#------------------------------------------------------------------------------ #$Date: 2019-12-11 11:29:32 +0200 (Wed, 11 Dec 2019) $ #$Revision: 244985 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/64/1556493.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556493 loop_ _publ_author_name 'Seifert, T.' 'Roesky, P.W.' _publ_section_title ; Alkali and Alkaline Earth Metal Complexes Ligated by an Ethynyl Substituted Cyclopentadienyl Ligand ; _journal_name_full Inorganics _journal_page_first 28 _journal_paper_doi 10.3390/inorganics5020028 _journal_volume 5 _journal_year 2017 _chemical_formula_moiety 'C44 H74 Ca2 I2 O4 Si2' _chemical_formula_sum 'C44 H74 Ca2 I2 O4 Si2' _chemical_formula_weight 1057.17 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary heavy _cell_angle_alpha 90 _cell_angle_beta 101.490(3) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 9.4746(4) _cell_length_b 14.9924(8) _cell_length_c 21.7467(8) _cell_measurement_reflns_used 9717 _cell_measurement_temperature 220 _cell_measurement_theta_max 29.80 _cell_measurement_theta_min 1.91 _cell_volume 3027.1(2) _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXS (Sheldrick, 2008)' _diffrn_ambient_temperature 220 _diffrn_detector Pilatus100K _diffrn_detector_area_resol_mean 5.81 _diffrn_detector_type 'DECTRIS PILATUS 100K' _diffrn_measured_fraction_theta_full 0.991 _diffrn_measured_fraction_theta_max 0.982 _diffrn_measurement_device 'Eulerian 4-circle diffractometer' _diffrn_measurement_device_type 'STOE STADIVARI' _diffrn_measurement_method 'rotation method, \w scans' _diffrn_radiation_collimation '0.5 mm diameter, monocapillary' _diffrn_radiation_monochromator 'plane graphite' _diffrn_radiation_polarisn_norm 0 _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0286 _diffrn_reflns_av_unetI/netI 0.0339 _diffrn_reflns_Laue_measured_fraction_full 0.991 _diffrn_reflns_Laue_measured_fraction_max 0.982 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 14525 _diffrn_reflns_point_group_measured_fraction_full 0.991 _diffrn_reflns_point_group_measured_fraction_max 0.982 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.125 _diffrn_reflns_theta_min 1.911 _diffrn_source 'Mo LFF Sealed Tube' _diffrn_source_current 1.000 _diffrn_source_power 0.050 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 1.278 _exptl_absorpt_correction_T_max 0.7284 _exptl_absorpt_correction_T_min 0.6478 _exptl_absorpt_correction_type integration _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.160 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1088 _exptl_crystal_size_max 0.329 _exptl_crystal_size_mid 0.295 _exptl_crystal_size_min 0.276 _refine_diff_density_max 0.587 _refine_diff_density_min -0.779 _refine_diff_density_rms 0.053 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.975 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 251 _refine_ls_number_reflns 5910 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.975 _refine_ls_R_factor_all 0.0636 _refine_ls_R_factor_gt 0.0392 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0646P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1089 _refine_ls_wR_factor_ref 0.1181 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3630 _reflns_number_total 5910 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file 3.cif _cod_data_source_block tps120-3h _cod_database_code 1556493 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C19(H19A,H19B), C21(H21A,H21B), C20(H20A,H20B), C18(H18A,H18B), C22(H22A, H22B), C15(H15A,H15B), C17(H17A,H17B), C16(H16A,H16B) 2.b Idealised Me refined as rotating group: C11(H11A,H11B,H11C), C14(H14A,H14B,H14C), C12(H12A,H12B,H12C), C13(H13A,H13B, H13C), C1(H1A,H1B,H1C), C3(H3A,H3B,H3C), C2(H2A,H2B,H2C) ; _shelx_res_file ; TITL TPS120-3h in P21/n #14 tps120-3h.res created by SHELXL-2016/6 at 14:57:54 on 24-Mar-2017 REM reset to P21/n #14 CELL 0.71073 9.4746 14.9924 21.7467 90 101.49 90 ZERR 2 0.0004 0.0008 0.0008 0 0.003 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Ca I O Si UNIT 88 148 4 4 8 4 L.S. 10 PLAN 10 BOND ABIN fmap 2 acta REM REM REM WGHT 0.064600 FVAR 0.35267 CA1 3 0.371751 0.530786 0.897830 11.00000 0.06248 0.06640 = 0.05322 0.00543 -0.00316 0.00359 I1 4 0.684537 0.484837 0.962101 11.00000 0.06375 0.14497 = 0.05795 0.00692 0.00620 0.01947 C5 1 0.129089 0.624905 0.770141 11.00000 0.08658 0.08214 = 0.06152 0.01258 -0.00331 0.01512 C6 1 0.241148 0.654648 0.821123 11.00000 0.08392 0.06688 = 0.06787 0.01340 -0.00526 0.00415 C7 1 0.219157 0.682920 0.880939 11.00000 0.11067 0.06640 = 0.07317 -0.00128 -0.00937 0.02316 C9 1 0.455435 0.700588 0.876479 11.00000 0.11628 0.07264 = 0.12712 0.03251 -0.03887 -0.02437 SI1 6 -0.100036 0.560012 0.662581 11.00000 0.08749 0.12185 = 0.06870 -0.00222 -0.01191 0.01732 O1 5 0.177270 0.428748 0.885423 11.00000 0.06584 0.08103 = 0.08325 0.00437 0.00271 -0.00643 O2 5 0.405229 0.433895 0.813450 11.00000 0.08194 0.10074 = 0.06949 -0.01038 0.00484 0.01667 C10 1 0.386713 0.665495 0.817891 11.00000 0.09250 0.08694 = 0.09468 0.03542 -0.00706 -0.00860 C19 1 0.026333 0.445061 0.876312 11.00000 0.06462 0.10386 = 0.11522 -0.01544 0.01559 -0.00021 AFIX 23 H19A 2 -0.006004 0.480386 0.838781 11.00000 -1.20000 H19B 2 0.003483 0.476841 0.911937 11.00000 -1.20000 AFIX 0 C21 1 0.061966 0.300845 0.912302 11.00000 0.14232 0.11803 = 0.15167 0.01066 0.03804 -0.04076 AFIX 23 H21A 2 0.054354 0.239040 0.898856 11.00000 -1.20000 H21B 2 0.046304 0.304300 0.954979 11.00000 -1.20000 AFIX 0 C4 1 0.037251 0.602050 0.726742 11.00000 0.08785 0.10865 = 0.06401 0.00982 -0.00150 0.01704 C8 1 0.353844 0.711187 0.912870 11.00000 0.14713 0.06812 = 0.08327 0.00334 -0.03169 0.00058 C20 1 -0.043062 0.356867 0.869894 11.00000 0.07837 0.10993 = 0.16427 -0.03474 0.01978 -0.01611 AFIX 23 H20A 2 -0.057543 0.335562 0.826977 11.00000 -1.20000 H20B 2 -0.135036 0.358355 0.883043 11.00000 -1.20000 AFIX 0 C18 1 0.291564 0.408952 0.762108 11.00000 0.11239 0.17062 = 0.07745 -0.03189 -0.02050 0.04681 AFIX 23 H18A 2 0.242266 0.356305 0.772968 11.00000 -1.20000 H18B 2 0.222054 0.456979 0.752536 11.00000 -1.20000 AFIX 0 C22 1 0.204337 0.337963 0.908073 11.00000 0.09226 0.09136 = 0.13974 0.01363 -0.01310 -0.00811 AFIX 23 H22A 2 0.268225 0.337597 0.948909 11.00000 -1.20000 H22B 2 0.248084 0.303301 0.879164 11.00000 -1.20000 AFIX 0 C11 1 0.078903 0.687937 0.900973 11.00000 0.16635 0.10112 = 0.08134 -0.00546 0.00998 0.05753 AFIX 137 H11A 2 0.005166 0.662622 0.869019 11.00000 -1.50000 H11B 2 0.056186 0.749165 0.907541 11.00000 -1.50000 H11C 2 0.084413 0.655278 0.939350 11.00000 -1.50000 AFIX 0 C15 1 0.530347 0.393020 0.801686 11.00000 0.09807 0.13760 = 0.11807 -0.03286 0.02544 0.02048 AFIX 23 H15A 2 0.560492 0.345644 0.831819 11.00000 -1.20000 H15B 2 0.607672 0.436337 0.805594 11.00000 -1.20000 AFIX 0 C17 1 0.355361 0.391066 0.709240 11.00000 0.22904 0.11256 = 0.09404 -0.04146 0.03384 -0.01551 AFIX 23 H17A 2 0.362997 0.445081 0.685566 11.00000 -1.20000 H17B 2 0.299740 0.347302 0.681713 11.00000 -1.20000 AFIX 0 C16 1 0.498325 0.356150 0.737405 11.00000 0.11495 0.18861 = 0.17587 -0.10699 0.04807 -0.03712 AFIX 23 H16A 2 0.569573 0.375587 0.713845 11.00000 -1.20000 H16B 2 0.497372 0.291472 0.738399 11.00000 -1.20000 AFIX 0 C14 1 0.451924 0.649045 0.760387 11.00000 0.11031 0.13377 = 0.13556 0.05869 0.03253 -0.00101 AFIX 137 H14A 2 0.523661 0.603122 0.769501 11.00000 -1.50000 H14B 2 0.495568 0.703000 0.749413 11.00000 -1.50000 H14C 2 0.377696 0.630632 0.725958 11.00000 -1.50000 AFIX 0 C12 1 0.379695 0.754134 0.979070 11.00000 0.23983 0.09084 = 0.11902 -0.02967 -0.06479 0.02185 AFIX 137 H12A 2 0.303956 0.736723 1.000048 11.00000 -1.50000 H12B 2 0.380538 0.817901 0.975143 11.00000 -1.50000 H12C 2 0.470586 0.734356 1.002987 11.00000 -1.50000 AFIX 0 C13 1 0.613612 0.727530 0.892686 11.00000 0.14045 0.12451 = 0.22910 0.07362 -0.05676 -0.06228 AFIX 137 H13A 2 0.666699 0.684048 0.920453 11.00000 -1.50000 H13B 2 0.622283 0.784783 0.912857 11.00000 -1.50000 H13C 2 0.651485 0.730730 0.854955 11.00000 -1.50000 AFIX 0 C1 1 -0.242199 0.640881 0.638800 11.00000 0.14829 0.20555 = 0.18006 -0.05286 -0.07382 0.08231 AFIX 137 H1A 2 -0.276333 0.661392 0.675035 11.00000 -1.50000 H1B 2 -0.320063 0.613642 0.609885 11.00000 -1.50000 H1C 2 -0.205626 0.690514 0.618864 11.00000 -1.50000 AFIX 0 C3 1 -0.013829 0.532738 0.595865 11.00000 0.17491 0.26124 = 0.08981 -0.02450 0.01211 0.04470 AFIX 137 H3A 2 0.037520 0.583934 0.585408 11.00000 -1.50000 H3B 2 -0.086340 0.515993 0.560297 11.00000 -1.50000 H3C 2 0.052142 0.484112 0.607213 11.00000 -1.50000 AFIX 0 C2 1 -0.173192 0.458289 0.686542 11.00000 0.23082 0.22068 = 0.15630 0.02546 -0.05391 -0.09917 AFIX 137 H2A 2 -0.111398 0.409380 0.681145 11.00000 -1.50000 H2B 2 -0.267312 0.448485 0.661394 11.00000 -1.50000 H2C 2 -0.179993 0.462597 0.729900 11.00000 -1.50000 AFIX 0 HKLF 4 REM TPS120-3h in P21/n #14 REM R1 = 0.0392 for 3630 Fo > 4sig(Fo) and 0.0636 for all 5910 data REM 251 parameters refined using 0 restraints END WGHT 0.0646 0.0000 REM Highest difference peak 0.587, deepest hole -0.779, 1-sigma level 0.053 Q1 1 0.6249 0.4324 0.9543 11.00000 0.05 0.59 Q2 1 0.6774 0.5079 0.9250 11.00000 0.05 0.39 Q3 1 0.6482 0.5222 0.9860 11.00000 0.05 0.35 Q4 1 -0.1188 0.6347 0.5951 11.00000 0.05 0.30 Q5 1 -0.1721 0.4323 0.6998 11.00000 0.05 0.28 Q6 1 0.7208 0.4969 1.0090 11.00000 0.05 0.27 Q7 1 0.6031 0.5393 0.9481 11.00000 0.05 0.26 Q8 1 -0.2876 0.6015 0.7039 11.00000 0.05 0.25 Q9 1 0.3362 0.3352 0.7430 11.00000 0.05 0.23 Q10 1 0.3394 0.4776 0.9230 11.00000 0.05 0.23 ; _shelx_res_checksum 5078 _shelx_hkl_file ; -2 6 6 1213.38 13.79 0 -2 6 7 323.86 7.14 0 -2 6 12 104.01 4.30 0 -2 6 13 131.96 5.04 0 -2 7 4 149.74 5.58 0 -2 7 14 87.21 4.45 0 -2 8 3 6.66 2.64 0 -2 8 15 121.53 5.48 0 -2 9 3 81.36 4.80 0 -1 3 1 1623.87 10.96 0 -1 3 17 63.90 2.24 0 -1 5 -2 144.93 4.38 0 -1 8 -4 10.74 2.72 0 -1 9 -4 15.47 2.81 0 0 3 -5 174.58 3.35 0 0 4 -6 -0.43 0.89 0 0 7 -8 618.15 9.77 0 1 3 -9 104.16 2.28 0 1 6 -11 312.45 6.05 0 1 9 -12 74.71 4.27 0 1 10 -12 56.82 4.25 0 -2 5 9 6.72 1.72 0 -2 5 10 89.35 3.67 0 -2 6 5 321.55 7.32 0 -2 6 14 129.94 4.78 0 -2 7 3 198.34 6.28 0 -2 7 15 39.02 3.36 0 -2 8 2 88.35 4.90 0 -2 8 16 39.82 3.81 0 -2 9 2 87.42 5.02 0 -1 2 3 1509.02 8.97 0 -1 4 -1 3624.75 18.71 0 -1 6 -3 579.84 9.09 0 -1 7 -4 320.39 7.53 0 -1 10 -5 53.99 4.77 0 0 5 -7 38.19 2.35 0 0 9 -9 96.34 4.87 0 0 10 -9 108.69 5.70 0 1 4 -10 17.71 1.39 0 2 6 -14 131.48 3.78 0 2 10 -15 20.23 2.94 0 2 11 -15 3.96 2.80 0 3 5 -16 63.13 2.04 0 -2 5 7 948.67 11.27 0 -2 5 8 16.59 1.80 0 -2 5 11 47.00 2.86 0 -2 5 12 94.28 3.79 0 -2 6 4 863.94 11.72 0 -2 6 15 64.00 3.76 0 -2 7 16 45.53 3.54 0 -2 8 17 4.56 2.62 0 -2 9 1 216.89 7.25 0 -1 1 8 5077.88 12.34 0 -1 1 9 0.57 0.85 0 -1 9 -5 21.27 2.97 0 0 2 -4 1176.34 6.95 0 0 6 -8 18.08 2.15 0 0 8 -9 244.12 6.80 0 -2 5 6 253.16 5.88 0 -2 5 13 414.85 7.40 0 -2 6 3 22.10 2.68 0 -2 7 2 46.04 3.24 0 -2 7 17 60.54 3.84 0 -2 8 1 443.57 9.65 0 -2 8 18 10.68 2.76 0 -2 9 0 282.02 8.65 0 -1 1 10 944.55 5.16 0 -1 3 0 564.60 6.62 0 -1 5 -3 1288.28 12.51 0 -1 6 -4 9.46 2.07 0 1 5 -11 210.39 4.50 0 1 7 -12 26.24 2.46 0 1 10 -13 24.81 3.50 0 -2 5 5 723.54 9.86 0 -2 5 14 30.44 2.61 0 -2 6 16 83.89 3.97 0 -2 7 1 425.36 9.07 0 -2 8 0 191.70 6.84 0 -2 9 -1 4.60 3.30 0 -1 1 7 329.73 3.23 0 -1 1 11 6.47 0.69 0 -1 2 2 472.54 5.13 0 -1 4 -2 1776.70 13.28 0 -1 7 -5 152.95 5.42 0 -1 9 -6 112.56 5.49 0 0 7 -9 323.96 7.19 0 0 9 -10 32.89 3.34 0 0 10 -10 8.62 2.44 0 1 9 -13 179.14 6.08 0 -2 4 8 1004.43 10.55 0 -2 4 9 69.12 3.02 0 -2 4 10 27.50 2.07 0 -2 4 11 79.24 3.26 0 -2 5 4 403.18 7.42 0 -2 5 15 118.39 4.21 0 -2 6 2 228.73 6.15 0 -2 6 17 -2.56 2.02 0 -2 7 18 45.76 3.43 0 -1 8 -6 97.71 4.81 0 -1 10 -7 75.61 5.26 0 0 4 -7 346.74 5.46 0 0 5 -8 586.81 8.04 0 1 8 -13 81.46 4.20 0 2 7 -15 42.40 2.71 0 -2 4 6 1169.83 11.49 0 -2 4 7 94.19 3.53 0 -2 4 12 295.73 5.71 0 -2 5 3 805.60 10.56 0 -2 6 1 396.14 8.17 0 -2 7 0 1145.45 14.52 0 -2 8 -1 205.52 6.77 0 -1 2 16 0.60 0.69 0 -1 5 -4 364.46 6.82 0 -1 6 -5 642.38 9.81 0 0 6 -9 313.54 6.50 0 0 8 -10 92.65 4.57 0 0 10 -11 6.60 2.92 0 2 5 -14 33.75 1.87 0 -3 9 6 3.18 3.50 0 -2 4 5 694.93 8.96 0 -2 4 13 404.53 6.63 0 -2 5 2 592.73 9.14 0 -2 5 16 65.59 3.22 0 -2 6 18 35.00 2.97 0 -2 7 -1 38.48 3.60 0 -1 3 -1 651.48 7.16 0 -1 7 -6 203.86 5.98 0 0 3 -6 3.83 0.86 0 0 9 -11 59.48 4.12 0 1 10 -14 78.68 4.76 0 -3 8 7 13.16 3.36 0 -3 8 8 109.30 5.34 0 -3 8 9 132.09 5.77 0 -3 8 10 1.65 2.19 0 -3 8 11 51.46 4.26 0 -3 8 12 20.90 3.49 0 -3 8 13 85.71 4.96 0 -2 6 0 739.31 10.93 0 -2 9 -3 38.90 3.78 0 -1 2 1 82.53 2.26 0 -1 4 -3 185.17 4.39 0 -1 8 -7 33.84 2.96 0 -1 10 -8 118.61 6.15 0 0 7 -10 43.87 3.17 0 1 7 -13 160.04 4.87 0 1 9 -14 -2.92 2.23 0 2 8 -16 41.21 2.97 0 -3 7 10 288.95 7.76 0 -3 8 5 27.56 3.71 0 -3 8 6 426.51 9.96 0 -3 8 14 17.25 3.15 0 -3 9 3 17.54 3.86 0 -3 9 4 34.89 3.88 0 -2 4 4 2610.85 17.21 0 -2 5 1 611.77 9.33 0 -2 5 17 144.39 4.42 0 -2 7 -2 65.16 4.14 0 -2 8 -3 185.79 6.66 0 -1 1 5 392.99 3.62 0 -1 6 -6 983.43 12.11 0 -1 9 -8 96.17 5.15 0 0 8 -11 8.06 2.36 0 2 6 -15 64.26 2.68 0 -3 7 6 4.40 2.64 0 -3 7 7 403.74 9.22 0 -3 7 8 12.01 2.22 0 -3 7 11 23.15 2.56 0 -3 7 12 179.44 6.23 0 -3 7 13 56.12 4.03 0 -3 8 4 271.96 8.38 0 -3 8 15 29.22 3.57 0 -2 4 3 74.05 3.27 0 -2 4 15 9.69 1.78 0 -2 6 -1 955.16 12.46 0 -2 9 -4 63.58 4.48 0 -1 5 -5 68.28 3.23 0 -1 7 -7 252.02 6.64 0 -1 8 -8 120.94 5.26 0 -1 10 -9 19.54 3.72 0 0 5 -9 36.19 2.42 0 0 10 -12 68.34 4.65 0 1 4 -11 222.85 3.86 0 1 5 -12 53.08 2.42 0 -3 7 5 431.16 9.58 0 -3 7 14 86.09 4.58 0 -3 8 3 127.74 5.80 0 -3 8 16 -0.64 2.49 0 -2 3 8 1.85 1.18 0 -2 3 9 254.10 4.79 0 -2 3 10 160.80 3.80 0 -2 5 0 1672.60 15.37 0 -2 5 18 45.65 2.75 0 -2 7 -3 108.68 4.97 0 -2 8 -4 -0.65 2.28 0 -2 9 -5 -1.58 2.84 0 -1 3 -2 6404.77 22.58 0 -1 4 -4 432.68 6.74 0 -1 9 -9 14.92 2.95 0 0 2 -5 567.41 4.91 0 0 4 -8 78.11 2.71 0 0 6 -10 122.82 4.23 0 0 9 -12 12.01 2.72 0 1 10 -15 8.18 2.64 0 -3 6 7 94.48 4.59 0 -3 6 8 251.19 6.89 0 -3 6 9 162.79 5.62 0 -3 6 10 23.38 2.76 0 -3 6 11 196.82 6.06 0 -3 7 4 92.44 4.64 0 -3 7 15 2.94 2.38 0 -3 8 2 -1.00 2.31 0 -3 8 17 2.69 2.57 0 -2 3 6 90.89 3.10 0 -2 3 7 1727.07 12.51 0 -2 3 11 211.49 4.29 0 -2 4 2 540.25 8.05 0 -2 6 -2 438.44 8.54 0 -1 1 4 191.78 2.62 0 0 7 -11 135.63 4.84 0 1 3 -10 538.67 4.81 0 1 6 -13 43.95 2.52 0 2 7 -16 44.01 2.56 0 -3 6 6 880.33 12.62 0 -3 6 12 0.65 1.95 0 -3 6 13 368.49 8.07 0 -3 7 3 126.94 5.32 0 -3 7 16 18.20 2.84 0 -3 8 1 90.12 5.22 0 -3 8 18 13.50 3.06 0 -2 3 12 7.96 1.35 0 -2 5 -1 483.36 8.47 0 -2 7 -4 17.12 2.75 0 -2 8 -5 66.39 4.40 0 -1 2 0 153.50 3.03 0 -1 2 17 32.60 1.07 0 -1 5 -6 1097.39 11.77 0 -1 6 -7 493.45 8.69 0 -1 7 -8 266.68 6.99 0 -1 8 -9 141.07 5.60 0 0 1 -3 257.40 2.35 0 0 8 -12 141.07 5.29 0 0 10 -13 30.26 3.77 0 1 7 -14 29.22 2.77 0 1 9 -15 96.17 4.58 0 -3 6 5 13.63 2.22 0 -3 6 14 50.03 3.64 0 -3 7 2 775.37 12.77 0 -3 7 17 4.74 2.41 0 -3 8 0 13.03 3.47 0 -2 3 5 1021.33 9.76 0 -2 3 13 791.78 8.00 0 -2 4 1 57.21 2.98 0 -2 6 -3 328.01 7.59 0 -2 9 -6 20.77 3.11 0 -1 9 -10 7.80 2.90 0 0 3 -7 4.96 0.88 0 -3 6 4 247.77 6.79 0 -3 6 15 109.80 4.54 0 -3 7 1 19.65 3.21 0 -2 3 4 2228.00 14.57 0 -2 4 17 -1.64 1.30 0 -2 8 -6 103.27 5.24 0 -1 3 -3 4.55 1.19 0 -1 4 -5 925.51 9.85 0 0 9 -13 1.43 2.21 0 1 8 -15 12.19 2.43 0 -3 5 7 319.63 7.26 0 -3 5 8 11.77 2.23 0 -3 5 9 163.26 5.07 0 -3 5 10 252.51 6.33 0 -3 5 11 74.41 3.70 0 -3 5 12 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5 1013.78 12.44 0 -1 -5 0 470.28 5.58 0 -1 -5 1 364.28 5.46 0 -1 -5 2 74.61 2.88 0 -1 -5 3 409.62 6.69 0 0 -4 11 285.28 8.00 0 0 -3 10 52.45 3.42 0 0 -1 6 8.00 1.46 0 1 -3 14 360.24 9.96 0 1 -1 12 422.65 9.13 0 2 1 13 9.08 2.06 0 -1 -12 -1 -2.05 1.87 0 -1 -12 0 130.21 4.99 0 -1 -12 1 3.34 2.28 0 -1 -12 2 55.08 3.97 0 -1 -12 3 5.31 2.13 0 -1 -10 -4 0.67 1.07 0 -1 -10 5 64.37 4.33 0 -1 -9 5 42.83 3.70 0 -1 -8 5 272.81 7.38 0 -1 -7 5 1.94 1.58 0 -1 -6 3 18.49 2.07 0 -1 -6 4 5.32 1.46 0 0 -3 9 96.63 4.49 0 0 -2 8 451.30 8.05 0 1 -2 13 112.98 5.21 0 2 0 14 219.16 6.99 0 2 2 11 9.57 1.81 0 2 3 9 1279.00 10.51 0 2 4 6 791.67 4.91 0 3 2 14 -1.61 1.98 0 4 2 16 107.59 5.54 0 4 6 9 125.58 2.55 0 -1 -11 -2 9.13 1.76 0 -1 -11 -1 195.27 5.49 0 -1 -11 0 0.30 2.26 0 -1 -11 1 107.07 4.71 0 -1 -11 2 16.66 2.81 0 -1 -11 3 -0.84 1.72 0 -1 -10 3 3.70 2.18 0 -1 -10 4 1.38 1.61 0 -1 -9 -4 20.11 1.41 0 -1 -9 4 83.89 4.43 0 -1 -8 -4 10.41 1.02 0 -1 -8 4 45.50 3.40 0 -1 -7 3 48.82 3.04 0 -1 -7 4 135.59 4.71 0 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23.01 3.12 0 1 -3 9 195.94 6.40 0 2 -3 12 3.97 2.91 0 2 -1 11 1000.78 14.04 0 3 1 12 179.28 6.02 0 3 2 11 27.38 2.48 0 4 3 12 132.36 4.92 0 4 6 8 346.06 4.11 0 0 -13 -2 9.24 2.48 0 0 -12 1 2.91 2.54 0 0 -9 4 134.69 5.77 0 0 -7 5 509.06 9.95 0 0 -6 5 711.15 11.06 0 0 -5 5 44.23 2.87 0 0 -3 4 10.94 1.70 0 0 -2 3 -0.12 0.89 0 1 -4 9 766.64 12.76 0 2 0 10 1252.94 14.31 0 2 1 9 1925.86 15.86 0 2 2 8 3413.46 18.27 0 2 4 5 253.45 2.44 0 3 -1 13 4.11 2.82 0 4 0 14 355.82 9.82 0 0 -13 -4 15.12 2.57 0 0 -13 -3 1.11 2.04 0 0 -12 0 -1.13 2.24 0 0 -11 2 78.72 4.51 0 0 -8 4 814.95 12.56 0 1 -7 9 143.70 6.57 0 1 -6 9 541.76 11.57 0 1 -5 9 182.50 6.64 0 2 -2 11 8.21 2.07 0 3 -2 13 554.11 12.33 0 3 0 12 0.36 2.22 0 5 2 14 1.09 2.61 0 5 5 11 37.27 2.66 0 0 -12 -1 5.57 2.49 0 0 -10 2 61.00 4.02 0 0 -7 4 208.29 6.31 0 0 -6 4 3.68 1.96 0 0 -5 4 287.18 6.46 0 0 -4 4 7.44 1.44 0 1 -3 8 1245.17 14.84 0 1 0 6 -1.04 1.05 0 1 1 5 4.21 0.92 0 2 -3 11 554.00 11.60 0 4 1 13 16.03 2.97 0 4 7 6 112.10 1.50 0 5 4 12 25.75 2.72 0 0 -12 -2 5.93 2.29 0 0 -11 0 2.09 2.27 0 0 -8 3 39.88 3.42 0 0 -3 3 3938.88 18.82 0 1 -6 8 163.37 6.70 0 1 -5 8 1817.74 19.71 0 1 -4 8 48.91 3.47 0 2 -5 11 140.55 6.87 0 2 -4 11 121.86 6.00 0 3 -1 12 172.95 6.61 0 3 2 10 240.88 5.98 0 3 4 8 594.51 6.79 0 4 2 12 89.61 4.50 0 4 5 9 461.00 6.33 0 5 1 14 26.10 3.93 0 0 -12 -3 10.52 2.27 0 0 -11 -1 21.74 3.00 0 0 -10 1 12.04 2.45 0 0 -9 2 11.32 2.50 0 0 -7 3 299.96 7.09 0 1 -9 7 74.23 5.21 0 1 -8 7 35.06 4.32 0 1 -2 7 2239.02 17.89 0 1 3 2 6237.11 7.99 0 2 -2 10 1065.23 14.67 0 2 0 9 3.30 1.36 0 3 -2 12 56.28 4.61 0 3 3 9 115.40 3.74 0 4 0 13 0.12 2.62 0 4 3 11 192.16 5.60 0 4 4 10 280.02 5.93 0 0 -12 -4 35.83 2.79 0 0 -10 0 0.72 1.84 0 0 -8 2 159.04 5.40 0 0 -6 3 161.42 4.89 0 0 -5 3 290.37 6.17 0 0 -4 3 49.53 2.52 0 0 -2 2 2364.44 11.87 0 1 -15 -3 1.10 2.64 0 1 -7 7 246.03 8.04 0 1 -3 7 864.06 11.91 0 2 -4 10 634.70 12.69 0 2 1 8 0.77 1.36 0 2 3 6 82.65 2.27 0 3 0 11 8.41 2.29 0 4 -1 13 17.83 3.62 0 5 2 13 107.68 5.43 0 0 -12 -7 142.76 4.06 0 0 -11 -2 79.68 3.93 0 0 -9 1 78.22 4.01 0 0 -7 2 14.28 2.25 0 1 -11 4 23.11 4.01 0 1 -10 5 51.32 4.60 0 1 -9 6 110.06 5.62 0 1 -6 7 483.71 10.32 0 1 -5 7 983.30 14.10 0 1 -4 7 1545.08 16.64 0 1 -1 6 4726.57 22.94 0 2 -1 9 1938.81 18.20 0 2 2 7 494.60 6.61 0 3 -1 11 2.35 2.13 0 4 1 12 2.12 2.37 0 5 3 12 88.67 4.58 0 0 -11 -3 11.23 2.01 0 0 -10 -1 14.64 2.19 0 0 -8 1 46.61 3.13 0 0 -6 2 818.14 10.29 0 0 -3 2 2735.16 14.46 0 1 -14 -1 12.85 3.24 0 1 -8 6 102.10 5.41 0 1 0 5 1441.29 10.84 0 3 1 10 233.80 6.37 0 4 0 12 215.66 7.40 0 4 2 11 -1.79 1.85 0 5 1 13 0.43 2.53 0 5 4 11 181.13 5.53 0 0 -11 -4 14.33 2.13 0 0 -9 0 2.13 1.32 0 0 -5 2 121.28 3.94 0 0 -4 2 8799.55 28.60 0 1 -14 -2 1.52 2.80 0 1 -13 0 2.69 2.93 0 1 -12 2 22.70 3.31 0 1 -10 4 -0.89 2.99 0 1 -9 5 21.57 3.24 0 1 -7 6 214.55 7.06 0 1 -6 6 924.87 13.85 0 2 -6 9 173.65 7.61 0 2 -5 9 806.44 14.37 0 2 -4 9 427.22 10.22 0 2 0 8 2917.34 20.08 0 3 -2 11 22.85 2.79 0 0 -10 -2 57.79 3.30 0 0 -7 1 475.96 8.02 0 1 -14 -3 6.61 2.78 0 1 -12 1 2.46 3.06 0 1 -8 5 21.50 3.31 0 1 -5 6 1084.50 14.14 0 1 -4 6 645.41 10.49 0 1 -3 6 1522.17 14.99 0 1 1 4 9999.99 22.48 0 3 0 10 1.05 1.86 0 4 3 10 6.18 1.85 0 5 2 12 -1.65 2.26 0 6 2 13 1.94 2.89 0 0 -10 -3 6.21 2.01 0 0 -9 -1 84.40 3.72 0 0 -8 0 2.59 1.62 0 0 -6 1 26.16 2.38 0 1 -14 -4 0.62 2.34 0 1 -13 -1 24.09 3.58 0 1 -10 3 69.11 4.72 0 1 -9 4 16.00 2.65 0 1 -7 5 157.57 6.19 0 1 -1 5 3.75 1.31 0 2 -7 8 32.39 3.68 0 3 -1 10 228.64 7.14 0 3 3 8 71.74 2.88 0 4 1 11 199.25 6.67 0 4 4 9 14.13 1.99 0 1 -14 -5 2.29 2.30 0 1 -13 -2 11.57 3.05 0 1 -12 0 138.68 6.27 0 1 -8 4 8.25 2.87 0 1 -6 5 665.37 11.38 0 2 -8 7 45.44 5.04 0 2 -6 8 709.02 13.51 0 2 -4 8 1741.51 19.46 0 2 -3 8 168.51 6.20 0 2 -2 8 3484.61 24.82 0 3 -4 10 157.31 7.10 0 3 -3 10 50.97 4.51 0 3 1 9 105.62 4.29 0 3 4 7 2.63 1.03 0 4 0 11 -1.14 2.26 0 4 6 7 133.65 2.77 0 5 3 11 -3.14 1.96 0 6 3 12 26.91 3.36 0 0 -11 -7 8.35 1.72 0 0 -10 -4 62.19 3.06 0 0 -9 -2 7.79 1.89 0 0 -8 -1 39.26 2.60 0 0 -7 0 0.39 1.47 0 0 -5 1 4822.39 21.58 0 0 -2 1 17.62 0.97 0 1 -13 -3 7.08 2.84 0 1 -11 1 186.99 6.90 0 1 -10 2 131.97 5.94 0 1 -9 3 26.61 3.58 0 1 -5 5 48.28 3.47 0 1 -4 5 895.09 11.79 0 1 -3 5 293.30 6.45 0 1 -2 5 1197.38 11.87 0 1 2 3 275.87 2.41 0 2 -7 7 692.49 13.65 0 3 5 6 12.62 0.96 0 4 2 10 349.01 7.87 0 5 0 12 -0.89 2.36 0 5 4 10 1.77 2.14 0 0 -4 1 964.06 8.79 0 0 -3 1 425.11 5.19 0 1 -12 -1 1.67 2.60 0 2 -6 7 8.98 3.48 0 2 0 7 0.05 1.37 0 2 2 6 2890.41 14.89 0 3 0 9 330.91 7.76 0 4 -2 11 -0.85 2.85 0 0 -11 -9 27.14 1.73 0 0 -9 -3 184.61 4.74 0 0 -6 0 981.80 10.03 0 1 -13 -4 0.68 2.34 0 1 -12 -2 60.53 4.17 0 1 -11 0 0.14 2.67 0 1 -10 1 5.34 2.60 0 1 -9 2 454.10 9.90 0 1 -8 3 1282.72 16.08 0 1 -6 4 10.89 2.50 0 1 0 4 -1.24 0.79 0 2 -8 6 100.06 5.69 0 2 -5 7 899.14 14.24 0 2 -1 7 1007.30 12.16 0 3 -5 9 63.83 5.05 0 3 -1 9 108.51 4.95 0 3 2 8 547.98 8.26 0 4 1 10 12.46 2.58 0 5 5 9 4.72 1.80 0 0 -8 -2 156.61 4.33 0 0 -7 -1 473.35 7.16 0 1 -13 -5 5.26 2.34 0 1 -5 4 365.50 7.78 0 2 -9 5 -0.74 2.52 0 2 -7 6 14.34 3.25 0 2 -4 7 10.94 2.19 0 2 -3 7 1039.41 13.86 0 2 -2 7 486.73 9.09 0 3 -4 9 0.18 1.89 0 3 -3 9 118.25 5.78 0 3 -2 9 116.57 5.20 0 4 0 10 1230.83 16.26 0 5 1 11 9.99 3.17 0 0 -5 0 0.62 1.24 0 1 -12 -3 4.67 2.33 0 1 -7 3 0.77 1.60 0 1 -4 4 440.60 7.97 0 1 -1 4 9965.96 29.25 0 2 -6 6 241.30 7.80 0 2 3 5 473.89 4.78 0 3 -6 8 536.76 12.59 0 3 1 8 3.35 1.62 0 4 -1 10 11.71 3.00 0 5 0 11 630.17 12.91 0 5 3 10 493.55 9.47 0 5 6 8 2.36 1.47 0 0 -9 -4 129.83 3.79 0 1 -13 -6 3.64 2.12 0 1 -10 0 327.05 8.09 0 1 -9 1 559.03 10.57 0 1 -8 2 158.82 5.66 0 1 -3 4 1960.00 15.44 0 1 -2 4 285.66 5.57 0 2 -11 2 110.46 6.28 0 2 -10 3 24.64 4.00 0 2 -9 4 63.92 5.10 0 2 1 6 34.72 2.11 0 3 -5 8 104.20 6.15 0 3 3 7 232.31 4.78 0 4 4 8 763.53 9.18 0 5 -1 11 13.03 3.35 0 6 2 11 14.38 3.29 0 0 -8 -3 35.91 2.20 0 0 -6 -1 34.58 2.09 0 0 -4 0 1212.49 9.06 0 1 -13 -7 2.25 1.93 0 1 -11 -2 14.19 2.70 0 2 -12 0 26.24 4.19 0 2 -7 5 17.02 3.19 0 2 -5 6 73.20 4.18 0 2 -4 6 763.42 12.13 0 2 0 6 1083.05 11.18 0 3 -4 8 583.77 12.07 0 3 -3 8 75.48 4.77 0 3 -1 8 2.23 1.92 0 3 0 8 0.44 1.57 0 6 1 11 9.82 3.15 0 6 4 10 5.38 2.37 0 7 3 11 5.41 2.73 0 0 -7 -2 20.30 1.73 0 1 -10 -1 -1.25 1.97 0 1 -7 2 280.38 7.18 0 1 -5 3 1285.73 13.69 0 2 -14 -4 11.27 3.22 0 2 -13 -2 3.15 3.53 0 2 -11 1 -2.07 3.12 0 2 -8 4 -0.45 2.50 0 2 -2 6 2922.09 21.02 0 2 -1 6 32.67 2.53 0 3 -6 7 6.25 3.34 0 3 -2 8 559.26 10.63 0 4 1 9 1459.95 16.31 0 5 1 10 1023.53 15.23 0 5 4 9 520.59 8.86 0 5 7 7 1.70 1.02 0 0 -3 0 1.41 0.73 0 1 -11 -3 -1.10 1.90 0 1 -9 0 61.86 3.63 0 1 -8 1 208.61 6.18 0 2 -14 -5 3.50 2.89 0 2 -12 -1 37.30 4.25 0 2 -10 2 11.11 2.87 0 2 -9 3 39.67 3.85 0 2 -6 5 205.33 6.78 0 3 -5 7 774.06 14.11 0 4 -3 9 800.77 14.65 0 4 -2 9 54.99 4.46 0 4 -1 9 1473.69 18.13 0 4 0 9 -2.34 2.12 0 5 0 10 -0.55 3.17 0 6 3 10 55.70 4.15 0 0 -10 -8 -0.36 1.28 0 0 -5 -1 5178.33 19.35 0 1 -12 -6 1.19 2.23 0 1 -10 -2 40.52 3.36 0 1 -6 2 1947.79 17.12 0 1 -4 3 164.66 4.66 0 2 -13 -3 33.47 3.94 0 2 -7 4 16.81 3.05 0 2 -5 5 100.91 4.91 0 3 -7 6 212.79 8.28 0 4 3 8 263.24 6.00 0 4 5 7 362.23 5.49 0 5 3 9 24.45 3.09 0 6 5 9 4.73 2.31 0 1 -11 -4 1.13 1.88 0 1 -9 -1 198.65 6.05 0 1 -7 1 1294.59 14.27 0 1 -3 3 2.77 1.46 0 1 1 3 271.20 3.26 0 2 -14 -6 4.15 2.79 0 2 -10 1 189.70 7.18 0 2 -9 2 163.71 6.68 0 2 -4 5 249.65 6.86 0 2 2 5 27.58 1.54 0 3 -6 6 127.66 6.31 0 3 -3 7 221.63 7.10 0 3 1 7 6.48 1.61 0 3 4 6 127.40 2.97 0 5 5 8 154.44 4.60 0 6 2 10 19.07 3.25 0 0 -7 -3 293.54 5.00 0 0 -6 -2 809.37 7.97 0 1 -8 0 746.61 11.00 0 1 -5 2 123.73 4.34 0 1 -2 3 266.46 5.02 0 2 -6 4 115.52 5.28 0 3 -2 7 9.29 2.33 0 3 -1 7 5.25 1.89 0 3 0 7 2.86 1.64 0 4 -4 8 786.13 14.62 0 4 2 8 553.16 9.26 0 5 2 9 456.68 9.59 0 1 -11 -5 0.81 2.05 0 1 -10 -3 4.54 1.88 0 1 -1 3 270.83 4.52 0 1 0 3 41.10 1.65 0 2 -13 -5 1.59 2.60 0 2 -11 -1 90.31 5.42 0 2 -7 3 102.96 5.16 0 2 -3 5 461.20 8.54 0 2 -2 5 28.27 2.53 0 2 1 5 1253.84 10.32 0 3 -7 5 1.63 3.20 0 3 -5 6 12.66 3.05 0 4 -3 8 253.70 8.25 0 4 -2 8 540.99 11.34 0 4 0 8 447.93 9.41 0 4 1 8 119.98 4.85 0 5 -2 9 453.89 11.53 0 5 -1 9 7.45 3.37 0 5 0 9 521.90 11.26 0 6 4 9 188.98 6.19 0 1 -9 -2 113.00 4.54 0 1 -6 1 63.05 3.39 0 2 -12 -3 5.64 3.02 0 2 -10 0 45.69 3.64 0 2 -9 1 5.99 2.78 0 2 -8 2 179.36 6.64 0 2 -5 4 8.80 1.90 0 2 -1 5 1307.42 12.55 0 2 0 5 0.45 1.12 0 3 -9 3 -1.51 3.35 0 3 -4 6 127.56 5.67 0 4 -5 7 362.68 10.37 0 1 -4 2 1673.16 13.78 0 3 -6 5 122.52 5.68 0 -9 1 7 3.91 2.30 0 -7 0 -2 0.00 0.68 0 -7 2 9 22.09 3.15 0 -7 2 10 29.42 3.47 0 -6 2 6 146.69 4.94 0 -5 2 5 1024.85 11.58 0 -4 2 5 8.61 1.91 0 -4 2 13 126.04 6.43 0 -3 2 7 72.02 3.39 0 -3 2 8 30.82 2.79 0 -3 2 9 498.96 9.48 0 -3 2 10 69.07 4.27 0 -3 2 11 1551.78 17.85 0 -1 1 3 2289.78 11.53 0 -1 1 12 244.45 7.21 0 -1 1 13 25.04 2.85 0 1 0 7 4436.95 20.24 0 2 -2 15 -0.76 2.27 0 2 -1 9 1944.24 14.46 0 3 -4 17 135.83 5.80 0 3 -3 14 500.20 9.28 0 -9 1 8 89.80 4.79 0 -8 1 4 1.08 1.72 0 -6 2 7 0.56 1.19 0 -6 2 8 66.45 3.85 0 -6 2 9 14.87 2.68 0 -6 2 10 406.57 9.52 0 -6 2 11 10.62 3.52 0 -5 2 6 53.08 3.26 0 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6.34 0 -2 -3 -19 62.79 5.84 0 -1 -9 -22 17.01 5.78 0 -1 -6 -20 60.11 7.00 0 -1 -5 -19 54.59 6.01 0 -1 -4 -18 31.42 4.76 0 0 -10 -20 -0.90 4.58 0 0 -8 -19 22.37 5.54 0 1 -13 -18 0.34 4.94 0 1 -10 -17 1.90 3.73 0 1 -9 -17 4.53 4.55 0 1 -8 -16 11.48 4.66 0 1 -7 -15 231.06 9.57 0 1 -6 -14 244.91 9.47 0 1 -4 -11 215.26 7.30 0 2 -16 -13 1.06 3.53 0 2 -15 -14 2.22 5.04 0 2 -14 -14 3.74 5.22 0 2 -13 -14 9.90 5.53 0 2 -11 -14 21.61 5.38 0 2 -10 -13 43.02 6.01 0 2 -9 -12 15.62 3.70 0 2 -8 -11 24.76 3.64 0 2 -7 -10 41.64 4.21 0 3 -15 -5 10.16 3.35 0 3 -15 -4 4.33 3.01 0 3 -15 -3 1.28 2.64 0 3 -14 -6 13.75 3.71 0 3 -14 -5 1.72 3.06 0 3 -14 -4 4.28 2.70 0 3 -14 -3 4.06 2.46 0 3 -14 -2 0.80 2.22 0 3 -14 -1 0.41 1.94 0 3 -13 -6 -2.43 2.86 0 3 -13 -5 25.57 4.00 0 3 -13 -4 16.81 3.25 0 3 -13 -3 7.50 2.58 0 3 -13 -2 5.50 2.23 0 3 -12 -5 19.67 3.47 0 3 -12 -4 43.46 3.96 0 3 -12 -3 34.26 3.43 0 -4 -1 -20 -0.02 2.67 0 -4 1 -17 181.68 6.60 0 -3 -5 -23 19.12 5.19 0 -3 -4 -22 11.33 4.58 0 -3 -3 -21 16.31 4.10 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-23 -1.05 4.33 0 -2 -5 -22 6.55 4.96 0 -1 -7 -22 25.12 5.96 0 -1 -6 -21 28.33 5.65 0 -1 -5 -20 83.01 6.62 0 -1 -4 -19 53.32 5.65 0 -1 -3 -18 87.85 6.17 0 0 -9 -21 3.10 5.57 0 0 -5 -18 0.27 3.68 0 0 -3 -15 462.37 11.57 0 0 -2 -13 69.06 4.67 0 1 -10 -19 0.22 4.73 0 1 -9 -18 17.87 5.40 0 1 -5 -14 38.86 4.64 0 1 -4 -12 155.61 6.38 0 2 -14 -16 7.67 5.54 0 2 -13 -16 4.60 5.43 0 2 -11 -15 1.33 3.59 0 2 -10 -15 18.82 5.70 0 2 -9 -14 100.25 7.86 0 2 -8 -13 141.33 7.98 0 2 -7 -12 18.64 4.06 0 2 -6 -10 9.26 2.96 0 3 -17 -7 0.06 3.52 0 3 -17 -6 -0.10 3.31 0 3 -16 -9 2.61 3.76 0 3 -16 -8 0.16 3.81 0 3 -15 -9 0.84 4.15 0 3 -14 -10 -2.18 3.72 0 3 -14 -9 7.04 4.35 0 3 -13 -9 1.92 4.04 0 3 -12 -9 25.79 4.79 0 3 -12 -8 34.90 4.25 0 3 -11 -8 61.70 5.39 0 3 -11 -7 93.63 5.57 0 3 -10 -6 97.77 5.36 0 3 -10 -5 -0.14 2.34 0 -4 -2 -22 37.23 5.09 0 -4 -1 -21 8.52 3.10 0 -4 1 -18 2.93 2.54 0 -3 -4 -23 1.42 4.21 0 -3 -3 -22 3.75 3.92 0 -3 -2 -21 1.36 3.27 0 -3 0 -18 2.15 2.69 0 -3 1 -16 619.00 11.36 0 -2 -2 -19 -0.37 2.12 0 -2 0 -16 1.42 2.20 0 -1 -8 -23 2.24 5.23 0 -1 -5 -21 18.55 5.01 0 -1 -2 -17 242.46 8.75 0 0 -10 -22 -0.92 5.12 0 0 -7 -20 17.25 4.46 0 0 -4 -17 21.50 4.48 0 1 -12 -20 -0.57 4.62 0 1 -9 -19 5.42 5.43 0 1 -8 -18 1.87 4.38 0 1 -7 -17 4.05 3.28 0 1 -6 -16 35.69 4.52 0 1 -5 -15 221.69 8.98 0 2 -14 -17 -0.48 5.27 0 2 -13 -17 11.26 5.84 0 2 -12 -17 2.82 5.02 0 2 -11 -16 -0.55 3.62 0 2 -10 -16 1.27 4.55 0 2 -9 -15 21.85 5.77 0 2 -8 -14 59.96 6.65 0 2 -6 -11 86.51 5.52 0 3 -17 -9 -2.23 4.05 0 3 -16 -10 1.87 4.29 0 3 -15 -11 -1.30 4.29 0 3 -15 -10 7.65 4.19 0 3 -14 -11 0.54 4.27 0 3 -13 -11 5.32 4.53 0 3 -13 -10 9.31 3.46 0 3 -12 -10 0.25 3.62 0 3 -11 -10 30.14 4.73 0 3 -11 -9 8.29 3.74 0 3 -10 -8 58.83 5.05 0 3 -10 -7 28.64 3.47 0 -4 0 -20 45.15 4.43 0 -3 -1 -20 8.72 3.37 0 -2 -5 -23 54.91 7.04 0 -2 -4 -22 78.65 7.33 0 -2 -3 -21 135.14 8.22 0 -2 -1 -18 5.68 2.78 0 -1 -7 -23 20.05 5.97 0 -1 -6 -22 17.81 4.51 0 -1 -4 -20 94.19 6.74 0 -1 -3 -19 19.62 4.39 0 0 -9 -22 31.04 6.21 0 0 -7 -21 -0.97 5.16 0 0 -6 -20 -0.76 4.62 0 0 -5 -19 -0.60 4.16 0 0 -3 -16 33.99 4.58 0 0 -2 -14 1383.88 18.18 0 1 -10 -20 2.78 4.57 0 1 -8 -19 21.75 5.90 0 1 -7 -18 50.30 6.49 0 1 -6 -17 7.02 4.05 0 1 -4 -14 198.95 7.84 0 2 -13 -18 -2.41 4.56 0 2 -11 -17 6.61 5.51 0 2 -9 -16 4.33 5.08 0 2 -8 -15 114.67 8.04 0 2 -7 -13 66.21 5.34 0 2 -6 -12 103.86 6.24 0 3 -16 -12 1.32 4.69 0 3 -16 -11 0.71 3.19 0 3 -15 -12 0.04 4.60 0 3 -14 -12 2.89 4.66 0 3 -13 -12 2.35 4.50 0 3 -12 -12 17.46 5.04 0 3 -12 -11 3.49 3.13 0 3 -11 -11 5.99 4.28 0 3 -10 -10 5.25 3.62 0 3 -10 -9 28.74 3.83 0 3 -9 -8 16.09 3.50 0 3 -9 -6 1.36 2.10 0 -3 -3 -23 16.11 4.55 0 -3 0 -19 55.57 4.49 0 -3 1 -17 -0.36 2.30 0 -2 -2 -20 78.34 6.05 0 -2 0 -17 -0.52 2.20 0 -1 -6 -23 11.98 5.04 0 -1 -5 -22 26.33 5.60 0 -1 -1 -16 82.55 5.05 0 0 -4 -18 23.77 3.87 0 1 -11 -21 -3.65 3.35 0 1 -10 -21 1.00 4.98 0 1 -9 -20 6.62 4.14 0 1 -7 -19 1.09 4.44 0 1 -5 -16 -1.92 2.80 0 1 -3 -12 325.68 8.74 0 2 -12 -18 8.86 4.38 0 2 -11 -18 -4.14 5.19 0 2 -10 -17 0.42 3.62 0 2 -9 -17 27.01 5.62 0 2 -7 -14 83.42 6.09 0 2 -6 -13 135.69 7.24 0 2 -5 -10 86.40 4.90 0 3 -15 -14 -1.90 4.51 0 3 -15 -13 -1.41 4.27 0 3 -14 -13 3.05 3.54 0 3 -13 -13 0.62 4.27 0 3 -12 -13 1.28 4.54 0 3 -11 -12 1.17 3.86 0 3 -10 -11 -0.94 3.46 0 3 -9 -10 94.00 6.20 0 3 -9 -9 21.99 3.93 0 -3 -2 -22 -0.55 3.00 0 -3 -1 -21 1.17 2.70 0 -2 -4 -23 -1.34 4.39 0 -2 -3 -22 7.74 4.49 0 -2 -1 -19 44.49 4.47 0 -1 -3 -20 128.29 7.87 0 0 -7 -22 37.18 6.60 0 0 -6 -21 64.92 6.46 0 0 -5 -20 22.35 5.14 0 0 -4 -19 18.81 4.71 0 0 -3 -17 173.03 7.67 0 1 -9 -21 3.73 5.41 0 1 -8 -20 -1.45 3.53 0 1 -6 -18 0.19 3.04 0 1 -5 -17 74.71 6.47 0 1 -4 -15 11.86 3.06 0 1 -3 -13 5.12 2.69 0 2 -13 -19 2.31 3.80 0 2 -12 -19 8.01 5.17 0 2 -11 -19 3.39 5.61 0 2 -10 -18 9.81 4.21 0 2 -7 -15 43.80 5.10 0 2 -6 -14 130.01 7.39 0 2 -5 -11 47.22 4.37 0 3 -15 -15 -0.74 4.87 0 3 -14 -15 5.25 5.19 0 3 -13 -15 -1.50 4.36 0 3 -13 -14 3.07 3.45 0 3 -12 -14 -2.55 4.17 0 3 -11 -13 0.07 3.03 0 3 -10 -13 8.95 4.15 0 3 -10 -12 20.61 3.92 0 3 -9 -11 6.32 3.72 0 3 -8 -9 134.40 6.56 0 3 -8 -8 110.48 5.82 0 3 -8 -7 11.35 2.27 0 -2 -2 -21 2.68 3.65 0 -1 -6 -24 5.38 4.90 0 -1 -5 -23 20.26 5.50 0 -1 -4 -22 22.69 5.43 0 -1 -2 -19 47.82 5.02 0 -1 -1 -17 6.89 2.36 0 -1 0 -15 468.06 10.18 0 0 -7 -23 0.46 4.70 0 0 -6 -22 20.26 5.93 0 0 -5 -21 1.11 4.25 0 0 -3 -18 -1.50 3.60 0 0 -2 -16 559.56 12.61 0 1 -10 -22 1.00 3.55 0 1 -9 -22 5.35 4.63 0 1 -8 -21 21.99 6.22 0 1 -7 -20 32.54 6.33 0 1 -6 -19 67.14 7.02 0 1 -3 -14 69.66 5.02 0 2 -12 -20 -0.93 5.25 0 2 -11 -20 10.44 5.26 0 2 -10 -19 22.46 6.52 0 2 -9 -18 6.10 3.97 0 2 -8 -17 2.75 3.64 0 2 -7 -16 52.74 6.16 0 2 -5 -12 92.40 5.26 0 3 -14 -16 -0.70 4.99 0 3 -13 -16 -1.03 4.98 0 3 -12 -15 -1.46 3.29 0 3 -10 -14 -2.14 4.31 0 3 -9 -13 15.44 4.43 0 3 -9 -12 39.74 4.63 0 3 -8 -10 0.25 3.18 0 -3 -2 -23 16.65 4.02 0 -3 0 -20 -0.04 2.53 0 -3 1 -18 171.95 6.62 0 -2 -4 -24 30.61 5.46 0 -2 -3 -23 80.66 7.26 0 -2 -1 -20 -1.77 2.94 0 -2 0 -18 26.46 3.08 0 -2 1 -16 18.75 2.79 0 -1 -3 -21 21.02 4.62 0 -1 -1 -18 400.38 10.93 0 0 -4 -20 19.57 4.74 0 0 -1 -14 44.64 4.15 0 1 -8 -22 0.83 4.74 0 1 -7 -21 -2.70 5.04 0 1 -6 -20 -3.48 4.29 0 1 -5 -18 62.77 5.64 0 1 -4 -17 21.19 4.27 0 2 -10 -20 4.37 5.64 0 2 -9 -19 20.40 5.86 0 2 -7 -17 64.80 6.94 0 2 -6 -15 64.45 5.51 0 3 -14 -17 3.32 5.39 0 3 -13 -17 -0.86 5.02 0 3 -12 -16 -0.35 3.42 0 3 -11 -16 3.57 4.96 0 3 -10 -15 8.18 5.01 0 3 -9 -14 7.95 4.59 0 3 -8 -12 19.09 4.72 0 3 -8 -11 51.61 4.70 0 3 -7 -9 120.21 6.07 0 3 -7 -8 10.94 2.76 0 -3 -1 -22 23.10 3.94 0 -2 -2 -22 173.43 8.84 0 -1 -5 -24 11.23 5.11 0 -1 -4 -23 24.39 5.35 0 -1 -2 -20 11.59 3.77 0 -1 0 -16 12.33 2.56 0 0 -7 -24 3.70 5.20 0 0 -6 -23 7.13 5.42 0 0 -5 -22 30.50 6.01 0 0 -4 -21 58.73 6.32 0 0 -3 -19 2.56 2.68 0 0 -2 -17 20.43 3.33 0 0 -1 -15 691.80 12.99 0 1 -9 -23 0.05 4.44 0 1 -5 -19 9.21 4.51 0 1 -3 -15 33.68 3.72 0 2 -11 -21 1.34 3.80 0 2 -10 -21 10.66 5.17 0 2 -9 -20 30.89 6.93 0 2 -8 -19 29.50 6.58 0 2 -7 -18 45.82 6.57 0 2 -6 -16 88.39 6.38 0 2 -5 -14 31.19 4.28 0 2 -4 -11 81.71 4.82 0 3 -13 -18 -5.44 5.06 0 3 -12 -18 2.58 4.75 0 3 -12 -17 0.44 3.71 0 3 -11 -17 2.78 5.17 0 3 -10 -16 4.90 4.99 0 3 -9 -15 -0.68 4.31 0 3 -8 -13 84.78 6.56 0 3 -7 -11 22.54 4.08 0 3 -7 -10 281.35 9.11 0 4 -16 -8 1.66 3.15 0 4 -16 -7 -1.06 2.74 0 4 -15 -9 3.28 3.60 0 4 -15 -8 -0.49 3.40 0 4 -15 -7 -0.05 3.19 0 4 -15 -6 2.04 3.03 0 4 -14 -9 -0.57 3.38 0 4 -14 -8 2.06 3.45 0 4 -14 -7 1.45 3.22 0 4 -14 -6 1.61 2.95 0 4 -13 -8 0.26 3.05 0 4 -13 -7 -1.42 2.75 0 -1 -3 -22 51.58 5.29 0 1 -7 -22 8.40 4.32 0 2 -6 -17 0.26 3.15 0 2 -5 -15 117.18 6.68 0 2 -4 -12 290.21 8.57 0 3 -8 -14 19.89 3.99 0 4 -16 -9 -1.64 2.54 0 4 -15 -10 0.12 2.96 0 4 -14 -10 3.72 3.13 0 2 2 -16 255.18 7.59 0 2 3 -15 402.18 10.11 0 2 4 -13 405.68 10.18 0 2 5 -11 50.30 4.42 0 3 1 -21 4.83 2.76 0 3 2 -20 34.23 4.24 0 3 3 -19 69.43 5.71 0 3 5 -16 64.17 5.66 0 3 6 -14 62.67 5.95 0 3 8 -7 11.70 3.93 0 3 8 -6 444.30 11.22 0 4 1 -24 -0.17 2.47 0 4 2 -23 1.76 3.26 0 4 3 -22 -1.01 3.46 0 4 4 -21 3.66 4.62 0 4 5 -20 -1.94 4.21 0 4 6 -18 62.18 6.10 0 4 8 -14 0.81 5.08 0 4 9 -10 60.77 5.91 0 5 4 -24 2.79 4.15 0 5 7 -20 2.04 5.28 0 5 8 -18 20.06 6.75 0 5 10 -12 58.99 6.79 0 5 11 -7 19.76 5.07 0 5 11 -6 6.87 4.79 0 5 11 -5 10.68 4.81 0 5 11 -4 9.80 4.52 0 5 11 -3 39.53 5.09 0 5 11 -2 53.00 5.26 0 5 11 -1 4.32 3.39 0 6 8 -21 13.75 6.53 0 6 9 -19 7.37 6.98 0 6 10 -16 1.01 4.58 0 6 11 -13 0.55 6.19 0 6 11 4 2.40 2.45 0 6 12 -8 5.79 4.84 0 6 12 -7 4.12 5.23 0 6 12 -6 10.76 5.30 0 6 12 -4 2.51 4.32 0 6 12 -3 11.96 4.45 0 6 12 -2 -0.02 3.67 0 7 11 -17 -3.96 6.13 0 7 12 -13 5.96 6.21 0 7 12 3 2.92 2.98 0 7 13 -6 -2.83 4.04 0 7 13 -5 1.75 4.11 0 8 13 1 3.55 3.55 0 3 0 -22 -0.29 2.40 0 3 4 -18 9.24 2.92 0 3 5 -17 5.59 3.51 0 3 6 -15 112.72 7.26 0 3 7 -12 204.21 8.75 0 3 8 -8 107.51 6.29 0 4 6 -19 -0.03 5.01 0 4 7 -17 25.66 5.77 0 4 8 -15 37.71 6.37 0 4 9 -12 127.41 8.91 0 4 10 -6 35.36 5.20 0 4 10 -4 23.30 4.36 0 4 10 -3 14.80 3.76 0 4 10 -2 10.62 3.31 0 4 10 -1 4.04 2.90 0 5 3 -25 0.14 3.74 0 5 5 -23 -2.41 4.09 0 5 6 -22 9.71 5.53 0 5 9 -16 5.28 4.33 0 5 10 -14 8.71 5.86 0 5 10 -13 8.20 4.74 0 5 10 5 2.44 1.82 0 5 11 -9 1.30 5.02 0 5 11 -8 3.02 4.45 0 5 11 0 25.73 4.00 0 6 10 -17 5.49 4.70 0 6 11 -14 4.45 4.63 0 6 11 5 12.49 2.71 0 6 12 -10 1.17 5.65 0 6 12 -9 0.72 4.86 0 6 12 -1 -0.76 2.49 0 6 12 0 0.01 3.24 0 7 12 -15 -0.14 5.67 0 7 12 -14 1.30 4.40 0 7 13 -9 2.82 5.44 0 7 13 -8 5.77 5.13 0 7 13 -7 1.41 3.57 0 7 13 -4 0.09 3.04 0 7 13 -3 0.14 3.70 0 7 13 -2 1.53 3.90 0 7 13 -1 -0.73 3.28 0 2 1 -18 2.16 2.12 0 2 2 -17 2.48 2.42 0 2 3 -16 23.12 3.41 0 2 4 -14 328.32 9.35 0 2 5 -12 97.47 5.48 0 2 6 -9 1.33 1.75 0 3 2 -21 50.10 5.01 0 3 3 -20 21.17 4.17 0 3 7 -13 54.40 5.39 0 3 8 -10 -1.03 3.86 0 4 2 -24 6.37 3.41 0 4 3 -23 22.15 4.61 0 4 4 -22 46.22 6.04 0 4 5 -21 68.39 7.18 0 4 7 -18 -1.74 4.89 0 4 8 -16 17.89 5.27 0 4 9 -13 16.40 6.09 0 4 10 -8 54.87 6.20 0 4 10 -7 34.30 4.67 0 4 10 0 20.26 3.52 0 5 7 -21 13.49 6.05 0 5 8 -19 1.60 4.33 0 5 9 -17 10.33 4.86 0 5 10 -15 15.71 6.31 0 5 11 -11 15.24 6.33 0 5 11 -10 -0.34 3.78 0 5 11 2 0.76 2.71 0 6 8 -22 0.74 5.47 0 6 9 -20 14.07 5.79 0 6 10 -18 0.04 4.86 0 6 11 -16 -0.28 5.31 0 6 11 -15 -1.16 4.36 0 6 12 -12 -1.11 5.58 0 6 12 -11 -2.32 5.25 0 6 12 1 0.56 2.82 0 7 13 -12 3.04 5.39 0 7 13 -11 2.31 6.12 0 7 13 -10 -0.24 3.85 0 7 13 0 0.86 3.55 0 2 4 -15 8.11 3.29 0 2 5 -13 404.52 10.92 0 2 6 -10 8.73 2.61 0 3 1 -22 44.34 4.47 0 3 4 -19 23.26 3.82 0 3 5 -18 6.32 3.72 0 3 6 -16 1.92 2.87 0 3 7 -14 88.19 6.97 0 3 8 -11 56.78 5.94 0 3 9 -5 201.47 8.39 0 3 9 -4 36.51 4.46 0 3 9 -3 19.98 3.65 0 4 6 -20 59.74 7.30 0 4 10 -10 30.59 6.30 0 4 10 1 119.51 5.82 0 5 4 -25 11.81 4.70 0 5 5 -24 5.37 3.73 0 5 6 -23 1.51 4.87 0 5 8 -20 9.52 6.49 0 5 9 -18 20.31 6.67 0 5 10 -16 0.31 5.51 0 5 11 -12 1.21 5.93 0 6 9 -21 0.46 6.05 0 6 10 -19 13.38 6.81 0 6 12 2 3.51 2.73 0 7 13 -13 -2.57 5.87 0 7 13 1 9.21 3.42 0 7 13 2 6.86 3.14 0 2 1 -19 104.83 5.48 0 2 2 -18 164.73 6.80 0 2 3 -17 153.02 6.81 0 2 6 -11 80.54 5.01 0 2 7 -7 357.49 9.79 0 3 3 -21 11.70 3.70 0 3 4 -20 53.64 5.63 0 3 6 -17 -1.47 3.50 0 3 7 -15 0.04 4.29 0 3 8 -12 21.18 5.00 0 3 9 -8 18.71 4.64 0 3 9 -7 268.57 10.04 0 3 9 -6 2.20 2.97 0 3 9 -2 95.93 5.26 0 3 9 -1 3.30 2.41 0 4 3 -24 -0.36 3.44 0 4 4 -23 1.06 3.99 0 4 5 -22 -4.13 4.22 0 4 7 -19 64.74 7.47 0 4 8 -17 1.26 3.72 0 4 10 -12 -5.34 4.93 0 4 10 -11 90.87 7.43 0 4 10 2 0.25 2.55 0 5 7 -22 0.78 3.70 0 5 8 -21 -0.03 5.05 0 5 9 -19 31.65 7.84 0 5 10 -17 11.01 6.33 0 5 11 -14 1.68 5.67 0 5 11 -13 13.67 5.04 0 5 11 3 36.91 3.83 0 5 12 -8 -2.44 4.93 0 5 12 -7 5.42 5.07 0 5 12 -6 19.47 5.52 0 5 12 -5 -2.79 3.97 0 5 12 -4 24.43 5.24 0 5 12 -3 9.99 4.47 0 5 12 -2 -1.55 3.32 0 6 10 -20 6.05 6.76 0 6 11 -18 8.96 6.45 0 6 12 -15 2.68 5.29 0 6 12 -14 0.62 4.12 0 6 12 3 -0.10 2.44 0 6 13 -9 2.98 5.58 0 6 13 -8 1.72 5.41 0 6 13 -7 11.19 5.16 0 6 13 -6 14.86 4.43 0 6 13 -5 6.57 3.70 0 6 13 -4 7.13 4.33 0 6 13 -3 3.87 4.19 0 7 14 -9 -0.97 4.76 0 7 14 -8 -1.58 5.01 0 7 14 -7 3.06 5.07 0 7 14 -6 -3.93 4.56 0 7 14 -5 3.72 4.65 0 7 14 -4 3.26 4.53 0 2 0 -20 54.47 4.02 0 2 4 -16 211.72 8.24 0 2 6 -12 108.22 6.28 0 2 7 -9 0.29 2.99 0 2 7 -8 47.31 4.17 0 3 1 -23 -1.63 2.64 0 3 2 -22 7.68 3.36 0 3 5 -19 92.35 7.19 0 3 7 -16 26.27 5.03 0 3 8 -13 87.37 6.62 0 4 2 -25 2.08 3.32 0 4 6 -21 1.27 3.54 0 4 7 -20 2.10 5.36 0 4 8 -18 32.66 6.77 0 4 9 -16 7.55 5.71 0 4 10 -13 53.26 7.68 0 4 10 3 114.50 5.46 0 4 11 -8 4.69 4.64 0 4 11 -7 -1.86 4.43 0 4 11 -6 10.41 4.47 0 4 11 -5 1.06 3.88 0 4 11 -4 39.96 5.24 0 4 11 -3 25.19 4.74 0 4 11 -2 3.10 3.36 0 5 6 -24 3.20 4.61 0 5 7 -23 3.07 5.23 0 5 9 -20 1.32 5.77 0 5 11 -15 8.33 6.70 0 5 11 4 -1.22 2.28 0 5 12 -10 12.36 6.08 0 5 12 -9 4.88 4.02 0 5 12 -1 5.91 3.74 0 5 12 0 10.32 3.61 0 6 11 -19 -0.30 5.94 0 6 12 -16 2.16 6.16 0 6 12 4 0.22 2.38 0 6 13 -12 -3.23 5.12 0 6 13 -11 -1.65 5.82 0 6 13 -10 5.11 4.35 0 6 13 -1 4.76 3.53 0 6 13 0 0.05 3.11 0 7 14 -10 2.89 5.24 0 7 14 -3 2.01 3.15 0 7 14 -2 6.40 4.23 0 7 14 -1 2.54 3.51 0 2 2 -19 11.53 3.33 0 2 3 -18 31.27 3.96 0 2 5 -15 115.13 6.64 0 2 6 -13 138.75 7.36 0 2 7 -10 42.65 4.44 0 3 4 -21 19.64 4.41 0 3 6 -18 30.24 4.58 0 3 8 -14 14.93 4.94 0 3 9 -11 3.55 4.52 0 4 3 -25 -0.24 3.12 0 4 4 -24 4.92 4.15 0 4 5 -23 10.71 4.75 0 4 6 -22 27.81 6.11 0 4 8 -19 2.87 5.59 0 4 9 -17 12.49 6.04 0 4 10 -14 -0.00 5.68 0 4 11 -10 29.44 6.58 0 4 11 -9 43.29 6.41 0 4 11 -1 12.39 3.55 0 5 8 -22 2.89 5.10 0 5 10 -18 18.38 5.88 0 5 11 -16 4.27 6.62 0 5 12 -11 -1.36 4.02 0 5 12 1 2.75 3.29 0 6 12 -17 4.10 6.41 0 6 13 -13 -0.98 5.55 0 7 14 0 -0.20 3.62 0 2 1 -20 5.54 2.45 0 2 4 -17 -3.33 2.81 0 2 6 -14 135.90 7.46 0 2 7 -11 65.38 5.54 0 2 8 -6 517.24 12.16 0 2 8 -5 218.64 7.93 0 2 8 -4 112.31 5.79 0 3 2 -23 18.26 3.74 0 3 3 -22 39.72 4.82 0 3 5 -20 29.59 5.17 0 3 6 -19 12.64 5.05 0 3 7 -17 5.79 3.40 0 3 8 -15 34.94 5.75 0 3 9 -12 44.18 6.07 0 3 10 -7 32.81 5.37 0 3 10 -6 106.07 7.21 0 3 10 -5 1.06 4.09 0 3 10 -4 87.51 6.18 0 3 10 -3 16.73 3.85 0 4 7 -21 19.21 5.63 0 4 9 -18 4.26 5.25 0 4 10 -15 3.51 5.35 0 4 11 -12 28.38 6.55 0 4 11 -11 6.22 5.37 0 4 11 0 20.86 3.24 0 4 11 1 20.18 3.69 0 5 8 -23 0.05 5.05 0 5 9 -21 0.14 5.32 0 5 10 -19 -1.74 4.32 0 5 11 -17 10.91 6.92 0 5 11 5 -0.94 1.97 0 5 12 -14 2.98 5.84 0 5 12 -13 3.31 4.52 0 5 12 2 24.32 3.81 0 5 13 -7 -0.35 4.43 0 5 13 -6 -0.07 4.27 0 5 13 -5 1.44 4.20 0 6 13 -15 -2.58 5.72 0 6 13 -14 0.78 4.07 0 6 13 2 -1.78 2.89 0 6 14 -9 -1.97 4.95 0 6 14 -8 1.53 5.51 0 6 14 -7 4.61 5.32 0 6 14 -6 13.37 5.61 0 6 14 -5 5.22 5.05 0 7 14 1 10.72 3.91 0 2 0 -21 0.42 2.20 0 2 3 -19 89.00 5.82 0 2 5 -16 65.36 5.18 0 2 7 -12 18.33 4.32 0 2 8 -7 161.93 7.18 0 3 4 -22 14.23 4.14 0 3 5 -21 14.10 4.62 0 3 7 -18 -1.39 4.63 0 3 8 -16 -0.42 4.68 0 3 9 -13 15.86 4.25 0 3 10 -9 30.51 5.55 0 3 10 -8 64.75 5.90 0 3 10 -2 10.47 3.36 0 3 10 -1 -0.31 2.65 0 4 4 -25 6.24 4.18 0 4 5 -24 0.55 4.15 0 4 6 -23 2.90 4.48 0 4 7 -22 -0.36 4.43 0 4 8 -20 8.53 4.33 0 4 10 -16 12.23 5.81 0 5 9 -22 2.09 5.79 0 5 10 -20 12.31 6.25 0 5 11 -18 8.48 6.96 0 5 12 -15 1.11 6.39 0 5 12 3 1.96 2.56 0 5 13 -10 1.41 5.70 0 5 13 -9 5.68 5.22 0 5 13 -8 -1.60 3.44 0 5 13 -4 2.61 3.20 0 5 13 -3 1.56 4.23 0 5 13 -2 8.64 4.42 0 6 13 3 1.33 2.86 0 6 14 -12 1.75 5.15 0 6 14 -11 -4.35 5.63 0 6 14 -10 -2.46 3.76 0 6 14 -3 2.07 4.08 0 6 14 -2 5.75 4.31 0 7 14 2 5.88 3.32 0 2 2 -20 57.69 4.68 0 2 4 -18 96.47 5.87 0 2 5 -17 146.66 7.68 0 2 6 -15 61.51 5.29 0 2 8 -10 1.63 3.46 0 2 8 -9 5.41 2.39 0 3 3 -23 2.86 3.30 0 3 6 -20 57.23 6.78 0 3 8 -17 -0.83 4.74 0 3 9 -14 9.47 4.02 0 3 10 -11 2.54 5.15 0 3 10 -10 5.81 3.81 0 3 10 0 20.27 3.23 0 4 3 -26 4.34 3.80 0 4 8 -21 -1.62 5.17 0 4 9 -19 14.79 4.89 0 4 10 -17 1.02 5.32 0 4 11 -14 29.58 6.84 0 4 12 -10 10.93 5.59 0 4 12 -9 0.32 5.23 0 4 12 -8 7.41 3.95 0 4 12 -7 1.03 3.51 0 4 12 -6 2.40 3.37 0 4 12 -5 2.31 3.18 0 4 12 -4 2.11 3.09 0 4 12 -2 18.48 4.25 0 5 10 -21 2.81 6.18 0 5 11 -19 5.08 6.86 0 5 12 -16 1.39 5.31 0 5 13 -12 -2.42 6.22 0 5 13 -11 4.10 4.48 0 5 13 -1 1.09 3.83 0 6 14 -13 3.12 5.76 0 6 14 -1 -1.30 3.42 0 6 14 0 -0.73 3.20 0 2 1 -21 125.43 6.03 0 2 4 -19 28.04 4.41 0 2 7 -14 87.93 6.87 0 2 8 -11 21.34 4.55 0 3 2 -24 2.17 2.75 0 3 4 -23 22.44 4.41 0 3 5 -22 10.71 4.69 0 3 6 -21 3.52 4.39 0 3 7 -19 39.48 5.41 0 3 8 -18 13.47 5.21 0 3 9 -15 3.25 3.61 0 3 10 -13 4.72 4.97 0 3 10 -12 18.73 4.68 0 3 10 1 26.93 3.36 0 4 5 -25 1.78 4.23 0 4 6 -24 0.99 4.24 0 4 7 -23 5.74 5.16 0 4 9 -20 -4.67 5.43 0 4 11 -16 0.25 5.61 0 4 11 -15 10.10 4.90 0 4 11 3 7.73 2.80 0 4 12 -11 20.35 6.22 0 4 12 -1 6.15 3.49 0 5 12 -17 2.28 4.42 0 5 12 4 7.65 2.63 0 5 13 -14 1.41 5.89 0 5 13 -13 9.74 4.96 0 5 13 0 4.06 2.76 0 6 14 1 1.14 3.30 0 6 15 -8 1.18 4.73 0 6 15 -7 3.40 4.97 0 1 5 -12 49.29 4.25 0 2 2 -21 5.94 2.87 0 2 5 -18 49.48 5.34 0 2 6 -17 0.68 3.59 0 2 7 -15 47.46 5.77 0 2 8 -13 138.18 8.35 0 2 8 -12 17.97 3.96 0 2 9 -8 31.46 4.84 0 2 9 -7 126.98 7.24 0 2 9 -6 180.14 8.15 0 2 9 -5 53.93 5.14 0 2 9 -4 21.67 3.91 0 2 9 -3 85.88 5.50 0 3 3 -24 17.67 4.25 0 3 7 -20 3.18 5.05 0 3 9 -16 10.78 4.18 0 3 11 -9 8.14 5.55 0 3 11 -7 96.16 7.04 0 3 11 -6 -0.07 3.30 0 3 11 -5 107.37 6.89 0 3 11 -4 17.82 4.49 0 3 11 -3 23.70 4.49 0 4 8 -22 9.15 4.31 0 4 9 -21 5.26 5.69 0 4 10 -19 2.67 5.95 0 4 11 -17 1.18 5.62 0 4 11 4 15.57 2.86 0 4 12 -13 30.30 7.15 0 4 12 0 41.46 4.69 0 5 12 -18 1.28 4.39 0 5 13 -15 3.47 5.52 0 5 13 2 3.20 2.99 0 5 14 -10 -0.09 5.88 0 5 14 -9 -1.06 5.62 0 5 14 -8 0.69 4.83 0 5 14 -7 0.50 4.67 0 5 14 -6 4.00 4.73 0 5 14 -5 -1.73 4.81 0 5 14 -4 7.47 4.87 0 6 14 2 1.98 3.25 0 6 15 -9 1.73 4.07 0 6 15 -6 2.33 4.00 0 6 15 -5 -0.79 4.35 0 6 15 -4 0.19 4.57 0 6 15 -3 -3.75 3.89 0 1 4 -14 197.21 7.16 0 1 6 -10 36.42 4.08 0 2 1 -22 -1.82 2.43 0 2 4 -20 83.48 6.23 0 2 5 -19 79.31 6.33 0 2 7 -16 51.85 6.04 0 2 8 -14 60.21 6.61 0 2 9 -10 1.15 3.86 0 2 9 -9 15.01 3.61 0 2 9 -2 92.20 5.40 0 3 5 -23 8.15 4.40 0 3 6 -22 20.85 5.53 0 3 7 -21 35.39 6.31 0 3 8 -19 -0.64 4.67 0 3 9 -17 7.75 4.12 0 3 10 -15 15.20 5.93 0 3 11 -11 2.61 5.38 0 3 11 -10 28.81 5.17 0 3 11 -1 2.31 3.04 0 4 6 -25 2.75 4.37 0 4 7 -24 -1.72 4.32 0 4 8 -23 -3.66 4.87 0 4 10 -20 -2.91 5.52 0 4 12 -15 4.68 6.63 0 4 12 -14 0.84 4.60 0 4 12 1 15.20 3.70 0 4 13 -10 3.52 5.25 0 4 13 -9 5.08 5.65 0 4 13 -8 0.84 5.34 0 4 13 -7 -0.51 4.50 0 4 13 -6 1.23 4.41 0 4 13 -5 3.10 4.74 0 4 13 -4 2.81 4.50 0 5 12 5 1.33 2.23 0 5 13 -17 2.87 6.39 0 5 13 -16 6.47 4.82 0 5 14 -12 9.22 5.82 0 5 14 -11 6.36 4.48 0 5 14 -3 2.77 3.17 0 5 14 -2 -1.06 4.11 0 6 15 -2 1.15 4.09 0 6 15 -1 1.35 3.61 0 1 3 -16 -0.37 2.26 0 1 4 -15 7.47 2.68 0 1 5 -13 46.51 4.05 0 2 2 -22 57.99 5.06 0 2 3 -21 65.41 5.37 0 2 6 -18 35.90 5.17 0 2 7 -17 61.49 6.38 0 2 8 -15 122.29 8.44 0 2 9 -12 17.23 5.04 0 2 9 -11 46.03 5.18 0 3 3 -25 1.16 3.01 0 3 4 -24 2.28 3.30 0 3 8 -20 45.94 7.21 0 3 9 -18 0.82 3.74 0 3 10 -16 6.24 5.65 0 3 11 -13 0.97 5.48 0 3 11 0 3.06 3.01 0 4 9 -22 -2.34 3.70 0 4 10 -21 -0.88 5.05 0 4 11 -19 0.53 5.31 0 4 12 -16 9.31 6.78 0 4 12 2 1.05 2.84 0 4 13 -12 6.88 6.52 0 4 13 -11 7.61 4.72 0 4 13 -3 3.48 3.19 0 4 13 -2 3.43 4.03 0 5 13 3 6.65 3.13 0 5 14 -15 2.07 5.56 0 5 14 -14 0.53 5.46 0 5 14 -1 1.59 3.77 0 5 14 0 0.89 3.46 0 6 15 0 0.74 3.62 0 1 5 -14 41.95 4.45 0 1 7 -9 36.02 4.45 0 2 4 -21 26.18 4.64 0 2 5 -20 25.56 5.01 0 2 6 -19 20.63 5.05 0 2 8 -16 47.02 6.28 0 2 9 -13 0.24 4.57 0 2 10 -9 34.24 5.42 0 2 10 -8 0.11 3.93 0 2 10 -7 77.07 6.48 0 2 10 -6 29.36 4.91 0 2 10 -5 91.83 6.32 0 2 10 -4 78.41 5.96 0 3 5 -24 8.85 4.49 0 3 6 -23 15.08 5.09 0 3 7 -22 3.07 4.97 0 3 8 -21 -2.43 4.55 0 3 9 -19 19.91 6.20 0 3 10 -17 -1.51 5.37 0 3 12 -10 -2.95 4.87 0 3 12 -9 24.22 6.42 0 3 12 -7 32.05 5.88 0 3 12 -6 15.44 5.04 0 3 12 -5 19.37 5.07 0 3 12 -4 45.17 5.73 0 4 11 -20 2.68 5.37 0 4 12 -17 3.73 5.78 0 4 13 -1 24.90 4.52 0 5 13 4 0.96 2.32 0 5 14 1 -0.25 3.22 0 5 15 -10 2.82 5.79 0 5 15 -9 1.37 5.48 0 5 15 -8 3.05 5.67 0 5 15 -7 -2.95 5.13 0 5 15 -6 7.32 5.51 0 5 15 -5 2.79 4.98 0 6 15 1 4.86 3.59 0 1 2 -18 -0.49 2.12 0 1 3 -17 64.61 4.64 0 1 4 -16 34.47 3.62 0 1 5 -15 215.08 8.43 0 1 6 -13 38.61 4.62 0 1 7 -11 99.06 6.21 0 1 7 -10 278.31 9.23 0 2 3 -22 0.05 3.06 0 2 7 -18 46.49 5.92 0 2 9 -14 101.18 8.20 0 2 10 -11 3.46 4.60 0 2 10 -10 0.72 4.22 0 2 10 -3 -0.64 3.22 0 2 10 -2 65.58 5.27 0 3 4 -25 21.00 4.39 0 3 9 -20 -2.77 5.34 0 3 10 -18 14.29 6.20 0 3 11 -16 1.55 5.84 0 3 11 -15 -0.60 4.05 0 3 11 2 1.28 2.57 0 3 12 -12 18.79 6.55 0 3 12 -11 0.82 4.04 0 3 12 -3 33.46 4.57 0 3 12 -2 12.30 4.06 0 4 10 -22 3.42 4.37 0 4 12 -18 0.19 4.31 0 4 13 -16 3.18 5.49 0 4 13 -15 10.09 5.92 0 4 13 0 15.28 3.50 0 4 14 -10 8.97 6.38 0 4 14 -9 -2.70 5.53 0 4 14 -8 4.18 5.55 0 4 14 -6 -0.73 4.91 0 4 14 -5 -4.65 4.51 0 5 15 -12 5.32 4.35 0 5 15 -4 2.28 3.39 0 5 15 -3 -1.94 4.47 0 1 3 -18 45.49 4.25 0 1 4 -17 24.65 3.69 0 1 5 -16 -2.25 3.01 0 1 6 -14 246.43 9.36 0 1 7 -12 28.94 4.27 0 1 8 -7 62.31 5.28 0 1 8 -6 74.66 5.52 0 2 2 -23 3.87 2.83 0 2 4 -22 19.69 4.29 0 2 5 -21 27.73 4.76 0 2 6 -20 77.70 6.88 0 2 7 -19 35.52 5.95 0 2 9 -15 20.98 4.72 0 2 10 -13 42.52 6.45 0 2 10 -1 193.50 7.76 0 3 6 -24 -0.23 3.82 0 3 7 -23 2.18 3.36 0 3 8 -22 16.98 5.92 0 3 9 -21 26.07 6.36 0 3 10 -19 3.41 5.89 0 3 11 -17 -0.31 5.74 0 3 12 -13 0.19 4.17 0 3 12 -1 5.38 3.48 0 4 12 -19 0.09 3.97 0 4 12 4 15.80 3.09 0 4 13 -17 5.37 6.17 0 4 13 1 -0.47 2.47 0 4 14 -13 4.89 6.06 0 4 14 -12 -0.41 5.55 0 4 14 -11 8.33 4.95 0 4 14 -4 -0.17 3.19 0 4 14 -3 2.79 4.39 0 5 14 2 6.67 3.30 0 5 15 -2 6.09 3.53 0 1 6 -15 -3.45 3.25 0 1 7 -13 165.36 8.22 0 1 8 -10 9.67 3.56 0 1 8 -9 22.68 3.39 0 1 8 -8 36.24 4.15 0 1 8 -5 256.84 8.28 0 2 3 -23 6.28 3.26 0 2 5 -22 7.31 3.77 0 2 6 -21 37.80 5.93 0 2 7 -20 42.51 6.03 0 2 8 -18 15.01 4.22 0 2 9 -16 7.09 3.99 0 2 10 -14 29.38 6.57 0 2 11 -10 -1.75 4.35 0 2 11 -9 -0.09 4.95 0 2 11 -8 70.85 6.92 0 2 11 -7 3.10 4.33 0 2 11 -6 72.21 6.55 0 2 11 -5 4.03 4.03 0 3 6 -25 10.53 4.48 0 3 7 -24 7.95 5.11 0 3 8 -23 12.13 5.31 0 3 10 -20 16.20 6.63 0 3 11 -18 0.42 6.05 0 3 11 3 3.41 2.48 0 3 12 -15 1.89 5.96 0 3 12 0 19.60 3.90 0 3 13 -11 1.16 5.46 0 3 13 -9 1.67 5.66 0 3 13 -8 20.23 5.95 0 3 13 -7 40.97 6.51 0 3 13 -6 2.15 5.08 0 3 13 -5 26.78 5.88 0 3 13 -4 20.14 4.99 0 4 13 -18 -3.49 5.64 0 4 13 2 22.37 4.18 0 4 14 -15 -3.23 5.80 0 4 14 -14 5.20 4.58 0 4 14 -2 7.67 3.41 0 4 14 -1 5.42 4.30 0 5 14 3 1.17 3.08 0 5 15 0 7.02 4.19 0 5 16 -7 4.89 5.49 0 5 16 -6 -1.88 5.11 0 5 16 -5 0.35 4.68 0 1 3 -19 16.65 3.39 0 1 4 -18 -2.54 2.49 0 1 6 -16 35.94 5.03 0 1 7 -14 28.71 4.96 0 1 8 -12 163.82 8.56 0 2 4 -23 11.53 3.90 0 2 8 -19 35.86 6.42 0 2 9 -17 27.14 5.06 0 2 10 -15 14.20 5.69 0 2 11 -12 13.77 5.84 0 2 11 -11 -0.07 4.56 0 2 11 -4 7.70 3.33 0 3 9 -22 -1.08 5.21 0 3 10 -21 2.25 5.80 0 3 11 -19 5.12 6.26 0 3 12 -17 -1.44 5.42 0 3 12 -16 3.12 4.45 0 3 12 1 11.63 3.37 0 3 13 -13 -0.80 6.06 0 3 13 -12 2.67 4.36 0 3 13 -3 8.26 4.61 0 4 12 5 2.81 2.36 0 4 13 3 0.87 2.71 0 4 14 -16 -0.41 5.46 0 4 14 0 9.08 4.26 0 4 15 -11 2.11 6.11 0 4 15 -10 1.96 5.96 0 4 15 -9 2.96 5.88 0 4 15 -8 0.69 5.05 0 4 15 -7 0.79 5.37 0 4 15 -6 1.01 5.18 0 4 15 -5 4.12 4.72 0 5 15 1 0.60 3.64 0 5 16 -4 -2.26 4.40 0 5 16 -3 2.32 4.34 0 1 4 -19 119.29 6.72 0 1 5 -18 62.47 5.49 0 1 7 -15 236.36 10.01 0 1 8 -13 79.12 6.83 0 1 9 -9 29.60 4.96 0 1 9 -8 63.24 5.84 0 1 9 -7 13.43 3.76 0 1 9 -6 29.31 4.51 0 1 9 -5 39.56 4.50 0 2 3 -24 3.99 3.07 0 2 5 -23 4.52 3.75 0 2 6 -22 3.31 4.35 0 2 7 -21 8.35 5.09 0 2 8 -20 31.67 6.42 0 2 9 -18 6.85 4.10 0 2 10 -16 7.58 4.17 0 2 11 -13 1.48 3.95 0 2 11 -2 48.76 4.72 0 3 9 -23 1.29 5.39 0 3 11 -20 -1.63 5.69 0 3 12 -18 3.79 6.14 0 3 12 2 2.38 2.86 0 3 13 -15 2.54 6.29 0 3 13 -14 1.37 4.51 0 3 13 -2 6.17 3.18 0 3 13 -1 0.12 3.52 0 4 14 1 10.63 4.06 0 4 15 -14 4.43 6.12 0 4 15 -13 -0.63 5.26 0 4 15 -12 4.85 4.42 0 4 15 -4 3.26 4.46 0 4 15 -3 1.93 4.41 0 5 15 2 2.00 3.06 0 5 16 -2 0.08 4.33 0 1 3 -20 264.46 9.17 0 1 7 -16 -2.44 3.57 0 1 8 -14 217.82 9.70 0 1 9 -12 79.26 7.13 0 1 9 -11 57.59 6.23 0 1 9 -10 25.21 4.25 0 1 9 -4 92.38 5.37 0 1 9 -3 16.13 3.27 0 2 4 -24 1.97 3.25 0 2 7 -22 11.26 4.68 0 2 8 -21 32.35 6.11 0 2 9 -19 14.95 5.49 0 2 10 -17 2.35 3.87 0 2 11 -1 82.99 5.53 0 2 12 -11 1.55 5.43 0 2 12 -10 -0.34 5.22 0 2 12 -9 19.86 4.70 0 2 12 -8 7.63 4.02 0 2 12 -6 7.71 4.68 0 2 12 -5 8.81 4.89 0 2 12 -4 24.70 5.03 0 3 10 -22 8.83 4.73 0 3 11 -21 15.29 6.75 0 3 12 -19 0.76 5.98 0 3 13 -16 2.10 5.77 0 3 13 0 2.22 3.45 0 3 14 -11 1.03 6.24 0 3 14 -10 -4.65 5.25 0 3 14 -9 5.94 4.41 0 3 14 -8 11.67 4.72 0 3 14 -7 0.11 3.86 0 3 14 -6 14.07 5.48 0 3 14 -5 2.32 5.05 0 3 14 -4 4.63 4.51 0 4 12 6 27.82 3.29 0 4 13 4 0.22 2.80 0 4 15 -2 0.76 4.38 0 5 16 -1 3.76 3.95 0 1 2 -21 277.59 9.06 0 1 4 -20 2.49 3.35 0 1 5 -19 6.16 3.66 0 1 6 -18 0.26 2.53 0 1 7 -17 3.84 4.07 0 1 8 -15 11.06 3.94 0 1 9 -13 193.42 10.04 0 1 10 -8 112.22 7.61 0 1 10 -7 43.90 5.54 0 2 5 -24 3.51 3.63 0 2 6 -23 8.49 3.39 0 2 9 -20 31.61 6.68 0 2 10 -18 12.68 4.58 0 2 11 0 54.65 4.58 0 2 12 -13 9.13 6.26 0 2 12 -12 -1.05 3.90 0 2 12 -3 7.35 4.23 0 3 12 -20 1.21 6.25 0 3 12 3 3.81 2.73 0 3 13 -18 2.08 5.37 0 3 13 -17 -0.89 3.83 0 3 13 1 -0.47 3.13 0 3 14 -14 3.78 5.88 0 3 14 -13 -1.39 4.39 0 3 14 -3 7.05 4.66 0 4 15 -1 14.13 4.59 0 4 16 -11 0.99 5.14 0 4 16 -10 2.44 4.44 0 4 16 -9 -2.17 3.85 0 4 16 -8 1.94 3.99 0 4 16 -7 1.53 5.10 0 4 16 -6 3.57 5.46 0 4 16 -5 2.40 4.75 0 5 15 3 -0.39 3.11 0 5 16 0 -0.65 3.46 0 0 5 -12 22.06 3.31 0 1 3 -21 -0.53 3.01 0 1 5 -20 90.69 6.78 0 1 6 -19 58.42 6.07 0 1 7 -18 51.89 6.12 0 1 8 -17 0.85 3.94 0 1 8 -16 11.30 3.77 0 1 9 -15 105.94 8.21 0 1 9 -14 -3.56 3.50 0 1 10 -12 54.99 6.75 0 1 10 -11 137.98 8.83 0 1 10 -10 -0.39 3.39 0 1 10 -9 7.57 3.69 0 1 10 -6 16.19 3.64 0 1 10 -5 71.29 5.72 0 1 10 -4 -1.16 3.30 0 2 4 -25 1.49 3.12 0 2 6 -24 0.41 3.85 0 2 7 -23 0.56 4.26 0 2 8 -22 -1.15 4.80 0 2 9 -21 0.89 5.17 0 2 10 -19 17.55 5.00 0 2 11 -18 4.66 5.40 0 2 11 -17 1.35 4.16 0 2 11 1 -0.14 2.42 0 2 12 -15 11.94 6.61 0 2 12 -14 2.74 4.43 0 2 12 -2 38.45 5.18 0 2 13 -10 1.13 5.07 0 2 13 -8 3.84 5.41 0 2 13 -7 5.87 5.41 0 3 14 -16 -3.62 5.57 0 3 14 -15 2.28 4.34 0 3 14 -2 -1.71 2.78 0 3 14 -1 1.52 3.71 0 3 15 -11 -0.23 5.28 0 3 15 -10 5.00 6.21 0 3 15 -7 8.70 5.54 0 4 13 5 9.17 2.84 0 4 14 3 12.15 3.71 0 4 15 0 3.24 3.07 0 4 16 -4 0.97 4.56 0 4 16 -3 0.28 4.75 0 5 16 1 -0.22 3.24 0 0 4 -14 789.41 14.07 0 0 5 -13 365.07 10.16 0 0 6 -11 -1.19 2.76 0 0 6 -10 116.65 5.75 0 1 4 -21 154.75 7.99 0 1 6 -20 0.87 4.04 0 1 7 -19 -1.22 4.23 0 1 9 -16 0.11 4.82 0 1 10 -13 30.91 6.46 0 1 10 -3 5.43 3.34 0 2 5 -25 3.33 3.78 0 2 7 -24 2.46 3.99 0 2 8 -23 4.16 4.85 0 2 9 -22 10.48 5.26 0 2 10 -20 6.31 4.33 0 2 11 -19 6.40 5.64 0 2 12 -16 4.63 5.62 0 2 13 -13 0.92 6.13 0 2 13 -12 5.79 5.74 0 2 13 -11 13.55 4.88 0 2 13 -6 4.78 3.81 0 2 13 -5 2.09 4.50 0 2 13 -4 -1.44 4.58 0 3 12 4 0.29 2.34 0 3 13 2 3.84 3.06 0 3 14 0 3.30 3.62 0 3 15 -14 -0.15 5.24 0 3 15 -13 -2.63 5.53 0 3 15 -12 0.63 4.06 0 3 15 -6 0.64 3.89 0 3 15 -5 12.23 5.76 0 3 15 -4 5.35 4.65 0 4 15 1 1.90 3.45 0 4 16 -2 -1.12 4.41 0 5 16 2 -0.26 3.38 0 0 4 -15 183.05 7.36 0 0 5 -14 3.47 3.29 0 0 6 -13 71.30 5.62 0 0 6 -12 248.88 8.66 0 0 7 -9 325.23 10.03 0 0 7 -7 -0.23 2.77 0 1 3 -22 159.13 7.60 0 1 5 -21 -2.39 3.63 0 1 8 -18 -0.04 3.06 0 1 9 -17 1.01 4.71 0 1 10 -15 10.13 5.82 0 1 10 -14 79.21 7.13 0 1 10 -2 40.69 4.53 0 1 11 -12 21.41 5.82 0 1 11 -11 0.56 5.21 0 1 11 -10 25.63 5.74 0 1 11 -9 41.75 5.49 0 1 11 -8 10.39 4.09 0 1 11 -7 5.26 4.50 0 1 11 -6 2.15 4.05 0 1 11 -5 -1.53 3.63 0 2 6 -25 0.13 3.98 0 2 10 -21 17.49 5.91 0 2 11 -20 3.71 6.26 0 2 12 -18 17.63 6.58 0 2 12 -17 3.99 4.50 0 2 12 0 24.39 4.26 0 2 13 -15 0.96 6.31 0 2 13 -14 20.43 5.56 0 2 13 -3 28.90 5.26 0 3 13 3 0.96 2.75 0 3 15 -3 -0.92 4.45 0 4 14 4 3.10 3.02 0 4 15 2 3.82 3.77 0 4 16 -1 3.49 4.50 0 4 17 -6 3.53 5.03 0 4 17 -5 3.33 5.42 0 0 4 -16 347.89 10.03 0 0 5 -15 438.01 11.65 0 0 6 -14 341.27 10.82 0 0 7 -12 19.11 4.13 0 0 7 -11 140.06 6.81 0 1 4 -22 1.55 3.41 0 1 5 -22 55.21 5.60 0 1 6 -21 57.83 6.26 0 1 7 -20 28.40 4.71 0 1 9 -18 17.45 5.52 0 1 10 -1 -1.47 2.89 0 1 11 -14 -5.26 4.92 0 1 11 -13 102.88 9.07 0 1 11 -4 -0.24 3.52 0 1 11 -3 0.05 3.41 0 2 8 -24 4.23 4.30 0 2 9 -23 -3.58 4.34 0 2 10 -22 -2.25 5.43 0 2 11 -21 0.40 5.20 0 2 11 3 22.43 3.14 0 2 12 -19 11.46 6.45 0 2 12 1 93.55 6.11 0 2 13 -17 11.28 6.14 0 2 13 -16 1.83 5.53 0 2 13 -2 1.71 3.09 0 2 13 -1 18.60 4.47 0 2 14 -13 4.92 5.88 0 2 14 -12 0.48 6.21 0 2 14 -11 3.54 5.63 0 2 14 -10 5.50 4.52 0 2 14 -9 -0.26 4.02 0 2 14 -8 5.92 4.26 0 2 14 -7 4.00 5.17 0 2 14 -6 5.77 5.48 0 2 14 -5 0.31 4.57 0 3 12 5 35.03 3.51 0 3 14 1 2.83 3.49 0 3 15 -2 0.01 2.99 0 3 16 -12 -5.30 5.46 0 3 16 -11 1.36 5.60 0 3 16 -10 1.21 5.47 0 3 16 -9 7.84 5.61 0 3 16 -8 1.16 5.10 0 3 16 -7 4.16 5.78 0 3 16 -6 3.18 5.49 0 4 16 0 1.42 4.11 0 4 17 -4 0.57 4.65 0 4 17 -3 -1.53 4.79 0 0 3 -17 173.11 6.78 0 0 4 -17 16.75 3.71 0 0 5 -16 61.72 5.45 0 0 6 -15 59.90 5.67 0 0 7 -14 3.33 3.77 0 0 7 -13 66.78 5.41 0 0 8 -11 7.77 4.30 0 0 8 -10 94.81 6.64 0 0 8 -9 237.41 9.01 0 0 8 -8 4.76 2.47 0 0 8 -7 234.35 8.41 0 0 8 -5 257.00 8.66 0 1 3 -23 -1.76 3.00 0 1 6 -22 -0.91 3.89 0 1 7 -21 -1.34 4.27 0 1 8 -20 -2.35 3.86 0 1 9 -19 -0.74 4.78 0 1 10 -17 0.35 3.71 0 1 10 0 345.87 9.69 0 1 11 -15 33.43 7.00 0 1 11 -2 16.78 4.05 0 1 12 -12 21.53 6.23 0 1 12 -11 30.35 6.68 0 1 12 -10 -3.04 5.23 0 1 12 -9 8.65 5.57 0 1 12 -8 37.69 6.61 0 1 12 -6 2.91 4.35 0 2 12 -20 5.56 6.07 0 2 13 -18 0.16 6.16 0 2 14 -15 4.43 5.87 0 2 14 -14 4.37 5.68 0 2 14 -4 10.99 5.31 0 3 13 4 4.66 2.69 0 3 14 2 -0.26 3.41 0 3 15 -1 -0.54 2.88 0 3 16 -5 2.98 3.83 0 4 15 3 2.94 3.05 0 4 16 1 -0.09 3.88 0 4 17 -2 3.33 4.88 0 0 5 -17 103.47 6.44 0 0 6 -16 79.37 6.14 0 0 8 -13 57.51 6.05 0 0 8 -12 140.63 7.59 0 0 9 -10 34.89 5.41 0 0 9 -9 97.11 7.07 0 0 9 -8 361.67 11.69 0 1 5 -23 1.80 3.53 0 1 7 -22 15.42 5.05 0 1 8 -21 22.90 5.57 0 1 9 -20 4.47 5.04 0 1 10 -18 1.99 3.68 0 1 11 -17 2.44 5.09 0 1 11 -16 -0.31 3.91 0 1 11 -1 104.63 6.48 0 1 12 -14 32.92 7.36 0 1 12 -13 0.45 5.32 0 1 12 -5 2.61 3.27 0 1 12 -4 1.77 3.91 0 2 12 2 2.30 2.30 0 2 13 0 17.85 3.67 0 2 14 -17 -2.77 5.15 0 2 14 -16 2.69 5.44 0 2 14 -3 4.61 3.48 0 2 14 -2 14.58 5.03 0 2 15 -12 0.85 5.94 0 2 15 -11 1.94 6.33 0 2 15 -10 -3.66 5.90 0 2 15 -9 1.47 5.88 0 2 15 -8 0.87 5.76 0 2 15 -7 6.68 6.01 0 3 15 0 4.20 3.21 0 3 16 -3 7.28 4.95 0 3 17 -9 0.11 5.92 0 3 17 -8 2.63 5.28 0 4 15 4 -1.48 2.59 0 4 16 2 3.80 3.38 0 4 17 -1 2.47 4.47 0 0 3 -18 -1.23 2.26 0 0 4 -18 23.67 3.69 0 0 5 -18 -2.38 2.92 0 0 7 -16 -1.32 3.65 0 0 8 -15 1.56 4.08 0 0 8 -14 15.98 3.91 0 0 9 -13 2.59 4.30 0 0 9 -12 15.03 4.74 0 0 9 -11 57.87 5.62 0 0 9 -7 10.69 2.95 0 0 9 -6 88.58 5.62 0 0 9 -5 34.91 4.68 0 1 6 -23 26.33 5.11 0 1 8 -22 3.51 4.42 0 1 9 -21 -0.72 4.93 0 1 10 -19 -1.50 3.44 0 1 11 -18 1.00 5.47 0 1 12 -16 12.71 6.06 0 1 12 -15 -2.33 4.04 0 1 12 -3 6.83 3.99 0 1 13 -12 6.57 5.72 0 1 13 -11 2.37 5.96 0 1 13 -10 11.18 6.26 0 1 13 -9 3.69 5.60 0 1 13 -8 -0.42 5.25 0 1 13 -7 3.05 5.31 0 2 12 3 0.33 2.66 0 2 13 1 1.16 3.26 0 2 14 -1 8.04 4.48 0 2 15 -15 -1.42 5.74 0 2 15 -14 -0.96 5.31 0 2 15 -13 0.37 4.05 0 2 15 -6 2.30 4.05 0 2 15 -5 6.63 5.55 0 2 15 -4 1.39 4.52 0 3 14 3 -0.97 3.11 0 3 15 1 0.87 3.50 0 3 16 -2 2.87 3.49 0 3 16 -1 1.55 4.01 0 3 17 -7 0.53 3.95 0 3 17 -6 -1.47 5.39 0 3 17 -5 0.68 4.91 0 4 17 0 3.17 4.20 0 0 2 -19 26.03 3.07 0 0 3 -19 3.05 2.43 0 0 4 -19 19.07 3.53 0 0 6 -18 23.40 4.53 0 0 7 -17 45.07 5.76 0 0 8 -16 50.60 6.26 0 0 9 -14 36.41 6.08 0 0 9 -4 136.84 7.02 0 0 10 -11 11.35 4.90 0 0 10 -10 6.51 4.64 0 0 10 -9 105.77 7.80 0 0 10 -8 -2.03 4.46 0 0 10 -7 460.53 13.57 0 1 5 -24 20.29 4.46 0 1 6 -24 0.98 3.99 0 1 7 -23 -0.14 3.90 0 1 9 -22 2.63 4.66 0 1 10 -20 2.27 3.78 0 1 11 -19 0.31 5.40 0 1 11 0 -0.96 2.37 0 1 12 -17 6.64 6.07 0 1 12 -2 53.83 5.14 0 1 13 -13 47.37 6.85 0 1 13 -6 2.27 3.66 0 1 13 -5 7.69 5.09 0 1 13 -4 1.79 4.16 0 2 13 2 22.56 4.07 0 2 14 0 -2.92 3.72 0 2 15 -3 11.04 5.21 0 2 16 -12 0.60 5.09 0 2 16 -11 1.49 5.59 0 2 16 -10 -0.50 5.86 0 2 16 -9 5.02 5.89 0 2 16 -8 7.37 5.75 0 3 13 5 3.93 2.51 0 3 15 2 1.76 3.63 0 3 16 0 0.26 3.80 0 3 17 -4 7.63 5.50 0 3 17 -3 -0.47 4.53 0 4 16 3 -1.53 3.24 0 4 17 1 2.47 4.05 0 0 5 -19 1.27 3.05 0 0 6 -19 27.57 4.84 0 0 8 -17 4.40 4.55 0 0 9 -16 3.07 4.81 0 0 9 -15 41.00 5.30 0 0 9 -3 182.44 7.23 0 0 10 -14 1.56 4.59 0 0 10 -12 61.05 6.24 0 0 10 -6 10.96 3.73 0 0 10 -5 26.13 4.67 0 1 7 -24 17.74 4.98 0 1 8 -23 8.17 4.65 0 1 10 -21 4.73 3.93 0 1 11 -20 4.37 5.53 0 1 11 1 186.73 7.70 0 1 12 -18 -2.88 3.79 0 1 12 -1 3.36 3.76 0 1 13 -16 5.46 6.17 0 1 13 -15 6.03 4.72 0 1 13 -3 5.48 4.28 0 1 14 -12 7.83 6.69 0 1 14 -11 8.53 6.48 0 1 14 -10 -0.16 6.01 0 1 14 -9 10.96 6.37 0 1 14 -8 1.79 5.69 0 1 14 -7 -0.10 5.01 0 2 15 -2 -0.18 4.56 0 2 16 -13 1.10 4.12 0 2 16 -7 1.10 4.04 0 2 16 -6 1.99 5.60 0 2 16 -5 4.36 5.19 0 4 17 2 2.23 3.84 0 0 2 -20 31.25 3.41 0 0 3 -20 6.94 2.68 0 0 4 -20 19.56 3.67 0 0 5 -20 17.41 4.16 0 0 7 -19 -3.15 3.71 0 0 8 -18 18.03 5.13 0 0 9 -17 21.02 5.59 0 0 9 -2 9.84 2.83 0 0 10 -15 -1.61 4.95 0 0 10 -4 62.11 5.16 0 0 10 -3 8.53 3.68 0 0 11 -13 5.71 5.05 0 0 11 -12 5.33 5.45 0 0 11 -11 17.20 5.40 0 0 11 -10 3.21 3.83 0 0 11 -9 25.98 4.95 0 0 11 -8 154.61 8.77 0 0 11 -7 4.62 5.19 0 0 11 -6 290.91 11.50 0 1 6 -25 4.98 3.95 0 1 8 -24 0.69 4.62 0 1 9 -23 2.20 4.45 0 1 10 -22 3.84 5.02 0 1 11 -21 -4.13 5.21 0 1 12 -20 -1.27 4.93 0 1 12 -19 0.96 3.97 0 1 12 0 130.58 7.32 0 1 13 -18 3.52 6.02 0 1 13 -17 3.47 4.28 0 1 13 -2 10.47 4.38 0 1 14 -15 1.93 5.92 0 1 14 -14 9.33 5.98 0 1 14 -13 3.01 4.72 0 1 14 -6 8.49 4.24 0 1 14 -5 1.35 5.02 0 2 12 4 33.10 3.69 0 2 13 3 19.58 3.74 0 2 14 1 12.52 3.45 0 2 15 -1 1.04 4.34 0 2 16 -4 5.30 5.47 0 2 17 -10 2.20 5.23 0 3 13 6 40.95 3.96 0 3 15 3 0.66 3.28 0 3 16 1 3.59 3.78 0 3 17 -1 3.06 4.66 0 0 4 -21 51.18 4.86 0 0 5 -21 2.77 3.21 0 0 6 -20 -0.91 2.73 0 0 7 -20 15.29 4.77 0 0 8 -19 19.63 5.40 0 0 9 -18 6.88 4.92 0 0 10 -17 1.43 5.00 0 0 10 -16 6.02 3.88 0 0 11 -15 10.17 5.64 0 0 11 -14 1.95 4.82 0 0 11 -5 22.25 5.03 0 0 11 -4 13.81 4.26 0 0 12 -11 15.44 5.69 0 0 12 -10 11.00 5.78 0 0 12 -9 8.59 5.71 0 0 12 -8 0.05 4.97 0 1 11 2 6.57 2.95 0 1 12 1 -1.02 3.20 0 1 13 -1 25.91 4.81 0 1 14 -17 4.41 5.82 0 1 14 -4 3.35 3.59 0 1 14 -3 6.37 4.51 0 1 15 -13 6.04 5.56 0 1 15 -12 8.99 6.20 0 1 15 -11 1.50 6.28 0 1 15 -10 4.09 6.27 0 1 15 -8 -1.59 5.64 0 1 15 -7 2.30 5.17 0 2 14 2 6.00 3.81 0 2 15 0 8.93 4.52 0 2 16 -3 0.31 3.52 0 2 16 -2 16.92 5.25 0 2 17 -9 -0.23 4.16 0 2 17 -8 -1.26 3.92 0 2 17 -7 1.69 5.70 0 2 17 -6 -1.19 5.61 0 3 14 5 12.81 3.32 0 3 16 2 -0.66 3.67 0 3 17 0 3.54 4.47 0 -1 5 -12 50.03 4.32 0 -1 6 -11 14.02 3.31 0 -1 6 -9 557.61 12.11 0 0 2 -21 3.57 2.46 0 0 6 -21 66.09 6.43 0 0 7 -21 0.15 3.90 0 0 8 -20 0.56 4.34 0 0 9 -19 -1.43 4.12 0 0 10 -18 5.30 5.12 0 0 11 -17 3.53 4.79 0 0 11 -16 1.84 4.76 0 0 11 -3 9.88 3.93 0 0 12 -14 2.06 5.80 0 0 12 -13 1.93 5.14 0 0 12 -12 4.43 4.10 0 0 12 -7 141.62 8.66 0 0 12 -6 30.82 6.10 0 1 13 0 5.78 3.80 0 1 14 -2 4.74 4.58 0 1 15 -14 -0.42 4.05 0 1 15 -6 0.77 5.12 0 1 15 -5 -2.38 5.18 0 2 12 5 14.41 2.79 0 2 13 4 13.46 3.23 0 2 15 1 1.14 3.99 0 2 16 -1 1.91 4.26 0 2 17 -5 -4.16 4.69 0 2 17 -4 -0.75 4.68 0 3 15 4 -0.47 3.03 0 3 17 1 -2.15 3.58 0 -1 5 -14 116.21 6.30 0 -1 5 -13 6.95 2.94 0 -1 6 -13 169.22 7.71 0 -1 6 -12 48.29 4.68 0 -1 7 -12 8.00 3.63 0 -1 7 -11 -1.18 3.06 0 -1 7 -10 7.31 3.10 0 -1 7 -9 145.00 6.99 0 -1 7 -8 278.02 9.26 0 -1 7 -7 246.81 8.59 0 0 3 -22 16.18 3.40 0 0 4 -22 4.75 3.19 0 0 5 -22 33.45 4.89 0 0 6 -22 12.70 4.45 0 0 8 -21 40.15 6.24 0 0 9 -20 17.10 5.37 0 0 10 -19 5.40 4.88 0 0 10 -1 14.20 3.03 0 0 11 -18 1.17 5.20 0 0 11 -2 84.97 6.22 0 0 12 -16 -3.18 5.40 0 0 12 -15 1.09 4.11 0 0 12 -5 34.78 5.07 0 0 12 -4 38.47 5.57 0 0 13 -13 3.16 5.59 0 0 13 -12 8.64 6.32 0 0 13 -11 0.90 5.87 0 0 13 -10 7.75 6.07 0 0 13 -9 10.09 5.94 0 0 13 -8 3.41 5.52 0 0 13 -7 -3.13 4.89 0 1 11 3 58.50 4.51 0 1 12 2 28.42 4.06 0 1 14 -1 10.59 4.79 0 1 15 -4 1.59 4.66 0 1 16 -13 2.15 5.82 0 1 16 -12 0.20 5.78 0 1 16 -11 3.07 5.84 0 1 16 -10 -1.92 5.45 0 1 16 -9 4.44 5.92 0 1 16 -8 -4.38 5.80 0 2 14 3 3.66 3.41 0 2 16 0 -0.26 4.03 0 2 17 -3 8.21 5.55 0 3 16 3 1.98 3.40 0 -1 4 -15 355.27 9.72 0 -1 4 -14 3.79 1.82 0 -1 5 -15 117.42 6.57 0 -1 6 -15 50.88 5.27 0 -1 6 -14 21.04 4.14 0 -1 7 -14 32.13 4.92 0 -1 7 -13 102.78 6.43 0 -1 8 -13 30.03 5.08 0 -1 8 -12 32.81 5.00 0 -1 8 -11 48.65 4.88 0 -1 8 -10 27.90 4.06 0 -1 8 -8 128.73 7.13 0 -1 8 -7 36.80 4.37 0 0 7 -22 34.46 5.57 0 0 8 -22 4.66 4.91 0 0 9 -21 2.95 5.20 0 0 10 -20 -4.10 4.41 0 0 10 0 3.68 2.63 0 0 11 -1 17.84 4.07 0 0 12 -18 1.23 5.12 0 0 12 -17 3.07 5.24 0 0 12 -3 11.70 4.40 0 0 13 -15 0.35 6.08 0 0 13 -14 1.17 4.24 0 0 13 -6 45.72 6.72 0 1 13 1 30.68 4.65 0 1 14 0 14.51 4.37 0 1 15 -3 -1.76 3.25 0 1 15 -2 -0.41 4.05 0 1 16 -7 4.89 4.44 0 1 16 -6 1.56 5.70 0 1 16 -5 8.03 5.36 0 2 15 2 2.98 3.57 0 2 17 -2 0.85 4.94 0 3 15 5 1.72 2.92 0 3 17 2 1.22 3.86 0 -1 5 -16 170.84 7.78 0 -1 6 -16 94.20 6.55 0 -1 7 -16 98.85 7.12 0 -1 7 -15 112.07 7.36 0 -1 8 -15 45.45 5.93 0 -1 8 -14 114.91 7.82 0 -1 8 -5 20.11 3.55 0 -1 9 -13 11.93 5.04 0 -1 9 -12 17.16 4.78 0 -1 9 -11 7.41 3.39 0 -1 9 -10 6.53 3.26 0 -1 9 -9 17.58 3.85 0 -1 9 -8 97.96 6.46 0 -1 9 -7 75.97 6.22 0 0 5 -23 12.77 3.68 0 0 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6 9 1.5466 0.0000 5 6 10 -2.1491 0.0000 5 6 11 1.6527 0.0000 5 6 12 -1.6945 0.0000 5 6 13 2.1058 0.0000 5 6 14 -1.0390 0.0000 5 6 15 1.6052 0.0000 5 6 16 -0.2223 0.0000 5 6 17 0.7992 0.0000 5 6 18 0.3419 0.0000 5 6 19 0.5998 0.0000 5 7 5 -0.4989 0.0000 5 7 6 -0.0783 0.0000 5 7 7 -1.3003 0.0000 5 7 8 1.4646 0.0000 5 7 9 -1.6706 0.0000 5 7 10 1.9010 0.0000 5 7 11 -1.7919 0.0000 5 7 12 2.0641 0.0000 5 7 13 -1.3062 0.0000 5 7 14 2.0230 0.0000 5 7 15 -0.4181 0.0000 5 7 16 1.1727 0.0000 5 7 17 -0.0222 0.0000 5 7 18 0.5576 0.0000 5 7 19 -0.0503 0.0000 5 8 5 -0.5491 0.0000 5 8 6 -0.2132 0.0000 5 8 7 0.8063 0.0000 5 8 8 -0.5296 0.0000 5 8 9 1.4194 0.0000 5 8 10 -0.9799 0.0000 5 8 11 1.7867 0.0000 5 8 12 -1.3048 0.0000 5 8 13 1.9624 0.0000 5 8 14 -0.7515 0.0000 5 8 15 1.6647 0.0000 5 8 16 -0.2954 0.0000 5 8 17 0.7848 0.0000 5 8 18 -0.4678 0.0000 5 9 5 0.7976 0.0000 5 9 6 -0.2679 0.0000 5 9 7 0.5321 0.0000 5 9 8 0.1183 0.0000 5 9 9 0.0637 0.0000 5 9 10 0.6158 0.0000 5 9 11 -0.6140 0.0000 5 9 12 1.2093 0.0000 5 9 13 -0.6450 0.0000 5 9 14 1.4748 0.0000 5 9 15 -0.3628 0.0000 5 9 16 1.0545 0.0000 5 9 17 -0.5034 0.0000 5 10 5 -0.9989 0.0000 5 10 6 0.6732 0.0000 5 10 7 -1.2967 0.0000 5 10 8 0.5581 0.0000 5 10 9 -1.0589 0.0000 5 10 10 -0.1834 0.0000 5 10 11 -0.3149 0.0000 5 10 12 -0.2889 0.0000 5 10 13 0.5261 0.0000 5 10 14 0.0613 0.0000 5 10 15 0.5781 0.0000 5 10 16 0.0010 0.0000 5 11 5 -0.2066 0.0000 5 11 6 -1.6354 0.0000 5 11 7 0.1195 0.0000 5 11 8 -1.9734 0.0000 5 11 9 -0.3698 0.0000 5 11 10 -1.4744 0.0000 5 11 11 -0.2810 0.0000 5 11 12 -0.5817 0.0000 5 11 13 0.3639 0.0000 5 11 14 -0.1325 0.0000 5 11 15 0.6715 0.0000 5 12 5 -0.8421 0.0000 5 12 6 -0.8164 0.0000 5 12 7 -1.6436 0.0000 5 12 8 -0.4950 0.0000 5 12 9 -1.4822 0.0000 5 12 10 -0.4130 0.0000 5 12 11 -0.8666 0.0000 5 12 12 0.1568 0.0000 5 12 13 -0.3950 0.0000 5 12 14 0.6936 0.0000 5 13 5 -1.0346 0.0000 5 13 6 -0.6621 0.0000 5 13 7 -0.6180 0.0000 5 13 8 -0.7899 0.0000 5 13 9 -0.1376 0.0000 5 13 10 -0.4826 0.0000 5 13 11 0.0927 0.0000 5 13 12 -0.3653 0.0000 5 14 5 0.3498 0.0000 5 14 6 -0.4072 0.0000 5 14 7 -0.2207 0.0000 5 14 8 0.0120 0.0000 5 14 9 -0.2271 0.0000 5 14 10 0.3757 0.0000 5 15 5 0.2764 0.0000 5 15 6 0.2590 0.0000 5 15 7 -0.0689 0.0000 5 15 8 -0.1307 0.0000 6 0 6 -1.2284 0.0000 6 0 8 -0.7359 0.0000 6 0 10 0.2583 0.0000 6 0 12 -0.4543 0.0000 6 0 14 -0.9772 0.0000 6 0 16 -1.0597 0.0000 6 1 6 0.5974 0.0000 6 1 7 -0.9184 0.0000 6 1 8 -0.3108 0.0000 6 1 9 -0.1412 0.0000 6 1 10 -0.2838 0.0000 6 1 11 0.1056 0.0000 6 1 12 0.0654 0.0000 6 1 13 -0.6926 0.0000 6 1 14 0.0158 0.0000 6 1 15 -0.8953 0.0000 6 1 16 0.2122 0.0000 6 1 17 -0.9953 0.0000 6 1 18 0.1073 0.0000 6 1 19 -0.9339 0.0000 6 2 6 -0.3542 0.0000 6 2 7 0.1884 0.0000 6 2 8 -0.3905 0.0000 6 2 9 -0.5166 0.0000 6 2 10 -0.1507 0.0000 6 2 11 0.0639 0.0000 6 2 12 -0.3322 0.0000 6 2 13 0.0882 0.0000 6 2 14 -0.6808 0.0000 6 2 15 -0.0201 0.0000 6 2 16 -0.6647 0.0000 6 2 17 0.1105 0.0000 6 2 18 -0.6012 0.0000 6 2 19 0.0185 0.0000 6 3 6 0.3361 0.0000 6 3 7 -0.2063 0.0000 6 3 8 -0.2677 0.0000 6 3 9 -0.6748 0.0000 6 3 10 -0.1374 0.0000 6 3 11 -0.7031 0.0000 6 3 12 0.3661 0.0000 6 3 13 -0.4352 0.0000 6 3 14 -0.0556 0.0000 6 3 15 -0.5583 0.0000 6 3 16 -0.1749 0.0000 6 3 17 -0.3019 0.0000 6 3 18 0.2958 0.0000 6 3 19 -0.1255 0.0000 6 4 6 -0.3219 0.0000 6 4 7 -0.3101 0.0000 6 4 8 -0.5273 0.0000 6 4 9 -0.1506 0.0000 6 4 10 -0.8302 0.0000 6 4 11 0.3029 0.0000 6 4 12 -0.4451 0.0000 6 4 13 -0.0600 0.0000 6 4 14 -0.1076 0.0000 6 4 15 -0.3476 0.0000 6 4 16 0.0616 0.0000 6 4 17 0.2675 0.0000 6 4 18 0.1666 0.0000 6 4 19 0.9227 0.0000 6 5 6 -0.3929 0.0000 6 5 7 -0.2159 0.0000 6 5 8 -0.2330 0.0000 6 5 9 -0.0759 0.0000 6 5 10 -0.1294 0.0000 6 5 11 0.1163 0.0000 6 5 12 -0.5002 0.0000 6 5 13 0.6151 0.0000 6 5 14 -0.6077 0.0000 6 5 15 0.9189 0.0000 6 5 16 -0.0820 0.0000 6 5 17 0.6009 0.0000 6 5 18 0.7469 0.0000 6 6 6 -0.5024 0.0000 6 6 7 -0.1461 0.0000 6 6 8 0.3616 0.0000 6 6 9 -0.3062 0.0000 6 6 10 0.9912 0.0000 6 6 11 -0.9067 0.0000 6 6 12 1.5879 0.0000 6 6 13 -1.1151 0.0000 6 6 14 1.6790 0.0000 6 6 15 -0.6095 0.0000 6 6 16 1.1970 0.0000 6 6 17 0.1641 0.0000 6 6 18 0.3174 0.0000 6 7 6 0.0967 0.0000 6 7 7 -0.1693 0.0000 6 7 8 -0.0390 0.0000 6 7 9 1.0974 0.0000 6 7 10 -0.7097 0.0000 6 7 11 1.8475 0.0000 6 7 12 -1.1430 0.0000 6 7 13 1.9505 0.0000 6 7 14 -0.7496 0.0000 6 7 15 1.4154 0.0000 6 7 16 -0.0898 0.0000 6 7 17 0.4495 0.0000 6 8 6 -0.5615 0.0000 6 8 7 0.3401 0.0000 6 8 8 0.1533 0.0000 6 8 9 -0.1507 0.0000 6 8 10 1.1174 0.0000 6 8 11 -0.6289 0.0000 6 8 12 1.5177 0.0000 6 8 13 -0.4295 0.0000 6 8 14 1.2102 0.0000 6 8 15 0.1203 0.0000 6 8 16 0.3509 0.0000 6 9 6 0.2137 0.0000 6 9 7 -0.3339 0.0000 6 9 8 0.2024 0.0000 6 9 9 0.0238 0.0000 6 9 10 -0.1721 0.0000 6 9 11 0.4123 0.0000 6 9 12 -0.1450 0.0000 6 9 13 0.6937 0.0000 6 9 14 0.1593 0.0000 6 9 15 0.2220 0.0000 6 10 6 -0.5250 0.0000 6 10 7 0.0821 0.0000 6 10 8 -0.6182 0.0000 6 10 9 -0.0946 0.0000 6 10 10 -0.5590 0.0000 6 10 11 -0.3320 0.0000 6 10 12 -0.0832 0.0000 6 10 13 -0.1322 0.0000 6 10 14 0.0319 0.0000 6 11 6 -0.2642 0.0000 6 11 7 -1.0459 0.0000 6 11 8 -0.5041 0.0000 6 11 9 -0.9462 0.0000 6 11 10 -0.4763 0.0000 6 11 11 -0.5410 0.0000 6 11 12 -0.5665 0.0000 6 11 13 -0.3205 0.0000 6 12 6 -1.0945 0.0000 6 12 7 -0.7077 0.0000 6 12 8 -1.1712 0.0000 6 12 9 -0.7027 0.0000 6 12 10 -0.3820 0.0000 6 12 11 -0.6250 0.0000 6 12 12 -0.2851 0.0000 6 13 6 -0.4420 0.0000 6 13 7 -0.8900 0.0000 6 13 8 -0.6853 0.0000 6 13 9 -0.3618 0.0000 6 13 10 -0.4956 0.0000 6 14 6 0.0460 0.0000 6 14 7 -0.1122 0.0000 7 0 7 -0.3798 0.0000 7 0 9 -0.1518 0.0000 7 0 11 0.0681 0.0000 7 0 13 -0.1102 0.0000 7 0 15 -0.2578 0.0000 7 1 7 0.6548 0.0000 7 1 8 -0.6399 0.0000 7 1 9 0.0245 0.0000 7 1 10 0.0235 0.0000 7 1 11 0.1739 0.0000 7 1 12 -0.0015 0.0000 7 1 13 0.2887 0.0000 7 1 14 -0.2694 0.0000 7 1 15 0.0519 0.0000 7 1 16 -0.1969 0.0000 7 1 17 -0.0033 0.0000 7 2 7 -1.0115 0.0000 7 2 8 0.3893 0.0000 7 2 9 -0.4624 0.0000 7 2 10 0.1010 0.0000 7 2 11 -0.1226 0.0000 7 2 12 0.3354 0.0000 7 2 13 -0.2848 0.0000 7 2 14 0.1344 0.0000 7 2 15 -0.3663 0.0000 7 2 16 -0.2185 0.0000 7 2 17 -0.2279 0.0000 7 3 7 0.3084 0.0000 7 3 8 -0.5686 0.0000 7 3 9 -0.0069 0.0000 7 3 10 -0.3205 0.0000 7 3 11 0.3071 0.0000 7 3 12 -0.3834 0.0000 7 3 13 0.0645 0.0000 7 3 14 -0.6555 0.0000 7 3 15 -0.4397 0.0000 7 3 16 -0.5760 0.0000 7 3 17 -0.0837 0.0000 7 4 7 -0.2055 0.0000 7 4 8 -0.2481 0.0000 7 4 9 -0.0209 0.0000 7 4 10 0.3370 0.0000 7 4 11 -0.3787 0.0000 7 4 12 -0.1620 0.0000 7 4 13 -0.7631 0.0000 7 4 14 -0.7348 0.0000 7 4 15 -0.7505 0.0000 7 4 16 -0.4038 0.0000 7 4 17 -0.3664 0.0000 7 5 7 -0.4216 0.0000 7 5 8 0.1298 0.0000 7 5 9 0.0211 0.0000 7 5 10 -0.2665 0.0000 7 5 11 -0.2068 0.0000 7 5 12 -0.4680 0.0000 7 5 13 -1.0600 0.0000 7 5 14 -0.4218 0.0000 7 5 15 -0.8532 0.0000 7 5 16 -0.2614 0.0000 7 6 7 -0.3964 0.0000 7 6 8 0.0345 0.0000 7 6 9 -0.8061 0.0000 7 6 10 -0.2718 0.0000 7 6 11 -0.2848 0.0000 7 6 12 -1.1348 0.0000 7 6 13 0.1621 0.0000 7 6 14 -1.3435 0.0000 7 6 15 0.3193 0.0000 7 6 16 -0.6524 0.0000 7 7 7 0.4676 0.0000 7 7 8 -1.3500 0.0000 7 7 9 0.0642 0.0000 7 7 10 -0.8983 0.0000 7 7 11 -0.9950 0.0000 7 7 12 0.2784 0.0000 7 7 13 -1.3199 0.0000 7 7 14 0.7766 0.0000 7 7 15 -0.9294 0.0000 7 8 7 -1.1047 0.0000 7 8 8 0.6466 0.0000 7 8 9 -1.0320 0.0000 7 8 10 -0.4914 0.0000 7 8 11 -0.0693 0.0000 7 8 12 -1.0514 0.0000 7 8 13 0.6578 0.0000 7 8 14 -0.6907 0.0000 7 9 7 0.5094 0.0000 7 9 8 -0.3519 0.0000 7 9 9 0.0358 0.0000 7 9 10 -0.1312 0.0000 7 9 11 -0.5882 0.0000 7 9 12 0.3286 0.0000 7 9 13 -0.4943 0.0000 7 10 7 -0.0038 0.0000 7 10 8 -0.2958 0.0000 7 10 9 -0.0805 0.0000 7 10 10 -0.2984 0.0000 7 10 11 0.1870 0.0000 7 10 12 -0.2736 0.0000 7 11 7 -0.9472 0.0000 7 11 8 -0.7326 0.0000 7 11 9 -0.5705 0.0000 7 11 10 -0.0856 0.0000 7 12 7 -1.0877 0.0000 7 12 8 -0.9508 0.0000 8 0 8 0.6013 0.0000 8 0 10 -0.0553 0.0000 8 0 12 0.0826 0.0000 8 1 8 -1.2685 0.0000 8 1 9 0.1436 0.0000 8 1 10 -0.4393 0.0000 8 1 11 0.0099 0.0000 8 1 12 0.0972 0.0000 8 1 13 0.0209 0.0000 8 1 14 0.2565 0.0000 8 1 15 -0.0291 0.0000 8 2 8 -0.6273 0.0000 8 2 9 -0.8484 0.0000 8 2 10 -0.0180 0.0000 8 2 11 -0.0011 0.0000 8 2 12 -0.0119 0.0000 8 2 13 0.4137 0.0000 8 2 14 -0.3124 0.0000 8 2 15 -0.0862 0.0000 8 3 8 -0.7217 0.0000 8 3 9 -0.4612 0.0000 8 3 10 0.1156 0.0000 8 3 11 0.1325 0.0000 8 3 12 0.3953 0.0000 8 3 13 -0.4635 0.0000 8 3 14 -0.1133 0.0000 8 3 15 -0.6651 0.0000 8 4 8 -0.5402 0.0000 8 4 9 0.1638 0.0000 8 4 10 0.1167 0.0000 8 4 11 0.1705 0.0000 8 4 12 -0.2446 0.0000 8 4 13 -0.3450 0.0000 8 4 14 -0.7251 0.0000 8 5 8 0.2127 0.0000 8 5 9 0.0024 0.0000 8 5 10 -0.0978 0.0000 8 5 11 -0.1177 0.0000 8 5 12 -0.6701 0.0000 8 5 13 -0.3462 0.0000 8 5 14 -0.7370 0.0000 8 6 8 0.0298 0.0000 8 6 9 0.1709 0.0000 8 6 10 -0.5080 0.0000 8 6 11 -0.6570 0.0000 8 6 12 -0.2788 0.0000 8 6 13 -0.9413 0.0000 8 7 8 1.1252 0.0000 8 7 9 -0.9867 0.0000 8 7 10 0.1123 0.0000 8 7 11 -0.8548 0.0000 8 7 12 -0.7072 0.0000 8 8 8 -1.0065 0.0000 8 8 9 0.9223 0.0000 8 8 10 -1.1479 0.0000 8 8 11 -0.1453 0.0000 8 9 8 0.3950 0.0000 8 9 9 -1.0715 0.0000 8 9 10 0.0584 0.0000 8 10 8 -0.8808 0.0000 8 10 9 -0.6795 0.0000 9 0 9 -0.0311 0.0000 9 0 11 0.1352 0.0000 9 1 9 -1.3186 0.0000 9 1 10 0.2019 0.0000 9 1 11 -0.4182 0.0000 9 1 12 0.4072 0.0000 9 2 9 0.2867 0.0000 9 2 10 -1.0016 0.0000 9 2 11 0.6535 0.0000 9 2 12 -0.0362 0.0000 9 3 9 -0.6952 0.0000 9 3 10 0.5692 0.0000 9 3 11 -0.0028 0.0000 9 3 12 0.4928 0.0000 9 4 9 0.1786 0.0000 9 4 10 0.4524 0.0000 9 4 11 0.2466 0.0000 9 5 9 1.1968 0.0000 9 5 10 -0.0495 0.0000 9 5 11 0.1946 0.0000 9 6 9 0.0364 0.0000 9 6 10 0.2611 0.0000 9 7 9 0.1197 0.0000 0 0 0 0.0 0.0 ; _shelx_fab_checksum 37695 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ca1 Ca 0.37175(8) 0.53079(5) 0.89783(3) 0.0627(2) Uani 1 1 d . . . . . I1 I 0.68454(3) 0.48484(2) 0.96210(2) 0.08971(15) Uani 1 1 d . . . . . C5 C 0.1291(4) 0.6249(3) 0.77014(17) 0.0792(11) Uani 1 1 d . . . . . C6 C 0.2411(4) 0.6546(2) 0.82112(17) 0.0757(10) Uani 1 1 d . . . . . C7 C 0.2192(5) 0.6829(3) 0.88094(19) 0.0872(12) Uani 1 1 d . . . . . C9 C 0.4554(6) 0.7006(3) 0.8765(3) 0.1141(19) Uani 1 1 d . . . . . Si1 Si -0.10004(14) 0.56001(10) 0.66258(5) 0.0965(4) Uani 1 1 d . . . . . O1 O 0.1773(3) 0.42875(17) 0.88542(12) 0.0784(7) Uani 1 1 d . . . . . O2 O 0.4052(3) 0.43389(19) 0.81345(11) 0.0855(8) Uani 1 1 d . . . . . C10 C 0.3867(5) 0.6655(3) 0.8179(2) 0.0949(14) Uani 1 1 d . . . . . C19 C 0.0263(4) 0.4451(3) 0.8763(2) 0.0949(13) Uani 1 1 d . . . . . H19A H -0.006004 0.480386 0.838781 0.114 Uiso 1 1 calc R . . . . H19B H 0.003483 0.476841 0.911937 0.114 Uiso 1 1 calc R . . . . C21 C 0.0620(7) 0.3008(4) 0.9123(3) 0.136(2) Uani 1 1 d . . . . . H21A H 0.054354 0.239040 0.898856 0.163 Uiso 1 1 calc R . . . . H21B H 0.046304 0.304300 0.954979 0.163 Uiso 1 1 calc R . . . . C4 C 0.0373(5) 0.6020(3) 0.72674(18) 0.0891(12) Uani 1 1 d . . . . . C8 C 0.3538(7) 0.7112(3) 0.9129(2) 0.1071(17) Uani 1 1 d . . . . . C20 C -0.0431(5) 0.3569(4) 0.8699(3) 0.1181(17) Uani 1 1 d . . . . . H20A H -0.057543 0.335562 0.826977 0.142 Uiso 1 1 calc R . . . . H20B H -0.135036 0.358355 0.883043 0.142 Uiso 1 1 calc R . . . . C18 C 0.2916(6) 0.4090(4) 0.7621(2) 0.126(2) Uani 1 1 d . . . . . H18A H 0.242266 0.356305 0.772968 0.151 Uiso 1 1 calc R . . . . H18B H 0.222054 0.456979 0.752536 0.151 Uiso 1 1 calc R . . . . C22 C 0.2043(5) 0.3380(3) 0.9081(3) 0.1128(16) Uani 1 1 d . . . . . H22A H 0.268225 0.337597 0.948909 0.135 Uiso 1 1 calc R . . . . H22B H 0.248084 0.303301 0.879164 0.135 Uiso 1 1 calc R . . . . C11 C 0.0789(7) 0.6879(3) 0.9010(2) 0.1183(19) Uani 1 1 d . . . . . H11A H 0.005166 0.662622 0.869019 0.177 Uiso 1 1 calc GR . . . . H11B H 0.056186 0.749165 0.907541 0.177 Uiso 1 1 calc GR . . . . H11C H 0.084413 0.655278 0.939350 0.177 Uiso 1 1 calc GR . . . . C15 C 0.5303(6) 0.3930(4) 0.8017(2) 0.1174(17) Uani 1 1 d . . . . . H15A H 0.560492 0.345644 0.831819 0.141 Uiso 1 1 calc R . . . . H15B H 0.607672 0.436337 0.805594 0.141 Uiso 1 1 calc R . . . . C17 C 0.3554(8) 0.3911(4) 0.7092(2) 0.145(2) Uani 1 1 d . . . . . H17A H 0.362997 0.445081 0.685566 0.174 Uiso 1 1 calc R . . . . H17B H 0.299740 0.347302 0.681713 0.174 Uiso 1 1 calc R . . . . C16 C 0.4983(7) 0.3561(5) 0.7374(3) 0.157(3) Uani 1 1 d . . . . . H16A H 0.569573 0.375587 0.713845 0.189 Uiso 1 1 calc R . . . . H16B H 0.497372 0.291472 0.738399 0.189 Uiso 1 1 calc R . . . . C14 C 0.4519(6) 0.6490(4) 0.7604(3) 0.1254(19) Uani 1 1 d . . . . . H14A H 0.523661 0.603122 0.769501 0.188 Uiso 1 1 calc GR . . . . H14B H 0.495568 0.703000 0.749413 0.188 Uiso 1 1 calc GR . . . . H14C H 0.377696 0.630632 0.725958 0.188 Uiso 1 1 calc GR . . . . C12 C 0.3797(8) 0.7541(4) 0.9791(2) 0.164(3) Uani 1 1 d . . . . . H12A H 0.303956 0.736723 1.000048 0.246 Uiso 1 1 calc GR . . . . H12B H 0.380538 0.817901 0.975143 0.246 Uiso 1 1 calc GR . . . . H12C H 0.470586 0.734356 1.002987 0.246 Uiso 1 1 calc GR . . . . C13 C 0.6136(7) 0.7275(4) 0.8927(3) 0.178(3) Uani 1 1 d . . . . . H13A H 0.666699 0.684048 0.920453 0.266 Uiso 1 1 calc GR . . . . H13B H 0.622283 0.784783 0.912857 0.266 Uiso 1 1 calc GR . . . . H13C H 0.651485 0.730730 0.854955 0.266 Uiso 1 1 calc GR . . . . C1 C -0.2422(7) 0.6409(5) 0.6388(3) 0.193(4) Uani 1 1 d . . . . . H1A H -0.276333 0.661392 0.675035 0.289 Uiso 1 1 calc GR . . . . H1B H -0.320063 0.613642 0.609885 0.289 Uiso 1 1 calc GR . . . . H1C H -0.205626 0.690514 0.618864 0.289 Uiso 1 1 calc GR . . . . C3 C -0.0138(9) 0.5327(6) 0.5959(3) 0.177(3) Uani 1 1 d . . . . . H3A H 0.037520 0.583934 0.585408 0.266 Uiso 1 1 calc GR . . . . H3B H -0.086340 0.515993 0.560297 0.266 Uiso 1 1 calc GR . . . . H3C H 0.052142 0.484112 0.607213 0.266 Uiso 1 1 calc GR . . . . C2 C -0.1732(10) 0.4583(6) 0.6865(4) 0.215(5) Uani 1 1 d . . . . . H2A H -0.111398 0.409380 0.681145 0.323 Uiso 1 1 calc GR . . . . H2B H -0.267312 0.448485 0.661394 0.323 Uiso 1 1 calc GR . . . . H2C H -0.179993 0.462597 0.729900 0.323 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ca1 0.0625(4) 0.0664(4) 0.0532(4) 0.0054(3) -0.0032(3) 0.0036(4) I1 0.06375(18) 0.1450(3) 0.05795(17) 0.00692(14) 0.00620(12) 0.01947(16) C5 0.087(3) 0.082(3) 0.062(2) 0.0126(19) -0.003(2) 0.015(2) C6 0.084(3) 0.067(2) 0.068(2) 0.0134(18) -0.005(2) 0.004(2) C7 0.111(3) 0.066(2) 0.073(2) -0.001(2) -0.009(2) 0.023(3) C9 0.116(4) 0.073(3) 0.127(4) 0.033(3) -0.039(3) -0.024(3) Si1 0.0875(8) 0.1218(10) 0.0687(7) -0.0022(7) -0.0119(6) 0.0173(8) O1 0.0658(15) 0.0810(18) 0.0832(16) 0.0044(14) 0.0027(12) -0.0064(14) O2 0.0819(18) 0.1007(19) 0.0695(15) -0.0104(14) 0.0048(13) 0.0167(17) C10 0.093(3) 0.087(3) 0.095(3) 0.035(2) -0.007(3) -0.009(3) C19 0.065(2) 0.104(3) 0.115(3) -0.015(3) 0.016(2) 0.000(3) C21 0.142(5) 0.118(4) 0.152(5) 0.011(4) 0.038(4) -0.041(4) C4 0.088(3) 0.109(3) 0.064(2) 0.010(2) -0.001(2) 0.017(3) C8 0.147(5) 0.068(3) 0.083(3) 0.003(2) -0.032(3) 0.001(3) C20 0.078(3) 0.110(4) 0.164(5) -0.035(4) 0.020(3) -0.016(3) C18 0.112(4) 0.171(5) 0.077(3) -0.032(3) -0.021(3) 0.047(4) C22 0.092(3) 0.091(3) 0.140(4) 0.014(3) -0.013(3) -0.008(3) C11 0.166(5) 0.101(3) 0.081(3) -0.005(3) 0.010(3) 0.058(4) C15 0.098(3) 0.138(4) 0.118(4) -0.033(3) 0.025(3) 0.020(3) C17 0.229(8) 0.113(4) 0.094(4) -0.041(3) 0.034(5) -0.016(5) C16 0.115(4) 0.189(7) 0.176(6) -0.107(6) 0.048(4) -0.037(5) C14 0.110(4) 0.134(4) 0.136(4) 0.059(4) 0.033(3) -0.001(3) C12 0.240(8) 0.091(3) 0.119(4) -0.030(3) -0.065(4) 0.022(4) C13 0.140(5) 0.125(5) 0.229(7) 0.074(5) -0.057(5) -0.062(4) C1 0.148(6) 0.206(8) 0.180(6) -0.053(6) -0.074(5) 0.082(6) C3 0.175(7) 0.261(9) 0.090(4) -0.025(5) 0.012(4) 0.045(7) C2 0.231(10) 0.221(9) 0.156(7) 0.025(6) -0.054(6) -0.099(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 I1 Ca1 I1 83.109(16) . 3_667 C6 Ca1 I1 120.49(9) . 3_667 C6 Ca1 I1 136.91(10) . . C6 Ca1 C7 30.99(12) . . C6 Ca1 C9 49.57(13) . . C6 Ca1 C10 30.58(13) . . C6 Ca1 C8 49.14(12) . . C7 Ca1 I1 90.29(10) . 3_667 C7 Ca1 I1 133.81(10) . . C7 Ca1 C9 49.64(18) . . C7 Ca1 C10 50.92(16) . . C7 Ca1 C8 29.74(15) . . C9 Ca1 I1 90.00(11) . . C9 Ca1 I1 109.78(15) . 3_667 C9 Ca1 C8 29.06(16) . . O1 Ca1 I1 77.76(7) . 3_667 O1 Ca1 I1 124.15(7) . . O1 Ca1 C6 97.27(11) . . O1 Ca1 C7 98.48(13) . . O1 Ca1 C9 145.85(13) . . O1 Ca1 O2 75.01(10) . . O1 Ca1 C10 123.50(11) . . O1 Ca1 C8 125.96(17) . . O2 Ca1 I1 138.75(7) . 3_667 O2 Ca1 I1 87.15(7) . . O2 Ca1 C6 93.39(11) . . O2 Ca1 C7 123.81(11) . . O2 Ca1 C9 110.20(18) . . O2 Ca1 C10 85.90(13) . . O2 Ca1 C8 135.08(14) . . C10 Ca1 I1 106.89(10) . . C10 Ca1 I1 135.26(12) . 3_667 C10 Ca1 C9 30.18(14) . . C10 Ca1 C8 49.18(16) . . C8 Ca1 I1 104.07(13) . . C8 Ca1 I1 86.13(13) . 3_667 Ca1 I1 Ca1 96.891(17) . 3_667 C4 C5 C6 178.1(5) . . C5 C6 Ca1 116.7(2) . . C7 C6 Ca1 76.5(2) . . C7 C6 C5 125.1(4) . . C10 C6 Ca1 76.8(2) . . C10 C6 C5 125.2(4) . . C10 C6 C7 109.6(4) . . C6 C7 Ca1 72.5(2) . . C6 C7 C11 126.0(4) . . C8 C7 Ca1 77.0(3) . . C8 C7 C6 105.1(5) . . C8 C7 C11 128.7(5) . . C11 C7 Ca1 119.5(3) . . C10 C9 Ca1 73.1(2) . . C10 C9 C13 124.3(7) . . C8 C9 Ca1 75.5(3) . . C8 C9 C10 108.3(5) . . C8 C9 C13 127.3(6) . . C13 C9 Ca1 120.8(3) . . C4 Si1 C3 108.6(3) . . C1 Si1 C4 111.4(3) . . C1 Si1 C3 110.1(4) . . C2 Si1 C4 109.3(3) . . C2 Si1 C1 110.1(4) . . C2 Si1 C3 107.3(5) . . C19 O1 Ca1 129.9(3) . . C19 O1 C22 108.2(3) . . C22 O1 Ca1 119.1(2) . . C18 O2 Ca1 123.8(3) . . C15 O2 Ca1 130.3(3) . . C15 O2 C18 105.9(3) . . C6 C10 Ca1 72.6(2) . . C6 C10 C9 106.2(5) . . C6 C10 C14 125.9(4) . . C9 C10 Ca1 76.7(2) . . C9 C10 C14 127.8(5) . . C14 C10 Ca1 119.5(3) . . O1 C19 C20 106.0(4) . . C20 C21 C22 104.9(4) . . C5 C4 Si1 176.3(4) . . C7 C8 Ca1 73.2(2) . . C7 C8 C12 123.3(6) . . C9 C8 Ca1 75.5(3) . . C9 C8 C7 110.8(4) . . C9 C8 C12 125.8(6) . . C12 C8 Ca1 121.3(3) . . C19 C20 C21 102.7(4) . . C17 C18 O2 107.6(5) . . O1 C22 C21 105.8(4) . . O2 C15 C16 108.3(4) . . C18 C17 C16 103.6(5) . . C17 C16 C15 105.1(5) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Ca1 I1 3.2039(7) 3_667 Ca1 I1 3.0920(7) . Ca1 C6 2.634(3) . Ca1 C7 2.686(4) . Ca1 C9 2.733(5) . Ca1 O1 2.369(3) . Ca1 O2 2.410(3) . Ca1 C10 2.687(4) . Ca1 C8 2.734(5) . C5 C6 1.444(5) . C5 C4 1.199(5) . C6 C7 1.422(6) . C6 C10 1.404(6) . C7 C8 1.392(7) . C7 C11 1.481(7) . C9 C10 1.412(6) . C9 C8 1.372(8) . C9 C13 1.524(7) . Si1 C4 1.820(4) . Si1 C1 1.809(6) . Si1 C3 1.847(7) . Si1 C2 1.795(8) . O1 C19 1.425(5) . O1 C22 1.453(5) . O2 C18 1.438(5) . O2 C15 1.403(5) . C10 C14 1.521(7) . C19 C20 1.471(7) . C21 C20 1.477(8) . C21 C22 1.479(7) . C8 C12 1.551(6) . C18 C17 1.427(7) . C15 C16 1.477(7) . C17 C16 1.467(8) .