 0.4126 0.7538 -0.0004 11.00000 0.05 0.24 Q7 1 0.3187 0.4434 0.0751 11.00000 0.05 0.23 Q8 1 0.4606 0.3529 0.0498 11.00000 0.05 0.22 Q9 1 0.5376 0.4219 0.0777 11.00000 0.05 0.22 Q10 1 0.1984 0.8053 0.0103 11.00000 0.05 0.22 Q11 1 0.2964 0.7746 0.0004 11.00000 0.05 0.22 Q12 1 0.5320 0.6818 0.0722 11.00000 0.05 0.21 Q13 1 0.7022 0.7553 0.1147 11.00000 0.05 0.21 Q14 1 0.4445 0.6379 -0.0003 11.00000 0.05 0.21 Q15 1 0.4639 0.3205 0.0025 11.00000 0.05 0.21 Q16 1 0.4218 0.4931 0.1166 11.00000 0.05 0.21 Q17 1 0.3609 0.3610 0.0543 11.00000 0.05 0.21 Q18 1 0.3057 0.6427 0.0178 11.00000 0.05 0.20 Q19 1 0.3557 0.8352 -0.0141 11.00000 0.05 0.20 Q20 1 0.3847 0.4329 0.0942 11.00000 0.05 0.20 ; _shelx_res_checksum 73470 _shelx_hkl_file ; -1 -1 0 494.53 27.74 2 1 0 62.97 3.89 2 1 0 60.80 3.82 2 1 0 63.42 3.91 -1 2 0 65.22 3.93 1 -2 0 65.42 3.91 1 -2 0 64.16 3.81 1 -2 0 64.97 3.85 1 -2 0 61.51 3.92 -1 2 0 68.92 3.88 -1 2 0 58.75 3.90 -1 2 0 66.93 3.82 -2 -1 0 64.63 3.90 -2 -1 0 69.35 3.84 -2 -1 0 68.23 3.95 -2 -1 0 62.97 3.88 0 2 0 354.72 20.08 -2 0 0 359.45 20.09 0 -2 0 371.77 20.08 0 -2 0 355.05 20.12 2 0 0 347.41 19.95 0 2 0 354.62 20.08 -2 0 0 341.16 20.10 -2 0 0 342.06 19.99 -2 0 0 362.78 19.95 2 0 0 355.62 20.00 0 2 0 345.07 19.86 0 2 0 376.68 20.14 2 0 0 356.13 20.09 2 0 0 372.31 20.14 0 -2 0 346.22 20.07 0 -2 0 352.78 19.86 -1 -2 0 67.30 3.94 1 2 0 62.94 3.90 -2 1 0 64.77 3.91 2 -1 0 63.17 3.88 2 -1 0 63.80 3.92 2 -1 0 64.14 3.76 -1 -2 0 69.63 3.69 -1 -2 0 63.94 3.91 2 -1 0 64.08 3.79 -2 1 0 59.65 3.75 -2 1 0 61.94 3.87 1 2 0 64.03 3.92 1 2 0 65.96 3.92 -2 1 0 60.57 3.78 -1 -2 0 62.98 3.89 2 -2 0 187.42 10.41 -2 -2 0 176.24 10.40 -2 2 0 168.61 10.25 2 -2 0 178.32 10.35 2 -2 0 188.38 10.27 -2 -2 0 170.75 10.24 -2 -2 0 183.37 10.43 -2 -2 0 172.56 10.36 2 2 0 184.15 10.43 2 2 0 171.03 10.40 2 -2 0 176.67 10.36 -2 2 0 180.26 10.35 -2 2 0 200.44 10.40 2 2 0 174.43 10.25 -2 3 0 2.53 0.65 2 -3 0 2.82 0.55 -3 -2 0 2.44 0.54 3 2 0 2.60 0.58 -2 3 0 2.42 0.56 -3 -2 0 3.35 0.67 3 2 0 2.18 0.51 -3 -2 0 3.31 0.65 2 -3 0 2.65 0.56 2 -3 0 2.84 0.65 3 2 0 2.80 0.65 -3 -2 0 2.01 0.57 -2 3 0 4.17 0.65 -2 3 0 2.57 0.57 -3 -2 0 3.03 0.53 1 -3 0 445.15 26.00 -1 3 0 460.28 26.22 -3 -1 0 507.04 26.26 -3 -1 0 476.48 26.17 1 -3 0 467.64 26.15 3 1 0 459.99 26.23 3 1 0 481.07 26.07 -1 3 0 464.10 26.26 1 -3 0 469.67 26.21 -3 -1 0 429.84 26.03 -3 -1 0 465.70 26.21 1 -3 0 459.95 26.26 -1 3 0 435.42 26.14 -1 3 0 461.87 26.01 3 0 0 0.11 0.26 0 -3 0 0.37 0.41 0 3 0 -0.03 0.16 -3 0 0 0.03 0.40 0 -3 0 0.21 0.40 0 -3 0 0.09 0.14 0 -3 0 0.24 0.38 -3 0 0 0.32 0.31 0 3 0 -0.52 0.36 0 3 0 -0.19 0.38 3 0 0 -0.03 0.31 0 3 0 0.37 0.35 -3 0 0 0.11 0.27 3 0 0 -0.57 0.35 3 0 0 0.27 0.29 -3 0 0 0.02 0.37 -1 -3 0 450.75 25.70 -1 -3 0 463.56 26.07 3 -1 0 437.76 25.87 -3 1 0 475.10 25.91 -3 1 0 438.02 26.04 -1 -3 0 467.96 26.13 -1 -3 0 445.11 25.71 3 -1 0 486.56 26.16 -3 1 0 487.76 26.14 -3 1 0 447.47 25.89 3 -1 0 460.84 26.07 1 3 0 479.51 26.14 3 -1 0 448.34 25.89 1 3 0 452.60 26.08 -1 -3 0 477.73 26.10 1 3 0 448.02 26.09 2 3 0 2.48 0.61 3 -2 0 3.71 0.59 2 3 0 2.57 0.63 2 3 0 2.87 0.49 2 3 0 3.21 0.66 -2 -3 0 3.30 0.49 3 -2 0 2.76 0.55 -2 -3 0 1.87 0.60 -2 -3 0 2.39 0.58 3 -2 0 3.56 0.70 -3 2 0 3.02 0.53 -3 2 0 3.23 0.60 -3 2 0 2.38 0.50 -3 2 0 2.21 0.57 3 -3 0 121.40 6.91 -3 -3 0 112.93 6.84 -3 -3 0 115.83 6.67 3 3 0 109.71 6.66 -3 3 0 105.45 6.99 -3 3 0 106.14 6.67 3 -3 0 115.52 6.68 -3 3 0 108.76 6.82 -3 3 0 109.47 6.85 3 3 0 111.25 6.90 -3 -3 0 116.28 6.90 3 -3 0 112.66 6.81 -3 -3 0 120.17 6.93 3 3 0 108.96 6.89 -3 4 0 35.79 2.67 3 -4 0 38.00 2.69 -3 4 0 32.54 3.13 3 -4 0 37.00 2.49 4 3 0 33.65 2.61 4 3 0 32.34 2.48 3 -4 0 28.72 2.46 4 3 0 33.07 2.64 -4 -3 0 36.28 2.65 -4 -3 0 36.88 2.72 -4 -3 0 37.94 2.59 -4 -3 0 30.92 2.46 -3 4 0 35.65 2.49 -3 4 0 32.59 2.52 3 -4 0 36.56 2.67 -4 -2 0 130.53 7.76 2 -4 0 133.64 7.79 -4 -2 0 132.36 7.77 -2 4 0 125.27 7.57 -4 -2 0 123.81 7.77 -4 -2 0 120.75 7.90 -4 -2 0 137.95 7.62 -2 4 0 133.94 7.85 2 -4 0 142.41 7.72 -2 4 0 131.34 7.83 2 -4 0 126.43 7.58 4 2 0 116.69 7.74 2 -4 0 123.84 7.80 4 2 0 125.85 7.75 -2 4 0 120.37 7.66 1 -4 0 1.11 0.34 -1 4 0 0.16 0.46 -1 4 0 0.34 0.45 -1 4 0 -0.19 0.39 1 -4 0 0.51 0.43 1 -4 0 0.87 0.59 4 1 0 0.53 0.47 4 1 0 1.01 0.35 -4 -1 0 0.41 0.43 1 -4 0 1.23 0.53 -4 -1 0 0.90 0.48 -4 -1 0 2.13 0.56 -4 -1 0 0.56 0.39 -4 -1 0 1.57 0.49 -1 4 0 0.71 0.33 0 -4 0 197.81 11.23 0 -4 0 195.04 11.66 0 -4 0 201.10 11.67 0 4 0 196.51 11.69 -4 0 0 195.19 11.51 0 4 0 205.57 11.79 0 4 0 206.43 11.25 4 0 0 215.88 11.77 4 0 0 190.49 11.75 0 4 0 189.52 11.68 0 -4 0 193.38 11.75 4 0 0 200.54 11.54 4 0 0 203.26 11.44 -4 0 0 199.86 11.69 -4 0 0 197.33 11.73 -4 0 0 206.85 11.43 -1 -4 0 0.98 0.51 1 4 0 1.25 0.63 -1 -4 0 1.19 0.18 4 -1 0 0.64 0.47 -1 -4 0 0.73 0.62 4 -1 0 1.26 0.39 4 -1 0 1.03 0.38 -1 -4 0 1.37 0.20 4 -1 0 0.54 0.50 -4 1 0 1.11 0.52 -4 1 0 1.02 0.41 -4 1 0 1.25 0.39 1 4 0 0.75 0.52 1 4 0 1.61 0.57 -4 1 0 0.45 0.42 -1 -4 0 1.92 0.59 2 4 0 124.68 7.88 -4 2 0 132.95 7.68 2 4 0 131.08 7.91 -4 2 0 124.72 7.83 4 -2 0 132.41 7.93 4 -2 0 126.49 7.84 4 -2 0 128.68 7.60 -2 -4 0 137.95 7.43 4 -2 0 129.84 7.64 -2 -4 0 123.18 7.87 -2 -4 0 127.35 7.44 -2 -4 0 134.76 7.87 -4 2 0 125.46 7.59 -4 2 0 122.36 7.85 2 4 0 134.83 7.95 -2 -4 0 132.25 7.90 -4 3 0 31.36 2.55 -3 -4 0 31.24 2.62 3 4 0 32.00 2.68 4 -3 0 36.32 2.68 -3 -4 0 36.36 2.73 -3 -4 0 34.45 2.32 -3 -4 0 37.58 2.70 4 -3 0 32.02 2.52 3 4 0 36.06 2.34 4 -3 0 33.56 2.63 -4 3 0 37.69 2.67 3 4 0 35.06 2.67 -4 3 0 35.18 2.43 -4 -4 0 206.04 12.55 -4 4 0 213.99 12.56 -4 -4 0 224.37 12.57 4 4 0 214.38 12.74 -4 -4 0 203.94 12.60 -4 -4 0 207.88 12.64 4 -4 0 236.75 12.65 -4 4 0 213.16 12.38 -4 4 0 196.64 12.63 -4 4 0 216.21 12.56 4 -4 0 220.28 12.65 4 4 0 203.15 12.34 4 -4 0 205.84 12.33 4 -4 0 203.44 12.50 -4 -4 0 208.74 12.32 4 4 0 216.69 12.76 -5 -4 0 214.41 12.74 5 4 0 210.32 12.48 -5 -4 0 203.86 12.98 -5 -4 0 209.36 12.70 -4 5 0 220.10 12.58 4 -5 0 200.81 12.66 -4 5 0 212.93 12.65 4 -5 0 235.53 12.48 -5 -4 0 219.60 12.48 5 4 0 204.73 12.76 -4 5 0 198.41 12.75 4 -5 0 219.09 12.71 -5 -4 0 196.22 12.47 3 -5 0 98.52 6.06 3 -5 0 101.30 6.25 -5 -3 0 98.45 6.27 5 3 0 93.27 6.34 -5 -3 0 90.27 6.08 -5 -3 0 98.25 6.28 -3 5 0 97.59 6.03 3 -5 0 100.04 6.06 -5 -3 0 91.09 6.01 5 3 0 89.05 6.12 3 -5 0 95.04 6.35 -3 5 0 104.17 6.43 -3 5 0 100.57 6.13 -5 -3 0 100.42 6.16 -3 5 0 100.96 6.30 -5 -2 0 2.08 0.72 2 -5 0 1.97 0.53 -5 -2 0 2.43 0.76 5 2 0 0.94 0.59 -5 -2 0 2.51 0.71 -2 5 0 3.35 1.13 -2 5 0 3.08 0.81 2 -5 0 1.41 0.99 -2 5 0 2.68 0.56 2 -5 0 2.56 0.74 -5 -2 0 3.24 0.88 2 -5 0 2.09 0.75 -5 -2 0 1.43 0.65 -2 5 0 3.71 0.95 -5 -1 0 160.34 8.56 -1 5 0 145.77 8.57 -1 5 0 122.85 8.76 5 1 0 115.38 8.09 -5 -1 0 139.94 8.15 -5 -1 0 142.21 8.31 -5 -1 0 135.33 8.53 -1 5 0 143.11 8.02 -5 -1 0 147.69 8.47 1 -5 0 145.22 8.45 1 -5 0 129.97 8.93 1 -5 0 145.54 8.40 -1 5 0 132.69 8.38 1 -5 0 137.96 8.01 5 1 0 134.05 8.55 0 -5 0 -0.51 0.47 5 0 0 -0.26 0.49 0 5 0 0.67 0.24 0 5 0 0.29 0.65 -5 0 0 0.22 0.61 0 -5 0 -0.67 0.53 -5 0 0 0.15 0.43 5 0 0 -0.56 0.40 -5 0 0 -0.65 0.36 5 0 0 0.39 0.39 0 5 0 -0.09 0.61 -5 0 0 0.56 0.52 0 -5 0 0.80 1.57 0 -5 0 -0.05 0.19 -5 1 0 143.73 8.58 -5 1 0 137.04 8.24 -1 -5 0 147.79 8.55 1 5 0 139.41 8.59 5 -1 0 145.60 8.53 5 -1 0 139.91 8.17 -1 -5 0 134.13 8.67 -5 1 0 144.84 8.21 5 -1 0 128.60 8.65 1 5 0 124.47 8.60 -1 -5 0 145.45 8.50 -5 2 0 2.30 0.66 -5 2 0 1.68 0.87 -5 2 0 3.55 0.72 5 -2 0 4.59 1.29 -2 -5 0 2.52 1.15 5 -2 0 1.86 0.61 5 -2 0 2.69 0.74 -2 -5 0 2.67 0.43 -2 -5 0 3.00 0.87 2 5 0 2.27 1.17 -2 -5 0 2.18 0.40 -5 2 0 1.44 0.94 5 -2 0 2.40 0.64 -2 -5 0 2.79 0.88 2 5 0 2.75 0.88 2 5 0 2.42 1.17 -3 -5 0 95.93 6.41 3 5 0 103.01 6.64 -5 3 0 101.43 6.11 -3 -5 0 99.19 5.89 -3 -5 0 92.67 6.50 -3 -5 0 101.77 6.41 -5 3 0 107.45 6.45 5 -3 0 103.64 6.19 3 5 0 91.62 6.51 5 -3 0 97.35 6.57 5 -3 0 101.39 6.39 -5 3 0 103.08 6.23 -5 3 0 98.95 6.50 -3 -5 0 98.48 5.92 5 -3 0 100.95 6.08 3 5 0 94.49 6.39 -5 4 0 223.30 12.70 4 5 0 215.11 12.97 -4 -5 0 210.53 12.38 -4 -5 0 224.58 12.91 -4 -5 0 211.08 12.83 5 -4 0 199.68 12.90 5 -4 0 215.13 12.82 -4 -5 0 201.88 12.86 5 -4 0 216.31 12.92 -5 4 0 207.02 12.49 -5 4 0 210.29 12.78 4 5 0 211.11 12.95 5 -4 0 212.49 12.48 -5 4 0 229.68 12.96 -5 5 0 137.02 8.45 5 -5 0 136.96 8.60 -5 -5 0 127.11 8.40 5 5 0 135.04 8.21 5 -5 0 138.08 8.21 -5 -5 0 138.78 8.63 -5 5 0 125.65 8.68 5 -5 0 139.38 8.55 -5 5 0 140.12 8.45 -5 -5 0 127.22 8.54 -5 -5 0 134.43 8.17 5 5 0 138.13 8.79 5 5 0 130.56 8.72 -5 5 0 137.37 8.33 5 -5 0 132.57 8.51 5 -6 0 124.86 7.60 -6 -5 0 118.53 7.95 -6 -5 0 114.58 7.73 -6 -5 0 117.35 7.89 -5 6 0 121.32 7.78 -6 -5 0 124.82 7.65 -5 6 0 132.15 8.26 -5 6 0 119.66 7.91 5 -6 0 127.17 8.09 5 -6 0 124.82 7.95 6 5 0 123.96 7.84 -6 -5 0 126.34 8.01 6 5 0 117.30 8.13 -5 6 0 116.08 7.72 5 -6 0 121.72 7.96 -6 -4 0 14.32 2.01 -6 -4 0 14.40 2.06 6 4 0 16.43 2.37 -6 -4 0 12.50 1.78 6 4 0 15.75 2.30 4 -6 0 14.41 1.96 4 -6 0 16.45 2.16 4 -6 0 18.16 2.44 -4 6 0 15.58 1.75 -4 6 0 13.40 2.06 -4 6 0 15.54 2.55 -6 -4 0 15.46 2.15 4 -6 0 16.83 1.76 -6 -4 0 15.78 1.80 -4 6 0 13.72 2.17 -6 -3 0 13.34 1.57 -3 6 0 12.56 1.41 -3 6 0 9.55 1.78 6 3 0 8.59 1.65 3 -6 0 12.19 1.42 -6 -3 0 9.90 1.75 -3 6 0 12.96 1.79 -6 -3 0 12.20 1.50 3 -6 0 14.98 1.54 3 -6 0 12.28 2.02 -3 6 0 10.91 1.83 -6 -3 0 14.22 1.67 3 -6 0 10.36 1.63 -6 -3 0 13.97 1.57 -6 -3 0 12.49 1.83 2 -6 0 112.96 7.17 -6 -2 0 118.83 7.56 -6 -2 0 125.98 7.40 -2 6 0 107.77 7.36 2 -6 0 120.13 7.31 2 -6 0 108.84 7.50 -6 -2 0 126.72 7.36 -6 -2 0 114.44 7.34 -6 -2 0 122.47 7.36 2 -6 0 107.45 6.89 -2 6 0 111.19 6.91 -2 6 0 119.39 7.47 6 2 0 111.45 7.47 -2 6 0 112.43 7.45 -6 -2 0 116.11 7.03 6 1 0 1.66 1.21 -1 6 0 1.62 1.17 1 -6 0 1.64 0.81 -1 6 0 2.96 0.88 -6 -1 0 2.01 0.84 1 -6 0 1.56 1.14 1 -6 0 1.72 0.82 -6 -1 0 1.24 1.12 -1 6 0 2.31 0.47 -6 -1 0 2.54 0.75 -6 -1 0 1.49 0.74 1 -6 0 2.11 0.46 -6 -1 0 2.13 0.83 -1 6 0 2.00 1.12 6 1 0 2.01 0.58 0 -6 0 73.80 4.37 0 -6 0 80.49 5.13 -6 0 0 79.41 4.75 0 6 0 76.00 5.24 0 -6 0 75.73 5.08 0 -6 0 74.48 5.40 6 0 0 82.00 4.94 -6 0 0 77.20 4.87 6 0 0 74.77 5.40 -6 0 0 74.45 5.26 -6 0 0 78.14 5.14 0 6 0 73.10 5.17 6 0 0 69.66 4.69 0 6 0 80.68 4.40 0 6 0 72.38 5.25 6 -1 0 2.15 1.30 6 -1 0 1.46 0.53 1 6 0 1.02 0.82 -1 -6 0 2.94 0.87 -6 1 0 2.02 1.00 -1 -6 0 2.81 1.32 -6 1 0 2.03 0.63 -1 -6 0 2.12 0.91 -6 1 0 2.07 0.78 1 6 0 1.99 1.33 -6 1 0 2.62 0.74 6 -1 0 1.73 0.74 1 6 0 2.02 1.18 6 -1 0 2.65 0.67 -6 2 0 111.61 7.60 -6 2 0 118.18 7.66 -2 -6 0 118.48 7.61 6 -2 0 124.86 7.26 2 6 0 119.12 7.69 6 -2 0 112.01 7.79 -6 2 0 124.36 7.29 6 -2 0 124.51 7.23 -2 -6 0 121.27 7.58 -6 2 0 117.97 7.25 2 6 0 121.68 7.78 2 6 0 123.45 7.79 -2 -6 0 122.77 7.83 6 -2 0 112.88 7.49 -3 -6 0 11.83 1.05 -3 -6 0 14.80 2.28 6 -3 0 14.94 1.77 -6 3 0 13.67 1.57 6 -3 0 12.67 1.44 3 6 0 11.57 2.03 3 6 0 12.51 2.11 6 -3 0 13.46 2.13 -3 -6 0 10.57 1.75 -3 -6 0 12.18 1.09 -6 3 0 12.87 2.00 -6 3 0 9.68 1.71 -3 -6 0 11.26 1.62 6 -3 0 13.15 1.45 3 6 0 9.92 1.70 -6 3 0 11.89 1.40 6 -4 0 18.27 2.16 6 -4 0 15.10 1.87 -6 4 0 18.39 2.32 6 -4 0 18.88 2.69 -4 -6 0 16.54 1.46 -4 -6 0 14.25 2.09 -6 4 0 15.86 2.50 -6 4 0 17.32 2.02 -4 -6 0 18.80 2.39 -6 4 0 17.32 2.11 -4 -6 0 14.41 1.49 4 6 0 15.98 2.45 4 6 0 12.93 2.28 6 -4 0 16.49 1.65 -4 -6 0 19.24 2.63 6 -5 0 126.53 8.09 -5 -6 0 119.69 8.01 -5 -6 0 113.43 7.84 -5 -6 0 117.18 7.90 -6 5 0 121.36 7.61 -5 -6 0 121.37 7.36 6 -5 0 123.10 7.47 -6 5 0 119.71 7.76 5 6 0 125.18 8.14 6 -5 0 122.53 7.80 6 -5 0 126.85 7.91 -6 5 0 111.64 8.04 5 6 0 116.69 8.15 -6 -6 0 -0.32 1.16 -6 -6 0 1.19 1.21 6 -6 0 1.13 0.87 -6 -6 0 2.94 1.52 -6 6 0 2.12 1.77 -6 6 0 2.26 1.29 -6 6 0 -0.34 1.04 6 -6 0 0.05 1.13 6 6 0 1.02 1.39 -6 -6 0 0.87 1.46 6 6 0 0.22 1.74 -6 -6 0 0.60 0.84 6 -6 0 -0.28 1.18 6 -6 0 0.39 1.48 -6 6 0 0.52 1.24 -7 -6 0 86.52 6.39 6 -7 0 87.08 6.38 -7 -6 0 90.53 5.87 -6 7 0 84.53 5.99 -7 -6 0 85.86 6.25 -6 7 0 86.04 6.53 7 6 0 85.33 6.53 -6 7 0 81.27 6.10 7 6 0 88.78 6.12 6 -7 0 86.81 6.46 6 -7 0 89.81 5.81 -7 -6 0 85.46 6.01 -6 7 0 84.51 6.21 -7 -5 0 8.67 1.83 -7 -5 0 14.95 2.36 -7 -5 0 11.59 1.83 -5 7 0 12.47 2.04 5 -7 0 8.43 1.70 7 5 0 9.71 2.05 -5 7 0 9.45 2.05 -7 -5 0 8.74 1.71 -5 7 0 10.75 1.85 5 -7 0 14.27 2.18 -5 7 0 11.85 1.98 7 5 0 8.16 1.92 5 -7 0 10.10 2.21 -7 -5 0 9.13 2.15 7 4 0 257.22 16.33 -7 -4 0 285.48 16.48 -7 -4 0 292.50 16.33 -4 7 0 253.92 16.21 -7 -4 0 272.78 16.24 -7 -4 0 284.18 16.44 -7 -4 0 278.91 16.41 -4 7 0 265.52 16.49 4 -7 0 274.03 16.54 -4 7 0 279.77 16.48 4 -7 0 279.10 16.15 -7 -4 0 273.15 16.06 -4 7 0 280.23 16.08 4 -7 0 262.43 16.06 4 -7 0 259.74 16.28 -7 -3 0 0.38 0.89 -7 -3 0 0.36 1.10 7 3 0 1.54 1.29 -7 -3 0 1.81 0.96 -7 -3 0 1.32 1.39 -3 7 0 0.17 0.63 3 -7 0 2.22 0.89 3 -7 0 1.09 0.64 3 -7 0 0.43 1.39 -3 7 0 1.79 1.18 -7 -3 0 -0.68 0.94 -7 -3 0 1.06 1.07 -3 7 0 0.75 1.04 -7 -3 0 2.38 1.09 -3 7 0 1.15 1.37 -7 -2 0 33.39 3.12 7 2 0 35.16 2.67 -2 7 0 38.05 3.10 2 -7 0 33.12 3.50 -2 7 0 32.90 3.34 2 -7 0 31.87 2.88 -7 -2 0 31.41 2.91 2 -7 0 35.99 2.88 2 -7 0 31.83 2.44 -7 -2 0 35.85 3.46 7 2 0 34.33 3.38 -7 -2 0 35.84 2.67 -7 -2 0 36.98 3.04 -2 7 0 33.44 2.39 -2 7 0 31.31 3.21 -7 -1 0 19.92 2.58 -1 7 0 17.95 1.38 1 -7 0 17.31 2.72 -7 -1 0 18.25 2.16 -1 7 0 18.64 2.63 -7 -1 0 18.93 2.15 7 1 0 17.75 2.66 -7 -1 0 17.83 1.77 1 -7 0 17.18 1.39 1 -7 0 16.96 2.03 1 -7 0 20.18 2.30 7 1 0 19.05 1.70 -1 7 0 19.05 2.67 -1 7 0 16.32 2.20 -7 0 0 0.89 0.66 0 -7 0 -0.02 1.23 7 0 0 0.86 0.55 0 -7 0 1.20 1.04 -7 0 0 -0.45 1.02 0 7 0 -0.84 0.95 7 0 0 -0.37 0.66 7 0 0 0.66 1.23 -7 0 0 0.06 0.86 0 7 0 0.66 1.15 0 7 0 -0.79 1.24 -7 0 0 -0.13 1.19 7 -1 0 21.61 1.76 1 7 0 19.58 2.21 1 7 0 16.99 2.48 -7 1 0 19.75 1.83 7 -1 0 18.93 1.86 -1 -7 0 18.48 2.80 -1 -7 0 19.55 2.07 -7 1 0 15.86 2.05 7 -1 0 19.17 2.77 1 7 0 16.57 2.39 -7 1 0 18.49 2.34 -7 1 0 17.46 2.27 7 -2 0 34.29 2.67 -2 -7 0 35.12 3.62 2 7 0 34.69 3.38 -7 2 0 38.30 3.43 2 7 0 30.93 3.02 -7 2 0 32.90 3.19 -2 -7 0 37.13 3.15 -2 -7 0 31.16 3.28 2 7 0 36.01 3.41 7 -2 0 35.46 3.62 7 -2 0 35.26 2.95 -7 2 0 36.70 2.75 -7 2 0 34.68 3.04 7 -2 0 33.81 2.57 3 7 0 1.51 1.13 7 -3 0 1.06 1.57 7 -3 0 2.68 0.72 3 7 0 1.98 1.32 -3 -7 0 0.92 1.02 7 -3 0 -0.98 0.95 -7 3 0 -0.45 0.79 7 -3 0 1.49 0.81 -7 3 0 -1.13 1.24 -3 -7 0 1.39 1.41 -3 -7 0 0.85 0.36 -7 3 0 0.57 1.09 -3 -7 0 2.02 1.14 3 7 0 -0.13 1.47 -3 -7 0 1.02 0.38 7 -4 0 275.16 15.98 4 7 0 260.62 16.59 -7 4 0 261.51 16.04 -7 4 0 285.76 16.19 -4 -7 0 276.56 15.63 -4 -7 0 272.90 16.51 7 -4 0 285.81 16.50 -4 -7 0 276.74 15.69 7 -4 0 270.51 16.12 7 -4 0 277.52 16.71 4 7 0 279.21 16.59 -4 -7 0 263.66 16.56 -7 4 0 274.13 16.49 -7 4 0 266.23 16.48 -4 -7 0 272.21 16.46 4 7 0 280.55 16.75 5 7 0 10.90 2.45 7 -5 0 10.98 1.95 7 -5 0 9.72 1.62 7 -5 0 12.86 2.35 -5 -7 0 10.82 1.47 -5 -7 0 11.12 1.50 -5 -7 0 12.80 2.08 7 -5 0 14.53 2.18 -7 5 0 12.95 2.05 5 7 0 9.47 2.16 -7 5 0 13.71 1.97 -5 -7 0 17.20 2.48 -7 5 0 12.72 2.43 -7 5 0 11.67 1.77 -5 -7 0 11.85 2.39 6 7 0 95.68 6.91 7 -6 0 82.21 6.52 7 -6 0 91.79 6.30 -6 -7 0 85.47 6.50 -7 6 0 77.23 6.03 -7 6 0 95.04 6.10 -6 -7 0 78.34 6.12 -6 -7 0 72.40 6.10 7 -6 0 91.63 5.82 -7 6 0 82.72 6.05 -6 -7 0 87.29 5.62 6 7 0 94.14 6.74 -6 -7 0 87.54 6.31 -7 6 0 85.85 6.49 -7 7 0 4.06 1.71 -7 -7 0 6.89 1.77 -7 7 0 4.99 1.82 -7 7 0 6.32 1.57 7 -7 0 5.90 1.25 7 -7 0 4.65 1.93 7 7 0 2.74 2.19 7 -7 0 5.92 2.23 -7 -7 0 5.77 1.31 -7 7 0 7.83 2.48 -7 -7 0 6.10 2.08 8 7 0 168.38 10.97 -7 8 0 173.42 11.05 -8 -7 0 151.47 10.24 -7 8 0 155.88 10.32 -8 -7 0 156.31 10.70 -8 -7 0 158.09 10.66 -8 -7 0 159.68 10.06 7 -8 0 161.00 10.63 7 -8 0 164.91 10.63 7 -8 0 147.04 9.90 -7 8 0 152.91 10.22 -8 -6 0 1.18 1.34 6 -8 0 1.34 1.73 -6 8 0 0.48 2.00 -8 -6 0 0.28 1.91 -8 -6 0 2.20 1.72 6 -8 0 -1.16 1.30 -6 8 0 4.05 2.06 8 6 0 -0.07 1.46 8 6 0 2.56 2.10 -8 -6 0 1.62 1.45 -6 8 0 0.08 1.30 -6 8 0 -0.24 1.54 6 -8 0 0.71 1.68 -5 8 0 204.27 12.12 -8 -5 0 196.47 12.53 -5 8 0 184.36 12.44 -5 8 0 201.88 12.43 -8 -5 0 195.94 12.38 5 -8 0 205.19 12.75 -5 8 0 210.78 12.85 -8 -5 0 189.05 12.48 8 5 0 194.20 12.47 -8 -5 0 206.67 12.50 -8 -5 0 195.87 12.22 5 -8 0 205.77 12.12 5 -8 0 191.07 12.24 -4 8 0 -0.10 1.60 -8 -4 0 -0.81 1.08 -8 -4 0 0.95 1.33 -8 -4 0 1.51 1.58 4 -8 0 -1.05 1.10 4 -8 0 -0.69 1.17 -4 8 0 0.45 1.46 8 4 0 0.74 1.48 -8 -4 0 1.30 1.35 4 -8 0 0.46 1.37 -8 -4 0 -1.04 1.23 -8 -4 0 0.33 1.52 -4 8 0 2.02 1.68 -4 8 0 0.89 0.88 8 3 0 132.41 8.94 -3 8 0 133.72 8.10 -8 -3 0 140.18 8.72 -8 -3 0 134.11 8.51 3 -8 0 126.72 8.99 -8 -3 0 134.02 8.66 3 -8 0 125.22 8.55 3 -8 0 150.24 8.54 -3 8 0 142.21 8.83 -8 -3 0 129.66 8.63 3 -8 0 132.36 8.12 -8 -3 0 125.97 8.87 -8 -3 0 139.38 8.27 -8 -3 0 121.73 8.62 -3 8 0 130.70 8.96 -3 8 0 129.43 8.85 -8 -2 0 1.65 1.36 2 -8 0 -0.82 1.04 -8 -2 0 -0.12 0.75 2 -8 0 1.83 1.62 -2 8 0 0.37 0.55 -8 -2 0 -0.09 1.36 -8 -2 0 2.96 1.26 8 2 0 1.09 1.56 2 -8 0 0.91 1.07 -2 8 0 -0.59 1.37 -2 8 0 -0.49 1.28 2 -8 0 0.16 0.55 -2 8 0 2.00 1.60 -8 -2 0 -0.46 1.17 -1 8 0 0.76 1.32 8 1 0 -0.58 1.52 -1 8 0 -0.89 1.27 8 1 0 0.88 0.64 -8 -1 0 -0.26 1.36 1 -8 0 -0.91 1.47 -8 -1 0 1.08 1.22 -1 8 0 0.11 0.43 -8 -1 0 0.01 0.70 -8 -1 0 1.52 1.13 1 -8 0 0.07 0.42 -8 -1 0 -0.04 1.19 1 -8 0 -0.42 1.00 -1 8 0 1.36 1.53 1 -8 0 0.46 1.08 8 0 0 49.94 3.44 8 0 0 47.02 3.65 0 -8 0 51.10 4.63 -8 0 0 50.58 3.50 -8 0 0 50.13 4.35 0 -8 0 49.92 3.92 0 8 0 49.02 4.00 -8 0 0 49.40 3.88 8 0 0 45.50 4.46 0 8 0 51.42 4.49 0 -8 0 52.51 3.97 0 8 0 44.90 4.26 -8 0 0 44.97 3.83 -8 1 0 -0.10 1.36 1 8 0 0.23 1.39 8 -1 0 2.16 0.80 1 8 0 0.18 1.50 -8 1 0 0.63 1.04 -1 -8 0 3.23 1.17 8 -1 0 2.77 1.15 -8 1 0 0.52 1.10 -1 -8 0 0.46 1.06 8 -1 0 0.73 0.64 -1 -8 0 -0.59 1.45 8 -1 0 0.06 1.49 -8 1 0 -0.82 0.69 1 8 0 -0.38 1.27 -8 2 0 -1.13 1.15 8 -2 0 0.38 0.68 -8 2 0 1.44 0.89 8 -2 0 0.91 1.61 2 8 0 -0.48 1.47 -2 -8 0 1.02 1.55 -8 2 0 1.28 1.19 -8 2 0 0.46 1.50 2 8 0 0.49 1.62 2 8 0 -1.22 1.21 8 -2 0 0.83 0.76 8 -2 0 2.60 1.22 -2 -8 0 0.79 1.19 -2 -8 0 1.59 1.19 -8 3 0 133.04 8.22 3 8 0 138.91 9.00 8 -3 0 128.42 8.99 -3 -8 0 128.95 8.88 8 -3 0 138.71 8.08 -8 3 0 133.86 8.16 -8 3 0 117.86 8.52 -3 -8 0 122.50 8.53 3 8 0 129.01 8.71 8 -3 0 131.37 8.10 8 -3 0 120.43 8.44 -8 3 0 128.29 8.76 3 8 0 140.28 9.02 -3 -8 0 125.78 8.50 8 -4 0 0.74 1.10 -8 4 0 1.13 1.05 4 8 0 1.79 2.04 -4 -8 0 0.77 0.47 -8 4 0 0.28 1.29 -4 -8 0 1.42 1.63 -4 -8 0 -2.21 1.33 -8 4 0 -0.79 1.52 4 8 0 -1.03 1.43 4 8 0 1.45 1.61 8 -4 0 1.37 1.96 -8 4 0 -0.78 1.40 -4 -8 0 0.69 0.50 8 -4 0 1.44 0.87 5 8 0 202.58 13.23 -8 5 0 203.40 13.06 8 -5 0 198.73 12.37 -5 -8 0 202.18 13.15 -5 -8 0 204.32 12.01 -5 -8 0 203.15 12.07 -8 5 0 211.22 13.14 5 8 0 202.56 13.28 8 -5 0 210.71 13.33 -8 5 0 228.77 12.67 8 -5 0 206.16 12.64 8 -6 0 0.37 1.51 6 8 0 0.16 2.24 6 8 0 1.64 1.94 8 -6 0 -0.68 1.08 -6 -8 0 2.79 1.93 -8 6 0 3.08 1.35 -6 -8 0 0.04 0.85 -6 -8 0 1.58 0.94 -8 6 0 2.51 1.95 -8 6 0 3.23 1.69 8 -6 0 -0.28 1.94 8 -7 0 176.69 10.78 -7 -8 0 163.05 11.11 -8 7 0 163.11 10.57 8 -7 0 189.23 11.30 7 8 0 160.81 11.31 -7 -8 0 161.99 10.13 -8 7 0 156.48 10.66 8 -7 0 157.68 10.21 -7 -8 0 165.32 10.34 -8 7 0 157.51 11.10 -8 -8 0 1.70 1.81 8 8 0 3.36 2.39 8 -8 0 1.73 2.22 -8 8 0 2.55 1.91 8 -8 0 -0.29 1.93 -8 -8 0 1.18 2.15 8 -8 0 2.75 1.45 -8 8 0 -0.91 2.29 -8 -8 0 4.16 1.71 8 -9 0 196.05 12.99 -9 -8 0 198.05 13.04 -9 -8 0 204.87 13.39 -8 9 0 188.43 13.15 -8 9 0 194.85 12.59 -9 -8 0 189.21 12.26 -9 -8 0 191.38 12.57 9 8 0 202.02 13.31 8 -9 0 196.55 12.94 -9 -7 0 3.37 2.55 9 7 0 1.73 2.13 7 -9 0 1.02 1.93 7 -9 0 2.30 2.19 -9 -7 0 2.66 2.10 -7 9 0 4.33 2.32 -9 -7 0 2.41 1.84 -7 9 0 1.68 2.51 6 -9 0 170.81 11.14 -9 -6 0 171.61 10.93 6 -9 0 168.01 10.79 -9 -6 0 160.84 11.05 9 6 0 157.24 10.92 -6 9 0 157.74 11.26 -9 -6 0 160.08 10.62 -6 9 0 180.27 10.99 -9 -6 0 171.53 10.66 -6 9 0 148.26 10.37 6 -9 0 174.26 10.89 -5 9 0 6.56 2.21 -9 -5 0 2.28 1.63 5 -9 0 5.04 1.50 5 -9 0 2.76 1.71 -9 -5 0 3.53 1.91 9 5 0 6.39 2.21 -9 -5 0 3.19 1.41 -5 9 0 3.74 2.19 5 -9 0 4.24 2.17 -5 9 0 4.96 1.25 -9 -5 0 4.95 2.12 -4 9 0 105.82 8.05 9 4 0 127.12 8.23 4 -9 0 110.36 7.41 4 -9 0 111.95 8.20 -4 9 0 116.99 7.21 -9 -4 0 112.05 7.37 4 -9 0 108.83 7.45 -4 9 0 119.18 8.05 -9 -4 0 117.23 7.90 -9 -4 0 107.61 7.63 -9 -4 0 105.18 7.63 -9 -4 0 111.80 8.16 -9 -4 0 117.07 8.01 -3 9 0 5.17 1.05 -9 -3 0 4.78 1.77 -9 -3 0 4.00 1.60 3 -9 0 7.60 1.58 -9 -3 0 7.31 1.28 -3 9 0 3.64 2.07 3 -9 0 7.63 2.31 -9 -3 0 4.19 1.70 -9 -3 0 7.86 1.90 -9 -3 0 4.49 2.13 9 3 0 5.81 2.13 -3 9 0 4.78 1.98 -9 -2 0 24.99 3.35 -9 -2 0 19.13 2.94 -9 -2 0 21.99 2.79 -2 9 0 20.98 3.23 9 2 0 23.27 3.47 -9 -2 0 20.51 2.25 2 -9 0 16.57 2.61 -9 -2 0 21.07 2.82 2 -9 0 17.97 3.07 -2 9 0 19.01 1.78 -2 9 0 21.10 3.41 2 -9 0 22.41 1.76 -9 -2 0 24.18 3.09 -1 9 0 9.74 2.32 -1 9 0 8.20 0.91 -9 -1 0 9.40 1.82 -9 -1 0 9.68 1.61 -9 -1 0 9.97 2.00 -9 -1 0 10.19 2.41 9 1 0 9.30 1.74 1 -9 0 4.21 1.46 -1 9 0 8.58 2.21 -9 -1 0 10.98 2.90 9 1 0 7.45 2.47 -9 -1 0 6.62 1.77 1 -9 0 7.80 2.41 0 -9 0 -0.25 1.35 -9 0 0 -0.78 1.39 0 -9 0 -1.26 1.72 -9 0 0 -1.15 1.26 0 9 0 -0.45 1.66 9 0 0 -1.92 1.74 0 9 0 -0.50 1.77 -9 0 0 -0.07 0.87 0 -9 0 1.33 1.36 -9 1 0 7.42 2.23 9 -1 0 13.55 1.86 -1 -9 0 10.02 2.44 9 -1 0 7.23 1.84 1 9 0 8.07 2.28 -9 1 0 9.59 1.48 -1 -9 0 7.04 1.89 -9 1 0 10.20 1.90 1 9 0 8.95 2.38 9 -1 0 9.21 2.59 9 -2 0 23.25 2.36 -9 2 0 21.32 3.11 -2 -9 0 23.49 3.85 9 -2 0 23.01 3.83 9 -2 0 21.97 2.58 2 9 0 23.98 3.52 -9 2 0 21.09 2.40 2 9 0 21.08 3.20 -9 2 0 26.18 2.92 3 9 0 7.90 2.21 -9 3 0 5.88 1.71 -3 -9 0 4.73 2.22 9 -3 0 3.83 2.20 9 -3 0 6.51 1.46 -9 3 0 5.89 2.05 3 9 0 7.75 2.40 9 -3 0 7.62 1.31 -9 3 0 8.19 1.56 4 9 0 114.13 8.26 -9 4 0 114.42 8.22 -4 -9 0 116.98 8.39 9 -4 0 109.96 7.33 9 -4 0 105.15 8.37 4 9 0 120.17 8.31 9 -4 0 101.50 7.46 -9 4 0 108.85 7.34 -9 4 0 115.96 7.48 -9 5 0 4.53 1.76 -9 5 0 4.86 2.43 -5 -9 0 5.73 2.35 9 -5 0 3.06 1.67 9 -5 0 5.87 2.39 5 9 0 4.88 2.46 -5 -9 0 5.56 0.89 -5 -9 0 5.77 0.91 9 -5 0 5.86 1.25 5 9 0 6.48 2.43 -9 5 0 3.59 1.68 9 -6 0 163.07 10.61 9 -6 0 165.54 11.42 -9 6 0 159.62 11.11 6 9 0 164.27 11.38 9 -6 0 169.89 10.27 -9 6 0 168.43 10.48 -6 -9 0 172.05 9.85 -6 -9 0 165.49 11.26 -6 -9 0 161.32 9.87 -9 6 0 155.65 10.60 6 9 0 166.18 11.47 -9 7 0 2.54 1.96 9 -7 0 2.57 2.06 -9 7 0 5.45 2.81 7 9 0 1.09 2.55 7 9 0 3.77 2.77 9 -7 0 3.40 1.48 9 -7 0 -1.38 2.42 -7 -9 0 -0.19 1.64 -7 -9 0 2.98 2.54 -7 -9 0 2.20 1.28 8 9 0 198.44 13.84 -8 -9 0 209.21 12.72 9 -8 0 194.35 13.17 9 -8 0 206.70 13.68 -8 -9 0 198.53 12.41 -9 8 0 218.45 13.05 -9 8 0 205.71 13.78 -8 -9 0 199.84 13.54 -9 -9 0 -2.70 1.94 -9 9 0 -2.51 2.10 9 -9 0 1.04 2.74 9 -9 0 3.53 2.41 9 9 0 -2.26 2.42 -9 -9 0 0.30 2.68 -9 -9 0 3.97 2.06 -9 9 0 -4.40 2.62 -9 -9 0 3.99 3.29 9 -10 0 137.79 10.54 10 9 0 135.93 10.78 -10 -9 0 127.12 11.55 -10 -9 0 137.48 10.48 9 -10 0 140.63 10.38 -10 -9 0 140.55 10.06 -9 10 0 149.07 10.30 -9 10 0 150.77 11.14 -8 10 0 1.12 2.42 -10 -8 0 -3.29 2.21 -10 -8 0 0.06 2.73 10 8 0 -0.20 2.37 8 -10 0 1.11 2.42 -8 10 0 -1.84 2.79 -10 -8 0 0.68 2.63 8 -10 0 2.50 2.70 7 -10 0 94.76 7.37 -10 -7 0 90.04 7.52 -7 10 0 96.15 8.10 7 -10 0 96.07 7.75 -10 -7 0 95.40 7.69 -7 10 0 96.38 7.42 -6 10 0 2.68 2.50 -10 -6 0 3.75 2.44 10 6 0 1.74 2.31 6 -10 0 -1.78 2.14 -10 -6 0 2.04 2.10 -6 10 0 4.70 1.72 6 -10 0 1.50 1.91 -6 10 0 2.13 2.23 -10 -6 0 -1.42 1.83 10 5 0 114.41 8.51 5 -10 0 112.87 8.71 -10 -5 0 112.74 8.06 -5 10 0 128.63 8.44 -10 -5 0 107.69 7.71 -5 10 0 103.31 8.57 -10 -5 0 111.82 8.28 -10 -5 0 114.29 8.62 5 -10 0 117.88 7.76 10 4 0 4.26 2.44 4 -10 0 0.71 2.07 -4 10 0 -0.63 2.19 4 -10 0 2.24 1.45 -10 -4 0 1.49 1.72 -10 -4 0 0.79 1.39 -10 -4 0 0.57 2.21 -10 -4 0 1.29 1.97 -4 10 0 2.34 2.21 -3 10 0 111.42 7.76 -10 -3 0 94.33 7.56 3 -10 0 97.93 6.27 -10 -3 0 94.98 7.25 -3 10 0 97.16 6.24 -10 -3 0 102.99 6.63 10 3 0 98.56 7.72 -10 -3 0 99.06 6.94 -3 10 0 96.87 7.54 3 -10 0 103.73 7.96 -10 -2 0 2.99 1.74 -2 10 0 0.45 2.07 -10 -2 0 0.90 1.86 2 -10 0 1.40 2.25 -2 10 0 2.74 2.40 -10 -2 0 -0.21 1.75 -2 10 0 2.31 0.72 10 2 0 0.13 1.89 2 -10 0 2.12 0.68 -10 -2 0 2.65 1.21 10 1 0 -1.78 1.09 -10 -1 0 0.96 1.49 10 1 0 3.94 2.10 -10 -1 0 0.34 1.14 -1 10 0 -1.53 1.79 -10 -1 0 -2.63 1.65 -1 10 0 3.27 2.01 1 -10 0 0.75 2.05 -10 -1 0 2.01 1.62 -10 0 0 6.89 1.87 10 0 0 3.60 2.43 -10 0 0 3.94 2.26 -10 0 0 7.96 1.48 10 0 0 5.10 1.48 0 -10 0 6.38 2.67 0 10 0 7.03 2.45 0 10 0 4.29 2.38 10 -1 0 0.86 1.20 -1 -10 0 1.06 2.27 -10 1 0 -0.62 1.36 10 -1 0 0.89 1.26 -10 1 0 -0.08 1.22 -10 1 0 2.18 1.89 10 -1 0 -1.63 2.09 1 10 0 -1.46 1.66 1 10 0 -0.63 2.08 -2 -10 0 0.14 2.10 -10 2 0 1.77 1.72 10 -2 0 0.71 1.19 -10 2 0 1.38 2.04 2 10 0 1.23 2.01 2 10 0 -0.07 2.02 10 -2 0 1.91 1.26 -10 2 0 1.64 1.26 10 -2 0 -0.52 2.15 10 -3 0 109.47 8.23 10 -3 0 101.15 6.68 -3 -10 0 95.58 7.98 -10 3 0 99.41 7.77 -10 3 0 97.62 6.94 -10 3 0 106.86 6.88 3 10 0 91.64 7.80 3 10 0 102.93 7.89 10 -3 0 100.95 6.71 10 -4 0 0.91 1.24 4 10 0 0.20 2.54 10 -4 0 0.47 2.37 4 10 0 -1.01 2.19 -10 4 0 0.48 1.67 -4 -10 0 2.58 2.26 10 -4 0 3.61 1.50 -10 4 0 2.71 2.12 10 -5 0 116.35 7.62 5 10 0 111.09 8.90 10 -5 0 107.55 7.32 5 10 0 108.66 8.68 -10 5 0 114.30 7.76 -10 5 0 110.97 7.68 10 -5 0 102.86 8.75 -10 5 0 110.43 8.58 -5 -10 0 122.65 8.90 10 -6 0 3.54 1.50 6 10 0 0.51 2.53 10 -6 0 0.27 2.70 -6 -10 0 1.53 0.81 10 -6 0 3.42 1.84 -10 6 0 -0.11 1.88 -10 6 0 -2.22 2.17 -6 -10 0 0.45 2.44 6 10 0 -1.83 2.63 -10 6 0 2.07 1.96 -6 -10 0 2.08 0.90 10 -7 0 98.22 6.63 10 -7 0 93.50 7.17 10 -7 0 100.58 8.23 -7 -10 0 94.47 6.10 7 10 0 97.54 8.34 -7 -10 0 86.63 8.03 -10 7 0 91.64 8.25 -10 7 0 82.76 7.00 7 10 0 99.92 8.40 -7 -10 0 98.25 6.13 10 -8 0 1.60 2.28 8 10 0 0.96 2.68 -10 8 0 -1.83 2.20 -10 8 0 0.38 2.98 10 -8 0 -0.64 2.86 -8 -10 0 -1.04 1.72 -8 -10 0 0.74 2.89 -9 -10 0 139.90 10.65 10 -9 0 151.32 10.96 9 10 0 157.13 11.33 -10 9 0 134.13 10.02 10 -9 0 148.88 10.43 -9 -10 0 132.27 9.65 -10 9 0 141.96 11.18 -10 -10 0 -0.98 2.54 10 -10 0 4.29 3.11 10 -10 0 0.24 3.25 -10 -10 0 4.64 3.57 10 10 0 -2.89 3.26 -10 10 0 5.47 3.73 -10 -10 0 -2.89 3.11 -10 10 0 -2.47 2.93 -10 11 0 30.08 5.50 10 -11 0 31.81 4.86 10 -11 0 40.84 6.81 -11 -10 0 33.16 5.15 -11 -10 0 33.10 4.62 -11 -10 0 30.76 5.85 -10 11 0 30.65 4.73 -11 -9 0 1.76 3.19 9 -11 0 6.23 3.46 -9 11 0 -2.59 3.43 -9 11 0 1.24 3.19 9 -11 0 -0.05 2.73 -11 -9 0 3.61 3.35 -11 -9 0 3.38 3.41 8 -11 0 68.98 6.86 8 -11 0 67.04 6.52 -11 -8 0 60.06 6.68 -11 -8 0 51.29 6.34 -8 11 0 59.17 6.90 -11 -8 0 52.73 6.72 -8 11 0 68.47 6.64 -7 11 0 -0.71 2.34 7 -11 0 0.04 2.49 7 -11 0 3.89 2.83 -11 -7 0 2.29 2.80 -11 -7 0 2.30 2.64 -11 -7 0 -2.32 2.58 -11 -6 0 63.39 6.01 -11 -6 0 63.87 6.26 -11 -6 0 56.34 6.35 11 6 0 53.04 5.96 -6 11 0 49.04 4.65 6 -11 0 66.00 5.59 -6 11 0 63.47 6.47 -6 11 0 59.75 6.19 6 -11 0 55.85 6.40 5 -11 0 5.89 2.02 -5 11 0 8.85 2.80 -11 -5 0 6.56 2.02 -5 11 0 8.94 2.94 -11 -5 0 4.79 2.77 11 5 0 5.71 2.65 -11 -5 0 7.27 2.65 -11 -5 0 4.85 2.20 5 -11 0 2.98 2.85 -11 -4 0 46.72 4.61 -11 -4 0 44.24 5.33 -4 11 0 42.31 3.63 -11 -4 0 47.08 5.16 -4 11 0 46.10 5.46 -11 -4 0 50.31 4.29 4 -11 0 44.51 5.42 -4 11 0 50.45 5.67 11 4 0 40.89 5.59 4 -11 0 46.33 4.13 3 -11 0 14.41 1.81 3 -11 0 16.17 3.41 -11 -3 0 14.24 3.09 -3 11 0 10.68 3.01 -3 11 0 10.77 3.15 -11 -3 0 14.36 2.44 -11 -3 0 10.84 2.65 11 3 0 15.38 3.42 -3 11 0 10.02 1.71 -11 -2 0 7.58 2.34 -2 11 0 8.79 2.74 -11 -2 0 8.20 1.69 -11 -2 0 8.95 2.89 -2 11 0 8.48 1.02 2 -11 0 7.23 2.71 -2 11 0 6.10 2.67 11 2 0 9.31 2.95 -1 11 0 19.90 3.74 -11 -1 0 21.52 2.69 -11 -1 0 21.73 3.60 -11 -1 0 18.81 2.90 11 1 0 22.47 3.79 -11 -1 0 21.03 3.61 -1 11 0 21.41 3.77 11 1 0 19.91 2.89 1 -11 0 23.49 3.97 0 11 0 1.61 2.04 0 11 0 -2.50 2.23 -11 0 0 -0.96 1.28 -11 0 0 1.06 2.22 0 -11 0 -0.68 2.36 11 0 0 -0.12 1.32 -11 0 0 -0.04 1.78 11 0 0 0.30 2.25 1 11 0 19.86 3.66 -11 1 0 22.14 2.76 -11 1 0 24.25 3.69 11 -1 0 18.98 2.87 -1 -11 0 20.70 3.78 -11 1 0 22.62 3.30 1 11 0 21.73 3.78 11 -1 0 20.97 3.71 11 -2 0 6.35 1.64 -11 2 0 9.31 2.28 -2 -11 0 7.60 3.12 2 11 0 6.72 2.82 -11 2 0 6.15 1.74 2 11 0 9.74 3.18 11 -2 0 9.66 1.82 -11 2 0 9.39 2.65 11 -2 0 5.65 2.56 11 -3 0 10.11 1.80 -11 3 0 12.92 2.49 3 11 0 11.27 3.24 3 11 0 11.80 3.18 11 -3 0 9.67 3.37 11 -3 0 18.40 2.81 -11 3 0 9.15 2.91 -11 3 0 11.22 2.41 -3 -11 0 12.03 3.31 11 -4 0 48.09 4.47 4 11 0 51.43 5.74 -11 4 0 48.58 4.80 -11 4 0 52.92 5.56 -4 -11 0 44.13 6.13 -11 4 0 51.98 4.66 4 11 0 49.55 5.81 11 -4 0 49.65 4.16 11 -5 0 5.70 1.76 -11 5 0 7.70 2.29 11 -5 0 6.85 2.01 11 -5 0 5.59 3.15 5 11 0 4.30 2.96 -11 5 0 4.20 2.19 5 11 0 7.48 3.25 -11 5 0 8.62 3.12 -5 -11 0 6.38 3.19 -11 6 0 63.21 6.76 11 -6 0 59.10 6.89 11 -6 0 71.70 5.51 -11 6 0 65.38 6.40 6 11 0 64.85 7.03 6 11 0 64.99 7.06 -11 6 0 54.14 5.64 -6 -11 0 66.96 7.02 11 -6 0 63.51 5.54 -7 -11 0 1.75 0.98 11 -7 0 -1.21 2.20 -11 7 0 -0.13 2.11 7 11 0 -0.06 2.88 7 11 0 -0.92 4.00 -7 -11 0 3.38 3.15 11 -7 0 1.38 3.07 -11 7 0 4.82 3.62 -11 8 0 77.89 7.77 11 -8 0 61.41 7.29 -8 -11 0 63.24 7.28 -11 8 0 58.04 6.02 8 11 0 63.88 7.59 11 -8 0 60.25 6.18 11 -9 0 -1.93 3.42 -9 -11 0 4.14 3.36 -9 -11 0 -1.71 2.18 -11 9 0 -3.92 3.24 11 -9 0 -2.87 2.68 -11 9 0 -5.12 2.67 9 11 0 -0.35 3.37 -10 -11 0 36.25 6.26 -11 10 0 34.87 4.90 10 11 0 34.60 5.72 11 -10 0 39.97 6.58 -11 10 0 27.63 5.41 11 -10 0 36.02 5.81 -11 -11 0 -0.96 4.16 11 -11 0 -5.11 3.98 -11 -11 0 -1.31 4.49 11 -11 0 -2.35 4.30 -11 11 0 -2.20 3.49 -11 11 0 -2.45 4.11 11 11 0 2.74 4.16 -10 12 0 2.34 3.99 10 -12 0 -1.46 3.71 -10 12 0 -5.26 4.48 10 -12 0 -1.09 4.43 -12 -10 0 -6.27 3.51 -12 -10 0 -2.23 4.16 -12 -9 0 62.03 7.95 9 -12 0 60.76 7.81 -9 12 0 62.43 8.17 9 -12 0 66.38 7.55 -9 12 0 70.35 7.35 -12 -9 0 68.13 7.54 -12 -9 0 61.19 7.45 8 -12 0 -0.55 3.22 -12 -8 0 -1.25 3.76 -8 12 0 -0.06 3.46 -8 12 0 1.75 3.32 -12 -8 0 -0.83 3.18 -12 -8 0 -3.82 3.10 -12 -8 0 3.70 3.64 -12 -7 0 28.40 4.69 -12 -7 0 28.36 4.26 -7 12 0 26.09 4.86 7 -12 0 28.51 4.78 7 -12 0 32.15 5.26 -7 12 0 24.90 4.28 -12 -6 0 7.46 2.91 -12 -6 0 13.67 3.67 6 -12 0 9.37 2.90 6 -12 0 10.18 3.68 -12 -6 0 8.90 3.61 -6 12 0 5.46 3.12 -6 12 0 8.92 3.26 -12 -5 0 41.10 5.65 -12 -5 0 36.43 4.92 -5 12 0 40.02 5.94 5 -12 0 36.64 4.47 -5 12 0 39.56 5.84 12 5 0 39.15 5.82 5 -12 0 37.81 5.90 -12 -5 0 32.37 4.38 -12 -5 0 35.27 5.56 -12 -4 0 34.55 5.06 -4 12 0 36.80 5.77 -12 -4 0 29.95 4.37 -12 -4 0 35.19 4.06 4 -12 0 32.63 4.89 -4 12 0 30.22 3.39 -4 12 0 32.51 5.39 -12 -4 0 34.94 5.25 12 4 0 29.97 4.86 -12 -3 0 23.13 3.93 -12 -3 0 22.85 3.64 -3 12 0 19.90 3.86 -3 12 0 24.08 4.30 12 3 0 23.60 4.29 -12 -3 0 25.28 3.36 3 -12 0 22.01 4.12 -12 -3 0 27.62 3.98 2 -12 0 59.24 6.77 12 2 0 67.23 6.72 -2 12 0 55.52 6.51 -12 -2 0 54.10 6.15 -12 -2 0 55.28 5.46 -2 12 0 58.71 6.34 1 -12 0 1.17 2.85 -12 -1 0 -0.02 2.50 12 1 0 1.65 2.67 -1 12 0 -0.22 2.57 -12 -1 0 0.28 1.70 -1 12 0 0.40 2.64 -12 -1 0 0.25 1.98 0 12 0 75.13 7.21 12 0 0 70.61 5.60 -12 0 0 77.90 6.97 -12 0 0 78.59 6.21 -12 0 0 83.91 5.75 0 12 0 74.73 6.87 12 0 0 74.38 7.47 0 -12 0 78.95 7.59 -12 1 0 -0.08 2.45 -1 -12 0 1.60 2.84 -12 1 0 0.39 1.62 12 -1 0 2.59 1.53 -12 1 0 -1.64 1.87 1 12 0 -0.39 2.91 1 12 0 1.53 2.83 12 -1 0 0.69 2.60 -12 2 0 53.51 5.87 12 -2 0 63.67 5.37 2 12 0 52.35 6.13 -12 2 0 59.38 5.37 12 -2 0 62.94 4.94 12 -2 0 60.87 6.84 -2 -12 0 68.21 7.09 2 12 0 49.66 6.35 12 -3 0 20.92 4.22 12 -3 0 22.20 3.00 -12 3 0 25.18 3.93 -12 3 0 28.03 4.47 -12 3 0 25.13 3.75 3 12 0 20.53 4.20 -3 -12 0 21.41 4.19 12 -3 0 26.68 3.68 3 12 0 25.33 4.46 12 -4 0 28.18 4.04 -12 4 0 39.25 5.81 4 12 0 35.95 5.20 -12 4 0 37.61 4.60 4 12 0 36.22 5.94 -12 4 0 31.34 4.52 -4 -12 0 40.90 6.13 12 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36.80 6.11 13 -9 0 7.46 3.51 -13 9 0 -2.25 3.45 -13 9 0 1.13 4.51 13 -9 0 0.52 4.85 9 13 0 9.84 4.94 -9 -13 0 4.55 4.86 -7 14 0 35.53 6.35 -14 -7 0 25.62 5.23 -14 -7 0 28.72 5.45 -14 -7 0 24.50 4.84 7 -14 0 24.72 5.62 -7 14 0 48.62 7.79 6 -14 0 9.01 4.26 -6 14 0 3.45 4.40 -6 14 0 3.26 4.52 -14 -6 0 8.13 3.91 -14 -6 0 8.55 4.38 -14 -6 0 4.86 3.61 -14 -5 0 17.69 4.41 -5 14 0 24.04 5.22 5 -14 0 22.88 5.00 -14 -5 0 19.88 4.11 -5 14 0 26.08 5.81 14 5 0 14.60 4.60 -14 -4 0 55.21 6.11 4 -14 0 49.29 7.61 14 4 0 44.77 7.39 -4 14 0 44.51 7.36 -14 -4 0 50.43 7.07 -4 14 0 47.64 7.64 -14 -4 0 47.59 6.53 14 3 0 9.97 4.43 -3 14 0 9.98 4.31 -14 -3 0 20.15 4.10 -14 -3 0 14.09 4.27 -14 -3 0 15.91 3.33 -3 14 0 18.77 4.87 3 -14 0 13.97 4.21 -14 -2 0 64.91 6.19 2 -14 0 67.43 8.33 -2 14 0 54.15 7.58 -14 -2 0 72.69 7.48 14 2 0 75.83 8.72 -2 14 0 57.39 7.83 -14 -2 0 67.83 6.70 14 1 0 4.65 3.99 -14 -1 0 2.31 3.06 -14 -1 0 1.88 2.94 1 -14 0 -5.21 3.19 -1 14 0 3.94 3.39 -1 14 0 6.19 3.78 14 0 0 62.32 8.06 -14 0 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6.27 -4 -3 28 13.68 3.17 -3 4 28 12.32 2.22 -4 -3 28 10.21 3.42 2 -4 -28 50.65 7.32 -2 4 -28 50.22 5.02 4 2 -28 50.37 7.16 -4 -2 -28 55.18 7.60 -2 4 -28 53.11 6.89 -4 -2 28 57.16 5.56 4 2 28 53.87 7.73 4 2 28 56.03 5.14 -2 4 28 51.97 3.51 -4 -2 28 58.76 5.67 2 -4 28 48.13 4.83 2 -4 28 56.85 6.64 -4 -2 28 52.15 6.13 -2 4 28 48.21 6.20 4 1 -28 -2.05 2.87 -1 4 -28 1.63 2.22 -4 -1 -28 2.01 4.06 -1 4 -28 -1.92 3.00 4 1 28 2.75 1.91 -4 -1 28 1.12 2.10 1 -4 28 0.58 2.15 -1 4 28 0.16 2.73 1 -4 28 1.29 3.18 4 1 28 1.31 3.36 -4 -1 28 2.38 2.43 -1 4 28 2.44 2.83 -4 -1 28 1.08 3.23 0 4 -28 76.37 7.38 4 0 -28 68.20 9.76 0 4 -28 64.85 5.76 -4 0 28 75.06 7.09 -4 0 28 71.56 6.01 0 -4 28 68.89 6.85 -4 0 28 59.45 5.67 0 -4 28 69.29 5.90 0 4 28 62.20 6.89 0 4 28 63.30 6.50 4 0 28 61.40 7.41 4 0 28 56.68 5.07 1 4 -28 -1.09 2.95 1 4 -28 -0.12 2.01 4 -1 -28 5.49 6.17 -4 1 28 -1.50 2.91 4 -1 28 -1.43 1.58 -4 1 28 -0.97 1.93 1 4 28 2.42 2.47 -1 -4 28 0.54 2.48 1 4 28 0.08 2.91 4 -1 28 -2.12 3.12 -4 1 28 -1.14 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49.00 7.85 5 3 -28 50.36 8.70 -3 5 -28 52.15 5.24 3 -5 -28 47.30 6.10 3 -5 28 42.61 6.84 -5 -3 28 47.11 6.12 -3 5 28 41.94 4.19 -5 -3 28 50.64 5.94 -5 -3 28 44.13 5.26 3 -5 28 39.03 4.00 5 3 28 42.97 5.06 5 3 28 46.65 6.99 -3 5 28 33.49 5.97 2 -5 -28 15.66 3.94 -5 -2 -28 18.38 5.15 -2 5 -28 18.14 3.22 -2 5 -28 16.45 4.33 2 -5 -28 16.65 4.70 2 -5 28 22.59 5.10 -2 5 28 16.46 4.14 5 2 28 15.53 4.40 -5 -2 28 20.88 3.75 2 -5 28 21.13 2.94 -5 -2 28 18.27 3.89 -2 5 28 21.89 2.18 5 2 28 19.03 3.00 -5 -2 28 20.17 3.25 5 1 -28 47.19 7.59 -1 5 -28 44.21 6.72 1 -5 -28 43.24 7.03 -5 -1 -28 58.42 7.98 -1 5 -28 46.81 5.81 -5 -1 28 72.64 7.01 1 -5 28 55.31 6.86 5 1 28 56.24 4.74 1 -5 28 61.88 5.25 -5 -1 28 56.90 5.54 -1 5 28 50.43 6.25 5 1 28 60.25 7.24 -5 -1 28 49.27 5.39 0 5 -28 0.62 3.28 0 -5 -28 -0.45 3.36 -5 0 -28 3.29 3.71 5 0 -28 -3.56 3.19 0 5 -28 -2.35 2.46 0 -5 28 0.48 2.58 -5 0 28 -0.47 2.23 0 -5 28 -1.34 3.01 -5 0 28 -0.66 3.01 0 5 28 1.50 2.85 5 0 28 -2.69 3.25 -5 0 28 -1.66 2.19 1 5 -28 57.18 5.73 -1 -5 -28 63.86 7.73 1 5 -28 65.00 7.14 5 -1 -28 64.67 7.69 -5 1 -28 62.36 7.95 1 5 28 40.34 6.55 1 5 28 51.22 6.21 5 -1 28 45.12 3.61 -1 -5 28 57.46 6.33 -1 -5 28 47.64 5.65 -5 1 28 53.35 5.30 -5 1 28 52.83 5.35 -5 1 28 58.53 6.63 5 -1 28 51.31 7.01 2 5 -28 21.59 4.35 -2 -5 -28 21.05 4.71 -5 2 -28 16.71 4.65 5 -2 -28 22.57 4.82 2 5 -28 17.78 3.60 2 5 28 14.67 3.48 2 5 28 7.16 3.97 5 -2 28 14.49 4.33 -2 -5 28 12.70 3.31 -5 2 28 10.03 2.69 -2 -5 28 22.26 3.86 -5 3 -28 43.07 3.43 5 -3 -28 32.00 5.84 -3 -5 -28 45.89 7.12 -5 3 -28 42.84 6.40 5 -3 -28 38.94 5.06 3 5 -28 33.90 4.94 3 5 -28 52.77 6.99 3 5 28 39.42 5.88 -3 -5 28 48.21 6.10 5 -3 28 48.19 7.11 3 5 28 52.70 5.96 -3 -5 28 49.40 5.69 -5 3 28 53.60 6.81 -5 3 28 51.57 5.01 5 -4 -28 19.13 3.33 4 5 -28 23.86 4.57 -4 -5 -28 20.08 5.18 -5 4 -28 21.37 4.88 -5 4 -28 23.07 3.18 5 -4 -28 20.87 5.09 -4 -5 28 18.90 4.18 4 5 28 18.15 4.78 -5 4 28 20.44 4.66 -4 -5 28 18.96 3.72 5 -4 28 24.32 5.01 -5 4 28 20.92 3.36 4 5 28 18.73 3.89 5 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4.80 6 3 28 42.97 7.01 -6 -3 28 27.86 5.04 -6 -2 -28 13.02 4.53 6 2 -28 17.44 4.25 -2 6 -28 11.85 4.13 2 -6 -28 15.96 3.72 -2 6 -28 12.43 3.35 2 -6 -28 9.91 4.31 6 2 28 8.55 4.13 -6 -2 28 9.82 3.91 -6 -2 28 2.42 2.94 6 2 28 6.93 2.35 2 -6 28 10.03 3.89 -2 6 28 5.91 3.75 2 -6 28 7.56 2.40 -6 -2 28 6.88 2.57 1 -6 -28 2.95 4.08 -1 6 -28 7.49 3.01 -6 -1 -28 2.73 4.26 6 1 -28 0.11 3.54 -1 6 -28 2.82 3.47 1 -6 -28 -0.14 3.21 6 1 28 6.81 3.95 -6 -1 28 2.94 2.22 1 -6 28 1.46 5.31 -1 6 28 6.07 3.66 1 -6 28 6.51 2.51 -6 -1 28 4.42 3.20 -6 -1 28 -0.29 2.64 0 -6 -28 45.32 6.70 0 6 -28 43.84 6.10 -6 0 -28 37.27 6.18 0 6 -28 32.05 4.51 6 0 -28 33.31 5.72 0 -6 -28 41.28 6.79 0 -6 28 36.07 4.95 -6 0 28 27.96 4.87 0 6 28 37.81 5.93 -6 0 28 32.87 5.28 0 -6 28 34.16 5.13 6 0 28 33.65 5.73 6 -1 -28 2.75 2.11 -1 -6 -28 0.65 3.49 1 6 -28 0.19 2.91 6 -1 -28 3.67 3.92 -6 1 -28 8.77 4.70 1 6 -28 2.84 3.24 -1 -6 28 6.58 3.27 -6 1 28 0.10 3.62 -6 1 28 5.31 2.73 -1 -6 28 1.73 2.62 6 -1 28 5.27 3.88 1 6 28 2.08 3.10 2 6 -28 10.51 3.66 2 6 -28 8.55 3.55 6 -2 -28 11.12 4.40 -2 -6 -28 8.92 4.16 -6 2 -28 7.97 4.28 6 -2 -28 5.64 2.25 -2 -6 28 11.00 3.17 2 6 28 10.53 3.32 -6 2 28 10.68 2.90 -2 -6 28 15.24 3.60 -6 2 28 8.02 4.30 6 -2 28 15.87 4.51 -3 -6 -28 27.64 5.30 -6 3 -28 35.74 6.24 6 -3 -28 38.23 4.51 6 -3 -28 30.02 5.70 3 6 -28 34.99 5.02 -3 -6 28 38.89 5.75 -3 -6 28 40.33 6.02 3 6 28 40.98 6.02 6 -3 28 30.14 5.22 -6 3 28 31.16 4.95 -6 3 28 31.01 5.21 6 -4 -28 10.24 4.67 6 -4 -28 10.09 2.85 -4 -6 -28 11.16 4.64 -6 4 -28 6.42 4.11 -6 4 -28 14.77 3.23 4 6 -28 13.53 4.20 4 6 -28 12.04 3.94 4 6 28 22.56 3.91 -4 -6 28 21.89 4.45 -6 4 28 17.60 4.63 -4 -6 28 22.00 3.89 -6 4 28 17.37 3.49 6 -4 28 12.50 4.40 -5 -6 -28 47.74 8.24 5 6 -28 52.28 7.02 6 -5 -28 39.68 5.81 -6 5 -28 61.33 8.25 6 -5 -28 51.92 8.24 -6 5 -28 47.58 5.77 -6 5 28 37.60 6.00 -5 -6 28 51.19 6.83 6 -5 28 42.44 6.48 5 6 28 43.67 6.27 5 6 28 31.75 6.18 -5 -6 28 43.82 6.16 -6 5 28 41.56 5.71 -6 6 -28 9.15 3.51 -6 -6 -28 13.69 5.67 6 -6 -28 5.26 4.87 -6 6 -28 11.14 4.86 -6 -6 28 11.76 3.90 -6 6 28 13.24 3.42 6 -6 28 11.17 4.74 -6 -6 28 2.73 3.18 6 6 28 10.63 3.73 6 6 28 3.53 4.67 -6 6 28 6.18 4.77 -6 7 -28 47.75 7.29 -7 -6 -28 55.99 9.53 6 -7 -28 47.16 7.53 7 6 -28 40.43 6.39 -6 7 -28 58.07 7.17 -6 7 28 54.82 8.24 -6 7 28 52.73 6.46 7 6 28 39.06 6.59 6 -7 28 59.43 8.94 -7 -6 28 58.87 7.71 7 6 28 51.93 7.58 5 -7 -28 -0.73 3.11 7 5 -28 -0.41 4.12 -7 -5 -28 0.15 4.33 5 -7 -28 1.16 4.54 -5 7 -28 1.40 3.70 -5 7 -28 6.63 4.27 -7 -5 28 1.94 4.07 -5 7 28 1.18 4.39 7 5 28 2.62 4.78 7 5 28 1.10 3.13 5 -7 28 6.12 4.47 -7 -5 28 -0.79 4.04 -5 7 28 0.02 2.79 -4 7 -28 29.61 4.58 4 -7 -28 25.44 4.53 7 4 -28 33.41 5.63 -7 -4 -28 23.66 5.82 -4 7 -28 29.33 6.42 4 -7 -28 24.39 5.85 4 -7 28 25.67 5.09 7 4 28 16.66 5.26 -4 7 28 24.54 5.38 7 4 28 22.62 3.66 -7 -4 28 24.38 5.08 -4 7 28 24.20 4.37 3 -7 -28 11.60 3.83 7 3 -28 7.84 4.12 -7 -3 -28 5.68 5.13 -3 7 -28 8.88 3.60 -3 7 -28 15.45 4.53 3 -7 -28 13.91 4.72 3 -7 28 3.50 3.95 -3 7 28 9.44 4.08 -7 -3 28 4.62 3.98 7 3 28 6.18 4.66 -7 -3 28 6.46 3.46 -2 7 -28 11.90 4.17 2 -7 -28 11.00 4.58 -2 7 -28 8.04 3.64 2 -7 -28 10.20 4.09 7 2 -28 17.24 4.86 -7 -2 -28 16.86 5.48 2 -7 28 13.06 2.77 7 2 28 10.55 4.41 -7 -2 28 13.90 4.67 2 -7 28 13.32 4.60 -7 -2 28 11.27 3.65 -2 7 28 15.21 4.39 1 -7 -28 0.16 3.51 -1 7 -28 6.10 3.29 1 -7 -28 -4.20 3.98 -7 -1 -28 4.03 4.46 7 1 -28 4.16 4.30 -1 7 -28 4.50 3.80 -7 -1 28 7.79 4.17 7 1 28 0.84 3.69 1 -7 28 3.63 2.43 -1 7 28 2.84 3.44 -7 -1 28 5.96 3.22 1 -7 28 -3.04 3.80 7 0 -28 5.94 4.15 -7 0 -28 4.45 4.62 0 -7 -28 4.27 3.89 0 7 -28 3.92 3.63 0 -7 -28 4.62 4.40 0 7 -28 10.65 3.44 -7 0 28 2.66 2.70 0 -7 28 -1.02 6.08 -7 0 28 7.50 4.43 7 0 28 2.41 3.87 0 7 28 3.67 3.42 0 -7 28 4.76 2.92 7 -1 -28 2.78 4.24 -7 1 -28 0.32 4.14 -1 -7 -28 7.21 4.34 1 7 -28 2.71 3.51 1 7 -28 4.67 3.50 -1 -7 -28 0.71 3.80 7 -1 28 7.79 3.88 -1 -7 28 5.77 3.06 -1 -7 28 -3.91 3.32 -7 1 28 1.55 2.91 -7 1 28 3.62 3.86 -7 2 -28 11.28 4.96 -2 -7 -28 10.78 4.42 2 7 -28 12.07 3.86 7 -2 -28 11.93 4.75 -2 -7 -28 9.79 4.62 2 7 -28 7.44 3.81 7 -2 28 13.97 4.51 2 7 28 12.87 4.20 -2 -7 28 6.97 3.74 -7 2 28 14.27 3.56 -7 2 28 8.97 4.37 -2 -7 28 13.55 3.60 3 7 -28 5.74 3.84 -7 3 -28 4.69 4.48 -3 -7 -28 13.82 4.86 7 -3 -28 11.38 4.97 3 7 -28 10.06 3.62 -7 3 28 7.55 4.45 3 7 28 7.56 3.99 -3 -7 28 5.47 3.70 -7 3 28 14.38 3.48 7 -3 28 11.31 4.79 -3 -7 28 10.27 3.62 4 7 -28 20.75 4.69 7 -4 -28 20.10 5.59 -4 -7 -28 21.48 5.61 -7 4 -28 27.36 5.91 4 7 -28 16.42 4.38 4 7 28 17.94 4.58 -4 -7 28 22.41 4.37 -7 4 28 35.24 5.83 -4 -7 28 23.07 4.42 7 -4 28 30.73 5.85 -7 4 28 23.71 5.82 7 -5 -28 -2.26 4.21 5 7 -28 3.35 3.76 -7 5 -28 -3.24 4.27 -5 -7 -28 1.14 4.70 5 7 -28 -0.06 3.96 5 7 28 -0.08 3.76 7 -5 28 0.12 4.80 -7 5 28 -1.35 3.23 -7 5 28 3.23 4.39 -5 -7 28 6.41 3.45 -5 -7 28 0.20 3.87 7 -6 -28 58.75 9.17 -7 6 -28 54.14 7.98 -6 -7 -28 55.93 9.09 -7 6 -28 43.24 7.18 -6 -7 28 37.46 6.28 -7 6 28 49.15 6.67 7 -6 28 43.23 6.84 -6 -7 28 64.46 7.01 -7 6 28 64.61 8.51 6 7 28 48.98 7.45 5 -8 -28 42.62 7.00 -5 8 -28 47.52 7.36 -8 -5 -28 37.91 7.12 8 5 -28 62.11 8.29 -5 8 -28 40.96 6.55 5 -8 -28 45.44 6.86 -5 8 28 36.94 6.47 -8 -5 28 37.44 6.33 -8 -5 28 61.41 8.17 8 5 28 42.89 7.11 5 -8 28 35.43 6.55 4 -8 -28 2.15 3.61 4 -8 -28 0.95 4.68 -8 -4 -28 -8.54 4.68 -4 8 -28 3.95 4.14 -4 8 -28 7.21 3.86 8 4 -28 4.89 4.42 4 -8 28 -0.60 4.58 -8 -4 28 4.99 4.54 -4 8 28 4.71 4.44 8 4 28 4.61 5.01 -8 -4 28 -0.72 4.04 3 -8 -28 23.23 4.60 -8 -3 -28 16.04 5.66 -3 8 -28 19.98 4.55 8 3 -28 17.52 4.89 3 -8 -28 15.93 5.16 -3 8 -28 22.48 4.72 -8 -3 28 8.17 4.78 -8 -3 28 18.03 4.62 3 -8 28 16.84 5.07 -3 8 28 13.80 5.04 8 3 28 14.63 5.21 2 -8 -28 3.09 4.41 -8 -2 -28 0.69 4.74 -2 8 -28 -3.02 3.37 2 -8 -28 4.28 3.67 -2 8 -28 1.14 3.66 8 2 -28 0.76 4.56 8 2 28 4.42 4.66 2 -8 28 2.53 4.38 -8 -2 28 0.91 4.49 -2 8 28 3.20 4.10 1 -8 -28 8.10 4.34 1 -8 -28 6.17 4.82 8 1 -28 8.86 4.67 -1 8 -28 11.34 3.84 -8 -1 -28 3.39 4.87 -1 8 -28 4.04 3.66 1 -8 28 11.65 4.26 -8 -1 28 3.58 3.45 -1 8 28 2.27 3.58 8 1 28 7.31 4.71 1 -8 28 1.63 2.63 -8 -1 28 6.02 3.92 0 8 -28 2.57 3.71 0 -8 -28 13.96 4.53 -8 0 -28 5.20 4.85 0 -8 -28 15.76 5.12 0 8 -28 9.23 3.84 8 0 -28 5.73 4.77 -8 0 28 7.14 4.37 0 8 28 12.79 4.11 -8 0 28 11.26 3.74 8 0 28 9.92 4.78 0 -8 28 10.63 4.22 0 -8 28 9.78 3.05 1 8 -28 -1.57 3.53 8 -1 -28 6.39 5.24 1 8 -28 5.51 3.73 -1 -8 -28 6.69 4.57 -1 -8 -28 3.89 4.57 -8 1 -28 5.10 4.61 1 8 28 5.55 4.01 -8 1 28 1.53 4.39 -1 -8 28 8.64 3.93 -1 -8 28 0.72 3.08 -8 1 28 7.23 3.33 8 -1 28 7.67 4.77 2 8 -28 5.37 3.96 -2 -8 -28 4.34 4.12 -8 2 -28 4.08 4.82 2 8 -28 -2.11 3.42 -2 -8 -28 -3.53 4.01 8 -2 -28 -2.48 4.10 -2 -8 28 0.03 2.93 -8 2 28 2.82 3.28 8 -2 28 -3.95 4.05 -8 2 28 -2.19 4.60 2 8 28 3.94 3.82 3 8 -28 17.76 4.35 -3 -8 -28 21.73 5.36 -8 3 -28 19.96 5.74 3 8 -28 12.56 4.97 8 -3 -28 6.74 5.38 -3 -8 -28 19.36 5.52 8 -3 28 15.01 4.99 -3 -8 28 24.98 6.96 -8 3 28 24.92 4.35 3 8 28 23.56 5.03 -8 3 28 13.48 5.00 -3 -8 28 19.23 4.36 8 -4 -28 -8.27 4.14 4 8 -28 1.87 3.66 -4 -8 -28 2.93 5.00 4 8 -28 4.99 3.99 -4 -8 -28 8.24 4.40 -8 4 -28 9.03 5.02 -8 4 28 6.37 3.56 -4 -8 28 -0.61 3.59 -4 -8 28 -0.68 3.56 -8 4 28 12.36 5.12 8 -4 28 2.20 4.83 4 8 28 2.43 3.97 8 -5 -28 49.79 8.62 -8 5 -28 43.17 7.04 -5 -8 -28 45.45 7.32 -5 -8 -28 42.85 7.60 5 8 -28 55.97 7.90 5 8 -28 40.12 6.98 8 -5 28 30.49 6.55 -5 -8 28 47.36 7.13 -8 5 28 42.08 7.31 -8 5 28 49.48 7.10 5 8 28 48.96 7.41 -5 -8 28 53.13 7.18 -9 -3 -28 -7.82 5.15 3 -9 -28 2.07 4.68 -3 9 -28 -4.50 3.95 -3 9 -28 -1.59 4.27 3 -9 -28 1.07 4.33 9 3 -28 2.17 4.88 9 3 28 -4.31 4.71 -9 -3 28 3.52 4.33 -3 9 28 3.69 4.59 3 -9 28 6.38 4.94 -9 -3 28 4.36 4.10 -2 9 -28 15.40 4.58 -9 -2 -28 11.51 5.79 9 2 -28 8.55 4.76 -2 9 -28 6.48 4.35 2 -9 -28 8.37 4.81 2 -9 -28 10.05 4.46 2 -9 28 8.85 5.10 -9 -2 28 14.40 5.05 -2 9 28 8.51 4.42 9 2 28 9.34 4.91 -9 -2 28 9.72 4.15 -1 9 -28 -0.64 5.86 -9 -1 -28 -4.26 4.89 9 1 -28 6.15 4.51 1 -9 -28 7.30 4.55 1 -9 -28 6.53 4.30 -1 9 -28 2.71 3.91 -1 9 28 -1.71 3.99 9 1 28 2.01 4.57 1 -9 28 2.55 2.91 1 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33.30 6.21 -5 -2 33 35.93 6.02 -5 -2 33 38.14 5.95 2 -5 33 32.65 6.13 -2 5 33 34.63 5.68 5 2 33 34.29 6.59 -1 5 -33 27.27 5.76 1 -5 -33 22.65 6.12 -5 -1 -33 22.42 6.19 5 1 -33 29.55 6.35 -1 5 33 23.27 5.06 5 1 33 17.79 5.87 1 -5 33 25.18 5.71 -5 -1 33 23.02 5.35 -5 -1 33 21.50 3.91 0 5 -33 -0.18 4.55 5 0 -33 4.16 4.74 0 -5 -33 14.07 5.35 -5 0 -33 8.06 5.71 5 0 33 5.73 4.86 -5 0 33 10.89 5.06 0 5 33 2.80 4.24 0 -5 33 10.09 4.69 0 -5 33 9.60 3.64 -1 -5 -33 17.73 5.98 5 -1 -33 11.52 5.77 1 5 -33 21.81 5.54 -5 1 -33 30.30 6.90 -5 1 33 27.60 5.65 5 -1 33 29.80 6.36 1 5 33 23.19 4.85 -1 -5 33 30.25 5.32 -1 -5 33 22.42 4.62 -5 2 -33 28.36 6.43 5 -2 -33 23.89 6.52 -2 -5 -33 32.80 6.61 2 5 -33 24.43 5.95 -2 -5 33 36.56 5.71 -5 2 33 36.08 6.18 -2 -5 33 25.31 5.54 5 -2 33 28.89 6.08 0 0 -34 4.42 4.28 0 0 34 1.27 4.14 0 0 34 3.32 3.42 1 0 -34 51.56 8.71 0 -1 -34 59.73 8.68 -1 0 -34 52.47 8.96 0 1 -34 53.17 8.76 1 0 34 56.76 6.49 1 0 34 64.81 8.17 0 1 34 56.51 8.04 -1 0 34 62.72 9.50 0 -1 34 59.04 6.95 0 1 34 56.09 6.77 0 -1 34 56.15 8.37 -1 0 34 48.42 7.15 -1 1 -34 0.52 4.45 1 1 -34 0.34 5.04 1 -1 -34 2.53 4.87 -1 -1 -34 9.60 5.14 1 1 34 -2.94 3.89 1 -1 34 -5.47 2.96 -1 -1 34 6.92 3.78 1 -1 34 -1.80 4.06 1 1 34 -1.45 3.18 -1 1 34 -2.16 3.31 2 1 -34 44.84 7.33 -1 2 -34 40.20 6.77 -2 -1 -34 40.93 7.00 1 -2 -34 50.72 8.61 -2 -1 34 52.42 7.80 1 -2 34 49.63 8.19 2 1 34 65.42 8.10 1 -2 34 46.12 5.97 -1 2 34 36.96 9.66 2 1 34 46.36 6.22 -1 2 34 42.58 6.64 0 -2 -34 4.78 5.13 2 0 -34 1.31 4.70 0 2 -34 -5.32 4.59 -2 0 -34 5.35 4.88 0 2 34 1.24 4.34 -2 0 34 2.42 3.94 0 -2 34 5.82 3.53 2 0 34 -2.57 4.41 -2 0 34 0.94 3.84 0 2 34 -1.96 3.60 2 0 34 0.33 2.97 0 -2 34 -1.82 4.29 -2 1 -34 63.36 8.49 1 2 -34 44.82 6.92 2 -1 -34 45.44 7.26 -1 -2 -34 45.15 7.44 -2 1 34 46.01 7.48 1 2 34 33.34 6.21 2 -1 34 38.90 5.80 2 -1 34 48.93 6.94 1 2 34 49.51 6.75 -1 -2 34 36.88 7.17 -1 -2 34 49.48 6.65 -2 1 34 46.96 7.40 -2 2 -34 9.59 5.24 -2 -2 -34 4.89 5.18 2 -2 -34 -2.95 4.79 2 2 -34 1.60 4.76 -2 2 34 -3.76 4.11 2 2 34 1.82 3.36 -2 2 34 1.61 3.85 2 2 34 5.53 4.37 2 -2 34 3.04 4.46 -2 -2 34 -3.31 4.22 3 2 -34 69.25 9.55 -2 3 -34 54.66 8.98 2 -3 -34 46.15 7.49 -3 -2 -34 51.60 8.25 2 -3 34 48.19 8.19 3 2 34 61.71 9.13 -3 -2 34 60.13 7.89 3 2 34 42.08 6.06 -3 -2 34 51.54 7.58 -2 3 34 50.09 7.47 3 1 -34 2.98 5.17 -1 3 -34 11.21 5.28 -3 -1 -34 5.18 5.14 1 -3 -34 -3.19 4.98 1 -3 34 3.52 3.38 -3 -1 34 5.57 4.14 -3 -1 34 7.22 4.08 3 1 34 7.56 4.97 1 -3 34 4.69 4.46 -1 3 34 2.44 4.12 -1 3 34 4.42 4.32 -3 0 -34 53.94 8.92 3 0 -34 54.26 8.94 0 3 -34 40.53 6.72 0 -3 -34 37.93 6.81 -3 0 34 49.61 7.41 0 3 34 33.42 8.30 3 0 34 40.88 6.91 0 3 34 39.47 6.31 -3 0 34 38.95 5.70 0 -3 34 36.86 6.15 0 -3 34 45.06 6.34 1 3 -34 0.16 4.41 3 -1 -34 2.23 4.85 -3 1 -34 11.20 5.54 -1 -3 -34 6.08 5.03 3 -1 34 -1.20 4.91 1 3 34 4.83 3.80 -1 -3 34 7.96 4.58 -3 1 34 4.96 3.93 1 3 34 11.91 4.77 -3 1 34 5.35 4.56 -1 -3 34 2.43 3.73 3 -2 -34 41.45 7.24 2 3 -34 58.20 8.56 -3 2 -34 47.05 7.50 -2 -3 -34 64.74 9.35 2 3 34 52.84 8.47 2 3 34 41.45 5.79 -3 2 34 56.13 8.10 -3 2 34 51.59 7.45 3 -2 34 51.22 7.55 -2 -3 34 61.61 9.59 -3 3 -34 -1.50 5.34 3 3 -34 4.21 4.93 -3 -3 -34 6.94 5.11 3 -3 -34 8.96 5.25 3 3 34 0.81 3.40 -3 -3 34 5.53 4.35 -3 -3 34 5.43 4.25 3 -3 34 2.57 4.96 3 3 34 -2.46 5.02 -3 3 34 3.46 4.56 -2 4 -34 2.17 4.57 2 -4 -34 0.86 4.81 4 2 -34 1.87 5.24 -4 -2 -34 -0.16 5.62 -4 -2 34 -2.17 4.27 -4 -2 34 1.47 4.21 2 -4 34 6.73 4.90 -2 4 34 10.04 4.98 4 2 34 3.64 5.14 -4 -1 -34 23.96 6.28 -1 4 -34 34.62 6.60 4 1 -34 25.91 6.43 1 -4 -34 25.76 6.66 -4 -1 34 24.54 5.55 -4 -1 34 40.11 5.35 -1 4 34 32.29 5.61 1 -4 34 38.53 5.98 0 4 -34 0.28 4.57 -4 0 -34 3.39 5.32 4 0 -34 2.84 5.11 0 -4 -34 8.63 5.66 -4 0 34 -0.80 3.88 0 4 34 -0.46 4.24 -4 0 34 -4.43 3.98 4 0 34 5.98 5.26 0 4 34 0.75 3.95 0 -4 34 2.26 4.40 0 -4 34 -3.84 3.36 -1 -4 -34 30.57 6.89 1 4 -34 38.48 6.70 4 -1 -34 31.70 6.70 -4 1 -34 41.12 6.95 1 4 34 23.54 5.10 -1 -4 34 32.07 5.92 1 4 34 25.65 5.66 -1 -4 34 32.27 4.98 -4 1 34 36.72 6.13 -4 1 34 25.09 4.93 4 -1 34 31.56 6.25 -2 -4 -34 4.53 5.26 4 -2 -34 2.30 4.86 -4 2 -34 -1.14 5.31 2 4 -34 -0.34 4.86 -4 2 34 4.33 4.82 2 4 34 -6.86 3.48 2 4 34 3.05 4.84 -2 -4 34 -2.59 6.57 4 -2 34 3.84 5.19 -2 -4 34 4.66 4.58 0 0 -35 -0.35 4.77 0 0 35 0.16 4.40 0 0 35 -2.59 3.53 -1 0 -35 -6.35 4.88 0 -1 -35 2.73 5.12 1 0 -35 3.87 5.05 0 1 -35 5.75 5.02 -1 0 35 3.42 4.23 1 0 35 -4.20 3.42 0 -1 35 1.19 4.69 0 1 35 0.95 3.49 0 1 35 5.60 4.53 0 -1 35 1.78 3.47 1 0 35 2.32 4.62 -1 1 -35 6.61 4.77 1 1 -35 1.22 4.63 1 -1 -35 1.22 4.92 -1 -1 -35 7.61 5.85 -1 1 35 1.00 3.87 -1 1 35 1.38 4.38 -1 -1 35 6.47 4.13 1 -1 35 2.86 4.50 1 1 35 8.24 4.57 1 1 35 11.17 3.73 -1 -1 35 11.39 4.92 1 -2 -35 7.54 5.48 2 1 -35 3.45 5.21 -1 2 -35 9.30 5.23 -2 -1 -35 8.71 5.07 -2 -1 35 14.57 4.68 2 1 35 6.39 3.66 1 -2 35 8.88 4.96 -2 -1 35 -3.15 5.25 -1 2 35 8.06 4.69 2 1 35 5.79 4.91 -1 2 35 6.42 4.02 0 -2 -35 4.32 5.03 0 2 -35 4.02 4.57 2 0 -35 -3.02 4.71 -2 0 -35 1.71 4.95 2 0 35 7.06 4.87 0 -2 35 3.45 3.73 -2 0 35 1.64 4.24 0 2 35 8.52 4.77 -2 0 35 -4.15 4.14 0 -2 35 -0.60 4.55 -2 1 -35 7.70 5.13 2 -1 -35 3.72 5.44 1 2 -35 12.41 4.90 -1 -2 -35 9.77 5.25 1 2 35 9.70 4.77 -1 -2 35 4.72 4.77 2 -1 35 4.50 4.95 -2 1 35 5.33 4.19 -2 1 35 8.96 4.80 1 2 35 6.21 3.71 -1 -2 35 9.51 4.00 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 42559 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+3/4' 'y+1/2, -x+1/2, z+1/4' '-x+1/2, y+1/2, -z+3/4' 'x+1/2, -y+1/2, -z+1/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group U1 U 0.47085(2) 0.47085(2) 0.000000 0.01169(4) Uani 1 2 d S T P . . P1 P 0.46751(8) 0.69739(6) 0.00935(3) 0.01813(16) Uani 1 1 d . . . . . Si1 Si 0.56945(8) 0.81349(8) 0.05454(3) 0.0227(2) Uani 1 1 d . . . . . C1 C 0.3922(3) 0.3056(3) 0.06060(12) 0.0246(8) Uani 1 1 d . . . . . C2 C 0.3481(3) 0.4059(3) 0.07901(11) 0.0232(7) Uani 1 1 d . . . . . C3 C 0.4364(2) 0.4673(3) 0.10010(10) 0.0195(7) Uani 1 1 d . . . . . C4 C 0.5348(3) 0.4051(3) 0.09468(9) 0.0185(6) Uani 1 1 d . . . . . C5 C 0.5074(3) 0.3061(2) 0.06954(11) 0.0213(8) Uani 1 1 d . . . . . C6 C 0.3300(4) 0.2028(3) 0.04597(14) 0.0417(11) Uani 1 1 d . . . . . H6A H 0.338938 0.146326 0.071793 0.063 Uiso 1 1 calc R U . . . H6B H 0.359180 0.174644 0.014457 0.063 Uiso 1 1 calc R U . . . H6C H 0.251226 0.220433 0.042134 0.063 Uiso 1 1 calc R U . . . C7 C 0.2292(3) 0.4418(4) 0.08191(14) 0.0376(11) Uani 1 1 d . . . . . H7A H 0.210187 0.458544 0.116471 0.056 Uiso 1 1 calc R U . . . H7B H 0.181457 0.382105 0.069672 0.056 Uiso 1 1 calc R U . . . H7C H 0.218461 0.508027 0.061472 0.056 Uiso 1 1 calc R U . . . C8 C 0.4239(3) 0.5696(3) 0.13129(10) 0.0278(7) Uani 1 1 d . . . . . H8A H 0.398225 0.548975 0.164535 0.042 Uiso 1 1 calc R U . . . H8B H 0.369853 0.619337 0.115815 0.042 Uiso 1 1 calc R U . . . H8C H 0.495542 0.607369 0.133859 0.042 Uiso 1 1 calc R U . . . C9 C 0.6427(3) 0.4314(3) 0.11922(11) 0.0253(8) Uani 1 1 d . . . . . H9A H 0.633169 0.430282 0.155349 0.038 Uiso 1 1 calc R U . . . H9B H 0.667614 0.505014 0.108771 0.038 Uiso 1 1 calc R U . . . H9C H 0.698094 0.376067 0.109606 0.038 Uiso 1 1 calc R U . . . C10 C 0.5810(3) 0.2070(3) 0.06094(13) 0.0311(9) Uani 1 1 d . . . . . H10A H 0.556549 0.145611 0.082064 0.047 Uiso 1 1 calc R U . . . H10B H 0.657703 0.226245 0.069177 0.047 Uiso 1 1 calc R U . . . H10C H 0.576663 0.184713 0.026008 0.047 Uiso 1 1 calc R U . . . C11 C 0.6854(3) 0.7349(3) 0.08440(14) 0.0362(9) Uani 1 1 d . . . . . H11A H 0.747594 0.785094 0.090641 0.054 Uiso 1 1 calc R U . . . H11B H 0.709373 0.675118 0.062264 0.054 Uiso 1 1 calc R U . . . H11C H 0.659822 0.703347 0.115903 0.054 Uiso 1 1 calc R U . . . C12 C 0.6314(3) 0.9222(3) 0.01347(13) 0.0353(9) Uani 1 1 d . . . . . H12A H 0.672702 0.975387 0.033767 0.053 Uiso 1 1 calc R U . . . H12B H 0.572257 0.960835 -0.004439 0.053 Uiso 1 1 calc R U . . . H12C H 0.681650 0.887248 -0.010423 0.053 Uiso 1 1 calc R U . . . C13 C 0.4826(3) 0.8848(3) 0.10262(12) 0.0346(9) Uani 1 1 d . . . . . H13A H 0.528024 0.938998 0.120504 0.052 Uiso 1 1 calc R U . . . H13B H 0.453799 0.829933 0.126094 0.052 Uiso 1 1 calc R U . . . H13C H 0.420745 0.922808 0.086385 0.052 Uiso 1 1 calc R U . . . C14 C 0.3516(3) 0.7910(2) -0.00498(11) 0.0192(7) Uani 1 1 d . . . . . C15 C 0.3587(3) 0.8699(3) -0.04310(12) 0.0235(8) Uani 1 1 d . . . . . H15A H 0.424850 0.875697 -0.061987 0.028 Uiso 1 1 calc R U . . . C16 C 0.2703(3) 0.9396(3) -0.05359(13) 0.0308(9) Uani 1 1 d . . . . . H16A H 0.276177 0.991779 -0.079836 0.037 Uiso 1 1 calc R U . . . C17 C 0.1740(3) 0.9335(3) -0.02622(13) 0.0341(9) Uani 1 1 d . . . . . H17A H 0.113632 0.981294 -0.033470 0.041 Uiso 1 1 calc R U . . . C18 C 0.1663(3) 0.8575(3) 0.01177(12) 0.0319(9) Uani 1 1 d . . . . . H18A H 0.100570 0.853544 0.031083 0.038 Uiso 1 1 calc R U . . . C19 C 0.2538(3) 0.7867(3) 0.02200(11) 0.0254(8) Uani 1 1 d . . . . . H19A H 0.246662 0.734065 0.048032 0.030 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 U1 0.01107(5) 0.01107(5) 0.01293(7) -0.00042(5) 0.00042(5) -0.00079(7) P1 0.0221(4) 0.0128(3) 0.0194(4) -0.0009(3) -0.0063(4) 0.0006(4) Si1 0.0285(5) 0.0150(5) 0.0244(5) -0.0040(4) -0.0055(4) -0.0039(4) C1 0.031(2) 0.0201(18) 0.0227(17) 0.0061(14) 0.0095(15) -0.0078(16) C2 0.0207(18) 0.028(2) 0.0204(16) 0.0064(15) 0.0111(13) -0.0024(14) C3 0.0231(17) 0.0208(16) 0.0146(13) 0.0053(13) 0.0060(11) 0.0016(16) C4 0.0234(17) 0.0202(16) 0.0120(13) 0.0072(12) 0.0043(14) 0.0052(15) C5 0.029(2) 0.0150(15) 0.0202(16) 0.0097(12) 0.0111(13) 0.0028(14) C6 0.052(3) 0.028(2) 0.044(2) 0.0046(19) 0.011(2) -0.018(2) C7 0.0205(19) 0.053(3) 0.039(2) 0.0023(19) 0.0108(16) -0.0007(17) C8 0.036(2) 0.029(2) 0.0187(15) -0.0008(14) 0.0060(15) 0.0117(15) C9 0.0263(19) 0.032(2) 0.0171(15) 0.0049(14) 0.0008(14) 0.0093(15) C10 0.044(2) 0.0171(18) 0.0320(19) 0.0098(15) 0.0125(18) 0.0090(17) C11 0.034(2) 0.030(2) 0.045(2) -0.0020(17) -0.0186(18) -0.0086(17) C12 0.046(2) 0.0217(18) 0.038(2) -0.0044(16) 0.0018(17) -0.0122(18) C13 0.046(2) 0.0254(18) 0.0322(19) -0.0127(15) -0.0012(18) -0.0062(19) C14 0.0259(17) 0.0144(15) 0.0174(15) -0.0042(14) -0.0056(15) 0.0010(12) C15 0.033(2) 0.0186(17) 0.0194(16) -0.0008(14) -0.0046(15) 0.0019(15) C16 0.045(2) 0.0206(19) 0.0269(18) 0.0021(14) -0.0176(17) 0.0035(16) C17 0.034(2) 0.032(2) 0.036(2) -0.0074(17) -0.0132(17) 0.0160(17) C18 0.027(2) 0.042(2) 0.0262(18) -0.0087(15) 0.0001(14) 0.0099(17) C19 0.031(2) 0.027(2) 0.0173(15) -0.0023(14) -0.0012(14) 0.0050(16) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C2 U1 C2 107.46(14) . 7 C2 U1 C3 30.23(9) . . C2 U1 C3 136.34(10) 7 . C2 U1 C3 136.34(10) . 7 C2 U1 C3 30.23(9) 7 7 C3 U1 C3 166.35(13) . 7 C2 U1 C1 30.01(10) . . C2 U1 C1 88.22(10) 7 . C3 U1 C1 49.38(10) . . C3 U1 C1 118.09(9) 7 . C2 U1 C1 88.22(10) . 7 C2 U1 C1 30.01(10) 7 7 C3 U1 C1 118.09(10) . 7 C3 U1 C1 49.38(10) 7 7 C1 U1 C1 81.40(14) . 7 C2 U1 P1 102.03(8) . . C2 U1 P1 127.76(7) 7 . C3 U1 P1 85.58(7) . . C3 U1 P1 104.00(6) 7 . C1 U1 P1 131.60(7) . . C1 U1 P1 112.83(8) 7 . C2 U1 P1 127.76(7) . 7 C2 U1 P1 102.03(8) 7 7 C3 U1 P1 104.00(6) . 7 C3 U1 P1 85.58(7) 7 7 C1 U1 P1 112.83(8) . 7 C1 U1 P1 131.60(7) 7 7 P1 U1 P1 92.16(4) . 7 C2 U1 C5 49.28(10) . . C2 U1 C5 100.64(10) 7 . C3 U1 C5 49.02(9) . . C3 U1 C5 124.18(9) 7 . C1 U1 C5 29.68(10) . . C1 U1 C5 105.63(10) 7 . P1 U1 C5 130.99(7) . . P1 U1 C5 83.83(7) 7 . C2 U1 C5 100.64(10) . 7 C2 U1 C5 49.28(10) 7 7 C3 U1 C5 124.18(9) . 7 C3 U1 C5 49.02(9) 7 7 C1 U1 C5 105.63(10) . 7 C1 U1 C5 29.68(10) 7 7 P1 U1 C5 83.83(7) . 7 P1 U1 C5 130.99(7) 7 7 C5 U1 C5 133.43(14) . 7 C2 U1 C4 130.13(10) . 7 C2 U1 C4 49.37(10) 7 7 C3 U1 C4 150.14(8) . 7 C3 U1 C4 29.71(9) 7 7 C1 U1 C4 130.37(10) . 7 C1 U1 C4 48.99(10) 7 7 P1 U1 C4 78.65(7) . 7 P1 U1 C4 101.80(7) 7 7 C5 U1 C4 149.99(10) . 7 C5 U1 C4 29.50(9) 7 7 C2 U1 C4 49.37(10) . . C2 U1 C4 130.13(10) 7 . C3 U1 C4 29.71(9) . . C3 U1 C4 150.14(8) 7 . C1 U1 C4 48.99(10) . . C1 U1 C4 130.37(10) 7 . P1 U1 C4 101.80(7) . . P1 U1 C4 78.65(7) 7 . C5 U1 C4 29.50(9) . . C5 U1 C4 149.99(10) 7 . C4 U1 C4 179.36(14) 7 . C14 P1 Si1 98.53(10) . . C14 P1 U1 127.13(10) . . Si1 P1 U1 131.96(4) . . C12 Si1 C11 108.07(18) . . C12 Si1 C13 108.01(17) . . C11 Si1 C13 110.75(17) . . C12 Si1 P1 109.83(12) . . C11 Si1 P1 109.19(12) . . C13 Si1 P1 110.94(13) . . C5 C1 C2 107.9(3) . . C5 C1 C6 122.8(3) . . C2 C1 C6 127.7(3) . . C5 C1 U1 75.94(18) . . C2 C1 U1 73.49(18) . . C6 C1 U1 128.1(2) . . C1 C2 C3 107.8(3) . . C1 C2 C7 128.7(3) . . C3 C2 C7 123.2(3) . . C1 C2 U1 76.50(18) . . C3 C2 U1 75.61(16) . . C7 C2 U1 118.7(2) . . C4 C3 C2 108.2(3) . . C4 C3 C8 125.4(3) . . C2 C3 C8 125.4(3) . . C4 C3 U1 77.19(15) . . C2 C3 U1 74.16(16) . . C8 C3 U1 123.7(2) . . C5 C4 C3 107.6(3) . . C5 C4 C9 126.5(3) . . C3 C4 C9 125.0(3) . . C5 C4 U1 74.75(16) . . C3 C4 U1 73.10(15) . . C9 C4 U1 125.9(2) . . C4 C5 C1 108.5(3) . . C4 C5 C10 127.4(3) . . C1 C5 C10 123.4(3) . . C4 C5 U1 75.75(16) . . C1 C5 U1 74.39(18) . . C10 C5 U1 124.1(2) . . C19 C14 C15 117.5(3) . . C19 C14 P1 120.9(2) . . C15 C14 P1 121.6(3) . . C16 C15 C14 120.9(3) . . C17 C16 C15 120.5(3) . . C18 C17 C16 119.3(3) . . C17 C18 C19 120.4(3) . . C18 C19 C14 121.4(3) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 U1 C2 2.709(3) . U1 C2 2.709(3) 7 U1 C3 2.728(3) . U1 C3 2.728(3) 7 U1 C1 2.748(3) . U1 C1 2.748(3) 7 U1 P1 2.7477(8) . U1 P1 2.7478(8) 7 U1 C5 2.768(3) . U1 C5 2.768(3) 7 U1 C4 2.780(3) 7 U1 C4 2.780(3) . P1 C14 1.841(3) . P1 Si1 2.2278(12) . Si1 C12 1.873(3) . Si1 C11 1.873(4) . Si1 C13 1.876(4) . C1 C5 1.413(5) . C1 C2 1.413(5) . C1 C6 1.503(5) . C2 C3 1.418(4) . C2 C7 1.502(5) . C3 C4 1.413(4) . C3 C8 1.502(4) . C4 C5 1.412(4) . C4 C9 1.495(5) . C5 C10 1.509(5) . C14 C19 1.387(4) . C14 C15 1.403(4) . C15 C16 1.388(5) . C16 C17 1.379(5) . C17 C18 1.378(5) . C18 C19 1.388(4) .