#------------------------------------------------------------------------------ #$Date: 2019-12-12 12:51:23 +0200 (Thu, 12 Dec 2019) $ #$Revision: 245021 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/65/1556533.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556533 loop_ _publ_author_name 'Craze, A.R.' 'Sciortino, N.F.' 'Badbhade, M.M.' 'Kepert, C.J.' 'Marjo, C.E.' 'Li, F.' _publ_section_title ; Investigation of the Spin Crossover Properties of Three Dinulear Fe(II) Triple Helicates by Variation of the Steric Nature of the Ligand Type ; _journal_name_full Inorganics _journal_page_first 62 _journal_paper_doi 10.3390/inorganics5040062 _journal_volume 5 _journal_year 2017 _chemical_formula_moiety 'C60 H48 Fe2 N18 S3, 3(B F4), B F3.5, 2(C2 H3 N)' _chemical_formula_sum 'C64 H54 B4 F15.5 Fe2 N20 S3' _chemical_formula_weight 1648.89 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _cell_angle_alpha 95.29(3) _cell_angle_beta 100.29(3) _cell_angle_gamma 92.93(3) _cell_formula_units_Z 2 _cell_length_a 9.5210(19) _cell_length_b 16.723(3) _cell_length_c 23.621(5) _cell_measurement_reflns_used 2499 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 20.00 _cell_measurement_theta_min 2.27 _cell_volume 3675.9(13) _computing_cell_refinement 'ShelXL least squares' _computing_data_collection XDS _computing_data_reduction XDS _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.909 _diffrn_measured_fraction_theta_max 0.900 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0971 _diffrn_reflns_av_unetI/netI 0.0898 _diffrn_reflns_Laue_measured_fraction_full 0.909 _diffrn_reflns_Laue_measured_fraction_max 0.900 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 45853 _diffrn_reflns_point_group_measured_fraction_full 0.909 _diffrn_reflns_point_group_measured_fraction_max 0.900 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.371 _diffrn_reflns_theta_min 0.881 _exptl_absorpt_coefficient_mu 0.575 _exptl_absorpt_correction_type none _exptl_crystal_colour 'light orange' _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary orange _exptl_crystal_density_diffrn 1.490 _exptl_crystal_description prism _exptl_crystal_F_000 1675 _exptl_crystal_preparation 'Diethyl ether diffusion into acetonitrile' _exptl_crystal_size_max 0.015 _exptl_crystal_size_mid 0.0075 _exptl_crystal_size_min 0.0075 _refine_diff_density_max 1.472 _refine_diff_density_min -1.550 _refine_diff_density_rms 0.153 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.138 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1047 _refine_ls_number_reflns 13521 _refine_ls_number_restraints 193 _refine_ls_restrained_S_all 1.179 _refine_ls_R_factor_all 0.1389 _refine_ls_R_factor_gt 0.1086 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2905 _refine_ls_wR_factor_ref 0.3308 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 8552 _reflns_number_total 13521 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; p-1_a.res created by SHELXL-2014/7 TITL p-1_a.res in P-1 REM Old TITL p-1 in P-1 REM SHELXT solution in P-1 REM R1 0.219, Rweak 0.014, Alpha 0.068, Orientation as input REM Formula found by SHELXT: C82 B4 N10 O5 F4 S3 Fe2 CELL 0.71073 9.521 16.723 23.621 95.295 100.294 92.934 ZERR 2 0.0019 0.0033 0.0047 0.03 0.03 0.03 LATT 1 SFAC C H B F Fe N S UNIT 128 108 8 31 4 40 6 EQIV $1 +X,+Y,1+Z EQIV $2 1-X,1-Y,1-Z EQIV $3 1+X,+Y,1+Z EQIV $4 -1+X,+Y,-1+Z DFIX 2.25 F007 F006 DFIX 2.25 F7AA F2AA DFIX 2.25 F7AA F1AA DFIX 1.4 F7AA B2 F2AA B2 F1AA B2 DFIX 1.4 B2 F1AA B2 F2AA B2 F7AA B2 F0BA B2 F1AB B2 F5AA DFIX 1.39 B2A F2AA B2A F7AA B2A F1AB B2A F5AA DFIX 1.39 B2 F1AA B2 F2AA B2 F0BA SADI 0.04 F8 F10 F8 F11 F8 F15 F10 F11 F10 F15 F11 F15 SADI B9 F8 B9 F10 B9 F11 B9 F15 SADI F15 B9 F0AA B9 F11 B9 F1 B9 F2 B9 F10 B9 F4 B9 F8 B9 SADI B9 F4 B9 F10 B9 F11 B9 F15 B9 F8 B9 F0AA B9 F2 B9 F1 DANG 2.25 F2AA F1AA DANG 2.25 F2AA F7AA DANG 2.25 F1AA F0BA DANG 2.25 F7AA F0BA DANG 2.25 F2AA F0BA RIGU N02E C02M C02X RIGU C030 RIGU C030 C02V RIGU F3AA > F8AA RIGU F1 > B9 F8 > F15 RIGU F1AA F2AA F7AA F0BA B2 RIGU F1AA > B2A RIGU F1 > B9 F8 > B9A RIGU F8 > B9A RIGU F1 > B9 ISOR C030 EADP B9 B9A EXYZ B9 B9A L.S. 8 PLAN 20 HTAB N2B F0AA_$1 HTAB N2B F15_$1 HTAB N2C N01B_$2 HTAB N2A F2_$3 HTAB N2A F10_$3 HTAB N5A F4AA_$4 HTAB N5A F3AA_$4 BOND $H LIST 6 fmap 2 ACTA SHEL 55 0.8 OMIT 0 3 0 REM REM REM WGHT 0.200000 FVAR 0.34909 FE01 5 0.701345 0.734915 0.757619 11.00000 0.04034 0.04715 = 0.05135 0.01395 0.01718 0.00222 FE02 5 0.377181 0.774024 0.256118 11.00000 0.04086 0.05332 = 0.04827 0.00268 0.01920 0.00220 S1A 7 0.779040 0.526828 0.468822 11.00000 0.07756 0.05787 = 0.07739 -0.00338 0.02288 0.02177 S1B 7 0.850149 0.991994 0.534751 11.00000 0.05470 0.04952 = 0.04945 0.00963 0.02072 -0.00862 S1C 7 0.048261 0.765757 0.529755 11.00000 0.03655 0.08497 = 0.05036 0.01991 0.01948 0.00612 N1A 6 0.878949 0.777299 0.809420 11.00000 0.05377 0.05238 = 0.05248 0.01101 0.01170 0.00022 N2A 6 1.068228 0.808478 0.878355 11.00000 0.07100 0.07754 = 0.06595 0.02620 -0.01342 -0.01337 AFIX 43 H2A 2 1.118822 0.827231 0.911240 11.00000 -1.20000 AFIX 0 N3A 6 0.843410 0.702423 0.705666 11.00000 0.03587 0.04323 = 0.06646 0.01270 0.01694 0.00129 N4A 6 0.345815 0.660389 0.293136 11.00000 0.04805 0.05016 = 0.06454 -0.00260 0.02297 -0.00015 N5A 6 -0.014228 0.668769 0.142928 11.00000 0.07167 0.08001 = 0.08344 -0.00746 -0.00426 0.00396 AFIX 43 H5A 2 -0.084990 0.663148 0.114276 11.00000 -1.20000 AFIX 0 N6A 6 0.181928 0.718982 0.201721 11.00000 0.04353 0.06312 = 0.05843 -0.00121 0.00960 0.00664 N1B 6 0.589116 0.771473 0.815995 11.00000 0.04528 0.05701 = 0.04669 0.01650 0.01284 -0.00260 N2B 6 0.491694 0.807116 0.890810 11.00000 0.05802 0.07525 = 0.04157 0.01574 0.01959 0.00591 AFIX 43 H2B 2 0.460688 0.804590 0.922678 11.00000 -1.20000 AFIX 0 N3B 6 0.651837 0.843686 0.731531 11.00000 0.03827 0.05225 = 0.04531 0.01170 0.01524 -0.00124 N4B 6 0.597634 0.818577 0.301930 11.00000 0.04482 0.04745 = 0.04968 0.00262 0.02102 0.00176 N5B 6 0.601282 0.739611 0.113874 11.00000 0.06949 0.07895 = 0.04737 0.00034 0.02477 0.01242 AFIX 43 H5B 2 0.611859 0.729773 0.078555 11.00000 -1.20000 AFIX 0 N6B 6 0.503759 0.739995 0.192613 11.00000 0.05324 0.06261 = 0.05131 -0.00035 0.02416 0.00340 N1C 6 0.722312 0.629776 0.790575 11.00000 0.04364 0.05042 = 0.05451 0.01228 0.01150 0.00247 N2C 6 0.737435 0.526423 0.841237 11.00000 0.06131 0.05320 = 0.05803 0.02028 0.01408 0.01692 AFIX 43 H2C 2 0.768708 0.496405 0.867752 11.00000 -1.20000 AFIX 0 N3C 6 0.526343 0.671745 0.708150 11.00000 0.03553 0.04693 = 0.05014 0.01266 0.01919 0.00545 N4C 6 0.242700 0.837473 0.310999 11.00000 0.03491 0.05368 = 0.04290 0.00673 0.01268 0.00455 N5C 6 0.246185 0.963962 0.152052 11.00000 0.05626 0.06860 = 0.03895 0.01151 0.01689 0.00526 AFIX 43 H5C 2 0.236383 0.989908 0.121960 11.00000 -1.20000 AFIX 0 N6C 6 0.331283 0.881378 0.215544 11.00000 0.04113 0.06354 = 0.04076 0.00751 0.01285 0.00579 C1A 1 0.923018 0.810921 0.862108 11.00000 0.05807 0.06008 = 0.06133 0.01876 0.00955 -0.00233 AFIX 43 H1A 2 0.863707 0.833582 0.885579 11.00000 -1.20000 AFIX 0 C2A 1 1.117625 0.771038 0.833047 11.00000 0.05174 0.08028 = 0.07631 0.02185 0.00769 0.00171 AFIX 43 H2AA 2 1.212320 0.761401 0.831599 11.00000 -1.20000 AFIX 0 C3A 1 1.001377 0.750166 0.789873 11.00000 0.04710 0.05657 = 0.06532 0.01760 0.01179 -0.00578 C4A 1 0.975150 0.711633 0.733497 11.00000 0.05567 0.05442 = 0.06507 0.01962 0.02538 0.00560 AFIX 43 H4A 2 1.049685 0.693120 0.716379 11.00000 -1.20000 AFIX 0 C5A 1 0.817847 0.660931 0.648926 11.00000 0.04689 0.04696 = 0.06667 0.00789 0.03247 -0.00218 C6A 1 0.878952 0.586900 0.639986 11.00000 0.06055 0.04838 = 0.07524 0.01764 0.03279 0.00946 AFIX 43 H6A 2 0.931318 0.564425 0.670966 11.00000 -1.20000 AFIX 0 C7A 1 0.860285 0.548275 0.584953 11.00000 0.06371 0.04732 = 0.08086 0.00471 0.03714 0.00892 AFIX 43 H7A 2 0.899110 0.498878 0.579384 11.00000 -1.20000 AFIX 0 C8A 1 0.784374 0.581025 0.536789 11.00000 0.05627 0.04382 = 0.06823 0.00986 0.02930 0.00536 C9A 1 0.724570 0.653802 0.547425 11.00000 0.06472 0.04143 = 0.06685 0.00720 0.02937 0.00183 AFIX 43 H9A 2 0.672848 0.677208 0.516762 11.00000 -1.20000 AFIX 0 C10A 1 0.740909 0.691812 0.602887 11.00000 0.04787 0.04122 = 0.06464 0.00906 0.02444 0.00390 AFIX 43 H10A 2 0.698058 0.739850 0.608857 11.00000 -1.20000 AFIX 0 C11A 1 0.647131 0.569650 0.420549 11.00000 0.05957 0.03994 = 0.07289 -0.00290 0.02620 0.00322 C12A 1 0.505523 0.577242 0.429507 11.00000 0.07882 0.04960 = 0.07308 0.00201 0.03714 -0.00523 AFIX 43 H12A 2 0.479241 0.561711 0.463169 11.00000 -1.20000 AFIX 0 C13A 1 0.404965 0.607880 0.388181 11.00000 0.04575 0.04689 = 0.07996 0.00752 0.02929 0.00151 AFIX 43 H13A 2 0.312766 0.614183 0.395028 11.00000 -1.20000 AFIX 0 C14A 1 0.441513 0.629417 0.336114 11.00000 0.05824 0.04224 = 0.07502 -0.00180 0.03046 -0.00520 C15A 1 0.583491 0.620660 0.327834 11.00000 0.04816 0.05135 = 0.06743 0.00036 0.02213 -0.00741 AFIX 43 H15A 2 0.609677 0.634289 0.293681 11.00000 -1.20000 AFIX 0 C16A 1 0.681585 0.592970 0.368424 11.00000 0.05353 0.04569 = 0.07530 -0.01076 0.02514 -0.00488 AFIX 43 H16A 2 0.774647 0.589083 0.361969 11.00000 -1.20000 AFIX 0 C17A 1 0.220351 0.622474 0.271660 11.00000 0.06393 0.04365 = 0.09508 -0.00627 0.03739 -0.00785 AFIX 43 H17A 2 0.188896 0.577676 0.287719 11.00000 -1.20000 AFIX 0 C18A 1 0.131987 0.652211 0.222241 11.00000 0.04372 0.06270 = 0.07360 -0.00580 0.00980 0.00600 C19A 1 0.006381 0.621389 0.183253 11.00000 0.06053 0.06130 = 0.08589 -0.01139 0.00839 -0.01481 AFIX 43 H19A 2 -0.050560 0.575620 0.186152 11.00000 -1.20000 AFIX 0 C20A 1 0.092124 0.729224 0.152060 11.00000 0.04807 0.08363 = 0.06457 -0.01115 0.00758 0.00235 AFIX 43 H20A 2 0.101075 0.769977 0.128418 11.00000 -1.20000 AFIX 0 C1B 1 0.557520 0.749615 0.865752 11.00000 0.05281 0.06603 = 0.04605 0.01672 0.01811 0.00904 AFIX 43 H1B 2 0.578749 0.701100 0.880536 11.00000 -1.20000 AFIX 0 C3B 1 0.480288 0.871499 0.858272 11.00000 0.04688 0.06608 = 0.05148 0.00954 0.01371 0.01105 AFIX 43 H3B 2 0.439562 0.919702 0.866153 11.00000 -1.20000 AFIX 0 C4B 1 0.542522 0.848729 0.811482 11.00000 0.03990 0.06186 = 0.04552 0.01626 0.01706 0.00480 C5B 1 0.575724 0.884662 0.761924 11.00000 0.03853 0.05437 = 0.04753 0.00987 0.01542 0.00162 AFIX 43 H5BA 2 0.544175 0.934307 0.752488 11.00000 -1.20000 AFIX 0 C6B 1 0.693906 0.878245 0.682977 11.00000 0.04227 0.04234 = 0.03989 0.00795 0.01678 0.00052 C7B 1 0.593676 0.901108 0.638309 11.00000 0.03739 0.05553 = 0.05654 0.01833 0.01780 0.00178 AFIX 43 H7B 2 0.496613 0.894409 0.639317 11.00000 -1.20000 AFIX 0 C8B 1 0.638708 0.934387 0.591533 11.00000 0.04399 0.05275 = 0.05405 0.01494 0.01499 0.00294 AFIX 43 H8B 2 0.571415 0.950033 0.561716 11.00000 -1.20000 AFIX 0 C9B 1 0.782850 0.943926 0.589735 11.00000 0.04483 0.04376 = 0.04843 0.00636 0.02266 0.00163 C10B 1 0.883986 0.921389 0.634657 11.00000 0.04895 0.04523 = 0.05098 0.00707 0.01947 -0.00708 AFIX 43 H10B 2 0.980943 0.927964 0.633425 11.00000 -1.20000 AFIX 0 C11B 1 0.839553 0.888663 0.681924 11.00000 0.03978 0.04584 = 0.04472 0.01142 0.01215 -0.00205 AFIX 43 H11B 2 0.906840 0.874122 0.712187 11.00000 -1.20000 AFIX 0 C12B 1 0.761586 0.939501 0.469038 11.00000 0.04452 0.05126 = 0.04873 0.01333 0.02203 0.00492 C13B 1 0.710195 0.857476 0.460933 11.00000 0.05205 0.04819 = 0.04355 0.00893 0.01966 -0.00070 AFIX 43 H13B 2 0.714835 0.828726 0.493017 11.00000 -1.20000 AFIX 0 C14B 1 0.654116 0.819409 0.407483 11.00000 0.05344 0.04397 = 0.04966 0.00652 0.02099 -0.00532 AFIX 43 H14B 2 0.618442 0.766011 0.403983 11.00000 -1.20000 AFIX 0 C15B 1 0.649489 0.859690 0.357690 11.00000 0.03725 0.04941 = 0.05180 0.00415 0.02099 0.00491 C16B 1 0.696779 0.941600 0.364406 11.00000 0.04636 0.05206 = 0.04525 0.01109 0.01559 -0.00075 AFIX 43 H16B 2 0.691709 0.970015 0.332144 11.00000 -1.20000 AFIX 0 C17B 1 0.751377 0.980372 0.419472 11.00000 0.05042 0.04596 = 0.04958 0.01239 0.01797 -0.00469 AFIX 43 H17B 2 0.781704 1.034677 0.423318 11.00000 -1.20000 AFIX 0 C18B 1 0.681928 0.820273 0.263722 11.00000 0.04753 0.04792 = 0.04874 0.00742 0.01869 0.00547 AFIX 43 H18B 2 0.772669 0.846496 0.274271 11.00000 -1.20000 AFIX 0 C19B 1 0.636906 0.782875 0.206828 11.00000 0.05212 0.04737 = 0.04598 0.00576 0.02010 0.00581 C20B 1 0.697191 0.782422 0.157565 11.00000 0.05128 0.07515 = 0.05153 0.00980 0.02403 0.01222 AFIX 43 H20B 2 0.785570 0.806515 0.154761 11.00000 -1.20000 AFIX 0 C21B 1 0.486465 0.715475 0.136323 11.00000 0.06864 0.07096 = 0.05428 -0.00511 0.02830 0.00257 AFIX 43 H21B 2 0.405944 0.685624 0.115141 11.00000 -1.20000 AFIX 0 C1C 1 0.798831 0.599529 0.833686 11.00000 0.05114 0.05768 = 0.06580 0.01788 0.01131 0.00166 AFIX 43 H1C 2 0.882990 0.624009 0.856109 11.00000 -1.20000 AFIX 0 C2C 1 0.618302 0.509402 0.799535 11.00000 0.05416 0.04876 = 0.05571 0.01488 0.01395 0.00247 AFIX 43 H2CA 2 0.556850 0.463171 0.794028 11.00000 -1.20000 AFIX 0 C3C 1 0.606453 0.573464 0.767290 11.00000 0.05014 0.04305 = 0.04992 0.00645 0.02412 0.00100 C4C 1 0.504757 0.598387 0.721228 11.00000 0.04487 0.04637 = 0.04977 0.01009 0.02041 0.00010 AFIX 43 H4C 2 0.427586 0.564337 0.701664 11.00000 -1.20000 AFIX 0 C5C 1 0.417729 0.696649 0.663699 11.00000 0.03423 0.04151 = 0.04232 0.00537 0.01440 -0.00557 C6C 1 0.396770 0.659882 0.607490 11.00000 0.05459 0.04493 = 0.03949 0.00606 0.01935 0.00250 AFIX 43 H6C 2 0.456691 0.620562 0.598007 11.00000 -1.20000 AFIX 0 C7C 1 0.287254 0.680843 0.564845 11.00000 0.05377 0.05244 = 0.04382 0.00732 0.01675 0.00015 AFIX 43 H7C 2 0.273027 0.655401 0.527364 11.00000 -1.20000 AFIX 0 C8C 1 0.199429 0.740922 0.579719 11.00000 0.03914 0.04968 = 0.04493 0.00997 0.01895 -0.00124 C9C 1 0.223004 0.778058 0.636712 11.00000 0.04732 0.05023 = 0.04633 0.00772 0.02071 0.00190 AFIX 43 H9C 2 0.165301 0.818471 0.646364 11.00000 -1.20000 AFIX 0 C10C 1 0.329649 0.755931 0.678582 11.00000 0.04266 0.05028 = 0.04592 0.00983 0.01919 0.00483 AFIX 43 H10C 2 0.342689 0.780284 0.716339 11.00000 -1.20000 AFIX 0 C11C 1 0.117717 0.778458 0.465699 11.00000 0.03998 0.05940 = 0.04195 0.01076 0.01433 0.00418 C12C 1 0.256618 0.808685 0.466284 11.00000 0.04562 0.05834 = 0.04212 0.00593 0.01345 -0.00473 AFIX 43 H12C 2 0.322172 0.817605 0.500868 11.00000 -1.20000 AFIX 0 C13C 1 0.296809 0.825558 0.414297 11.00000 0.03349 0.05994 = 0.04298 0.00429 0.01388 -0.00378 AFIX 43 H13C 2 0.390672 0.843975 0.414344 11.00000 -1.20000 AFIX 0 C14C 1 0.200101 0.815398 0.363239 11.00000 0.03224 0.04996 = 0.04126 0.00479 0.01207 0.00669 C15C 1 0.061245 0.784463 0.362502 11.00000 0.04176 0.08900 = 0.04585 0.00972 0.01094 -0.00703 AFIX 43 H15C 2 -0.004956 0.776801 0.328057 11.00000 -1.20000 AFIX 0 C16C 1 0.022290 0.764939 0.414474 11.00000 0.03794 0.08758 = 0.05583 0.01407 0.01203 -0.00973 AFIX 43 H16C 2 -0.069387 0.742570 0.414077 11.00000 -1.20000 AFIX 0 C17C 1 0.176584 0.893704 0.285483 11.00000 0.03876 0.05303 = 0.04270 0.00469 0.01492 0.00374 AFIX 43 H17C 2 0.103449 0.918239 0.300269 11.00000 -1.20000 AFIX 0 C18C 1 0.219096 0.917278 0.233684 11.00000 0.03546 0.05829 = 0.04357 0.00887 0.01483 0.00417 C19C 1 0.162442 0.968219 0.193732 11.00000 0.05442 0.06306 = 0.04241 0.01283 0.01826 0.00870 AFIX 43 H19C 2 0.084046 0.998884 0.194918 11.00000 -1.20000 AFIX 0 C20C 1 0.346810 0.911682 0.166786 11.00000 0.04172 0.07651 = 0.04475 0.01010 0.01724 0.00863 AFIX 43 H20C 2 0.417478 0.898652 0.145632 11.00000 -1.20000 AFIX 0 PART 1 F1 4 0.424073 0.905119 0.048893 10.50000 0.07911 0.16897 = 0.05149 0.03346 0.04723 0.00981 F2 4 0.291217 0.881711 -0.034815 10.50000 0.09259 0.09217 = 0.04483 -0.00142 0.01360 0.02760 F4 4 0.218172 0.833037 0.046333 10.50000 0.08001 0.07664 = 0.07275 -0.00658 0.01399 0.01561 F0AA 4 0.436207 0.795102 0.003329 10.50000 0.16962 0.19244 = 0.06679 0.04253 0.03839 0.09931 B9 3 0.322930 0.841148 0.015503 10.50000 0.09962 0.12271 = 0.06692 0.01413 0.01994 0.03678 PART 0 F006 4 0.114227 1.036688 0.751008 11.00000 0.04554 0.07365 = 0.07483 0.03565 0.01906 0.00834 F007 4 0.155105 0.952374 0.820401 11.00000 0.09156 0.08743 = 0.06094 0.03720 0.04535 0.03057 F008 4 0.341721 1.015256 0.791002 11.00000 0.04583 0.06512 = 0.10810 0.01810 -0.00845 -0.00304 F009 4 0.208599 0.916667 0.732909 11.00000 0.09173 0.08997 = 0.05857 -0.01750 0.01426 0.01708 B02Q 3 0.206682 0.980227 0.774530 11.00000 0.04950 0.05275 = 0.04474 0.00627 0.02046 0.00375 PART 2 F8 4 0.256848 0.802146 0.056153 10.50000 0.08858 0.13079 = 0.07217 -0.00807 0.02046 0.02540 F10 4 0.219821 0.879756 -0.018893 10.50000 0.17705 0.10266 = 0.11460 -0.02972 -0.06132 0.03937 F11 4 0.445590 0.883587 0.044461 10.50000 0.10131 0.15559 = 0.08715 0.02898 0.02762 0.01450 F15 4 0.344797 0.770216 -0.017395 10.50000 0.09718 0.10031 = 0.11518 0.00182 0.06780 -0.00501 B9A 3 0.322930 0.841148 0.015503 10.50000 0.09962 0.12271 = 0.06692 0.01413 0.01994 0.03678 PART 0 PART 1 F1AA 4 0.270327 0.485475 0.785233 10.50000 0.13827 0.13158 = 0.26627 -0.00327 0.13903 0.00031 PART 0 F2AA 4 0.263757 0.626803 0.778225 11.00000 0.14482 0.14033 = 0.25199 0.03851 0.12769 0.01716 PART 2 F5AA 4 0.191998 0.554016 0.713625 10.50000 0.09118 0.18925 = 0.21668 0.05154 0.06583 0.03186 F7AA 4 0.052280 0.538099 0.765362 10.50000 0.06731 0.10755 = 0.21671 0.10929 0.05278 0.02252 F1AB 4 0.281200 0.487784 0.768810 10.50000 0.07187 0.13386 = 0.13118 0.03374 0.05885 0.00963 PART 0 PART 1 F0BA 4 0.141020 0.562936 0.830017 10.50000 0.18012 0.09150 = 0.19226 -0.02002 0.15639 -0.03906 B2 3 0.195536 0.551824 0.777215 10.50000 0.17214 0.13055 = 0.20425 0.02413 0.16191 0.01546 PART 0 PART 2 B2A 3 0.200320 0.546805 0.773536 10.50000 0.07684 0.11742 = 0.20851 0.06343 0.06928 0.02376 PART 0 PART 1 F3AA 4 0.818868 0.621964 1.029201 11.00000 0.16155 0.13022 = 0.19151 0.02993 -0.05903 -0.02819 F4AA 4 0.854249 0.748676 1.045625 11.00000 0.21483 0.15995 = 0.09312 -0.00572 0.04441 0.05206 F6AA 4 0.838260 0.699350 0.954010 11.00000 0.15857 0.34778 = 0.06774 0.05772 0.05195 0.12315 F8AA 4 0.648822 0.705730 0.995753 11.00000 0.12696 0.32728 = 0.07355 0.06239 0.03253 0.07199 B0AA 3 0.793310 0.691896 1.002649 11.00000 0.08813 0.13980 = 0.06100 0.03684 0.02880 0.04749 PART 0 N01B 6 0.198426 0.575267 0.066468 11.00000 0.07584 0.06686 = 0.06290 0.01355 0.00448 0.02180 C030 1 0.139722 0.609299 -0.041257 11.00000 0.15346 0.29203 = 0.07367 0.05966 0.01542 0.09315 AFIX 137 H03A 2 0.053517 0.578937 -0.060673 11.00000 -1.50000 H03B 2 0.217251 0.595307 -0.060403 11.00000 -1.50000 H03C 2 0.126881 0.665766 -0.042131 11.00000 -1.50000 AFIX 0 C02V 1 0.172809 0.590672 0.019383 11.00000 0.09249 0.10143 = 0.06074 0.01580 0.00438 0.02723 N02E 6 1.192636 1.051233 1.050151 11.00000 0.11551 0.10101 = 0.05445 0.02452 0.02044 0.03901 C02M 1 1.187009 1.057067 1.003058 11.00000 0.09992 0.07137 = 0.05002 0.01555 0.01154 0.00905 C02X 1 1.191621 1.064329 0.942480 11.00000 0.21340 0.10351 = 0.05608 0.02838 0.03235 -0.00993 AFIX 137 H02A 2 1.179743 1.011749 0.921462 11.00000 -1.50000 H02B 2 1.282171 1.089884 0.939402 11.00000 -1.50000 H02C 2 1.115990 1.096146 0.926616 11.00000 -1.50000 AFIX 0 HKLF 4 REM p-1_a.res in P-1 REM R1 = 0.1086 for 8552 Fo > 4sig(Fo) and 0.1389 for all 13521 data REM 1047 parameters refined using 193 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 1.472, deepest hole -1.550, 1-sigma level 0.153 Q1 1 0.5000 0.5000 0.0000 10.50000 0.05 1.47 Q2 1 0.0591 0.4424 0.7007 11.00000 0.05 1.30 Q3 1 0.3458 0.5815 0.8596 11.00000 0.05 1.23 Q4 1 0.7034 0.5742 1.0959 11.00000 0.05 1.09 Q5 1 0.2575 0.5318 0.8368 11.00000 0.05 0.87 Q6 1 0.3556 0.5336 -0.0093 11.00000 0.05 0.86 Q7 1 0.3953 0.7351 0.2006 11.00000 0.05 0.83 Q8 1 0.7326 0.6332 0.9569 11.00000 0.05 0.81 Q9 1 0.3811 0.8211 0.3111 11.00000 0.05 0.81 Q10 1 0.3977 0.8048 0.3181 11.00000 0.05 0.76 Q11 1 0.7482 0.7758 0.8171 11.00000 0.05 0.75 Q12 1 0.7003 0.7834 0.8137 11.00000 0.05 0.75 Q13 1 0.4780 0.8099 0.3110 11.00000 0.05 0.74 Q14 1 0.4801 0.5176 -0.0628 11.00000 0.05 0.71 Q15 1 0.8096 0.6246 0.9690 11.00000 0.05 0.68 Q16 1 0.6133 0.7052 0.6974 11.00000 0.05 0.67 Q17 1 0.4112 0.4862 -0.0659 11.00000 0.05 0.66 Q18 1 0.1044 0.5721 0.8146 11.00000 0.05 0.65 Q19 1 0.0470 0.7364 0.4697 11.00000 0.05 0.61 Q20 1 0.6911 0.6961 0.7003 11.00000 0.05 0.60 REM The information below was added by Olex2. REM REM R1 = 0.1086 for 8552 Fo > 4sig(Fo) and 0.1389 for all 62412 data REM n/a parameters refined using n/a restraints REM Highest difference peak 1.47, deepest hole -1.55 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1389 REM R1_gt = 0.1086 REM wR_ref = 0.3308 REM GOOF = 1.138 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 62412 REM Reflections_gt = 8552 REM Parameters = n/a REM Hole = -1.55 REM Peak = 1.47 REM Flack = n/a ; _cod_data_source_file FL273.cif _cod_data_source_block p-1_a _cod_original_cell_volume 3675.8(13) _cod_original_formula_sum 'C64 H54 B4 F15.50 Fe2 N20 S3' _cod_database_code 1556533 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2. Shared sites {B9, B9A} 3. Restrained distances F007-F006 2.25 with sigma of 0.02 F7AA-F2AA 2.25 with sigma of 0.02 F7AA-F1AA 2.25 with sigma of 0.02 F7AA-B2 = F2AA-B2 = F1AA-B2 1.4 with sigma of 0.02 B2-F1AA = B2-F2AA = B2-F7AA = B2-F0BA = B2-F1AB = B2-F5AA 1.4 with sigma of 0.02 B2A-F2AA = B2A-F7AA = B2A-F1AB = B2A-F5AA 1.39 with sigma of 0.02 B2-F1AA = B2-F2AA = B2-F0BA 1.39 with sigma of 0.02 F2AA-F1AA 2.25 with sigma of 0.04 F2AA-F7AA 2.25 with sigma of 0.04 F1AA-F0BA 2.25 with sigma of 0.04 F7AA-F0BA 2.25 with sigma of 0.04 F2AA-F0BA 2.25 with sigma of 0.04 F8-F10 \\sim F8-F11 \\sim F8-F15 \\sim F10-F11 \\sim F10-F15 \\sim F11-F15 with sigma of 0.04 B9-F8 \\sim B9-F10 \\sim B9-F11 \\sim B9-F15 with sigma of 0.02 F15-B9 \\sim F0AA-B9 \\sim F11-B9 \\sim F1-B9 \\sim F2-B9 \\sim F10-B9 \\sim F4-B9 \\sim F8-B9 with sigma of 0.02 B9-F4 \\sim B9-F10 \\sim B9-F11 \\sim B9-F15 \\sim B9-F8 \\sim B9-F0AA \\sim B9-F2 \\sim B9-F1 with sigma of 0.02 4. Uiso/Uaniso restraints and constraints Uanis(C030) \\sim Ueq: with sigma of 0.1 and sigma for terminal atoms of 0.2 Uanis(B9) = Uanis(B9A) 5. Rigid body (RIGU) restrains N02E, C02M, C02X with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C030 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C030, C02V with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 F3AA, F4AA, F6AA, F8AA with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 F1, F2, F4, F0AA, B9, F8, F10, F11, F15 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 F1AA, F2AA, F7AA, F0BA, B2 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 F1AA, F2AA, F5AA, F7AA, F1AB, F0BA, B2, B2A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 F1, F2, F4, F0AA, B9, F8, F10, F11, F15, B9A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 F8, F10, F11, F15, B9A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 F1, F2, F4, F0AA, B9 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 6. Others Fixed Sof: F1(0.5) F2(0.5) F4(0.5) F0AA(0.5) B9(0.5) F8(0.5) F10(0.5) F11(0.5) F15(0.5) B9A(0.5) F1AA(0.5) F5AA(0.5) F7AA(0.5) F1AB(0.5) F0BA(0.5) B2(0.5) B2A(0.5) 7.a Aromatic/amide H refined with riding coordinates: N2A(H2A), N5A(H5A), N2B(H2B), N5B(H5B), N2C(H2C), N5C(H5C), C1A(H1A), C2A(H2AA), C4A(H4A), C6A(H6A), C7A(H7A), C9A(H9A), C10A(H10A), C12A(H12A), C13A(H13A), C15A(H15A), C16A(H16A), C17A(H17A), C19A(H19A), C20A(H20A), C1B(H1B), C3B(H3B), C5B(H5BA), C7B(H7B), C8B(H8B), C10B(H10B), C11B(H11B), C13B(H13B), C14B(H14B), C16B(H16B), C17B(H17B), C18B(H18B), C20B(H20B), C21B(H21B), C1C(H1C), C2C(H2CA), C4C(H4C), C6C(H6C), C7C(H7C), C9C(H9C), C10C(H10C), C12C(H12C), C13C(H13C), C15C(H15C), C16C(H16C), C17C(H17C), C19C(H19C), C20C(H20C) 7.b Idealised Me refined as rotating group: C030(H03A,H03B,H03C), C02X(H02A,H02B,H02C) ; _olex2_exptl_crystal_mounting_method 'mounted with parafin oil' _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe01 Fe 0.70134(8) 0.73491(5) 0.75762(4) 0.0447(3) Uani 1 1 d . . . . . Fe02 Fe 0.37718(9) 0.77402(5) 0.25612(4) 0.0463(3) Uani 1 1 d . . . . . S1A S 0.7790(2) 0.52683(10) 0.46882(10) 0.0699(5) Uani 1 1 d . . . . . S1B S 0.85015(17) 0.99199(8) 0.53475(7) 0.0500(4) Uani 1 1 d . . . . . S1C S 0.04826(16) 0.76576(11) 0.52975(8) 0.0550(4) Uani 1 1 d . . . . . N1A N 0.8789(6) 0.7773(3) 0.8094(3) 0.0524(13) Uani 1 1 d . . . . . N2A N 1.0682(7) 0.8085(4) 0.8784(3) 0.0742(19) Uani 1 1 d . . . . . H2A H 1.1188 0.8272 0.9112 0.089 Uiso 1 1 calc R . . . . N3A N 0.8434(5) 0.7024(3) 0.7057(3) 0.0472(12) Uani 1 1 d . . . . . N4A N 0.3458(6) 0.6604(3) 0.2931(3) 0.0534(13) Uani 1 1 d . . . . . N5A N -0.0142(8) 0.6688(4) 0.1429(4) 0.082(2) Uani 1 1 d . . . . . H5A H -0.0850 0.6631 0.1143 0.098 Uiso 1 1 calc R . . . . N6A N 0.1819(6) 0.7190(3) 0.2017(3) 0.0554(13) Uani 1 1 d . . . . . N1B N 0.5891(5) 0.7715(3) 0.8160(2) 0.0486(12) Uani 1 1 d . . . . . N2B N 0.4917(6) 0.8071(3) 0.8908(2) 0.0563(13) Uani 1 1 d . . . . . H2B H 0.4607 0.8046 0.9227 0.068 Uiso 1 1 calc R . . . . N3B N 0.6518(5) 0.8437(3) 0.7315(2) 0.0441(11) Uani 1 1 d . . . . . N4B N 0.5976(5) 0.8186(3) 0.3019(2) 0.0460(11) Uani 1 1 d . . . . . N5B N 0.6013(7) 0.7396(4) 0.1139(3) 0.0637(15) Uani 1 1 d . . . . . H5B H 0.6119 0.7298 0.0786 0.076 Uiso 1 1 calc R . . . . N6B N 0.5038(6) 0.7400(3) 0.1926(3) 0.0543(13) Uani 1 1 d . . . . . N1C N 0.7223(5) 0.6298(3) 0.7906(2) 0.0488(12) Uani 1 1 d . . . . . N2C N 0.7374(6) 0.5264(3) 0.8412(3) 0.0558(14) Uani 1 1 d . . . . . H2C H 0.7687 0.4964 0.8678 0.067 Uiso 1 1 calc R . . . . N3C N 0.5263(5) 0.6717(3) 0.7082(2) 0.0422(11) Uani 1 1 d . . . . . N4C N 0.2427(5) 0.8375(3) 0.3110(2) 0.0430(10) Uani 1 1 d . . . . . N5C N 0.2462(6) 0.9640(3) 0.1521(2) 0.0532(13) Uani 1 1 d . . . . . H5C H 0.2364 0.9899 0.1220 0.064 Uiso 1 1 calc R . . . . N6C N 0.3313(5) 0.8814(3) 0.2155(2) 0.0476(11) Uani 1 1 d . . . . . C1A C 0.9230(7) 0.8109(4) 0.8621(3) 0.0594(17) Uani 1 1 d . . . . . H1A H 0.8637 0.8336 0.8856 0.071 Uiso 1 1 calc R . . . . C2A C 1.1176(8) 0.7710(5) 0.8330(4) 0.069(2) Uani 1 1 d . . . . . H2AA H 1.2123 0.7614 0.8316 0.083 Uiso 1 1 calc R . . . . C3A C 1.0014(7) 0.7502(4) 0.7899(3) 0.0558(16) Uani 1 1 d . . . . . C4A C 0.9751(7) 0.7116(4) 0.7335(3) 0.0557(16) Uani 1 1 d . . . . . H4A H 1.0497 0.6931 0.7164 0.067 Uiso 1 1 calc R . . . . C5A C 0.8178(6) 0.6609(3) 0.6489(3) 0.0508(15) Uani 1 1 d . . . . . C6A C 0.8790(7) 0.5869(3) 0.6400(3) 0.0580(18) Uani 1 1 d . . . . . H6A H 0.9313 0.5644 0.6710 0.070 Uiso 1 1 calc R . . . . C7A C 0.8603(8) 0.5483(4) 0.5850(4) 0.0610(19) Uani 1 1 d . . . . . H7A H 0.8991 0.4989 0.5794 0.073 Uiso 1 1 calc R . . . . C8A C 0.7844(7) 0.5810(3) 0.5368(3) 0.0536(16) Uani 1 1 d . . . . . C9A C 0.7246(7) 0.6538(3) 0.5474(3) 0.0555(16) Uani 1 1 d . . . . . H9A H 0.6728 0.6772 0.5168 0.067 Uiso 1 1 calc R . . . . C10A C 0.7409(6) 0.6918(3) 0.6029(3) 0.0492(15) Uani 1 1 d . . . . . H10A H 0.6981 0.7399 0.6089 0.059 Uiso 1 1 calc R . . . . C11A C 0.6471(7) 0.5697(3) 0.4205(3) 0.0563(16) Uani 1 1 d . . . . . C12A C 0.5055(8) 0.5772(4) 0.4295(4) 0.0649(19) Uani 1 1 d . . . . . H12A H 0.4792 0.5617 0.4632 0.078 Uiso 1 1 calc R . . . . C13A C 0.4050(7) 0.6079(3) 0.3882(3) 0.0553(17) Uani 1 1 d . . . . . H13A H 0.3128 0.6142 0.3950 0.066 Uiso 1 1 calc R . . . . C14A C 0.4415(7) 0.6294(3) 0.3361(3) 0.0570(17) Uani 1 1 d . . . . . C15A C 0.5835(7) 0.6207(3) 0.3278(3) 0.0550(16) Uani 1 1 d . . . . . H15A H 0.6097 0.6343 0.2937 0.066 Uiso 1 1 calc R . . . . C16A C 0.6816(7) 0.5930(3) 0.3684(3) 0.0579(17) Uani 1 1 d . . . . . H16A H 0.7746 0.5891 0.3620 0.069 Uiso 1 1 calc R . . . . C17A C 0.2204(8) 0.6225(4) 0.2717(4) 0.066(2) Uani 1 1 d . . . . . H17A H 0.1889 0.5777 0.2877 0.079 Uiso 1 1 calc R . . . . C18A C 0.1320(7) 0.6522(4) 0.2222(4) 0.0609(17) Uani 1 1 d . . . . . C19A C 0.0064(8) 0.6214(4) 0.1833(4) 0.072(2) Uani 1 1 d . . . . . H19A H -0.0506 0.5756 0.1862 0.086 Uiso 1 1 calc R . . . . C20A C 0.0921(8) 0.7292(5) 0.1521(4) 0.0670(18) Uani 1 1 d . . . . . H20A H 0.1011 0.7700 0.1284 0.080 Uiso 1 1 calc R . . . . C1B C 0.5575(7) 0.7496(4) 0.8658(3) 0.0530(15) Uani 1 1 d . . . . . H1B H 0.5787 0.7011 0.8805 0.064 Uiso 1 1 calc R . . . . C3B C 0.4803(7) 0.8715(4) 0.8583(3) 0.0538(15) Uani 1 1 d . . . . . H3B H 0.4396 0.9197 0.8662 0.065 Uiso 1 1 calc R . . . . C4B C 0.5425(6) 0.8487(4) 0.8115(3) 0.0472(13) Uani 1 1 d . . . . . C5B C 0.5757(6) 0.8847(3) 0.7619(3) 0.0456(13) Uani 1 1 d . . . . . H5BA H 0.5442 0.9343 0.7525 0.055 Uiso 1 1 calc R . . . . C6B C 0.6939(6) 0.8782(3) 0.6830(3) 0.0402(12) Uani 1 1 d . . . . . C7B C 0.5937(6) 0.9011(3) 0.6383(3) 0.0479(14) Uani 1 1 d . . . . . H7B H 0.4966 0.8944 0.6393 0.058 Uiso 1 1 calc R . . . . C8B C 0.6387(6) 0.9344(3) 0.5915(3) 0.0489(14) Uani 1 1 d . . . . . H8B H 0.5714 0.9500 0.5617 0.059 Uiso 1 1 calc R . . . . C9B C 0.7828(6) 0.9439(3) 0.5897(3) 0.0439(13) Uani 1 1 d . . . . . C10B C 0.8840(6) 0.9214(3) 0.6347(3) 0.0473(14) Uani 1 1 d . . . . . H10B H 0.9809 0.9280 0.6334 0.057 Uiso 1 1 calc R . . . . C11B C 0.8396(6) 0.8887(3) 0.6819(3) 0.0427(12) Uani 1 1 d . . . . . H11B H 0.9068 0.8741 0.7122 0.051 Uiso 1 1 calc R . . . . C12B C 0.7616(6) 0.9395(3) 0.4690(3) 0.0459(13) Uani 1 1 d . . . . . C13B C 0.7102(6) 0.8575(3) 0.4609(3) 0.0465(13) Uani 1 1 d . . . . . H13B H 0.7148 0.8287 0.4930 0.056 Uiso 1 1 calc R . . . . C14B C 0.6541(6) 0.8194(3) 0.4075(3) 0.0478(14) Uani 1 1 d . . . . . H14B H 0.6184 0.7660 0.4040 0.057 Uiso 1 1 calc R . . . . C15B C 0.6495(6) 0.8597(3) 0.3577(3) 0.0446(13) Uani 1 1 d . . . . . C16B C 0.6968(6) 0.9416(3) 0.3644(3) 0.0468(13) Uani 1 1 d . . . . . H16B H 0.6917 0.9700 0.3321 0.056 Uiso 1 1 calc R . . . . C17B C 0.7514(6) 0.9804(3) 0.4195(3) 0.0474(14) Uani 1 1 d . . . . . H17B H 0.7817 1.0347 0.4233 0.057 Uiso 1 1 calc R . . . . C18B C 0.6819(6) 0.8203(3) 0.2637(3) 0.0466(13) Uani 1 1 d . . . . . H18B H 0.7727 0.8465 0.2743 0.056 Uiso 1 1 calc R . . . . C19B C 0.6369(7) 0.7829(3) 0.2068(3) 0.0470(13) Uani 1 1 d . . . . . C20B C 0.6972(7) 0.7824(4) 0.1576(3) 0.0570(16) Uani 1 1 d . . . . . H20B H 0.7856 0.8065 0.1548 0.068 Uiso 1 1 calc R . . . . C21B C 0.4865(8) 0.7155(4) 0.1363(3) 0.0633(18) Uani 1 1 d . . . . . H21B H 0.4059 0.6856 0.1151 0.076 Uiso 1 1 calc R . . . . C1C C 0.7988(7) 0.5995(4) 0.8337(3) 0.0575(17) Uani 1 1 d . . . . . H1C H 0.8830 0.6240 0.8561 0.069 Uiso 1 1 calc R . . . . C2C C 0.6183(7) 0.5094(3) 0.7995(3) 0.0518(15) Uani 1 1 d . . . . . H2CA H 0.5568 0.4632 0.7940 0.062 Uiso 1 1 calc R . . . . C3C C 0.6065(6) 0.5735(3) 0.7673(3) 0.0458(13) Uani 1 1 d . . . . . C4C C 0.5048(6) 0.5984(3) 0.7212(3) 0.0453(13) Uani 1 1 d . . . . . H4C H 0.4276 0.5643 0.7017 0.054 Uiso 1 1 calc R . . . . C5C C 0.4177(5) 0.6966(3) 0.6637(3) 0.0387(12) Uani 1 1 d . . . . . C6C C 0.3968(7) 0.6599(3) 0.6075(3) 0.0449(13) Uani 1 1 d . . . . . H6C H 0.4567 0.6206 0.5980 0.054 Uiso 1 1 calc R . . . . C7C C 0.2873(7) 0.6808(3) 0.5648(3) 0.0490(14) Uani 1 1 d . . . . . H7C H 0.2730 0.6554 0.5274 0.059 Uiso 1 1 calc R . . . . C8C C 0.1994(6) 0.7409(3) 0.5797(3) 0.0430(12) Uani 1 1 d . . . . . C9C C 0.2230(6) 0.7781(3) 0.6367(3) 0.0463(13) Uani 1 1 d . . . . . H9C H 0.1653 0.8185 0.6464 0.056 Uiso 1 1 calc R . . . . C10C C 0.3296(6) 0.7559(3) 0.6786(3) 0.0446(13) Uani 1 1 d . . . . . H10C H 0.3427 0.7803 0.7163 0.053 Uiso 1 1 calc R . . . . C11C C 0.1177(6) 0.7785(3) 0.4657(3) 0.0459(13) Uani 1 1 d . . . . . C12C C 0.2566(6) 0.8087(3) 0.4663(3) 0.0483(13) Uani 1 1 d . . . . . H12C H 0.3222 0.8176 0.5009 0.058 Uiso 1 1 calc R . . . . C13C C 0.2968(6) 0.8256(3) 0.4143(3) 0.0449(13) Uani 1 1 d . . . . . H13C H 0.3907 0.8440 0.4143 0.054 Uiso 1 1 calc R . . . . C14C C 0.2001(6) 0.8154(3) 0.3632(3) 0.0404(12) Uani 1 1 d . . . . . C15C C 0.0612(7) 0.7845(4) 0.3625(3) 0.0587(16) Uani 1 1 d . . . . . H15C H -0.0050 0.7768 0.3281 0.070 Uiso 1 1 calc R . . . . C16C C 0.0223(7) 0.7649(4) 0.4145(3) 0.0601(17) Uani 1 1 d . . . . . H16C H -0.0694 0.7426 0.4141 0.072 Uiso 1 1 calc R . . . . C17C C 0.1766(6) 0.8937(3) 0.2855(3) 0.0439(12) Uani 1 1 d . . . . . H17C H 0.1034 0.9182 0.3003 0.053 Uiso 1 1 calc R . . . . C18C C 0.2191(6) 0.9173(3) 0.2337(3) 0.0446(13) Uani 1 1 d . . . . . C19C C 0.1624(7) 0.9682(4) 0.1937(3) 0.0515(14) Uani 1 1 d . . . . . H19C H 0.0840 0.9989 0.1949 0.062 Uiso 1 1 calc R . . . . C20C C 0.3468(7) 0.9117(4) 0.1668(3) 0.0528(14) Uani 1 1 d . . . . . H20C H 0.4175 0.8987 0.1456 0.063 Uiso 1 1 calc R . . . . F1 F 0.4241(17) 0.9051(12) 0.0489(7) 0.094(4) Uani 0.5 1 d D U P A 1 F2 F 0.2912(13) 0.8817(7) -0.0348(4) 0.076(3) Uani 0.5 1 d D U P A 1 F4 F 0.2182(12) 0.8330(7) 0.0463(6) 0.077(3) Uani 0.5 1 d D U P A 1 F0AA F 0.4362(19) 0.7951(11) 0.0033(6) 0.136(5) Uani 0.5 1 d D U P A 1 B9 B 0.3229(10) 0.8411(6) 0.0155(4) 0.095(2) Uani 0.5 1 d D U P A 1 F006 F 0.1142(4) 1.0367(2) 0.75101(19) 0.0618(11) Uani 1 1 d D . . . . F007 F 0.1551(5) 0.9524(2) 0.82040(19) 0.0734(13) Uani 1 1 d D . . . . F008 F 0.3417(4) 1.0153(2) 0.7910(2) 0.0755(13) Uani 1 1 d . . . . . F009 F 0.2086(5) 0.9167(3) 0.7329(2) 0.0813(12) Uani 1 1 d . . . . . B02Q B 0.2067(8) 0.9802(4) 0.7745(3) 0.0475(15) Uani 1 1 d . . . . . F8 F 0.2568(14) 0.8021(8) 0.0562(6) 0.097(4) Uani 0.5 1 d D U P B 2 F10 F 0.2198(18) 0.8798(9) -0.0189(7) 0.144(6) Uani 0.5 1 d D U P B 2 F11 F 0.4456(18) 0.8836(12) 0.0445(9) 0.112(6) Uani 0.5 1 d D U P B 2 F15 F 0.3448(13) 0.7702(6) -0.0174(6) 0.099(4) Uani 0.5 1 d D U P B 2 B9A B 0.3229(10) 0.8411(6) 0.0155(4) 0.095(2) Uani 0.5 1 d . U P B 2 F1AA F 0.270(2) 0.4855(12) 0.7852(13) 0.168(11) Uani 0.5 1 d D U P C 1 F2AA F 0.2638(8) 0.6268(4) 0.7782(4) 0.166(3) Uani 1 1 d D U . . . F5AA F 0.1920(15) 0.5540(10) 0.7136(7) 0.158(5) Uani 0.5 1 d D U P D 2 F7AA F 0.0523(9) 0.5381(6) 0.7654(7) 0.121(5) Uani 0.5 1 d D U P D 2 F1AB F 0.281(2) 0.4878(11) 0.7688(10) 0.106(5) Uani 0.5 1 d D U P D 2 F0BA F 0.1410(16) 0.5629(6) 0.8300(7) 0.143(6) Uani 0.5 1 d D U P C 1 B2 B 0.1955(13) 0.5518(7) 0.7772(7) 0.153(8) Uani 0.5 1 d D U P C 1 B2A B 0.2003(16) 0.5468(10) 0.7735(10) 0.125(6) Uani 0.5 1 d D U P D 2 F3AA F 0.8189(9) 0.6220(4) 1.0292(4) 0.173(4) Uani 1 1 d . U . E 1 F4AA F 0.8542(11) 0.7487(5) 1.0456(4) 0.154(3) Uani 1 1 d . U . E 1 F6AA F 0.8383(9) 0.6993(7) 0.9540(3) 0.182(4) Uani 1 1 d . U . E 1 F8AA F 0.6488(9) 0.7057(7) 0.9958(3) 0.170(4) Uani 1 1 d . U . E 1 B0AA B 0.7933(13) 0.6919(9) 1.0026(5) 0.091(3) Uani 1 1 d . . . E 1 N01B N 0.1984(7) 0.5753(3) 0.0665(3) 0.0685(16) Uani 1 1 d . . . . . C030 C 0.1397(17) 0.6093(11) -0.0413(6) 0.168(7) Uani 1 1 d . U . . . H03A H 0.0535 0.5789 -0.0607 0.253 Uiso 1 1 calc GR . . . . H03B H 0.2173 0.5953 -0.0604 0.253 Uiso 1 1 calc GR . . . . H03C H 0.1269 0.6658 -0.0421 0.253 Uiso 1 1 calc GR . . . . C02V C 0.1728(11) 0.5907(6) 0.0194(4) 0.085(2) Uani 1 1 d . U . . . N02E N 1.1926(9) 1.0512(5) 1.0502(3) 0.088(2) Uani 1 1 d . U . . . C02M C 1.1870(10) 1.0571(5) 1.0031(4) 0.073(2) Uani 1 1 d . U . . . C02X C 1.1916(17) 1.0643(6) 0.9425(4) 0.123(4) Uani 1 1 d . U . . . H02A H 1.1797 1.0117 0.9215 0.184 Uiso 1 1 calc GR . . . . H02B H 1.2822 1.0899 0.9394 0.184 Uiso 1 1 calc GR . . . . H02C H 1.1160 1.0961 0.9266 0.184 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe01 0.0403(5) 0.0472(4) 0.0514(6) 0.0140(4) 0.0172(4) 0.0022(3) Fe02 0.0409(5) 0.0533(5) 0.0483(5) 0.0027(4) 0.0192(4) 0.0022(4) S1A 0.0776(13) 0.0579(9) 0.0774(14) -0.0034(9) 0.0229(10) 0.0218(8) S1B 0.0547(9) 0.0495(7) 0.0495(9) 0.0096(6) 0.0207(7) -0.0086(6) S1C 0.0365(8) 0.0850(10) 0.0504(10) 0.0199(8) 0.0195(7) 0.0061(7) N1A 0.054(3) 0.052(3) 0.052(3) 0.011(2) 0.012(3) 0.000(2) N2A 0.071(4) 0.078(4) 0.066(4) 0.026(3) -0.013(3) -0.013(3) N3A 0.036(3) 0.043(2) 0.066(4) 0.013(2) 0.017(2) 0.0013(19) N4A 0.048(3) 0.050(3) 0.065(4) -0.003(2) 0.023(3) 0.000(2) N5A 0.072(4) 0.080(4) 0.083(6) -0.007(4) -0.004(4) 0.004(3) N6A 0.044(3) 0.063(3) 0.058(4) -0.001(3) 0.010(2) 0.007(2) N1B 0.045(3) 0.057(3) 0.047(3) 0.017(2) 0.013(2) -0.003(2) N2B 0.058(3) 0.075(3) 0.042(3) 0.016(3) 0.020(3) 0.006(3) N3B 0.038(2) 0.052(2) 0.045(3) 0.012(2) 0.015(2) -0.001(2) N4B 0.045(3) 0.047(2) 0.050(3) 0.003(2) 0.021(2) 0.002(2) N5B 0.069(4) 0.079(3) 0.047(3) 0.000(3) 0.025(3) 0.012(3) N6B 0.053(3) 0.063(3) 0.051(3) 0.000(2) 0.024(3) 0.003(2) N1C 0.044(3) 0.050(2) 0.055(3) 0.012(2) 0.011(2) 0.002(2) N2C 0.061(3) 0.053(3) 0.058(4) 0.020(3) 0.014(3) 0.017(2) N3C 0.036(2) 0.047(2) 0.050(3) 0.013(2) 0.019(2) 0.0054(19) N4C 0.035(2) 0.054(2) 0.043(3) 0.007(2) 0.013(2) 0.0046(19) N5C 0.056(3) 0.069(3) 0.039(3) 0.012(2) 0.017(2) 0.005(2) N6C 0.041(3) 0.064(3) 0.041(3) 0.008(2) 0.013(2) 0.006(2) C1A 0.058(4) 0.060(4) 0.061(5) 0.019(3) 0.010(3) -0.002(3) C2A 0.052(4) 0.080(4) 0.076(6) 0.022(4) 0.008(4) 0.002(3) C3A 0.047(3) 0.057(3) 0.065(5) 0.018(3) 0.012(3) -0.006(3) C4A 0.056(4) 0.054(3) 0.065(5) 0.020(3) 0.025(3) 0.006(3) C5A 0.047(3) 0.047(3) 0.067(4) 0.008(3) 0.032(3) -0.002(2) C6A 0.061(4) 0.048(3) 0.075(5) 0.018(3) 0.033(4) 0.009(3) C7A 0.064(4) 0.047(3) 0.081(5) 0.005(3) 0.037(4) 0.009(3) C8A 0.056(4) 0.044(3) 0.068(5) 0.010(3) 0.029(3) 0.005(3) C9A 0.065(4) 0.041(3) 0.067(5) 0.007(3) 0.029(3) 0.002(3) C10A 0.048(3) 0.041(3) 0.065(4) 0.009(3) 0.024(3) 0.004(2) C11A 0.060(4) 0.040(3) 0.073(5) -0.003(3) 0.026(3) 0.003(3) C12A 0.079(5) 0.050(3) 0.073(5) 0.002(3) 0.037(4) -0.005(3) C13A 0.046(3) 0.047(3) 0.080(5) 0.008(3) 0.029(3) 0.002(3) C14A 0.058(4) 0.042(3) 0.075(5) -0.002(3) 0.030(4) -0.005(3) C15A 0.048(4) 0.051(3) 0.067(5) 0.000(3) 0.022(3) -0.007(3) C16A 0.054(4) 0.046(3) 0.075(5) -0.011(3) 0.025(3) -0.005(3) C17A 0.064(4) 0.044(3) 0.095(6) -0.006(3) 0.037(4) -0.008(3) C18A 0.044(4) 0.063(4) 0.074(5) -0.006(3) 0.010(3) 0.006(3) C19A 0.061(4) 0.061(4) 0.086(6) -0.011(4) 0.008(4) -0.015(3) C20A 0.048(4) 0.084(4) 0.065(5) -0.011(4) 0.008(3) 0.002(3) C1B 0.053(4) 0.066(3) 0.046(4) 0.017(3) 0.018(3) 0.009(3) C3B 0.047(3) 0.066(3) 0.051(4) 0.010(3) 0.014(3) 0.011(3) C4B 0.040(3) 0.062(3) 0.046(3) 0.016(3) 0.017(3) 0.005(2) C5B 0.039(3) 0.054(3) 0.048(4) 0.010(3) 0.015(3) 0.002(2) C6B 0.042(3) 0.042(2) 0.040(3) 0.008(2) 0.017(2) 0.001(2) C7B 0.037(3) 0.056(3) 0.057(4) 0.018(3) 0.018(3) 0.002(2) C8B 0.044(3) 0.053(3) 0.054(4) 0.015(3) 0.015(3) 0.003(2) C9B 0.045(3) 0.044(3) 0.048(3) 0.006(2) 0.023(3) 0.002(2) C10B 0.049(3) 0.045(3) 0.051(4) 0.007(2) 0.019(3) -0.007(2) C11B 0.040(3) 0.046(3) 0.045(3) 0.011(2) 0.012(2) -0.002(2) C12B 0.045(3) 0.051(3) 0.049(4) 0.013(3) 0.022(3) 0.005(2) C13B 0.052(3) 0.048(3) 0.044(3) 0.009(2) 0.020(3) -0.001(2) C14B 0.053(3) 0.044(3) 0.050(4) 0.007(2) 0.021(3) -0.005(2) C15B 0.037(3) 0.049(3) 0.052(4) 0.004(2) 0.021(3) 0.005(2) C16B 0.046(3) 0.052(3) 0.045(3) 0.011(3) 0.016(3) -0.001(2) C17B 0.050(3) 0.046(3) 0.050(4) 0.012(2) 0.018(3) -0.005(2) C18B 0.048(3) 0.048(3) 0.049(4) 0.007(3) 0.019(3) 0.005(2) C19B 0.052(3) 0.047(3) 0.046(4) 0.006(2) 0.020(3) 0.006(2) C20B 0.051(4) 0.075(4) 0.052(4) 0.010(3) 0.024(3) 0.012(3) C21B 0.069(5) 0.071(4) 0.054(4) -0.005(3) 0.028(4) 0.003(3) C1C 0.051(4) 0.058(3) 0.066(5) 0.018(3) 0.011(3) 0.002(3) C2C 0.054(4) 0.049(3) 0.056(4) 0.015(3) 0.014(3) 0.002(3) C3C 0.050(3) 0.043(3) 0.050(4) 0.006(2) 0.024(3) 0.001(2) C4C 0.045(3) 0.046(3) 0.050(4) 0.010(2) 0.020(3) 0.000(2) C5C 0.034(3) 0.042(2) 0.042(3) 0.005(2) 0.014(2) -0.006(2) C6C 0.055(3) 0.045(3) 0.039(3) 0.006(2) 0.019(3) 0.003(2) C7C 0.054(3) 0.052(3) 0.044(3) 0.007(3) 0.017(3) 0.000(3) C8C 0.039(3) 0.050(3) 0.045(3) 0.010(2) 0.019(2) -0.001(2) C9C 0.047(3) 0.050(3) 0.046(3) 0.008(2) 0.021(3) 0.002(2) C10C 0.043(3) 0.050(3) 0.046(3) 0.010(2) 0.019(3) 0.005(2) C11C 0.040(3) 0.059(3) 0.042(3) 0.011(3) 0.014(2) 0.004(2) C12C 0.046(3) 0.058(3) 0.042(3) 0.006(3) 0.013(3) -0.005(2) C13C 0.033(3) 0.060(3) 0.043(3) 0.004(3) 0.014(2) -0.004(2) C14C 0.032(3) 0.050(3) 0.041(3) 0.005(2) 0.012(2) 0.007(2) C15C 0.042(3) 0.089(4) 0.046(4) 0.010(3) 0.011(3) -0.007(3) C16C 0.038(3) 0.088(4) 0.056(4) 0.014(3) 0.012(3) -0.010(3) C17C 0.039(3) 0.053(3) 0.043(3) 0.005(2) 0.015(2) 0.004(2) C18C 0.035(3) 0.058(3) 0.044(3) 0.009(3) 0.015(2) 0.004(2) C19C 0.054(4) 0.063(3) 0.042(3) 0.013(3) 0.018(3) 0.009(3) C20C 0.042(3) 0.077(4) 0.045(4) 0.010(3) 0.017(3) 0.009(3) F1 0.079(6) 0.169(9) 0.051(5) 0.033(5) 0.047(4) 0.010(6) F2 0.093(7) 0.092(6) 0.045(4) -0.001(4) 0.014(4) 0.028(5) F4 0.080(6) 0.077(6) 0.073(7) -0.007(5) 0.014(5) 0.016(5) F0AA 0.170(10) 0.192(10) 0.067(8) 0.043(7) 0.038(8) 0.099(9) B9 0.100(5) 0.123(6) 0.067(5) 0.014(4) 0.020(4) 0.037(4) F006 0.046(2) 0.074(2) 0.075(3) 0.036(2) 0.0191(19) 0.0083(17) F007 0.092(3) 0.087(3) 0.061(3) 0.037(2) 0.045(2) 0.031(2) F008 0.046(2) 0.065(2) 0.108(4) 0.018(2) -0.008(2) -0.0030(17) F009 0.092(3) 0.090(3) 0.059(3) -0.017(2) 0.014(2) 0.017(2) B02Q 0.049(4) 0.053(3) 0.045(4) 0.006(3) 0.020(3) 0.004(3) F8 0.089(8) 0.131(10) 0.072(7) -0.008(6) 0.020(6) 0.025(6) F10 0.177(12) 0.103(7) 0.115(10) -0.030(7) -0.061(8) 0.039(8) F11 0.101(8) 0.156(11) 0.087(10) 0.029(7) 0.028(7) 0.015(7) F15 0.097(7) 0.100(5) 0.115(9) 0.002(5) 0.068(7) -0.005(5) B9A 0.100(5) 0.123(6) 0.067(5) 0.014(4) 0.020(4) 0.037(4) F1AA 0.138(15) 0.132(9) 0.27(3) -0.003(10) 0.139(17) 0.000(8) F2AA 0.145(6) 0.140(4) 0.252(10) 0.039(5) 0.128(6) 0.017(4) F5AA 0.091(8) 0.189(11) 0.217(11) 0.052(7) 0.066(7) 0.032(7) F7AA 0.067(5) 0.108(7) 0.217(13) 0.109(8) 0.053(6) 0.023(4) F1AB 0.072(7) 0.134(8) 0.131(12) 0.034(7) 0.059(8) 0.010(6) F0BA 0.180(12) 0.092(6) 0.192(13) -0.020(7) 0.156(12) -0.039(7) B2 0.172(17) 0.131(9) 0.204(16) 0.024(9) 0.162(13) 0.015(8) B2A 0.077(8) 0.117(8) 0.209(14) 0.063(7) 0.069(8) 0.024(6) F3AA 0.162(7) 0.130(5) 0.192(9) 0.030(6) -0.059(7) -0.028(5) F4AA 0.215(9) 0.160(6) 0.093(6) -0.006(5) 0.044(6) 0.052(6) F6AA 0.159(7) 0.348(13) 0.068(5) 0.058(7) 0.052(5) 0.123(8) F8AA 0.127(6) 0.327(11) 0.074(5) 0.062(6) 0.033(4) 0.072(7) B0AA 0.088(8) 0.140(10) 0.061(7) 0.037(7) 0.029(6) 0.047(7) N01B 0.076(4) 0.067(3) 0.063(4) 0.014(3) 0.004(3) 0.022(3) C030 0.153(12) 0.29(2) 0.074(7) 0.060(10) 0.015(8) 0.093(13) C02V 0.092(6) 0.101(6) 0.061(5) 0.016(5) 0.004(4) 0.027(5) N02E 0.116(6) 0.101(5) 0.054(4) 0.025(3) 0.020(4) 0.039(4) C02M 0.100(6) 0.071(4) 0.050(4) 0.016(3) 0.012(4) 0.009(4) C02X 0.213(14) 0.104(7) 0.056(5) 0.028(5) 0.032(6) -0.010(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 N1A Fe01 N3A 81.2(2) . . N1A Fe01 N1B 90.6(2) . . N1A Fe01 N3B 94.0(2) . . N1A Fe01 N1C 89.2(2) . . N1A Fe01 N3C 169.97(19) . . N1B Fe01 N3A 171.8(2) . . N1B Fe01 N3B 80.12(19) . . N1B Fe01 N1C 90.6(2) . . N1B Fe01 N3C 91.4(2) . . N3B Fe01 N3A 100.98(18) . . N3B Fe01 N3C 96.01(19) . . N1C Fe01 N3A 88.7(2) . . N1C Fe01 N3B 170.2(2) . . N1C Fe01 N3C 81.0(2) . . N3C Fe01 N3A 96.6(2) . . N4A Fe02 N4B 102.0(2) . . N4A Fe02 N4C 92.33(18) . . N6A Fe02 N4A 77.2(2) . . N6A Fe02 N4B 170.3(2) . . N6A Fe02 N4C 88.2(2) . . N6B Fe02 N4A 101.89(19) . . N6B Fe02 N6A 92.5(2) . . N6B Fe02 N4B 78.1(2) . . N6B Fe02 N4C 165.57(18) . . N4C Fe02 N4B 101.53(18) . . N6C Fe02 N4A 160.7(2) . . N6C Fe02 N6A 86.9(2) . . N6C Fe02 N4B 95.54(18) . . N6C Fe02 N6B 89.3(2) . . N6C Fe02 N4C 76.30(18) . . C8A S1A C11A 105.5(3) . . C12B S1B C9B 105.3(3) . . C11C S1C C8C 103.7(3) . . C1A N1A Fe01 139.9(5) . . C1A N1A C3A 106.2(6) . . C3A N1A Fe01 112.3(5) . . C1A N2A H2A 126.2 . . C2A N2A H2A 126.2 . . C2A N2A C1A 107.5(7) . . C4A N3A Fe01 112.0(5) . . C4A N3A C5A 117.5(5) . . C5A N3A Fe01 129.7(4) . . C14A N4A Fe02 126.4(4) . . C17A N4A Fe02 112.7(5) . . C17A N4A C14A 120.9(5) . . C19A N5A H5A 124.7 . . C19A N5A C20A 110.6(7) . . C20A N5A H5A 124.7 . . C18A N6A Fe02 112.4(5) . . C20A N6A Fe02 140.0(5) . . C20A N6A C18A 107.5(6) . . C1B N1B Fe01 139.0(4) . . C1B N1B C4B 105.8(5) . . C4B N1B Fe01 114.4(3) . . C1B N2B H2B 125.0 . . C1B N2B C3B 110.0(5) . . C3B N2B H2B 125.0 . . C5B N3B Fe01 115.7(4) . . C5B N3B C6B 118.2(5) . . C6B N3B Fe01 126.1(4) . . C15B N4B Fe02 132.1(3) . . C18B N4B Fe02 108.6(4) . . C18B N4B C15B 117.4(5) . . C20B N5B H5B 126.2 . . C21B N5B H5B 126.2 . . C21B N5B C20B 107.6(6) . . C19B N6B Fe02 109.4(4) . . C21B N6B Fe02 139.3(5) . . C21B N6B C19B 105.8(5) . . C1C N1C Fe01 139.2(5) . . C1C N1C C3C 107.3(5) . . C3C N1C Fe01 112.4(4) . . C1C N2C H2C 125.9 . . C2C N2C H2C 125.9 . . C2C N2C C1C 108.2(5) . . C4C N3C Fe01 114.6(4) . . C4C N3C C5C 114.9(5) . . C5C N3C Fe01 130.3(3) . . C14C N4C Fe02 129.3(3) . . C17C N4C Fe02 111.9(4) . . C17C N4C C14C 117.5(5) . . C19C N5C H5C 126.1 . . C20C N5C H5C 126.1 . . C20C N5C C19C 107.7(5) . . C18C N6C Fe02 111.6(3) . . C20C N6C Fe02 138.1(4) . . C20C N6C C18C 106.4(5) . . N1A C1A N2A 111.1(7) . . N1A C1A H1A 124.4 . . N2A C1A H1A 124.4 . . N2A C2A H2AA 126.5 . . N2A C2A C3A 107.0(7) . . C3A C2A H2AA 126.5 . . C2A C3A N1A 108.2(7) . . C2A C3A C4A 137.2(7) . . C4A C3A N1A 114.7(6) . . N3A C4A C3A 118.1(6) . . N3A C4A H4A 120.9 . . C3A C4A H4A 120.9 . . C6A C5A N3A 118.9(6) . . C10A C5A N3A 122.1(5) . . C10A C5A C6A 119.0(7) . . C5A C6A H6A 120.4 . . C7A C6A C5A 119.2(7) . . C7A C6A H6A 120.4 . . C6A C7A H7A 118.9 . . C6A C7A C8A 122.1(6) . . C8A C7A H7A 118.9 . . C7A C8A S1A 116.5(5) . . C9A C8A S1A 126.6(6) . . C9A C8A C7A 116.9(7) . . C8A C9A H9A 119.5 . . C10A C9A C8A 120.9(7) . . C10A C9A H9A 119.5 . . C5A C10A C9A 121.8(6) . . C5A C10A H10A 119.1 . . C9A C10A H10A 119.1 . . C12A C11A S1A 123.4(6) . . C12A C11A C16A 117.8(7) . . C16A C11A S1A 118.7(5) . . C11A C12A H12A 119.8 . . C13A C12A C11A 120.3(6) . . C13A C12A H12A 119.8 . . C12A C13A H13A 119.7 . . C12A C13A C14A 120.7(6) . . C14A C13A H13A 119.7 . . N4A C14A C13A 123.4(6) . . N4A C14A C15A 118.6(6) . . C13A C14A C15A 118.0(7) . . C14A C15A H15A 119.4 . . C16A C15A C14A 121.3(7) . . C16A C15A H15A 119.4 . . C11A C16A H16A 119.1 . . C15A C16A C11A 121.8(6) . . C15A C16A H16A 119.1 . . N4A C17A H17A 120.7 . . N4A C17A C18A 118.5(6) . . C18A C17A H17A 120.7 . . N6A C18A C17A 118.0(6) . . N6A C18A C19A 107.3(7) . . C19A C18A C17A 134.1(6) . . N5A C19A C18A 107.0(6) . . N5A C19A H19A 126.5 . . C18A C19A H19A 126.5 . . N5A C20A H20A 126.2 . . N6A C20A N5A 107.6(7) . . N6A C20A H20A 126.2 . . N1B C1B H1B 124.9 . . N2B C1B N1B 110.2(5) . . N2B C1B H1B 124.9 . . N2B C3B H3B 127.6 . . N2B C3B C4B 104.8(6) . . C4B C3B H3B 127.6 . . N1B C4B C5B 113.9(5) . . C3B C4B N1B 109.2(5) . . C3B C4B C5B 136.8(6) . . N3B C5B C4B 115.7(5) . . N3B C5B H5BA 122.1 . . C4B C5B H5BA 122.1 . . C7B C6B N3B 121.6(5) . . C7B C6B C11B 120.3(5) . . C11B C6B N3B 118.1(5) . . C6B C7B H7B 120.0 . . C6B C7B C8B 120.0(5) . . C8B C7B H7B 120.0 . . C7B C8B H8B 119.9 . . C9B C8B C7B 120.1(6) . . C9B C8B H8B 119.9 . . C8B C9B S1B 123.1(5) . . C8B C9B C10B 120.1(5) . . C10B C9B S1B 116.6(4) . . C9B C10B H10B 120.0 . . C9B C10B C11B 120.1(5) . . C11B C10B H10B 120.0 . . C6B C11B C10B 119.4(5) . . C6B C11B H11B 120.3 . . C10B C11B H11B 120.3 . . C13B C12B S1B 125.7(5) . . C17B C12B S1B 117.1(4) . . C17B C12B C13B 116.9(6) . . C12B C13B H13B 119.0 . . C14B C13B C12B 122.0(5) . . C14B C13B H13B 119.0 . . C13B C14B H14B 119.5 . . C13B C14B C15B 120.9(5) . . C15B C14B H14B 119.5 . . C14B C15B N4B 120.7(5) . . C14B C15B C16B 118.4(6) . . C16B C15B N4B 120.9(5) . . C15B C16B H16B 120.0 . . C17B C16B C15B 120.1(5) . . C17B C16B H16B 120.0 . . C12B C17B H17B 119.2 . . C16B C17B C12B 121.6(5) . . C16B C17B H17B 119.2 . . N4B C18B H18B 119.5 . . N4B C18B C19B 121.0(5) . . C19B C18B H18B 119.5 . . N6B C19B C18B 118.8(5) . . C20B C19B N6B 108.6(6) . . C20B C19B C18B 132.5(6) . . N5B C20B C19B 106.6(6) . . N5B C20B H20B 126.7 . . C19B C20B H20B 126.7 . . N5B C21B H21B 124.3 . . N6B C21B N5B 111.4(7) . . N6B C21B H21B 124.3 . . N1C C1C N2C 110.1(6) . . N1C C1C H1C 125.0 . . N2C C1C H1C 125.0 . . N2C C2C H2CA 126.6 . . N2C C2C C3C 106.7(5) . . C3C C2C H2CA 126.6 . . N1C C3C C4C 115.5(4) . . C2C C3C N1C 107.6(6) . . C2C C3C C4C 136.7(6) . . N3C C4C C3C 116.2(5) . . N3C C4C H4C 121.9 . . C3C C4C H4C 121.9 . . C6C C5C N3C 120.8(5) . . C6C C5C C10C 120.2(6) . . C10C C5C N3C 118.9(5) . . C5C C6C H6C 119.4 . . C5C C6C C7C 121.2(5) . . C7C C6C H6C 119.4 . . C6C C7C H7C 120.7 . . C6C C7C C8C 118.6(6) . . C8C C7C H7C 120.7 . . C7C C8C S1C 121.6(5) . . C7C C8C C9C 119.5(6) . . C9C C8C S1C 118.7(4) . . C8C C9C H9C 119.3 . . C10C C9C C8C 121.4(6) . . C10C C9C H9C 119.3 . . C5C C10C H10C 120.4 . . C9C C10C C5C 119.1(6) . . C9C C10C H10C 120.4 . . C12C C11C S1C 123.2(5) . . C16C C11C S1C 116.5(4) . . C16C C11C C12C 119.9(5) . . C11C C12C H12C 120.4 . . C11C C12C C13C 119.3(6) . . C13C C12C H12C 120.4 . . C12C C13C H13C 119.5 . . C14C C13C C12C 121.1(5) . . C14C C13C H13C 119.5 . . C13C C14C N4C 119.7(5) . . C13C C14C C15C 119.7(5) . . C15C C14C N4C 120.6(5) . . C14C C15C H15C 120.4 . . C14C C15C C16C 119.2(6) . . C16C C15C H15C 120.4 . . C11C C16C C15C 120.8(5) . . C11C C16C H16C 119.6 . . C15C C16C H16C 119.6 . . N4C C17C H17C 120.9 . . N4C C17C C18C 118.3(5) . . C18C C17C H17C 120.9 . . N6C C18C C17C 118.0(5) . . N6C C18C C19C 109.3(5) . . C19C C18C C17C 132.5(6) . . N5C C19C C18C 105.6(6) . . N5C C19C H19C 127.2 . . C18C C19C H19C 127.2 . . N5C C20C H20C 124.5 . . N6C C20C N5C 110.9(5) . . N6C C20C H20C 124.5 . . F2 B9 F1 95.6(11) . . F4 B9 F1 105.2(10) . . F4 B9 F2 116.7(9) . . F4 B9 F0AA 135.6(11) . . F0AA B9 F1 91.4(13) . . F0AA B9 F2 101.8(9) . . F007 B02Q F006 108.2(5) . . F007 B02Q F009 109.4(5) . . F008 B02Q F006 109.7(5) . . F008 B02Q F007 111.8(6) . . F008 B02Q F009 108.5(6) . . F009 B02Q F006 109.3(6) . . F10 B9A F8 108.4(11) . . F10 B9A F15 106.6(10) . . F11 B9A F8 108.6(12) . . F11 B9A F10 119.9(13) . . F11 B9A F15 114.8(12) . . F15 B9A F8 95.7(9) . . F1AA B2 F2AA 121.5(14) . . F1AA B2 F0BA 101.6(14) . . F2AA B2 F0BA 99.7(9) . . F5AA B2A F2AA 81.9(12) . . F7AA B2A F2AA 116.8(12) . . F7AA B2A F5AA 90.0(14) . . F1AB B2A F2AA 118.2(15) . . F1AB B2A F5AA 88.9(16) . . F1AB B2A F7AA 124.2(17) . . F3AA B0AA F8AA 110.1(10) . . F4AA B0AA F3AA 101.2(9) . . F4AA B0AA F8AA 103.1(10) . . F6AA B0AA F3AA 118.5(11) . . F6AA B0AA F4AA 113.1(12) . . F6AA B0AA F8AA 109.7(9) . . H03A C030 H03B 109.5 . . H03A C030 H03C 109.5 . . H03B C030 H03C 109.5 . . C02V C030 H03A 109.5 . . C02V C030 H03B 109.5 . . C02V C030 H03C 109.5 . . N01B C02V C030 179.3(13) . . N02E C02M C02X 175.6(12) . . C02M C02X H02A 109.5 . . C02M C02X H02B 109.5 . . C02M C02X H02C 109.5 . . H02A C02X H02B 109.5 . . H02A C02X H02C 109.5 . . H02B C02X H02C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Fe01 N1A 1.959(6) . Fe01 N3A 2.044(5) . Fe01 N1B 1.963(5) . Fe01 N3B 2.025(4) . Fe01 N1C 1.993(4) . Fe01 N3C 2.038(5) . Fe02 N4A 2.192(5) . Fe02 N6A 2.170(6) . Fe02 N4B 2.239(5) . Fe02 N6B 2.141(5) . Fe02 N4C 2.219(5) . Fe02 N6C 2.140(5) . S1A C8A 1.760(8) . S1A C11A 1.767(8) . S1B C9B 1.784(5) . S1B C12B 1.760(7) . S1C C8C 1.784(6) . S1C C11C 1.782(6) . N1A C1A 1.304(9) . N1A C3A 1.409(9) . N2A H2A 0.8600 . N2A C1A 1.371(9) . N2A C2A 1.358(11) . N3A C4A 1.302(9) . N3A C5A 1.425(9) . N4A C14A 1.394(9) . N4A C17A 1.316(9) . N5A H5A 0.8600 . N5A C19A 1.289(11) . N5A C20A 1.368(10) . N6A C18A 1.355(8) . N6A C20A 1.353(9) . N1B C1B 1.342(8) . N1B C4B 1.394(8) . N2B H2B 0.8600 . N2B C1B 1.326(8) . N2B C3B 1.377(8) . N3B C5B 1.287(7) . N3B C6B 1.440(6) . N4B C15B 1.420(8) . N4B C18B 1.312(7) . N5B H5B 0.8600 . N5B C20B 1.368(9) . N5B C21B 1.357(9) . N6B C19B 1.394(8) . N6B C21B 1.333(9) . N1C C1C 1.300(8) . N1C C3C 1.410(8) . N2C H2C 0.8600 . N2C C1C 1.368(8) . N2C C2C 1.362(9) . N3C C4C 1.307(6) . N3C C5C 1.443(7) . N4C C14C 1.439(7) . N4C C17C 1.294(7) . N5C H5C 0.8600 . N5C C19C 1.372(8) . N5C C20C 1.351(8) . N6C C18C 1.366(7) . N6C C20C 1.329(8) . C1A H1A 0.9300 . C2A H2AA 0.9300 . C2A C3A 1.370(10) . C3A C4A 1.399(10) . C4A H4A 0.9300 . C5A C6A 1.409(8) . C5A C10A 1.358(9) . C6A H6A 0.9300 . C6A C7A 1.375(10) . C7A H7A 0.9300 . C7A C8A 1.407(10) . C8A C9A 1.391(8) . C9A H9A 0.9300 . C9A C10A 1.381(9) . C10A H10A 0.9300 . C11A C12A 1.412(10) . C11A C16A 1.413(10) . C12A H12A 0.9300 . C12A C13A 1.393(10) . C13A H13A 0.9300 . C13A C14A 1.409(9) . C14A C15A 1.413(9) . C15A H15A 0.9300 . C15A C16A 1.346(10) . C16A H16A 0.9300 . C17A H17A 0.9300 . C17A C18A 1.455(11) . C18A C19A 1.414(10) . C19A H19A 0.9300 . C20A H20A 0.9300 . C1B H1B 0.9300 . C3B H3B 0.9300 . C3B C4B 1.377(9) . C4B C5B 1.440(8) . C5B H5BA 0.9300 . C6B C7B 1.386(8) . C6B C11B 1.394(8) . C7B H7B 0.9300 . C7B C8B 1.405(8) . C8B H8B 0.9300 . C8B C9B 1.382(8) . C9B C10B 1.393(9) . C10B H10B 0.9300 . C10B C11B 1.408(7) . C11B H11B 0.9300 . C12B C13B 1.417(8) . C12B C17B 1.400(8) . C13B H13B 0.9300 . C13B C14B 1.364(9) . C14B H14B 0.9300 . C14B C15B 1.403(8) . C15B C16B 1.405(8) . C16B H16B 0.9300 . C16B C17B 1.397(9) . C17B H17B 0.9300 . C18B H18B 0.9300 . C18B C19B 1.412(9) . C19B C20B 1.386(8) . C20B H20B 0.9300 . C21B H21B 0.9300 . C1C H1C 0.9300 . C2C H2CA 0.9300 . C2C C3C 1.369(8) . C3C C4C 1.430(9) . C4C H4C 0.9300 . C5C C6C 1.387(8) . C5C C10C 1.391(8) . C6C H6C 0.9300 . C6C C7C 1.397(9) . C7C H7C 0.9300 . C7C C8C 1.399(8) . C8C C9C 1.404(8) . C9C H9C 0.9300 . C9C C10C 1.376(8) . C10C H10C 0.9300 . C11C C12C 1.389(8) . C11C C16C 1.370(9) . C12C H12C 0.9300 . C12C C13C 1.398(8) . C13C H13C 0.9300 . C13C C14C 1.371(8) . C14C C15C 1.391(8) . C15C H15C 0.9300 . C15C C16C 1.406(9) . C16C H16C 0.9300 . C17C H17C 0.9300 . C17C C18C 1.437(8) . C18C C19C 1.386(8) . C19C H19C 0.9300 . C20C H20C 0.9300 . F1 B9 1.470(13) . F2 B9 1.416(10) . F4 B9 1.344(11) . F0AA B9 1.412(11) . F006 B02Q 1.408(8) . F007 B02Q 1.375(7) . F008 B02Q 1.360(8) . F009 B02Q 1.383(8) . F8 B9A 1.426(11) . F10 B9A 1.385(11) . F11 B9A 1.369(13) . F15 B9A 1.403(11) . F1AA B2 1.359(11) . F2AA B2 1.378(10) . F2AA B2A 1.426(16) . F5AA B2A 1.420(19) . F7AA B2A 1.386(15) . F1AB B2A 1.291(16) . F0BA B2 1.435(12) . F3AA B0AA 1.389(13) . F4AA B0AA 1.351(16) . F6AA B0AA 1.310(12) . F8AA B0AA 1.390(13) . N01B C02V 1.151(10) . C030 H03A 0.9600 . C030 H03B 0.9600 . C030 H03C 0.9600 . C030 C02V 1.476(14) . N02E C02M 1.118(10) . C02M C02X 1.455(11) . C02X H02A 0.9600 . C02X H02B 0.9600 . C02X H02C 0.9600 . loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N2A H2A F2 0.86 2.01 2.816(15) 156.0 1_656 N2A H2A F10 0.86 1.87 2.726(16) 173.2 1_656 N5A H5A F3AA 0.86 2.09 2.883(12) 152.8 1_454 N5A H5A F4AA 0.86 2.28 2.889(11) 128.1 1_454 N2B H2B F0AA 0.86 1.98 2.824(14) 166.7 1_556 N2B H2B F15 0.86 2.05 2.878(11) 161.8 1_556 N2C H2C N01B 0.86 2.04 2.887(8) 168.4 2_666 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 -1 9.33 1.11 0 0 1 12.75 2.13 0 0 -2 2052.47 154.7 0 0 -2 2359.28 176.05 0 0 2 2207.73 164.86 0 0 2 2317.7 174.2 0 0 -3 133.72 13.86 0 0 -3 138.9 11.37 0 0 3 116.62 9.89 0 0 3 128.92 12.85 0 0 -4 2186.47 166.99 0 0 -4 2663.32 199.24 0 0 4 2268.72 170.04 0 0 4 2475.72 187.5 0 0 -5 1903.69 147.21 0 0 -5 2273.34 170.5 0 0 5 1993.33 149.98 0 0 5 2143.96 163.66 0 0 -6 10.44 9.8 0 0 -6 3.6 3.33 0 0 6 2.31 3.51 0 0 6 -0.28 7.39 0 0 7 62.38 7.76 0 0 7 80.95 13.03 0 0 -8 14.51 13.49 0 0 -8 22.27 4.9 0 0 8 20.7 5.73 0 0 8 13.86 9.43 0 0 -9 7.58 19.59 0 0 -9 50.46 8.32 0 0 9 25.23 8.04 0 0 9 46.85 14.79 0 0 10 867.38 70.7 0 0 10 1096.01 94.72 0 0 -11 -16.91 24.67 0 0 11 12.57 15.25 0 0 11 -0.74 7.58 0 0 -12 137.51 45.28 0 0 -12 200.16 21.44 0 0 12 166.99 23.2 0 0 12 235.28 35.86 0 0 -13 13.12 7.21 0 0 13 22.46 16.73 0 0 -14 378.61 35.95 0 0 -14 407.54 76.61 0 0 14 346.64 39.18 0 0 14 454.67 56.56 0 0 -15 471.12 86.78 0 0 -15 377.69 36.5 0 0 15 363.92 51.84 0 0 15 388.96 43.9 0 0 -16 25.88 46.58 0 0 -16 19.04 8.59 0 0 16 33.18 16.82 0 0 16 17.28 21.35 0 0 -17 848.25 71.99 0 0 -17 990.66 136.4 0 0 17 913.68 95.09 0 0 17 892.15 84.93 0 0 -18 928.74 142.5 0 0 -18 738.28 63.21 0 0 18 766.74 83.45 0 0 18 912.2 88.62 0 0 -19 557.25 49.44 0 0 -19 785.32 129.38 0 0 19 812.86 82.8 0 0 19 567.13 67.55 0 0 -20 35.58 51.01 0 0 20 13.31 18.85 0 0 -21 22.64 7.3 0 0 -21 3.05 7.49 0 0 21 14.32 18.39 0 0 21 16.17 13.58 0 0 -22 4.16 4.16 0 0 -22 21.81 6.75 0 0 22 28.28 13.86 0 0 22 53.14 21.35 0 0 -23 6.93 3.97 0 0 -23 25.32 7.58 0 0 23 21.35 17.1 0 0 23 44.73 15.34 0 0 -24 32.44 7.49 0 0 -24 11.55 4.99 0 0 24 27.54 13.12 0 0 24 35.58 11.74 0 0 -25 2.4 3.51 0 0 -25 3.42 4.07 0 0 25 -2.22 6.01 0 0 -26 -2.13 3.6 0 0 -26 -2.22 2.68 0 0 26 0.83 4.07 0 0 -27 -2.03 2.96 0 0 -27 6.19 4.07 0 0 27 0.74 3.05 0 -1 31 -0.74 2.96 0 1 -31 -2.31 3.05 0 -1 30 17.1 5.82 0 -1 30 8.5 4.34 0 -1 29 1.94 4.53 0 -1 29 1.76 3.6 0 1 -29 10.44 4.44 0 1 -29 3.23 3.33 0 -1 28 -0.46 4.44 0 -1 28 0 3.14 0 1 -28 10.81 4.62 0 1 -28 0.74 2.96 0 -1 27 0.09 3.23 0 -1 27 4.07 50.36 0 1 -27 -1.76 2.77 0 1 -27 7.12 3.97 0 -1 26 36.6 9.8 0 -1 25 13.21 8.5 0 -1 25 15.16 7.86 0 -1 24 30.96 15.06 0 -1 24 18.57 8.96 0 -1 23 0.65 8.96 0 -1 23 9.15 14.69 0 1 -23 -2.5 2.96 0 1 -23 1.94 3.79 0 -1 21 83.91 24.86 0 -1 21 59.79 15.8 0 -1 20 198.87 35.12 0 1 -20 191.02 71.25 0 -1 19 252.75 34.01 0 -1 19 277.88 42.6 0 1 -19 232.51 22.46 0 1 -19 277.61 89.18 0 -1 18 1.02 11.55 0 -1 18 11.46 15.99 0 1 -18 33.08 51.01 0 1 -18 9.89 4.99 0 -1 17 26.61 16.54 0 -1 17 25.04 13.12 0 1 -17 24.67 6.65 0 1 -17 15.71 48.24 0 -1 16 19.13 15.34 0 -1 16 6.28 11.27 0 1 -16 1.57 4.34 0 1 -16 2.59 46.11 0 -1 15 15.99 11.83 0 -1 15 0.18 13.4 0 1 -15 -44.45 39.64 0 1 -15 -0.46 3.97 0 -1 14 10.44 10.72 0 -1 14 15.62 11.92 0 1 -14 -1.94 36.13 0 1 -14 11 4.81 0 -1 13 3.97 11 0 1 -13 2.4 4.07 0 -1 12 6.56 10.07 0 -1 12 -4.9 9.61 0 1 -12 -4.53 28.56 0 1 -12 5.18 4.25 0 -1 11 41.4 10.44 0 1 -11 53.51 23.75 0 -1 10 9.61 6.75 0 -1 10 2.03 8.59 0 1 -10 9.61 4.07 0 1 -10 20.89 17.1 0 -1 9 3.88 5.27 0 -1 9 -2.77 7.86 0 1 -9 5.36 3.42 0 1 -9 -3.05 13.4 0 -1 8 31.97 5.91 0 -1 8 34.75 9.06 0 1 -8 47.32 6.1 0 1 -8 20.98 10.63 0 -1 7 5.82 3.51 0 -1 7 6.1 5.36 0 1 -7 10.17 2.77 0 1 -7 11.74 8.13 0 -1 6 17.28 3.88 0 -1 6 27.91 6.65 0 1 -6 25.23 3.7 0 1 -6 23.57 7.86 0 -1 5 39 5.08 0 -1 5 47.04 7.21 0 1 -5 57.02 5.54 0 1 -5 42.14 8.59 0 -1 4 102.12 9.06 0 -1 4 109.88 11 0 1 -4 117.46 9.61 0 1 -4 103.59 11.74 0 -1 3 66.72 5.73 0 -1 3 69.12 6.84 0 1 -3 76.52 6.19 0 1 -3 63.76 6.84 0 -1 2 0.09 0.65 0 -1 2 1.29 1.66 0 1 -2 -0.18 1.48 0 1 -2 1.11 0.65 0 -1 1 242.21 18.3 0 1 -1 238.42 17.93 0 -1 0 211.53 15.89 0 1 0 198.5 14.97 0 -1 -1 146.57 11.37 0 1 1 130.67 10.81 0 -1 -2 7.02 3.6 0 -1 -2 2.77 1.48 0 1 2 4.07 1.29 0 1 2 6.65 3.79 0 -1 -3 61.08 6.28 0 -1 -3 52.03 8.87 0 1 3 53.97 5.36 0 1 3 55.82 10.26 0 -1 -4 79.47 8.32 0 -1 -4 86.22 13.68 0 1 4 87.33 8.41 0 1 4 98.23 15.43 0 -1 -5 14.32 4.34 0 -1 -5 12.48 10.53 0 1 5 8.13 3.23 0 1 5 9.06 10.44 0 -1 -6 18.85 4.81 0 -1 -6 15.89 11.46 0 1 6 11.55 3.6 0 1 6 12.57 10.07 0 -1 -7 5.73 11.18 0 -1 -7 1.85 4.07 0 1 7 -0.55 3.33 0 1 7 -2.03 9.52 0 -1 -8 176.14 16.91 0 -1 -8 167.27 28.74 0 1 8 184.27 24.95 0 1 8 192.12 18.57 0 -1 -9 55.45 9.43 0 -1 -9 66.63 26.25 0 1 9 74.48 11.37 0 1 9 70.51 18.76 0 -1 -10 108.03 14.88 0 -1 -10 194.9 38.91 0 1 10 197.95 21.16 0 -1 -11 -13.49 25.88 0 -1 -11 3.23 6.47 0 1 11 -1.2 15.62 0 1 11 0.46 7.3 0 -1 -12 -9.24 7.02 0 -1 -12 -17.1 34.38 0 1 12 3.51 9.33 0 1 12 -4.44 16.26 0 -1 -13 164.4 19.78 0 1 13 169.95 31.97 0 -1 -14 270.03 29.2 0 -1 -14 398.67 77.16 0 1 14 348.12 51.38 0 1 14 318.08 37.24 0 -1 -15 57.94 47.22 0 -1 -15 61.82 13.95 0 1 15 85.76 19.5 0 1 15 80.86 29.02 0 -1 -16 196.56 26.25 0 -1 -16 257.92 69.31 0 1 16 202.94 30.96 0 1 16 190.28 43.43 0 -1 -17 112.28 54.15 0 -1 -17 68.2 16.08 0 1 17 101.01 22.55 0 1 17 49.44 30.59 0 -1 -18 620.83 108.77 0 -1 -18 563.07 53.88 0 1 18 479.8 55.08 0 1 18 463.91 69.86 0 -1 -19 62.1 52.95 0 -1 -19 46.39 13.58 0 1 19 49.35 29.02 0 1 19 43.62 18.85 0 -1 -20 389.61 79.84 0 1 20 430.27 51.94 0 -1 -21 -2.13 5.82 0 -1 -21 1.02 7.67 0 1 21 -8.87 12.66 0 1 21 11.83 14.79 0 -1 -22 13.86 8.32 0 -1 -22 0.74 5.08 0 1 22 8.22 13.03 0 1 22 27.26 14.23 0 -1 -23 -0.46 4.81 0 -1 -23 16.08 7.76 0 1 23 12.48 11 0 1 23 12.85 12.38 0 -1 -24 10.9 6.1 0 -1 -24 -1.29 5.18 0 1 24 11.18 9.43 0 1 24 11.55 6.38 0 -1 -25 2.68 4.16 0 -1 -25 2.96 5.08 0 1 25 0.46 5.08 0 1 25 0.74 5.08 0 -1 -26 2.22 3.42 0 1 26 17.47 6.19 0 -1 -27 11.27 4.71 0 1 27 1.2 4.9 0 -1 -28 15.25 5.36 0 -1 -28 0.37 3.33 0 1 28 12.66 5.54 0 1 28 7.39 4.07 0 -1 -29 3.05 3.33 0 -1 -29 9.8 4.44 0 1 29 1.02 2.96 0 1 29 3.97 4.53 0 1 30 5.36 4.16 0 1 30 11.74 5.18 0 -2 31 1.85 3.33 0 2 -31 2.5 3.33 0 -2 30 1.39 4.44 0 -2 30 2.86 3.6 0 2 -30 11.74 4.62 0 2 -30 0.74 2.96 0 -2 29 -0.65 3.42 0 -2 29 0.74 4.62 0 2 -29 4.34 3.79 0 2 -29 1.48 2.96 0 -2 28 -0.65 4.99 0 -2 28 0.83 3.6 0 -2 27 0 3.7 0 -2 27 8.04 5.45 0 -2 26 -2.5 5.64 0 -2 26 -1.11 3.7 0 2 -26 3.6 3.23 0 2 -26 -2.31 2.86 0 -2 25 43.34 10.53 0 -2 25 16.17 10.35 0 -2 24 12.94 8.69 0 -2 24 20.42 14.23 0 -2 23 4.34 16.08 0 -2 23 13.21 9.52 0 2 -23 1.39 3.05 0 2 -23 0.65 3.33 0 -2 22 49.35 12.75 0 -2 22 37.43 22.83 0 -2 21 145.92 31.05 0 -2 21 89.92 16.73 0 -2 20 278.72 41.77 0 2 -20 123.83 65.34 0 -2 19 72.45 15.34 0 -2 19 56.83 23.2 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2.77 0 10 -8 15.99 3.51 0 10 -8 14.14 2.68 0 -10 7 1195.81 90.38 0 -10 7 1199.51 90.56 0 10 -7 1205.05 91.77 0 10 -7 1171.79 88.81 0 -10 6 0.92 1.29 0 -10 6 -0.65 1.11 0 10 -6 0.28 1.66 0 10 -6 1.02 1.94 0 -10 5 411.6 32.16 0 10 -5 418.44 33.27 0 -10 4 12.94 2.5 0 10 -4 9.61 3.05 0 -10 3 565.19 43.71 0 10 -3 603.27 47.78 0 -10 2 40.94 4.81 0 10 -2 46.48 6.56 0 -10 1 24.67 3.7 0 10 -1 19.78 4.71 0 -10 0 39.92 5.64 0 10 0 26.89 6.56 0 -10 -1 31.33 5.36 0 10 1 50.09 11.83 0 -10 -2 132.24 13.58 0 10 2 116.25 20.42 0 -10 -3 175.4 16.17 0 -10 -3 151.56 15.16 0 10 3 132.43 21.9 0 10 3 134.83 11.92 0 -10 -4 44.27 6.38 0 -10 -4 42.51 7.12 0 10 4 23.38 12.66 0 10 4 47.68 5.36 0 -10 -5 19.31 4.25 0 -10 -5 22.92 6.47 0 10 5 23.66 14.51 0 10 5 14.51 2.86 0 -10 -6 115.79 16.82 0 -10 -6 99.9 11.18 0 10 6 92.78 9.06 0 10 6 112.93 30.77 0 -10 -7 1314.1 108.95 0 -10 -7 1005.44 78.92 0 10 7 1019.31 78.18 0 10 7 1381.56 144.9 0 -10 -8 122.17 20.89 0 -10 -8 80.31 11.83 0 10 8 99.99 10.44 0 10 8 141.39 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5.64 0 -12 13 59.51 8.22 0 12 -13 55.72 6.93 0 12 -13 57.2 13.4 0 -12 12 143.24 14.32 0 -12 12 116.44 11 0 12 -12 130.86 18.48 0 12 -12 111.45 11 0 -12 11 12.94 2.86 0 -12 11 18.57 4.07 0 12 -11 14.88 6.19 0 12 -11 15.53 3.33 0 -12 10 9.8 2.86 0 -12 10 8.04 2.31 0 12 -10 10.44 2.86 0 12 -10 11.09 4.53 0 -12 9 577.21 44.82 0 -12 9 511.04 39.92 0 12 -9 495.24 40.2 0 12 -9 527.86 41.59 0 -12 8 240.27 20.05 0 -12 8 220.5 18.39 0 12 -8 179.37 16.45 0 12 -8 192.86 17 0 -12 7 153.03 13.4 0 -12 7 138.16 12.01 0 12 -7 143.7 13.77 0 12 -7 140 13.21 0 -12 6 113.57 10.17 0 -12 6 109.42 10.35 0 12 -6 113.76 11.18 0 12 -6 115.61 12.38 0 -12 5 111.63 10.07 0 -12 5 123.09 11.37 0 12 -5 129.1 12.01 0 12 -5 130.12 14.05 0 -12 4 12.2 2.68 0 -12 4 8.32 2.5 0 12 -4 11.74 4.25 0 12 -4 11.64 2.96 0 -12 3 34.47 4.81 0 -12 3 30.59 4.16 0 12 -3 40.38 7.02 0 12 -3 37.61 4.62 0 -12 2 0.83 1.29 0 -12 2 0.37 1.76 0 12 -2 1.29 1.29 0 12 -2 -0.18 3.42 0 -12 1 56.56 7.12 0 -12 1 50.83 5.54 0 12 -1 54.25 5.82 0 12 -1 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8.22 7.39 0 -14 11 501.24 40.48 0 14 -11 459.1 40.75 0 -14 10 134.74 13.86 0 -14 10 162.09 14.88 0 14 -10 115.98 14.88 0 14 -10 152.39 16.17 0 -14 9 -1.66 1.76 0 -14 9 1.48 1.85 0 14 -9 2.4 2.96 0 14 -9 1.02 3.05 0 -14 8 64.6 6.93 0 -14 8 79.38 8.78 0 14 -8 59.51 7.86 0 14 -8 71.16 10.07 0 -14 7 32.99 4.53 0 -14 7 39 5.73 0 14 -7 40.57 7.76 0 14 -7 32.07 5.64 0 -14 6 5.08 2.03 0 -14 6 3.23 2.22 0 14 -6 4.07 2.77 0 14 -6 1.85 4.16 0 -14 5 5.18 2.03 0 -14 5 8.04 2.68 0 14 -5 0.28 3.97 0 14 -5 2.68 2.5 0 -14 4 -0.55 1.48 0 -14 4 -2.4 1.76 0 14 -4 -2.03 3.7 0 14 -4 1.11 1.94 0 -14 3 23.75 4.53 0 -14 3 24.58 3.97 0 14 -3 21.53 6.65 0 14 -3 25.51 4.07 0 -14 2 -1.39 24.86 0 -14 2 0 1.57 0 14 -2 1.48 5.54 0 14 -2 0 1.57 0 -14 1 84.19 10.63 0 -14 1 82.06 8.5 0 14 -1 78.74 8.04 0 14 -1 73.74 15.53 0 -14 0 3.42 3.7 0 -14 0 2.31 1.76 0 14 0 0.65 1.66 0 14 0 -1.48 9.89 0 -14 -1 37.98 7.95 0 -14 -1 45.84 5.91 0 14 1 39.09 4.99 0 14 1 53.41 17.56 0 -14 -2 11.74 5.27 0 -14 -2 7.49 2.59 0 14 2 15.16 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15.53 7.76 4 13 -15 14.14 4.34 -4 -13 14 5.82 2.68 -4 -13 14 6.01 3.05 4 13 -14 1.39 2.96 4 13 -14 3.33 5.36 -4 -13 13 4.25 2.59 -4 -13 13 7.02 2.77 4 13 -13 8.96 4.07 4 13 -13 3.05 4.62 -4 -13 12 2.22 2.13 -4 -13 12 -0.92 2.03 4 13 -12 3.42 3.33 4 13 -12 -2.31 3.23 -4 -13 11 -0.74 2.22 -4 -13 11 1.85 1.94 4 13 -11 -1.11 3.7 4 13 -11 0.46 2.96 -4 -13 10 21.25 4.53 4 13 -10 25.6 6.75 -4 -13 9 49.81 7.49 4 13 -9 41.4 9.15 -4 -13 8 1.11 2.03 -4 -13 8 -1.66 2.22 4 13 -8 2.86 3.6 4 13 -8 1.29 4.34 -4 -13 7 -0.83 2.13 -4 -13 7 -1.11 1.76 4 13 -7 1.2 4.9 4 13 -7 -1.39 2.59 -4 -13 6 128.18 12.11 -4 -13 6 120.51 12.38 4 13 -6 105.26 14.69 4 13 -6 127.53 12.66 -4 -13 5 127.07 12.11 -4 -13 5 108.68 11.92 4 13 -5 101.19 14.6 4 13 -5 130.58 12.57 -4 -13 4 -1.66 2.77 -4 -13 4 -0.92 1.76 4 13 -4 -4.71 5.73 4 13 -4 2.03 1.85 -4 -13 3 0.55 3.33 -4 -13 3 1.85 1.94 4 13 -3 2.03 6.93 4 13 -3 -0.18 1.85 -4 -13 2 10.44 5.18 -4 -13 2 14.32 3.14 4 13 -2 1.76 9.43 4 13 -2 13.68 3.05 -4 -13 1 52.49 9.52 -4 -13 1 37.7 5.36 4 13 -1 51.38 17.1 4 13 -1 41.96 5.54 -4 -13 0 8.13 5.45 -4 -13 0 3.23 2.31 4 13 0 3.05 2.13 4 13 0 -0.74 11.64 -4 -13 -1 0.18 5.27 4 13 1 -5.45 12.29 -4 -13 -2 2.03 5.18 4 13 2 9.8 13.12 -4 -13 -3 1.57 2.77 -4 -13 -3 -1.02 5.08 4 13 3 -7.02 11.18 4 13 3 1.2 2.03 -4 -13 -4 97.03 11.55 -4 -13 -4 67.46 13.03 -4 -13 -5 11.64 4.62 -4 -13 -5 15.43 8.87 4 13 5 16.54 14.23 4 13 5 13.31 3.42 -4 -13 -6 23.66 6.19 -4 -13 -6 26.52 12.38 4 13 6 0.18 13.03 4 13 6 24.21 4.71 -4 -13 -7 1.85 3.79 -4 -13 -7 1.02 10.17 4 13 7 -6.19 11.83 4 13 7 -0.83 1.85 -4 -13 -8 109.32 14.05 -4 -13 -8 73.47 16.54 -4 -13 -9 43.34 8.59 -4 -13 -9 25.14 10.26 -4 -13 -10 15.43 8.13 -4 -13 -10 26.15 6.84 4 13 10 4.99 7.12 4 13 10 24.58 4.99 -4 -13 -11 8.22 6.1 -4 -13 -11 4.62 5.08 4 13 11 7.39 3.51 4 13 11 -0.46 3.97 -4 -13 -13 18.94 6.28 -4 -13 -13 7.76 4.62 -4 -13 -14 1.66 3.88 4 13 14 -0.83 3.23 -4 -13 -15 -1.39 3.33 -4 -13 -15 9.7 4.99 4 13 15 2.31 3.14 4 13 15 10.81 4.16 -4 -13 -16 1.48 3.6 -4 -13 -16 12.66 5.18 4 13 16 -1.2 3.14 4 13 16 6.1 3.51 -4 -13 -17 -1.48 3.6 -4 -13 -17 6.65 4.71 4 13 17 0.28 3.05 4 13 17 9.24 4.25 -4 -13 -18 -3.7 3.23 -4 -13 -18 0.83 3.79 4 13 18 2.5 3.05 4 13 18 -1.57 2.96 -4 -13 -19 16.08 5.36 4 13 19 18.21 5.54 -4 -14 25 3.23 4.9 4 14 -25 0.46 3.6 -4 -14 24 1.66 2.96 -4 -14 24 -6.84 4.44 4 14 -24 0 4.07 4 14 -24 0.65 3.7 -4 -14 23 2.5 3.14 -4 -14 23 -2.77 4.62 4 14 -23 1.11 4.99 4 14 -23 -2.13 3.42 -4 -14 22 7.49 5.36 -4 -14 22 17.84 4.71 4 14 -22 13.68 4.9 4 14 -22 7.3 5.64 -4 -14 21 24.95 5.36 -4 -14 21 9.15 5.73 4 14 -21 3.51 5.36 4 14 -21 22.27 6.01 -4 -14 20 5.27 3.42 4 14 -20 9.15 4.44 -4 -14 19 2.86 4.16 -4 -14 19 3.88 3.23 4 14 -19 6.65 3.97 4 14 -19 2.96 6.01 -4 -14 18 106.55 13.12 4 14 -18 55.17 12.48 -4 -14 17 13.86 4.07 -4 -14 17 10.44 4.71 4 14 -17 20.52 5.18 -4 -14 16 130.39 14.6 -4 -14 16 145.36 14.69 4 14 -16 113.67 13.31 4 14 -16 119.67 17.84 -4 -14 15 35.86 5.91 -4 -14 15 49.35 7.67 4 14 -15 36.78 9.98 4 14 -15 43.25 7.67 -4 -14 14 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2.5 2.77 -4 -16 8 4.07 2.77 4 16 -8 1.85 5.27 4 16 -8 -2.59 3.88 -4 -16 7 5.73 3.6 4 16 -7 4.99 4.07 4 16 -7 3.14 5.73 -4 -16 6 26.52 6.28 4 16 -6 16.45 7.58 4 16 -6 34.28 6.56 -4 -16 5 40.48 8.69 4 16 -5 28.56 10.35 4 16 -5 60.07 8.41 -4 -16 4 0 3.88 4 16 -4 -0.55 7.58 4 16 -4 -0.83 2.68 -4 -16 3 5.82 4.71 4 16 -3 -2.77 8.22 4 16 -3 0.37 2.5 -4 -16 2 3.33 5.36 4 16 -2 7.49 10.44 4 16 -2 4.62 2.96 -4 -16 1 23.66 7.76 4 16 -1 19.87 4.44 4 16 -1 8.69 10.63 -4 -16 0 7.49 6.01 4 16 0 2.03 2.59 4 16 0 6.1 10.07 -4 -16 -1 2.86 5.91 4 16 1 8.78 9.33 4 16 1 1.48 2.59 -4 -16 -2 15.25 7.3 4 16 2 31.79 5.73 4 16 2 8.22 7.67 -4 -16 -3 14.51 7.67 -4 -16 -4 5.45 6.38 4 16 5 37.15 6.38 -4 -16 -6 4.44 5.08 -4 -16 -7 -1.57 4.07 4 16 7 9.24 3.7 4 16 7 1.48 3.79 -4 -16 -8 -0.92 3.88 4 16 8 1.39 3.51 -4 -16 -9 -1.29 3.6 4 16 9 0.46 131.41 4 16 9 3.51 3.23 -4 -16 -10 0 3.79 4 16 10 1.2 3.6 4 16 10 5.73 3.42 -4 -16 -11 2.4 4.25 4 16 11 3.79 3.79 4 16 11 14.42 4.9 -4 -16 -12 0.74 4.25 4 16 12 1.2 3.51 4 16 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23.66 5.73 -5 -11 20 11.46 4.9 -5 -11 20 24.58 4.81 5 11 -20 15.62 8.87 5 11 -20 23.93 5.45 -5 -11 19 8.32 4.53 -5 -11 19 8.59 3.23 5 11 -19 14.23 4.16 5 11 -19 9.15 7.58 -5 -11 18 0.74 2.22 -5 -11 18 5.54 3.6 5 11 -18 4.07 2.77 5 11 -18 2.03 7.3 -5 -11 17 11.64 4.44 -5 -11 17 13.49 3.51 5 11 -17 9.7 8.69 5 11 -17 11.27 3.97 -5 -11 16 1.57 2.22 -5 -11 16 8.96 4.16 5 11 -16 5.73 2.96 5 11 -16 7.67 8.69 -5 -11 15 65.15 7.67 -5 -11 15 71.06 9.24 5 11 -15 83.45 14.42 5 11 -15 48.61 7.02 -5 -11 14 20.52 4.53 -5 -11 14 23.01 4.25 5 11 -14 24.03 7.49 5 11 -14 18.02 4.44 -5 -11 13 32.62 5.08 5 11 -13 34.28 6.1 -5 -11 12 244.15 20.7 -5 -11 12 275.2 23.47 5 11 -12 253.21 23.47 5 11 -12 278.62 25.32 -5 -11 11 23.75 4.34 -5 -11 11 23.2 4.34 5 11 -11 24.49 5.82 5 11 -11 22.83 5.73 -5 -11 10 26.25 4.07 -5 -11 10 32.99 5.27 5 11 -10 33.73 7.21 5 11 -10 30.4 5.54 -5 -11 9 102.39 9.8 5 11 -9 118.2 12.29 -5 -11 8 247.48 20.42 5 11 -8 280.19 24.12 -5 -11 7 21.07 3.7 5 11 -7 22.27 4.53 -5 -11 6 142.41 14.6 -5 -11 5 2.86 2.59 -5 -11 5 0.83 1.85 5 11 -5 0.18 5.08 5 11 -5 4.07 2.31 -5 -11 4 3.05 2.68 -5 -11 4 2.96 1.94 5 11 -4 1.02 1.85 5 11 -4 0.65 5.91 -5 -11 3 44.91 5.64 -5 -11 3 43.62 7.21 5 11 -3 43.25 5.54 5 11 -3 52.21 12.75 -5 -11 2 47.59 8.69 -5 -11 2 37.7 5.08 5 11 -2 52.49 16.08 5 11 -2 42.88 5.45 -5 -11 1 0.65 1.76 5 11 -1 2.68 1.94 -5 -11 0 2.96 1.94 5 11 0 0.65 1.66 -5 -11 -1 7.95 2.96 5 11 1 14.23 3.05 -5 -11 -2 0.18 2.22 -5 -11 -2 -1.2 4.44 5 11 2 12.94 13.86 5 11 2 1.66 1.76 -5 -11 -3 116.72 12.66 -5 -11 -3 83.26 13.4 -5 -11 -4 62.75 9.06 -5 -11 -4 54.8 12.01 5 11 4 53.97 6.84 5 11 4 21.81 15.99 -5 -11 -5 77.35 15.34 5 11 5 45.1 20.61 -5 -11 -6 107.11 19.87 -5 -11 -6 68.94 11 5 11 6 78.09 9.33 5 11 6 33.82 19.5 -5 -11 -7 12.57 4.9 -5 -11 -7 17.28 12.66 5 11 7 11.09 3.33 5 11 7 -14.51 15.62 -5 -11 -8 36.5 14.97 -5 -11 -8 25.41 6.38 5 11 8 22.18 4.44 5 11 8 17.19 17.93 -5 -11 -9 24.67 12.01 -5 -11 -9 14.32 5.27 5 11 9 14.14 12.94 5 11 9 18.76 4.16 -5 -11 -10 4.62 4.16 -5 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11.27 5 13 -9 117.64 12.85 5 13 -9 94.63 14.05 -5 -13 8 84.1 9.98 -5 -13 8 84.46 8.96 5 13 -8 96.2 11.09 5 13 -8 68.85 11.64 -5 -13 7 4.25 2.96 -5 -13 7 2.77 2.13 5 13 -7 3.14 2.77 5 13 -7 6.56 5.08 -5 -13 6 23.29 4.16 -5 -13 6 12.48 4.07 5 13 -6 20.61 4.44 5 13 -6 18.57 7.02 -5 -13 5 95 11.46 -5 -13 5 100.54 10.44 5 13 -5 90.01 9.8 5 13 -5 71.16 13.4 -5 -13 4 202.94 20.61 -5 -13 4 228.91 19.87 5 13 -4 171.79 23.2 5 13 -4 192.03 17.19 -5 -13 3 89.46 12.57 -5 -13 3 75.96 8.5 5 13 -3 75.13 8.32 5 13 -3 60.71 16.08 -5 -13 2 7.39 5.36 -5 -13 2 1.66 2.13 5 13 -2 -5.36 9.98 5 13 -2 2.31 2.03 -5 -13 1 1.2 2.03 -5 -13 1 10.81 5.73 5 13 -1 8.78 12.11 5 13 -1 1.02 2.03 -5 -13 0 100.36 14.97 -5 -13 0 74.76 8.69 5 13 0 77.72 8.87 5 13 0 39.28 17.28 -5 -13 -1 1.94 5.82 -5 -13 -1 0.74 2.13 5 13 1 -1.94 1.76 5 13 1 11.37 13.58 -5 -13 -2 113.76 16.73 -5 -13 -2 137.79 13.68 -5 -13 -3 2.96 6.1 -5 -13 -3 1.94 2.86 5 13 3 0.09 1.94 5 13 3 -7.21 11.37 -5 -13 -4 66.35 14.14 -5 -13 -4 69.96 9.43 5 13 4 76.24 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10.07 14.6 7 7 7 34.28 5.45 -7 -7 -8 72.64 10.81 -7 -7 -8 74.02 20.24 -7 -7 -9 -5.54 8.59 7 7 9 -0.65 6.75 -7 -7 -10 -7.12 7.39 -7 -7 -10 -2.13 3.33 7 7 10 -0.09 2.13 7 7 10 -1.39 4.9 -7 -7 -11 0.37 3.97 -7 -7 -11 -2.5 4.71 7 7 11 1.76 2.4 7 7 11 1.39 3.51 -7 -7 -12 1.02 4.44 -7 -7 -12 -1.11 3.23 7 7 12 0 2.68 7 7 12 -1.02 3.14 -7 -7 -13 -2.22 3.51 -7 -7 -13 1.76 3.14 7 7 13 -0.09 3.23 7 7 13 1.29 2.68 -7 -7 -14 6.38 4.07 -7 -7 -14 12.38 5.08 -7 -7 -15 4.16 4.07 -7 -7 -15 1.11 4.16 7 7 15 0 2.86 7 7 15 0.37 6.47 -7 -7 -16 2.03 4.53 -7 -7 -16 -0.18 3.14 7 7 16 -0.92 3.33 7 7 16 -2.03 2.96 -7 -7 -17 2.4 3.97 -7 -7 -17 -1.02 3.88 7 7 17 6.19 4.07 7 7 17 0.18 3.6 -7 -7 -18 6.38 4.71 -7 -7 -18 2.31 4.34 -7 -7 -19 1.29 3.97 -7 -7 -19 -0.83 4.44 7 7 19 -1.57 2.59 7 7 19 1.2 3.7 -7 -7 -20 3.97 4.53 -7 -7 -20 0.46 3.7 7 7 20 1.48 3.79 7 7 20 -0.83 2.68 -7 -8 28 0.46 5.45 7 8 -28 1.29 3.6 -7 -8 27 4.62 5.64 -7 -8 27 18.39 5.64 7 8 -27 15.43 5.08 7 8 -27 -0.28 3.42 -7 -8 26 2.77 3.7 -7 -8 26 0.28 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2.59 -7 -9 13 56.65 7.3 7 9 -13 53.14 8.5 -7 -9 12 16.36 3.79 -7 -9 12 19.04 4.16 7 9 -12 19.68 5.54 7 9 -12 11 4.71 -7 -9 11 54.52 6.65 -7 -9 11 59.7 7.76 7 9 -11 51.1 7.86 7 9 -11 66.54 10.44 -7 -9 10 8.87 2.68 -7 -9 10 10.35 3.42 7 9 -10 6.93 3.7 7 9 -10 12.94 5.82 -7 -9 9 32.53 4.71 7 9 -9 36.41 6.38 -7 -9 8 78.09 8.22 7 9 -8 88.44 10.44 -7 -9 7 92.78 9.43 -7 -9 6 9.89 3.7 -7 -9 6 12.29 2.96 7 9 -6 16.17 3.97 7 9 -6 11.09 6.38 -7 -9 5 65.98 9.89 -7 -9 5 60.16 7.12 7 9 -5 58.03 7.21 7 9 -5 53.32 12.01 -7 -9 4 15.71 3.33 -7 -9 4 12.57 4.99 7 9 -4 6.01 8.69 7 9 -4 12.38 3.14 -7 -9 3 2.13 1.94 -7 -9 3 -4.53 4.25 7 9 -3 1.2 1.85 7 9 -3 2.22 11.09 -7 -9 2 146.57 13.49 7 9 -2 148.6 13.58 7 9 -2 104.7 24.12 -7 -9 1 20.89 3.97 7 9 -1 19.68 3.7 -7 -9 0 1.29 2.03 7 9 0 1.66 1.85 -7 -9 -1 0.92 1.94 -7 -9 -1 -2.13 5.36 7 9 1 0.55 1.66 7 9 1 13.58 13.49 -7 -9 -2 85.67 14.88 -7 -9 -2 119.4 12.29 7 9 2 113.85 11.27 7 9 2 58.96 19.31 -7 -9 -3 58.4 8.04 -7 -9 -3 50.55 13.31 -7 -9 -4 15.06 11.74 7 9 4 7.21 15.99 -7 -9 -5 21.53 12.2 7 9 5 16.45 16.36 -7 -9 -6 15.16 9.24 -7 -9 -6 39.46 7.58 7 9 6 24.95 4.81 7 9 6 3.7 9.98 -7 -9 -7 16.17 8.87 -7 -9 -7 10.35 4.62 7 9 7 -0.18 8.41 7 9 7 18.57 4.16 -7 -9 -8 77.44 11.55 -7 -9 -8 40.29 11.27 -7 -9 -9 1.66 3.97 -7 -9 -9 1.85 5.36 7 9 9 -0.74 3.05 7 9 9 2.96 2.59 -7 -9 -10 8.87 5.08 -7 -9 -10 6.47 5.45 7 9 10 8.87 3.42 7 9 10 2.31 3.42 -7 -9 -12 -1.11 3.7 -7 -9 -12 -3.33 3.05 7 9 12 0.09 3.05 7 9 12 1.57 2.5 -7 -9 -13 4.9 4.07 -7 -9 -13 4.07 4.44 7 9 13 7.86 3.79 -7 -9 -14 2.13 3.33 7 9 14 3.33 3.33 -7 -9 -15 3.88 3.97 -7 -9 -15 7.12 4.25 7 9 15 3.42 3.51 7 9 15 2.5 3.42 -7 -9 -16 9.89 4.9 -7 -9 -16 2.86 4.07 7 9 16 10.53 4.53 7 9 16 -0.46 3.33 -7 -9 -17 3.7 4.07 -7 -9 -17 0.28 3.6 7 9 17 10.9 4.34 7 9 17 -0.83 3.23 -7 -9 -18 -0.18 4.62 -7 -9 -18 5.64 3.88 7 9 18 2.86 3.6 7 9 18 2.77 4.07 -7 -9 -19 -2.13 3.23 7 9 19 -0.46 3.14 -7 -10 27 -4.9 4.81 7 10 -27 0.65 3.7 -7 -10 26 0.65 3.23 -7 -10 26 0.92 4.71 7 10 -26 2.13 3.7 7 10 -26 -0.83 3.33 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2.86 -7 -10 12 3.05 2.13 7 10 -12 2.96 3.79 7 10 -12 0.74 4.25 -7 -10 11 8.04 3.23 7 10 -11 15.16 5.91 -7 -10 10 17.19 4.25 7 10 -10 17.56 6.56 -7 -10 9 81.05 9.15 -7 -10 9 86.59 10.07 7 10 -9 98.7 11.83 7 10 -9 98.79 13.77 -7 -10 8 0.46 2.5 -7 -10 8 0.55 1.76 7 10 -8 3.42 4.9 7 10 -8 -1.02 2.86 -7 -10 7 38.17 5.36 -7 -10 7 30.59 5.64 7 10 -7 47.22 6.93 7 10 -7 26.89 8.04 -7 -10 6 26.06 4.34 -7 -10 6 27.35 5.64 7 10 -6 36.87 5.91 7 10 -6 24.86 8.32 -7 -10 5 6.84 2.68 -7 -10 5 1.76 3.51 7 10 -5 1.57 7.67 7 10 -5 9.61 3.05 -7 -10 4 42.69 8.41 -7 -10 4 41.12 5.82 7 10 -4 36.41 5.36 7 10 -4 30.22 12.57 -7 -10 3 15.8 6.19 -7 -10 3 14.23 3.42 7 10 -3 12.38 3.23 7 10 -3 20.98 12.48 -7 -10 2 10.35 2.96 -7 -10 2 3.97 5.27 7 10 -2 12.66 12.94 7 10 -2 8.59 2.77 -7 -10 1 14.69 6.38 -7 -10 1 15.62 3.42 7 10 -1 11.74 3.14 7 10 -1 9.06 12.48 -7 -10 0 2.13 5.18 7 10 0 10.17 11.09 -7 -10 -1 28.56 8.78 7 10 1 28.28 13.95 -7 -10 -2 68.29 13.68 -7 -10 -2 50.36 7.86 7 10 2 57.48 7.86 7 10 2 59.7 18.21 -7 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8.87 5.45 7 11 -11 7.12 4.53 -7 -11 10 90.38 10.63 -7 -11 10 92.78 9.61 7 11 -10 87.51 11 7 11 -10 85.02 12.85 -7 -11 9 49.63 7.3 -7 -11 9 59.79 7.12 7 11 -9 56.93 8.32 7 11 -9 49.72 9.61 -7 -11 8 6.56 2.5 -7 -11 8 7.02 3.33 7 11 -8 9.98 3.88 7 11 -8 8.69 5.45 -7 -11 7 3.79 3.23 -7 -11 7 2.59 2.03 7 11 -7 1.29 5.36 7 11 -7 3.88 2.96 -7 -11 6 88.53 11.46 -7 -11 6 115.61 11.46 7 11 -6 120.78 12.57 7 11 -6 84.93 14.97 -7 -11 5 45 6.19 -7 -11 5 48.89 8.78 7 11 -5 29.94 11.74 7 11 -5 39.18 6.01 -7 -11 4 21.53 6.84 -7 -11 4 18.21 3.97 7 11 -4 28.19 12.01 7 11 -4 19.5 3.97 -7 -11 3 1.94 4.62 -7 -11 3 0.37 2.03 7 11 -3 0.46 1.94 7 11 -3 -2.5 10.9 -7 -11 2 145.73 18.48 -7 -11 2 131.59 12.85 7 11 -2 65.98 19.59 7 11 -2 125.03 12.2 -7 -11 1 3.05 2.4 -7 -11 1 5.27 5.64 7 11 -1 2.68 11.55 7 11 -1 4.53 2.4 -7 -11 0 39.28 5.91 -7 -11 0 39.74 9.52 7 11 0 55.45 7.02 7 11 0 30.03 13.4 -7 -11 -1 26.61 8.41 -7 -11 -1 33.92 5.64 7 11 1 15.8 10.9 7 11 1 38.44 5.73 -7 -11 -2 4.99 5.91 -7 -11 -2 1.11 2.31 7 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15.8 -8 -5 -6 110.06 23.93 -8 -5 -7 11.74 4.44 8 5 7 12.66 3.42 8 5 7 5.64 7.3 -8 -5 -8 -12.01 8.69 -8 -5 -8 3.97 3.42 8 5 8 4.71 2.4 8 5 8 -1.02 4.9 -8 -5 -9 37.7 12.66 -8 -5 -9 67.65 10.35 -8 -5 -10 -0.92 3.51 8 5 10 2.59 3.97 -8 -5 -11 1.48 3.6 -8 -5 -11 12.29 5.64 8 5 11 11 3.79 8 5 11 2.5 3.97 -8 -5 -12 2.22 3.51 -8 -5 -12 4.44 4.25 8 5 12 1.2 2.86 8 5 12 -2.22 3.51 -8 -5 -13 22.18 6.19 -8 -5 -13 5.73 3.97 -8 -5 -15 -0.28 4.16 -8 -5 -15 -2.68 3.79 8 5 15 1.11 3.6 -8 -5 -16 0 4.16 -8 -5 -16 -3.51 3.51 8 5 16 1.94 3.7 8 5 16 -0.37 3.33 -8 -5 -17 -1.85 4.16 8 5 17 1.48 3.88 -8 -5 -18 4.71 4.44 -8 -5 -18 1.94 4.44 8 5 18 8.5 4.34 8 5 18 2.22 3.97 -8 -5 -19 -0.65 3.7 -8 -5 -19 0.18 4.16 8 5 19 -0.92 2.86 8 5 19 -0.09 3.79 -8 -5 -20 0.46 4.53 -8 -5 -20 0.65 3.51 8 5 20 2.4 3.42 8 5 20 1.39 4.16 -8 -5 -21 -0.18 6.65 8 5 21 4.34 3.51 -8 -6 29 3.51 5.73 8 6 -29 0.92 3.88 -8 -6 28 0.18 5.36 -8 -6 28 1.76 3.42 8 6 -28 0.83 3.51 8 6 -28 -0.92 3.7 -8 -6 26 0.09 3.14 -8 -6 26 -11.46 5.45 8 6 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21.25 5.08 8 6 4 24.12 4.44 8 6 4 -6.47 15.06 -8 -6 -5 26.15 14.51 -8 -6 -5 16.08 4.99 8 6 5 18.76 4.07 8 6 5 8.87 13.21 -8 -6 -6 20.52 5.54 8 6 6 24.77 4.99 -8 -6 -7 7.21 8.96 -8 -6 -7 10.63 4.44 8 6 7 0.37 6.93 8 6 7 13.31 3.6 -8 -6 -8 27.63 11.09 8 6 8 2.13 5.54 -8 -6 -9 2.5 4.25 -8 -6 -9 -4.16 3.51 8 6 9 -1.85 3.42 8 6 9 1.29 2.03 -8 -6 -10 1.39 3.51 -8 -6 -10 0.28 3.7 8 6 10 0.83 2.31 8 6 10 -0.28 3.51 -8 -6 -12 1.39 3.7 -8 -6 -12 1.02 3.79 8 6 12 1.48 2.86 8 6 12 1.48 3.6 -8 -6 -14 3.14 3.6 -8 -6 -14 6.56 4.71 8 6 14 7.67 3.97 8 6 14 -1.2 3.51 -8 -6 -15 1.66 3.6 -8 -6 -15 1.66 5.08 8 6 15 -2.5 3.97 8 6 15 0.65 3.33 -8 -6 -16 -0.74 4.34 8 6 16 -0.65 3.51 -8 -6 -17 8.96 4.71 -8 -6 -17 0.18 4.25 8 6 17 5.73 4.25 8 6 17 17.56 5.27 -8 -6 -18 5.36 4.81 -8 -6 -18 2.5 4.07 8 6 18 2.59 4.25 8 6 18 9.06 4.34 -8 -6 -19 3.33 3.7 -8 -6 -19 -1.76 4.16 8 6 19 0.65 4.25 8 6 19 0.83 3.14 -8 -6 -20 -0.09 3.6 8 6 20 1.11 2.96 -8 -7 28 -4.44 5.27 8 7 -28 0.46 3.79 -8 -7 27 3.33 5.91 -8 -7 27 15.16 4.99 8 7 -27 4.99 3.88 8 7 -27 14.88 5.08 -8 -7 26 4.16 5.36 -8 -7 26 19.41 5.54 -8 -7 25 -1.11 5.36 -8 -7 25 9.24 4.62 8 7 -25 8.41 4.25 8 7 -25 0.46 3.6 -8 -7 24 20.79 5.45 8 7 -24 22.46 5.82 -8 -7 23 12.38 6.1 -8 -7 23 24.21 5.73 8 7 -23 -1.76 3.14 -8 -7 21 0.83 2.68 -8 -7 21 -0.65 4.62 8 7 -21 3.51 3.23 8 7 -21 -0.09 3.88 -8 -7 20 12.85 3.97 -8 -7 20 7.95 5.54 -8 -7 19 38.07 6.19 -8 -7 19 25.97 6.93 8 7 -18 21.07 8.96 8 7 -18 43.8 7.02 -8 -7 17 42.51 6.19 -8 -7 17 33.64 6.93 8 7 -17 38.81 6.56 8 7 -17 14.69 8.59 -8 -7 16 31.51 5.27 8 7 -16 33.82 6.1 -8 -7 15 20.24 4.25 -8 -7 15 21.16 5.82 8 7 -15 23.75 5.27 8 7 -15 17.93 9.43 -8 -7 14 16.82 4.07 -8 -7 14 16.82 4.99 8 7 -14 22.46 5.54 8 7 -14 25.41 9.61 -8 -7 13 58.59 8.13 -8 -7 13 67 8.96 8 7 -13 73.1 13.86 -8 -7 12 2.4 2.68 8 7 -12 3.42 5.73 -8 -7 11 27.91 4.71 -8 -7 11 23.47 4.71 8 7 -11 25.6 6.65 8 7 -11 23.29 6.28 -8 -7 10 3.14 2.13 -8 -7 10 6.28 2.86 8 7 -10 6.01 3.79 8 7 -10 1.39 3.88 -8 -7 9 54.34 7.21 -8 -7 9 58.59 6.75 8 7 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4.34 -8 -8 5 159.04 18.3 -8 -8 5 186.67 16.54 8 8 -5 169.76 15.99 8 8 -5 120.88 21.72 -8 -8 4 34.65 5.18 -8 -8 4 26.61 7.95 8 8 -4 42.97 15.89 8 8 -4 38.63 5.73 -8 -8 3 6.84 6.38 -8 -8 3 4.25 2.22 8 8 -3 4.71 2.4 8 8 -3 10.35 12.48 -8 -8 2 61.73 7.39 8 8 -2 62.29 7.3 -8 -8 1 133.81 12.75 8 8 -1 138.43 12.94 -8 -8 0 2.96 2.22 8 8 0 2.22 2.13 -8 -8 -1 3.05 6.93 -8 -8 -1 1.2 2.22 8 8 1 3.7 2.13 8 8 1 8.59 12.01 -8 -8 -2 -1.2 1.94 -8 -8 -2 1.2 7.21 8 8 2 0.65 2.03 8 8 2 2.13 11.74 -8 -8 -3 13.21 8.59 -8 -8 -3 5.91 3.33 8 8 3 9.52 3.23 8 8 3 6.84 10.53 -8 -8 -4 12.94 8.22 8 8 4 5.27 9.52 -8 -8 -5 -1.48 3.14 -8 -8 -5 0.28 6.28 8 8 5 3.88 7.21 8 8 5 3.7 2.59 -8 -8 -6 10.53 6.93 -8 -8 -6 27.82 6.65 -8 -8 -7 -2.96 5.36 -8 -8 -7 1.11 3.97 8 8 7 1.94 2.68 8 8 7 0.09 3.42 -8 -8 -8 3.97 4.07 -8 -8 -8 0.37 4.71 8 8 8 -0.18 3.14 8 8 8 4.99 2.96 -8 -8 -10 12.94 5.36 -8 -8 -10 3.05 3.7 -8 -8 -11 1.11 3.51 -8 -8 -11 15.89 5.82 -8 -8 -12 1.02 3.79 8 8 12 0.74 2.5 -8 -8 -13 6.19 4.25 -8 -8 -13 19.59 6.19 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14 27.54 5.36 8 9 -14 18.39 8.22 8 9 -14 29.94 7.39 -8 -9 13 63.67 8.32 -8 -9 13 63.67 8.32 8 9 -13 52.95 10.44 8 9 -13 75.59 11.55 -8 -9 12 57.02 7.86 -8 -9 12 52.86 7.12 8 9 -12 42.88 8.59 8 9 -12 50.18 9.61 -8 -9 11 26.52 5.08 8 9 -11 18.76 6.56 -8 -9 10 2.68 2.59 8 9 -10 3.42 4.81 -8 -9 9 49.35 7.21 -8 -9 9 50.18 7.3 8 9 -9 49.35 8.69 8 9 -9 62.47 10.63 -8 -9 8 15.99 4.53 -8 -9 8 17.74 3.7 8 9 -8 20.24 5.18 8 9 -8 17.19 6.84 -8 -9 7 91.77 9.61 -8 -9 7 84.19 10.81 -8 -9 6 72.45 8.22 -8 -9 6 56.19 9.43 8 9 -6 81.97 9.89 8 9 -6 64.69 14.14 -8 -9 5 5.82 2.5 -8 -9 5 4.44 4.9 8 9 -5 0 9.15 8 9 -5 7.39 3.14 -8 -9 4 10.81 3.14 -8 -9 4 7.76 5.64 8 9 -4 12.01 3.42 8 9 -4 5.54 10.81 -8 -9 3 13.58 3.42 -8 -9 3 8.87 5.73 8 9 -3 13.03 3.42 8 9 -3 -2.03 10.81 -8 -9 2 13.03 3.42 -8 -9 2 11.92 6.28 8 9 -2 -3.6 10.07 8 9 -2 11.09 3.14 -8 -9 1 2.5 2.68 -8 -9 1 8.13 5.36 8 9 -1 4.25 10.07 8 9 -1 4.62 2.59 -8 -9 0 0.55 5.08 8 9 0 0.92 9.06 -8 -9 -1 18.39 7.39 8 9 1 11.46 9.8 -8 -9 -2 22.18 4.71 -8 -9 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5.27 10 7 -25 -0.65 3.88 10 7 -25 3.6 3.7 10 7 -24 17.47 5.64 10 7 -24 0.28 4.16 -10 -7 23 4.07 5.36 -10 -7 23 10.07 4.44 10 7 -23 -1.2 3.7 10 7 -23 4.44 3.88 -10 -7 21 29.66 6.47 -10 -7 21 8.41 5.82 10 7 -21 0.65 3.79 10 7 -21 17.56 5.64 -10 -7 20 7.21 5.73 10 7 -20 2.68 3.97 10 7 -19 8.87 5.54 10 7 -19 31.14 7.58 -10 -7 18 14.79 6.01 -10 -7 18 23.75 5.82 10 7 -18 4.62 5.27 10 7 -18 20.98 6.28 -10 -7 17 3.42 4.16 -10 -7 17 1.29 3.05 10 7 -17 4.16 5.64 10 7 -17 -1.29 4.07 -10 -7 16 56.93 8.78 -10 -7 16 32.9 7.67 -10 -7 15 12.57 4.34 -10 -7 15 10.44 5.45 10 7 -15 0.74 4.81 10 7 -15 6.93 5.08 -10 -7 14 9.52 3.88 -10 -7 14 4.07 4.81 10 7 -14 1.11 5.36 10 7 -14 11 5.27 -10 -7 13 17.19 4.81 -10 -7 13 21.62 6.38 10 7 -13 14.14 6.65 10 7 -13 15.16 5.91 -10 -7 12 4.53 3.23 -10 -7 12 1.39 3.7 10 7 -12 3.14 4.44 10 7 -12 -1.57 5.36 -10 -7 11 1.76 3.05 10 7 -11 -3.7 4.25 -10 -7 10 40.85 7.86 10 7 -10 23.38 6.93 -10 -7 9 12.38 4.9 10 7 -9 7.67 5.36 10 7 -9 9.06 5.54 -10 -7 8 4.81 4.07 -10 -7 8 9.8 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18 2.86 4.71 10 8 -18 2.59 4.53 10 8 -18 3.79 5.18 -10 -8 17 2.13 3.6 -10 -8 17 7.21 4.71 10 8 -17 4.71 5.64 10 8 -17 5.45 4.44 -10 -8 16 15.25 4.99 -10 -8 16 16.82 5.73 10 8 -16 10.17 5.54 10 8 -16 7.12 5.91 -10 -8 15 0.09 4.16 -10 -8 15 4.25 3.51 10 8 -15 3.7 4.44 10 8 -15 5.54 5.36 -10 -8 14 18.57 5.27 -10 -8 14 20.42 6.38 10 8 -14 12.38 6.28 10 8 -14 3.23 4.99 -10 -8 13 4.34 3.6 -10 -8 13 10.07 4.99 10 8 -13 -0.46 4.62 10 8 -13 4.16 5.27 -10 -8 12 4.81 3.6 -10 -8 12 0.37 3.33 10 8 -12 0.28 4.07 10 8 -12 -1.39 4.53 -10 -8 11 22.83 5.45 -10 -8 11 18.02 5.36 10 8 -11 6.75 4.99 10 8 -11 16.82 6.56 -10 -8 10 22.09 5.18 -10 -8 10 16.17 5.36 10 8 -10 5.54 5.18 10 8 -10 13.49 6.01 -10 -8 9 -1.2 2.4 -10 -8 9 -2.13 3.7 10 8 -9 -3.05 62.38 10 8 -9 3.23 4.34 -10 -8 8 9.24 3.6 -10 -8 8 4.71 4.44 10 8 -8 8.78 4.81 10 8 -8 -0.09 4.53 -10 -8 7 0.74 2.86 -10 -8 7 4.07 4.53 10 8 -7 1.57 4.07 10 8 -7 2.4 4.71 -10 -8 5 24.4 5.27 -10 -8 5 14.05 5.73 -10 -8 4 2.31 4.25 -10 -8 4 4.44 2.96 10 8 -4 -0.46 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4.07 10 8 13 -0.37 3.7 10 8 13 11.55 5.18 -10 -8 -14 10.35 4.9 10 8 14 6.01 4.07 -10 -9 24 5.27 5.82 10 9 -24 4.07 4.25 -10 -9 23 0.28 5.08 -10 -9 23 4.71 3.88 10 9 -23 -1.85 3.51 10 9 -23 4.07 4.07 -10 -9 22 6.75 5.27 -10 -9 22 23.47 6.19 10 9 -22 0.83 3.88 10 9 -22 14.97 5.36 -10 -9 21 0.09 4.99 -10 -9 21 6.65 4.25 10 9 -21 -4.25 4.53 10 9 -21 3.51 4.25 -10 -9 20 12.11 6.28 -10 -9 20 27.63 6.56 -10 -9 19 0.92 4.81 -10 -9 19 0.28 3.33 10 9 -19 -2.86 3.51 10 9 -19 2.68 5.54 -10 -9 18 10.44 4.9 -10 -9 18 -0.55 4.9 10 9 -18 4.53 5.54 10 9 -18 7.49 5.08 -10 -9 17 4.25 3.51 -10 -9 17 9.61 5.08 10 9 -17 -1.85 4.99 10 9 -17 4.53 4.99 -10 -9 16 1.11 4.16 10 9 -16 -0.28 4.62 10 9 -16 10.9 5.36 -10 -9 15 4.81 4.07 -10 -9 15 -2.13 3.14 10 9 -15 -1.85 4.71 10 9 -15 -2.22 4.25 -10 -9 14 23.1 6.19 -10 -9 14 20.33 5.45 10 9 -14 14.69 5.73 10 9 -14 10.53 6.19 -10 -9 13 34.65 7.21 -10 -9 13 27.54 6.28 10 9 -13 15.62 6.19 10 9 -13 18.57 7.02 -10 -9 12 17.56 5.27 -10 -9 12 22.18 5.54 10 9 -12 9.06 5.73 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9 0.37 3.7 12 11 -9 -1.66 4.16 12 11 -9 -3.14 4.16 -12 -11 8 2.86 4.34 -12 -11 8 -1.66 3.23 12 11 -8 -3.7 4.16 12 11 -8 -3.79 3.97 -12 -11 7 -1.48 3.79 -12 -11 7 -1.85 4.16 12 11 -7 -1.48 4.44 12 11 -7 -1.48 4.53 -12 -11 6 -1.57 3.33 -12 -11 6 -1.48 4.07 12 11 -6 -0.46 4.62 12 11 -6 4.25 4.53 -12 -11 5 2.5 4.62 -12 -11 5 9.24 4.81 12 11 -5 -0.46 4.25 12 11 -5 9.06 5.36 -12 -11 4 2.96 5.08 -12 -11 4 5.08 4.16 12 11 -4 -0.65 4.53 12 11 -4 2.68 4.44 -12 -11 3 7.39 4.62 -12 -11 3 4.71 5.36 12 11 -3 0.37 4.62 12 11 -3 3.97 4.71 -12 -11 2 3.79 3.97 -12 -11 2 3.14 4.9 12 11 -2 -0.28 3.79 12 11 -2 0.74 4.34 -12 -11 1 -0.92 3.6 12 11 -1 -3.51 3.97 12 11 -1 1.11 3.6 -12 -11 0 5.18 4.34 12 11 0 6.47 4.44 -12 -11 -1 11.09 4.81 12 11 1 7.67 5.08 -12 -12 10 0.55 3.88 12 12 -10 1.39 4.53 -12 -12 9 7.02 4.44 12 12 -9 2.13 4.71 -12 -12 8 3.51 4.07 12 12 -8 2.4 4.44 -12 -12 7 5.64 4.16 12 12 -7 -0.83 4.25 -12 -12 6 3.79 4.07 12 12 -6 -1.76 4.07 -12 -12 5 32.71 7.76 12 12 -5 18.3 6.75