Crystallography Open Database

Information card for entry 1556443

Preview

Coordinates	1556443.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H44 N4 Si4 Zn
Calculated formula	C22 H44 N4 Si4 Zn
SMILES	[Zn]1([n]2ccccc2c2[n]1cccc2)(N([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
Title of publication	Reduction of 2,2'-Bipyridine by Quasi-Linear 3d-Metal(I) Silylamides-A Structural and Spectroscopic Study
Authors of publication	Muller, I.; Schneider, C.; Pietzonka, C.; Kraus, F.; Werncke, C.G.
Journal of publication	Inorganics
Year of publication	2019
Journal volume	7
Pages of publication	117
a	18.8806 ± 0.0012 Å
b	18.056 ± 0.0013 Å
c	17.6133 ± 0.0017 Å
α	90°
β	90°
γ	90°
Cell volume	6004.5 ± 0.8 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	29
Hermann-Mauguin space group symbol	P c a 21
Hall space group symbol	P 2c -2ac
Residual factor for all reflections	0.0445
Residual factor for significantly intense reflections	0.034
Weighted residual factors for significantly intense reflections	0.07
Weighted residual factors for all reflections included in the refinement	0.0718
Goodness-of-fit parameter for all reflections included in the refinement	0.969
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
275434 (current)	2022-05-16	cif/1 Fixing some Z values and formulae	1556443.cif
244940	2019-12-06	cif/ Adding structures of 1556443 via cif-deposit CGI script.	1556443.cif