Crystallography Open Database

Information card for entry 1556518

Preview

Coordinates	1556518.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H86 N6 Na2 Si4
Calculated formula	C32 H86 N6 Na2 Si4
SMILES	C([Si](C)(C)C)([Si](C)(C)C)[Na]1([N](C)(C)CC[N]1(C)C)[N](C)(C)CC[N](C)(C)[Na]1(C([Si](C)(C)C)[Si](C)(C)C)[N](C)(C)CC[N]1(C)C
Title of publication	[Bis(Trimethylsilyl)Methyl]Lithium and -Sodium: Solubility in Alkanes and Complexes with O- and N- Donor Ligands
Authors of publication	Von Pilgrim, M.; Mondeshki, M.; Klett, J.
Journal of publication	Inorganics
Year of publication	2017
Journal volume	5
Pages of publication	39
a	10.45 ± 0.004 Å
b	17.414 ± 0.006 Å
c	14.258 ± 0.005 Å
α	90°
β	100.824 ± 0.009°
γ	90°
Cell volume	2548.5 ± 1.6 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0932
Residual factor for significantly intense reflections	0.0441
Weighted residual factors for significantly intense reflections	0.103
Weighted residual factors for all reflections included in the refinement	0.1193
Goodness-of-fit parameter for all reflections included in the refinement	0.916
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
282761 (current)	2023-04-20	cif/1 Fixing some Z values and formulae	1556518.cif
244999	2019-12-11	cif/ Adding structures of 1556518 via cif-deposit CGI script.	1556518.cif