#------------------------------------------------------------------------------ #$Date: 2019-12-06 11:37:22 +0200 (Fri, 06 Dec 2019) $ #$Revision: 244933 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/64/1556436.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556436 loop_ _publ_author_name 'Yang, X.' 'Lunsford, A.' 'Darensbourg, M.Y.' _publ_section_title ; Connecting Main-Group Metals (Al, Ga, In) and Tungsten(0) Carbonyls via the N2S2 Metallo-Ligand Strategy ; _journal_name_full Inorganics _journal_page_first 115 _journal_paper_doi 10.3390/inorganics7090115 _journal_volume 7 _journal_year 2019 _chemical_formula_moiety 'C14 H18 Cl Ga N2 O5 S2 W' _chemical_formula_sum 'C14 H18 Cl Ga N2 O5 S2 W' _chemical_formula_weight 647.44 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _cell_angle_alpha 90 _cell_angle_beta 95.932(8) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.2266(11) _cell_length_b 19.245(2) _cell_length_c 12.8581(18) _cell_measurement_reflns_used 9874 _cell_measurement_temperature 100 _cell_measurement_theta_max 61.28 _cell_measurement_theta_min 4.60 _cell_volume 2024.8(4) _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 100.15 _diffrn_detector 'Bruker CMOS area detector' _diffrn_detector_area_resol_mean 10.5 _diffrn_detector_type 'CMOS area detector' _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker Micro-Source CMOS' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator 'mirror optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0442 _diffrn_reflns_av_unetI/netI 0.0267 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 21370 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 61.262 _diffrn_reflns_theta_max 61.262 _diffrn_reflns_theta_min 4.150 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_target Mo _diffrn_source_type 'Incoatec I\ms' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 15.370 _exptl_absorpt_correction_T_max 0.1560 _exptl_absorpt_correction_T_min 0.0455 _exptl_absorpt_correction_type multi-scan _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 2.124 _exptl_crystal_description needle _exptl_crystal_F_000 1240 _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.01 _exptl_crystal_size_min 0.01 _refine_diff_density_max 0.855 _refine_diff_density_min -0.522 _refine_diff_density_rms 0.115 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.026 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 239 _refine_ls_number_reflns 3117 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.026 _refine_ls_R_factor_all 0.0344 _refine_ls_R_factor_gt 0.0320 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0302P)^2^+12.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0781 _refine_ls_wR_factor_ref 0.0800 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 2951 _reflns_number_total 3117 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file gawco5.cif _cod_data_source_block gawco5 _cod_original_cell_volume 2024.8(5) _cod_database_code 1556436 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.861 _shelx_estimated_absorpt_t_min 0.309 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups, All C(H,H,H,H) groups 2. Uiso/Uaniso restraints and constraints Uanis(S2) = Uanis(S2A) 3. Others Sof(S2A)=Sof(H14c)=Sof(H14d)=1-FVAR(1) Sof(S2)=Sof(H14a)=Sof(H14b)=FVAR(1) 4.a Secondary CH2 refined with riding coordinates: C6(H6a,H6b), C7(H7a,H7b), C8(H8a,H8b), C9(H9a,H9b), C10(H10a,H10b), C11(H11a, H11b), C12(H12a,H12b), C13(H13a,H13b), C14(H14a,H14b), C14(H14c,H14d) ; _shelx_res_file ; TITL T_a.res in P2(1)/n gawco5.res created by SHELXL-2017/1 at 15:19:06 on 02-Aug-2017 CELL 1.54184 8.2266 19.2453 12.8581 90 95.932 90 ZERR 4 0.0011 0.0024 0.0018 0 0.008 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl Ga N O S W UNIT 56 72 4 4 8 20 8 4 EADP S2 S2A L.S. 40 PLAN -5 0 0 SIZE 0.01 0.01 0.1 TEMP -173 fmap 2 acta REM REM REM WGHT 0.030200 12.000000 FVAR 0.27334 0.88100 W1 8 0.373019 0.514224 0.760606 11.00000 0.04382 0.03635 = 0.03337 -0.00115 0.00607 -0.00644 GA1 4 0.492108 0.719952 0.660059 11.00000 0.03825 0.03098 = 0.03928 0.00158 0.00817 0.00031 CL1 3 0.727842 0.664075 0.688657 11.00000 0.03877 0.04661 = 0.05948 -0.00064 0.00728 0.00469 S1 7 0.307933 0.643874 0.735328 11.00000 0.05060 0.03908 = 0.04066 0.00148 0.01213 -0.00473 PART 1 S2 7 0.462043 0.806064 0.776596 21.00000 0.04544 0.03761 = 0.04037 -0.00560 -0.00254 0.00451 PART 0 PART 2 S2A 7 0.438496 0.814629 0.731478 -21.00000 0.04544 0.03761 = 0.04037 -0.00560 -0.00254 0.00451 PART 0 O1 6 0.438678 0.360783 0.835889 11.00000 0.05367 0.04510 = 0.07879 0.02285 -0.00115 -0.00036 O2 6 0.640970 0.500411 0.600193 11.00000 0.08044 0.04772 = 0.07665 -0.00805 0.03591 -0.00258 O3 6 0.098637 0.525818 0.917352 11.00000 0.09722 0.05507 = 0.08604 -0.00116 0.05411 -0.00869 O4 6 0.111315 0.456338 0.581466 11.00000 0.08903 0.05812 = 0.04869 0.00945 -0.01779 -0.02908 O5 6 0.647703 0.561481 0.938330 11.00000 0.11432 0.11796 = 0.05264 0.01793 -0.02236 -0.06345 N1 5 0.357439 0.702252 0.516201 11.00000 0.06235 0.04782 = 0.04072 0.00375 0.00395 -0.00572 N2 5 0.574500 0.799502 0.560595 11.00000 0.05339 0.05681 = 0.06072 0.01144 0.00718 -0.00006 C1 1 0.415801 0.417573 0.806969 11.00000 0.03873 0.06536 = 0.04075 0.00036 -0.00120 -0.00426 C2 1 0.544853 0.507764 0.657003 11.00000 0.05976 0.03410 = 0.04744 -0.00035 0.01716 0.00029 C3 1 0.198607 0.520810 0.861449 11.00000 0.06732 0.03854 = 0.05736 0.00371 0.02678 -0.00700 C4 1 0.203827 0.478679 0.644954 11.00000 0.06255 0.03975 = 0.03884 0.00711 0.00046 -0.01058 C5 1 0.549268 0.545357 0.874225 11.00000 0.06892 0.06234 = 0.04514 0.01256 -0.00123 -0.02528 C6 1 0.149355 0.657253 0.626920 11.00000 0.03978 0.05215 = 0.07406 -0.00723 0.00759 0.00262 AFIX 23 H6A 2 0.061879 0.622207 0.629945 11.00000 -1.20000 H6B 2 0.100401 0.703946 0.632249 11.00000 -1.20000 AFIX 0 C7 1 0.224261 0.650728 0.523664 11.00000 0.05215 0.05072 = 0.05630 0.00099 -0.00518 -0.01058 AFIX 23 H7A 2 0.268516 0.603239 0.517496 11.00000 -1.20000 H7B 2 0.138187 0.657944 0.464952 11.00000 -1.20000 AFIX 0 C8 1 0.469083 0.673709 0.440026 11.00000 0.07514 0.05935 = 0.05534 -0.00774 0.01568 0.00631 AFIX 23 H8A 2 0.536605 0.636063 0.474603 11.00000 -1.20000 H8B 2 0.401600 0.653246 0.379476 11.00000 -1.20000 AFIX 0 C9 1 0.579673 0.727730 0.401320 11.00000 0.07534 0.06529 = 0.06078 -0.00040 0.02596 0.00286 AFIX 23 H9A 2 0.512323 0.758978 0.353235 11.00000 -1.20000 H9B 2 0.657829 0.703941 0.359727 11.00000 -1.20000 AFIX 0 C10 1 0.678038 0.772816 0.483648 11.00000 0.06175 0.07322 = 0.06644 0.02081 0.02155 -0.00136 AFIX 23 H10A 2 0.767884 0.744883 0.519773 11.00000 -1.20000 H10B 2 0.727246 0.812265 0.448677 11.00000 -1.20000 AFIX 0 C11 1 0.289383 0.772194 0.482693 11.00000 0.06017 0.04995 = 0.04168 0.00720 -0.00379 -0.00726 AFIX 23 H11A 2 0.193425 0.782739 0.520508 11.00000 -1.20000 H11B 2 0.252929 0.771440 0.406874 11.00000 -1.20000 AFIX 0 C12 1 0.419231 0.828722 0.505722 11.00000 0.05541 0.04934 = 0.05774 0.01628 -0.00125 0.00268 AFIX 23 H12A 2 0.442917 0.850612 0.439263 11.00000 -1.20000 H12B 2 0.376366 0.865119 0.549965 11.00000 -1.20000 AFIX 0 C13 1 0.668796 0.849983 0.630178 11.00000 0.05434 0.05177 = 0.07463 0.01648 -0.00520 -0.00918 AFIX 23 H13A 2 0.697734 0.890493 0.588358 11.00000 -1.20000 H13B 2 0.771722 0.827914 0.660368 11.00000 -1.20000 AFIX 0 C14 1 0.573134 0.875023 0.718860 11.00000 0.06916 0.04362 = 0.06151 -0.00024 -0.01389 -0.00076 PART 1 AFIX 23 H14A 2 0.494764 0.911317 0.691545 21.00000 -1.20000 H14B 2 0.650117 0.896459 0.773937 21.00000 -1.20000 AFIX 23 PART 0 PART 2 H14C 2 0.519052 0.920013 0.700822 -21.00000 -1.20000 H14D 2 0.646382 0.880655 0.784401 -21.00000 -1.20000 AFIX 0 HKLF 4 REM T_a.res in P2(1)/n REM R1 = 0.0320 for 2951 Fo > 4sig(Fo) and 0.0344 for all 3117 data REM 239 parameters refined using 0 restraints END WGHT 0.0283 8.6925 REM Highest difference peak 0.855, deepest hole -0.522, 1-sigma level 0.115 Q1 1 0.2992 0.6367 0.6460 11.00000 0.05 0.85 Q2 1 0.3846 0.5388 0.7062 11.00000 0.05 0.79 Q3 1 0.3752 0.5620 0.7308 11.00000 0.05 0.76 Q4 1 0.5532 0.7588 0.4983 11.00000 0.05 0.76 Q5 1 0.4767 0.5044 0.7740 11.00000 0.05 0.74 ; _shelx_res_checksum 63407 _shelx_hkl_file ; -1 0 0 0.74428 0.52541 9 -2 0 0 362.775 19.7025 9 -2 0 0 335.750 19.6349 4 3 0 0 4.52491 2.09879 8 -3 0 0 1.31575 1.34247 9 -4 0 0 806.948 45.3166 4 -4 0 0 824.089 45.5117 9 4 0 0 822.661 45.3854 8 4 0 0 790.716 45.4701 1 -5 0 0 4.08166 2.62335 9 5 0 0 4.65423 2.17683 8 -5 0 0 2.65124 2.16789 4 -6 0 0 90.4539 9.10794 4 -6 0 0 95.7140 8.05353 1 6 0 0 97.9776 7.29919 8 -6 0 0 96.3177 9.28784 9 7 0 0 1.89755 3.99908 2 -7 0 0 -1.1819 3.25946 4 -7 0 0 6.69187 6.09932 10 7 0 0 -0.4355 3.09112 8 -8 0 0 371.964 22.4490 4 -8 0 0 372.044 22.2371 1 -8 0 0 372.296 24.0252 10 -9 0 0 -1.3609 5.87902 10 -9 0 0 3.52990 5.12758 4 -9 0 0 12.2752 3.53863 1 0 -1 0 0.54303 0.48428 9 1 1 0 3657.26 200.260 9 -2 -1 0 4.08364 1.41458 4 -2 -1 0 4.14753 1.44047 9 -2 1 0 2.55168 1.32971 9 -2 1 0 2.78856 1.47988 4 3 -1 0 1429.25 80.9165 8 -3 -1 0 1481.37 80.9995 9 -3 1 0 1437.18 81.0568 9 -3 1 0 1464.80 80.9470 4 3 1 0 1467.07 81.2296 3 -3 1 0 1499.97 80.5374 6 3 1 0 1480.55 81.0396 8 -4 -1 0 12.5588 2.29763 4 4 -1 0 11.8187 2.45998 8 -4 -1 0 15.6840 2.69735 9 4 1 0 15.7956 2.66548 8 -4 1 0 18.7405 3.25735 9 -4 1 0 13.3832 2.46039 4 -5 -1 0 326.876 19.2070 9 5 -1 0 312.513 18.6424 8 5 -1 0 341.669 21.0526 11 -5 -1 0 311.706 18.7513 4 5 -1 0 302.178 21.2965 1 -5 1 0 319.451 19.1701 9 -5 1 0 306.871 18.7331 4 -5 1 0 312.150 19.0578 1 5 1 0 327.494 18.8575 8 -6 -1 0 16.7232 4.13241 1 -6 -1 0 11.6043 4.57055 9 6 -1 0 9.64012 2.57613 8 -6 -1 0 17.2351 3.51523 4 6 1 0 2.66468 3.43876 2 -6 1 0 10.6846 4.85045 9 6 1 0 9.75607 3.13218 8 -6 1 0 15.4952 3.70162 4 -6 1 0 12.8252 4.63480 10 -6 1 0 11.1772 3.37555 1 7 -1 0 367.523 21.9028 8 -7 -1 0 359.785 24.1350 10 -7 -1 0 356.329 21.6093 4 7 -1 0 341.778 21.3101 2 -7 -1 0 366.231 22.0916 1 -7 1 0 351.956 21.7983 1 -7 1 0 352.187 21.5546 4 -7 1 0 352.587 23.8323 10 7 1 0 364.384 22.8517 8 -8 -1 0 76.5248 7.45653 1 -8 -1 0 68.1576 7.65386 4 -8 -1 0 66.5579 9.56012 10 -8 1 0 80.5817 7.22823 1 -8 1 0 66.8430 9.91038 10 -8 1 0 70.2863 7.64637 4 -9 -1 0 104.119 9.95071 4 -9 -1 0 116.867 9.17266 1 -9 -1 0 86.4981 11.0244 10 -9 1 0 97.5210 10.2114 4 -9 1 0 106.694 7.98518 1 -9 1 0 102.719 11.6291 10 0 -2 0 435.159 23.7220 9 0 2 0 422.643 23.7267 9 -1 -2 0 309.663 17.5379 9 1 2 0 307.848 17.4406 6 -1 2 0 332.091 17.9288 4 1 2 0 309.164 17.5753 9 2 -2 0 456.397 30.1952 4 -2 -2 0 546.823 29.5630 9 -2 -2 0 543.909 29.3841 4 -2 2 0 558.688 29.6324 4 2 2 0 536.277 29.6467 9 -3 -2 0 7.53855 1.57461 9 3 -2 0 6.76407 1.93088 8 -3 -2 0 6.55274 2.04732 4 -3 2 0 8.46118 2.01099 4 -3 2 0 12.1689 2.90280 1 3 2 0 6.86869 2.69752 3 3 2 0 10.1487 2.62162 8 -3 2 0 7.61882 1.99328 6 -3 2 0 6.06042 1.58870 9 -4 -2 0 6064.30 329.526 4 4 -2 0 5598.84 329.386 8 4 -2 0 6534.56 330.949 11 4 -2 0 5833.37 329.426 1 -4 -2 0 6034.00 329.804 9 -4 2 0 6017.92 328.875 6 -4 2 0 5837.29 329.617 1 -4 2 0 6063.84 329.590 4 4 2 0 6210.33 329.744 8 4 2 0 5952.17 329.686 3 -4 2 0 5949.61 329.737 9 -5 -2 0 393.902 23.0231 9 5 -2 0 409.403 24.6003 11 -5 -2 0 381.649 22.5784 4 5 -2 0 373.447 22.3961 8 -5 2 0 406.577 23.0837 9 -5 2 0 373.640 22.5649 4 -5 2 0 366.412 22.7544 1 5 2 0 401.347 22.8111 8 -5 2 0 387.780 23.8247 10 6 -2 0 59.4858 5.24477 8 -6 -2 0 55.3788 7.88754 9 -6 -2 0 57.9430 6.11838 4 -6 2 0 62.5318 5.98805 4 -6 2 0 50.8503 8.58460 9 -6 2 0 60.9892 6.26591 1 6 2 0 56.3553 6.12113 8 -6 2 0 45.2769 7.66102 10 -7 -2 0 14.5804 7.10786 1 7 -2 0 7.36810 3.54330 2 -7 -2 0 8.21612 3.62614 4 -7 2 0 12.6074 3.70582 4 -8 -2 0 179.939 11.8478 1 -8 -2 0 169.606 13.2347 10 -8 -2 0 154.847 11.7628 4 -8 2 0 176.424 11.4807 1 -8 2 0 167.061 11.9722 4 -8 2 0 159.279 14.0764 10 -9 -2 0 -0.8670 5.38972 10 -9 -2 0 0.69831 5.03824 4 -9 2 0 3.06606 5.88514 4 -9 2 0 1.40906 3.11819 1 -9 2 0 0.27701 5.96230 10 0 -3 0 2.97837 0.92834 9 0 3 0 2.48050 0.96183 9 1 -3 0 1806.37 116.070 4 -1 -3 0 2101.87 115.797 9 -1 -3 0 2177.25 115.729 4 1 3 0 2262.06 115.922 9 1 3 0 2125.11 115.884 6 -1 3 0 2190.93 115.904 4 2 -3 0 7.50967 3.15052 4 -2 -3 0 10.6105 1.43162 4 2 3 0 8.73853 1.95159 9 2 3 0 8.39820 1.20402 6 3 -3 0 1241.63 71.8756 4 3 -3 0 1233.91 71.5287 1 3 -3 0 1105.53 73.4074 11 3 -3 0 1285.68 71.5885 8 -3 -3 0 1364.85 71.7777 9 -3 -3 0 1312.82 71.4815 4 -3 3 0 1399.68 71.7891 4 3 3 0 1329.18 71.9353 8 -3 3 0 1346.64 71.6746 9 3 3 0 1233.10 71.8937 3 -3 3 0 1393.94 72.7067 10 -3 3 0 1294.65 71.8357 1 4 -3 0 173.594 11.1823 8 4 -3 0 162.927 11.6653 1 -4 -3 0 198.054 11.5683 9 4 -3 0 216.708 14.5353 11 -4 -3 0 176.166 11.1453 4 -4 3 0 184.278 11.3895 4 -4 3 0 190.557 12.9998 10 -4 3 0 189.057 11.3151 6 4 3 0 163.382 11.8298 3 -4 3 0 176.627 11.6106 1 4 3 0 178.430 11.7832 8 -4 3 0 180.373 11.4517 9 5 -3 0 1721.61 99.2736 8 -5 -3 0 1790.15 99.4558 4 5 -3 0 1915.99 101.292 11 -5 -3 0 1828.01 99.8810 9 5 3 0 1753.06 99.7413 8 -5 3 0 1785.26 99.5018 4 -5 3 0 1734.57 99.5250 1 -5 3 0 1811.94 100.522 10 -5 3 0 1826.51 99.9340 9 -6 -3 0 187.021 12.2491 4 6 -3 0 193.718 11.7916 8 -6 -3 0 174.989 13.6840 9 -6 3 0 182.106 12.0983 4 -6 3 0 193.113 13.7844 10 6 3 0 172.411 12.4818 8 -6 3 0 190.568 14.6615 9 -6 3 0 186.922 12.2095 1 -7 -3 0 359.027 21.6429 4 -7 3 0 360.244 21.5512 4 -7 3 0 369.258 21.8398 1 -7 3 0 376.794 24.6817 10 7 3 0 329.077 22.5142 8 -8 -3 0 16.1388 4.02825 1 -8 -3 0 12.8106 5.26375 10 -8 -3 0 9.23291 4.05776 4 8 -3 0 9.26532 3.93401 2 -8 3 0 6.64355 5.79012 10 -8 3 0 0.47872 4.13930 4 -8 3 0 12.2606 3.19208 1 -9 -3 0 4.75792 5.29149 4 -9 -3 0 1.40194 6.73782 10 -9 -3 0 4.59530 3.88788 1 -9 3 0 -0.7882 3.34937 1 -9 3 0 -0.9125 5.12149 5 -9 3 0 14.7626 11.5817 10 0 -4 0 7408.90 399.296 4 0 -4 0 7584.90 399.180 9 0 4 0 6886.28 399.211 9 -1 -4 0 17.9656 2.76166 4 1 -4 0 20.3692 2.99693 4 -1 -4 0 18.1486 2.41543 9 1 4 0 22.8821 2.78457 9 1 4 0 16.2636 2.63579 6 -1 4 0 22.5920 2.90529 4 2 -4 0 754.846 40.9560 4 -2 -4 0 739.510 40.6352 9 -2 -4 0 701.948 40.3856 4 -2 4 0 733.281 40.6408 4 2 4 0 719.544 40.8932 9 2 4 0 732.223 40.3810 6 3 -4 0 14.7103 2.58285 8 3 -4 0 11.3783 3.82984 11 -3 -4 0 13.1188 2.36491 4 -3 -4 0 9.73792 2.01528 9 3 -4 0 8.88948 3.47298 4 3 -4 0 15.7175 2.89955 1 -3 4 0 7.37429 2.86108 6 3 4 0 11.3480 3.45837 8 -3 4 0 13.2087 2.25321 4 3 4 0 10.4222 2.74838 3 -3 4 0 9.25149 2.54672 1 -3 4 0 10.6479 4.02466 10 4 -4 0 1115.51 70.6572 1 4 -4 0 1287.15 70.6098 8 4 -4 0 1119.57 72.4426 11 -4 -4 0 1344.94 70.9907 9 -4 -4 0 1308.63 70.5786 4 -4 4 0 1379.04 71.0021 9 -4 4 0 1436.01 73.0697 10 -4 4 0 1223.25 70.8059 6 -4 4 0 1295.39 70.8575 1 4 4 0 1234.76 70.9614 3 -4 4 0 1386.06 70.8774 4 4 4 0 1152.48 70.9220 8 5 -4 0 3.93255 3.89917 11 5 -4 0 3.25970 2.08179 8 -5 -4 0 1.59899 3.44860 9 -5 -4 0 3.06596 2.50300 4 5 -4 0 11.2020 4.33357 1 -5 4 0 -2.2265 4.29416 10 -5 4 0 5.61497 2.85193 1 -5 4 0 3.22069 2.33215 4 -5 4 0 8.55815 3.71306 9 5 4 0 0.00228 3.12360 8 -6 -4 0 129.413 9.63834 4 -6 -4 0 133.009 11.8502 9 6 -4 0 141.856 9.25770 8 -6 4 0 138.626 9.67312 4 -6 4 0 135.101 11.6606 10 -6 4 0 134.582 9.67305 1 -6 4 0 139.790 13.6262 9 -7 -4 0 62.9801 6.68024 4 -7 -4 0 64.7173 7.39115 1 7 4 0 40.7439 7.05908 8 -7 4 0 56.8837 9.50549 10 -7 4 0 61.3884 6.46680 4 -7 4 0 67.0102 6.57867 1 -8 -4 0 535.768 31.5048 4 -8 -4 0 537.166 32.6059 10 8 -4 0 545.877 31.3768 2 -8 -4 0 558.542 31.5301 1 -8 4 0 560.694 31.1852 1 -8 4 0 530.447 33.1223 10 -8 4 0 519.344 31.4691 4 -9 -4 0 39.6967 8.34172 10 -9 -4 0 32.0118 5.15753 1 -9 -4 0 16.5004 5.95886 4 -9 4 0 21.7611 4.15071 1 -9 4 0 23.1855 7.32234 10 0 -5 0 0.29318 1.62020 4 0 5 0 2.30276 1.47301 9 1 -5 0 2299.20 119.852 4 -1 -5 0 2239.19 119.686 9 -1 5 0 2265.10 119.735 4 1 5 0 2138.06 119.880 9 1 5 0 1948.46 119.932 6 2 -5 0 352.782 25.2806 11 -2 -5 0 424.102 23.2403 4 -2 -5 0 420.108 23.4382 9 2 -5 0 434.392 23.6835 4 2 5 0 414.750 24.0459 9 2 5 0 423.648 24.4237 3 2 5 0 393.317 24.2929 5 -2 5 0 421.175 23.4571 4 2 5 0 444.626 23.4118 6 -2 5 0 403.292 25.1937 10 -3 -5 0 373.620 21.9689 4 3 -5 0 428.449 22.6084 4 3 -5 0 327.985 22.3321 1 -3 -5 0 401.543 22.3988 9 3 -5 0 402.970 22.3540 8 -3 5 0 440.568 27.3920 10 -3 5 0 373.365 22.7274 6 3 5 0 370.572 23.2371 3 -3 5 0 393.296 22.2790 4 4 -5 0 19.7794 3.57573 1 -4 -5 0 24.7926 4.22071 9 -4 -5 0 18.9635 3.20450 4 -4 5 0 23.6509 3.69785 9 4 5 0 22.5544 3.58939 3 -4 5 0 24.2601 5.38291 10 -4 5 0 14.1791 4.18414 6 -4 5 0 22.0592 3.19638 1 4 5 0 14.9614 3.92263 8 -4 5 0 20.6457 3.69335 4 5 -5 0 127.311 8.54416 8 5 -5 0 117.283 9.50740 1 -5 -5 0 124.528 11.2419 9 -5 -5 0 120.867 8.51335 4 -5 5 0 122.581 8.81119 1 5 5 0 123.816 9.36507 3 -5 5 0 123.727 11.0558 10 -5 5 0 132.987 10.5523 9 -5 5 0 134.062 14.8504 6 -5 5 0 123.061 8.68375 4 -6 -5 0 137.001 9.66125 4 6 -5 0 130.649 14.4823 11 -6 -5 0 143.390 12.6663 9 -6 5 0 137.237 9.57541 1 -6 5 0 141.723 15.2957 9 -6 5 0 141.176 11.9042 10 -6 5 0 131.809 9.46693 4 6 5 0 118.313 10.0316 8 -7 -5 0 693.254 40.1475 4 7 5 0 700.461 40.3820 8 -7 5 0 698.312 40.0084 4 -7 5 0 740.069 40.0782 1 -7 5 0 672.544 41.7016 10 -8 -5 0 -2.2544 4.70344 10 -8 -5 0 6.67276 4.52530 1 -8 -5 0 2.52866 4.02405 4 8 -5 0 1.64803 3.91747 2 -8 5 0 2.34551 4.95291 4 -8 5 0 0.29683 5.94703 10 -8 5 0 2.93517 4.71246 5 -8 5 0 0.75073 2.94631 1 -9 -5 0 192.693 15.9717 10 -9 -5 0 177.812 20.2379 4 -9 -5 0 210.809 13.9807 1 -9 5 0 195.885 16.0293 10 -9 5 0 195.730 12.2823 1 -9 5 0 186.445 14.5770 5 0 -6 0 9999.99 532.063 4 0 6 0 9440.74 532.050 9 -1 -6 0 26.6468 2.99334 9 -1 -6 0 29.9780 3.24405 4 1 -6 0 25.2288 4.40450 1 1 -6 0 28.6372 3.30413 4 1 -6 0 39.5721 6.83424 11 -1 6 0 36.8339 4.04409 4 1 6 0 21.8077 5.74423 10 1 6 0 28.4184 4.12764 9 1 6 0 27.4422 4.90490 5 -1 6 0 19.5703 5.63245 10 -1 6 0 28.5111 3.15520 9 -1 6 0 29.8604 5.96954 5 2 -6 0 449.548 28.1568 11 -2 -6 0 467.108 26.4205 4 2 -6 0 472.409 26.5922 4 -2 -6 0 464.534 26.5358 9 2 6 0 471.977 27.5650 5 -2 6 0 465.339 26.7055 1 -2 6 0 466.499 26.5290 4 -2 6 0 457.300 27.2832 5 2 6 0 472.381 26.7245 6 2 6 0 490.996 27.6971 3 -2 6 0 481.908 28.4924 10 -3 -6 0 421.214 23.1857 9 -3 -6 0 420.129 22.8222 4 3 6 0 348.300 23.5518 8 3 6 0 413.910 23.8468 3 -3 6 0 416.511 23.6285 6 3 6 0 385.940 22.4597 6 -3 6 0 411.691 22.9993 4 -3 6 0 389.305 24.5864 10 -3 6 0 396.805 23.1084 1 4 -6 0 1421.54 74.4850 11 -4 -6 0 1232.91 71.9842 4 4 -6 0 1310.37 72.1311 8 -4 -6 0 1303.18 72.5088 9 -4 6 0 1223.47 72.1897 1 -4 6 0 1237.70 72.5838 9 -4 6 0 1326.42 72.2659 4 4 6 0 1301.86 72.7702 3 -4 6 0 1336.71 73.7223 10 5 -6 0 170.280 15.8844 11 -5 -6 0 191.412 12.3519 4 -5 -6 0 211.865 13.7100 9 5 -6 0 192.994 12.6827 1 5 6 0 217.447 13.4838 3 -5 6 0 206.426 15.0134 10 -5 6 0 197.264 12.6397 1 -5 6 0 203.325 12.6552 4 5 6 0 203.055 13.1816 8 -5 6 0 183.097 14.8115 6 -6 -6 0 22.0953 7.27400 9 6 -6 0 16.0293 5.71736 11 -6 6 0 1.87253 9.47000 9 -7 -6 0 83.7826 8.06612 4 -7 6 0 99.6318 11.3901 10 -7 6 0 93.4920 8.97806 5 7 6 0 97.5123 8.23004 8 -7 6 0 86.5837 8.09655 4 -7 6 0 92.6174 7.56428 1 8 -6 0 119.070 9.56010 2 -8 -6 0 122.202 10.0712 1 -8 -6 0 105.952 10.7735 4 -8 6 0 100.679 12.3820 10 -8 6 0 119.497 8.54957 1 -8 6 0 98.8785 11.0012 4 -8 6 0 116.112 10.4188 5 0 -7 0 6.56071 2.40419 1 0 7 0 6.52619 4.27006 5 0 7 0 8.42073 2.17416 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11 4 -7 0 89.5606 7.60319 1 -4 -7 0 106.772 7.29112 4 -4 -7 0 105.311 8.12061 9 -4 7 0 107.021 10.4300 10 -4 7 0 104.293 7.59460 1 4 7 0 110.065 8.84997 3 -4 7 0 104.744 7.46677 4 -4 7 0 91.3643 9.18976 6 4 7 0 103.003 8.32734 8 5 -7 0 474.597 27.8493 1 -5 -7 0 494.018 29.0719 9 5 -7 0 500.324 31.0792 11 -5 -7 0 479.061 28.0902 4 -5 7 0 460.111 28.0845 1 5 7 0 498.299 29.1163 3 5 7 0 503.751 28.3296 8 -5 7 0 488.901 28.1915 4 -5 7 0 483.709 30.3676 10 -6 -7 0 279.293 17.4033 4 -6 -7 0 272.191 20.9447 9 6 -7 0 247.475 21.1879 11 -6 7 0 299.018 18.2200 5 -6 7 0 285.950 17.2309 1 6 7 0 311.063 17.4864 8 -6 7 0 296.201 19.9261 10 -6 7 0 278.098 17.3723 4 -6 7 0 254.806 24.4835 9 7 -7 0 -0.8807 5.97932 11 -7 -7 0 1.97641 3.74526 4 7 7 0 1.10908 3.47153 8 -7 7 0 9.91866 3.06799 1 -7 7 0 3.88870 5.51660 10 -7 7 0 0.33331 4.26426 5 -7 7 0 7.57529 4.05288 4 -8 -7 0 31.5613 5.42463 1 8 -7 0 24.5813 4.73162 2 -8 -7 0 20.8665 5.30347 4 -8 7 0 24.4623 6.92328 10 -8 7 0 18.7911 5.44927 5 -8 7 0 18.3005 7.06294 4 0 -8 0 1677.01 88.8933 4 0 -8 0 1688.87 90.1658 11 0 -8 0 1640.00 88.9246 1 0 8 0 1662.59 89.4902 6 0 8 0 1515.42 89.8540 5 0 8 0 1526.76 88.9923 1 0 8 0 1629.84 89.0145 9 0 8 0 1556.21 89.3865 3 -1 -8 0 737.228 41.8036 9 1 -8 0 834.284 43.1044 11 1 -8 0 738.891 41.6574 1 -1 -8 0 855.099 41.7959 4 1 -8 0 775.211 41.6528 4 -1 -8 0 791.988 42.0177 1 -1 8 0 701.688 41.9143 1 -1 8 0 744.736 42.0018 9 -1 8 0 712.864 42.5682 3 1 8 0 771.149 42.8150 3 1 8 0 670.947 43.5993 10 1 8 0 766.728 42.2865 9 -1 8 0 739.638 42.0943 4 -1 8 0 627.859 43.5829 10 -1 8 0 748.720 42.2174 6 -1 8 0 697.135 43.0703 5 1 8 0 852.010 42.4256 6 1 8 0 664.081 43.1602 5 2 -8 0 108.679 7.08562 4 2 -8 0 104.183 7.24521 1 -2 -8 0 107.606 7.54090 9 -2 -8 0 90.7079 8.21995 1 2 8 0 81.4681 11.0974 3 -2 8 0 118.344 7.92330 6 -2 8 0 112.542 8.22812 4 -2 8 0 112.503 9.52355 5 2 8 0 97.7130 7.86117 6 -2 8 0 111.828 11.2561 10 2 8 0 113.598 10.0133 5 -2 8 0 105.558 7.62904 1 3 -8 0 254.395 16.2794 1 -3 -8 0 288.030 16.4953 4 3 -8 0 270.009 16.2217 4 3 -8 0 305.766 18.1359 11 -3 -8 0 272.321 16.5832 9 3 8 0 285.039 17.7822 5 -3 8 0 266.325 16.2870 4 -3 8 0 271.751 16.4090 1 3 8 0 245.621 17.5833 3 -3 8 0 279.588 17.0438 6 -3 8 0 279.490 17.3430 5 -3 8 0 265.185 18.7730 10 3 8 0 288.587 16.8801 8 -4 -8 0 924.943 53.1220 9 4 -8 0 996.749 54.7018 11 -4 -8 0 1001.98 52.8698 4 4 -8 0 894.349 52.5118 1 -4 8 0 923.042 52.7004 4 -4 8 0 909.240 52.7290 1 -4 8 0 928.707 53.4261 5 4 8 0 903.980 53.7175 3 -4 8 0 941.116 54.7306 10 -4 8 0 975.324 53.7446 6 4 8 0 949.453 52.7113 8 5 -8 0 630.350 37.8986 1 -5 -8 0 683.888 40.8021 9 5 -8 0 716.909 41.0622 11 -5 -8 0 683.741 38.7347 4 -5 8 0 715.087 40.8944 10 -5 8 0 692.896 38.4295 4 5 8 0 684.126 38.2445 8 5 8 0 676.359 39.4292 3 -5 8 0 681.080 39.1837 5 -5 8 0 669.418 38.3272 1 -5 8 0 577.621 39.6598 9 -6 -8 0 11.7465 3.94942 4 -6 8 0 16.1866 6.37532 10 6 8 0 19.1928 3.93496 8 -6 8 0 21.6157 5.35515 5 -6 8 0 20.3353 4.12701 4 -6 8 0 13.7553 3.34141 1 7 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3 2374.05 121.835 7 3 6 -3 2087.79 120.303 4 3 6 -3 2049.62 120.535 8 -3 6 3 2083.24 120.123 1 3 6 -3 2249.68 120.731 5 3 6 -3 2306.05 120.499 1 -3 6 3 2247.44 121.702 10 -3 6 3 2304.86 120.224 4 3 6 -3 1902.66 119.913 6 -3 6 3 2254.44 120.728 6 -3 6 3 2268.09 120.738 5 -2 -6 3 145.287 8.92572 4 2 -6 -3 135.697 8.56903 1 2 -6 -3 149.757 8.54609 4 -2 -6 3 131.670 9.59831 9 -2 6 3 144.955 11.6866 7 2 6 -3 136.454 11.0720 5 -2 6 3 141.481 12.4779 10 2 6 -3 144.962 10.2057 8 2 6 -3 140.029 9.57561 1 2 6 -3 121.400 9.71815 4 -2 6 3 144.788 9.57686 6 -2 6 3 134.350 9.56039 1 -1 -6 3 2921.82 159.837 11 1 -6 -3 2900.27 156.721 4 -1 -6 3 2821.47 157.006 4 1 -6 -3 2716.57 156.754 1 -1 -6 3 2995.54 157.337 9 -1 6 3 2839.58 157.928 7 1 6 -3 2906.77 157.348 4 1 6 -3 2765.70 157.515 3 -1 6 3 2937.93 157.687 6 -1 6 3 2757.37 157.600 2 0 -6 3 104.224 10.3775 11 0 -6 -3 89.0021 5.56997 4 0 -6 3 101.738 6.88710 4 0 -6 3 94.2658 7.06791 1 0 6 -3 104.891 6.75594 1 0 6 3 73.0015 7.96659 2 0 6 -3 99.2378 9.68345 5 0 6 -3 80.8625 6.50773 4 0 6 3 77.5344 10.7259 10 0 6 3 80.9879 8.17786 7 0 6 3 91.4857 6.70764 6 1 -6 3 323.631 20.5311 11 1 -6 3 290.694 18.3583 2 1 -6 3 327.926 17.8025 4 -1 -6 -3 310.890 16.9178 9 1 -6 3 303.549 18.0339 1 1 6 3 288.051 18.4901 7 1 6 3 305.061 17.8809 6 1 6 3 299.113 19.0675 5 -1 6 -3 266.449 17.6503 1 -1 6 -3 308.046 17.5906 4 -1 6 -3 286.369 18.7967 5 2 -6 3 108.825 9.20555 1 -2 -6 -3 129.031 7.84194 9 2 -6 3 132.274 11.9640 11 -2 6 -3 129.038 8.62427 1 -2 6 -3 131.032 9.60690 5 -2 6 -3 130.982 8.19371 4 2 6 3 123.904 8.38290 6 -2 6 -3 140.958 13.7869 10 2 6 3 112.519 10.0379 7 -3 -6 -3 470.514 26.6198 9 3 -6 3 498.802 29.9835 11 3 6 3 445.050 26.6070 6 -3 6 -3 481.512 26.8363 1 -3 6 -3 458.663 26.6171 4 3 6 3 439.203 27.3975 2 -3 6 -3 476.358 28.8265 10 4 -6 3 798.733 47.0663 11 -4 -6 -3 767.151 43.4754 4 -4 -6 -3 767.222 44.1148 9 -4 6 -3 783.741 45.6908 10 -4 6 -3 798.621 44.0821 1 -4 6 -3 770.262 43.9142 4 5 -6 3 195.664 16.1265 11 5 -6 3 183.037 13.0935 2 -5 -6 -3 190.043 11.9519 4 -5 6 -3 173.290 15.1432 10 -5 6 -3 187.013 14.4927 9 -5 6 -3 183.089 12.0353 4 -5 6 -3 199.468 12.3080 1 6 -6 3 119.249 16.6461 11 -6 -6 -3 121.592 9.38934 4 6 -6 3 127.217 10.5659 2 -6 -6 -3 112.313 12.2898 1 -6 6 -3 125.142 9.04129 4 -6 6 -3 139.476 9.58324 1 -6 6 -3 121.481 13.8365 10 -7 -6 -3 229.015 18.6291 1 -7 -6 -3 258.597 16.3356 4 7 -6 3 259.385 16.9580 2 -7 6 -3 241.796 17.0577 5 -7 6 -3 268.435 16.0589 1 -7 6 -3 264.517 16.1140 4 -7 6 -3 273.688 20.2652 10 -8 -6 -3 69.2904 12.1049 10 -8 -6 -3 77.6362 8.73748 4 8 -6 3 63.9133 7.88002 2 -8 6 -3 57.4158 11.4548 10 -8 6 -3 60.3121 8.47527 5 -8 6 -3 62.8256 6.73605 1 -8 6 -3 65.0316 8.22788 4 -8 -7 3 59.6115 8.15147 4 -8 -7 3 77.6531 10.6684 10 -8 -7 3 59.6891 7.48465 1 8 7 -3 71.3029 6.24430 8 -8 7 3 65.3279 10.5672 10 -8 7 3 68.3915 6.37688 1 -7 -7 3 112.591 10.0571 4 7 -7 -3 112.162 8.91807 1 7 -7 -3 87.6022 14.2651 11 -7 7 3 103.813 8.10332 1 7 7 -3 109.059 8.30314 8 -7 7 3 116.590 12.1133 10 6 -7 -3 20.7461 3.91984 1 -6 -7 3 24.8961 4.53527 4 6 -7 -3 23.5661 3.68205 8 6 7 -3 26.0860 3.93172 8 -6 7 3 16.7935 5.94120 10 -6 7 3 24.1543 3.69954 1 -6 7 3 25.4141 6.07423 5 6 7 -3 24.8132 4.57684 3 -5 -7 3 109.350 9.05104 4 5 -7 -3 115.543 15.3565 11 -5 -7 3 104.459 11.2547 9 5 -7 -3 112.518 7.97552 1 -5 7 3 104.895 11.2500 10 5 7 -3 115.335 9.63004 3 5 7 -3 117.306 8.65718 8 -5 7 3 116.840 10.3217 5 -5 7 3 116.644 8.60401 1 4 -7 -3 77.3937 5.75451 1 -4 -7 3 84.8374 7.99899 9 -4 -7 3 78.8884 6.39361 4 -4 7 3 79.4184 8.99234 5 -4 7 3 74.9464 6.54638 1 4 7 -3 65.3646 7.66364 3 -4 7 3 76.3228 9.23383 10 4 7 -3 73.4681 7.79050 1 4 7 -3 82.5724 7.01418 8 -4 7 3 81.0577 8.38722 6 3 -7 -3 172.806 12.0455 4 -3 -7 3 185.551 11.9151 4 -3 -7 3 182.790 12.7504 9 3 -7 -3 187.231 11.4437 1 3 -7 -3 199.971 12.3730 8 3 7 -3 175.028 13.1457 3 -3 7 3 181.680 11.9367 1 3 7 -3 191.673 12.5405 8 3 7 -3 211.013 15.0649 5 3 7 -3 193.905 12.6519 1 -3 7 3 195.496 13.0476 6 -3 7 3 200.450 14.3495 5 -3 7 3 206.149 14.7111 7 -3 7 3 207.841 14.7301 10 2 -7 -3 6088.56 344.872 1 -2 -7 3 6001.95 345.642 9 2 -7 -3 6452.45 345.110 4 -2 -7 3 6545.34 345.215 4 2 7 -3 5889.88 345.645 3 2 7 -3 6765.34 346.242 5 2 7 -3 6519.83 345.496 8 2 7 -3 5833.78 345.584 1 -2 7 3 5409.25 345.662 5 2 7 -3 6712.79 345.383 4 -2 7 3 6609.28 347.108 10 -2 7 3 6462.12 345.099 1 -2 7 3 6532.82 346.233 6 1 -7 -3 29.4862 2.81343 4 -1 -7 3 33.7816 3.83781 9 -1 -7 3 29.0371 4.09386 4 1 -7 -3 27.2097 3.52556 1 -1 7 3 35.9284 6.39050 7 1 7 -3 35.6376 6.86621 5 1 7 -3 27.1103 4.88828 3 -1 7 3 44.9815 7.47430 10 -1 7 3 26.5658 4.68543 6 1 7 -3 24.7373 4.77375 4 1 7 -3 26.4588 3.99015 1 -1 7 3 31.4828 5.07900 2 0 -7 3 976.738 49.8071 4 0 -7 -3 945.369 49.1137 4 0 -7 3 876.182 49.8763 1 0 -7 3 911.094 52.3865 11 0 7 -3 902.207 50.6777 5 0 7 3 827.718 50.0855 2 0 7 3 890.002 50.6445 7 0 7 3 930.611 50.4420 6 0 7 -3 874.811 49.7200 4 0 7 3 874.450 51.3336 10 0 7 -3 825.028 49.9754 3 0 7 -3 862.382 52.4495 10 0 7 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30.5900 7.03813 5 6 8 -3 26.9216 4.10773 8 5 -8 -3 802.486 48.2039 11 -5 -8 3 832.474 46.0108 4 -5 -8 3 804.882 47.2910 9 5 -8 -3 799.034 45.2773 8 5 -8 -3 789.955 45.4927 1 -5 8 3 773.092 46.3612 5 5 8 -3 794.702 46.6363 3 5 8 -3 829.023 45.5833 8 -5 8 3 768.803 47.5352 10 -5 8 3 864.473 45.6515 1 4 -8 -3 363.715 25.9695 4 -4 -8 3 473.873 26.0130 4 4 -8 -3 443.695 25.3993 1 -4 -8 3 469.064 27.3923 9 -4 8 3 450.344 27.0580 5 -4 8 3 448.272 27.8898 10 4 8 -3 475.379 25.8825 8 4 8 -3 408.203 26.7545 3 -4 8 3 444.819 25.6254 1 -4 8 3 450.020 27.5137 6 3 -8 -3 3.41988 2.90501 4 -3 -8 3 8.58895 2.92698 4 -3 -8 3 9.19765 3.83953 9 3 -8 -3 15.7911 2.27923 1 -3 8 3 6.53126 6.44752 5 -3 8 3 13.6112 5.36891 10 3 8 -3 18.4576 4.88554 5 3 8 -3 6.20732 2.99984 8 -3 8 3 12.0292 4.59544 6 -3 8 3 13.6398 5.09175 7 3 8 -3 10.4804 4.00596 3 2 -8 -3 54.1758 4.97551 4 2 -8 -3 58.5879 4.63269 1 -2 -8 3 54.1258 5.62879 9 -2 -8 3 58.6853 5.54671 4 2 8 -3 59.8138 6.16055 8 2 8 -3 57.9103 7.04220 4 -2 8 3 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58.0997 10 2 -8 3 43.0186 5.46066 1 -2 -8 -3 44.9782 6.37217 1 2 -8 3 45.4476 8.86629 11 -2 -8 -3 33.0382 3.74509 4 -2 8 -3 22.8857 8.42850 10 2 8 3 47.0706 5.29244 6 2 8 3 55.7500 9.32775 7 2 8 3 58.6249 8.79836 3 -2 8 -3 41.2759 4.99557 1 -2 8 -3 38.1632 5.82330 5 -2 8 -3 46.7388 4.62914 4 3 -8 3 327.040 18.7798 1 -3 -8 -3 324.663 18.8862 9 -3 -8 -3 310.420 18.0198 4 3 -8 3 265.167 21.7273 11 3 8 3 274.072 18.6335 6 -3 8 -3 331.893 18.8003 1 -3 8 -3 327.400 19.5527 5 -3 8 -3 326.690 18.4539 4 -3 8 -3 314.484 21.9230 10 -4 -8 -3 228.631 13.6928 4 -4 -8 -3 223.984 15.7614 9 -4 8 -3 226.183 13.8287 4 -4 8 -3 215.908 14.8370 5 -4 8 -3 211.958 17.5140 10 -4 8 -3 225.913 14.0644 1 -5 -8 -3 356.882 25.0088 9 -5 -8 -3 401.392 22.9264 4 5 -8 3 388.562 24.0637 2 -5 8 -3 376.895 26.0210 10 -5 8 -3 411.678 24.1797 5 -5 8 -3 427.143 23.2145 1 -5 8 -3 406.556 23.0637 4 -5 8 -3 329.608 25.9988 9 6 -8 3 31.4912 5.84481 2 -6 -8 -3 33.3161 6.17521 4 6 -8 3 23.4534 7.34781 11 -6 8 -3 36.3559 5.49193 4 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77.1331 6.56506 1 -5 9 3 69.7408 8.86619 5 5 9 -3 71.5400 6.31825 8 4 -9 -3 329.206 19.1425 4 -4 -9 3 302.723 20.4016 9 -4 -9 3 347.334 19.3510 4 4 -9 -3 312.605 18.4821 1 4 9 -3 260.532 19.6309 3 -4 9 3 307.953 21.3937 10 4 9 -3 306.069 18.5576 8 -4 9 3 293.922 21.1052 5 -4 9 3 324.757 18.5749 1 3 -9 -3 975.992 54.1937 1 -3 -9 3 1102.28 54.9883 4 -3 -9 3 942.343 55.2122 9 3 9 -3 993.815 54.3535 8 -3 9 3 852.003 56.3398 5 3 9 -3 954.756 55.2524 3 -3 9 3 940.625 56.7361 10 3 9 -3 1020.93 55.9061 5 3 9 -3 900.906 54.6218 1 -3 9 3 1012.12 54.3299 1 2 -9 -3 10.7029 2.38363 1 -2 -9 3 5.49113 2.95170 9 -2 -9 3 10.3447 3.17761 4 2 -9 -3 6.48597 2.70228 4 -2 9 3 -0.1984 4.37706 7 2 9 -3 -1.4526 5.14081 5 -2 9 3 5.77661 4.49405 1 2 9 -3 6.87292 3.17959 3 -2 9 3 1.57427 5.06787 10 -2 9 3 1.32248 5.36623 5 -2 9 3 0.90003 4.04836 6 2 9 -3 2.25607 3.04946 8 1 -9 -3 254.040 18.1242 4 -1 -9 3 297.394 18.7172 4 1 -9 -3 307.546 18.2254 1 1 9 -3 354.238 18.5548 1 1 9 -3 319.249 18.4968 4 -1 9 3 347.299 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33.5060 9 4 -10 3 610.701 31.9936 1 -4 10 -3 493.629 31.8689 1 -4 10 -3 453.808 34.7773 10 -4 10 -3 560.819 32.0197 4 -4 10 -3 560.774 33.2641 5 5 -10 3 20.2927 4.47042 2 5 -10 3 16.7100 6.07817 11 -5 -10 -3 25.2618 4.75703 4 -5 10 -3 20.6753 4.32415 4 -5 10 -3 17.5811 9.16267 10 -5 10 -3 20.0601 6.18121 5 -5 10 -3 17.5676 4.13129 1 6 -10 3 23.2363 6.97338 11 -6 -10 -3 43.1834 7.73705 4 6 -10 3 33.6263 6.03358 2 -6 10 -3 26.2597 4.37328 1 -6 10 -3 33.3904 5.13652 4 -6 10 -3 27.7826 10.0404 10 -6 10 -3 28.5958 6.39624 5 7 -10 3 63.4607 6.89423 2 -7 -10 -3 52.4983 7.17213 4 -7 10 -3 50.6084 7.41253 4 -7 10 -3 55.1185 12.3247 10 -7 10 -3 54.6281 9.07308 5 -7 10 -3 56.1681 6.33685 1 -8 -11 3 11.3258 5.00367 1 -8 11 3 21.5725 4.94599 1 -8 11 3 16.0016 7.94092 10 -7 -11 3 131.924 14.9177 4 7 -11 -3 160.264 12.9018 11 7 -11 -3 178.448 10.3709 1 -7 11 3 140.804 14.6679 10 -7 11 3 161.263 11.3197 1 -6 -11 3 34.8013 7.07760 4 6 -11 -3 56.1259 5.22140 1 6 11 -3 49.0585 5.89070 8 6 11 -3 47.8514 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544.074 32.8693 10 -2 11 3 522.563 31.2163 5 -1 -11 3 499.973 35.5386 11 1 -11 -3 500.819 28.5426 1 1 -11 -3 476.200 28.6651 4 -1 -11 3 459.240 29.1802 4 -1 11 3 548.889 30.8061 7 -1 11 3 546.138 30.7289 6 1 11 -3 496.271 28.6259 1 1 11 -3 508.917 29.8884 5 1 11 -3 481.503 28.9136 3 -1 11 3 491.525 29.9597 5 -1 11 3 501.018 30.5933 10 1 11 -3 489.176 28.8557 8 0 -11 3 160.625 12.0224 4 0 -11 -3 175.211 11.1856 4 0 -11 -3 170.533 11.0614 1 0 -11 3 183.026 11.8649 1 0 -11 3 189.893 15.6797 11 0 11 3 191.241 13.5957 6 0 11 -3 164.747 12.6557 5 0 11 -3 181.328 12.0747 4 0 11 3 180.342 13.3372 10 0 11 -3 174.278 11.8131 3 0 11 -3 190.295 14.1160 10 0 11 3 187.423 14.0153 5 0 11 -3 174.737 11.1492 1 0 11 3 182.488 14.0214 7 -1 -11 -3 810.361 45.0093 4 1 -11 3 808.270 45.9218 4 1 -11 3 817.660 45.5635 1 1 -11 3 860.159 48.3534 11 1 11 3 821.340 47.2587 7 -1 11 -3 777.020 46.9893 10 -1 11 -3 841.106 46.9434 5 -1 11 -3 841.635 46.1325 3 -1 11 -3 838.731 45.8769 4 -1 11 -3 783.582 45.3043 1 1 11 3 769.084 47.0637 5 1 11 3 723.119 47.0359 6 -2 -11 -3 60.7496 7.09610 1 2 -11 3 54.8156 5.21125 1 2 -11 3 40.4473 7.93145 11 -2 -11 -3 43.5616 4.07717 4 2 11 3 38.8649 7.26024 7 -2 11 -3 44.9107 8.37665 10 -2 11 -3 46.0899 4.85707 1 -2 11 -3 58.2562 6.45298 4 2 11 3 32.6888 6.99821 5 -2 11 -3 41.7652 6.92998 5 2 11 3 42.1237 7.38518 6 -2 11 -3 50.5849 6.77076 3 3 -11 3 94.5153 10.3503 11 -3 -11 -3 92.5979 6.69228 4 3 -11 3 84.2951 7.13042 1 -3 11 -3 77.3784 14.0536 10 -3 11 -3 76.3247 9.87048 5 -3 11 -3 83.5963 7.16355 1 4 -11 3 12.4258 4.21427 1 4 -11 3 9.05601 3.16240 2 -4 -11 -3 12.4726 4.06298 4 -4 11 -3 2.41023 8.42055 10 -4 11 -3 7.63572 5.37858 5 -4 11 -3 3.66828 3.91438 4 -4 11 -3 9.46446 3.06196 1 -4 11 -3 23.9926 8.46157 6 5 -11 3 531.485 29.6952 2 5 -11 3 569.141 33.4802 11 -5 -11 -3 456.025 29.5708 4 -5 11 -3 456.681 29.2925 1 -5 11 -3 498.421 31.2723 5 -5 11 -3 505.149 29.8280 4 6 -11 3 589.529 32.0670 2 -6 -11 -3 509.342 32.2727 4 6 -11 3 604.327 35.7677 11 -6 11 -3 520.766 31.5677 1 -6 11 -3 533.841 33.2448 5 -6 11 -3 522.948 32.3464 4 7 -11 3 158.153 19.0123 11 -7 -11 -3 157.821 14.2441 4 7 -11 3 196.833 11.9855 2 -7 11 -3 161.216 13.9234 5 -7 11 -3 185.770 11.4999 1 7 -12 -3 -2.3114 3.20447 11 -7 -12 3 8.40459 7.71505 4 7 -12 -3 -0.4602 2.90662 1 -7 12 3 0.76909 6.64228 10 -7 12 3 9.53864 4.38883 1 -6 -12 3 3.73898 6.37195 4 6 -12 -3 11.8811 2.76155 1 -6 12 3 5.44046 8.74998 5 6 12 -3 14.6927 4.24524 3 -6 12 3 13.6903 4.27922 1 -6 12 3 17.0961 7.10028 10 6 12 -3 10.9847 3.82625 8 -5 -12 3 60.9061 9.31366 4 5 -12 -3 42.1842 8.90476 11 -5 12 3 64.6073 9.75330 10 4 -12 -3 738.157 40.5099 4 4 -12 -3 751.265 42.6830 11 4 -12 -3 718.910 40.4823 1 -4 -12 3 693.130 42.6935 9 -4 12 3 731.364 42.3518 5 -4 12 3 600.808 40.6833 1 4 12 -3 750.556 41.4481 3 -4 12 3 735.208 45.0951 6 3 -12 -3 618.446 33.4329 4 3 -12 -3 623.391 35.4868 11 -3 -12 3 538.132 36.0263 9 3 -12 -3 601.506 33.1843 1 -3 -12 3 486.856 34.1999 4 -3 12 3 589.315 34.8638 5 3 12 -3 592.080 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5.59154 1 -6 6 4 8.81981 2.95475 1 6 6 -4 9.05576 3.65586 3 -5 -6 4 1048.09 60.7078 4 5 -6 -4 1069.12 60.2138 8 -5 -6 4 1125.88 62.3071 9 5 -6 -4 1090.62 60.2209 1 -5 6 4 1075.79 62.2664 10 5 6 -4 1027.23 60.8688 8 5 6 -4 1169.13 61.3399 3 5 6 -4 1047.22 60.6459 1 -5 6 4 1089.51 60.5783 1 4 -6 -4 515.693 30.6974 4 -4 -6 4 516.350 30.5634 4 4 -6 -4 545.589 30.2511 8 -4 -6 4 537.888 31.5474 9 4 -6 -4 543.581 30.1538 1 -4 6 4 531.415 30.5128 1 -4 6 4 549.275 32.4569 10 -4 6 4 516.095 31.8816 5 4 6 -4 561.677 31.3797 3 4 6 -4 495.004 30.8978 8 4 6 -4 552.620 30.7707 1 -3 -6 4 109.648 8.99019 9 3 -6 -4 113.196 7.27293 1 3 -6 -4 120.151 8.20274 8 -3 -6 4 107.914 7.77989 4 3 -6 -4 121.602 7.31229 4 -3 6 4 95.4960 11.4669 7 -3 6 4 110.009 8.43317 6 3 6 -4 108.627 8.39823 1 -3 6 4 107.766 8.12016 1 3 6 -4 112.297 8.71820 8 3 6 -4 102.742 9.17172 4 3 6 -4 113.768 9.35339 5 3 6 -4 112.521 8.99422 3 2 -6 -4 5.14327 1.53726 4 -2 -6 4 2.19591 2.63268 9 -2 -6 4 2.72058 2.25648 4 2 -6 -4 5.89114 1.79750 1 2 6 -4 4.01659 2.88382 4 -2 6 4 1.00371 3.87302 1 2 6 -4 0.82148 4.63282 5 2 6 -4 8.15627 3.43901 8 -2 6 4 5.45761 2.65474 6 2 6 -4 4.98262 2.33669 1 2 6 -4 3.45116 3.36103 3 -2 6 4 -1.7173 4.45436 7 1 -6 -4 8.14180 2.27064 1 -1 -6 4 7.60896 2.60805 4 -1 -6 4 4.63913 3.53114 11 1 -6 -4 10.5055 1.60985 4 1 6 -4 1.36556 5.92931 5 -1 6 4 1.85024 3.31211 2 -1 6 4 4.84889 5.95056 10 -1 6 4 7.51362 2.74261 6 1 6 -4 9.49810 2.68016 4 0 -6 4 2141.69 121.669 2 0 -6 4 2347.75 123.421 11 0 -6 4 2217.01 121.006 4 0 -6 -4 2168.86 120.500 4 0 6 4 2137.09 121.654 7 0 6 4 2244.68 121.516 2 0 6 4 2259.32 121.695 6 0 6 -4 2183.56 121.322 1 0 6 -4 2258.58 122.116 5 0 6 4 2002.27 122.638 10 0 6 -4 2258.10 121.312 4 0 6 -4 2141.58 121.965 3 1 -6 4 736.505 39.9176 11 -1 -6 -4 652.511 36.3611 9 1 -6 4 669.460 37.1716 1 1 -6 4 630.297 37.7130 2 1 6 4 655.962 37.4807 6 1 6 4 669.735 37.4557 2 -1 6 -4 614.477 38.0634 5 -1 6 -4 655.720 37.0901 1 1 6 4 643.546 37.6580 7 -1 6 -4 651.178 37.1088 4 2 -6 4 376.904 20.7900 1 -2 -6 -4 355.107 19.7664 9 2 -6 4 337.901 21.0032 2 -2 6 -4 296.318 20.2759 1 2 6 4 348.804 20.4386 6 -2 6 -4 360.330 20.1088 4 -2 6 -4 368.152 21.2749 5 -2 6 -4 326.198 25.5578 10 2 6 4 343.265 20.6258 2 3 -6 4 1374.64 73.1504 11 3 -6 4 1258.61 70.8188 2 -3 -6 -4 1232.10 69.8363 9 -3 6 -4 1271.23 69.9301 4 -3 6 -4 1242.40 70.0432 1 3 6 4 1279.67 70.6033 2 -3 6 -4 1260.04 70.6146 5 3 6 4 1155.12 70.8006 7 -3 6 -4 1251.15 71.9249 10 -4 -6 -4 471.809 27.7472 9 4 -6 4 513.220 31.0958 11 -4 -6 -4 419.175 27.2161 4 4 -6 4 487.525 28.5762 2 -4 6 -4 485.799 30.2742 10 -4 6 -4 473.304 27.3940 4 -4 6 -4 491.952 27.6216 1 5 -6 4 89.6147 12.5588 11 5 -6 4 74.4262 7.92638 2 5 -6 4 70.0739 8.93033 7 -5 -6 -4 79.6838 6.84241 4 -5 6 -4 81.9807 13.0312 10 -5 6 -4 75.5083 6.58982 4 -5 6 -4 87.2047 7.13933 1 -5 6 -4 81.3297 11.3572 9 6 -6 4 -7.8302 6.11734 11 -6 -6 -4 4.45102 3.56205 4 6 -6 4 1.37161 4.08575 2 -6 6 -4 2.40613 3.51749 1 -6 6 -4 8.90256 10.3229 10 -6 6 -4 3.97381 2.84028 4 -6 6 -4 2.93412 4.13354 5 -7 -6 -4 41.2909 7.18207 4 7 -6 4 47.7387 7.16782 2 -7 6 -4 51.2212 7.84724 5 -7 6 -4 50.3729 12.0630 10 -7 6 -4 42.4766 6.19719 4 -7 6 -4 41.9029 6.14087 1 8 -6 4 160.370 15.2617 2 -8 -6 -4 156.297 17.2418 10 -8 -6 -4 164.354 13.0846 4 -8 6 -4 168.377 12.6020 5 -8 6 -4 137.379 12.0298 4 -8 -7 4 44.4117 7.93592 10 -8 -7 4 37.7146 9.29423 4 -8 -7 4 33.6281 5.15522 1 -8 7 4 50.0852 5.81994 1 8 7 -4 28.9015 5.08875 8 -8 7 4 37.6943 7.65754 10 7 -7 -4 184.106 17.6183 11 -7 -7 4 192.109 14.5095 4 7 -7 -4 174.187 12.8381 1 7 7 -4 225.592 12.8073 8 -7 7 4 197.054 15.6920 10 -7 7 4 193.777 12.5810 1 6 -7 -4 40.6795 5.67130 8 -6 -7 4 40.7419 7.07836 4 6 -7 -4 39.3412 5.37092 1 6 7 -4 44.6526 6.64841 3 -6 7 4 38.2040 7.56573 10 6 7 -4 44.6110 5.93502 8 -6 7 4 49.1908 5.73226 1 5 -7 -4 33.8199 5.14877 8 5 -7 -4 32.6413 3.91588 1 -5 -7 4 34.9820 7.48115 9 -5 -7 4 20.7227 5.12256 4 5 -7 -4 34.5114 6.22683 4 -5 7 4 32.6898 6.13778 10 5 7 -4 28.3938 4.97954 3 -5 7 4 26.7205 3.78385 1 5 7 -4 39.7677 5.50330 8 5 7 -4 25.1889 4.84457 1 4 -7 -4 6.69614 1.95927 1 4 -7 -4 5.30946 3.23350 8 -4 -7 4 1.50640 3.67752 4 -4 -7 4 11.9180 4.74429 9 4 -7 -4 8.03370 3.74615 4 -4 7 4 9.96435 3.00680 1 4 7 -4 8.84854 3.77147 3 4 7 -4 5.71338 3.26413 1 -4 7 4 1.80908 5.13185 10 4 7 -4 5.24557 2.91983 8 -3 -7 4 406.016 23.3940 4 3 -7 -4 405.978 22.8763 1 -3 -7 4 360.790 24.1042 9 3 -7 -4 423.819 23.1916 4 3 7 -4 418.811 24.3884 5 3 7 -4 406.690 23.9197 4 3 7 -4 333.891 24.1020 3 -3 7 4 387.678 25.6698 7 -3 7 4 383.414 23.2274 1 -3 7 4 426.170 27.0343 5 -3 7 4 416.411 24.3030 6 -3 7 4 431.420 26.1362 10 3 7 -4 420.280 23.7971 8 3 7 -4 402.628 23.7404 1 -2 -7 4 2404.54 129.795 9 -2 -7 4 2338.37 129.331 4 2 -7 -4 2291.61 128.943 1 2 -7 -4 2464.59 129.022 4 2 7 -4 2062.26 129.508 1 -2 7 4 2312.07 129.267 1 -2 7 4 2369.51 130.902 7 2 7 -4 2420.19 129.625 4 2 7 -4 2408.98 130.418 5 -2 7 4 2079.74 130.980 10 2 7 -4 2491.55 129.747 8 -2 7 4 2490.58 130.230 6 -1 -7 4 2168.41 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4 3 4 6 669.223 39.2990 7 -3 4 -6 703.009 39.4794 5 -4 -4 -6 1533.18 85.5613 9 4 -4 6 1612.45 85.6035 7 4 -4 6 1647.15 85.6617 2 4 -4 6 1497.08 87.2108 11 4 4 6 1533.73 85.1511 2 -4 4 -6 1393.42 84.7979 1 -4 4 -6 1462.96 85.3988 4 5 -4 6 58.2100 6.78315 2 5 -4 6 53.1520 11.0645 11 -5 -4 -6 58.8705 6.32158 4 -5 -4 -6 61.3348 9.79150 9 -5 4 -6 44.2895 7.39558 1 5 4 6 65.6614 8.58257 2 -5 4 -6 58.9667 5.75130 4 -6 -4 -6 263.946 16.9269 4 -6 -4 -6 243.173 22.3946 10 6 -4 6 292.233 17.6784 2 -6 4 -6 250.640 17.4814 1 -6 4 -6 274.124 16.6918 4 -6 4 -6 301.016 18.3440 5 -7 -4 -6 4.96831 4.61376 4 7 -4 6 7.84184 3.98873 2 -7 4 -6 6.42918 5.10674 5 -7 4 -6 6.12074 3.62815 4 -7 4 -6 7.72954 5.13488 1 8 -5 -6 36.7948 4.83720 8 -8 -5 6 38.6414 6.18267 1 -8 -5 6 41.9553 16.9275 10 8 5 -6 37.2113 5.22426 8 -8 5 6 37.8546 8.73127 10 -8 5 6 42.4264 6.20205 1 -7 -5 6 203.471 16.7517 10 7 -5 -6 200.603 12.3885 1 7 -5 -6 196.302 12.4518 8 -7 5 6 194.718 13.0216 1 -7 5 6 193.350 16.6831 10 -6 -5 6 382.056 24.4038 10 6 -5 -6 362.026 20.9047 8 6 -5 -6 370.822 21.2651 1 6 5 -6 352.123 22.5493 1 6 5 -6 302.089 21.8660 8 -5 -5 6 308.759 23.2482 9 5 -5 -6 355.858 19.2453 1 5 -5 -6 322.575 20.3486 4 5 -5 -6 362.741 20.0746 8 -5 5 6 313.208 19.6820 1 5 5 -6 325.761 20.1003 3 -5 5 6 352.949 22.6501 10 5 5 -6 274.632 19.9989 8 5 5 -6 341.912 19.7291 1 -4 -5 6 3.40609 4.24515 4 4 -5 -6 5.94291 2.01373 4 4 -5 -6 5.26573 1.89223 1 4 -5 -6 6.83273 2.83237 8 -4 -5 6 8.28521 5.16243 9 -4 5 6 11.3060 6.49918 10 4 5 -6 10.1603 3.36644 3 4 5 -6 6.11456 2.68185 1 -4 5 6 8.87268 4.73919 6 -4 5 6 3.14857 3.43292 1 4 5 -6 -1.1402 4.07484 4 4 5 -6 4.51626 3.44347 8 -4 5 6 16.2363 7.84797 7 3 -5 -6 2098.34 109.307 4 3 -5 -6 1937.82 109.162 8 3 -5 -6 1952.75 109.165 1 -3 5 6 2001.79 110.569 7 -3 5 6 1996.65 110.045 6 -3 5 6 1986.18 112.110 10 3 5 -6 2100.96 109.760 1 3 5 -6 2082.90 110.205 3 3 5 -6 1704.62 110.009 8 -3 5 6 1938.34 110.867 2 2 -5 -6 3.83230 3.75307 8 -2 -5 6 0.41153 6.54423 2 -2 -5 6 4.75537 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6 -6 720.116 38.9396 1 -4 6 6 645.199 39.4711 6 -4 6 6 599.866 40.8123 7 -3 -6 6 14.8982 4.29178 9 3 -6 -6 10.9265 1.97502 4 -3 -6 6 1.27872 4.28541 4 3 -6 -6 7.38855 1.95473 1 3 -6 -6 14.3206 4.82281 8 -3 6 6 1.64353 5.18455 7 3 6 -6 7.42500 3.60071 4 3 6 -6 6.47062 3.87548 3 3 6 -6 6.13320 3.24466 8 -3 6 6 15.5696 4.12961 6 3 6 -6 9.93877 2.94585 1 -3 6 6 9.65458 7.39414 10 2 -6 -6 9.16713 2.12210 1 -2 -6 6 3.55575 3.84606 7 2 -6 -6 7.76288 1.80378 4 2 6 -6 4.27295 2.82710 1 2 6 -6 9.57226 3.46515 8 2 6 -6 4.33328 3.33538 3 2 6 -6 2.31301 6.82205 5 -2 6 6 6.43411 3.20308 6 -2 6 6 9.91872 8.33503 10 2 6 -6 10.0786 3.37508 4 -2 6 6 13.9327 4.53495 2 -2 6 6 10.5156 4.18046 7 -1 -6 6 108.323 9.25700 7 1 -6 -6 118.810 7.22308 4 -1 -6 6 86.1390 11.9009 2 -1 6 6 131.515 15.3355 10 -1 6 6 108.485 8.81977 7 1 6 -6 118.513 14.0769 5 1 6 -6 118.856 8.41823 4 1 6 -6 104.772 8.63697 1 -1 6 6 112.657 8.70373 6 1 6 -6 124.722 9.10556 3 -1 6 6 125.028 9.06186 2 0 -6 6 1819.66 99.4602 11 0 -6 6 1781.73 97.1829 7 0 -6 6 1646.67 97.3388 2 0 -6 -6 1761.00 95.9618 4 0 6 6 1743.32 97.3112 6 0 6 6 1698.25 97.2362 7 0 6 -6 1864.25 96.9176 4 0 6 6 1847.88 97.1798 2 0 6 -6 1538.42 96.7730 1 0 6 -6 1749.61 97.1623 3 1 -6 6 3.22946 3.32274 11 1 -6 6 -3.2893 3.71122 2 -1 6 -6 4.54360 2.89475 1 -1 6 -6 3.28770 2.37826 4 1 6 6 4.31303 3.05905 6 1 6 6 1.66196 2.64589 2 -1 6 -6 4.67907 6.11227 5 1 6 6 2.30095 3.22112 7 2 -6 6 379.804 23.3526 7 2 -6 6 413.080 26.1208 11 -2 -6 -6 399.702 22.4168 9 2 -6 6 391.205 23.8235 2 -2 6 -6 383.585 22.6843 4 2 6 6 391.373 23.5950 7 2 6 6 373.786 22.9831 2 -2 6 -6 372.690 24.1458 5 -2 6 -6 393.241 22.7704 1 3 -6 6 187.080 13.3893 7 3 -6 6 199.249 16.5073 11 3 -6 6 206.214 14.0410 2 -3 -6 -6 194.703 13.1351 9 -3 6 -6 216.304 12.6167 4 -3 6 -6 187.962 12.8907 1 -3 6 -6 217.581 14.4690 5 3 6 6 187.983 13.0657 2 3 6 6 195.057 13.6685 7 4 -6 6 443.291 25.8650 2 4 -6 6 412.761 25.2632 7 -4 -6 -6 403.643 25.6916 9 4 -6 6 422.884 28.0774 11 -4 6 -6 433.666 25.6776 5 -4 6 -6 455.810 24.5410 4 -4 6 -6 349.726 24.4953 1 5 -6 6 145.234 12.1162 7 -5 -6 -6 145.313 10.5146 4 5 -6 6 142.725 12.9361 2 5 -6 6 160.353 18.5898 11 -5 6 -6 144.543 10.1755 4 6 -6 6 13.4073 6.81709 11 6 -6 6 14.0937 4.48411 2 -6 -6 -6 9.65559 4.81258 4 -6 6 -6 19.6492 4.17891 1 -6 6 -6 12.3723 5.42037 5 -6 6 -6 17.9409 3.75485 4 -7 -6 -6 161.718 12.8231 4 7 -6 6 148.289 11.9059 2 -7 6 -6 154.877 12.9990 5 -7 6 -6 151.611 11.2487 1 -7 6 -6 159.619 11.4229 4 8 -7 -6 22.3835 4.12818 1 -8 -7 6 25.0110 4.87989 1 -8 -7 6 21.3074 13.1129 10 -8 7 6 15.3938 9.53643 10 8 7 -6 28.7448 4.50889 8 7 -7 -6 558.085 33.6600 1 7 -7 -6 601.278 34.0484 8 -7 -7 6 628.401 37.3559 10 7 -7 -6 610.156 36.4494 11 7 7 -6 633.721 33.8534 8 -7 7 6 574.520 36.7853 10 -7 7 6 529.657 33.7150 1 6 -7 -6 18.8913 10.8376 11 6 -7 -6 19.4270 4.26442 8 6 -7 -6 21.7086 3.19933 1 6 7 -6 15.5506 3.50683 8 6 7 -6 23.3252 4.59340 3 -6 7 6 17.1031 4.12304 1 -6 7 6 28.1799 7.91518 10 -5 -7 6 32.7195 9.48227 9 5 -7 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59.8313 5.47856 4 4 -4 -10 62.7649 5.22757 1 4 4 -10 67.0093 7.30546 8 -4 4 10 69.7080 12.0887 7 4 4 -10 66.8753 6.01011 1 4 4 -10 47.5625 8.02176 4 3 -4 -10 -0.4029 3.91449 8 3 -4 -10 5.07231 2.29015 1 3 -4 -10 1.39327 2.17866 4 -3 -4 10 3.02112 5.56200 7 -3 4 10 10.3963 5.38628 7 3 4 -10 3.41458 2.73547 1 3 4 -10 -2.3651 3.81408 4 3 4 -10 11.9677 5.73942 3 -3 4 10 -9.7767 6.49455 2 3 4 -10 2.39446 3.90279 8 -2 -4 10 151.756 14.5981 2 2 -4 -10 186.322 11.3839 4 2 -4 -10 171.093 12.5372 8 -2 -4 10 180.164 12.8264 7 2 -4 -10 172.567 11.2737 1 -2 4 10 197.849 13.3252 7 2 4 -10 192.740 11.8976 1 2 4 -10 200.049 14.0597 3 2 4 -10 170.308 12.9508 4 1 -4 -10 47.5527 7.99932 8 1 -4 -10 51.1255 5.02776 4 -1 -4 10 45.0160 6.50067 7 -1 -4 10 45.6656 8.82007 2 1 -4 -10 49.8844 5.75696 1 1 4 -10 36.0680 6.92312 4 1 4 -10 54.9393 7.73799 3 -1 4 10 53.3464 6.70115 7 1 4 -10 60.1393 5.68393 1 0 -4 -10 711.102 39.5121 4 0 -4 -10 688.429 41.8155 8 0 -4 10 699.289 40.7026 7 0 -4 10 699.298 41.4989 2 0 4 10 687.702 40.7161 7 0 4 -10 721.360 40.0367 1 0 4 10 702.275 40.5855 2 1 -4 10 50.2072 7.30534 2 -1 -4 -10 35.1911 5.42386 4 1 -4 10 37.5039 6.20373 7 -1 4 -10 44.0528 6.62521 1 1 4 10 39.3665 5.97499 2 1 4 10 50.5367 6.29871 7 -1 4 -10 56.9670 7.62088 3 2 -4 10 466.877 29.5480 7 -2 -4 -10 456.985 27.4687 4 2 -4 10 480.820 30.5135 2 -2 4 -10 490.698 28.4908 1 2 4 10 453.764 31.7034 2 -2 4 -10 490.256 30.8174 3 -2 4 -10 517.035 28.8657 4 3 -4 10 100.431 9.57912 2 3 -4 10 99.2374 8.93598 7 -3 4 -10 81.3075 8.90770 4 3 4 10 101.025 9.37963 7 3 4 10 105.896 8.74753 2 4 -4 10 137.400 10.7674 2 4 -4 10 128.790 10.6621 7 4 4 10 130.021 10.1754 2 -4 4 -10 130.378 10.7387 4 5 -4 10 8.57367 4.29772 2 5 -4 10 7.51107 6.85594 7 5 4 10 0.73066 4.64917 2 -5 4 -10 12.3215 5.01463 4 7 -5 -10 368.628 27.1458 11 7 -5 -10 336.340 19.3840 1 7 5 -10 314.628 20.0591 1 5 -5 -10 16.4723 4.76592 4 5 -5 -10 18.1335 2.72371 1 5 5 -10 16.8879 3.27359 1 5 5 -10 9.27276 3.72355 8 4 -5 -10 4.74269 2.53515 4 4 -5 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10 901.982 51.1049 2 1 5 10 876.907 51.2421 7 2 -5 10 42.2451 6.75051 7 2 -5 10 45.4847 8.11269 2 2 5 10 45.7670 6.49128 2 -2 5 -10 55.0106 6.95587 4 -2 5 -10 48.3384 8.21210 3 2 5 10 48.7923 7.07811 7 -2 5 -10 49.4989 8.49546 1 3 -5 10 19.4344 5.26049 2 3 -5 10 23.6616 4.76815 7 -3 5 -10 30.4590 5.99018 3 3 5 10 25.0765 5.23888 7 3 5 10 24.4422 4.70102 2 -3 5 -10 25.3656 4.73300 4 4 -5 10 41.2805 7.15067 2 4 -5 10 35.2554 6.84840 7 4 5 10 35.2175 5.28441 2 -4 5 -10 26.7576 5.18515 4 5 -5 10 191.752 13.7215 2 -5 5 -10 184.240 13.4419 4 6 -6 -10 130.169 21.2103 11 6 -6 -10 190.005 22.8911 4 6 -6 -10 194.693 10.6485 1 6 6 -10 166.800 11.3511 8 6 6 -10 169.980 11.5102 1 5 -6 -10 15.4967 2.50920 1 5 -6 -10 8.95633 5.34670 4 5 6 -10 21.6842 6.09047 3 5 6 -10 10.8920 3.25708 1 5 6 -10 10.1030 3.50232 8 4 -6 -10 446.516 25.4230 4 4 -6 -10 434.945 25.1144 1 4 6 -10 470.494 27.0677 3 4 6 -10 487.204 26.1573 1 4 6 -10 405.000 26.7714 4 4 6 -10 398.248 26.2205 8 3 -6 -10 60.6462 5.21526 4 3 -6 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3 11 -12 132.565 9.38010 8 3 11 -12 154.686 9.82329 1 2 -11 -12 37.1284 6.61708 4 2 11 -12 42.7469 4.88224 8 -2 11 12 48.3797 9.13213 7 2 11 -12 56.1759 8.26778 3 2 11 -12 48.9118 5.59093 1 -1 -11 12 36.9414 7.30201 7 1 -11 -12 36.6671 6.48146 4 -1 11 12 17.7237 6.26578 7 1 11 -12 36.9827 8.78102 3 1 11 -12 32.2653 4.65013 8 1 11 -12 33.2263 4.39356 1 0 -11 12 80.7759 12.1719 7 0 11 -12 71.8000 9.40501 4 0 11 -12 81.5374 6.69690 8 0 11 -12 97.6093 7.27121 1 0 11 -12 75.0457 10.9336 3 1 -11 12 20.1882 7.97302 7 -1 11 -12 40.1904 5.37409 1 1 11 12 18.7847 6.32143 7 -1 11 -12 32.3733 5.47955 3 -1 11 -12 29.1316 6.04855 4 2 12 -12 37.2359 5.22594 3 2 12 -12 25.0151 4.31325 8 2 12 -12 23.9692 3.79252 1 -2 12 12 32.8397 5.61691 7 -1 -12 12 229.079 17.6149 7 1 12 -12 234.622 14.5082 8 1 12 -12 240.607 15.1861 3 -1 12 12 227.028 17.2853 7 1 12 -12 266.749 14.7932 1 0 -12 12 10.6322 5.26128 7 0 12 -12 8.83981 2.64420 1 0 12 -12 10.7699 3.03865 8 0 12 -12 4.48154 3.57042 3 0 12 12 7.87753 5.51241 7 5 0 -13 463.158 24.7080 1 5 0 -13 410.171 25.1847 8 4 0 -13 5.72727 3.68974 8 4 0 -13 -7.3626 3.78643 4 4 0 -13 0.30840 1.91132 1 3 0 -13 4.07861 2.25231 1 3 0 -13 4.07490 3.41822 8 -3 0 13 7.52025 9.29205 2 3 0 -13 0.10170 2.92083 4 2 0 -13 0.60704 3.38645 8 -2 0 13 2.67061 3.82011 7 2 0 -13 -2.1680 2.52635 1 -1 0 13 269.682 18.2076 7 1 0 -13 278.940 17.4932 4 1 0 -13 295.727 17.4913 1 -1 0 13 336.363 19.9614 2 1 0 -13 282.414 17.8610 8 0 0 13 3.50563 3.16670 7 0 0 -13 2.72592 4.19451 8 0 0 13 8.68544 4.10411 2 1 0 13 49.5986 6.14702 7 1 0 13 48.3731 6.70705 2 -1 0 -13 53.2800 6.25417 4 -1 0 -13 49.3706 8.06902 8 2 0 13 -0.7285 3.20958 2 2 0 13 0.61853 3.33449 7 -2 0 -13 -3.3960 4.08499 4 3 0 13 428.251 25.3420 7 5 -1 -13 15.7462 2.29708 1 5 1 -13 20.1779 3.80019 8 5 1 -13 14.8016 2.62671 1 4 -1 -13 280.385 16.1759 1 4 -1 -13 270.174 17.5983 8 4 -1 -13 266.413 16.9273 4 4 1 -13 274.732 17.6026 4 4 1 -13 277.770 17.9147 8 4 1 -13 297.159 16.2582 1 3 -1 -13 10.2299 4.11181 8 3 -1 -13 11.0082 2.99542 4 -3 -1 13 -5.1434 6.77867 7 3 -1 -13 15.3403 2.73939 1 3 1 -13 11.1514 2.44614 1 -3 1 13 2.40732 8.71954 2 -3 1 13 4.06967 6.31060 7 3 1 -13 13.4721 3.62497 4 3 1 -13 7.83691 3.36749 8 2 -1 -13 155.754 9.80913 1 -2 -1 13 147.556 16.9504 2 2 -1 -13 139.360 11.3772 8 -2 -1 13 153.028 11.5125 7 2 1 -13 150.283 9.78649 1 2 1 -13 142.825 10.5051 8 -2 1 13 156.174 14.7536 7 1 -1 -13 27.3695 4.78584 8 1 -1 -13 32.7782 4.40928 1 1 -1 -13 25.9048 3.77197 4 -1 -1 13 25.2952 4.41070 7 1 1 -13 35.4144 5.42981 4 1 1 -13 29.7166 4.08874 1 1 1 -13 26.6177 4.74245 8 -1 1 13 33.8844 5.96442 7 0 -1 13 167.940 12.3156 2 0 -1 -13 131.064 11.5149 8 0 -1 13 142.123 10.9067 7 0 1 13 154.215 11.1229 7 0 1 -13 161.288 11.4304 8 0 1 13 155.908 11.4186 2 1 -1 13 -0.1963 2.99139 7 1 -1 13 5.64859 3.89819 2 -1 -1 -13 -0.3797 3.46578 4 -1 -1 -13 -5.5057 5.20467 8 -1 1 -13 1.35862 4.54880 8 1 1 13 2.31442 3.19095 7 1 1 13 4.00756 3.45034 2 -1 1 -13 5.29491 3.85491 4 2 -1 13 220.296 14.7040 7 2 -1 13 231.641 15.1343 2 2 1 13 238.280 14.7752 2 2 1 13 221.670 14.8341 7 3 -1 13 31.3573 4.82631 7 3 1 13 20.2970 4.72160 7 3 1 13 21.0478 5.72916 2 5 -2 -13 111.471 7.70247 1 5 2 -13 132.382 8.00150 1 5 2 -13 124.778 8.77664 8 4 -2 -13 6.85477 2.15852 1 4 -2 -13 -0.4440 3.30443 4 4 2 -13 8.52381 3.54176 8 4 2 -13 3.50029 5.38282 4 4 2 -13 7.55199 2.24676 1 3 -2 -13 -1.5886 2.43443 1 3 -2 -13 -2.1068 2.56738 4 3 2 -13 -7.6498 3.64272 4 3 2 -13 4.97312 2.38047 1 3 2 -13 6.34712 3.30718 8 -3 2 13 -5.4840 6.14338 7 2 -2 -13 6.23107 2.91503 1 -2 -2 13 6.80310 8.56212 2 -2 -2 13 1.26306 4.25832 7 2 -2 -13 3.78399 3.12461 4 2 2 -13 -0.3648 3.52917 8 2 2 -13 0.00678 4.37882 4 2 2 -13 2.32557 2.49411 1 -2 2 13 8.99738 4.22482 7 -1 -2 13 515.534 31.0470 7 -1 2 13 498.518 30.9599 7 1 2 -13 550.594 31.0085 8 1 2 -13 533.437 30.0532 1 1 2 -13 540.451 31.6187 4 0 -2 13 52.0626 6.44459 7 0 -2 13 61.8032 8.81652 2 0 -2 -13 54.3910 5.85109 4 0 2 -13 61.6820 7.96356 8 0 2 13 61.5393 6.81898 7 1 -2 13 41.4702 7.20793 2 1 -2 13 35.0841 5.58753 7 -1 -2 -13 33.1951 5.99247 4 -1 2 -13 40.3274 6.09284 8 -1 2 -13 31.0463 5.28841 4 1 2 13 46.0752 5.98756 2 1 2 13 42.4055 6.04919 7 2 -2 13 3.36135 3.26333 7 2 -2 13 -5.5171 3.68103 2 -2 -2 -13 1.05434 4.90983 4 -2 2 -13 -7.8005 4.55202 4 2 2 13 7.56452 3.33977 2 2 2 13 2.14495 3.41752 7 3 -2 13 237.198 17.0296 2 3 -2 13 201.306 13.4127 7 3 2 13 192.865 12.9912 2 3 2 13 177.906 13.4719 7 4 -3 -13 195.678 11.4858 1 4 -3 -13 169.587 12.0275 4 4 3 -13 193.763 11.6555 1 4 3 -13 199.993 12.4855 8 3 -3 -13 107.314 7.32069 1 3 -3 -13 92.8711 7.41906 4 3 3 -13 102.193 9.49370 4 3 3 -13 109.050 7.42367 1 -3 3 13 110.630 12.3733 7 3 3 -13 103.238 8.42992 8 -2 -3 13 205.951 19.1067 2 2 -3 -13 205.607 13.2832 4 2 -3 -13 227.024 13.5723 1 -2 -3 13 206.416 15.2191 7 -2 3 13 210.842 15.1864 7 2 3 -13 221.320 13.4417 1 -2 3 13 258.597 19.0633 2 2 3 -13 220.167 14.5452 8 2 3 -13 221.405 14.6472 4 1 -3 -13 6.96976 3.45823 4 -1 -3 13 9.04359 6.55049 2 -1 -3 13 5.94575 3.85671 7 -1 3 13 10.9867 3.94678 7 1 3 -13 6.62640 4.44564 8 1 3 -13 6.28499 3.02518 1 0 -3 -13 323.907 19.1509 4 0 -3 13 311.693 20.0695 7 0 3 13 320.108 20.2383 7 0 3 13 344.090 20.3411 2 0 3 -13 350.019 20.4682 4 0 3 -13 303.048 20.5966 8 -1 -3 -13 11.3710 3.82088 4 1 -3 13 12.9705 3.81255 7 1 -3 13 8.56748 4.98177 2 -1 3 -13 7.14636 4.98139 8 1 3 13 13.7975 3.68345 2 1 3 13 13.2365 3.89361 7 -1 3 -13 7.94535 4.70459 4 2 -3 13 44.3116 7.83952 2 2 -3 13 44.6612 6.15696 7 2 3 13 54.1871 6.11174 2 2 3 13 51.8381 6.77213 7 3 -3 13 5.33359 4.42170 2 3 -3 13 1.97857 3.77216 7 3 3 13 6.92610 3.33461 2 3 3 13 -7.0366 4.40931 7 4 -4 -13 42.7291 6.09165 4 4 4 -13 56.4481 7.06439 8 4 4 -13 57.9321 5.18940 1 3 -4 -13 41.6922 5.29569 4 3 -4 -13 64.3086 5.43976 1 -3 4 13 60.8702 10.5478 7 3 4 -13 57.7821 5.51006 1 3 4 -13 57.0365 6.83834 8 -2 -4 13 96.7690 10.5529 7 -2 -4 13 109.940 11.9486 2 2 -4 -13 100.524 8.23674 1 2 -4 -13 103.267 7.35005 4 2 4 -13 93.6671 9.07285 8 2 4 -13 113.767 7.75590 1 2 4 -13 85.3727 9.45953 4 -2 4 13 116.302 13.1526 2 1 -4 -13 189.725 11.5943 4 -1 -4 13 186.057 13.0422 7 -1 -4 13 170.846 15.3878 2 1 4 -13 171.744 13.3492 4 1 4 -13 154.427 13.1428 8 -1 4 13 198.838 13.3386 7 1 4 -13 202.399 11.9915 1 0 -4 13 16.9652 4.06583 7 0 -4 -13 16.5077 3.48471 4 0 4 -13 16.7683 5.03949 8 0 4 -13 13.6856 3.80063 1 0 4 -13 21.5230 5.21360 4 0 4 13 20.7408 4.56591 7 1 -4 13 3.47135 5.11755 2 -1 -4 -13 1.72691 4.14307 4 1 -4 13 5.31567 3.63399 7 1 4 13 7.31566 3.90250 7 -1 4 -13 2.80543 4.88777 4 1 4 13 11.3641 3.62848 2 -1 4 -13 10.0536 4.90091 8 2 -4 13 16.8059 3.94467 7 2 -4 13 13.2545 5.37833 2 -2 4 -13 2.09655 5.48715 4 2 4 13 30.0411 5.43868 2 2 4 13 19.6659 4.49569 7 3 -4 13 445.118 24.1315 7 3 -4 13 377.471 24.4957 2 3 4 13 411.365 23.5925 2 3 4 13 365.798 24.4381 7 4 -5 -13 287.231 18.6307 4 4 -5 -13 299.760 17.8024 1 4 5 -13 344.935 18.8346 1 3 -5 -13 6.67281 4.86129 1 -3 5 13 12.5024 6.27862 7 3 5 -13 5.00416 2.80482 1 3 5 -13 6.02987 3.80251 8 3 5 -13 -3.3585 5.62494 4 2 -5 -13 23.5055 3.25385 4 -2 -5 13 22.6371 6.52953 7 -2 5 13 13.6336 6.45919 2 2 5 -13 17.1207 5.44662 4 2 5 -13 30.6162 5.10647 1 2 5 -13 11.1067 4.29586 8 -1 -5 13 49.5276 7.46708 7 1 -5 -13 45.7981 5.13836 4 -1 -5 13 32.0003 7.77324 2 1 5 -13 46.0640 5.72016 1 1 5 -13 36.8234 6.18461 4 1 5 -13 30.7336 5.39362 8 0 -5 -13 89.6593 7.06622 4 0 -5 13 85.2330 8.19978 7 0 -5 13 70.6797 10.6507 2 0 5 -13 76.7287 7.50613 1 0 5 -13 60.8256 8.45151 8 -1 -5 -13 182.410 14.2153 4 1 -5 13 201.360 13.8435 7 -1 5 -13 180.626 14.0861 8 1 5 13 216.360 14.1435 7 1 5 13 223.545 14.0646 2 2 -5 13 342.309 20.6258 7 2 5 13 327.455 21.4110 7 2 5 13 328.714 20.3287 2 4 -6 -13 -0.3203 2.63600 1 4 -6 -13 12.9062 5.07303 4 4 6 -13 4.25135 3.49347 8 4 6 -13 0.58405 3.03840 1 3 -6 -13 8.28620 3.22821 1 3 -6 -13 -2.2345 2.97078 4 3 6 -13 4.92207 3.06636 1 3 6 -13 7.59908 3.86574 8 3 6 -13 -10.303 6.07845 4 -3 6 13 1.96839 9.24246 7 -2 -6 13 3.85250 7.18600 7 2 -6 -13 14.0439 2.95757 4 2 6 -13 13.8895 3.73964 1 2 6 -13 12.6652 3.99832 8 2 6 -13 9.13992 5.44437 4 -2 6 13 13.5825 6.16137 7 -2 6 13 0.41286 5.89933 2 1 -6 -13 366.999 21.1509 4 -1 -6 13 350.615 22.9630 7 1 6 -13 370.536 22.4203 8 1 6 -13 319.191 22.6414 4 -1 6 13 413.933 24.4678 2 1 6 -13 378.667 21.8409 1 0 -6 13 94.4491 11.4960 2 0 -6 -13 116.796 8.32262 4 0 -6 13 115.067 9.93181 7 0 6 -13 98.3621 9.03078 1 0 6 -13 124.322 9.49463 8 0 6 -13 102.878 10.3601 4 1 -6 13 8.81040 5.55275 2 1 -6 13 10.3070 4.31297 7 -1 6 -13 20.9813 5.32396 4 -1 6 -13 18.2847 4.35369 8 2 -6 13 101.313 11.0491 7 2 -6 13 82.1021 9.94504 2 2 6 13 101.582 10.5353 7 2 6 13 99.0603 9.45634 2 -2 6 -13 87.8685 10.1108 4 3 -7 -13 249.354 15.6821 4 3 -7 -13 258.172 15.5592 1 3 7 -13 234.028 15.5889 1 3 7 -13 267.537 15.6759 8 2 -7 -13 249.903 14.8312 4 -2 7 13 231.951 17.6380 7 2 7 -13 246.754 16.6689 4 2 7 -13 236.630 15.5435 1 2 7 -13 261.561 15.5844 8 1 -7 -13 5.02589 3.12976 4 -1 -7 13 17.3408 5.97433 7 -1 7 13 -4.8382 5.91429 2 1 7 -13 3.73542 5.03150 4 1 7 -13 13.4710 3.72014 8 1 7 -13 8.50291 3.81229 1 -1 7 13 11.2499 6.38253 7 0 -7 13 293.126 20.0103 7 0 -7 13 270.000 20.4096 2 0 -7 -13 339.599 18.6354 4 0 7 13 368.411 21.4344 7 0 7 -13 295.028 19.6700 4 0 7 -13 292.950 19.0556 1 0 7 -13 318.349 19.1185 8 1 -7 13 91.3622 9.86826 2 1 -7 13 85.8799 9.00456 7 -1 7 -13 77.6670 9.32919 4 -1 7 -13 96.9430 8.01196 8 2 -7 13 3.78257 4.88680 2 2 -7 13 10.5289 4.62391 7 2 7 13 -0.6315 6.11106 2 -2 7 -13 0.86304 3.44373 8 2 7 13 7.98467 5.95619 7 -2 7 -13 -3.4531 5.91840 1 -2 7 -13 -1.5342 5.12698 4 3 8 -13 5.15388 3.01021 8 -3 8 13 9.20529 6.32488 7 3 8 -13 7.67109 3.41557 1 2 -8 -13 132.271 9.16135 4 -2 -8 13 80.2683 15.9184 7 -2 8 13 92.2646 11.6183 7 2 8 -13 118.766 11.1583 4 1 -8 -13 141.738 9.35327 4 1 8 -13 127.534 10.8516 4 1 8 -13 131.904 9.13987 8 1 8 -13 94.3893 9.56464 1 -1 8 13 110.274 12.1168 7 0 -8 13 11.1326 5.54122 7 0 8 -13 12.6735 5.01018 4 0 8 13 24.8645 6.60166 7 0 8 -13 18.4675 3.74320 8 0 8 13 17.8192 6.64820 2 1 -8 13 -5.0400 5.90649 2 1 8 13 9.91045 6.19284 2 -1 8 -13 0.13793 4.61293 4 -1 8 -13 2.33411 4.52252 1 1 8 13 2.28894 6.11378 7 -1 8 -13 6.36713 8.44570 3 2 -9 -13 20.2894 5.53001 4 -2 9 13 7.05438 6.06938 7 2 9 -13 11.0550 3.91521 1 2 9 -13 20.3335 3.79705 8 1 -9 -13 9.79999 6.44481 4 -1 -9 13 5.77831 6.69380 7 1 9 -13 0.82986 6.57425 1 -1 9 13 0.39239 8.47555 7 1 9 -13 -0.8743 3.68970 8 1 9 -13 -1.7203 5.95015 4 0 -9 13 1.94007 5.42005 7 0 9 -13 18.1339 5.08481 4 0 9 -13 17.6091 7.88116 3 0 9 13 8.61659 6.10342 2 0 9 -13 13.7597 3.92382 1 0 9 13 -7.1193 8.27777 7 -1 9 -13 102.218 7.53929 8 1 9 13 87.6499 10.8537 7 1 10 -13 63.6684 5.36387 8 -1 10 13 41.0437 7.30402 7 3 0 -14 2.06214 3.67555 4 3 0 -14 7.89045 2.61059 1 2 0 -14 230.558 14.0637 4 -2 0 14 208.914 19.4657 7 2 0 -14 233.598 13.7676 1 0 0 -14 62.3236 6.39345 4 0 0 14 57.5140 6.55185 7 1 0 14 -1.6165 3.77100 7 1 0 14 7.59605 4.98695 2 -1 0 -14 4.33205 4.17445 4 3 -1 -14 483.230 26.4885 1 3 -1 -14 449.777 26.8574 4 3 1 -14 473.125 27.2885 4 3 1 -14 460.509 27.0800 8 3 1 -14 487.799 26.5226 1 -3 1 14 457.676 30.6668 7 2 -1 -14 22.6485 3.67275 4 2 -1 -14 26.3762 3.79969 1 -2 -1 14 14.2009 9.78202 2 -2 -1 14 27.5227 6.46263 7 2 1 -14 25.9255 4.24803 4 2 1 -14 30.9769 4.65262 1 -2 1 14 26.5326 10.1888 2 2 1 -14 28.3743 4.60638 8 -1 -1 14 11.8812 4.07407 7 -1 -1 14 29.2056 8.19340 2 1 1 -14 0.61148 4.38945 8 1 1 -14 1.32190 3.82138 1 1 1 -14 8.91750 3.56320 4 -1 1 14 7.67988 3.74111 7 0 -1 -14 15.0532 3.62359 4 0 -1 14 11.4590 3.69321 7 0 -1 14 23.5828 5.81012 2 0 1 -14 17.5269 5.07167 8 0 1 14 10.8001 3.67328 7 0 1 -14 14.3211 3.95183 4 1 -1 14 222.903 16.7329 7 1 1 14 262.528 18.3737 7 1 1 14 239.813 17.0728 2 3 -2 -14 -3.5083 2.75576 1 3 -2 -14 -4.5417 3.09935 4 3 2 -14 2.94602 2.47038 1 -3 2 14 16.0435 8.67787 7 3 2 -14 -1.7591 3.95844 8 3 2 -14 -9.9217 4.75627 4 -2 -2 14 208.075 15.6307 7 2 -2 -14 194.951 13.9482 1 2 -2 -14 226.282 13.4101 4 2 2 -14 219.080 13.2725 1 -2 2 14 201.319 17.7864 7 2 2 -14 227.410 14.3386 4 -2 2 14 269.028 19.4872 2 2 2 -14 221.301 14.0891 8 1 -2 -14 3.96190 2.98390 4 -1 -2 14 6.88067 4.06308 7 1 2 -14 4.50053 4.42045 8 1 2 -14 9.68195 4.10585 4 1 2 -14 3.00576 3.52670 1 -1 2 14 13.3590 4.07532 7 0 -2 14 83.2595 7.87529 7 0 -2 14 77.8668 11.1758 2 0 -2 -14 86.3454 7.54462 4 0 2 14 92.2521 8.03808 7 0 2 -14 104.597 9.12491 8 0 2 -14 92.7500 8.49063 4 1 -2 14 30.7569 5.75898 2 -1 2 -14 19.5346 5.61822 8 1 2 14 37.7920 7.59071 7 3 -3 -14 241.964 15.9125 4 3 -3 -14 253.421 15.7426 1 -3 3 14 311.284 20.2974 7 3 3 -14 270.398 15.6954 1 3 3 -14 272.953 16.4558 8 -2 -3 14 77.9843 10.5278 7 2 -3 -14 70.8806 6.50195 4 2 3 -14 87.0231 7.95477 8 2 3 -14 71.7970 8.72032 4 2 3 -14 90.7581 6.60245 1 -2 3 14 74.1577 10.1891 7 -2 3 14 86.0165 10.5541 2 -1 -3 14 71.0001 10.8973 2 -1 -3 14 108.122 10.0986 7 1 -3 -14 98.8094 7.57861 4 1 3 -14 91.4892 9.60597 8 -1 3 14 111.862 9.38386 7 1 3 -14 104.607 9.33556 4 0 -3 14 20.9946 7.57761 2 0 -3 14 35.6533 6.07607 7 0 -3 -14 29.2182 4.24549 4 0 3 -14 30.7473 5.48126 8 0 3 14 44.8259 6.38287 7 0 3 -14 29.3630 5.36523 4 1 -3 14 352.649 20.4596 7 -1 3 -14 289.099 20.5710 8 1 3 14 360.536 20.3880 2 1 3 14 323.592 20.2332 7 3 4 -14 11.2877 3.98225 8 -2 -4 14 183.787 16.1610 7 2 -4 -14 205.011 11.8988 4 -2 4 14 209.711 14.8399 7 2 4 -14 158.810 13.8535 4 2 4 -14 184.209 12.9890 8 1 -4 -14 161.157 9.98345 4 -1 -4 14 160.593 12.0299 7 -1 -4 14 124.951 13.1447 2 1 4 -14 135.412 11.2038 8 1 4 -14 149.581 11.9371 4 0 -4 14 41.1383 7.25703 2 0 4 -14 34.2901 5.73980 8 0 4 -14 48.5073 8.50660 4 1 -4 14 18.0924 5.87039 2 1 -4 14 26.0833 4.48074 7 -1 4 -14 34.9958 5.47840 8 -2 -5 14 -14.675 8.63571 7 2 -5 -14 5.18810 3.21664 4 2 5 -14 -13.107 7.59634 4 2 5 -14 -1.7047 4.07939 8 2 5 -14 -2.9938 3.17465 1 -2 5 14 -1.6222 5.20407 7 1 -5 -14 -4.6893 3.43954 4 -1 -5 14 4.56719 5.51558 7 1 5 -14 2.77900 3.47736 1 1 5 -14 -10.468 5.53252 4 1 5 -14 1.15058 4.23028 8 -1 5 14 6.78841 6.33762 7 -1 5 14 -1.1521 8.97154 2 0 -5 14 3.89099 6.52959 2 0 -5 14 28.0780 5.22550 7 0 5 -14 16.2700 5.93422 4 0 5 -14 16.7086 4.85766 8 -1 -6 14 0.39866 5.89344 7 -1 6 14 0.83166 5.61910 2 -1 6 14 2.04460 5.36183 7 1 6 -14 5.11464 3.72023 1 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details ) SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ) _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.1560 _exptl_absorpt_correction_T_min 0.0455 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 1.54185 8.224 19.248 12.863 89.970 95.944 90.001 ) ; _shelx_hkl_checksum 4061 _olex2_diffrn_ambient_temperature_device 'Oxford 700' _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group W1 W 0.37302(4) 0.51422(2) 0.76061(2) 0.03770(12) Uani 1 1 d . . . . . Ga1 Ga 0.49211(9) 0.71995(4) 0.66006(6) 0.03588(19) Uani 1 1 d . . . . . Cl1 Cl 0.72784(19) 0.66408(8) 0.68866(14) 0.0481(4) Uani 1 1 d . . . . . S1 S 0.3079(2) 0.64387(8) 0.73533(12) 0.0429(4) Uani 1 1 d . . . . . S2 S 0.4620(3) 0.80606(12) 0.7766(4) 0.0416(8) Uani 0.881(13) 1 d . . P A 1 S2A S 0.438(2) 0.8146(10) 0.731(3) 0.0416(8) Uani 0.119(13) 1 d . . P A 2 O1 O 0.4387(6) 0.3608(3) 0.8359(4) 0.0597(13) Uani 1 1 d . . . . . O2 O 0.6410(7) 0.5004(3) 0.6002(5) 0.0663(15) Uani 1 1 d . . . . . O3 O 0.0986(8) 0.5258(3) 0.9174(5) 0.0763(18) Uani 1 1 d . . . . . O4 O 0.1113(7) 0.4563(3) 0.5815(4) 0.0670(15) Uani 1 1 d . . . . . O5 O 0.6477(9) 0.5615(4) 0.9383(5) 0.097(2) Uani 1 1 d . . . . . N1 N 0.3574(7) 0.7023(3) 0.5162(4) 0.0504(14) Uani 1 1 d . . . . . N2 N 0.5745(7) 0.7995(3) 0.5606(5) 0.0569(15) Uani 1 1 d . . . . . C1 C 0.4158(8) 0.4176(4) 0.8070(5) 0.0487(17) Uani 1 1 d . . . . . C2 C 0.5449(9) 0.5078(3) 0.6570(6) 0.0463(16) Uani 1 1 d . . . . . C3 C 0.1986(10) 0.5208(4) 0.8614(6) 0.0530(18) Uani 1 1 d . . . . . C4 C 0.2038(9) 0.4787(3) 0.6450(5) 0.0474(17) Uani 1 1 d . . . . . C5 C 0.5493(10) 0.5454(4) 0.8742(6) 0.059(2) Uani 1 1 d . . . . . C6 C 0.1494(8) 0.6573(4) 0.6269(6) 0.0552(18) Uani 1 1 d . . . . . H6A H 0.061879 0.622207 0.629945 0.066 Uiso 1 1 calc R . . . . H6B H 0.100401 0.703946 0.632249 0.066 Uiso 1 1 calc R . . . . C7 C 0.2243(9) 0.6507(4) 0.5237(6) 0.0538(18) Uani 1 1 d . . . . . H7A H 0.268516 0.603239 0.517496 0.065 Uiso 1 1 calc R . . . . H7B H 0.138187 0.657944 0.464952 0.065 Uiso 1 1 calc R . . . . C8 C 0.4691(10) 0.6737(4) 0.4400(6) 0.063(2) Uani 1 1 d . . . . . H8A H 0.536605 0.636063 0.474603 0.075 Uiso 1 1 calc R . . . . H8B H 0.401600 0.653246 0.379476 0.075 Uiso 1 1 calc R . . . . C9 C 0.5797(11) 0.7277(4) 0.4013(7) 0.066(2) Uani 1 1 d . . . . . H9A H 0.512323 0.758978 0.353235 0.079 Uiso 1 1 calc R . . . . H9B H 0.657829 0.703941 0.359727 0.079 Uiso 1 1 calc R . . . . C10 C 0.6780(10) 0.7728(5) 0.4836(7) 0.066(2) Uani 1 1 d . . . . . H10A H 0.767884 0.744883 0.519773 0.079 Uiso 1 1 calc R . . . . H10B H 0.727246 0.812265 0.448677 0.079 Uiso 1 1 calc R . . . . C11 C 0.2894(9) 0.7722(4) 0.4827(5) 0.0512(17) Uani 1 1 d . . . . . H11A H 0.193425 0.782739 0.520508 0.061 Uiso 1 1 calc R . . . . H11B H 0.252929 0.771440 0.406874 0.061 Uiso 1 1 calc R . . . . C12 C 0.4192(9) 0.8287(4) 0.5057(6) 0.0547(18) Uani 1 1 d . . . . . H12A H 0.442917 0.850612 0.439263 0.066 Uiso 1 1 calc R . . . . H12B H 0.376366 0.865119 0.549965 0.066 Uiso 1 1 calc R . . . . C13 C 0.6688(9) 0.8500(4) 0.6302(7) 0.061(2) Uani 1 1 d . . . . . H13A H 0.697734 0.890493 0.588358 0.073 Uiso 1 1 calc R . . . . H13B H 0.771722 0.827914 0.660368 0.073 Uiso 1 1 calc R . . . . C14 C 0.5731(10) 0.8750(4) 0.7189(6) 0.060(2) Uani 1 1 d . . . . . H14A H 0.494764 0.911317 0.691545 0.071 Uiso 0.881(13) 1 calc R . P A 1 H14B H 0.650117 0.896459 0.773937 0.071 Uiso 0.881(13) 1 calc R . P A 1 H14C H 0.519052 0.920013 0.700822 0.071 Uiso 0.119(13) 1 calc R . P A 2 H14D H 0.646382 0.880655 0.784401 0.071 Uiso 0.119(13) 1 calc R . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 W1 0.04382(19) 0.03635(19) 0.03337(18) -0.00115(12) 0.00607(12) -0.00644(12) Ga1 0.0383(4) 0.0310(4) 0.0393(4) 0.0016(3) 0.0082(3) 0.0003(3) Cl1 0.0388(8) 0.0466(9) 0.0595(10) -0.0006(7) 0.0073(7) 0.0047(7) S1 0.0506(9) 0.0391(8) 0.0407(8) 0.0015(7) 0.0121(7) -0.0047(7) S2 0.0454(11) 0.0376(10) 0.040(2) -0.0056(11) -0.0025(12) 0.0045(8) S2A 0.0454(11) 0.0376(10) 0.040(2) -0.0056(11) -0.0025(12) 0.0045(8) O1 0.054(3) 0.045(3) 0.079(4) 0.023(3) -0.001(3) 0.000(2) O2 0.080(4) 0.048(3) 0.077(4) -0.008(3) 0.036(3) -0.003(3) O3 0.097(4) 0.055(3) 0.086(4) -0.001(3) 0.054(4) -0.009(3) O4 0.089(4) 0.058(3) 0.049(3) 0.009(3) -0.018(3) -0.029(3) O5 0.114(5) 0.118(6) 0.053(3) 0.018(3) -0.022(4) -0.063(5) N1 0.062(4) 0.048(3) 0.041(3) 0.004(3) 0.004(3) -0.006(3) N2 0.053(4) 0.057(4) 0.061(4) 0.011(3) 0.007(3) 0.000(3) C1 0.039(4) 0.065(5) 0.041(4) 0.000(3) -0.001(3) -0.004(3) C2 0.060(4) 0.034(3) 0.047(4) 0.000(3) 0.017(4) 0.000(3) C3 0.067(5) 0.039(4) 0.057(4) 0.004(3) 0.027(4) -0.007(3) C4 0.063(4) 0.040(4) 0.039(4) 0.007(3) 0.000(3) -0.011(3) C5 0.069(5) 0.062(5) 0.045(4) 0.013(4) -0.001(4) -0.025(4) C6 0.040(4) 0.052(4) 0.074(5) -0.007(4) 0.008(3) 0.003(3) C7 0.052(4) 0.051(4) 0.056(4) 0.001(3) -0.005(3) -0.011(3) C8 0.075(5) 0.059(5) 0.055(5) -0.008(4) 0.016(4) 0.006(4) C9 0.075(5) 0.065(5) 0.061(5) 0.000(4) 0.026(4) 0.003(4) C10 0.062(5) 0.073(5) 0.066(5) 0.021(4) 0.022(4) -0.001(4) C11 0.060(4) 0.050(4) 0.042(4) 0.007(3) -0.004(3) -0.007(3) C12 0.055(4) 0.049(4) 0.058(4) 0.016(3) -0.001(3) 0.003(3) C13 0.054(4) 0.052(4) 0.075(5) 0.016(4) -0.005(4) -0.009(4) C14 0.069(5) 0.044(4) 0.062(5) 0.000(3) -0.014(4) -0.001(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ga Ga -1.2846 0.7763 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' W W -5.4734 5.5774 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C1 W1 S1 169.5(2) . . C1 W1 C2 91.5(3) . . C1 W1 C3 89.0(3) . . C1 W1 C4 89.5(3) . . C1 W1 C5 88.2(3) . . C2 W1 S1 97.23(18) . . C2 W1 C4 88.3(3) . . C3 W1 S1 82.4(2) . . C3 W1 C2 178.9(3) . . C3 W1 C4 90.7(3) . . C3 W1 C5 91.2(3) . . C4 W1 S1 96.64(19) . . C5 W1 S1 85.9(2) . . C5 W1 C2 89.8(3) . . C5 W1 C4 177.0(3) . . Cl1 Ga1 S1 102.52(7) . . Cl1 Ga1 S2 113.52(11) . . S2 Ga1 S1 93.63(9) . . S2A Ga1 Cl1 124.5(7) . . S2A Ga1 S1 100.6(6) . . S2A Ga1 N2 74.7(8) . . N1 Ga1 Cl1 116.37(18) . . N1 Ga1 S1 87.60(16) . . N1 Ga1 S2 128.5(2) . . N1 Ga1 S2A 114.3(9) . . N1 Ga1 N2 76.1(2) . . N2 Ga1 Cl1 96.90(17) . . N2 Ga1 S1 158.79(17) . . N2 Ga1 S2 86.3(2) . . Ga1 S1 W1 121.05(7) . . C6 S1 W1 110.9(2) . . C6 S1 Ga1 92.1(3) . . C14 S2 Ga1 99.8(3) . . C14 S2A Ga1 113.5(11) . . C7 N1 Ga1 112.3(4) . . C7 N1 C8 107.5(6) . . C7 N1 C11 111.1(6) . . C8 N1 Ga1 109.3(5) . . C11 N1 Ga1 104.8(4) . . C11 N1 C8 111.9(6) . . C10 N2 Ga1 113.2(5) . . C10 N2 C12 109.9(6) . . C10 N2 C13 109.4(6) . . C12 N2 Ga1 103.9(4) . . C13 N2 Ga1 106.6(4) . . C13 N2 C12 113.8(6) . . O1 C1 W1 178.5(6) . . O2 C2 W1 176.3(6) . . O3 C3 W1 178.5(7) . . O4 C4 W1 177.4(6) . . O5 C5 W1 178.7(7) . . C7 C6 S1 109.4(5) . . N1 C7 C6 111.6(6) . . C9 C8 N1 113.1(6) . . C8 C9 C10 117.3(7) . . N2 C10 C9 111.3(6) . . N1 C11 C12 110.4(6) . . N2 C12 C11 111.5(6) . . N2 C13 C14 112.3(6) . . C13 C14 S2 113.2(5) . . C13 C14 S2A 104.9(9) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 W1 S1 2.5656(17) . W1 C1 1.974(8) . W1 C2 2.044(7) . W1 C3 2.035(7) . W1 C4 2.047(7) . W1 C5 2.039(8) . Ga1 Cl1 2.2147(17) . Ga1 S1 2.3831(17) . Ga1 S2 2.265(3) . Ga1 S2A 2.107(18) . Ga1 N1 2.084(6) . Ga1 N2 2.149(6) . S1 C6 1.826(8) . S2 C14 1.813(8) . S2A C14 1.63(2) . O1 C1 1.164(9) . O2 C2 1.139(8) . O3 C3 1.151(9) . O4 C4 1.141(8) . O5 C5 1.137(9) . N1 C7 1.488(9) . N1 C8 1.513(9) . N1 C11 1.504(9) . N2 C10 1.464(10) . N2 C12 1.503(9) . N2 C13 1.484(10) . C6 C7 1.526(10) . C8 C9 1.500(11) . C9 C10 1.533(12) . C11 C12 1.532(10) . C13 C14 1.529(11) .