#------------------------------------------------------------------------------ #$Date: 2019-12-13 10:28:38 +0200 (Fri, 13 Dec 2019) $ #$Revision: 245048 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/65/1556549.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556549 loop_ _publ_author_name 'Van de Watering, F.F.' 'Heijtbrink, N.' 'Van der Vlugt, J.I.' 'Dzik, W.I.' 'De Bruin, B.' 'Reek, J.N.H.' _publ_section_title ; 3-Methylindole-Based Tripodal Tetraphosphine Ruthenium Complexes in N2 Coordination and Reduction and Formic Acid Dehydrogenation ; _journal_name_full Inorganics _journal_page_first 73 _journal_paper_doi 10.3390/inorganics5040073 _journal_volume 5 _journal_year 2017 _chemical_formula_sum 'C69 H45 F18 N5 P4 Ru' _chemical_formula_weight 1511.05 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _cell_angle_alpha 90 _cell_angle_beta 97.011(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 14.2851(6) _cell_length_b 18.9090(8) _cell_length_c 29.8721(12) _cell_measurement_reflns_used 9441 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 26.3776 _cell_measurement_theta_min 2.3650 _cell_volume 8008.6(6) _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _diffrn_ambient_temperature 150(2) _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.983 _diffrn_measurement_device_type 'Bruker D8 Quest ECO PHOTON 50' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0702 _diffrn_reflns_av_unetI/netI 0.0442 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.983 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 37 _diffrn_reflns_limit_l_min -37 _diffrn_reflns_number 111783 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.983 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.450 _diffrn_reflns_theta_min 2.261 _diffrn_source 'sealed tube' _exptl_absorpt_coefficient_mu 0.356 _exptl_absorpt_correction_T_max 0.88 _exptl_absorpt_correction_T_min 0.72 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2014/5 (Bruker AXS Inc.)' _exptl_crystal_colour dark-red _exptl_crystal_density_diffrn 1.253 _exptl_crystal_description block _exptl_crystal_F_000 3040 _exptl_crystal_size_max 0.621 _exptl_crystal_size_mid 0.406 _exptl_crystal_size_min 0.362 _refine_diff_density_max 1.238 _refine_diff_density_min -0.786 _refine_diff_density_rms 0.097 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.436 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 877 _refine_ls_number_reflns 16238 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.436 _refine_ls_R_factor_all 0.0880 _refine_ls_R_factor_gt 0.0666 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1867 _refine_ls_wR_factor_ref 0.2002 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 12710 _reflns_number_total 16240 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file FF471_0m_a_sq.cif _cod_data_source_block FF471_0m_a_sq _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 1556549 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.809 _shelx_estimated_absorpt_t_max 0.882 _shelx_res_file ; FF471_0m_a_sq.res created by SHELXL-2014/7 TITL FF471_0m_a.res in P2(1)/c CELL 0.71073 14.2851 18.9090 29.8721 90.000 97.011 90.000 ZERR 4.000 0.0006 0.0008 0.0012 0.000 0.002 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N F P Ru UNIT 276 180 20 72 16 4 REM Old TITL FF471_0m in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.184, Rweak 0.015, Alpha 0.061, Orientation as input REM Formula found by SHELXT: C67 N11 O4 F12 P4 Ru L.S. 5 0 145 BOND $H FMAP 2 PLAN 20 SIZE 0.362 0.406 0.621 ABIN ACTA OMIT 0 2 2 OMIT 0 2 1 WGHT 0.100000 FVAR 0.22010 RU1 6 0.647649 0.698553 0.651959 11.00000 0.02144 0.01601 = 0.01476 -0.00060 0.00119 -0.00060 P1 5 0.493837 0.684398 0.625079 11.00000 0.02008 0.02358 = 0.01644 -0.00222 0.00223 0.00162 P4 5 0.671407 0.690310 0.580097 11.00000 0.02066 0.01757 = 0.01522 -0.00027 0.00143 0.00000 P3 5 0.741875 0.602676 0.661628 11.00000 0.02492 0.01603 = 0.01796 0.00134 0.00312 -0.00111 P2 5 0.716501 0.806259 0.648265 11.00000 0.02579 0.01732 = 0.02126 -0.00143 0.00210 -0.00092 N3 3 0.793377 0.588069 0.612494 11.00000 0.02245 0.02072 = 0.02198 0.00141 0.00289 0.00455 N1 3 0.484603 0.664332 0.567724 11.00000 0.02328 0.02448 = 0.01727 -0.00595 -0.00310 0.00099 F9 4 0.196859 0.437444 0.694879 11.00000 0.05111 0.09025 = 0.07647 0.03911 0.00751 -0.02505 N2 3 0.734418 0.823420 0.592776 11.00000 0.02682 0.01836 = 0.02469 0.00423 -0.00101 -0.00563 N4 3 0.629779 0.706217 0.719386 11.00000 0.02437 0.01804 = 0.02037 0.00060 -0.00231 -0.00089 F6 4 0.501683 0.326834 0.733092 11.00000 0.08861 0.07100 = 0.07213 0.03224 -0.00599 -0.04216 F8 4 0.227370 0.396236 0.631696 11.00000 0.07587 0.05792 = 0.09390 0.00014 -0.00131 -0.03495 C42 1 0.423872 0.609808 0.642761 11.00000 0.01955 0.03192 = 0.01994 0.00335 -0.00181 -0.00513 F12 4 0.263831 0.993788 0.607059 11.00000 0.12621 0.04938 = 0.08671 0.03329 0.05213 0.04625 F7 4 0.320844 0.376020 0.693201 11.00000 0.06482 0.06915 = 0.14214 0.06747 -0.00258 -0.01387 F5 4 0.502068 0.298029 0.663816 11.00000 0.11440 0.05425 = 0.07184 0.00683 -0.01756 -0.05043 C63 1 0.833776 0.821093 0.679117 11.00000 0.02706 0.01503 = 0.03170 -0.00569 -0.00006 -0.00183 C49 1 0.411489 0.758035 0.625821 11.00000 0.01640 0.02811 = 0.02752 -0.00114 0.00147 0.00220 C18 1 0.410702 0.633089 0.540014 11.00000 0.02776 0.01978 = 0.02044 -0.00120 -0.00270 -0.00151 C10 1 0.567373 0.654805 0.546413 11.00000 0.02501 0.01901 = 0.02199 -0.00067 0.00336 0.00409 C35 1 0.692084 0.515509 0.672539 11.00000 0.03129 0.01666 = 0.02035 0.00479 -0.00269 -0.00206 C13 1 0.446784 0.604654 0.502288 11.00000 0.03141 0.02360 = 0.02162 -0.00232 -0.00066 -0.00152 C69 1 0.914048 0.832501 0.658339 11.00000 0.02950 0.03051 = 0.02978 0.00228 0.00157 -0.00263 AFIX 43 H69 2 0.908925 0.836497 0.627105 11.00000 -1.20000 AFIX 0 F4 4 0.618774 0.271564 0.714128 11.00000 0.09876 0.03359 = 0.15567 0.03553 -0.01935 -0.01431 C28 1 0.847260 0.601813 0.703582 11.00000 0.02280 0.01782 = 0.02369 -0.00557 -0.00044 0.00263 C27 1 0.752311 0.887151 0.572193 11.00000 0.02854 0.02144 = 0.03379 0.00901 0.00249 -0.00412 C47 1 0.451377 0.542399 0.630729 11.00000 0.02922 0.03100 = 0.02511 -0.00301 0.00422 -0.00310 AFIX 43 H47 2 0.504741 0.537212 0.616041 11.00000 -1.20000 AFIX 0 C2 1 0.837785 0.625825 0.545585 11.00000 0.02862 0.03330 = 0.02267 -0.00479 0.00353 -0.00125 C9 1 0.875873 0.551801 0.605973 11.00000 0.02903 0.02634 = 0.02537 -0.00688 0.00093 0.00145 C40 1 0.703732 0.455356 0.646736 11.00000 0.04916 0.02612 = 0.02853 -0.00292 -0.00498 -0.00202 AFIX 43 H40 2 0.741155 0.457264 0.623380 11.00000 -1.20000 AFIX 0 C1 1 0.772056 0.633371 0.574651 11.00000 0.02201 0.02162 = 0.02167 -0.00282 -0.00014 0.00149 C46 1 0.401227 0.483697 0.640150 11.00000 0.03670 0.03022 = 0.03077 0.00192 -0.00310 -0.00427 AFIX 43 H46 2 0.420053 0.439273 0.631316 11.00000 -1.20000 AFIX 0 C11 1 0.545897 0.618356 0.506751 11.00000 0.02756 0.02279 = 0.02182 -0.00467 0.00190 0.00084 C4 1 0.902884 0.573910 0.564345 11.00000 0.02746 0.03418 = 0.02636 -0.00995 0.00576 0.00128 C26 1 0.788375 0.950478 0.591287 11.00000 0.04551 0.02227 = 0.04216 0.00807 0.00429 -0.00931 AFIX 43 H26 2 0.804056 0.955362 0.622273 11.00000 -1.20000 AFIX 0 C8 1 0.926555 0.501477 0.632387 11.00000 0.04226 0.02998 = 0.03512 -0.00255 0.00083 0.01526 AFIX 43 H8 2 0.907137 0.486192 0.659373 11.00000 -1.20000 AFIX 0 C54 1 0.370162 0.792964 0.586867 11.00000 0.04274 0.03482 = 0.02223 -0.00350 0.00162 0.00164 AFIX 43 H54 2 0.378694 0.775347 0.558581 11.00000 -1.20000 AFIX 0 F16 4 1.153959 0.893049 0.746293 11.00000 0.07292 0.08819 = 0.19849 0.06192 -0.07501 -0.04984 C50 1 0.397004 0.785176 0.667654 11.00000 0.04516 0.03291 = 0.02462 -0.00531 0.00382 0.00590 AFIX 43 H50 2 0.424890 0.763137 0.693765 11.00000 -1.20000 AFIX 0 F11 4 0.261234 0.975732 0.674965 11.00000 0.20609 0.06200 = 0.06776 -0.00748 0.02078 0.07346 C17 1 0.315369 0.627015 0.546044 11.00000 0.02708 0.04026 = 0.02567 -0.00387 0.00085 0.00040 AFIX 43 H17 2 0.291684 0.646453 0.570958 11.00000 -1.20000 AFIX 0 N5 3 0.625480 0.709673 0.754617 11.00000 0.06973 0.04130 = 0.03010 -0.00026 0.01459 -0.00014 C33 1 0.923042 0.644447 0.695835 11.00000 0.03560 0.02029 = 0.03170 0.00537 -0.00156 0.00177 AFIX 43 H33 2 0.917481 0.674123 0.670824 11.00000 -1.20000 AFIX 0 C36 1 0.636007 0.510969 0.706897 11.00000 0.04189 0.02770 = 0.03676 0.00271 0.00621 -0.00430 AFIX 43 H36 2 0.626667 0.551251 0.723656 11.00000 -1.20000 AFIX 0 C20 1 0.691035 0.809378 0.517357 11.00000 0.03165 0.03205 = 0.02684 0.00964 0.00175 -0.00093 C32 1 1.006584 0.643458 0.724714 11.00000 0.02612 0.02731 = 0.04693 -0.00351 -0.00409 -0.00078 AFIX 43 H32 2 1.057103 0.671470 0.718724 11.00000 -1.20000 AFIX 0 C19 1 0.697774 0.776023 0.558128 11.00000 0.02309 0.02348 = 0.02314 0.00105 -0.00134 0.00213 C64 1 0.843738 0.813600 0.726432 11.00000 0.03833 0.02997 = 0.02802 -0.00166 0.00399 -0.00336 AFIX 43 H64 2 0.791181 0.803854 0.740940 11.00000 -1.20000 AFIX 0 F10 4 0.156224 0.934783 0.630635 11.00000 0.04936 0.04229 = 0.35188 -0.01453 0.04477 0.01735 F13 4 0.428245 1.068867 0.698240 11.00000 0.20377 0.07582 = 0.18674 0.03026 0.14083 0.07105 C43 1 0.346169 0.615642 0.666444 11.00000 0.03262 0.03769 = 0.03639 0.01206 0.00856 0.00708 AFIX 43 H43 2 0.327377 0.659712 0.675906 11.00000 -1.20000 AFIX 0 C52 1 0.301858 0.878667 0.632353 11.00000 0.03185 0.02711 = 0.04207 0.00022 0.00852 0.00404 C51 1 0.341239 0.844993 0.671016 11.00000 0.03640 0.03604 = 0.03500 -0.00621 0.01221 0.00572 AFIX 43 H51 2 0.330700 0.862044 0.699171 11.00000 -1.20000 AFIX 0 C62 1 0.573359 0.904002 0.630279 11.00000 0.03946 0.02725 = 0.04719 0.00048 0.00450 -0.00629 AFIX 43 H62 2 0.553294 0.873012 0.606888 11.00000 -1.20000 AFIX 0 C53 1 0.317120 0.853075 0.590209 11.00000 0.05052 0.03065 = 0.03257 0.00796 0.00143 0.01126 AFIX 43 H53 2 0.291447 0.876611 0.564240 11.00000 -1.20000 AFIX 0 C5 1 0.985555 0.546025 0.550139 11.00000 0.03698 0.05138 = 0.03241 -0.00703 0.00792 0.01144 AFIX 43 H5 2 1.006030 0.560893 0.523294 11.00000 -1.20000 AFIX 0 C3 1 0.845977 0.663583 0.502391 11.00000 0.03685 0.05774 = 0.02969 0.00376 0.01415 0.00927 AFIX 137 H3A 2 0.815411 0.708762 0.502718 11.00000 -1.50000 H3B 2 0.816416 0.636010 0.477615 11.00000 -1.50000 H3C 2 0.911374 0.670277 0.499041 11.00000 -1.50000 AFIX 0 C22 1 0.727576 0.879705 0.525754 11.00000 0.03011 0.02763 = 0.03541 0.01046 0.00402 0.00055 C56 1 0.653867 0.888097 0.659957 11.00000 0.03456 0.01237 = 0.03587 0.00556 0.00679 0.00449 C38 1 0.604934 0.389577 0.691141 11.00000 0.04906 0.02695 = 0.04443 0.01111 -0.01651 -0.01328 C68 1 1.001295 0.837992 0.683371 11.00000 0.02661 0.03944 = 0.04149 0.00130 0.00083 -0.00226 AFIX 43 H68 2 1.054654 0.845023 0.668935 11.00000 -1.20000 AFIX 0 C39 1 0.659554 0.392952 0.655954 11.00000 0.05830 0.02224 = 0.04105 -0.00352 -0.01215 -0.00637 AFIX 43 H39 2 0.666523 0.353054 0.638459 11.00000 -1.20000 AFIX 0 C6 1 1.035334 0.496416 0.576745 11.00000 0.04348 0.06275 = 0.04861 -0.01490 0.00720 0.02401 AFIX 43 H6 2 1.089379 0.476935 0.567282 11.00000 -1.20000 AFIX 0 C21 1 0.653431 0.782060 0.471475 11.00000 0.06045 0.04786 = 0.02190 0.01021 -0.00263 -0.00544 AFIX 137 H21A 2 0.705078 0.770942 0.454936 11.00000 -1.50000 H21B 2 0.614471 0.817537 0.455542 11.00000 -1.50000 H21C 2 0.616698 0.740234 0.474609 11.00000 -1.50000 AFIX 0 C61 1 0.523014 0.965683 0.635392 11.00000 0.03206 0.02324 = 0.08029 0.00715 0.00920 0.00344 AFIX 43 H61 2 0.470274 0.976651 0.615154 11.00000 -1.20000 AFIX 0 C30 1 0.937973 0.560057 0.771736 11.00000 0.05056 0.04445 = 0.03442 0.01378 -0.00820 0.00013 AFIX 43 H30 2 0.942241 0.532394 0.797647 11.00000 -1.20000 AFIX 0 C14 1 0.386154 0.568660 0.469464 11.00000 0.03835 0.04458 = 0.02400 -0.01202 -0.00330 -0.00526 AFIX 43 H14 2 0.408796 0.549750 0.444131 11.00000 -1.20000 AFIX 0 C29 1 0.856022 0.560779 0.742659 11.00000 0.03600 0.04043 = 0.02848 0.00833 -0.00307 -0.00386 AFIX 43 H29 2 0.805276 0.533385 0.749102 11.00000 -1.20000 AFIX 0 C12 1 0.609035 0.595348 0.473307 11.00000 0.03775 0.05313 = 0.02584 -0.01707 0.00424 0.00158 AFIX 137 H12A 2 0.597682 0.624174 0.446745 11.00000 -1.50000 H12B 2 0.596472 0.546752 0.465434 11.00000 -1.50000 H12C 2 0.673624 0.600296 0.486198 11.00000 -1.50000 AFIX 0 C45 1 0.323058 0.490074 0.662636 11.00000 0.03471 0.04499 = 0.03218 0.01647 -0.00794 -0.00796 C7 1 1.007496 0.474563 0.617188 11.00000 0.05130 0.05040 = 0.04399 -0.00663 -0.00314 0.02146 AFIX 43 H7 2 1.043523 0.441272 0.634548 11.00000 -1.20000 AFIX 0 C57 1 0.681492 0.933371 0.695079 11.00000 0.04283 0.03289 = 0.04312 -0.01108 0.00203 0.00195 AFIX 43 H57 2 0.734766 0.923238 0.715180 11.00000 -1.20000 AFIX 0 C37 1 0.593190 0.448367 0.717227 11.00000 0.04077 0.03598 = 0.04181 0.01317 0.00095 -0.01174 AFIX 43 H37 2 0.557372 0.446005 0.741175 11.00000 -1.20000 AFIX 0 C66 1 1.009992 0.833066 0.730202 11.00000 0.03020 0.02242 = 0.04267 -0.00379 -0.00822 -0.00046 F18 4 1.159313 0.786468 0.751304 11.00000 0.07039 0.07774 = 0.27259 -0.04297 -0.09632 0.02513 C55 1 0.245220 0.945149 0.635651 11.00000 0.04782 0.02853 = 0.06224 -0.00239 0.01212 0.00799 C44 1 0.296588 0.554874 0.675909 11.00000 0.03197 0.05598 = 0.04698 0.01996 0.01292 0.00593 AFIX 43 H44 2 0.244477 0.558935 0.691599 11.00000 -1.20000 AFIX 0 C58 1 0.629087 0.995053 0.700583 11.00000 0.05569 0.03260 = 0.07504 -0.02218 0.01438 -0.00169 AFIX 43 H58 2 0.647130 1.025331 0.724627 11.00000 -1.20000 AFIX 0 C23 1 0.739651 0.936102 0.496976 11.00000 0.05165 0.04545 = 0.04444 0.02660 0.00182 -0.00575 AFIX 43 H23 2 0.723185 0.931590 0.466015 11.00000 -1.20000 AFIX 0 C15 1 0.292809 0.561848 0.475404 11.00000 0.03916 0.05526 = 0.03673 -0.01196 -0.00661 -0.01568 AFIX 43 H15 2 0.252135 0.537681 0.453990 11.00000 -1.20000 AFIX 0 C31 1 1.014576 0.600352 0.762736 11.00000 0.03540 0.03429 = 0.03890 -0.00370 -0.01120 0.00435 C65 1 0.930922 0.820662 0.751176 11.00000 0.03613 0.03556 = 0.03315 -0.00734 -0.00786 0.00096 AFIX 43 H65 2 0.936554 0.817019 0.782437 11.00000 -1.20000 AFIX 0 C25 1 0.799631 1.005410 0.562025 11.00000 0.05028 0.02684 = 0.06518 0.01499 -0.00027 -0.01102 AFIX 43 H25 2 0.823356 1.048347 0.573596 11.00000 -1.20000 AFIX 0 C48 1 0.268063 0.425528 0.670832 11.00000 0.04121 0.04779 = 0.07335 0.02546 0.00003 -0.00894 C67 1 1.105025 0.839088 0.756687 11.00000 0.04577 0.03900 = 0.05586 -0.00532 -0.02032 -0.00474 C59 1 0.552009 1.010472 0.670761 11.00000 0.04043 0.01968 = 0.07980 -0.00150 0.02500 0.00109 C16 1 0.258076 0.590585 0.513025 11.00000 0.02958 0.04969 = 0.03331 -0.00115 -0.00483 -0.01048 AFIX 43 H16 2 0.194460 0.585152 0.516075 11.00000 -1.20000 AFIX 0 F17 4 1.104163 0.844526 0.799387 11.00000 0.05484 0.36444 = 0.06337 -0.02965 -0.02065 -0.03844 C41 1 0.559062 0.320587 0.699870 11.00000 0.06961 0.03832 = 0.06511 0.01886 -0.02523 -0.02469 F14 4 0.451636 1.101330 0.639106 11.00000 0.24301 0.10984 = 0.16551 0.04808 0.08522 0.13321 C24 1 0.776059 0.998118 0.514968 11.00000 0.06154 0.03686 = 0.06178 0.02936 0.00252 -0.00746 AFIX 43 H24 2 0.785397 1.035861 0.496050 11.00000 -1.20000 AFIX 0 F1 4 1.177628 0.608295 0.773747 11.00000 0.04173 0.35774 = 0.11318 0.04276 -0.02137 0.02295 C34 1 1.103560 0.596383 0.793160 11.00000 0.03781 0.07484 = 0.05916 0.00959 -0.02135 0.00241 C60 1 0.497965 1.077174 0.676800 11.00000 0.07821 0.01879 = 0.12830 0.00770 0.03893 0.00929 F3 4 1.116533 0.647293 0.820229 11.00000 0.11396 0.30639 = 0.17727 -0.13535 -0.09904 0.05570 F2 4 1.116617 0.544477 0.815370 11.00000 0.12846 0.21598 = 0.36147 0.21356 -0.18103 -0.08334 F15 4 0.545949 1.126464 0.691454 11.00000 0.10014 0.04821 = 0.65400 -0.14166 -0.08012 0.03575 HKLF 4 REM FF471_0m_a.res in P2(1)/c REM R1 = 0.0666 for 12709 Fo > 4sig(Fo) and 0.0880 for all 16238 data REM 877 parameters refined using 0 restraints END WGHT 0.0445 40.0263 REM Highest difference peak 1.238, deepest hole -0.786, 1-sigma level 0.097 Q1 1 1.1543 0.5390 0.7781 11.00000 0.05 1.24 Q2 1 0.5179 1.0930 0.7295 11.00000 0.05 1.19 Q3 1 0.5282 1.1274 0.6617 11.00000 0.05 1.00 Q4 1 0.6781 0.7380 0.6583 11.00000 0.05 0.98 Q5 1 0.5495 1.1292 0.6679 11.00000 0.05 0.93 Q6 1 1.0856 0.5842 0.8318 11.00000 0.05 0.93 Q7 1 0.6311 0.2572 0.6792 11.00000 0.05 0.92 Q8 1 0.6132 0.7359 0.6521 11.00000 0.05 0.87 Q9 1 1.1531 0.6451 0.7937 11.00000 0.05 0.87 Q10 1 0.1806 0.9525 0.5928 11.00000 0.05 0.87 Q11 1 0.6838 0.6586 0.6545 11.00000 0.05 0.86 Q12 1 1.1837 0.6183 0.7635 11.00000 0.05 0.85 Q13 1 0.6111 0.6588 0.6483 11.00000 0.05 0.81 Q14 1 1.1173 0.7947 0.7857 11.00000 0.05 0.78 Q15 1 0.7209 0.6980 0.6807 11.00000 0.05 0.76 Q16 1 0.2006 0.9490 0.6619 11.00000 0.05 0.75 Q17 1 1.1742 0.8389 0.7358 11.00000 0.05 0.70 Q18 1 0.5573 0.6973 0.6568 11.00000 0.05 0.68 Q19 1 0.5749 0.6946 0.6218 11.00000 0.05 0.62 Q20 1 1.1671 0.8909 0.7380 11.00000 0.05 0.61 ; _shelx_res_checksum 92700 _shelx_hkl_file ; 2 0 0 516.05 23.30 2 0 0 589.04 23.70 3 0 0 2253.77 92.49 3 0 0 2260.17 91.99 3 0 0 2220.48 92.19 -3 0 0 2286.57 92.99 -3 0 0 2206.08 91.69 -4 0 0 574.84 24.70 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12.60 12.90 -13 4 0 7.80 14.10 -13 4 0 10.50 7.30 13 4 0 1.70 15.60 13 4 0 10.70 10.10 13 4 0 0.60 7.40 14 -4 0 10.10 12.30 -14 -4 0 34.30 13.80 14 -4 0 2.50 7.30 -14 -4 0 9.50 7.30 14 -4 0 7.00 11.40 -14 4 0 18.80 7.60 -14 4 0 30.90 12.80 14 4 0 17.30 10.30 14 4 0 -3.40 15.00 14 4 0 -7.50 7.30 15 -4 0 -16.40 11.70 -15 -4 0 -10.80 6.80 -15 -4 0 24.70 13.20 -15 4 0 -7.80 6.40 15 4 0 4.20 10.10 -15 4 0 21.60 12.50 -16 -4 0 -1.90 7.00 16 -4 0 -0.60 12.60 16 4 0 4.00 9.70 -16 4 0 1.80 7.40 -17 -4 0 20.20 8.30 17 -4 0 32.20 13.20 -17 4 0 22.80 8.70 17 4 0 33.00 11.50 0 -5 0 -8.80 2.00 0 5 0 -9.60 2.90 0 5 0 -7.50 2.60 -1 -5 0 253.27 11.20 1 -5 0 229.58 11.10 -1 -5 0 247.68 11.40 1 -5 0 244.18 11.60 1 5 0 235.98 10.80 1 5 0 214.48 12.20 1 5 0 239.98 11.40 -1 5 0 254.87 12.50 -1 5 0 223.88 11.10 -1 5 0 233.98 11.30 2 -5 0 39.00 3.90 2 -5 0 37.10 4.70 -2 -5 0 40.50 3.70 -2 -5 0 27.00 4.40 -2 5 0 36.50 3.50 2 5 0 39.90 4.20 -2 5 0 35.20 3.90 -2 5 0 43.80 7.80 -3 -5 0 258.97 12.40 -3 -5 0 261.17 13.30 3 -5 0 272.07 12.70 3 -5 0 265.87 13.60 3 -5 0 263.67 12.30 3 5 0 282.77 12.40 -3 5 0 257.37 12.40 3 5 0 262.27 12.70 -3 5 0 268.77 15.50 3 5 0 250.27 14.70 4 -5 0 108.59 7.30 -4 -5 0 86.79 6.70 -4 -5 0 85.09 8.80 4 -5 0 92.49 8.30 4 -5 0 97.89 7.80 -4 5 0 100.49 7.00 -4 5 0 113.19 13.70 4 5 0 91.59 6.80 4 5 0 93.09 7.50 4 5 0 64.99 10.90 5 -5 0 30.90 7.60 5 -5 0 27.90 6.10 -5 -5 0 31.70 5.00 5 5 0 21.30 6.30 -5 5 0 39.20 12.80 5 5 0 37.40 6.10 -5 5 0 20.70 4.90 6 -5 0 39.60 7.00 6 -5 0 44.30 9.50 -6 -5 0 46.90 6.60 6 -5 0 35.40 6.90 -6 -5 0 15.70 9.30 6 5 0 33.70 7.20 -6 5 0 23.50 13.50 6 5 0 10.10 14.40 6 5 0 31.90 5.80 -6 5 0 32.50 5.60 -7 -5 0 132.39 9.10 7 -5 0 143.59 12.70 7 -5 0 140.99 11.10 -7 -5 0 96.79 13.80 7 -5 0 134.19 11.80 7 5 0 131.69 10.80 -7 5 0 102.59 18.20 7 5 0 125.09 11.20 -7 5 0 138.89 10.10 7 5 0 125.89 17.80 8 -5 0 183.18 13.80 8 -5 0 172.68 13.20 8 -5 0 178.48 12.10 -8 -5 0 139.19 13.70 -8 -5 0 178.08 10.70 -8 5 0 146.69 18.00 8 5 0 175.08 11.80 8 5 0 157.48 18.70 8 5 0 151.98 12.20 -8 5 0 193.78 11.50 -9 -5 0 6.70 9.10 9 -5 0 5.80 12.10 9 -5 0 12.60 5.60 9 -5 0 9.50 7.00 -9 -5 0 9.00 5.10 9 5 0 6.60 6.40 9 5 0 12.00 11.30 -9 5 0 13.20 4.80 9 5 0 15.60 5.90 -9 5 0 5.60 10.90 10 -5 0 115.89 13.60 10 -5 0 99.19 11.40 -10 -5 0 122.69 10.50 10 -5 0 123.09 13.70 -10 -5 0 105.29 15.50 10 5 0 117.79 20.60 -10 5 0 102.09 18.50 -10 5 0 133.29 10.20 10 5 0 112.89 12.50 10 5 0 103.59 10.90 -11 -5 0 194.38 17.90 11 -5 0 221.48 19.00 11 -5 0 202.48 15.20 11 -5 0 212.88 18.00 -11 -5 0 199.48 14.30 11 5 0 185.38 18.90 -11 5 0 212.48 14.80 11 5 0 207.78 14.80 -11 5 0 219.48 20.80 11 5 0 215.88 22.40 12 -5 0 26.90 10.70 -12 -5 0 28.60 9.20 -12 -5 0 9.40 11.40 12 -5 0 23.30 7.80 12 -5 0 21.80 10.30 -12 5 0 33.30 14.90 -12 5 0 20.70 7.00 12 5 0 11.60 13.80 12 5 0 15.60 7.70 12 5 0 22.70 9.30 -13 -5 0 4.90 6.80 13 -5 0 11.30 11.90 -13 -5 0 7.70 11.20 13 -5 0 -0.20 7.60 13 -5 0 6.10 10.40 -13 5 0 23.20 7.70 13 5 0 6.10 15.90 -13 5 0 18.40 13.00 13 5 0 1.80 9.10 13 5 0 -6.10 6.70 -14 -5 0 50.09 8.80 14 -5 0 40.40 12.30 14 -5 0 38.40 11.90 -14 -5 0 48.60 13.10 14 5 0 40.50 15.70 14 5 0 52.59 11.30 -14 5 0 38.20 8.40 -14 5 0 64.29 16.00 -15 -5 0 -10.60 6.40 15 -5 0 -4.70 10.80 -15 -5 0 14.70 11.20 -15 5 0 27.00 14.00 -15 5 0 -5.40 6.90 15 5 0 3.90 9.50 -16 -5 0 -1.20 6.60 -16 -5 0 7.10 9.70 16 -5 0 -0.40 13.20 16 5 0 -4.70 9.30 -16 5 0 -5.40 6.50 17 -5 0 20.60 14.80 -17 -5 0 15.70 7.70 17 5 0 36.40 10.90 -17 5 0 25.50 8.90 0 -6 0 728.23 31.10 0 6 0 735.13 31.50 0 6 0 741.03 31.20 -1 -6 0 8.50 2.80 -1 -6 0 8.20 2.60 1 -6 0 9.50 2.70 1 -6 0 9.60 3.40 1 6 0 7.90 2.80 -1 6 0 7.10 4.20 1 6 0 6.70 3.60 -1 6 0 6.10 2.50 1 6 0 8.30 2.50 -1 6 0 9.60 2.80 -2 -6 0 604.34 26.00 2 -6 0 626.64 26.60 2 -6 0 616.24 26.00 -2 -6 0 583.24 26.30 2 6 0 594.24 26.00 -2 6 0 615.34 27.60 -2 6 0 588.54 26.00 -2 6 0 612.34 25.70 2 6 0 569.34 27.00 2 6 0 626.44 25.70 -3 -6 0 440.26 19.40 3 -6 0 424.26 20.50 3 -6 0 440.96 19.60 -3 -6 0 427.46 20.20 3 6 0 452.75 19.20 -3 6 0 418.56 19.40 -3 6 0 429.76 22.40 3 6 0 453.85 19.80 3 6 0 400.46 21.80 -4 -6 0 20.60 6.80 4 -6 0 36.90 7.60 4 -6 0 24.10 4.70 -4 -6 0 25.00 4.40 4 -6 0 26.00 5.50 -4 6 0 38.80 11.40 4 6 0 21.30 5.00 4 6 0 28.10 5.30 -4 6 0 21.00 4.60 -5 -6 0 1222.18 53.69 -5 -6 0 1176.18 52.09 5 -6 0 1273.87 52.69 5 -6 0 1203.78 53.49 5 -6 0 1255.27 52.29 5 6 0 1109.29 55.49 -5 6 0 1310.57 56.79 5 6 0 1293.87 52.39 -5 6 0 1266.67 52.29 5 6 0 1244.98 52.59 -6 -6 0 1009.70 43.90 6 -6 0 1040.20 44.50 6 -6 0 998.00 45.50 -6 -6 0 982.60 46.00 6 -6 0 1081.29 44.30 6 6 0 1054.99 44.40 6 6 0 1000.80 47.90 -6 6 0 1012.00 44.00 6 6 0 1042.00 44.40 -6 6 0 1013.00 48.80 7 -6 0 519.45 24.20 -7 -6 0 485.05 26.20 -7 -6 0 509.85 23.50 7 -6 0 495.25 25.60 7 -6 0 503.35 24.10 -7 6 0 530.35 23.70 7 6 0 507.35 24.00 7 6 0 508.35 23.90 -7 6 0 491.05 28.20 7 6 0 478.85 27.50 -8 -6 0 -1.90 7.00 8 -6 0 1.40 8.00 8 -6 0 -6.00 5.50 -8 -6 0 -0.70 4.40 8 -6 0 4.40 5.60 8 6 0 1.80 5.00 -8 6 0 3.60 4.80 8 6 0 1.50 5.80 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17.70 -14 -6 0 109.39 18.20 -14 6 0 125.79 18.40 -14 6 0 115.59 13.60 14 6 0 97.89 13.90 14 6 0 100.59 20.10 14 6 0 78.99 11.20 -15 -6 0 26.70 11.60 15 -6 0 0.90 13.20 15 -6 0 -14.00 10.90 -15 -6 0 3.70 7.50 15 6 0 9.20 9.10 -15 6 0 1.50 7.60 15 6 0 -9.50 15.20 -16 -6 0 25.60 11.30 16 -6 0 -19.30 10.70 16 6 0 5.90 9.40 -16 6 0 -2.30 7.50 17 -6 0 9.10 14.20 -17 -6 0 4.10 7.30 17 6 0 -4.60 8.70 -17 6 0 1.50 8.20 0 -7 0 -3.10 2.80 0 7 0 0.50 4.90 0 7 0 -0.80 2.80 1 -7 0 492.85 22.70 1 -7 0 551.34 23.20 -1 -7 0 498.65 22.70 -1 -7 0 539.85 23.10 1 7 0 527.65 22.40 -1 7 0 508.35 22.90 1 7 0 512.15 22.90 1 7 0 512.95 23.60 -1 7 0 509.75 22.90 -1 7 0 540.05 24.20 -2 -7 0 545.75 23.90 2 -7 0 518.65 23.40 -2 -7 0 507.95 23.20 2 -7 0 567.74 24.20 -2 7 0 517.05 23.40 2 7 0 489.65 25.00 -2 7 0 513.75 23.00 2 7 0 511.45 23.50 -2 7 0 565.34 25.20 2 7 0 534.65 23.00 3 -7 0 853.81 36.50 -3 -7 0 824.22 35.40 -3 -7 0 786.02 36.00 3 -7 0 831.02 35.50 -3 7 0 782.52 35.20 3 7 0 859.21 35.00 3 7 0 775.12 37.80 -3 7 0 853.31 38.20 -3 7 0 799.92 34.70 3 7 0 858.11 35.70 -4 -7 0 436.56 20.80 4 -7 0 463.85 22.30 -4 -7 0 425.96 22.30 4 7 0 444.76 21.50 -4 7 0 508.05 26.90 4 7 0 447.16 20.60 -4 7 0 448.86 21.10 4 7 0 404.66 24.30 5 -7 0 1771.52 73.09 5 -7 0 1734.93 74.59 -5 -7 0 1723.63 74.79 5 -7 0 1827.62 73.79 -5 -7 0 1726.33 73.29 5 7 0 1688.53 75.79 -5 7 0 1718.93 73.29 5 7 0 1787.32 73.19 -5 7 0 1775.82 77.09 5 7 0 1825.92 73.79 6 -7 0 269.17 17.30 -6 -7 0 243.98 16.80 6 -7 0 269.57 14.20 6 -7 0 266.37 15.10 -6 -7 0 264.97 14.20 6 7 0 256.27 14.80 -6 7 0 273.57 21.80 -6 7 0 266.57 14.50 6 7 0 260.87 14.50 6 7 0 226.88 18.60 -7 -7 0 220.88 15.50 7 -7 0 242.68 13.80 -7 -7 0 234.98 13.40 7 -7 0 236.28 15.80 7 -7 0 236.78 14.30 7 7 0 244.18 14.10 7 7 0 226.68 19.80 7 7 0 246.08 14.00 -7 7 0 239.68 19.00 -7 7 0 243.98 13.80 -8 -7 0 3.60 7.10 -8 -7 0 7.10 4.50 8 -7 0 2.60 5.30 8 -7 0 10.00 5.70 8 -7 0 11.10 8.50 -8 7 0 2.40 9.80 8 7 0 -4.20 10.00 -8 7 0 6.20 4.50 8 7 0 2.00 4.80 8 7 0 0.00 5.50 9 -7 0 33.80 7.00 -9 -7 0 23.10 9.30 9 -7 0 14.90 6.40 9 -7 0 25.20 9.10 -9 -7 0 21.20 5.30 -9 7 0 27.10 6.20 -9 7 0 31.30 12.40 9 7 0 26.90 7.20 9 7 0 23.70 6.30 9 7 0 19.00 12.30 10 -7 0 -2.20 8.80 -10 -7 0 4.60 5.90 10 -7 0 -2.70 6.70 10 -7 0 -1.90 7.10 -10 -7 0 -1.30 10.10 -10 7 0 -9.90 5.80 10 7 0 -7.20 13.10 10 7 0 -5.70 7.00 10 7 0 -8.70 5.70 -10 7 0 -5.00 10.90 -11 -7 0 51.99 8.20 11 -7 0 40.30 8.80 -11 -7 0 55.99 11.90 11 -7 0 42.10 9.20 11 -7 0 60.69 12.90 11 7 0 41.30 7.70 -11 7 0 35.70 13.40 11 7 0 36.40 15.40 -11 7 0 45.30 9.60 11 7 0 51.89 14.40 -12 -7 0 88.39 14.70 12 -7 0 109.79 15.60 12 -7 0 84.89 14.40 12 -7 0 75.19 10.40 -12 -7 0 79.49 10.20 12 7 0 77.49 11.60 -12 7 0 87.79 10.90 12 7 0 80.29 16.40 -12 7 0 75.49 15.30 12 7 0 74.59 12.60 13 -7 0 5.80 9.60 13 -7 0 16.10 12.60 13 -7 0 12.80 8.20 -13 -7 0 10.60 7.10 -13 -7 0 28.80 13.00 -13 7 0 26.20 14.90 -13 7 0 13.90 8.20 13 7 0 -6.60 6.80 13 7 0 9.70 16.60 13 7 0 9.70 8.90 -14 -7 0 6.20 7.20 -14 -7 0 18.20 11.20 14 -7 0 1.40 11.30 14 -7 0 -3.00 9.90 -14 7 0 27.30 12.80 14 7 0 2.00 8.70 14 7 0 -6.20 14.60 -14 7 0 8.10 7.50 15 -7 0 81.49 13.60 -15 -7 0 113.49 13.00 -15 -7 0 128.29 18.60 15 -7 0 107.99 17.40 -15 7 0 104.29 13.50 15 7 0 99.29 14.00 15 7 0 74.49 20.80 16 -7 0 -19.90 11.20 -16 -7 0 -6.40 7.30 -16 -7 0 28.40 12.80 16 7 0 0.40 9.10 -16 7 0 -0.50 7.50 0 -8 0 2333.77 98.99 0 8 0 2395.66 99.29 0 8 0 2277.77 99.59 0 8 0 2623.34 100.49 1 -8 0 5.40 4.30 1 -8 0 15.10 5.80 -1 -8 0 7.10 4.40 -1 -8 0 5.60 4.20 -1 8 0 17.80 7.40 -1 8 0 0.70 4.40 1 8 0 4.30 4.60 1 8 0 12.80 4.10 -1 8 0 -3.40 4.30 -2 -8 0 22.50 6.20 2 -8 0 15.60 4.50 -2 -8 0 21.00 5.10 2 -8 0 27.70 6.60 2 8 0 2.20 6.80 -2 8 0 22.90 5.20 2 8 0 14.50 4.70 -2 8 0 14.20 4.50 2 8 0 21.00 5.40 -3 -8 0 -1.20 4.50 3 -8 0 13.80 7.60 3 -8 0 5.20 5.30 -3 -8 0 0.80 5.30 -3 8 0 3.90 4.60 3 8 0 4.50 5.20 3 8 0 -11.90 8.60 3 8 0 1.60 4.80 -3 8 0 -1.50 3.70 -4 -8 0 86.19 8.40 -4 -8 0 76.49 9.50 4 8 0 77.49 7.90 4 8 0 68.59 13.50 4 8 0 89.09 8.40 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279.67 15.20 2 -12 0 298.87 16.20 -2 -12 0 283.07 14.90 2 12 0 279.27 15.40 2 12 0 274.47 14.10 -2 12 0 275.77 18.60 2 12 0 252.77 17.50 -2 12 0 284.97 15.20 -2 12 0 270.27 15.40 -3 -12 0 480.35 23.50 3 -12 0 531.25 24.90 -3 -12 0 469.05 22.60 3 -12 0 479.05 23.00 3 12 0 482.75 26.00 3 12 0 482.15 22.20 -3 12 0 471.55 22.80 -3 12 0 474.85 22.50 -3 12 0 476.05 26.00 3 12 0 484.45 23.30 4 -12 0 415.96 20.50 -4 -12 0 400.06 20.00 4 -12 0 444.16 22.30 -4 -12 0 407.36 20.90 -4 12 0 389.76 20.10 -4 12 0 401.76 24.50 4 12 0 419.46 24.30 -4 12 0 406.66 19.50 4 12 0 418.56 20.60 4 12 0 408.96 19.50 5 -12 0 -10.20 5.40 -5 -12 0 -4.50 5.50 5 -12 0 1.50 8.00 -5 -12 0 -5.30 4.60 -5 12 0 0.00 3.60 -5 12 0 -10.30 10.70 5 12 0 -4.70 4.60 5 12 0 -3.10 4.40 5 12 0 -2.00 9.00 -5 12 0 1.70 5.00 -6 -12 0 268.07 15.30 6 -12 0 274.77 19.70 -6 -12 0 290.17 18.30 6 -12 0 278.77 16.50 6 12 0 269.97 22.10 6 12 0 259.37 14.90 -6 12 0 264.37 13.90 -6 12 0 296.67 16.40 -6 12 0 274.67 22.90 6 12 0 277.97 16.30 7 -12 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14.80 7 9 -4 46.80 11.20 7 9 -4 61.19 8.30 -6 -9 4 9.50 6.10 6 -9 -4 15.60 6.60 -6 -9 4 13.70 4.60 6 -9 -4 18.50 5.70 6 -9 -4 18.70 5.80 6 9 -4 12.20 9.30 6 9 -4 10.00 5.60 6 9 -4 14.30 5.70 -6 9 4 28.90 12.70 -6 9 4 26.70 5.30 -5 -9 4 31.70 6.30 -5 -9 4 37.90 5.40 5 -9 -4 31.00 6.10 5 -9 -4 41.90 7.80 5 -9 -4 34.40 6.30 5 9 -4 40.80 6.60 5 9 -4 33.70 5.80 -5 9 4 27.60 5.20 -5 9 4 35.60 12.40 5 9 -4 19.40 9.20 4 -9 -4 176.88 11.60 4 -9 -4 177.68 12.70 -4 -9 4 177.78 11.00 -4 -9 4 168.38 10.60 -4 9 4 203.78 18.50 -4 9 4 181.88 11.10 4 9 -4 158.98 17.20 4 9 -4 150.18 11.10 4 9 -4 157.08 11.10 3 -9 -4 8.30 6.30 -3 -9 4 0.90 4.00 -3 -9 4 -2.70 4.20 3 -9 -4 0.40 5.10 3 9 -4 2.80 5.30 -3 9 4 5.00 11.10 3 9 -4 5.20 5.70 3 9 -4 -8.50 9.10 -3 9 4 -2.40 4.40 -3 9 4 5.20 4.70 2 -9 -4 1848.32 79.09 -2 -9 4 1903.71 78.89 -2 -9 4 1902.11 78.39 2 -9 -4 2014.70 79.09 -2 9 4 1950.70 82.19 -2 9 4 1828.92 79.49 -2 9 4 1903.61 78.99 2 9 -4 1881.21 79.29 2 9 -4 1898.91 79.39 2 9 -4 1861.41 80.79 -1 -9 4 243.48 13.20 1 -9 -4 235.08 13.70 1 -9 -4 284.87 13.60 1 9 -4 267.27 14.10 1 9 -4 229.38 16.50 1 9 -4 251.27 14.20 -1 9 4 218.88 14.60 -1 9 4 249.58 13.50 -1 9 4 247.88 19.00 0 -9 -4 241.58 11.50 0 -9 -4 208.68 12.20 0 -9 4 208.68 11.90 0 9 -4 205.68 12.60 0 9 -4 214.88 12.70 0 9 -4 193.98 14.70 0 9 4 213.88 12.30 0 9 4 172.78 13.90 1 -9 4 1999.30 83.19 -1 -9 -4 2204.28 82.49 -1 -9 -4 1998.50 84.79 -1 -9 -4 1939.51 83.39 1 9 4 2009.80 83.39 -1 9 -4 1889.51 83.49 -1 9 -4 2159.58 83.69 -1 9 -4 1981.50 83.89 1 9 4 1911.31 84.79 -2 -9 -4 52.29 8.90 2 -9 4 58.79 9.00 2 -9 4 50.99 7.90 -2 -9 -4 48.90 6.00 2 9 4 53.09 6.20 -2 9 -4 46.90 5.80 -2 9 -4 56.99 8.00 3 -9 4 357.46 19.40 -3 -9 -4 326.97 16.70 -3 -9 -4 331.27 18.60 3 -9 4 360.36 16.70 3 9 4 292.97 19.90 -3 9 -4 311.97 15.50 -3 9 -4 338.87 17.10 3 9 4 330.07 14.90 -3 9 -4 377.56 20.40 3 9 4 349.57 16.80 -4 -9 -4 764.72 34.40 4 -9 4 805.42 36.50 -4 -9 -4 774.22 36.00 -4 9 -4 819.92 36.80 4 9 4 811.52 33.10 -4 9 -4 782.82 34.50 4 9 4 848.02 34.50 -4 9 -4 762.32 32.40 -4 9 -4 733.73 32.50 4 9 4 740.93 37.00 5 -9 4 62.49 9.70 5 -9 4 63.19 8.10 -5 -9 -4 58.89 7.30 -5 -9 -4 64.49 10.30 -5 9 -4 48.80 9.70 -5 9 -4 62.49 7.70 5 9 4 60.69 5.90 5 9 4 44.50 8.70 5 9 4 63.59 7.30 6 -9 4 22.20 8.70 -6 -9 -4 20.20 5.10 6 -9 4 13.20 6.40 -6 -9 -4 7.10 7.20 -6 9 -4 9.70 4.80 6 9 4 14.10 4.20 -6 9 -4 13.70 8.50 6 9 4 13.90 7.90 6 9 4 11.70 4.60 -7 -9 -4 -4.00 6.80 7 -9 4 -5.90 8.30 -7 -9 -4 -2.00 4.70 7 9 4 -0.40 8.20 7 9 4 0.40 5.70 -7 9 -4 4.20 5.10 7 9 4 3.40 4.70 -7 9 -4 2.20 8.90 -8 -9 -4 166.38 16.00 -8 -9 -4 186.98 12.90 8 -9 4 199.48 17.60 8 9 4 186.08 12.60 -8 9 -4 199.28 13.40 -8 9 -4 185.48 18.40 8 9 4 195.08 19.80 8 9 4 192.58 12.00 -9 -9 -4 62.29 12.30 9 -9 4 68.59 6.20 9 -9 4 88.09 13.60 -9 -9 -4 82.69 13.20 -9 9 -4 65.19 15.40 9 9 4 63.99 12.80 9 9 4 80.19 9.70 -9 9 -4 74.39 10.30 9 9 4 81.39 9.50 -10 -9 -4 122.59 11.90 10 -9 4 109.69 8.90 10 -9 4 131.99 16.40 -10 -9 -4 109.29 16.90 -10 9 -4 128.59 19.00 10 9 4 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33.50 -6 11 -5 800.62 37.80 -7 -11 -5 127.79 11.70 -7 -11 -5 121.99 14.90 7 -11 5 152.78 16.70 7 11 5 128.19 16.60 7 11 5 140.99 9.30 -7 11 -5 138.69 17.10 -7 11 -5 136.29 18.40 7 11 5 144.69 10.90 8 -11 5 122.99 17.30 -8 -11 -5 136.49 16.50 -8 -11 -5 134.89 12.10 8 11 5 130.79 20.00 -8 11 -5 144.09 12.80 -8 11 -5 158.78 18.80 8 11 5 148.99 12.00 8 11 5 147.19 10.40 -9 -11 -5 197.28 17.70 9 -11 5 215.78 21.00 -9 -11 -5 226.98 15.10 9 11 5 226.78 14.40 -9 11 -5 222.88 15.60 9 11 5 227.08 13.60 -9 11 -5 162.08 28.60 9 11 5 214.88 21.10 -10 -11 -5 78.29 11.30 -10 -11 -5 96.19 16.80 10 -11 5 77.19 14.00 -10 11 -5 82.59 12.20 10 11 5 119.69 13.70 10 11 5 77.39 14.80 -10 11 -5 115.19 17.80 10 11 5 94.49 10.50 -11 -11 -5 272.37 21.60 -11 -11 -5 260.27 18.30 11 -11 5 292.87 24.70 11 11 5 295.47 28.20 -11 11 -5 326.37 23.80 11 11 5 284.77 17.10 -11 11 -5 285.77 18.90 12 -11 5 144.09 18.90 -12 -11 -5 143.89 14.20 -12 -11 -5 133.39 16.70 12 11 5 159.38 25.70 -12 11 -5 149.09 15.00 -13 -11 -5 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7.30 0 -12 7 3.30 3.90 0 -12 -7 -6.50 4.40 0 -12 -7 3.30 3.60 0 12 7 9.70 9.00 0 12 -7 3.00 5.00 0 12 -7 -7.00 5.90 0 12 7 2.50 5.90 0 12 -7 0.30 6.60 0 12 7 -3.30 3.90 -1 -12 -7 72.49 8.30 -1 -12 -7 81.09 5.40 1 -12 7 76.79 8.20 -1 12 -7 86.49 8.90 -1 12 -7 99.79 7.00 1 12 7 81.19 11.40 -1 12 -7 60.39 10.50 1 12 7 81.89 8.20 -2 -12 -7 130.19 9.70 2 -12 7 135.49 12.90 -2 -12 -7 128.59 12.20 -2 12 -7 97.99 10.50 2 12 7 121.39 12.00 2 12 7 127.09 9.20 -2 12 -7 117.29 10.00 -3 -12 -7 161.18 11.30 3 -12 7 170.78 14.70 -3 -12 -7 175.48 13.00 -3 12 -7 145.29 10.30 3 12 7 170.38 15.30 3 12 7 169.38 10.70 -3 12 -7 176.78 12.00 -4 -12 -7 -3.10 6.10 -4 -12 -7 -0.10 4.80 4 12 7 -1.60 8.40 -4 12 -7 -2.70 5.30 4 12 7 0.60 6.90 -5 -12 -7 35.40 12.90 5 -12 7 45.60 10.10 -5 -12 -7 39.70 6.90 5 12 7 28.40 10.50 -5 12 -7 31.00 11.00 -6 -12 -7 238.68 15.20 6 -12 7 241.98 18.50 -6 -12 -7 249.08 19.10 -6 12 -7 269.37 18.20 6 12 7 263.47 11.90 6 12 7 237.38 19.40 -6 12 -7 243.98 15.40 7 -12 7 78.39 13.90 -7 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90.99 13.80 13 -13 -7 75.59 15.70 13 -13 -7 70.99 12.30 13 13 -7 94.79 13.70 13 13 -7 62.29 10.70 -13 13 7 81.49 21.80 -13 13 7 61.09 9.90 12 -13 -7 12.40 8.50 12 -13 -7 4.10 12.10 -12 -13 7 0.50 6.60 -12 -13 7 23.20 10.70 12 -13 -7 -6.30 9.00 12 13 -7 -2.50 8.30 12 13 -7 -20.20 19.10 -12 13 7 -10.10 16.00 -12 13 7 -6.30 7.90 12 13 -7 15.80 8.50 11 -13 -7 56.69 11.20 -11 -13 7 57.69 8.50 11 -13 -7 92.79 15.00 11 13 -7 78.19 19.90 -11 13 7 58.79 9.60 11 13 -7 55.19 9.70 11 13 -7 73.39 12.80 -11 13 7 58.59 19.00 10 -13 -7 203.38 16.10 -10 -13 7 191.98 17.20 10 -13 -7 177.88 19.10 -10 -13 7 208.18 14.40 10 -13 -7 192.48 17.60 10 13 -7 188.58 16.50 10 13 -7 184.28 25.30 -10 13 7 195.88 15.80 -10 13 7 152.18 29.50 10 13 -7 195.78 15.40 -9 -13 7 -2.20 5.40 9 -13 -7 1.90 10.30 -9 -13 7 15.30 8.60 -9 13 7 10.90 7.00 -9 13 7 -13.10 18.80 9 13 -7 1.10 8.00 9 13 -7 2.90 15.80 9 13 -7 -3.90 7.20 -8 -13 7 397.06 20.50 -8 -13 7 392.56 22.10 8 -13 -7 401.06 22.90 8 -13 -7 380.36 23.70 8 13 -7 368.06 28.80 8 13 -7 361.26 21.90 -8 13 7 395.16 21.30 -8 13 7 364.86 33.40 8 13 -7 372.46 22.50 7 -13 -7 209.78 20.60 -7 -13 7 229.48 15.40 -7 -13 7 213.08 13.90 -7 13 7 240.58 15.00 -7 13 7 220.58 27.20 7 13 -7 197.58 16.00 7 13 -7 211.68 25.10 -7 13 7 210.08 14.70 7 13 -7 205.48 14.90 6 -13 -7 11.40 7.40 -6 -13 7 11.20 5.70 6 -13 -7 4.00 8.30 -6 -13 7 10.30 5.10 6 13 -7 5.00 7.10 -6 13 7 1.60 15.80 -6 13 7 11.20 6.20 -6 13 7 14.00 6.30 6 13 -7 17.90 13.10 6 13 -7 21.10 7.60 5 -13 -7 20.10 6.80 -5 -13 7 23.50 5.20 -5 -13 7 23.20 5.20 5 -13 -7 24.80 8.40 -5 13 7 19.80 5.60 -5 13 7 16.70 6.10 5 13 -7 19.60 7.00 5 13 -7 24.90 7.60 -5 13 7 26.60 18.10 5 13 -7 17.10 11.90 -4 -13 7 18.40 4.10 -4 -13 7 19.60 5.10 4 -13 -7 15.20 7.20 4 -13 -7 9.40 6.20 4 13 -7 14.00 7.00 -4 13 7 18.60 6.20 4 13 -7 10.60 10.70 -4 13 7 18.30 5.60 -4 13 7 15.10 13.40 4 13 -7 11.40 6.40 -3 -13 7 -2.20 2.90 3 -13 -7 -4.90 6.00 3 -13 -7 5.10 5.30 -3 -13 7 5.50 4.40 3 13 -7 -6.40 5.60 -3 13 7 -0.50 5.60 3 13 -7 5.20 6.10 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35.00 9.40 9 -10 -15 17.60 10.40 9 -10 -15 12.00 9.70 9 -10 -15 19.20 8.90 -9 -10 15 19.50 9.20 -9 10 15 24.90 21.50 9 10 -15 29.80 9.50 9 10 -15 22.10 15.40 -9 10 15 37.60 6.80 9 10 -15 25.70 10.80 8 -10 -15 5.60 8.20 8 -10 -15 2.00 8.60 8 -10 -15 4.70 10.30 -8 -10 15 15.30 7.80 8 10 -15 -8.40 13.40 8 10 -15 5.20 8.10 -8 10 15 19.00 19.80 8 10 -15 9.80 9.90 -8 10 15 -0.10 5.60 7 -10 -15 42.60 11.40 7 -10 -15 24.40 7.90 7 -10 -15 26.20 8.90 -7 -10 15 49.00 9.70 -7 10 15 37.10 17.50 7 10 -15 31.50 9.30 7 10 -15 39.70 8.30 7 10 -15 32.50 15.50 6 -10 -15 17.00 6.90 6 -10 -15 14.90 9.70 6 -10 -15 3.40 7.30 6 10 -15 3.20 7.70 6 10 -15 -0.20 6.60 6 10 -15 -0.40 12.90 -6 10 15 11.20 17.30 -5 -10 15 13.80 4.90 5 -10 -15 6.90 8.50 5 -10 -15 8.70 6.40 5 -10 -15 4.10 6.10 5 10 -15 2.00 6.40 -5 10 15 11.80 14.50 5 10 -15 4.20 8.60 5 10 -15 10.00 12.30 4 -10 -15 132.99 11.00 -4 -10 15 173.48 8.90 4 -10 -15 158.68 12.40 4 10 -15 149.49 14.40 -4 10 15 142.99 23.20 4 10 -15 157.18 19.30 4 10 -15 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424.96 23.70 5 -2 -28 527.15 23.80 -5 -2 28 491.65 33.00 -5 2 28 461.85 35.90 5 2 -28 449.95 24.00 5 2 -28 487.05 28.80 5 2 -28 550.14 23.70 5 2 -28 468.25 31.50 -4 -2 28 184.28 22.80 4 -2 -28 193.78 23.10 4 -2 -28 158.58 12.50 4 -2 -28 176.58 15.80 4 -2 -28 194.68 12.20 4 2 -28 198.08 12.50 4 2 -28 176.68 23.00 4 2 -28 173.88 13.20 -4 2 28 192.18 23.10 4 2 -28 215.18 18.00 3 -2 -28 11.00 8.60 3 -2 -28 9.90 5.00 3 -2 -28 -0.40 10.90 3 -2 -28 13.80 4.60 -3 -2 28 7.10 13.50 3 2 -28 6.00 12.30 3 2 -28 12.50 4.80 3 2 -28 17.90 5.50 -3 2 28 18.20 15.60 3 2 -28 13.20 10.20 2 -2 -28 159.08 18.50 2 -2 -28 143.19 9.20 2 -2 -28 124.89 9.80 2 -2 -28 137.59 13.80 -2 -2 28 135.49 19.60 2 2 -28 132.69 10.10 2 2 -28 138.19 15.90 -2 2 28 121.69 19.90 2 2 -28 159.88 9.50 2 2 -28 155.18 20.20 -1 -2 28 167.08 21.90 1 -2 -28 148.09 15.20 1 -2 -28 184.28 21.30 1 -2 -28 169.58 9.40 1 -2 -28 159.98 9.70 -1 2 28 184.78 23.20 1 2 -28 162.98 16.20 1 2 -28 149.99 19.90 1 2 -28 148.99 10.00 1 2 -28 176.88 9.80 0 -2 28 24.60 12.10 0 -2 -28 24.90 8.80 0 -2 -28 13.80 3.20 0 -2 -28 15.30 3.40 0 2 -28 21.20 3.40 0 2 -28 17.60 10.10 0 2 -28 23.60 11.40 0 2 28 30.60 14.40 0 2 -28 23.50 3.80 1 -2 28 675.23 37.20 -1 -2 -28 621.44 28.00 -1 -2 -28 669.73 32.50 -1 -2 -28 635.94 27.70 1 2 28 670.23 34.30 -1 2 -28 694.33 34.40 -1 2 -28 657.23 36.40 -2 -2 -28 402.26 18.10 -2 -2 -28 427.96 23.50 -2 -2 -28 448.66 28.50 2 2 28 450.95 26.10 -2 2 -28 417.86 24.20 3 -2 28 133.59 14.70 -3 -2 -28 103.29 17.70 -3 2 -28 119.69 15.80 3 2 28 141.19 15.20 3 2 28 126.29 12.90 -4 -2 -28 110.29 17.80 -4 -2 -28 131.29 8.10 -4 -2 -28 105.49 7.30 4 -2 28 114.69 14.50 4 -2 28 148.19 13.30 -4 2 -28 104.29 6.30 4 2 28 139.39 14.90 -4 2 -28 126.79 18.80 4 2 28 106.19 12.50 -5 -2 -28 111.39 8.00 5 -2 28 112.59 14.80 -5 -2 -28 132.09 9.20 -5 -2 -28 124.99 18.10 5 2 28 115.89 14.00 -5 2 -28 110.09 7.10 -5 2 -28 116.19 15.70 -5 2 -28 116.59 8.40 -6 -2 -28 21.40 6.00 6 -2 28 43.70 11.30 -6 -2 -28 28.30 11.90 -6 -2 -28 19.80 4.50 6 2 28 19.80 9.30 -6 2 -28 22.80 3.90 -6 2 -28 17.40 4.90 -6 2 -28 22.50 10.20 -7 -2 -28 11.10 11.40 -7 2 -28 10.70 10.30 8 -2 28 113.79 17.50 -8 -2 -28 117.09 10.20 -8 -2 -28 132.39 12.70 -8 -2 -28 157.18 17.70 -8 2 -28 107.39 9.70 8 2 28 121.29 15.40 -9 -2 -28 134.99 21.30 -9 2 -28 167.58 19.00 13 -3 -28 60.49 13.40 13 -3 -28 26.20 11.20 -13 -3 28 31.70 17.50 -13 3 28 -6.70 24.30 13 3 -28 8.40 10.60 13 3 -28 33.60 11.30 -12 -3 28 14.00 17.10 12 -3 -28 -3.30 9.90 12 -3 -28 31.90 12.10 12 3 -28 23.20 11.90 12 3 -28 4.70 10.00 11 -3 -28 19.70 10.40 11 -3 -28 6.40 9.40 -11 -3 28 -13.30 17.50 11 3 -28 19.10 10.60 -11 3 28 -23.00 22.30 11 3 -28 17.60 9.90 10 -3 -28 181.48 17.80 -10 -3 28 162.58 26.50 10 -3 -28 161.08 16.20 10 3 -28 159.88 16.60 10 3 -28 186.88 19.80 -10 3 28 134.09 27.70 9 -3 -28 1.30 8.00 9 -3 -28 7.00 9.20 -9 -3 28 -18.00 16.90 9 -3 -28 -9.70 15.00 9 3 -28 1.40 8.50 9 3 -28 17.30 11.60 9 3 -28 10.00 16.80 -9 3 28 -13.20 18.40 8 -3 -28 49.50 16.70 8 -3 -28 47.90 9.20 -8 -3 28 26.30 17.50 8 -3 -28 50.09 11.20 8 3 -28 57.69 13.30 8 3 -28 42.60 9.20 8 3 -28 40.70 15.20 -8 3 28 38.10 21.40 7 -3 -28 113.79 13.00 7 -3 -28 124.09 14.60 7 -3 -28 114.09 20.20 -7 -3 28 92.29 19.20 -7 3 28 107.39 23.10 7 3 -28 78.19 11.10 7 3 -28 115.29 16.60 7 3 -28 97.59 19.00 7 3 -28 109.09 12.90 6 -3 -28 95.59 13.20 6 -3 -28 97.69 10.50 6 -3 -28 115.69 22.30 6 -3 -28 90.69 11.50 -6 -3 28 74.79 17.40 6 3 -28 70.29 11.90 6 3 -28 100.89 10.80 -6 3 28 92.29 21.60 6 3 -28 76.09 15.80 6 3 -28 112.09 14.20 -5 -3 28 -14.60 13.80 5 -3 -28 -2.80 5.70 5 -3 -28 -2.90 4.90 5 -3 -28 5.00 13.30 5 -3 -28 11.60 8.90 5 3 -28 -3.00 5.50 5 3 -28 -1.20 12.80 -5 3 28 -1.80 17.30 5 3 -28 5.10 6.50 5 3 -28 4.60 8.90 -4 -3 28 116.99 19.70 4 -3 -28 119.19 13.60 4 -3 -28 118.59 11.20 4 -3 -28 112.69 20.90 4 -3 -28 125.79 10.00 4 3 -28 118.99 21.00 4 3 -28 129.29 14.40 -4 3 28 102.69 21.30 4 3 -28 120.69 11.60 4 3 -28 133.59 10.60 3 -3 -28 169.38 11.80 3 -3 -28 167.48 15.50 3 -3 -28 177.18 11.10 3 -3 -28 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0.00 -7 11 32 4.46 0.00 -6 11 32 3.63 0.00 3 11 32 1.07 0.00 4 11 32 1.37 0.00 -7 12 32 -0.34 0.00 -6 12 32 1.20 0.00 -5 12 32 2.41 0.00 -4 12 32 2.83 0.00 0 12 32 0.42 0.00 1 12 32 -1.55 0.00 2 12 32 0.34 0.00 3 12 32 -1.44 0.00 -6 13 32 -0.60 0.00 -5 13 32 0.54 0.00 -4 13 32 -0.96 0.00 -3 13 32 -1.69 0.00 -2 13 32 0.17 0.00 -1 13 32 -0.39 0.00 0 13 32 -0.17 0.00 1 13 32 -1.51 0.00 2 13 32 -0.94 0.00 -3 14 32 -3.74 0.00 -2 14 32 -3.10 0.00 -1 14 32 -1.02 0.00 -11 1 33 1.28 0.00 4 1 33 1.84 0.00 5 1 33 1.37 0.00 6 1 33 -0.23 0.00 7 1 33 0.09 0.00 -11 2 33 3.28 0.00 5 2 33 -3.22 0.00 7 2 33 -0.28 0.00 -11 3 33 -1.72 0.00 -10 3 33 -1.43 0.00 3 3 33 -7.93 0.00 5 3 33 -2.38 0.00 6 3 33 -0.48 0.00 7 3 33 2.23 0.00 -11 4 33 -2.10 0.00 -10 4 33 -5.39 0.00 6 4 33 -1.61 0.00 7 4 33 0.47 0.00 -11 5 33 1.57 0.00 -10 5 33 -0.89 0.00 6 5 33 1.87 0.00 7 5 33 -0.45 0.00 -10 6 33 0.38 0.00 -9 6 33 1.15 0.00 6 6 33 2.32 0.00 -10 7 33 0.77 0.00 -9 7 33 -0.11 0.00 5 7 33 -1.73 0.00 6 7 33 -0.26 0.00 -9 8 33 -0.90 0.00 -8 8 33 -0.19 0.00 4 8 33 3.40 0.00 5 8 33 0.99 0.00 -9 9 33 -0.57 0.00 -8 9 33 0.89 0.00 -7 9 33 1.56 0.00 3 9 33 -1.48 0.00 4 9 33 1.84 0.00 5 9 33 1.33 0.00 -8 10 33 -0.35 0.00 -7 10 33 0.14 0.00 -6 10 33 2.95 0.00 2 10 33 -3.30 0.00 3 10 33 -3.90 0.00 4 10 33 -3.33 0.00 -7 11 33 -1.67 0.00 -6 11 33 0.82 0.00 -5 11 33 0.40 0.00 -4 11 33 -1.66 0.00 0 11 33 -1.73 0.00 1 11 33 -1.38 0.00 2 11 33 -1.27 0.00 3 11 33 1.34 0.00 -6 12 33 -2.63 0.00 -5 12 33 -2.42 0.00 -4 12 33 0.38 0.00 -3 12 33 -1.68 0.00 -2 12 33 -0.16 0.00 -1 12 33 -0.79 0.00 0 12 33 -3.15 0.00 1 12 33 -1.52 0.00 2 12 33 0.56 0.00 -3 13 33 1.96 0.00 -2 13 33 0.98 0.00 -1 13 33 2.58 0.00 -11 0 34 -0.79 0.00 -10 0 34 1.16 0.00 4 0 34 3.15 0.00 5 0 34 2.86 0.00 6 0 34 3.83 0.00 7 0 34 0.48 0.00 -11 1 34 -2.11 0.00 -10 1 34 -6.14 0.00 4 1 34 -0.19 0.00 5 1 34 -0.07 0.00 6 1 34 -0.55 0.00 7 1 34 -0.32 0.00 -10 2 34 -1.71 0.00 3 2 34 -0.96 0.00 4 2 34 -3.23 0.00 6 2 34 -2.29 0.00 7 2 34 -0.75 0.00 -10 3 34 0.10 0.00 5 3 34 4.41 0.00 6 3 34 2.19 0.00 -10 4 34 3.20 0.00 -9 4 34 0.61 0.00 5 4 34 0.48 0.00 6 4 34 0.83 0.00 -10 5 34 2.37 0.00 -9 5 34 -0.59 0.00 5 5 34 -3.53 0.00 6 5 34 -2.26 0.00 -9 6 34 1.07 0.00 -8 6 34 0.41 0.00 4 6 34 3.06 0.00 5 6 34 0.19 0.00 -9 7 34 1.30 0.00 -8 7 34 0.70 0.00 4 7 34 2.12 0.00 5 7 34 0.89 0.00 -8 8 34 -3.33 0.00 -7 8 34 -1.00 0.00 3 8 34 -3.21 0.00 4 8 34 -2.26 0.00 -8 9 34 -1.81 0.00 -7 9 34 -1.43 0.00 -6 9 34 -2.80 0.00 -5 9 34 -0.04 0.00 1 9 34 -0.98 0.00 2 9 34 -0.12 0.00 3 9 34 -2.10 0.00 4 9 34 -1.87 0.00 -7 10 34 0.51 0.00 -6 10 34 -1.66 0.00 -5 10 34 -2.90 0.00 -4 10 34 -3.73 0.00 -3 10 34 1.23 0.00 -2 10 34 0.68 0.00 -1 10 34 2.96 0.00 0 10 34 2.84 0.00 1 10 34 1.81 0.00 2 10 34 1.68 0.00 3 10 34 1.46 0.00 -5 11 34 3.73 0.00 -4 11 34 1.14 0.00 -3 11 34 2.51 0.00 -2 11 34 0.32 0.00 -1 11 34 -0.34 0.00 0 11 34 2.69 0.00 1 11 34 1.32 0.00 -3 12 34 -2.15 0.00 -2 12 34 -0.93 0.00 -1 12 34 -2.28 0.00 -10 1 35 1.88 0.00 -9 1 35 -0.06 0.00 3 1 35 2.75 0.00 4 1 35 0.16 0.00 5 1 35 -0.85 0.00 6 1 35 -0.57 0.00 -10 2 35 3.41 0.00 -9 2 35 -0.32 0.00 -8 2 35 0.54 0.00 4 2 35 -3.06 0.00 5 2 35 -2.80 0.00 6 2 35 -0.50 0.00 -9 3 35 0.49 0.00 -8 3 35 -0.62 0.00 4 3 35 -0.16 0.00 5 3 35 -0.24 0.00 -9 4 35 -0.83 0.00 -8 4 35 -1.76 0.00 4 4 35 3.79 0.00 5 4 35 0.19 0.00 -9 5 35 0.04 0.00 -8 5 35 -0.72 0.00 3 5 35 0.31 0.00 4 5 35 0.00 0.00 5 5 35 2.04 0.00 -8 6 35 1.69 0.00 -7 6 35 0.14 0.00 3 6 35 -3.48 0.00 4 6 35 0.21 0.00 -8 7 35 1.24 0.00 -7 7 35 0.15 0.00 -6 7 35 0.10 0.00 2 7 35 0.85 0.00 3 7 35 0.17 0.00 4 7 35 -0.12 0.00 -7 8 35 -0.41 0.00 -6 8 35 -0.60 0.00 -5 8 35 3.66 0.00 -4 8 35 4.52 0.00 0 8 35 2.49 0.00 1 8 35 1.71 0.00 2 8 35 1.41 0.00 3 8 35 2.45 0.00 -6 9 35 2.71 0.00 -5 9 35 0.81 0.00 -4 9 35 1.58 0.00 -3 9 35 -0.55 0.00 -2 9 35 0.37 0.00 -1 9 35 -1.56 0.00 0 9 35 -1.92 0.00 1 9 35 0.26 0.00 2 9 35 -2.36 0.00 -5 10 35 -2.96 0.00 -4 10 35 -2.30 0.00 -3 10 35 0.10 0.00 -2 10 35 0.71 0.00 -1 10 35 0.51 0.00 0 10 35 -2.24 0.00 1 10 35 -1.77 0.00 -9 0 36 2.08 0.00 -8 0 36 0.36 0.00 -7 0 36 1.60 0.00 3 0 36 -1.60 0.00 4 0 36 3.31 0.00 5 0 36 3.64 0.00 -9 1 36 0.09 0.00 -8 1 36 2.09 0.00 -7 1 36 2.64 0.00 3 1 36 -0.14 0.00 4 1 36 -3.73 0.00 5 1 36 -0.33 0.00 -9 2 36 -0.37 0.00 -8 2 36 -1.16 0.00 -7 2 36 -0.87 0.00 3 2 36 1.36 0.00 4 2 36 -2.15 0.00 -8 3 36 -1.22 0.00 -7 3 36 -2.42 0.00 3 3 36 6.72 0.00 4 3 36 2.00 0.00 -8 4 36 2.11 0.00 -7 4 36 0.39 0.00 -6 4 36 -2.18 0.00 2 4 36 2.05 0.00 3 4 36 -1.23 0.00 4 4 36 -0.34 0.00 -8 5 36 2.25 0.00 -7 5 36 3.49 0.00 -6 5 36 1.98 0.00 1 5 36 1.90 0.00 2 5 36 -3.15 0.00 3 5 36 1.42 0.00 4 5 36 -2.18 0.00 -7 6 36 -0.25 0.00 -6 6 36 0.28 0.00 -5 6 36 0.43 0.00 -4 6 36 -1.07 0.00 0 6 36 0.94 0.00 1 6 36 0.80 0.00 2 6 36 0.11 0.00 3 6 36 3.26 0.00 -6 7 36 -2.45 0.00 -5 7 36 -2.39 0.00 -4 7 36 -1.09 0.00 -3 7 36 -1.98 0.00 -2 7 36 -1.19 0.00 -1 7 36 0.09 0.00 0 7 36 -1.87 0.00 1 7 36 1.51 0.00 2 7 36 -0.25 0.00 -6 8 36 0.86 0.00 -5 8 36 2.28 0.00 -4 8 36 1.91 0.00 -3 8 36 0.03 0.00 -2 8 36 -1.22 0.00 -1 8 36 0.19 0.00 0 8 36 0.01 0.00 1 8 36 -0.43 0.00 -4 9 36 0.28 0.00 -3 9 36 2.82 0.00 -2 9 36 1.05 0.00 -1 9 36 -0.29 0.00 0 9 36 0.22 0.00 -8 1 37 0.41 0.00 -7 1 37 -1.44 0.00 -6 1 37 -0.65 0.00 -5 1 37 -0.73 0.00 1 1 37 -0.23 0.00 2 1 37 -2.61 0.00 3 1 37 -2.07 0.00 -7 2 37 0.58 0.00 -6 2 37 -1.74 0.00 -5 2 37 -0.23 0.00 0 2 37 -1.52 0.00 1 2 37 -6.00 0.00 2 2 37 -4.35 0.00 3 2 37 -7.32 0.00 -7 3 37 1.06 0.00 -6 3 37 0.61 0.00 -5 3 37 -0.36 0.00 -4 3 37 -1.28 0.00 -1 3 37 0.80 0.00 0 3 37 0.96 0.00 1 3 37 2.72 0.00 2 3 37 2.81 0.00 3 3 37 1.23 0.00 -7 4 37 -0.99 0.00 -6 4 37 1.03 0.00 -5 4 37 1.38 0.00 -4 4 37 2.85 0.00 -3 4 37 -0.26 0.00 -2 4 37 -0.67 0.00 -1 4 37 -0.24 0.00 0 4 37 2.90 0.00 1 4 37 1.62 0.00 2 4 37 6.95 0.00 -6 5 37 0.92 0.00 -5 5 37 0.54 0.00 -4 5 37 1.43 0.00 -3 5 37 2.39 0.00 -2 5 37 0.83 0.00 -1 5 37 1.76 0.00 0 5 37 -0.05 0.00 1 5 37 -2.51 0.00 2 5 37 -1.80 0.00 -6 6 37 -0.65 0.00 -5 6 37 -2.63 0.00 -4 6 37 -1.75 0.00 -3 6 37 -0.54 0.00 -2 6 37 0.69 0.00 -1 6 37 -1.43 0.00 0 6 37 -0.09 0.00 1 6 37 -4.69 0.00 -4 7 37 -1.00 0.00 -3 7 37 -1.66 0.00 -2 7 37 -1.69 0.00 -1 7 37 -0.05 0.00 0 7 37 0.39 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 140116) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 -0.069 0.500 0.000 1114 257 ' ' 2 0.078 1.000 0.500 1113 257 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 1 0 0 1.436 1 1 0 1.795 0 2 0 2.154 -1 1 1 1.858 0 1 1 1.277 1 1 1 1.984 1 2 1 2.724 -1 0 2 1.862 0 0 2 1.374 1 0 2 2.105 -1 1 2 2.151 0 1 2 1.746 0 1 3 2.325 -1 0 4 2.942 0 0 4 2.748 3 0 4 5.393 -1 0 6 4.198 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL FF471_0m_a.res in P2(1)/c CELL 14.2851 18.9090 29.8721 90.00 97.01 90.00 SPGR P21/c # Solvent Accessible Volume = 2224 # Electrons Found in S.A.V. = 514 # Note: Atoms in Void as Cxxx and Qxxx all others C101 0.938 0.208 0.421 ! 7.66 eA-3 C102 0.115 0.796 0.120 ! 5.26 eA-3 C103 0.062 0.737 0.573 ! 3.34 eA-3 C104 0.997 0.091 0.472 ! 3.12 eA-3 C105 0.097 0.769 0.074 ! 3.06 eA-3 C106 0.998 0.672 0.041 ! 2.99 eA-3 C107 0.507 0.485 0.002 ! 2.86 eA-3 C108 0.952 0.173 0.470 ! 2.64 eA-3 C109 0.529 0.063 0.496 ! 2.63 eA-3 C110 0.391 0.828 0.462 ! 2.55 eA-3 C111 0.215 0.329 0.139 ! 2.10 eA-3 C112 0.951 0.765 0.391 ! 2.09 eA-3 C113 0.049 0.235 0.609 ! 2.09 eA-3 C114 0.905 0.206 0.071 ! 2.06 eA-3 C115 0.562 0.405 0.042 ! 2.00 eA-3 C116 0.422 0.873 0.475 ! 1.92 eA-3 C117 0.170 0.296 0.148 ! 1.81 eA-3 C118 0.375 0.784 0.435 ! 1.73 eA-3 C119 0.982 0.741 0.398 ! 1.66 eA-3 C120 0.731 0.268 0.049 ! 1.57 eA-3 C121 0.901 0.802 0.356 ! 1.55 eA-3 C122 0.155 0.351 0.114 ! 1.53 eA-3 Q123 0.675 0.767 0.154 ! 1.42 eA-3 Q124 0.519 0.098 0.728 ! 1.41 eA-3 C125 0.892 0.826 0.374 ! 1.41 eA-3 C126 0.119 0.283 0.111 ! 1.40 eA-3 C127 0.871 0.263 0.076 ! 1.38 eA-3 C128 0.059 0.757 0.406 ! 1.37 eA-3 C129 0.814 0.250 0.574 ! 1.30 eA-3 C130 0.186 0.750 0.426 ! 1.30 eA-3 Q131 0.623 0.767 0.147 ! 1.28 eA-3 Q132 0.918 0.418 0.170 ! 1.20 eA-3 Q133 0.155 0.949 0.285 ! 1.18 eA-3 C134 0.333 0.831 0.403 ! 1.16 eA-3 C135 0.123 0.331 0.094 ! 1.15 eA-3 C136 0.750 0.250 0.567 ! 1.13 eA-3 Q137 0.684 0.841 0.153 ! 1.13 eA-3 Q138 0.184 0.954 0.594 ! 1.12 eA-3 C139 0.109 0.373 0.125 ! 1.10 eA-3 Q140 0.379 0.344 0.351 ! 1.07 eA-3 Q141 0.156 0.854 0.293 ! 1.05 eA-3 C142 0.228 0.738 0.413 ! 1.04 eA-3 Q143 0.456 0.873 0.333 ! 1.02 eA-3 C144 0.840 0.755 0.367 ! 0.98 eA-3 Q145 0.168 0.606 0.244 ! 0.97 eA-3 Q146 0.637 0.266 0.677 ! 0.96 eA-3 C147 0.736 0.796 0.358 ! 0.94 eA-3 C148 0.010 0.281 0.416 ! 0.93 eA-3 C149 0.918 0.638 0.897 ! 0.92 eA-3 C150 0.954 0.190 0.040 ! 0.91 eA-3 C151 0.033 0.330 0.098 ! 0.90 eA-3 C152 0.351 0.874 0.422 ! 0.89 eA-3 C153 0.039 0.407 0.076 ! 0.89 eA-3 Q154 0.561 0.906 0.367 ! 0.88 eA-3 C155 0.136 0.713 0.086 ! 0.87 eA-3 C156 0.108 0.669 0.463 ! 0.87 eA-3 Q157 0.168 0.661 0.238 ! 0.86 eA-3 Q158 0.832 0.152 0.269 ! 0.86 eA-3 C159 0.787 0.298 0.036 ! 0.86 eA-3 C160 0.127 0.863 0.097 ! 0.86 eA-3 Q161 0.120 0.613 0.281 ! 0.84 eA-3 C162 0.035 0.808 0.115 ! 0.83 eA-3 Q163 0.813 0.377 0.238 ! 0.83 eA-3 C164 0.984 0.261 0.122 ! 0.83 eA-3 Q165 0.886 0.500 0.202 ! 0.82 eA-3 C166 0.966 0.890 0.442 ! 0.81 eA-3 C167 0.954 0.825 0.371 ! 0.80 eA-3 C168 0.863 0.175 0.466 ! 0.79 eA-3 Q169 0.440 0.201 0.842 ! 0.78 eA-3 C170 0.901 0.364 0.369 ! 0.78 eA-3 C171 0.125 0.796 0.566 ! 0.78 eA-3 C172 0.986 0.689 0.437 ! 0.78 eA-3 C173 0.378 0.924 0.444 ! 0.76 eA-3 Q174 0.703 0.999 0.354 ! 0.74 eA-3 C175 0.238 0.339 0.179 ! 0.74 eA-3 Q176 0.704 0.937 0.166 ! 0.73 eA-3 C177 0.939 0.091 0.502 ! 0.73 eA-3 C178 0.045 0.296 0.053 ! 0.72 eA-3 Q179 0.201 0.541 0.168 ! 0.72 eA-3 Q180 0.797 0.221 0.421 ! 0.72 eA-3 Q181 0.413 0.439 0.195 ! 0.72 eA-3 Q182 0.685 0.918 0.663 ! 0.71 eA-3 C183 0.365 0.890 0.466 ! 0.71 eA-3 Q184 0.718 0.799 0.184 ! 0.71 eA-3 C185 0.909 0.281 0.026 ! 0.70 eA-3 Q186 0.719 0.623 0.370 ! 0.70 eA-3 C187 0.543 0.047 0.452 ! 0.70 eA-3 C188 0.016 0.121 0.520 ! 0.70 eA-3 C189 0.095 0.408 0.072 ! 0.69 eA-3 Q190 0.301 0.154 0.346 ! 0.69 eA-3 C191 0.145 0.687 0.948 ! 0.68 eA-3 C192 0.012 0.551 0.012 ! 0.68 eA-3 C193 0.310 0.780 0.385 ! 0.68 eA-3 C194 0.844 0.245 0.454 ! 0.67 eA-3 Q195 0.164 0.720 0.242 ! 0.67 eA-3 C196 0.044 0.828 0.414 ! 0.66 eA-3 Q197 0.439 0.067 0.475 ! 0.66 eA-3 Q198 0.582 0.577 0.841 ! 0.65 eA-3 Q199 0.111 0.705 0.374 ! 0.65 eA-3 ) ; _shelx_fab_checksum 9838 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.64765(2) 0.69855(2) 0.65196(2) 0.01749(11) Uani 1 1 d . . . . . P1 P 0.49384(7) 0.68440(5) 0.62508(3) 0.0200(2) Uani 1 1 d . . . . . P4 P 0.67141(7) 0.69031(5) 0.58010(3) 0.0179(2) Uani 1 1 d . . . . . P3 P 0.74188(7) 0.60268(5) 0.66163(3) 0.0196(2) Uani 1 1 d . . . . . P2 P 0.71650(7) 0.80626(5) 0.64826(3) 0.0215(2) Uani 1 1 d . . . . . N3 N 0.7934(2) 0.58807(16) 0.61249(10) 0.0217(7) Uani 1 1 d . . . . . N1 N 0.4846(2) 0.66433(17) 0.56772(10) 0.0221(7) Uani 1 1 d . . . . . F9 F 0.1969(2) 0.4374(2) 0.69488(12) 0.0726(11) Uani 1 1 d . . . . . N2 N 0.7344(2) 0.82342(17) 0.59278(10) 0.0236(7) Uani 1 1 d . . . . . N4 N 0.6298(2) 0.70622(16) 0.71939(11) 0.0213(7) Uani 1 1 d . . . . . F6 F 0.5017(3) 0.3268(2) 0.73309(13) 0.0786(12) Uani 1 1 d . . . . . F8 F 0.2274(3) 0.39624(19) 0.63170(13) 0.0769(11) Uani 1 1 d . . . . . C42 C 0.4239(3) 0.6098(2) 0.64276(12) 0.0241(8) Uani 1 1 d . . . . . F12 F 0.2638(3) 0.99379(18) 0.60706(13) 0.0842(13) Uani 1 1 d . . . . . F7 F 0.3208(3) 0.3760(2) 0.69320(16) 0.0933(15) Uani 1 1 d . . . . . F5 F 0.5021(3) 0.29803(18) 0.66382(13) 0.0825(13) Uani 1 1 d . . . . . C63 C 0.8338(3) 0.8211(2) 0.67912(13) 0.0249(8) Uani 1 1 d . . . . . C49 C 0.4115(3) 0.7580(2) 0.62582(13) 0.0241(8) Uani 1 1 d . . . . . C18 C 0.4107(3) 0.6331(2) 0.54001(12) 0.0231(8) Uani 1 1 d . . . . . C10 C 0.5674(3) 0.65481(19) 0.54641(12) 0.0220(8) Uani 1 1 d . . . . . C35 C 0.6921(3) 0.51551(19) 0.67254(12) 0.0232(8) Uani 1 1 d . . . . . C13 C 0.4468(3) 0.6047(2) 0.50229(12) 0.0259(9) Uani 1 1 d . . . . . C69 C 0.9140(3) 0.8325(2) 0.65834(14) 0.0301(9) Uani 1 1 d . . . . . H69 H 0.9089 0.8365 0.6271 0.036 Uiso 1 1 calc R U . . . F4 F 0.6188(3) 0.27156(18) 0.71413(17) 0.0989(15) Uani 1 1 d . . . . . C28 C 0.8473(3) 0.60181(19) 0.70358(12) 0.0217(8) Uani 1 1 d . . . . . C27 C 0.7523(3) 0.8872(2) 0.57219(14) 0.0280(9) Uani 1 1 d . . . . . C47 C 0.4514(3) 0.5424(2) 0.63073(13) 0.0284(9) Uani 1 1 d . . . . . H47 H 0.5047 0.5372 0.6160 0.034 Uiso 1 1 calc R U . . . C2 C 0.8378(3) 0.6258(2) 0.54558(13) 0.0282(9) Uani 1 1 d . . . . . C9 C 0.8759(3) 0.5518(2) 0.60597(13) 0.0271(9) Uani 1 1 d . . . . . C40 C 0.7037(4) 0.4554(2) 0.64674(14) 0.0354(10) Uani 1 1 d . . . . . H40 H 0.7412 0.4573 0.6234 0.042 Uiso 1 1 calc R U . . . C1 C 0.7721(3) 0.6334(2) 0.57465(12) 0.0220(8) Uani 1 1 d . . . . . C46 C 0.4012(3) 0.4837(2) 0.64015(14) 0.0332(10) Uani 1 1 d . . . . . H46 H 0.4201 0.4393 0.6313 0.040 Uiso 1 1 calc R U . . . C11 C 0.5459(3) 0.6184(2) 0.50675(12) 0.0242(8) Uani 1 1 d . . . . . C4 C 0.9029(3) 0.5739(2) 0.56435(13) 0.0291(9) Uani 1 1 d . . . . . C26 C 0.7884(3) 0.9505(2) 0.59129(16) 0.0367(10) Uani 1 1 d . . . . . H26 H 0.8041 0.9554 0.6223 0.044 Uiso 1 1 calc R U . . . C8 C 0.9266(3) 0.5015(2) 0.63239(15) 0.0361(10) Uani 1 1 d . . . . . H8 H 0.9071 0.4862 0.6594 0.043 Uiso 1 1 calc R U . . . C54 C 0.3702(3) 0.7930(2) 0.58687(14) 0.0335(10) Uani 1 1 d . . . . . H54 H 0.3787 0.7753 0.5586 0.040 Uiso 1 1 calc R U . . . F16 F 1.1540(3) 0.8930(2) 0.7463(2) 0.127(2) Uani 1 1 d . . . . . C50 C 0.3970(3) 0.7852(2) 0.66765(14) 0.0343(10) Uani 1 1 d . . . . . H50 H 0.4249 0.7631 0.6938 0.041 Uiso 1 1 calc R U . . . F11 F 0.2612(4) 0.9757(2) 0.67497(13) 0.1116(19) Uani 1 1 d . . . . . C17 C 0.3154(3) 0.6270(2) 0.54604(13) 0.0312(9) Uani 1 1 d . . . . . H17 H 0.2917 0.6465 0.5710 0.037 Uiso 1 1 calc R U . . . N5 N 0.6255(3) 0.7097(2) 0.75462(13) 0.0463(11) Uani 1 1 d . . . . . C33 C 0.9230(3) 0.6444(2) 0.69583(14) 0.0297(9) Uani 1 1 d . . . . . H33 H 0.9175 0.6741 0.6708 0.036 Uiso 1 1 calc R U . . . C36 C 0.6360(3) 0.5110(2) 0.70690(15) 0.0353(10) Uani 1 1 d . . . . . H36 H 0.6267 0.5513 0.7237 0.042 Uiso 1 1 calc R U . . . C20 C 0.6910(3) 0.8094(2) 0.51736(14) 0.0303(9) Uani 1 1 d . . . . . C32 C 1.0066(3) 0.6435(2) 0.72471(15) 0.0342(10) Uani 1 1 d . . . . . H32 H 1.0571 0.6715 0.7187 0.041 Uiso 1 1 calc R U . . . C19 C 0.6978(3) 0.7760(2) 0.55813(12) 0.0236(8) Uani 1 1 d . . . . . C64 C 0.8437(3) 0.8136(2) 0.72643(14) 0.0321(10) Uani 1 1 d . . . . . H64 H 0.7912 0.8039 0.7409 0.039 Uiso 1 1 calc R U . . . F10 F 0.1562(3) 0.9348(2) 0.6306(3) 0.146(3) Uani 1 1 d . . . . . F13 F 0.4282(5) 1.0689(2) 0.6982(2) 0.146(3) Uani 1 1 d . . . . . C43 C 0.3462(3) 0.6156(2) 0.66644(14) 0.0352(10) Uani 1 1 d . . . . . H43 H 0.3274 0.6597 0.6759 0.042 Uiso 1 1 calc R U . . . C52 C 0.3019(3) 0.8787(2) 0.63235(15) 0.0333(10) Uani 1 1 d . . . . . C51 C 0.3412(3) 0.8450(2) 0.67102(15) 0.0352(10) Uani 1 1 d . . . . . H51 H 0.3307 0.8620 0.6992 0.042 Uiso 1 1 calc R U . . . C62 C 0.5734(3) 0.9040(2) 0.63028(16) 0.0380(11) Uani 1 1 d . . . . . H62 H 0.5533 0.8730 0.6069 0.046 Uiso 1 1 calc R U . . . C53 C 0.3171(4) 0.8531(2) 0.59021(15) 0.0382(11) Uani 1 1 d . . . . . H53 H 0.2914 0.8766 0.5642 0.046 Uiso 1 1 calc R U . . . C5 C 0.9856(3) 0.5460(3) 0.55014(15) 0.0400(11) Uani 1 1 d . . . . . H5 H 1.0060 0.5609 0.5233 0.048 Uiso 1 1 calc R U . . . C3 C 0.8460(3) 0.6636(3) 0.50239(14) 0.0406(11) Uani 1 1 d . . . . . H3A H 0.8154 0.7088 0.5027 0.061 Uiso 1 1 calc R U . . . H3B H 0.8164 0.6360 0.4776 0.061 Uiso 1 1 calc R U . . . H3C H 0.9114 0.6703 0.4990 0.061 Uiso 1 1 calc R U . . . C22 C 0.7276(3) 0.8797(2) 0.52575(14) 0.0311(9) Uani 1 1 d . . . . . C56 C 0.6539(3) 0.8881(2) 0.65996(14) 0.0274(9) Uani 1 1 d . . . . . C38 C 0.6049(4) 0.3896(2) 0.69114(16) 0.0420(12) Uani 1 1 d . . . . . C68 C 1.0013(3) 0.8380(2) 0.68337(15) 0.0361(10) Uani 1 1 d . . . . . H68 H 1.0547 0.8450 0.6689 0.043 Uiso 1 1 calc R U . . . C39 C 0.6596(4) 0.3930(2) 0.65595(15) 0.0420(12) Uani 1 1 d . . . . . H39 H 0.6665 0.3531 0.6385 0.050 Uiso 1 1 calc R U . . . C6 C 1.0353(4) 0.4964(3) 0.57674(17) 0.0515(14) Uani 1 1 d . . . . . H6 H 1.0894 0.4769 0.5673 0.062 Uiso 1 1 calc R U . . . C21 C 0.6534(4) 0.7821(3) 0.47147(14) 0.0440(12) Uani 1 1 d . . . . . H21A H 0.7051 0.7709 0.4549 0.066 Uiso 1 1 calc R U . . . H21B H 0.6145 0.8175 0.4555 0.066 Uiso 1 1 calc R U . . . H21C H 0.6167 0.7402 0.4746 0.066 Uiso 1 1 calc R U . . . C61 C 0.5230(3) 0.9657(2) 0.6354(2) 0.0450(12) Uani 1 1 d . . . . . H61 H 0.4703 0.9767 0.6152 0.054 Uiso 1 1 calc R U . . . C30 C 0.9380(4) 0.5601(3) 0.77174(16) 0.0442(12) Uani 1 1 d . . . . . H30 H 0.9422 0.5324 0.7976 0.053 Uiso 1 1 calc R U . . . C14 C 0.3862(3) 0.5687(2) 0.46946(14) 0.0362(10) Uani 1 1 d . . . . . H14 H 0.4088 0.5497 0.4441 0.043 Uiso 1 1 calc R U . . . C29 C 0.8560(3) 0.5608(2) 0.74266(14) 0.0356(10) Uani 1 1 d . . . . . H29 H 0.8053 0.5334 0.7491 0.043 Uiso 1 1 calc R U . . . C12 C 0.6090(3) 0.5953(3) 0.47331(14) 0.0389(11) Uani 1 1 d . . . . . H12A H 0.5977 0.6242 0.4467 0.058 Uiso 1 1 calc R U . . . H12B H 0.5965 0.5468 0.4654 0.058 Uiso 1 1 calc R U . . . H12C H 0.6736 0.6003 0.4862 0.058 Uiso 1 1 calc R U . . . C45 C 0.3231(3) 0.4901(3) 0.66264(15) 0.0383(11) Uani 1 1 d . . . . . C7 C 1.0075(4) 0.4746(3) 0.61719(17) 0.0493(13) Uani 1 1 d . . . . . H7 H 1.0435 0.4413 0.6345 0.059 Uiso 1 1 calc R U . . . C57 C 0.6815(4) 0.9334(2) 0.69508(16) 0.0399(11) Uani 1 1 d . . . . . H57 H 0.7348 0.9232 0.7152 0.048 Uiso 1 1 calc R U . . . C37 C 0.5932(3) 0.4484(2) 0.71723(16) 0.0399(11) Uani 1 1 d . . . . . H37 H 0.5574 0.4460 0.7412 0.048 Uiso 1 1 calc R U . . . C66 C 1.0100(3) 0.8331(2) 0.73020(15) 0.0328(10) Uani 1 1 d . . . . . F18 F 1.1593(3) 0.7865(2) 0.7513(2) 0.150(3) Uani 1 1 d . . . . . C55 C 0.2452(4) 0.9451(3) 0.63565(19) 0.0457(12) Uani 1 1 d . . . . . C44 C 0.2966(3) 0.5549(3) 0.67591(17) 0.0443(12) Uani 1 1 d . . . . . H44 H 0.2445 0.5589 0.6916 0.053 Uiso 1 1 calc R U . . . C58 C 0.6291(4) 0.9951(3) 0.7006(2) 0.0539(14) Uani 1 1 d . . . . . H58 H 0.6471 1.0253 0.7246 0.065 Uiso 1 1 calc R U . . . C23 C 0.7397(4) 0.9361(3) 0.49698(17) 0.0475(13) Uani 1 1 d . . . . . H23 H 0.7232 0.9316 0.4660 0.057 Uiso 1 1 calc R U . . . C15 C 0.2928(4) 0.5618(3) 0.47540(16) 0.0446(12) Uani 1 1 d . . . . . H15 H 0.2521 0.5377 0.4540 0.054 Uiso 1 1 calc R U . . . C31 C 1.0146(3) 0.6004(2) 0.76274(15) 0.0375(11) Uani 1 1 d . . . . . C65 C 0.9309(3) 0.8207(2) 0.75118(15) 0.0359(10) Uani 1 1 d . . . . . H65 H 0.9366 0.8170 0.7824 0.043 Uiso 1 1 calc R U . . . C25 C 0.7996(4) 1.0054(3) 0.56203(19) 0.0480(13) Uani 1 1 d . . . . . H25 H 0.8234 1.0483 0.5736 0.058 Uiso 1 1 calc R U . . . C48 C 0.2681(4) 0.4255(3) 0.6708(2) 0.0547(15) Uani 1 1 d . . . . . C67 C 1.1050(4) 0.8391(3) 0.75669(18) 0.0491(13) Uani 1 1 d . . . . . C59 C 0.5520(4) 1.0105(2) 0.6708(2) 0.0452(13) Uani 1 1 d . . . . . C16 C 0.2581(3) 0.5906(3) 0.51302(14) 0.0382(11) Uani 1 1 d . . . . . H16 H 0.1945 0.5852 0.5161 0.046 Uiso 1 1 calc R U . . . F17 F 1.1042(3) 0.8445(5) 0.79939(15) 0.163(3) Uani 1 1 d . . . . . C41 C 0.5591(5) 0.3206(3) 0.6999(2) 0.0604(17) Uani 1 1 d . . . . . F14 F 0.4516(6) 1.1013(3) 0.6391(2) 0.168(3) Uani 1 1 d . . . . . C24 C 0.7761(4) 0.9981(3) 0.51497(19) 0.0538(14) Uani 1 1 d . . . . . H24 H 0.7854 1.0359 0.4961 0.065 Uiso 1 1 calc R U . . . F1 F 1.1776(3) 0.6083(5) 0.77375(19) 0.173(3) Uani 1 1 d . . . . . C34 C 1.1036(4) 0.5964(4) 0.7932(2) 0.0595(16) Uani 1 1 d . . . . . C60 C 0.4980(5) 1.0772(3) 0.6768(3) 0.073(2) Uani 1 1 d . . . . . F3 F 1.1165(5) 0.6473(5) 0.8202(3) 0.209(4) Uani 1 1 d . . . . . F2 F 1.1166(5) 0.5445(4) 0.8154(3) 0.253(6) Uani 1 1 d . . . . . F15 F 0.5459(4) 1.1265(3) 0.6915(4) 0.278(6) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.02144(18) 0.01601(18) 0.01476(16) -0.00060(10) 0.00119(11) -0.00060(11) P1 0.0201(5) 0.0236(5) 0.0164(4) -0.0022(4) 0.0022(4) 0.0016(4) P4 0.0207(5) 0.0176(5) 0.0152(4) -0.0003(3) 0.0014(4) 0.0000(4) P3 0.0249(5) 0.0160(5) 0.0180(4) 0.0013(4) 0.0031(4) -0.0011(4) P2 0.0258(5) 0.0173(5) 0.0213(5) -0.0014(4) 0.0021(4) -0.0009(4) N3 0.0224(16) 0.0207(16) 0.0220(15) 0.0014(13) 0.0029(13) 0.0045(13) N1 0.0233(17) 0.0245(17) 0.0173(14) -0.0059(13) -0.0031(13) 0.0010(13) F9 0.051(2) 0.090(3) 0.076(2) 0.039(2) 0.0075(18) -0.0250(18) N2 0.0268(18) 0.0184(16) 0.0247(16) 0.0042(13) -0.0010(14) -0.0056(14) N4 0.0244(17) 0.0180(16) 0.0204(17) 0.0006(12) -0.0023(13) -0.0009(13) F6 0.089(3) 0.071(2) 0.072(2) 0.032(2) -0.006(2) -0.042(2) F8 0.076(3) 0.058(2) 0.094(3) 0.0001(19) -0.001(2) -0.0350(19) C42 0.0195(19) 0.032(2) 0.0199(17) 0.0034(16) -0.0018(15) -0.0051(16) F12 0.126(4) 0.049(2) 0.087(2) 0.0333(19) 0.052(2) 0.046(2) F7 0.065(2) 0.069(2) 0.142(4) 0.067(3) -0.003(2) -0.0139(19) F5 0.114(3) 0.054(2) 0.072(2) 0.0068(17) -0.018(2) -0.050(2) C63 0.027(2) 0.0150(18) 0.032(2) -0.0057(16) -0.0001(17) -0.0018(16) C49 0.0164(18) 0.028(2) 0.0275(19) -0.0011(16) 0.0015(15) 0.0022(16) C18 0.028(2) 0.0198(19) 0.0204(17) -0.0012(15) -0.0027(16) -0.0015(16) C10 0.025(2) 0.0190(19) 0.0220(17) -0.0007(15) 0.0034(15) 0.0041(15) C35 0.031(2) 0.0167(19) 0.0204(17) 0.0048(14) -0.0027(16) -0.0021(16) C13 0.031(2) 0.024(2) 0.0216(18) -0.0023(15) -0.0007(16) -0.0015(17) C69 0.030(2) 0.031(2) 0.030(2) 0.0023(18) 0.0016(18) -0.0026(18) F4 0.099(3) 0.0336(18) 0.156(4) 0.036(2) -0.019(3) -0.0143(19) C28 0.0228(19) 0.0178(19) 0.0237(17) -0.0056(15) -0.0004(15) 0.0026(15) C27 0.029(2) 0.021(2) 0.034(2) 0.0090(17) 0.0025(17) -0.0041(17) C47 0.029(2) 0.031(2) 0.0251(19) -0.0030(17) 0.0042(17) -0.0031(18) C2 0.029(2) 0.033(2) 0.0227(18) -0.0048(17) 0.0035(17) -0.0013(18) C9 0.029(2) 0.026(2) 0.0254(19) -0.0069(16) 0.0009(17) 0.0014(17) C40 0.049(3) 0.026(2) 0.029(2) -0.0029(17) -0.005(2) -0.002(2) C1 0.022(2) 0.0216(19) 0.0217(17) -0.0028(15) -0.0001(15) 0.0015(15) C46 0.037(2) 0.030(2) 0.031(2) 0.0019(18) -0.0031(19) -0.0043(19) C11 0.028(2) 0.023(2) 0.0218(17) -0.0047(15) 0.0019(16) 0.0008(16) C4 0.027(2) 0.034(2) 0.0264(19) -0.0099(17) 0.0058(17) 0.0013(18) C26 0.046(3) 0.022(2) 0.042(2) 0.0081(19) 0.004(2) -0.009(2) C8 0.042(3) 0.030(2) 0.035(2) -0.0026(19) 0.001(2) 0.015(2) C54 0.043(3) 0.035(2) 0.0222(19) -0.0035(17) 0.0016(18) 0.002(2) F16 0.073(3) 0.088(3) 0.198(5) 0.062(3) -0.075(3) -0.050(2) C50 0.045(3) 0.033(2) 0.025(2) -0.0053(18) 0.0038(19) 0.006(2) F11 0.206(6) 0.062(2) 0.068(2) -0.007(2) 0.021(3) 0.073(3) C17 0.027(2) 0.040(3) 0.0257(19) -0.0039(18) 0.0009(17) 0.0004(19) N5 0.070(3) 0.041(2) 0.030(2) -0.0003(17) 0.015(2) 0.000(2) C33 0.036(2) 0.020(2) 0.032(2) 0.0054(17) -0.0016(18) 0.0018(17) C36 0.042(3) 0.028(2) 0.037(2) 0.0027(18) 0.006(2) -0.0043(19) C20 0.032(2) 0.032(2) 0.027(2) 0.0096(17) 0.0018(18) -0.0009(18) C32 0.026(2) 0.027(2) 0.047(3) -0.0035(19) -0.004(2) -0.0008(18) C19 0.023(2) 0.023(2) 0.0231(18) 0.0011(16) -0.0013(16) 0.0021(16) C64 0.038(3) 0.030(2) 0.028(2) -0.0017(17) 0.0040(19) -0.0034(19) F10 0.049(2) 0.042(2) 0.352(9) -0.015(3) 0.045(4) 0.0173(18) F13 0.204(6) 0.076(3) 0.187(5) 0.030(3) 0.141(5) 0.071(4) C43 0.033(2) 0.038(3) 0.036(2) 0.0121(19) 0.0086(19) 0.007(2) C52 0.032(2) 0.027(2) 0.042(2) 0.0002(19) 0.009(2) 0.0040(18) C51 0.036(3) 0.036(3) 0.035(2) -0.0062(19) 0.012(2) 0.006(2) C62 0.039(3) 0.027(2) 0.047(3) 0.000(2) 0.004(2) -0.006(2) C53 0.051(3) 0.031(2) 0.033(2) 0.0080(19) 0.001(2) 0.011(2) C5 0.037(3) 0.051(3) 0.032(2) -0.007(2) 0.008(2) 0.011(2) C3 0.037(3) 0.058(3) 0.030(2) 0.004(2) 0.014(2) 0.009(2) C22 0.030(2) 0.028(2) 0.035(2) 0.0105(18) 0.0040(18) 0.0005(18) C56 0.035(2) 0.0124(18) 0.036(2) 0.0056(16) 0.0068(18) 0.0045(16) C38 0.049(3) 0.027(2) 0.044(3) 0.011(2) -0.017(2) -0.013(2) C68 0.027(2) 0.039(3) 0.041(2) 0.001(2) 0.0008(19) -0.0023(19) C39 0.058(3) 0.022(2) 0.041(3) -0.0035(19) -0.012(2) -0.006(2) C6 0.043(3) 0.063(3) 0.049(3) -0.015(3) 0.007(2) 0.024(3) C21 0.060(3) 0.048(3) 0.022(2) 0.010(2) -0.003(2) -0.005(2) C61 0.032(3) 0.023(2) 0.080(4) 0.007(2) 0.009(2) 0.0034(19) C30 0.051(3) 0.044(3) 0.034(2) 0.014(2) -0.008(2) 0.000(2) C14 0.038(3) 0.045(3) 0.024(2) -0.0120(19) -0.0033(18) -0.005(2) C29 0.036(2) 0.040(3) 0.028(2) 0.0083(19) -0.0031(19) -0.004(2) C12 0.038(3) 0.053(3) 0.026(2) -0.017(2) 0.0042(19) 0.002(2) C45 0.035(3) 0.045(3) 0.032(2) 0.016(2) -0.0079(19) -0.008(2) C7 0.051(3) 0.050(3) 0.044(3) -0.007(2) -0.003(2) 0.021(3) C57 0.043(3) 0.033(2) 0.043(2) -0.011(2) 0.002(2) 0.002(2) C37 0.041(3) 0.036(3) 0.042(2) 0.013(2) 0.001(2) -0.012(2) C66 0.030(2) 0.022(2) 0.043(2) -0.0038(18) -0.0082(19) -0.0005(18) F18 0.070(3) 0.078(3) 0.273(8) -0.043(4) -0.096(4) 0.025(2) C55 0.048(3) 0.029(3) 0.062(3) -0.002(2) 0.012(3) 0.008(2) C44 0.032(3) 0.056(3) 0.047(3) 0.020(2) 0.013(2) 0.006(2) C58 0.056(4) 0.033(3) 0.075(4) -0.022(3) 0.014(3) -0.002(2) C23 0.052(3) 0.045(3) 0.044(3) 0.027(2) 0.002(2) -0.006(2) C15 0.039(3) 0.055(3) 0.037(2) -0.012(2) -0.007(2) -0.016(2) C31 0.035(3) 0.034(2) 0.039(2) -0.004(2) -0.011(2) 0.004(2) C65 0.036(3) 0.036(2) 0.033(2) -0.0073(19) -0.008(2) 0.001(2) C25 0.050(3) 0.027(2) 0.065(3) 0.015(2) 0.000(3) -0.011(2) C48 0.041(3) 0.048(3) 0.073(4) 0.025(3) 0.000(3) -0.009(2) C67 0.046(3) 0.039(3) 0.056(3) -0.005(2) -0.020(3) -0.005(2) C59 0.040(3) 0.020(2) 0.080(4) -0.002(2) 0.025(3) 0.001(2) C16 0.030(2) 0.050(3) 0.033(2) -0.001(2) -0.0048(19) -0.010(2) F17 0.055(3) 0.364(10) 0.063(3) -0.030(4) -0.021(2) -0.038(4) C41 0.070(4) 0.038(3) 0.065(4) 0.019(3) -0.025(3) -0.025(3) F14 0.243(8) 0.110(4) 0.166(5) 0.048(4) 0.085(6) 0.133(5) C24 0.062(4) 0.037(3) 0.062(3) 0.029(3) 0.003(3) -0.007(3) F1 0.042(3) 0.358(11) 0.113(4) 0.043(5) -0.021(3) 0.023(4) C34 0.038(3) 0.075(4) 0.059(3) 0.010(3) -0.021(3) 0.002(3) C60 0.078(5) 0.019(3) 0.128(6) 0.008(3) 0.039(5) 0.009(3) F3 0.114(5) 0.306(11) 0.177(6) -0.135(7) -0.099(5) 0.056(6) F2 0.128(5) 0.216(7) 0.361(11) 0.214(8) -0.181(7) -0.083(5) F15 0.100(4) 0.048(3) 0.654(18) -0.142(6) -0.080(7) 0.036(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 N4 Ru1 P4 178.31(9) . . N4 Ru1 P3 94.26(9) . . P4 Ru1 P3 84.73(3) . . N4 Ru1 P1 97.13(9) . . P4 Ru1 P1 84.54(4) . . P3 Ru1 P1 119.28(4) . . N4 Ru1 P2 95.18(9) . . P4 Ru1 P2 84.13(4) . . P3 Ru1 P2 118.16(4) . . P1 Ru1 P2 119.79(4) . . N1 P1 C49 101.91(16) . . N1 P1 C42 97.84(17) . . C49 P1 C42 101.98(19) . . N1 P1 Ru1 109.17(12) . . C49 P1 Ru1 120.35(13) . . C42 P1 Ru1 121.75(13) . . C19 P4 C10 108.84(17) . . C19 P4 C1 107.25(18) . . C10 P4 C1 109.48(17) . . C19 P4 Ru1 110.60(13) . . C10 P4 Ru1 110.49(13) . . C1 P4 Ru1 110.11(12) . . N3 P3 C28 100.26(16) . . N3 P3 C35 102.67(16) . . C28 P3 C35 99.99(17) . . N3 P3 Ru1 109.05(11) . . C28 P3 Ru1 121.39(12) . . C35 P3 Ru1 120.34(14) . . N2 P2 C63 102.65(18) . . N2 P2 C56 98.94(17) . . C63 P2 C56 102.21(18) . . N2 P2 Ru1 109.20(11) . . C63 P2 Ru1 119.20(13) . . C56 P2 Ru1 121.40(14) . . C9 N3 C1 106.7(3) . . C9 N3 P3 130.2(3) . . C1 N3 P3 120.2(2) . . C18 N1 C10 107.0(3) . . C18 N1 P1 129.6(3) . . C10 N1 P1 120.0(2) . . C27 N2 C19 107.2(3) . . C27 N2 P2 129.8(3) . . C19 N2 P2 119.5(3) . . N5 N4 Ru1 176.2(4) . . C43 C42 C47 118.1(4) . . C43 C42 P1 125.4(3) . . C47 C42 P1 116.5(3) . . C69 C63 C64 118.5(4) . . C69 C63 P2 123.7(3) . . C64 C63 P2 117.6(3) . . C50 C49 C54 118.5(4) . . C50 C49 P1 117.4(3) . . C54 C49 P1 123.7(3) . . N1 C18 C17 129.6(4) . . N1 C18 C13 108.3(3) . . C17 C18 C13 122.0(3) . . C11 C10 N1 109.9(3) . . C11 C10 P4 138.1(3) . . N1 C10 P4 111.9(2) . . C36 C35 C40 118.7(4) . . C36 C35 P3 117.4(3) . . C40 C35 P3 123.9(3) . . C18 C13 C14 119.4(4) . . C18 C13 C11 108.2(3) . . C14 C13 C11 132.3(4) . . C68 C69 C63 120.8(4) . . C68 C69 H69 119.6 . . C63 C69 H69 119.6 . . C33 C28 C29 118.0(4) . . C33 C28 P3 118.1(3) . . C29 C28 P3 123.9(3) . . N2 C27 C22 108.3(4) . . N2 C27 C26 129.8(4) . . C22 C27 C26 121.9(4) . . C46 C47 C42 121.2(4) . . C46 C47 H47 119.4 . . C42 C47 H47 119.4 . . C1 C2 C4 106.9(3) . . C1 C2 C3 129.4(4) . . C4 C2 C3 123.8(4) . . C8 C9 N3 130.5(4) . . C8 C9 C4 121.8(4) . . N3 C9 C4 107.7(3) . . C39 C40 C35 119.9(4) . . C39 C40 H40 120.1 . . C35 C40 H40 120.1 . . C2 C1 N3 110.3(3) . . C2 C1 P4 137.1(3) . . N3 C1 P4 112.4(3) . . C47 C46 C45 120.3(4) . . C47 C46 H46 119.8 . . C45 C46 H46 119.8 . . C10 C11 C13 106.6(3) . . C10 C11 C12 129.5(4) . . C13 C11 C12 123.9(3) . . C5 C4 C9 119.1(4) . . C5 C4 C2 132.4(4) . . C9 C4 C2 108.5(4) . . C25 C26 C27 116.9(4) . . C25 C26 H26 121.6 . . C27 C26 H26 121.6 . . C9 C8 C7 117.7(4) . . C9 C8 H8 121.2 . . C7 C8 H8 121.2 . . C53 C54 C49 120.5(4) . . C53 C54 H54 119.7 . . C49 C54 H54 119.7 . . C49 C50 C51 120.9(4) . . C49 C50 H50 119.5 . . C51 C50 H50 119.5 . . C16 C17 C18 116.6(4) . . C16 C17 H17 121.7 . . C18 C17 H17 121.7 . . C32 C33 C28 121.2(4) . . C32 C33 H33 119.4 . . C28 C33 H33 119.4 . . C35 C36 C37 122.1(4) . . C35 C36 H36 118.9 . . C37 C36 H36 118.9 . . C19 C20 C22 106.7(4) . . C19 C20 C21 129.4(4) . . C22 C20 C21 124.0(4) . . C33 C32 C31 119.7(4) . . C33 C32 H32 120.2 . . C31 C32 H32 120.2 . . C20 C19 N2 109.8(3) . . C20 C19 P4 138.1(3) . . N2 C19 P4 112.1(3) . . C65 C64 C63 120.2(4) . . C65 C64 H64 119.9 . . C63 C64 H64 119.9 . . C42 C43 C44 119.6(4) . . C42 C43 H43 120.2 . . C44 C43 H43 120.2 . . C51 C52 C53 120.3(4) . . C51 C52 C55 119.9(4) . . C53 C52 C55 119.7(4) . . C52 C51 C50 119.5(4) . . C52 C51 H51 120.2 . . C50 C51 H51 120.2 . . C61 C62 C56 120.6(4) . . C61 C62 H62 119.7 . . C56 C62 H62 119.7 . . C54 C53 C52 120.1(4) . . C54 C53 H53 119.9 . . C52 C53 H53 119.9 . . C6 C5 C4 118.5(4) . . C6 C5 H5 120.7 . . C4 C5 H5 120.7 . . C2 C3 H3A 109.5 . . C2 C3 H3B 109.5 . . H3A C3 H3B 109.5 . . C2 C3 H3C 109.5 . . H3A C3 H3C 109.5 . . H3B C3 H3C 109.5 . . C23 C22 C27 120.0(4) . . C23 C22 C20 132.0(4) . . C27 C22 C20 108.0(4) . . C57 C56 C62 119.2(4) . . C57 C56 P2 124.6(3) . . C62 C56 P2 116.2(3) . . C37 C38 C39 120.7(4) . . C37 C38 C41 121.2(5) . . C39 C38 C41 118.1(5) . . C69 C68 C66 120.3(4) . . C69 C68 H68 119.9 . . C66 C68 H68 119.9 . . C40 C39 C38 120.3(4) . . C40 C39 H39 119.9 . . C38 C39 H39 119.9 . . C5 C6 C7 121.9(5) . . C5 C6 H6 119.1 . . C7 C6 H6 119.1 . . C20 C21 H21A 109.5 . . C20 C21 H21B 109.5 . . H21A C21 H21B 109.5 . . C20 C21 H21C 109.5 . . H21A C21 H21C 109.5 . . H21B C21 H21C 109.5 . . C59 C61 C62 119.3(5) . . C59 C61 H61 120.3 . . C62 C61 H61 120.3 . . C29 C30 C31 120.3(4) . . C29 C30 H30 119.8 . . C31 C30 H30 119.8 . . C15 C14 C13 118.8(4) . . C15 C14 H14 120.6 . . C13 C14 H14 120.6 . . C30 C29 C28 121.2(4) . . C30 C29 H29 119.4 . . C28 C29 H29 119.4 . . C11 C12 H12A 109.5 . . C11 C12 H12B 109.5 . . H12A C12 H12B 109.5 . . C11 C12 H12C 109.5 . . H12A C12 H12C 109.5 . . H12B C12 H12C 109.5 . . C44 C45 C46 119.6(4) . . C44 C45 C48 121.4(5) . . C46 C45 C48 119.0(5) . . C6 C7 C8 121.1(5) . . C6 C7 H7 119.5 . . C8 C7 H7 119.5 . . C56 C57 C58 119.9(5) . . C56 C57 H57 120.0 . . C58 C57 H57 120.0 . . C38 C37 C36 118.4(5) . . C38 C37 H37 120.8 . . C36 C37 H37 120.8 . . C65 C66 C68 119.4(4) . . C65 C66 C67 121.1(4) . . C68 C66 C67 119.5(4) . . F10 C55 F11 103.7(6) . . F10 C55 F12 108.1(5) . . F11 C55 F12 104.5(5) . . F10 C55 C52 113.6(4) . . F11 C55 C52 113.1(4) . . F12 C55 C52 113.1(4) . . C45 C44 C43 121.2(4) . . C45 C44 H44 119.4 . . C43 C44 H44 119.4 . . C59 C58 C57 120.1(5) . . C59 C58 H58 120.0 . . C57 C58 H58 120.0 . . C24 C23 C22 118.9(5) . . C24 C23 H23 120.5 . . C22 C23 H23 120.5 . . C14 C15 C16 121.0(4) . . C14 C15 H15 119.5 . . C16 C15 H15 119.5 . . C30 C31 C32 119.5(4) . . C30 C31 C34 119.7(4) . . C32 C31 C34 120.8(5) . . C64 C65 C66 120.8(4) . . C64 C65 H65 119.6 . . C66 C65 H65 119.6 . . C26 C25 C24 121.7(5) . . C26 C25 H25 119.2 . . C24 C25 H25 119.2 . . F7 C48 F9 105.7(5) . . F7 C48 F8 107.6(5) . . F9 C48 F8 104.9(4) . . F7 C48 C45 112.4(4) . . F9 C48 C45 113.7(5) . . F8 C48 C45 111.8(4) . . F17 C67 F18 105.4(6) . . F17 C67 F16 104.3(5) . . F18 C67 F16 103.2(6) . . F17 C67 C66 114.6(5) . . F18 C67 C66 113.5(4) . . F16 C67 C66 114.6(4) . . C58 C59 C61 120.9(4) . . C58 C59 C60 119.2(5) . . C61 C59 C60 119.9(6) . . C17 C16 C15 122.0(4) . . C17 C16 H16 119.0 . . C15 C16 H16 119.0 . . F4 C41 F5 110.4(5) . . F4 C41 F6 104.6(5) . . F5 C41 F6 104.6(5) . . F4 C41 C38 113.3(5) . . F5 C41 C38 112.0(4) . . F6 C41 C38 111.4(5) . . C23 C24 C25 120.6(4) . . C23 C24 H24 119.7 . . C25 C24 H24 119.7 . . F2 C34 F3 105.9(8) . . F2 C34 F1 108.4(8) . . F3 C34 F1 95.2(7) . . F2 C34 C31 116.9(6) . . F3 C34 C31 114.0(6) . . F1 C34 C31 114.1(5) . . F15 C60 F13 111.2(8) . . F15 C60 F14 104.3(7) . . F13 C60 F14 97.6(7) . . F15 C60 C59 114.5(6) . . F13 C60 C59 114.0(5) . . F14 C60 C59 113.6(6) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Ru1 N4 2.066(3) . Ru1 P4 2.2194(9) . Ru1 P3 2.2555(10) . Ru1 P1 2.2613(10) . Ru1 P2 2.2702(10) . P1 N1 1.744(3) . P1 C49 1.825(4) . P1 C42 1.843(4) . P4 C19 1.805(4) . P4 C10 1.818(4) . P4 C1 1.819(4) . P3 N3 1.742(3) . P3 C28 1.838(4) . P3 C35 1.840(4) . P2 N2 1.738(3) . P2 C63 1.832(4) . P2 C56 1.842(4) . N3 C9 1.398(5) . N3 C1 1.421(5) . N1 C18 1.391(5) . N1 C10 1.421(5) . F9 C48 1.334(7) . N2 C27 1.391(5) . N2 C19 1.420(5) . N4 N5 1.064(5) . F6 C41 1.367(8) . F8 C48 1.359(7) . C42 C43 1.392(6) . C42 C47 1.394(6) . F12 C55 1.304(6) . F7 C48 1.330(6) . F5 C41 1.338(6) . C63 C69 1.386(6) . C63 C64 1.410(6) . C49 C50 1.390(6) . C49 C54 1.404(6) . C18 C17 1.400(6) . C18 C13 1.402(5) . C10 C11 1.373(5) . C35 C36 1.380(6) . C35 C40 1.395(6) . C13 C14 1.403(5) . C13 C11 1.429(6) . C69 C68 1.377(6) . C69 H69 0.9300 . F4 C41 1.296(7) . C28 C33 1.392(6) . C28 C29 1.394(6) . C27 C22 1.396(6) . C27 C26 1.397(6) . C47 C46 1.369(6) . C47 H47 0.9300 . C2 C1 1.362(6) . C2 C4 1.420(6) . C2 C3 1.492(6) . C9 C8 1.383(6) . C9 C4 1.410(6) . C40 C39 1.382(6) . C40 H40 0.9300 . C46 C45 1.377(7) . C46 H46 0.9300 . C11 C12 1.490(6) . C4 C5 1.405(6) . C26 C25 1.380(6) . C26 H26 0.9300 . C8 C7 1.389(7) . C8 H8 0.9300 . C54 C53 1.376(6) . C54 H54 0.9300 . F16 C67 1.296(7) . C50 C51 1.394(6) . C50 H50 0.9300 . F11 C55 1.304(6) . C17 C16 1.386(6) . C17 H17 0.9300 . C33 C32 1.385(6) . C33 H33 0.9300 . C36 C37 1.384(6) . C36 H36 0.9300 . C20 C19 1.364(5) . C20 C22 1.439(6) . C20 C21 1.501(6) . C32 C31 1.391(6) . C32 H32 0.9300 . C64 C65 1.375(6) . C64 H64 0.9300 . F10 C55 1.277(7) . F13 C60 1.258(8) . C43 C44 1.397(7) . C43 H43 0.9300 . C52 C51 1.377(6) . C52 C53 1.391(6) . C52 C55 1.505(6) . C51 H51 0.9300 . C62 C61 1.388(7) . C62 C56 1.396(6) . C62 H62 0.9300 . C53 H53 0.9300 . C5 C6 1.371(7) . C5 H5 0.9300 . C3 H3A 0.9600 . C3 H3B 0.9600 . C3 H3C 0.9600 . C22 C23 1.394(6) . C56 C57 1.374(6) . C38 C37 1.380(7) . C38 C39 1.385(7) . C38 C41 1.497(7) . C68 C66 1.392(6) . C68 H68 0.9300 . C39 H39 0.9300 . C6 C7 1.380(8) . C6 H6 0.9300 . C21 H21A 0.9600 . C21 H21B 0.9600 . C21 H21C 0.9600 . C61 C59 1.378(8) . C61 H61 0.9300 . C30 C29 1.370(6) . C30 C31 1.386(7) . C30 H30 0.9300 . C14 C15 1.373(7) . C14 H14 0.9300 . C29 H29 0.9300 . C12 H12A 0.9600 . C12 H12B 0.9600 . C12 H12C 0.9600 . C45 C44 1.356(7) . C45 C48 1.488(7) . C7 H7 0.9300 . C57 C58 1.406(7) . C57 H57 0.9300 . C37 H37 0.9300 . C66 C65 1.377(7) . C66 C67 1.490(6) . F18 C67 1.284(7) . C44 H44 0.9300 . C58 C59 1.361(8) . C58 H58 0.9300 . C23 C24 1.366(8) . C23 H23 0.9300 . C15 C16 1.393(7) . C15 H15 0.9300 . C31 C34 1.472(6) . C65 H65 0.9300 . C25 C24 1.412(8) . C25 H25 0.9300 . C67 F17 1.281(7) . C59 C60 1.501(7) . C16 H16 0.9300 . F14 C60 1.316(10) . C24 H24 0.9300 . F1 C34 1.287(8) . C34 F2 1.187(8) . C34 F3 1.256(9) . C60 F15 1.207(8) .