#------------------------------------------------------------------------------ #$Date: 2019-12-13 11:04:13 +0200 (Fri, 13 Dec 2019) $ #$Revision: 245052 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/65/1556554.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556554 loop_ _publ_author_name 'Sunada, Y.' 'Taniyama, N.' 'Shimamoto, K.' 'Kyushin, S.' 'Nagashima, H.' _publ_section_title ; Construction of a Planar Tetrapalladium Cluster by the Reaction of Palladium(0) Bis(isocyanide) with Cyclic Tetrasilane ; _journal_name_full Inorganics _journal_page_first 84 _journal_paper_doi 10.3390/inorganics5040084 _journal_volume 5 _journal_year 2017 _chemical_formula_moiety 'C38 H78 N4 Pd4 Si3' _chemical_formula_sum 'C38 H78 N4 Pd4 Si3' _chemical_formula_weight 1100.92 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 90.0000 _cell_angle_beta 92.1391(12) _cell_angle_gamma 90.0000 _cell_formula_units_Z 4 _cell_length_a 10.8179(6) _cell_length_b 22.0783(12) _cell_length_c 22.8654(12) _cell_measurement_reflns_used 20078 _cell_measurement_temperature 193 _cell_measurement_theta_max 30.43 _cell_measurement_theta_min 2.25 _cell_volume 5457.4(5) _computing_cell_refinement CrystalClear _computing_data_collection 'CrystalClear (Rigaku Inc., 2008)' _computing_data_reduction CrystalClear _computing_molecular_graphics 'CrystalStructure 4.2.5' _computing_publication_material 'CrystalStructure 4.2.5 (Rigaku, 2017)' _computing_structure_refinement 'SHELXL97 (Sheldrick, 2008)' _computing_structure_solution 'SIR2011 (Burla, et al., 2012)' _diffrn_ambient_temperature 193 _diffrn_detector_area_resol_mean 14.222 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Rigaku Saturn724' _diffrn_measurement_method \w _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71075 _diffrn_reflns_av_R_equivalents 0.0336 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 28 _diffrn_reflns_limit_k_min -28 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 77678 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.520 _diffrn_reflns_theta_min 3.144 _diffrn_standards_interval_count . _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.389 _exptl_absorpt_correction_T_max 0.895 _exptl_absorpt_correction_T_min 0.784 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'REQAB (Rigaku, 1998)' _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.340 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 2240.00 _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.080 _refine_diff_density_max 2.30 _refine_diff_density_min -0.81 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.101 _refine_ls_hydrogen_treatment constr _refine_ls_number_parameters 470 _refine_ls_number_reflns 12489 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0537 _refine_ls_R_factor_gt 0.0516 _refine_ls_shift/su_max 0.001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w = 1/[\s^2^(Fo^2^)+(0.0898P)^2^+12.9959P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1496 _refine_ls_wR_factor_ref 0.1518 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 11907 _reflns_number_total 12489 _reflns_threshold_expression F^2^>2.0\s(F^2^) _cod_data_source_file Inorganics-2017-5-84.cif _cod_data_source_block Pd4Si3(CNtBu)4 _cod_database_code 1556554 _shelxl_version_number 2014-1 _shelx_res_file ; TITL Pd4Si3(CNtBu)4 CELL 0.71075 10.81790 22.07830 22.86540 90.00000 92.13910 90.00000 ZERR 4 0.00060 0.00120 0.00120 0.00000 0.00120 0.00000 LATT 1 SYMM .50-X, .50+Y, .50-Z SFAC C H N PD SI UNIT 152 312 16 16 12 L.S. 50 FMAP 2 PLAN 25 WPDB -2 HTAB BOND $H CONF LIST 4 TEMP -80.0 ACTA SIZE 0.150 0.100 0.080 WGHT 0.089800 12.995900 FVAR 0.55376 PD1 4 1.084415 0.347143 0.480050 11.00000 0.02821 0.04460 = 0.02250 -0.00255 -0.00339 -0.01021 PD2 4 1.070480 0.372661 0.283403 11.00000 0.03975 0.05647 = 0.02411 0.00626 -0.00301 -0.02397 PD3 4 0.757542 0.253726 0.369377 11.00000 0.02163 0.03306 = 0.02005 -0.00019 -0.00122 -0.00557 PD4 4 0.972663 0.320314 0.376649 11.00000 0.02231 0.03282 = 0.01951 -0.00014 -0.00139 -0.00602 SI1 5 1.146628 0.380904 0.384602 11.00000 0.02232 0.03286 = 0.02862 -0.00071 -0.00129 -0.00559 SI2 5 0.879927 0.298433 0.288875 11.00000 0.02385 0.03163 = 0.01962 0.00006 -0.00168 -0.00303 SI3 5 0.896767 0.277371 0.458028 11.00000 0.02390 0.03476 = 0.01925 0.00050 -0.00113 -0.00264 N1 3 1.264296 0.405951 0.574129 11.00000 0.03035 0.04308 = 0.03598 -0.00406 -0.00728 -0.00284 N2 3 1.251246 0.441822 0.203253 11.00000 0.03927 0.05020 = 0.03357 0.00704 0.00022 -0.01589 N3 3 0.561293 0.215514 0.270609 11.00000 0.02902 0.03891 = 0.02565 -0.00072 -0.00319 -0.00676 N4 3 0.590445 0.186839 0.458461 11.00000 0.03205 0.05521 = 0.02921 0.00107 0.00409 -0.01430 C1 1 1.196351 0.383884 0.541209 11.00000 0.03297 0.04983 = 0.02810 -0.00488 -0.00333 -0.00954 C2 1 1.356716 0.435168 0.611995 11.00000 0.03185 0.03615 = 0.04438 -0.00791 -0.01333 -0.00332 C3 1 1.475323 0.400299 0.607619 11.00000 0.03427 0.08012 = 0.06603 -0.01594 -0.01054 0.00776 AFIX 33 H3A 2 1.501173 0.400673 0.566997 11.00000 -1.20000 H3B 2 1.462458 0.358389 0.620132 11.00000 -1.20000 H3C 2 1.539680 0.419098 0.632873 11.00000 -1.20000 AFIX 0 C4 1 1.367031 0.500245 0.592515 11.00000 0.06687 0.04785 = 0.06676 0.00897 -0.00731 -0.01781 AFIX 33 H4A 2 1.286540 0.520202 0.595268 11.00000 -1.20000 H4B 2 1.392837 0.501501 0.551903 11.00000 -1.20000 H4C 2 1.428414 0.521278 0.617730 11.00000 -1.20000 AFIX 0 C5 1 1.310829 0.432234 0.674190 11.00000 0.05604 0.04758 = 0.03857 -0.00551 -0.01411 -0.00590 AFIX 33 H5A 2 1.300782 0.389800 0.685657 11.00000 -1.20000 H5B 2 1.231116 0.453135 0.675836 11.00000 -1.20000 H5C 2 1.371102 0.451880 0.701043 11.00000 -1.20000 AFIX 0 C6 1 1.182132 0.417332 0.231517 11.00000 0.04778 0.06280 = 0.02471 0.00690 -0.00349 -0.02559 C7 1 1.345474 0.473229 0.171537 11.00000 0.03332 0.03942 = 0.04015 0.00931 0.00757 -0.00647 C8 1 1.432738 0.503025 0.217001 11.00000 0.05181 0.08112 = 0.06114 0.00763 -0.00462 -0.03272 AFIX 33 H8A 2 1.470100 0.471833 0.242517 11.00000 -1.20000 H8B 2 1.386156 0.531536 0.240552 11.00000 -1.20000 H8C 2 1.497966 0.524831 0.197115 11.00000 -1.20000 AFIX 0 C9 1 1.412548 0.426768 0.135265 11.00000 0.05864 0.05569 = 0.06910 0.00581 0.02054 0.00949 AFIX 33 H9A 2 1.353387 0.407202 0.107807 11.00000 -1.20000 H9B 2 1.450598 0.396148 0.161218 11.00000 -1.20000 H9C 2 1.476894 0.447008 0.113390 11.00000 -1.20000 AFIX 0 C10 1 1.282764 0.520047 0.132739 11.00000 0.06161 0.05526 = 0.05575 0.02000 0.00739 0.00747 AFIX 33 H10A 2 1.238652 0.548979 0.156892 11.00000 -1.20000 H10B 2 1.223836 0.500047 0.105472 11.00000 -1.20000 H10C 2 1.345020 0.541562 0.110622 11.00000 -1.20000 AFIX 0 C11 1 0.640918 0.231838 0.301989 11.00000 0.02796 0.03316 = 0.02362 0.00168 0.00032 -0.00288 C12 1 0.458795 0.196555 0.231192 11.00000 0.02698 0.04639 = 0.02809 -0.00650 -0.00692 -0.00476 C13 1 0.514237 0.165162 0.178967 11.00000 0.04534 0.06685 = 0.03298 -0.01502 -0.00439 0.00074 AFIX 33 H13A 2 0.541229 0.124312 0.190318 11.00000 -1.20000 H13B 2 0.585355 0.188468 0.166081 11.00000 -1.20000 H13C 2 0.451800 0.162506 0.146897 11.00000 -1.20000 AFIX 0 C14 1 0.388005 0.253077 0.211199 11.00000 0.03891 0.06199 = 0.03816 0.00081 -0.01003 0.00349 AFIX 33 H14A 2 0.443379 0.280053 0.190427 11.00000 -1.20000 H14B 2 0.356766 0.274131 0.245368 11.00000 -1.20000 H14C 2 0.318387 0.241362 0.184957 11.00000 -1.20000 AFIX 0 C15 1 0.376906 0.154109 0.264978 11.00000 0.03474 0.05646 = 0.05499 -0.00419 -0.00536 -0.01205 AFIX 33 H15A 2 0.427495 0.121609 0.282607 11.00000 -1.20000 H15B 2 0.313651 0.136568 0.238255 11.00000 -1.20000 H15C 2 0.336781 0.176787 0.295854 11.00000 -1.20000 AFIX 0 C16 1 0.657172 0.213879 0.431107 11.00000 0.02747 0.04835 = 0.02302 0.00050 -0.00195 -0.00746 C17 1 0.506015 0.150051 0.492342 11.00000 0.04130 0.05712 = 0.03677 0.00495 0.01129 -0.01896 C18 1 0.432310 0.110885 0.448030 11.00000 0.07958 0.09422 = 0.06458 -0.02245 0.02971 -0.05424 AFIX 33 H18A 2 0.489383 0.085691 0.426298 11.00000 -1.20000 H18B 2 0.385306 0.137089 0.420688 11.00000 -1.20000 H18C 2 0.375122 0.084835 0.468773 11.00000 -1.20000 AFIX 0 C19 1 0.420234 0.192735 0.523957 11.00000 0.04389 0.07736 = 0.03699 0.00065 0.01163 -0.01630 AFIX 33 H19A 2 0.382601 0.171113 0.556224 11.00000 -1.20000 H19B 2 0.355147 0.207232 0.496462 11.00000 -1.20000 H19C 2 0.467786 0.227314 0.539518 11.00000 -1.20000 AFIX 0 C20 1 0.584329 0.113381 0.535347 11.00000 0.05870 0.09215 = 0.08197 0.04578 0.01789 0.00206 AFIX 33 H20A 2 0.631895 0.140762 0.561330 11.00000 -1.20000 H20B 2 0.641214 0.087716 0.514002 11.00000 -1.20000 H20C 2 0.530727 0.087853 0.558632 11.00000 -1.20000 AFIX 0 C21 1 1.313411 0.353137 0.377931 11.00000 0.02413 0.04745 = 0.03607 0.00216 0.00265 -0.00372 AFIX 13 H21 2 1.344725 0.370191 0.340770 11.00000 -1.20000 AFIX 0 C22 1 1.314711 0.284051 0.372122 11.00000 0.03558 0.05252 = 0.05117 -0.00759 0.00350 0.00928 AFIX 33 H22A 2 1.290576 0.265710 0.409020 11.00000 -1.20000 H22B 2 1.398126 0.270529 0.363052 11.00000 -1.20000 H22C 2 1.256263 0.271697 0.340577 11.00000 -1.20000 AFIX 0 C23 1 1.403555 0.372355 0.427305 11.00000 0.02527 0.07122 = 0.05641 -0.00536 -0.00621 -0.00538 AFIX 33 H23A 2 1.487266 0.359178 0.418357 11.00000 -1.20000 H23B 2 1.379289 0.353700 0.464036 11.00000 -1.20000 H23C 2 1.402067 0.416544 0.431268 11.00000 -1.20000 AFIX 0 C24 1 1.151887 0.467282 0.399620 11.00000 0.03768 0.03512 = 0.03810 -0.00255 -0.00354 -0.00698 AFIX 13 H24 2 1.197655 0.472723 0.438069 11.00000 -1.20000 AFIX 0 C25 1 1.221916 0.503811 0.354852 11.00000 0.04863 0.04332 = 0.05354 0.00567 0.00451 -0.01464 AFIX 33 H25A 2 1.228551 0.546050 0.367766 11.00000 -1.20000 H25B 2 1.177212 0.502049 0.316816 11.00000 -1.20000 H25C 2 1.304944 0.486788 0.351235 11.00000 -1.20000 AFIX 0 C26 1 1.022399 0.493051 0.406995 11.00000 0.05043 0.03658 = 0.07737 -0.00079 0.01147 0.00193 AFIX 33 H26A 2 0.985673 0.474505 0.441200 11.00000 -1.20000 H26B 2 0.970681 0.484192 0.371937 11.00000 -1.20000 H26C 2 1.027745 0.536995 0.412582 11.00000 -1.20000 AFIX 0 C27 1 0.933467 0.235552 0.238141 11.00000 0.03378 0.04067 = 0.02670 -0.00889 0.00326 -0.00565 AFIX 13 H27 2 0.858667 0.218241 0.217258 11.00000 -1.20000 AFIX 0 C28 1 0.997751 0.184395 0.272840 11.00000 0.04474 0.04289 = 0.04659 -0.01336 0.00184 0.00629 AFIX 33 H28A 2 1.072543 0.200129 0.293023 11.00000 -1.20000 H28B 2 1.020322 0.151955 0.246000 11.00000 -1.20000 H28C 2 0.941505 0.168380 0.301691 11.00000 -1.20000 AFIX 0 C29 1 1.019969 0.260202 0.191870 11.00000 0.06172 0.05792 = 0.03874 -0.01160 0.02734 -0.00883 AFIX 33 H29A 2 1.042109 0.227405 0.165345 11.00000 -1.20000 H29B 2 1.095133 0.276447 0.211310 11.00000 -1.20000 H29C 2 0.977788 0.292462 0.169470 11.00000 -1.20000 AFIX 0 C30 1 0.790965 0.355445 0.240646 11.00000 0.03281 0.04089 = 0.03566 0.00856 -0.00769 -0.00534 AFIX 13 H30 2 0.856033 0.380385 0.222138 11.00000 -1.20000 AFIX 0 C31 1 0.720507 0.398904 0.276272 11.00000 0.06581 0.06356 = 0.07387 0.01054 -0.00355 0.03215 AFIX 33 H31A 2 0.647712 0.378620 0.291383 11.00000 -1.20000 H31B 2 0.693972 0.433332 0.251835 11.00000 -1.20000 H31C 2 0.773406 0.413398 0.309074 11.00000 -1.20000 AFIX 0 C32 1 0.712014 0.329665 0.189193 11.00000 0.05487 0.06834 = 0.05213 0.02440 -0.02635 -0.01830 AFIX 33 H32A 2 0.685429 0.362726 0.163036 11.00000 -1.20000 H32B 2 0.639167 0.309314 0.204175 11.00000 -1.20000 H32C 2 0.761107 0.300517 0.167563 11.00000 -1.20000 AFIX 0 C33 1 0.958805 0.202836 0.490514 11.00000 0.03045 0.04111 = 0.02680 0.00476 -0.00204 -0.00426 AFIX 13 H33 2 0.887267 0.174985 0.496001 11.00000 -1.20000 AFIX 0 C34 1 1.046851 0.172820 0.448086 11.00000 0.04633 0.04246 = 0.04155 0.00760 -0.00105 0.00888 AFIX 33 H34A 2 1.073734 0.133482 0.463813 11.00000 -1.20000 H34B 2 1.119156 0.198857 0.443342 11.00000 -1.20000 H34C 2 1.003870 0.166958 0.410018 11.00000 -1.20000 AFIX 0 C35 1 1.027318 0.211527 0.550084 11.00000 0.04766 0.04895 = 0.03165 0.00705 -0.01110 0.00004 AFIX 33 H35A 2 1.096614 0.239550 0.545701 11.00000 -1.20000 H35B 2 1.058774 0.172371 0.564290 11.00000 -1.20000 H35C 2 0.970216 0.228197 0.578214 11.00000 -1.20000 AFIX 0 C36 1 0.818681 0.321004 0.519128 11.00000 0.02645 0.04648 = 0.02207 -0.00439 -0.00124 -0.00631 AFIX 13 H36 2 0.887446 0.333394 0.547037 11.00000 -1.20000 AFIX 0 C37 1 0.762816 0.380002 0.495880 11.00000 0.03396 0.04210 = 0.04179 -0.00269 0.00270 0.00394 AFIX 33 H37A 2 0.740885 0.405802 0.528792 11.00000 -1.20000 H37B 2 0.688408 0.371131 0.471631 11.00000 -1.20000 H37C 2 0.823217 0.401027 0.472262 11.00000 -1.20000 AFIX 0 C38 1 0.726855 0.287392 0.556069 11.00000 0.04191 0.05595 = 0.02957 -0.00231 0.01101 -0.00550 AFIX 33 H38A 2 0.759562 0.247141 0.565989 11.00000 -1.20000 H38B 2 0.648000 0.283182 0.533928 11.00000 -1.20000 H38C 2 0.713842 0.310198 0.592090 11.00000 -1.20000 AFIX 0 C39 1 0.719860 0.520871 0.084476 10.50000 0.04706 C40 1 0.728367 0.569794 0.122976 10.50000 0.04722 C41 1 0.806235 0.567029 0.171480 10.50000 0.05044 C42 1 0.884199 0.517296 0.183337 10.50000 0.05529 C43 1 0.874937 0.470997 0.141158 10.50000 0.06604 C44 1 0.800819 0.470086 0.104496 10.50000 0.03855 C45 1 0.643566 0.524741 0.038252 10.50000 0.06433 HKLF 4 REM Pd4Si3(CNtBu)4 REM R1 = 0.0516 for 11907 Fo > 4sig(Fo) and 0.0537 for all 12489 data REM 470 parameters refined using 0 restraints END WGHT 0.0898 13.0213 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 2.305, deepest hole -0.813, 1-sigma level 0.142 Q1 1 0.6949 0.5774 0.1027 11.00000 0.05 2.30 Q2 1 0.8362 0.5171 0.1567 11.00000 0.05 1.99 Q3 1 0.7396 0.4661 0.0718 11.00000 0.05 1.98 Q4 1 0.7523 0.4724 0.0829 11.00000 0.05 1.89 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381.95 53.09 0 6 -13 342.44 35.76 0 6 13 267.38 19.70 0 6 -13 299.50 34.33 0 -6 13 367.38 50.11 0 -6 13 302.15 43.68 0 -6 -13 295.55 34.92 0 -6 -13 269.34 51.67 0 -6 13 284.07 16.07 0 -6 -13 352.72 45.19 0 -6 -13 393.82 56.39 0 6 14 1018.36 80.20 0 6 14 1021.64 47.30 0 6 -14 843.38 55.82 0 6 -14 1011.63 68.02 0 6 -14 835.54 45.47 0 -6 -14 865.79 48.78 0 -6 -14 875.70 54.73 0 -6 14 925.29 50.30 0 -6 -14 986.59 60.94 0 -6 14 831.89 44.66 0 6 -15 6668.85 134.22 0 6 15 6799.58 139.87 0 6 -15 6341.18 139.04 0 6 15 6652.91 136.74 0 -6 15 6749.91 143.00 0 -6 15 6062.46 123.15 0 -6 -15 6657.17 138.74 0 -6 -15 6833.44 150.98 0 6 -16 660.31 53.75 0 6 16 754.58 68.68 0 6 -16 702.63 70.71 0 6 16 711.91 60.33 0 -6 16 693.21 58.86 0 -6 16 614.94 50.61 0 -6 -16 741.62 61.13 0 -6 -16 834.60 95.78 0 6 17 367.91 62.31 0 6 -17 371.19 51.77 0 6 -17 351.21 55.31 0 6 17 278.91 49.49 0 -6 17 425.08 59.79 0 -6 -17 309.59 50.51 0 -6 -17 408.76 57.31 0 6 18 127.02 24.17 0 6 -18 101.02 23.80 0 6 -18 97.05 19.27 0 -6 18 141.78 24.27 0 -6 -18 104.42 25.74 0 -6 -18 160.12 28.29 0 -6 18 83.39 17.21 0 6 -19 2596.30 92.58 0 6 19 2640.86 96.94 0 6 -19 2733.16 165.00 0 -6 -19 2819.41 106.57 0 -6 19 2694.29 95.93 0 -6 -19 2657.02 96.22 0 -6 19 2535.61 87.56 0 6 -20 1039.83 63.74 0 6 20 1117.27 76.00 0 6 -20 1265.62 106.21 0 -6 -20 1294.20 123.82 0 -6 20 1121.14 69.57 0 -6 -20 1173.08 78.01 0 -6 20 1082.74 63.46 0 6 21 196.13 82.75 0 6 -21 169.53 34.46 0 6 -21 174.11 36.27 0 -6 21 208.78 33.11 0 -6 -21 199.80 41.04 0 -6 -21 182.80 39.67 0 -6 21 100.48 29.12 0 6 22 2491.66 540.04 0 6 -22 2412.37 111.36 0 6 -22 2434.76 527.53 0 -6 22 2438.44 531.05 0 -6 -22 2400.41 186.93 0 -6 -22 2287.32 99.12 0 6 -23 282.76 43.26 0 6 23 274.32 30.82 0 -6 23 349.14 48.66 0 -6 -23 397.10 69.48 0 -6 -23 285.16 41.15 0 6 24 426.07 88.54 0 6 -24 534.22 90.65 0 6 -24 376.44 53.85 0 -6 24 570.76 80.85 0 -6 -24 546.25 119.12 0 -6 -24 428.62 67.67 0 6 -25 171.17 43.44 0 6 25 277.08 59.76 0 6 -25 264.84 82.52 0 -6 -25 301.16 72.12 0 -6 25 319.98 132.33 0 -6 -25 226.38 68.64 0 6 -26 62.31 24.67 0 6 26 33.34 14.44 0 -6 26 3.30 11.13 0 -6 -26 20.97 20.52 0 -6 -26 23.54 11.73 0 6 -27 323.42 63.17 0 6 27 361.25 58.27 0 -6 27 317.65 55.26 0 -6 -27 290.24 83.28 0 6 -28 566.93 120.22 0 6 28 596.80 80.57 0 -6 28 773.45 79.73 0 -6 -28 491.99 108.27 0 -6 -28 344.75 86.51 0 6 -29 149.60 41.81 0 6 29 142.57 40.46 0 -6 29 159.07 40.01 0 -6 -29 148.18 31.55 0 7 0 0.13 6.38 0 7 0 10.03 5.92 0 7 0 15.44 8.52 0 -7 0 25.73 8.81 0 -7 0 -6.26 11.44 0 -7 0 1.85 3.43 0 7 1 9330.25 146.96 0 7 -1 9053.33 142.79 0 7 -1 9050.83 146.15 0 7 1 9473.33 158.59 0 -7 -1 9415.70 149.68 0 -7 1 9242.98 145.75 0 -7 -1 8766.79 147.43 0 -7 -1 9364.80 152.51 0 -7 1 8957.15 143.73 0 -7 1 9307.10 150.90 0 7 -2 80.88 8.61 0 7 2 94.60 17.09 0 7 2 107.93 21.14 0 7 -2 112.15 17.24 0 7 2 104.87 16.93 0 7 -2 102.41 16.00 0 -7 -2 99.43 19.05 0 -7 -2 105.96 13.97 0 -7 2 95.67 15.81 0 -7 2 94.23 20.67 0 -7 2 94.06 16.50 0 -7 -2 110.12 22.81 0 7 -3 945.87 34.68 0 7 3 973.59 36.79 0 7 -3 1006.22 39.75 0 7 -3 935.16 36.93 0 7 3 983.72 40.97 0 7 3 939.19 36.41 0 -7 -3 986.68 38.16 0 -7 3 992.82 39.92 0 -7 3 929.36 34.28 0 -7 -3 931.51 36.32 0 -7 -3 985.18 36.04 0 -7 3 802.79 31.97 0 7 -4 6133.78 122.27 0 7 4 6310.22 127.39 0 7 4 6080.07 125.11 0 7 -4 6046.65 121.85 0 7 -4 6325.07 129.24 0 -7 -4 6431.80 129.91 0 -7 4 5898.01 119.58 0 -7 4 6141.00 126.45 0 -7 -4 6003.63 127.15 0 7 -5 6311.48 127.24 0 7 -5 6195.70 123.94 0 7 5 6427.69 129.90 0 7 5 6264.77 128.87 0 7 -5 5943.82 123.80 0 7 5 6313.76 130.48 0 -7 5 6073.44 121.50 0 -7 -5 5918.71 119.51 0 -7 -5 6247.81 128.27 0 -7 5 6300.43 127.27 0 -7 -5 6072.68 125.29 0 -7 5 6257.95 135.39 0 7 6 44.20 11.37 0 7 -6 53.24 7.56 0 7 6 52.68 9.02 0 7 6 55.49 9.49 0 7 -6 45.27 8.84 0 7 -6 76.73 15.01 0 -7 -6 37.52 6.65 0 -7 -6 49.46 9.58 0 -7 6 35.78 6.94 0 -7 6 38.77 7.60 0 -7 -6 49.98 12.04 0 -7 6 55.27 10.98 0 7 7 25.78 11.41 0 7 -7 7.67 6.02 0 7 7 14.38 6.98 0 7 7 -2.49 8.93 0 7 -7 7.76 5.65 0 7 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0 -7 -15 126.98 28.85 0 7 -16 224.64 28.66 0 7 16 179.80 34.52 0 7 -16 170.84 33.36 0 7 16 143.30 25.77 0 -7 16 202.18 36.31 0 -7 16 185.64 31.89 0 -7 -16 156.00 27.62 0 -7 -16 242.97 31.35 0 7 -17 827.37 53.29 0 7 17 815.05 65.56 0 7 -17 880.38 99.07 0 -7 -17 857.13 117.58 0 -7 17 970.67 86.85 0 -7 -17 840.55 73.24 0 7 18 502.19 52.88 0 7 -18 533.23 61.47 0 7 -18 486.29 42.02 0 -7 18 527.50 73.42 0 -7 -18 496.36 78.94 0 -7 18 449.34 46.54 0 -7 -18 597.26 72.25 0 7 -19 54.17 14.13 0 7 19 56.67 13.71 0 7 -19 49.74 18.17 0 -7 -19 86.63 28.31 0 -7 19 36.88 12.58 0 -7 -19 65.13 21.33 0 -7 19 43.22 13.44 0 7 20 247.44 50.82 0 7 -20 159.81 40.42 0 7 -20 166.10 33.15 0 -7 20 230.30 41.44 0 -7 -20 197.35 82.34 0 -7 20 121.65 29.06 0 -7 -20 224.44 39.04 0 7 -21 2214.10 96.48 0 7 21 2082.31 104.34 0 7 -21 2132.12 175.46 0 -7 -21 2368.25 216.82 0 -7 21 2253.33 97.48 0 -7 -21 2469.10 154.54 0 7 -22 124.30 24.33 0 7 22 166.34 32.09 0 7 -22 145.85 22.15 0 -7 -22 173.91 27.83 0 -7 22 184.23 20.68 0 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399.45 24.49 0 8 -2 1865.20 49.07 0 8 2 1838.62 48.80 0 8 2 1943.89 62.05 0 8 -2 1929.60 52.30 0 8 2 1861.99 53.37 0 8 -2 1947.93 63.45 0 -8 -2 2014.46 53.85 0 -8 2 1898.65 53.43 0 -8 2 1929.89 52.85 0 -8 -2 1877.27 52.90 0 -8 -2 1896.03 53.78 0 -8 2 1919.24 65.59 0 8 -3 2521.46 66.00 0 8 3 2431.67 64.03 0 8 -3 2626.20 74.56 0 8 -3 2519.49 67.14 0 8 3 2406.65 66.97 0 8 3 2420.04 66.91 0 -8 -3 2428.39 67.47 0 -8 3 2434.03 66.78 0 -8 3 2487.15 66.25 0 -8 -3 2452.15 67.32 0 -8 3 2526.20 69.44 0 8 -4 318.80 21.33 0 8 4 325.11 24.72 0 8 -4 270.93 18.73 0 8 -4 311.49 26.53 0 8 4 289.53 19.22 0 8 4 246.87 16.21 0 -8 -4 289.15 17.92 0 -8 4 285.14 18.92 0 -8 4 276.08 15.98 0 -8 -4 272.34 18.44 0 -8 -4 294.83 23.56 0 -8 4 290.90 22.09 0 8 -5 850.50 31.69 0 8 5 899.11 34.12 0 8 5 880.01 35.78 0 8 5 856.82 36.13 0 8 -5 873.17 36.90 0 8 -5 857.98 33.52 0 -8 -5 847.03 36.26 0 -8 -5 885.87 34.26 0 -8 5 855.88 33.31 0 -8 -5 895.87 53.26 0 -8 5 872.77 35.30 0 8 6 355.09 20.61 0 8 -6 344.17 17.76 0 8 6 362.71 24.20 0 8 6 319.94 18.56 0 8 -6 369.75 23.59 0 8 -6 369.62 37.62 0 -8 -6 356.55 23.90 0 -8 -6 337.87 17.39 0 -8 6 338.44 21.27 0 -8 6 340.94 17.10 0 -8 -6 347.30 24.65 0 -8 6 332.18 20.62 0 8 7 49.33 12.02 0 8 -7 45.01 8.30 0 8 7 17.89 5.66 0 8 7 29.07 8.57 0 8 -7 28.37 9.94 0 8 -7 35.18 9.20 0 -8 -7 21.32 8.82 0 -8 -7 22.97 5.19 0 -8 7 29.97 5.21 0 -8 7 18.37 10.42 0 -8 -7 31.95 6.99 0 -8 7 37.17 6.88 0 8 8 183.49 24.63 0 8 -8 163.49 20.51 0 8 8 209.70 30.85 0 8 8 180.78 35.26 0 8 -8 178.54 31.03 0 8 -8 174.49 24.44 0 -8 -8 174.96 21.04 0 -8 -8 161.31 24.15 0 -8 8 181.16 15.30 0 -8 8 204.90 27.75 0 -8 -8 175.77 28.07 0 -8 8 171.50 14.24 0 8 9 668.13 55.50 0 8 -9 730.53 28.69 0 8 9 661.03 27.88 0 8 9 722.78 34.98 0 8 -9 755.31 32.77 0 8 -9 749.65 40.37 0 -8 -9 735.39 54.00 0 -8 -9 720.86 37.46 0 -8 9 729.23 30.99 0 -8 9 676.46 26.73 0 -8 -9 766.03 53.08 0 -8 9 765.11 37.15 0 8 10 68.12 13.62 0 8 -10 84.35 11.19 0 8 10 58.61 12.14 0 8 10 29.88 8.53 0 8 -10 73.06 12.17 0 8 -10 81.17 13.89 0 -8 -10 68.51 9.55 0 -8 -10 60.13 10.28 0 -8 10 76.30 12.32 0 -8 10 72.75 13.99 0 -8 -10 98.67 14.93 0 -8 10 74.77 14.77 0 8 11 1708.06 63.94 0 8 -11 1767.64 59.50 0 8 11 1789.52 70.07 0 8 11 1804.88 62.65 0 8 -11 1724.44 59.09 0 8 -11 1671.41 81.60 0 -8 -11 1724.68 67.43 0 -8 -11 1731.66 61.57 0 -8 11 1810.56 68.30 0 -8 11 1693.00 60.42 0 -8 -11 1758.45 63.87 0 -8 11 1744.46 64.87 0 8 -12 1270.28 49.89 0 8 12 1242.73 52.98 0 8 12 1142.64 56.13 0 8 -12 1234.33 50.59 0 8 -12 1237.36 53.39 0 -8 12 1262.72 49.97 0 -8 -12 1200.60 65.72 0 -8 -12 1197.67 48.96 0 -8 12 1175.20 49.20 0 -8 -12 1238.71 63.78 0 -8 12 1241.23 53.80 0 8 13 3380.58 100.34 0 8 -13 3403.72 95.26 0 8 13 3559.86 104.96 0 8 -13 3312.08 115.62 0 8 -13 3540.54 99.33 0 -8 -13 3034.90 85.27 0 -8 -13 3527.23 124.94 0 -8 13 3423.37 93.58 0 -8 -13 3302.96 98.47 0 -8 13 3546.30 97.62 0 8 -14 3617.35 115.72 0 8 14 3794.86 120.04 0 8 -14 3401.16 114.71 0 8 14 3516.00 111.53 0 -8 14 3461.83 108.16 0 -8 14 3478.39 107.50 0 -8 -14 3367.33 123.59 0 -8 -14 3650.37 123.35 0 8 -15 1260.16 52.21 0 8 15 1307.10 60.08 0 8 -15 1135.40 75.36 0 8 15 1101.16 65.82 0 -8 15 1141.29 67.70 0 -8 15 1146.04 67.02 0 -8 -15 1145.65 80.84 0 -8 -15 1311.39 93.38 0 8 -16 1444.50 73.03 0 8 16 1507.48 68.32 0 8 -16 1306.09 63.99 0 -8 -16 1413.47 147.68 0 -8 16 1575.58 89.54 0 -8 16 1356.40 63.72 0 -8 -16 1460.59 92.28 0 8 -17 1994.51 86.38 0 8 17 2041.86 91.65 0 8 -17 1905.57 87.44 0 -8 -17 2129.96 163.73 0 -8 17 2053.08 89.54 0 -8 17 1947.90 85.43 0 -8 -17 1957.15 107.30 0 8 -18 58.61 13.03 0 8 18 79.62 18.64 0 8 -18 51.96 18.88 0 -8 -18 85.06 21.01 0 -8 18 74.67 18.04 0 -8 18 60.35 11.72 0 -8 -18 80.71 19.63 0 8 -19 2595.57 103.53 0 8 19 2542.10 104.45 0 8 -19 2480.10 127.52 0 -8 -19 2441.27 124.93 0 -8 19 2742.33 111.73 0 -8 19 2503.89 100.38 0 -8 -19 2662.14 111.77 0 8 -20 26.01 11.25 0 8 20 79.29 19.91 0 8 -20 57.65 20.55 0 -8 -20 31.71 20.33 0 -8 20 33.65 10.73 0 -8 20 50.87 12.17 0 -8 -20 49.13 18.25 0 8 -21 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28.70 9.16 0 9 -5 14.44 5.14 0 9 5 32.14 9.90 0 9 5 13.50 7.05 0 -9 -5 19.11 10.16 0 -9 5 43.24 6.99 0 -9 5 45.16 9.61 0 -9 -5 35.72 7.84 0 -9 -5 34.55 11.46 0 9 6 412.58 32.83 0 9 -6 363.05 18.34 0 9 6 372.84 21.41 0 9 6 428.43 56.29 0 9 -6 408.61 28.06 0 9 -6 345.50 27.20 0 -9 -6 438.91 45.51 0 -9 -6 375.83 28.66 0 -9 6 401.19 28.79 0 -9 6 350.38 17.86 0 -9 -6 451.91 59.00 0 -9 6 379.78 44.25 0 9 7 8140.14 170.38 0 9 -7 7948.56 156.17 0 9 7 7799.95 154.63 0 9 7 8136.23 169.05 0 9 -7 8244.36 163.93 0 9 -7 8134.33 167.82 0 -9 -7 7910.23 161.48 0 -9 -7 8637.38 171.51 0 -9 7 8045.75 158.82 0 -9 7 8069.61 163.36 0 -9 -7 7853.77 162.97 0 -9 7 8246.73 168.18 0 9 8 327.40 48.50 0 9 -8 306.06 24.20 0 9 8 313.91 21.92 0 9 8 320.94 32.63 0 9 -8 302.22 41.66 0 9 -8 364.17 43.26 0 -9 -8 284.83 33.31 0 -9 -8 290.37 38.53 0 -9 8 299.73 27.26 0 -9 8 292.40 29.35 0 -9 -8 347.86 48.91 0 -9 8 293.88 48.17 0 9 9 26.06 16.00 0 9 -9 5.02 4.24 0 9 9 -1.17 5.62 0 9 -9 35.07 10.52 0 9 -9 5.61 4.04 0 9 9 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13 508.73 33.18 0 -9 -13 618.38 56.78 0 -9 13 689.25 64.06 0 9 14 983.41 87.93 0 9 -14 992.11 58.36 0 9 14 1012.82 60.82 0 9 -14 1168.35 205.26 0 9 -14 991.38 60.46 0 -9 14 1086.82 65.85 0 -9 14 1026.00 60.21 0 -9 -14 1012.04 61.69 0 -9 -14 1088.65 75.75 0 9 -15 11.29 5.27 0 9 15 8.52 11.60 0 9 -15 24.32 10.17 0 -9 -15 -7.70 17.32 0 -9 15 13.23 7.18 0 -9 -15 21.72 8.53 0 9 -16 2536.01 101.25 0 9 16 2798.11 122.78 0 9 -16 2575.81 111.63 0 -9 -16 2652.80 160.44 0 -9 16 2800.69 115.85 0 -9 16 2546.10 100.59 0 -9 -16 2587.81 102.90 0 9 -17 369.79 49.30 0 9 17 450.82 72.70 0 9 -17 391.93 32.37 0 -9 -17 393.66 48.59 0 -9 17 518.92 73.91 0 -9 17 362.47 60.58 0 -9 -17 474.98 72.14 0 9 -18 727.38 46.10 0 9 18 767.42 54.65 0 9 -18 839.14 67.50 0 -9 -18 841.72 111.60 0 -9 18 785.05 74.07 0 -9 18 661.43 65.82 0 -9 -18 743.37 72.56 0 9 -19 2870.54 122.08 0 9 19 2763.43 119.34 0 9 -19 2668.33 143.65 0 -9 -19 2890.27 129.76 0 -9 19 2852.25 120.35 0 -9 19 2588.57 109.64 0 -9 -19 2743.20 140.67 0 9 -20 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74.90 14.53 0 -10 12 59.19 10.42 0 -10 -12 89.42 13.44 0 -10 12 130.60 22.15 0 10 13 249.56 41.77 0 10 13 233.63 28.71 0 10 -13 176.63 26.86 0 10 -13 225.81 32.18 0 10 -13 229.64 31.78 0 -10 -13 190.63 27.35 0 -10 13 284.02 41.77 0 -10 13 205.25 25.17 0 -10 -13 272.21 29.91 0 10 -14 21.13 6.19 0 10 14 6.72 6.91 0 10 -14 40.33 16.41 0 10 -14 12.45 6.75 0 -10 14 18.84 6.41 0 -10 -14 24.52 16.39 0 -10 14 31.62 5.60 0 -10 -14 40.60 13.14 0 10 -15 1362.52 61.17 0 10 15 1459.86 65.65 0 10 -15 1410.46 94.88 0 -10 -15 1472.63 79.66 0 -10 15 1438.77 67.08 0 -10 15 1368.36 60.93 0 -10 -15 1399.02 65.38 0 10 -16 498.26 42.51 0 10 16 662.81 83.64 0 10 -16 563.80 77.19 0 -10 -16 550.74 98.76 0 -10 16 642.95 38.59 0 -10 16 493.12 48.02 0 -10 -16 535.82 64.20 0 10 -17 5349.89 152.92 0 10 17 5560.72 177.53 0 10 -17 5161.80 175.77 0 -10 -17 5431.32 172.69 0 -10 17 5240.87 150.97 0 -10 17 5093.33 45.65 0 -10 -17 5265.89 154.33 0 10 -18 2558.46 103.06 0 10 18 2649.12 110.40 0 10 -18 2585.12 110.93 0 -10 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2034.03 65.45 0 11 -4 4526.94 104.86 0 11 4 4541.51 108.22 0 11 4 4616.10 112.04 0 11 -4 4712.60 111.56 0 11 4 4536.47 117.58 0 11 -4 4671.49 119.62 0 -11 -4 4475.58 112.04 0 -11 4 4520.64 109.90 0 -11 4 4590.53 109.99 0 -11 -4 4605.46 112.69 0 -11 4 4721.73 115.22 0 11 -5 7335.74 143.94 0 11 5 7437.88 149.42 0 11 5 7317.15 151.32 0 11 -5 7374.49 147.31 0 11 5 7499.66 153.06 0 11 -5 7485.10 154.02 0 -11 -5 7358.10 150.86 0 -11 5 7494.76 156.11 0 -11 5 7049.85 141.51 0 -11 -5 7373.99 152.48 0 -11 5 7396.06 154.21 0 -11 -5 7235.68 155.36 0 11 -6 5068.74 118.96 0 11 6 5234.90 123.84 0 11 -6 5185.90 127.10 0 11 -6 5144.16 125.09 0 11 6 5184.71 126.80 0 11 6 5059.14 124.07 0 -11 -6 5148.92 124.74 0 -11 6 5192.54 126.72 0 -11 6 5073.32 123.71 0 -11 -6 5072.73 125.17 0 -11 -6 5018.41 118.64 0 -11 6 5206.66 125.93 0 11 -7 1478.71 47.50 0 11 7 1486.99 54.81 0 11 -7 1594.38 62.83 0 11 -7 1289.65 49.22 0 11 7 1609.49 68.96 0 11 7 1613.00 58.36 0 -11 -7 1478.90 57.73 0 -11 7 1532.08 260.58 0 -11 7 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5590.83 127.85 0 12 7 6151.40 116.55 0 12 -7 5751.79 976.35 0 12 -7 5941.23 1004.63 0 12 7 5832.42 986.74 0 12 7 5478.99 132.56 0 -12 -7 5652.40 132.83 0 -12 7 5909.84 999.19 0 -12 -7 5782.49 980.16 0 -12 -7 5587.53 135.19 0 -12 7 5878.61 995.51 0 12 -8 8116.63 170.41 0 12 8 7694.80 162.08 0 12 -8 7837.28 175.93 0 12 -8 8393.08 183.13 0 12 8 8347.47 185.18 0 12 8 8241.56 179.09 0 -12 -8 7906.34 167.56 0 -12 8 8190.50 173.27 0 -12 -8 8311.48 181.58 0 -12 -8 7024.34 158.69 0 -12 8 8231.12 176.77 0 12 -9 1661.13 56.26 0 12 9 1463.99 58.41 0 12 -9 1670.60 61.38 0 12 -9 1717.25 60.42 0 12 9 1660.09 63.27 0 12 -9 1605.49 69.71 0 12 9 1579.73 36.24 0 -12 -9 1607.73 58.30 0 -12 -9 1612.38 60.26 0 -12 9 1522.46 69.03 0 12 10 543.32 47.83 0 12 -10 528.12 38.88 0 12 10 519.63 36.11 0 12 -10 590.14 44.34 0 12 -10 553.75 37.48 0 -12 -10 487.64 49.84 0 -12 10 516.16 43.50 0 -12 10 494.95 33.40 0 -12 -10 623.09 74.07 0 12 11 26.39 8.49 0 12 -11 44.57 7.80 0 12 11 51.70 10.66 0 12 -11 36.39 14.81 0 12 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1905.47 72.11 0 13 -8 1965.67 81.98 0 13 -8 1909.83 74.12 0 -13 -8 1860.39 80.45 0 -13 8 1857.63 64.41 0 -13 -8 1792.24 73.37 0 -13 8 1911.69 68.41 0 13 -9 3337.05 102.92 0 13 9 3362.63 104.70 0 13 9 3304.08 110.02 0 13 -9 3411.93 112.03 0 13 -9 3371.01 110.41 0 -13 -9 3375.02 106.05 0 -13 9 3203.39 108.33 0 -13 -9 3435.89 113.16 0 -13 9 3378.47 121.92 0 13 -10 1679.51 57.55 0 13 10 1589.11 66.51 0 13 10 1710.43 65.67 0 13 -10 1631.54 309.49 0 13 -10 1632.68 311.65 0 -13 -10 1645.17 59.25 0 -13 10 1586.40 71.18 0 -13 -10 1843.30 70.41 0 13 11 404.47 65.07 0 13 -11 281.75 36.15 0 13 11 398.01 53.34 0 13 -11 438.67 48.32 0 13 -11 369.11 45.26 0 -13 -11 255.98 57.42 0 -13 11 330.06 27.12 0 -13 11 327.72 29.44 0 -13 -11 426.01 61.54 0 13 12 20.25 8.07 0 13 -12 14.64 6.78 0 13 12 4.74 9.67 0 13 -12 20.98 10.76 0 13 -12 41.73 13.17 0 -13 -12 4.92 8.21 0 -13 12 22.37 8.30 0 -13 12 16.58 7.14 0 -13 -12 -14.47 14.56 0 13 -13 12.81 11.48 0 13 13 28.90 11.49 0 13 -13 4.18 5.85 0 13 13 15.24 9.70 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1401.11 66.27 0 15 -5 1558.43 68.92 0 15 5 1612.99 314.48 0 -15 -5 1572.83 80.62 0 -15 5 1523.30 65.52 0 -15 -5 1436.32 68.72 0 -15 5 1571.78 92.61 0 15 -612765.47 260.78 0 -15 -612913.26 254.56 0 -15 -612385.48 251.02 0 -15 612702.58 265.55 0 15 -7 4696.48 135.31 0 15 7 5127.16 146.73 0 15 7 5028.55 149.99 0 15 -7 4946.06 143.69 0 15 -7 5000.62 151.33 0 -15 -7 4621.13 139.77 0 -15 7 4763.29 137.90 0 -15 -7 4807.33 145.27 0 -15 7 4841.99 150.58 0 15 -8 2040.74 76.30 0 15 8 2067.11 78.76 0 15 8 2164.84 100.31 0 15 -8 2132.94 82.80 0 15 -8 2074.74 95.30 0 -15 -8 2060.07 79.46 0 -15 -8 2053.45 85.43 0 -15 8 2096.53 86.81 0 15 -9 120.21 22.57 0 15 9 169.75 29.34 0 15 9 190.27 34.44 0 15 -9 167.59 29.00 0 15 -9 138.13 30.75 0 -15 -9 112.69 25.30 0 -15 9 113.75 26.43 0 -15 -9 45.14 10.10 0 -15 9 168.08 31.63 0 15 -10 1846.56 79.52 0 15 10 1854.95 81.46 0 15 10 1890.73 89.22 0 15 -10 1830.17 82.77 0 15 -10 1936.96 94.08 0 -15 -10 1788.89 78.84 0 -15 10 1697.90 74.09 0 -15 -10 1848.24 105.81 0 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396.95 60.07 0 15 -18 849.18 24.28 0 15 18 803.51 82.15 0 15 -18 861.45 106.26 0 -15 -18 915.43 112.09 0 -15 18 820.36 41.83 0 -15 -18 914.16 32.05 0 15 -19 1579.95 42.21 0 15 19 1766.15 77.09 0 15 -19 1608.33 53.61 0 -15 -19 1732.02 89.10 0 -15 19 1646.48 492.74 0 -15 -19 1583.73 60.67 0 15 -20 6.18 5.29 0 15 20 15.24 10.13 0 15 -20 21.06 21.91 0 -15 -20 79.79 27.44 0 -15 20 20.71 13.71 0 -15 -20 11.69 20.62 0 15 -21 34.99 12.57 0 15 21 67.31 17.19 0 15 -21 91.83 27.26 0 -15 -21 67.92 30.39 0 -15 21 112.49 16.27 0 -15 -21 31.08 15.69 0 15 -22 2527.87 111.80 0 15 22 2574.85 112.52 0 -15 22 2758.24 176.32 0 -15 -22 2742.27 130.05 0 -15 -22 2560.23 110.81 0 15 -23 32.25 22.31 0 15 23 27.07 11.74 0 -15 23 56.01 11.26 0 -15 -23 22.16 26.63 0 -15 -23 48.28 14.90 0 15 -24 192.94 38.24 0 15 24 148.07 34.91 0 -15 24 201.85 28.08 0 -15 -24 132.45 23.91 0 -15 -24 131.01 27.51 0 15 -25 181.18 50.18 0 15 25 160.70 44.26 0 -15 25 219.55 44.85 0 -15 -25 167.17 48.84 0 -15 -25 127.21 32.25 0 16 0 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6 374.95 65.81 0 16 -6 356.03 41.91 0 16 -6 333.79 38.94 0 -16 -6 289.24 27.26 0 -16 -6 372.07 58.44 0 -16 6 394.64 73.58 0 16 -7 1250.05 75.54 0 16 7 1246.53 80.64 0 16 7 1285.89 167.79 0 16 -7 1368.10 60.89 0 16 -7 1472.04 119.81 0 -16 -7 1358.56 63.15 0 -16 -7 1315.35 61.67 0 -16 7 1319.42 62.87 0 16 -8 2579.07 97.68 0 16 8 2598.82 107.51 0 16 8 2588.82 104.91 0 16 -8 2621.50 103.75 0 16 -8 2670.45 106.54 0 -16 -8 2499.43 97.02 0 -16 -8 2629.17 123.63 0 -16 8 2628.53 105.86 0 16 -9 507.15 43.23 0 16 9 535.54 43.46 0 16 9 608.75 96.66 0 16 -9 588.91 69.70 0 16 -9 676.94 77.50 0 -16 -9 429.56 65.72 0 -16 -9 656.55 84.91 0 -16 9 593.27 50.84 0 16 -10 150.64 32.58 0 16 10 232.87 44.89 0 16 10 300.06 60.77 0 16 -10 240.55 41.69 0 16 -10 243.24 46.17 0 -16 -10 164.41 40.98 0 -16 -10 220.72 38.16 0 -16 10 302.13 52.45 0 16 -11 82.95 20.55 0 16 11 190.90 34.27 0 16 -11 178.22 30.14 0 16 11 221.86 45.52 0 16 -11 218.66 40.41 0 -16 -11 207.82 33.39 0 -16 11 167.63 29.10 0 16 12 7688.43 252.85 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4085.73 122.57 0 -17 -3 3984.46 156.44 0 -17 3 3956.80 120.33 0 17 -4 1239.23 75.70 0 17 4 1198.94 73.66 0 17 -4 1150.87 70.67 0 17 -4 1123.85 81.30 0 17 4 1224.98 78.28 0 -17 -4 1205.41 74.72 0 -17 -4 1156.18 90.84 0 -17 4 1248.69 81.00 0 17 -5 3961.69 128.30 0 17 5 4001.12 132.36 0 17 -5 3965.65 126.18 0 17 -5 3884.76 131.62 0 17 5 3818.02 158.10 0 -17 -5 3856.53 124.45 0 -17 -5 3889.42 130.50 0 -17 5 3919.28 154.35 0 17 -6 1995.76 86.42 0 17 6 2226.90 87.93 0 17 6 2203.90 89.51 0 17 -6 1997.03 87.54 0 17 -6 2021.93 113.95 0 -17 -6 2061.44 88.88 0 -17 -6 2059.97 94.35 0 -17 6 2033.35 94.43 0 17 -7 1000.06 61.93 0 17 7 1075.25 75.29 0 17 -7 1056.51 71.56 0 17 7 1128.25 74.32 0 17 -7 1146.53 83.57 0 -17 -7 1130.62 90.24 0 -17 7 1197.93 78.06 0 17 -8 1447.20 76.18 0 17 8 1530.19 87.68 0 17 8 1482.76 93.29 0 17 -8 1583.65 85.08 0 17 -8 1580.78 96.92 0 -17 -8 1434.32 87.20 0 -17 -8 1600.91 95.54 0 -17 8 1594.92 90.45 0 17 -9 1675.75 88.03 0 17 9 1689.01 94.84 0 17 9 1801.01 88.32 0 17 -9 1780.68 76.50 0 17 -9 1849.60 155.48 0 -17 -9 1558.62 86.13 0 -17 -9 1748.28 84.05 0 -17 9 1709.20 53.29 0 17 -10 1176.80 63.98 0 17 10 1196.53 127.07 0 17 10 1149.44 74.46 0 17 -10 1131.92 70.42 0 17 -10 1266.40 101.08 0 -17 -10 1075.37 61.53 0 -17 -10 1155.59 103.61 0 -17 10 1223.94 68.66 0 17 -11 1365.30 68.51 0 17 11 1601.95 82.38 0 17 -11 1507.12 79.93 0 17 11 1623.46 87.81 0 17 -11 1553.36 85.70 0 -17 -11 1645.38 89.31 0 -17 11 1549.35 86.08 0 17 -12 968.76 49.04 0 17 12 1083.15 62.81 0 17 -12 1140.23 439.81 0 17 12 1113.02 102.77 0 17 -12 1138.84 79.40 0 -17 -12 1300.70 100.67 0 -17 12 1235.86 64.35 0 17 -13 113.10 53.11 0 17 13 233.70 47.05 0 17 -13 250.18 49.13 0 17 13 216.07 45.27 0 17 -13 219.01 37.99 0 -17 -13 247.08 40.30 0 -17 13 235.43 49.01 0 17 14 2325.09 103.85 0 17 -14 2187.41 97.73 0 17 14 2299.25 115.22 0 17 -14 2066.97 120.09 0 -17 -14 2079.09 100.56 0 -17 14 2074.33 91.90 0 17 15 327.11 63.02 0 17 -15 369.06 59.15 0 17 15 365.72 50.27 0 17 -15 334.27 58.35 0 -17 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1197.75 113.29 0 18 0 595.40 46.69 0 18 0 719.46 105.76 0 -18 0 547.65 45.43 0 -18 0 630.39 62.37 0 18 -1 2376.91 90.49 0 18 1 2408.62 92.64 0 18 -1 2315.88 91.29 0 18 -1 2626.23 108.06 0 -18 -1 2372.18 92.89 0 -18 1 2459.28 99.00 0 -18 -1 2368.42 122.70 0 18 2 716.37 55.55 0 18 -2 630.54 48.76 0 18 -2 749.67 73.50 0 18 2 731.82 104.32 0 -18 -2 605.09 49.86 0 -18 -2 705.25 93.26 0 -18 2 650.65 65.28 0 18 -3 303.31 32.52 0 18 3 307.17 30.33 0 18 -3 311.75 40.01 0 18 3 344.71 65.08 0 -18 -3 255.24 39.06 0 -18 -3 327.07 60.87 0 -18 3 365.31 59.69 0 18 -4 309.27 45.21 0 18 4 361.19 44.91 0 18 4 474.27 64.14 0 18 -4 367.00 49.98 0 18 -4 384.78 65.25 0 -18 -4 302.97 49.59 0 -18 -4 372.02 76.54 0 -18 4 423.35 86.09 0 18 -5 1685.55 89.32 0 18 5 1769.91 74.07 0 18 5 1738.78 79.72 0 18 -5 1825.81 79.07 0 18 -5 1902.31 86.80 0 -18 -5 1783.53 75.77 0 -18 -5 1610.22 89.85 0 -18 5 1757.19 83.00 0 18 -6 9.68 7.11 0 18 6 13.63 6.45 0 18 -6 5.31 3.32 0 18 -6 -2.64 14.36 0 18 6 31.96 11.58 0 -18 -6 6.92 6.18 0 -18 -6 9.19 19.46 0 -18 6 -6.53 14.19 0 18 -7 4595.91 159.86 0 18 7 4636.95 169.59 0 18 7 4588.47 166.58 0 18 -7 4690.08 166.64 0 18 -7 4657.71 171.25 0 -18 -7 4490.49 166.55 0 -18 -7 4602.11 172.83 0 -18 7 4577.79 170.08 0 18 -8 1176.64 62.62 0 18 8 1203.92 63.78 0 18 8 1193.01 122.93 0 18 -8 1120.88 65.99 0 18 -8 1183.41 97.32 0 -18 -8 1160.07 66.81 0 -18 -8 1179.92 75.96 0 -18 8 1261.39 69.72 0 18 -9 11.20 4.72 0 18 9 19.15 7.27 0 18 -9 10.13 5.28 0 18 9 34.19 10.78 0 18 -9 43.11 17.62 0 -18 -9 18.89 10.75 0 -18 9 28.86 14.95 0 18 -10 -0.18 3.36 0 18 10 6.40 5.12 0 18 -10 11.04 9.72 0 18 10 6.01 13.94 0 18 -10 7.46 13.84 0 -18 -10 16.40 8.84 0 -18 10 7.90 9.41 0 18 -11 82.33 26.23 0 18 11 139.18 28.56 0 18 -11 141.63 25.94 0 18 11 157.39 32.89 0 18 -11 142.72 29.35 0 -18 -11 114.78 27.18 0 -18 11 165.32 34.22 0 18 -12 95.32 27.60 0 18 12 182.59 38.63 0 18 -12 171.40 34.33 0 18 12 202.65 39.22 0 18 -12 259.57 38.00 0 -18 -12 180.80 39.66 0 -18 12 182.47 36.39 0 18 13 4646.56 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154.95 31.93 0 -19 18 195.46 43.46 0 19 19 1.00 9.21 0 19 -19 3.22 10.70 0 19 -19 12.69 11.57 0 -19 -19 56.97 20.72 0 -19 -19 16.00 11.60 0 -19 19 -5.44 11.93 0 19 20 67.57 22.44 0 19 -20 33.44 9.29 0 19 -20 98.47 27.41 0 -19 -20 71.71 28.45 0 -19 -20 83.39 18.60 0 19 21 118.28 41.52 0 19 -21 192.14 33.74 0 -19 -21 116.95 51.32 0 19 22 24.39 9.09 0 19 -22 30.06 14.14 0 19 -22 42.84 12.68 0 -19 -22 48.20 21.10 0 20 0 32.37 9.08 0 20 0 58.94 15.61 0 -20 0 49.05 17.37 0 20 -1 911.37 49.36 0 20 1 875.59 54.47 0 20 -1 902.96 49.55 0 20 -1 985.41 103.20 0 20 1 778.82 96.66 0 -20 -1 799.25 52.20 0 -20 -1 924.10 56.71 0 -20 1 934.46 62.75 0 20 -2 392.56 43.18 0 20 2 456.34 47.40 0 20 -2 414.28 46.25 0 20 -2 545.59 96.10 0 20 2 513.18 44.84 0 -20 -2 324.12 47.51 0 -20 -2 468.47 81.98 0 -20 2 446.84 95.40 0 20 -3 98.90 24.44 0 20 3 133.39 34.24 0 20 -3 141.38 30.15 0 20 3 204.48 50.46 0 20 -3 209.06 44.79 0 -20 -3 138.69 41.01 0 20 -4 431.00 23.36 0 20 4 465.83 27.56 0 20 -4 423.11 42.40 0 20 -4 506.40 77.01 0 20 4 517.45 64.58 0 -20 -4 386.52 25.31 0 -20 -4 442.79 68.79 0 -20 4 447.09 69.24 0 20 -5 735.12 52.50 0 20 5 844.71 43.95 0 20 -5 685.30 54.54 0 20 -5 855.92 121.10 0 20 5 866.46 59.05 0 -20 -5 637.58 45.74 0 -20 -5 804.69 80.52 0 -20 5 796.51 70.24 0 20 6 562.01 42.82 0 20 -6 586.06 49.99 0 20 6 590.95 83.97 0 20 -6 609.47 83.64 0 -20 -6 674.48 101.50 0 -20 6 658.07 89.21 0 20 -7 556.66 45.02 0 20 7 714.68 50.32 0 20 -7 695.38 68.68 0 20 -7 689.91 68.55 0 20 7 768.48 70.54 0 -20 -7 510.80 55.26 0 -20 -7 769.53 92.86 0 -20 7 603.25 98.08 0 20 -8 156.98 33.80 0 20 8 259.62 41.05 0 20 8 357.87 50.68 0 20 -8 250.62 32.12 0 20 -8 270.35 51.62 0 -20 -8 137.26 42.11 0 -20 -8 276.03 35.68 0 -20 8 274.21 55.07 0 20 9 120.15 28.61 0 20 -9 144.02 37.97 0 20 9 170.73 36.90 0 20 -9 179.12 36.06 0 -20 -9 165.53 36.11 0 -20 9 142.64 32.03 0 20 10 10.13 7.86 0 20 10 -3.50 8.84 0 20 -10 23.20 19.69 0 -20 -10 11.59 12.63 0 -20 10 16.14 7.94 0 20 11 -0.06 8.53 0 20 -11 -1.87 8.96 0 20 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37.71 0 -20 -19 122.47 36.40 0 -20 19 104.74 32.11 0 20 20 19.21 11.06 0 20 -20 8.41 8.63 0 20 -20 20.46 21.02 0 -20 -20 36.26 20.57 0 -20 -20 -1.53 10.10 0 20 21 277.82 79.42 0 20 -21 319.77 103.50 0 -20 -21 345.28 113.27 0 -20 -21 242.77 98.52 0 21 0 7.37 3.60 0 21 0 5.87 2.36 0 21 0 34.43 15.63 0 -21 0 21.90 14.92 0 21 -1 128.18 26.81 0 21 1 162.24 36.04 0 21 -1 149.31 34.84 0 21 -1 223.59 44.58 0 21 1 183.06 38.48 0 -21 -1 131.16 31.73 0 -21 -1 201.84 62.49 0 -21 1 186.27 47.02 0 21 -2 44.14 10.41 0 21 2 44.66 13.16 0 21 -2 34.84 11.60 0 21 -2 62.38 22.83 0 21 2 48.57 16.11 0 -21 -2 45.40 11.36 0 -21 -2 56.79 21.82 0 -21 2 79.41 25.35 0 21 -3 51.71 15.72 0 21 3 87.27 23.35 0 21 -3 78.73 18.43 0 21 -3 103.64 25.28 0 21 3 99.84 25.54 0 -21 -3 45.66 14.91 0 -21 -3 87.33 19.20 0 -21 3 137.92 29.60 0 21 -4 25.03 10.50 0 21 4 29.06 10.23 0 21 -4 35.59 10.38 0 21 -4 51.20 22.33 0 21 4 26.11 16.82 0 -21 -4 10.66 8.33 0 -21 -4 23.93 18.49 0 -21 4 62.84 20.09 0 21 5 389.78 27.16 0 21 -5 363.08 22.15 0 21 -5 325.36 61.82 0 21 5 450.49 54.98 0 -21 -5 269.11 34.16 0 -21 -5 380.16 53.60 0 -21 5 476.85 83.96 0 21 6 11.52 5.47 0 21 -6 1.86 4.54 0 21 6 -29.48 13.90 0 21 -6 10.49 11.29 0 -21 -6 10.02 12.97 0 -21 6 24.54 16.94 0 21 7 414.54 18.01 0 21 -7 401.38 30.00 0 21 7 423.82 73.74 0 21 -7 372.62 61.91 0 -21 -7 417.81 68.15 0 -21 7 389.63 75.68 0 21 8 1162.29 37.05 0 21 8 1047.09 74.70 0 21 -8 1207.18 113.07 0 -21 -8 1127.17 64.61 0 -21 8 1098.37 75.15 0 21 9 3.01 7.43 0 21 9 16.06 7.15 0 21 -9 1.99 9.07 0 -21 -9 -5.67 13.84 0 -21 9 1.03 8.61 0 21 10 12.78 5.63 0 21 -10 -0.47 7.23 0 21 10 29.39 13.54 0 21 -10 11.93 9.10 0 -21 -10 -5.85 13.03 0 -21 10 35.64 16.52 0 21 11 61.42 19.98 0 21 -11 30.03 7.69 0 21 11 68.42 19.94 0 21 -11 79.28 26.65 0 -21 -11 68.08 16.00 0 -21 11 93.62 20.13 0 21 12 140.18 37.81 0 21 -12 153.75 33.99 0 21 12 220.07 43.52 0 21 -12 184.66 36.27 0 -21 -12 188.87 29.19 0 -21 12 200.41 42.02 0 21 13 57.94 13.07 0 21 -13 50.12 11.51 0 21 13 38.85 10.25 0 21 -13 35.86 15.15 0 -21 -13 65.90 18.99 0 -21 13 35.66 12.58 0 21 14 752.42 24.56 0 21 -14 629.48 26.67 0 21 14 816.87 84.98 0 21 -14 795.82 46.77 0 -21 -14 639.60 84.92 0 -21 14 630.88 31.70 0 21 15 77.56 18.25 0 21 -15 58.16 16.94 0 21 15 64.21 16.21 0 -21 -15 61.85 30.76 0 -21 15 39.35 14.81 0 21 16 1458.30 82.94 0 21 -16 1408.15 77.74 0 21 16 1437.60 76.43 0 21 -16 1565.33 107.19 0 -21 -16 1094.23 160.28 0 -21 16 1388.68 83.53 0 21 17 -8.10 8.77 0 21 -17 1.51 4.05 0 21 17 17.88 14.04 0 21 -17 11.10 17.36 0 -21 -17 17.54 9.22 0 -21 17 28.08 7.51 0 21 18 231.83 75.29 0 21 18 327.82 59.94 0 21 -18 227.10 67.73 0 -21 -18 247.59 72.61 0 -21 18 268.64 71.73 0 21 19 666.11 69.59 0 21 19 591.45 125.02 0 21 -19 476.63 138.66 0 -21 -19 480.16 114.66 0 -21 19 344.91 104.38 0 21 20 15.63 8.56 0 21 -20 34.15 12.58 0 -21 -20 46.28 20.17 0 -21 -20 44.26 20.46 0 22 0 387.76 16.38 0 22 0 474.86 50.58 0 -22 0 423.04 54.62 0 22 1 204.78 45.67 0 22 -1 183.63 42.76 0 22 1 155.01 37.57 0 22 -1 248.37 50.36 0 -22 1 191.49 40.60 0 -22 -1 269.42 43.28 0 22 2 55.70 22.67 0 22 -2 38.09 10.21 0 22 2 73.09 19.54 0 22 -2 39.59 14.88 0 -22 -2 57.56 24.71 0 -22 2 29.99 16.24 0 22 3 76.83 19.86 0 22 -3 80.68 19.55 0 22 3 146.33 25.21 0 22 -3 115.22 21.67 0 -22 -3 111.26 21.78 0 -22 3 107.03 19.13 0 22 -4 11.22 7.87 0 22 4 9.47 9.52 0 22 -4 11.85 10.77 0 -22 -4 40.50 19.66 0 -22 4 1.43 6.81 0 22 5 11.62 9.64 0 22 -5 17.87 8.24 0 22 5 19.13 10.72 0 22 -5 -6.40 15.11 0 -22 -5 35.32 23.33 0 -22 5 12.24 14.42 0 22 6 531.47 26.21 0 22 -6 561.04 16.23 0 22 6 520.13 89.13 0 22 -6 566.35 47.00 0 -22 -6 585.43 90.59 0 -22 6 557.49 74.25 0 22 7 261.11 46.71 0 22 -7 257.24 29.35 0 22 7 305.10 60.53 0 22 -7 263.66 74.89 0 -22 -7 329.85 52.91 0 -22 7 256.39 54.89 0 22 8 57.19 17.97 0 22 -8 55.30 16.31 0 22 8 125.55 20.07 0 22 -8 91.80 19.18 0 -22 -8 103.59 36.15 0 -22 8 103.89 37.28 0 22 9 229.00 37.94 0 22 -9 196.76 39.93 0 22 9 278.41 57.19 0 22 -9 224.26 45.93 0 -22 -9 313.65 66.28 0 -22 9 291.98 55.04 0 22 10 21.54 10.14 0 22 -10 12.26 6.94 0 22 10 35.68 11.75 0 22 -10 23.81 11.06 0 -22 -10 41.42 16.66 0 -22 10 32.06 18.26 0 22 11 -7.48 8.10 0 22 11 29.32 13.85 0 22 -11 25.18 10.28 0 -22 -11 11.70 12.46 0 -22 11 -9.72 13.12 0 22 12 7.67 7.30 0 22 -12 6.71 6.93 0 22 12 1.43 8.12 0 22 -12 27.74 10.32 0 -22 -12 14.45 10.70 0 -22 12 18.22 10.59 0 22 13 144.56 37.54 0 22 13 169.19 43.96 0 22 -13 133.52 34.59 0 -22 -13 225.92 45.64 0 -22 13 181.85 35.49 0 22 14 91.72 24.51 0 22 14 105.08 18.67 0 22 -14 111.19 31.49 0 -22 -14 94.03 30.49 0 -22 14 103.66 23.05 0 22 15 103.70 21.23 0 22 15 92.38 12.68 0 22 -15 81.03 25.22 0 -22 -15 65.47 31.25 0 -22 15 72.37 24.61 0 22 16 8.96 6.61 0 22 16 38.60 18.15 0 22 -16 33.55 12.92 0 -22 -16 -1.86 10.35 0 -22 16 16.75 7.41 0 22 17 821.37 84.95 0 22 17 748.57 113.95 0 22 -17 783.50 107.07 0 -22 -17 806.50 119.91 0 -22 17 500.19 123.78 0 22 18 130.09 37.10 0 22 18 188.90 31.17 0 22 -18 186.22 34.52 0 -22 -18 110.32 19.55 0 -22 18 71.48 27.32 0 22 19 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366.97 57.99 -3 13 13 236.41 40.26 -3 13 13 232.54 43.53 3 13 -13 237.57 45.32 3 13 -13 249.75 43.03 3 -13 -13 138.72 36.32 -3 -13 13 179.38 30.88 3 -13 -13 230.89 48.01 -3 -13 13 200.56 29.43 -3 13 12 796.25 72.74 -3 13 12 837.44 81.92 3 13 -12 719.73 88.34 3 13 -12 799.11 67.19 3 -13 -12 685.28 63.88 -3 -13 12 754.33 56.87 3 -13 -12 864.98 84.10 -3 -13 12 743.13 68.38 -3 13 11 160.88 28.51 -3 13 11 125.08 22.12 3 13 -11 209.50 28.40 3 13 -11 176.96 26.79 3 -13 -11 102.50 26.65 -3 -13 11 139.92 23.09 -3 -13 11 156.40 22.52 3 -13 -11 180.50 30.85 -3 13 10 8.52 3.60 -3 13 10 10.03 7.56 3 13 -10 10.16 6.40 3 13 -10 23.75 14.41 3 -13 -10 6.76 5.53 -3 -13 10 11.71 6.52 -3 -13 10 12.42 5.34 3 -13 -10 -1.38 11.06 3 13 -9 29.13 8.41 -3 13 9 14.72 4.62 -3 13 9 15.10 10.74 3 13 -9 17.33 7.25 3 13 -9 37.15 11.09 3 -13 -9 15.97 7.55 -3 -13 9 31.81 6.27 -3 -13 9 34.35 7.37 3 -13 -9 30.45 13.54 3 13 -8 2054.71 80.71 -3 13 8 2011.62 75.57 -3 13 8 1978.84 93.16 3 13 -8 2075.94 83.22 3 13 -8 2148.08 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1023.99 42.07 4 -11 0 1131.40 40.45 -4 -11 0 1144.37 50.77 4 -11 0 1153.99 41.96 4 11 1 491.14 32.69 4 11 1 468.55 25.46 -4 11 -1 461.86 30.42 4 11 1 567.73 46.64 -4 11 -1 469.91 24.69 -4 -11 -1 501.85 28.29 4 -11 1 518.15 26.77 4 -11 1 485.23 25.05 -4 -11 -1 433.18 24.34 -4 -11 -1 513.36 51.63 4 11 2 19.88 10.13 4 11 2 13.30 5.20 4 11 2 17.96 10.71 -4 11 -2 -7.30 8.99 -4 11 -2 2.79 8.85 -4 -11 -2 -1.36 5.60 -4 -11 -2 16.43 7.44 4 -11 2 10.88 7.21 -4 -11 -2 -8.29 10.45 4 -11 2 -6.27 7.92 4 11 3 97.70 18.84 4 11 3 68.41 12.57 4 11 3 73.73 16.15 -4 11 -3 72.10 15.71 -4 11 -3 110.76 20.87 -4 -11 -3 73.04 13.20 -4 -11 -3 82.58 17.48 4 -11 3 94.45 14.98 -4 -11 -3 79.30 17.16 4 -11 3 72.78 14.36 4 11 4 67.02 10.24 4 11 4 95.56 18.73 4 11 4 78.05 15.03 -4 11 -4 59.68 7.42 -4 11 -4 78.71 12.07 -4 11 -4 83.95 13.96 -4 -11 -4 92.49 15.96 4 -11 4 80.72 14.19 4 -11 4 63.70 7.00 4 -11 4 78.63 17.11 -4 -11 -4 70.14 15.67 -4 -11 -4 80.93 15.34 4 11 5 588.64 48.19 4 11 5 546.60 34.41 4 11 5 530.64 36.96 -4 11 -5 545.44 29.30 -4 11 -5 614.20 41.08 -4 11 -5 566.70 33.49 -4 -11 -5 602.13 51.20 4 -11 5 553.09 33.11 4 -11 5 553.31 28.85 4 -11 5 501.25 16.63 -4 -11 -5 628.38 62.43 -4 -11 -5 535.60 77.70 -4 11 -6 8731.16 186.57 4 11 6 9237.44 198.61 -4 11 -6 8784.93 180.61 4 11 6 8952.13 195.97 -4 11 -6 8929.43 193.25 4 -11 6 9436.73 192.64 4 -11 6 7857.33 174.11 -4 -11 -6 8961.29 190.07 -4 -11 -6 8778.80 190.20 4 11 7 321.21 54.32 -4 11 -7 278.00 22.66 4 11 7 336.77 46.18 -4 11 -7 321.35 42.98 -4 11 -7 304.44 40.02 4 -11 7 267.93 13.17 -4 -11 -7 247.26 39.17 4 -11 7 274.16 50.24 -4 -11 -7 348.41 52.75 -4 11 -8 2356.78 77.25 4 11 8 2323.00 82.69 4 11 8 2392.68 84.96 -4 11 -8 2556.84 89.07 -4 11 -8 2479.62 93.86 4 -11 8 2566.63 85.42 -4 -11 -8 2397.32 82.08 4 -11 8 2324.52 81.04 -4 -11 -8 2361.44 102.59 -4 11 -9 -8.61 5.35 4 11 9 26.58 9.81 4 11 9 10.55 8.96 -4 11 -9 11.67 9.39 -4 11 -9 21.94 7.34 4 -11 9 8.34 6.33 -4 -11 -9 12.66 5.91 4 -11 9 17.65 12.34 -4 -11 -9 12.93 11.65 -4 11 -10 2019.68 97.91 -4 11 -10 1821.53 69.17 4 11 10 1941.71 77.33 4 11 10 1984.57 84.16 -4 11 -10 2028.65 80.62 4 -11 10 1930.32 77.20 4 -11 10 2138.73 82.24 -4 -11 -10 2085.69 85.07 -4 11 -11 6450.28 194.38 -4 11 -11 5953.39 161.92 4 11 11 6173.34 172.45 4 11 11 6568.38 194.69 -4 11 -11 6733.98 196.71 4 -11 11 6737.56 182.77 -4 -11 -11 6783.64 193.29 -4 11 -12 2530.89 100.51 4 11 12 2430.56 96.24 4 11 12 2536.75 114.62 -4 11 -12 2394.53 96.89 4 -11 12 2593.51 97.29 -4 -11 -12 2613.44 110.14 -4 11 -13 -2.45 12.74 -4 11 -13 5.28 3.32 4 11 13 18.18 7.99 4 11 13 13.93 9.97 -4 11 -13 -6.35 10.14 4 -11 13 2.76 5.35 -4 -11 -13 28.00 12.65 -4 11 -14 1610.93 80.58 4 11 14 2088.98 93.38 -4 11 -14 1786.04 91.88 -4 11 -14 1953.34 85.20 4 -11 14 1985.13 80.57 -4 -11 -14 1986.89 133.53 -4 -11 -14 1867.31 204.54 4 11 15 486.85 54.81 -4 11 -15 348.61 50.20 -4 11 -15 515.47 70.64 -4 11 -15 469.57 74.07 4 -11 15 481.07 40.30 -4 -11 -15 575.55 78.59 -4 -11 -15 583.37 82.00 -4 11 -16 327.67 38.15 4 11 16 364.03 62.26 -4 11 -16 304.34 46.17 -4 -11 -16 229.78 40.10 4 -11 16 313.53 43.75 -4 -11 -16 319.90 56.70 -4 11 -17 26.77 9.88 4 11 17 19.00 12.43 -4 11 -17 10.14 8.81 -4 -11 -17 13.76 13.71 4 -11 17 14.80 7.57 -4 -11 -17 40.06 11.96 -4 11 -18 586.13 46.63 4 11 18 557.20 82.59 -4 11 -18 634.08 54.98 -4 -11 -18 613.64 98.56 4 -11 18 627.59 70.75 -4 -11 -18 699.76 75.80 -4 11 -19 2007.10 86.23 4 11 19 1963.47 99.09 -4 11 -19 1913.38 85.78 -4 -11 -19 1889.94 152.40 4 -11 19 2070.63 94.55 -4 -11 -19 1819.95 90.58 -4 11 -20 6.40 15.36 4 11 20 29.17 10.37 -4 11 -20 24.44 13.20 -4 -11 -20 83.24 19.11 4 -11 20 19.21 9.18 -4 -11 -20 14.72 14.67 -4 11 -21 172.49 29.64 4 11 21 166.91 23.04 -4 11 -21 182.39 32.87 -4 -11 -21 109.19 23.88 4 -11 21 151.25 33.41 -4 -11 -21 215.54 30.37 -4 11 -22 160.28 38.84 4 11 22 164.11 44.57 -4 11 -22 228.40 53.83 -4 -11 -22 259.69 34.82 4 -11 22 200.00 48.99 -4 -11 -22 195.89 54.18 -4 11 -23 340.10 48.36 4 11 23 288.01 60.32 4 -11 23 265.76 57.62 -4 -11 -23 309.85 56.65 -4 -11 -23 313.90 66.49 -4 11 -24 1196.55 110.05 4 11 24 1240.92 72.96 -4 11 -24 999.59 142.33 -4 -11 -24 955.82 154.15 4 -11 24 1178.63 110.63 -4 -11 -24 1208.00 118.18 -4 11 -25 -2.49 16.82 4 11 25 -0.04 12.08 4 -11 25 23.28 9.83 -4 -11 -25 33.12 14.00 -4 12 25 91.62 28.74 4 12 -25 151.30 46.45 4 12 -25 124.73 33.65 4 -12 -25 113.81 38.24 -4 12 24 2126.00 96.36 4 12 -24 2180.51 109.58 4 12 -24 2018.86 800.68 4 -12 -24 2130.82 119.42 4 -12 -24 2030.99 799.27 -4 12 23 20.58 11.36 4 12 -23 28.39 23.46 4 12 -23 3.85 13.37 4 -12 -23 22.70 22.72 4 -12 -23 42.88 17.20 -4 12 22 175.78 39.73 4 12 -22 176.06 37.69 4 12 -22 166.20 25.57 4 -12 -22 155.27 46.61 4 -12 -22 153.19 34.71 -4 12 21 726.23 51.27 4 12 -21 738.63 71.09 4 12 -21 748.43 86.97 4 -12 -21 786.63 93.10 4 -12 -21 606.13 103.86 -4 12 20 242.24 45.64 4 12 -20 253.70 53.91 4 12 -20 287.95 58.09 4 -12 -20 258.36 45.33 4 -12 -20 269.53 52.34 -4 12 19 1518.26 43.28 4 12 -19 1512.64 58.79 4 12 -19 1608.58 130.34 4 -12 -19 1442.05 150.37 4 -12 -19 1498.73 43.40 -4 12 18 240.87 48.65 4 12 -18 231.00 39.76 4 12 -18 268.12 44.38 4 -12 -18 234.56 40.55 4 -12 -18 254.87 33.09 -4 12 17 9.81 6.63 4 12 -17 23.77 12.72 4 12 -17 31.57 19.79 4 -12 -17 32.26 15.29 4 -12 -17 30.05 10.97 -4 -12 17 8.59 4.21 -4 12 16 910.96 48.64 4 12 -16 1035.89 129.87 4 12 -16 890.30 119.70 4 -12 -16 992.13 100.04 -4 -12 16 859.87 42.78 4 -12 -16 1040.74 71.65 -4 -12 16 884.31 42.52 -4 12 15 -22.02 8.63 4 12 -15 8.29 7.89 4 12 -15 42.40 17.00 4 -12 -15 23.37 21.11 -4 -12 15 6.21 3.48 4 -12 -15 19.92 12.86 -4 -12 15 4.41 3.30 -4 12 14 76.55 19.15 4 12 -14 91.18 23.12 4 12 -14 146.72 33.67 4 -12 -14 163.70 40.01 -4 -12 14 107.64 23.10 -4 -12 14 64.96 14.21 4 -12 -14 115.35 26.21 -4 12 13 854.64 62.29 -4 12 13 813.59 54.27 4 12 -13 873.69 65.60 4 12 -13 955.28 101.58 4 -12 -13 856.85 52.19 -4 -12 13 780.24 44.71 4 -12 -13 913.30 80.93 -4 -12 13 742.42 41.91 -4 12 1210774.37 305.57 -4 12 1210189.51 289.36 4 12 -1210570.88 299.70 4 12 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1129.64 47.35 4 -12 -3 1131.99 65.02 4 -12 -3 1283.15 57.33 4 12 -2 436.99 39.38 -4 12 2 384.81 22.65 4 12 -2 523.94 61.38 4 12 -2 402.14 44.34 -4 -12 2 431.76 27.57 4 -12 -2 414.50 26.36 -4 -12 2 463.69 52.73 -4 -12 2 409.71 28.83 4 -12 -2 450.09 59.31 4 -12 -2 493.55 28.11 4 12 -1 3493.45 103.29 4 12 -1 3503.97 103.16 -4 12 1 3359.35 97.85 4 12 -1 3416.53 101.33 -4 -12 1 3460.63 101.50 -4 -12 1 3399.79 96.59 -4 -12 1 3430.75 101.33 4 -12 -1 3532.90 103.13 4 12 0 9448.35 203.36 4 12 0 9239.27 196.51 -4 12 0 9194.96 195.71 4 12 0 8940.21 201.13 -4 12 0 9184.38 206.32 -4 -12 0 8278.68 178.67 4 -12 0 8962.10 193.83 -4 -12 0 8889.02 192.33 -4 -12 0 8705.23 185.68 4 12 1 3046.89 89.73 4 12 1 3370.71 95.17 -4 12 -1 3278.62 97.67 4 12 1 3150.34 92.81 -4 12 -1 3264.05 110.58 -4 -12 -1 3300.93 94.71 -4 -12 -1 3116.51 88.32 -4 -12 -1 3059.03 107.53 4 -12 1 3183.94 92.55 4 12 2 1311.83 55.56 -4 12 -2 1436.02 57.40 4 12 2 1364.42 55.47 4 12 2 1297.28 88.72 -4 12 -2 1102.03 56.90 -4 -12 -2 1264.02 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35.92 13.73 7 -14 -14 8.16 25.97 7 -14 -14 -0.13 14.50 7 14 -13 29.65 13.68 7 14 -13 27.59 14.03 7 -14 -13 11.29 10.60 7 -14 -13 23.61 20.20 7 -14 -13 -13.33 14.06 7 14 -12 1887.12 84.20 7 14 -12 2104.15 95.46 7 -14 -12 1902.94 84.17 7 -14 -12 1927.30 93.06 7 -14 -12 2008.62 88.98 -7 14 11 108.92 22.69 7 14 -11 94.07 15.00 7 14 -11 80.24 28.56 7 -14 -11 106.34 20.73 -7 -14 11 72.78 15.10 7 -14 -11 91.92 22.01 7 14 -10 858.60 98.63 7 14 -10 774.58 82.99 -7 14 10 773.44 61.22 7 -14 -10 726.08 45.23 -7 -14 10 731.04 40.19 7 -14 -10 762.50 117.73 7 14 -9 320.40 52.44 7 14 -9 384.26 33.38 -7 14 9 301.19 48.47 7 -14 -9 239.90 29.04 7 -14 -9 200.06 37.78 -7 -14 9 242.83 42.49 7 -14 -9 315.95 53.62 7 14 -8 914.60 83.72 7 14 -8 859.78 54.05 -7 14 8 889.66 63.84 7 14 -8 748.43 47.37 7 -14 -8 812.89 44.95 7 -14 -8 823.85 40.82 7 -14 -8 840.02 92.19 -7 -14 8 787.26 73.09 7 14 -7 129.63 27.80 7 14 -7 138.88 31.88 7 14 -7 54.68 19.59 -7 14 7 157.44 35.39 7 -14 -7 91.17 23.86 -7 -14 7 112.49 46.66 7 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26.57 -10 7 7 1060.41 230.64 10 7 -7 1109.31 46.86 10 7 -7 952.09 27.83 10 -7 -7 946.19 22.50 10 -7 -7 1060.02 230.79 -10 7 6 24.22 8.00 10 7 -6 99.67 17.53 10 7 -6 61.77 12.44 10 -7 -6 51.50 11.71 10 -7 -6 112.59 18.75 -10 7 5 515.02 41.18 10 7 -5 450.48 72.77 10 7 -5 409.84 21.11 10 -7 -5 468.18 15.82 10 -7 -5 397.12 44.91 -10 -7 5 440.97 163.84 10 7 -4 -9.19 14.72 10 7 -4 2.16 2.43 -10 7 4 20.98 6.06 10 -7 -4 20.33 10.87 10 -7 -4 4.85 3.07 -10 -7 4 11.34 6.18 10 7 -3 37.46 13.74 10 7 -3 6.63 5.17 -10 7 3 20.24 9.30 10 -7 -3 14.09 8.88 10 -7 -3 6.48 4.78 -10 -7 3 -0.18 8.45 10 7 -2 772.80 88.58 10 7 -2 636.85 10.41 -10 7 2 772.94 86.38 10 -7 -2 719.35 47.23 10 -7 -2 616.82 8.95 -10 -7 2 726.29 40.96 10 7 -1 102.74 21.84 10 7 -1 169.54 33.58 -10 7 1 164.35 40.41 10 -7 -1 185.13 38.01 -10 -7 1 191.37 34.12 10 7 0 182.49 39.40 -10 7 0 211.04 47.00 10 -7 0 167.08 42.74 -10 -7 0 189.56 41.94 10 7 1 47.96 15.56 -10 7 -1 48.05 14.77 10 -7 1 29.67 11.27 -10 -7 -1 58.68 26.76 -10 7 -2 2506.27 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743.66 95.37 10 11 -18 24.96 11.95 10 11 -17 317.49 87.33 10 11 -17 290.46 75.44 10 -11 -17 361.72 52.82 10 11 -16 169.35 59.92 10 11 -16 277.94 71.80 10 -11 -16 195.26 49.67 10 -11 -16 272.24 51.27 10 11 -15 953.21 132.39 10 -11 -15 890.66 95.02 10 11 -14 1797.35 111.75 10 11 -14 1747.89 131.10 10 -11 -14 1958.54 104.66 10 -11 -14 1840.19 102.55 10 11 -13 59.25 24.56 10 11 -13 16.70 17.22 10 -11 -13 25.34 11.88 10 -11 -13 42.41 14.55 10 11 -12 626.49 79.37 10 -11 -12 448.00 101.31 10 11 -11 70.44 20.70 10 11 -11 49.92 16.75 10 -11 -11 24.58 9.85 10 -11 -11 18.56 14.14 10 11 -10 127.91 26.83 10 11 -10 146.33 23.36 10 -11 -10 87.47 20.30 10 -11 -10 85.19 21.79 10 11 -9 255.17 58.57 10 11 -9 274.49 69.77 10 -11 -9 292.16 41.92 10 -11 -9 239.94 52.93 10 -11 -9 261.25 57.12 10 11 -8 1252.25 28.85 10 11 -8 1289.96 43.68 10 -11 -8 1476.32 75.57 10 -11 -8 1304.97 42.13 10 -11 -8 1487.02 85.36 10 11 -7 108.06 25.01 10 11 -7 173.51 49.48 10 -11 -7 134.91 64.72 -10 -11 7 134.20 57.94 10 -11 -7 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13 220.79 52.33 -10 11 -13 203.74 55.09 -10 -11 -13 148.21 50.73 10 11 14 350.33 81.01 -10 11 -14 497.24 73.07 -10 -11 -14 222.97 88.59 10 11 15 2385.98 116.56 -10 11 -15 2239.63 133.81 -10 -11 -15 2263.93 120.87 10 11 16 193.31 52.13 -10 11 -16 203.02 45.73 -10 -11 -16 173.31 49.52 10 12 -17 203.25 76.33 10 -12 -17 117.58 38.16 10 -12 -17 127.92 54.03 10 12 -16 166.80 50.24 10 12 -16 241.09 126.79 10 -12 -16 153.31 49.44 10 -12 -16 147.43 41.55 10 12 -15 223.93 62.69 10 12 -15 221.42 50.01 10 -12 -15 182.97 55.76 10 -12 -15 171.18 49.30 10 -12 -15 164.46 47.70 10 12 -14 432.48 106.48 10 -12 -14 394.41 69.30 10 -12 -14 366.26 159.32 10 -12 -14 379.55 65.09 10 12 -13 61.65 14.72 10 12 -13 33.17 11.09 10 -12 -13 41.76 11.74 10 -12 -13 62.82 15.73 10 12 -12 1404.46 113.43 10 12 -12 1538.76 80.27 10 -12 -12 1628.70 81.60 10 -12 -12 1533.69 88.94 10 12 -11 10.41 14.06 10 -12 -11 19.77 11.13 10 12 -10 1366.23 53.75 10 12 -10 1421.68 63.36 10 -12 -10 1287.54 59.64 10 -12 -10 1220.75 93.84 10 12 -9 144.72 23.81 10 12 -9 154.13 42.29 10 -12 -9 122.90 34.02 10 -12 -9 108.88 30.70 10 -12 -9 141.75 38.25 10 12 -8 249.44 63.11 10 12 -8 327.08 89.23 10 -12 -8 336.50 22.68 10 -12 -8 234.32 61.23 10 -12 -8 295.36 53.56 10 12 -7 104.20 19.37 10 12 -7 133.76 71.54 10 -12 -7 85.50 26.00 10 -12 -7 97.89 30.55 -10 -12 7 106.45 24.36 10 -12 -7 138.95 35.48 10 12 -6 2126.84 99.70 10 12 -6 1944.04 72.12 10 -12 -6 2006.66 73.27 -10 -12 6 2073.71 76.53 10 12 -5 255.57 40.90 -10 12 5 225.00 41.95 -10 -12 5 138.67 35.76 10 12 -4 2558.93 982.42 10 12 -4 2352.61 83.90 -10 12 4 2510.51 98.03 10 -12 -4 2319.29 88.25 -10 -12 4 2369.62 90.39 10 12 -3 1002.79 129.43 10 12 -3 1085.92 24.41 -10 12 3 1161.80 33.08 -10 -12 3 1119.63 30.35 -10 12 2 370.74 57.75 10 12 -2 301.20 63.50 -10 12 2 238.04 14.30 10 12 -2 158.84 65.03 10 -12 -2 229.56 37.70 -10 -12 2 251.67 53.55 10 12 -1 102.66 23.77 -10 12 1 60.91 15.26 10 12 -1 65.66 19.19 -10 12 1 110.06 20.05 -10 -12 1 69.85 22.16 -10 12 0 33.28 14.64 10 12 0 20.15 12.98 -10 12 0 18.26 6.35 10 12 0 9.71 5.92 10 -12 0 7.40 4.99 -10 -12 0 10.33 10.22 -10 12 -1 282.21 47.24 10 12 1 227.27 40.89 10 -12 1 174.13 40.61 -10 -12 -1 249.35 55.03 10 12 2 112.63 36.97 10 12 2 176.59 46.73 -10 12 -2 177.55 26.94 10 -12 2 162.28 29.04 -10 -12 -2 216.88 40.82 10 12 3 1664.08 103.03 10 12 3 1479.39 71.95 -10 12 -3 1686.37 87.41 -10 -12 -3 1636.76 86.26 10 12 4 466.00 100.83 -10 12 -4 474.27 63.25 -10 -12 -4 457.85 65.15 10 12 5 2687.78 126.13 -10 12 -5 3093.94 144.47 -10 -12 -5 3044.40 149.34 10 12 6 1989.81 81.13 -10 12 -6 2678.79 121.54 -10 -12 -6 2699.97 121.08 10 12 7 27.35 16.95 -10 12 -7 38.00 19.70 -10 -12 -7 48.73 12.44 10 12 8 2073.87 94.33 -10 12 -8 1960.33 90.18 -10 -12 -8 1905.42 101.49 10 12 9 18.92 7.06 -10 12 -9 9.04 9.33 -10 -12 -9 6.49 10.75 10 12 10 95.37 21.39 -10 -12 -10 45.81 20.84 10 12 11 912.84 119.23 -10 12 -11 1019.00 75.59 10 12 12 22.98 11.45 -10 12 -12 33.17 20.08 -10 -12 -12 42.11 17.30 10 12 13 322.84 67.59 -10 12 -13 229.05 87.88 -10 -12 -13 267.93 81.06 10 12 14 93.06 18.41 -10 12 -14 62.06 21.28 -10 -12 -14 51.21 12.33 10 12 15 124.40 51.31 -10 12 -15 131.75 26.87 -10 -12 -15 100.76 31.16 10 12 16 468.19 117.19 -10 12 -16 408.86 126.53 -10 -12 -16 271.90 122.10 10 13 -16 2387.13 141.79 10 -13 -16 2104.85 128.94 10 13 -15 22.85 17.22 10 13 -15 43.74 10.78 10 -13 -15 5.99 9.95 10 -13 -15 12.82 10.96 10 13 -14 1315.10 153.57 10 13 -14 1344.03 78.99 10 -13 -14 1247.38 74.65 10 -13 -14 1224.99 534.54 10 13 -13 622.45 127.93 10 -13 -13 661.19 32.34 10 -13 -13 470.22 107.96 10 13 -12 530.24 101.86 10 13 -12 385.17 95.78 10 -13 -12 353.27 89.87 10 -13 -12 489.55 106.04 10 13 -11 24.66 17.94 10 13 -11 15.96 11.84 10 -13 -11 26.20 6.78 10 13 -10 97.95 25.15 10 13 -10 69.44 19.10 10 -13 -10 117.02 24.76 10 13 -9 528.12 122.74 10 -13 -9 589.40 91.36 10 13 -8 1230.50 102.47 10 13 -8 1215.82 31.94 10 -13 -8 1171.24 40.66 10 -13 -8 1203.25 44.12 10 13 -7 247.70 50.30 10 13 -7 163.39 43.04 10 -13 -7 202.77 44.33 10 13 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18.43 9.50 -10 -13 -5 -50.38 17.12 10 13 6 385.36 107.90 -10 13 -6 465.04 74.86 -10 -13 -6 438.12 83.79 10 13 7 1435.89 75.35 -10 13 -7 1315.21 84.15 -10 -13 -7 1221.29 40.51 10 13 8 810.93 131.45 -10 13 -8 832.64 82.06 -10 -13 -8 608.77 101.93 10 13 9 45.19 18.56 -10 13 -9 -21.43 18.44 -10 -13 -9 3.54 11.15 10 13 10 1550.21 89.23 -10 13 -10 1632.89 92.80 -10 -13 -10 1595.57 93.23 10 13 11 13.09 8.58 -10 13 -11 34.03 13.51 -10 -13 -11 24.82 11.83 10 13 12 -3.12 18.30 -10 13 -12 43.67 21.87 -10 -13 -12 47.75 16.15 10 13 13 1843.54 802.43 -10 13 -13 1890.37 822.23 -10 -13 -13 1570.17 93.11 10 13 14 292.54 92.83 -10 13 -14 293.65 75.65 -10 -13 -14 229.29 73.62 10 13 15 640.07 103.45 -10 13 -15 582.42 81.50 -10 -13 -15 319.51 119.92 10 14 -15 65.19 26.33 10 14 -15 3.71 14.97 10 -14 -15 35.76 18.86 10 14 -14 1737.31 126.99 10 14 -14 1759.00 99.62 10 -14 -14 1812.50 103.06 10 -14 -14 1761.77 124.76 10 14 -13 271.92 48.02 10 14 -13 139.38 47.82 10 -14 -13 159.77 48.38 10 -14 -13 173.37 56.28 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10 14 0 2134.60 89.11 -10 14 0 2358.36 103.90 -10 -14 0 2138.85 95.67 10 14 1 143.07 37.24 10 14 1 87.89 24.68 -10 14 -1 202.35 27.11 -10 -14 -1 171.01 22.90 10 14 2 807.66 77.88 10 14 2 744.76 21.03 -10 14 -2 830.40 83.94 -10 -14 -2 873.44 31.48 10 14 3 546.46 61.79 -10 14 -3 573.87 74.89 -10 -14 -3 476.24 61.42 10 14 4 498.28 112.78 -10 14 -4 584.82 74.84 -10 -14 -4 541.62 62.13 10 14 5 94.79 36.26 -10 14 -5 171.63 31.58 -10 -14 -5 62.43 19.48 10 14 6 3320.47 142.63 -10 14 -6 3153.32 133.60 -10 -14 -6 3053.88 127.79 10 14 7 2375.52 106.29 -10 14 -7 2211.50 112.03 -10 -14 -7 1993.02 100.42 10 14 8 438.83 119.36 -10 14 -8 560.78 92.23 -10 -14 -8 522.75 93.71 10 14 9 219.22 71.99 -10 14 -9 206.94 62.43 -10 -14 -9 248.40 37.87 10 14 10 71.70 22.11 -10 14 -10 105.82 29.76 -10 -14 -10 88.02 14.62 10 14 11 1203.55 112.07 -10 14 -11 1180.90 117.22 -10 -14 -11 1141.40 114.75 10 14 12 835.55 171.95 -10 14 -12 1170.00 110.42 10 14 13 12.08 11.79 -10 14 -13 37.96 13.94 -10 -14 -13 -9.19 21.59 10 14 14 988.85 135.38 -10 14 -14 1048.41 94.15 -10 -14 -14 856.91 177.18 10 15 -14 37.35 15.19 10 -15 -14 15.21 14.45 10 -15 -14 8.42 9.60 10 15 -13 130.35 30.56 10 -15 -13 26.57 14.51 10 -15 -13 75.86 21.91 10 15 -12 821.06 92.44 10 15 -12 772.89 82.33 10 -15 -12 751.08 93.24 10 -15 -12 845.59 80.23 10 15 -11 11.27 11.32 10 15 -11 11.59 10.25 10 -15 -11 25.16 13.98 10 -15 -11 -8.69 13.42 10 15 -10 1597.07 95.61 10 15 -10 1417.85 91.51 10 -15 -10 1412.74 82.66 10 -15 -10 1569.08 90.49 10 15 -9 24.50 16.95 10 -15 -9 35.87 17.84 10 -15 -9 4.40 13.80 10 15 -8 828.96 155.45 10 -15 -8 1034.52 74.95 10 -15 -8 938.65 91.95 10 15 -7 29.10 12.00 10 15 -7 16.10 11.59 10 -15 -7 11.17 9.12 10 -15 -7 51.61 19.08 10 15 -6 221.91 41.55 10 -15 -6 202.61 49.87 10 15 -5 21.23 21.30 -10 15 5 24.57 12.13 -10 -15 5 -13.61 9.75 10 -15 -5 8.03 11.48 10 15 -4 2628.01 123.40 10 -15 -4 2704.64 123.14 10 15 -3 2321.13 109.66 -10 15 3 2124.00 95.21 -10 -15 3 2076.34 92.47 10 15 -2 284.22 47.04 -10 15 2 311.54 80.85 -10 -15 2 272.44 55.45 10 15 -1 101.85 26.20 10 15 -1 76.14 22.86 -10 15 1 126.42 15.02 -10 -15 1 112.25 18.46 10 15 0 345.43 82.48 10 15 0 178.89 58.96 -10 15 0 377.23 68.77 -10 -15 0 313.92 58.08 10 15 1 94.56 28.78 -10 15 -1 94.56 16.45 -10 -15 -1 128.64 25.54 10 15 2 3611.10 160.05 -10 15 -2 3568.14 131.71 -10 -15 -2 3520.42 131.03 10 15 3 13.33 15.05 -10 15 -3 82.63 22.05 -10 -15 -3 12.64 13.15 10 15 4 3181.79 144.29 -10 15 -4 3012.99 151.26 -10 -15 -4 3087.11 130.51 10 15 5 709.82 60.32 -10 15 -5 735.43 44.65 -10 -15 -5 560.89 74.40 10 15 6 18.47 9.00 -10 15 -6 24.63 11.45 -10 -15 -6 21.48 9.13 10 15 7 15.09 8.70 -10 15 -7 -9.42 15.86 -10 -15 -7 19.23 13.55 10 15 8 102.81 27.95 -10 15 -8 91.04 28.45 -10 -15 -8 92.17 20.55 10 15 9 473.14 110.49 -10 15 -9 565.37 82.77 -10 -15 -9 497.05 81.38 10 15 10 2105.38 106.72 -10 15 -10 2008.49 104.21 -10 -15 -10 1943.30 112.31 10 15 11 129.33 28.02 -10 15 -11 92.59 18.20 -10 -15 -11 63.85 16.77 10 15 12 1843.30 114.31 -10 15 -12 1866.67 113.73 -10 -15 -12 1767.16 110.88 10 15 13 111.61 37.95 -10 15 -13 118.60 24.35 -10 -15 -13 89.12 37.15 10 16 -13 654.81 158.61 10 16 -13 668.20 86.45 10 -16 -13 771.31 110.05 10 16 -12 63.37 16.78 10 16 -12 59.30 15.80 10 -16 -12 69.07 14.26 10 16 -11 105.14 35.70 10 16 -11 58.50 19.06 10 -16 -11 69.57 24.95 10 -16 -11 101.50 23.74 10 16 -10 283.30 114.47 10 16 -10 291.44 73.21 10 -16 -10 368.44 94.42 10 16 -9 84.55 29.82 10 16 -9 54.42 14.39 10 -16 -9 53.28 22.56 10 -16 -9 56.21 16.57 10 16 -8 2918.82 137.77 10 16 -8 2632.47 111.15 10 -16 -8 2529.09 147.94 10 -16 -8 2772.24 124.67 10 16 -7 23.29 17.41 10 -16 -7 -4.33 15.30 10 16 -6 1269.90 109.29 -10 16 6 1060.33 89.41 10 16 -6 1009.47 87.52 10 -16 -6 1130.45 101.10 10 16 -5 1355.57 155.05 10 16 -5 1315.08 88.38 10 -16 -5 1411.18 78.29 10 16 -4 151.66 28.82 -10 16 4 137.81 28.05 10 16 -4 76.79 28.74 -10 -16 4 75.89 23.33 10 -16 -4 145.95 35.34 10 16 -3 103.09 18.83 -10 -16 3 32.01 14.33 10 -16 -3 77.26 26.76 10 16 -2 460.43 91.84 -10 16 2 489.11 89.08 -10 -16 2 382.87 72.06 10 16 -1 544.77 85.92 -10 16 1 634.66 51.60 -10 -16 1 444.45 65.36 10 16 0 1920.82 114.43 -10 16 0 1972.36 98.97 -10 -16 0 1985.06 98.51 10 16 1 213.51 60.16 -10 16 -1 240.58 45.20 -10 -16 -1 169.56 49.75 10 16 2 1349.31 95.41 -10 16 -2 1393.93 74.27 -10 -16 -2 1347.03 93.08 10 16 3 227.82 59.05 -10 16 -3 281.66 39.08 -10 -16 -3 197.83 31.56 10 16 4 591.60 134.50 -10 16 -4 933.23 85.09 -10 -16 -4 547.89 153.84 10 16 5 327.35 77.54 -10 16 -5 403.90 54.81 -10 -16 -5 261.05 51.80 10 16 6 130.82 25.40 -10 16 -6 119.90 31.76 -10 -16 -6 120.36 17.09 10 16 7 678.40 137.73 -10 16 -7 840.29 68.34 -10 -16 -7 672.53 98.12 10 16 8 45.82 23.69 -10 16 -8 49.73 16.57 -10 -16 -8 85.52 20.22 10 16 9 104.82 37.50 -10 16 -9 80.20 32.23 -10 -16 -9 78.79 25.03 10 16 10 691.11 112.29 -10 16 -10 744.18 106.60 -10 -16 -10 636.69 107.26 10 16 11 212.62 45.73 -10 16 -11 223.77 62.44 -10 -16 -11 120.05 52.63 10 17 -11 157.03 73.14 10 17 -11 129.17 48.79 10 -17 -11 169.58 39.08 10 17 -10 580.02 82.24 10 17 -10 261.30 85.51 10 -17 -10 358.75 84.32 10 -17 -10 417.55 118.59 10 17 -9 332.62 77.20 10 17 -9 137.03 60.81 10 -17 -9 158.80 57.21 10 -17 -9 213.98 71.51 10 17 -8 657.99 139.55 10 17 -8 760.08 86.03 10 -17 -8 873.71 96.35 10 17 -7 902.83 179.28 10 17 -7 965.45 100.53 10 -17 -7 1016.03 96.40 10 17 -6 293.39 72.64 10 17 -6 192.86 62.89 10 -17 -6 218.53 57.19 10 17 -5 154.30 62.99 10 17 -5 149.97 33.66 10 -17 -5 207.57 64.72 10 17 -4 20.95 10.67 10 -17 -4 36.97 20.57 10 17 -3 533.22 74.78 -10 -17 3 434.62 91.36 10 -17 -3 436.43 102.45 10 17 -2 46.28 9.84 -10 -17 2 28.94 9.34 10 -17 -2 35.47 26.22 10 17 -1 24.09 13.66 -10 17 1 8.71 10.85 -10 -17 1 32.03 9.27 10 17 0 771.57 84.28 -10 -17 0 818.47 64.71 10 17 1 1183.56 106.13 -10 17 -1 1248.34 104.53 -10 -17 -1 991.86 94.12 10 17 2 1913.46 106.83 -10 17 -2 1924.89 104.65 -10 -17 -2 1886.37 103.25 10 17 3 -3.66 15.38 -10 17 -3 29.42 14.31 -10 -17 -3 -2.94 14.85 10 17 4 309.63 78.78 -10 17 -4 329.96 54.26 -10 -17 -4 243.90 62.43 10 17 5 196.03 67.98 -10 17 -5 339.61 27.70 -10 -17 -5 182.17 51.78 10 17 6 13.68 9.00 -10 17 -6 3.46 11.53 -10 -17 -6 17.56 12.17 10 17 7 134.48 33.17 -10 17 -7 186.78 85.01 -10 -17 -7 149.65 44.56 10 17 8 34.43 8.93 -10 17 -8 58.59 17.33 -10 -17 -8 44.22 16.43 10 17 9 628.01 92.35 -10 17 -9 730.28 94.27 -10 -17 -9 449.06 133.55 10 17 10 268.85 89.67 -10 17 -10 262.49 67.44 -10 -17 -10 211.15 85.49 10 18 -10 667.87 158.28 10 18 -10 664.55 80.66 10 -18 -10 619.53 133.38 10 18 -9 1165.76 134.40 10 18 -9 1099.30 98.59 10 -18 -9 1137.66 97.55 10 -18 -9 1268.45 130.88 10 18 -8 61.94 20.63 10 18 -8 77.73 16.31 10 -18 -8 29.70 21.83 10 18 -7 19.84 10.72 10 18 -7 20.82 14.42 10 -18 -7 -5.91 17.17 10 18 -6 143.80 43.07 10 18 -6 100.89 33.81 10 -18 -6 173.99 49.01 10 18 -5 231.82 60.14 10 18 -5 148.37 54.47 10 -18 -5 249.06 59.35 10 18 -4 17.36 16.57 10 18 -4 9.23 8.54 10 -18 -4 35.64 15.64 10 18 -3 724.48 106.84 10 18 -3 643.20 73.91 -10 -18 3 774.91 79.75 10 -18 -3 821.26 87.17 10 18 -2 12.91 11.45 10 18 -2 6.02 6.21 -10 -18 2 -0.31 12.92 10 -18 -2 -13.42 16.50 10 18 -1 465.19 105.92 -10 -18 1 582.78 70.54 10 -18 -1 679.48 78.40 10 18 0 35.95 18.46 -10 18 0 43.74 21.82 -10 -18 0 9.69 11.06 10 18 1 309.23 84.14 -10 18 -1 392.10 57.01 -10 -18 -1 168.33 45.60 10 18 2 834.66 121.53 -10 18 -2 1091.85 101.32 -10 -18 -2 824.13 114.98 10 18 3 2126.24 106.87 -10 18 -3 1997.53 98.52 -10 -18 -3 2009.25 101.78 10 18 4 101.30 43.79 -10 18 -4 120.07 17.09 -10 -18 -4 76.11 22.36 10 18 5 245.12 76.81 -10 18 -5 398.64 66.58 -10 -18 -5 256.34 92.56 10 18 6 76.97 51.24 -10 18 -6 162.54 26.90 -10 -18 -6 129.64 38.07 10 18 7 23.84 10.51 -10 18 -7 15.45 12.05 -10 -18 -7 11.34 9.02 10 18 8 5.73 12.54 -10 18 -8 56.22 14.14 -10 -18 -8 25.14 17.32 10 19 -7 1346.28 131.53 10 19 -7 1143.42 97.08 10 -19 -7 1169.70 135.19 10 19 -6 80.34 29.88 10 19 -6 31.28 18.32 10 -19 -6 52.55 18.72 10 19 -5 160.60 43.82 10 19 -4 118.10 40.34 10 19 -4 106.87 30.22 10 -19 -4 112.01 34.21 10 19 -3 6.05 13.94 10 -19 -3 33.65 15.77 10 19 -2 79.73 32.17 -10 -19 2 52.43 24.72 10 -19 -2 34.21 9.44 10 19 -1 47.31 26.34 -10 -19 1 41.91 12.11 10 -19 -1 58.61 27.01 10 19 0 127.70 40.85 -10 -19 0 121.52 17.33 10 -19 0 104.32 26.31 10 19 1 2581.09 130.94 -10 -19 -1 2665.18 127.86 10 19 2 11.65 11.17 -10 19 -2 40.99 13.19 -10 -19 -2 -0.34 16.17 10 19 3 28.78 14.81 -10 19 -3 12.12 12.49 -10 -19 -3 33.06 15.05 10 19 4 11.63 10.97 -10 19 -4 8.40 10.84 10 19 5 50.36 22.30 -10 19 -5 24.64 12.58 -10 -19 -5 31.43 14.64 10 19 6 342.81 96.18 -10 19 -6 442.70 91.54 10 20 -3 25.51 16.23 10 -20 -3 10.50 10.23 10 20 -2 102.59 46.73 -10 -20 2 82.28 23.70 10 -20 -2 74.68 51.66 10 20 -1 52.89 20.86 -10 -20 1 14.81 12.01 10 -20 -1 13.00 22.77 10 20 0 7.15 12.61 -10 -20 0 16.67 6.42 10 -20 0 29.29 16.31 10 20 1 89.25 30.11 -10 -20 -1 53.32 16.79 10 -20 1 61.71 34.51 11 0 -19 536.72 125.53 11 0 -18 -9.99 17.21 11 0 -17 2898.70 156.23 11 0 -16 -14.08 19.42 11 0 -15 487.29 69.17 11 0 -14 15.80 11.94 11 0 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135.06 11 2 9 7.96 14.13 -11 2 -9 59.80 19.90 11 -2 9 73.24 20.13 -11 -2 -9 64.98 21.33 11 2 10 637.82 96.40 -11 2 -10 611.46 106.14 11 -2 10 600.44 96.73 -11 -2 -10 616.36 117.85 11 2 11 8.56 8.47 -11 2 -11 3.28 8.71 11 -2 11 17.71 6.51 -11 -2 -11 -14.96 18.50 11 2 12 752.49 98.23 -11 2 -12 741.78 101.47 11 -2 12 716.86 28.67 -11 -2 -12 727.85 176.84 11 2 13 13.35 10.76 -11 2 -13 -10.90 15.83 11 -2 13 20.28 7.55 -11 -2 -13 1.15 12.19 11 2 14 2043.36 803.54 -11 2 -14 1997.12 785.55 11 -2 14 1934.73 110.00 -11 -2 -14 1876.90 108.33 11 2 15 210.55 41.91 -11 2 -15 151.85 54.41 11 -2 15 161.45 35.96 -11 -2 -15 168.52 40.82 11 2 16 128.52 40.64 -11 2 -16 132.58 38.32 11 -2 16 135.00 45.90 -11 -2 -16 110.27 45.79 -11 2 -17 53.09 10.64 11 -2 17 24.43 11.22 -11 -2 -17 0.52 11.97 11 3 -19 173.07 56.43 11 -3 -19 201.64 57.38 11 3 -18 -2.98 19.54 11 -3 -18 8.22 10.32 11 3 -17 84.34 31.42 11 -3 -17 147.65 41.32 11 3 -16 218.01 53.97 11 -3 -16 138.92 47.81 11 3 -15 112.12 25.91 11 -3 -15 77.27 26.17 11 3 -14 170.75 45.63 11 -3 -14 161.02 48.88 11 3 -13 196.89 32.50 11 -3 -13 134.55 25.92 11 3 -12 240.25 51.65 11 -3 -12 197.01 55.65 11 3 -11 752.63 102.06 11 -3 -11 669.83 81.27 11 -3 -11 408.36 73.41 -11 3 10 2435.23 86.11 11 3 -10 2393.30 103.56 11 -3 -10 2563.49 984.79 11 3 -9 19.74 13.55 -11 3 9 20.40 6.33 11 -3 -9 46.87 15.71 -11 -3 9 7.05 6.66 -11 3 8 393.64 28.54 11 3 -8 389.69 63.92 11 -3 -8 386.19 87.71 -11 -3 8 402.72 22.53 -11 3 7 142.85 24.17 11 3 -7 152.09 40.36 11 -3 -7 185.70 47.51 -11 -3 7 162.48 27.09 11 3 -6 912.89 36.60 -11 3 6 937.60 24.51 11 -3 -6 990.27 36.32 -11 -3 6 954.03 24.82 -11 3 5 14.41 7.30 11 3 -5 20.21 8.37 11 -3 -5 24.61 9.66 -11 -3 5 14.09 9.45 11 3 -4 1222.50 56.57 -11 3 4 1084.03 45.27 11 -3 -4 1115.10 48.99 -11 -3 4 1131.12 36.84 11 3 -3 438.87 73.32 -11 3 3 472.92 24.39 -11 -3 3 375.83 61.46 11 -3 -3 446.52 53.49 11 3 -2 7675.41 252.65 -11 3 2 7822.62 255.36 -11 -3 2 7407.28 238.84 11 -3 -2 7782.16 257.91 11 3 -1 94.55 22.01 -11 3 1 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385.41 72.94 -11 4 -14 302.75 70.51 11 -4 14 339.04 48.63 -11 -4 -14 275.23 78.75 11 4 15 24.09 12.83 -11 4 -15 37.31 16.99 11 -4 15 58.64 17.67 -11 -4 -15 27.67 16.84 -11 4 -16 250.39 86.88 11 4 16 286.07 81.99 11 -4 16 292.89 64.25 -11 -4 -16 357.57 67.99 -11 4 -17 980.53 85.09 11 4 17 1023.29 89.87 11 -4 17 931.69 90.33 -11 -4 -17 1089.84 95.04 11 5 -18 124.54 51.45 11 5 -17 151.58 45.37 11 -5 -17 136.24 24.62 11 5 -16 12.06 11.40 11 -5 -16 17.91 9.00 11 5 -15 16.52 17.37 11 -5 -15 14.50 13.76 11 5 -14 837.17 106.33 11 -5 -14 788.53 50.05 11 5 -13 298.38 52.69 11 -5 -13 273.15 52.25 11 5 -12 40.26 20.10 11 -5 -12 96.20 16.19 11 -5 -12 19.47 10.66 11 5 -11 3002.22 119.18 11 -5 -11 2763.01 123.62 11 -5 -11 2877.39 119.90 11 5 -10 27.97 21.29 11 -5 -10 83.25 21.16 11 -5 -10 37.02 12.90 -11 5 9 203.27 36.05 11 5 -9 289.88 55.26 11 -5 -9 202.38 41.21 -11 5 8 4.52 6.46 11 5 -8 13.46 14.61 11 -5 -8 6.70 15.92 -11 -5 8 14.53 11.02 -11 5 7 492.44 49.78 11 5 -7 418.41 60.83 11 -5 -7 441.21 52.77 -11 -5 7 443.71 32.18 11 5 -6 49.33 14.25 -11 5 6 46.17 15.41 11 -5 -6 35.36 12.01 -11 -5 6 34.14 8.09 11 5 -5 191.81 28.01 -11 5 5 141.98 29.26 11 -5 -5 130.86 33.52 -11 -5 5 136.04 27.58 11 5 -4 347.53 43.60 -11 5 4 297.24 54.52 11 -5 -4 309.37 47.22 -11 -5 4 295.03 31.77 11 5 -3 1304.74 67.33 -11 5 3 1239.62 39.29 11 -5 -3 1396.23 115.70 -11 -5 3 1266.94 36.35 11 5 -2 1512.02 55.48 -11 5 2 1363.83 41.73 11 -5 -2 1558.69 46.71 -11 -5 2 1563.48 41.97 -11 5 1 1304.10 41.90 11 5 -1 1482.05 136.64 11 -5 -1 1267.96 100.67 -11 -5 1 1257.07 39.13 11 5 0 35.65 14.65 -11 5 0 25.52 8.87 11 -5 0 47.31 9.25 -11 -5 0 28.10 15.35 11 5 1 2782.79 109.90 -11 5 -1 2993.16 126.44 11 -5 1 2852.96 108.80 -11 -5 -1 2833.96 116.13 11 5 2 50.55 14.77 11 -5 2 52.52 16.48 -11 -5 -2 76.51 21.70 -11 5 -3 899.16 270.20 11 5 3 902.24 82.82 11 -5 3 963.17 46.14 -11 -5 -3 949.60 32.50 -11 5 -4 12.46 9.66 11 5 4 33.62 16.93 11 -5 4 12.94 8.98 -11 -5 -4 38.87 11.54 11 5 5 -11.22 18.01 -11 5 -5 55.85 17.60 11 -5 5 12.18 9.11 -11 -5 -5 48.94 16.29 -11 5 -6 629.39 73.00 11 5 6 720.70 73.55 11 -5 6 540.51 67.36 -11 -5 -6 547.78 98.32 -11 5 -7 1402.25 74.80 11 5 7 1496.25 80.17 11 -5 7 1397.74 72.68 -11 -5 -7 1458.22 80.11 -11 5 -8 166.06 18.17 11 5 8 151.23 33.45 11 -5 8 115.25 25.76 -11 -5 -8 43.72 12.07 11 5 9 4709.10 170.51 -11 5 -9 5076.35 178.19 -11 -5 -9 4958.99 201.03 11 5 10 64.20 20.79 -11 5 -10 42.26 15.46 11 -5 10 35.51 16.20 -11 -5 -10 -5.91 18.95 11 5 11 170.38 31.75 -11 5 -11 155.40 35.93 11 -5 11 176.71 32.72 -11 -5 -11 180.01 40.72 11 5 12 18.30 9.44 -11 5 -12 13.67 13.45 11 -5 12 7.18 8.13 -11 -5 -12 15.79 11.88 11 5 13 11.58 8.40 -11 5 -13 48.10 16.84 11 -5 13 8.08 6.26 -11 -5 -13 62.34 20.16 11 5 14 104.08 43.63 -11 5 -14 94.07 26.35 11 -5 14 86.44 30.14 -11 -5 -14 80.90 21.25 -11 5 -15 3576.52 174.77 11 5 15 3834.50 178.07 11 -5 15 3639.74 166.72 -11 -5 -15 3596.54 189.25 -11 5 -16 23.07 20.28 11 5 16 9.69 14.61 11 -5 16 -6.83 12.88 -11 -5 -16 -6.01 19.86 11 6 -18 31.26 26.43 11 -6 -18 34.86 14.26 11 6 -17 455.31 135.19 11 -6 -17 671.72 108.56 11 6 -16 1076.64 117.37 11 -6 -16 983.58 91.78 11 6 -15 174.53 38.48 11 -6 -15 110.65 52.16 11 6 -14 6.80 10.99 11 -6 -14 11.59 16.91 11 6 -13 360.68 48.11 11 -6 -13 282.41 72.14 11 6 -12 -12.36 18.39 11 -6 -12 19.21 13.56 11 -6 -12 16.51 13.23 11 6 -11 928.92 115.80 11 -6 -11 900.26 39.91 11 -6 -11 818.88 41.75 11 6 -10 13.51 14.15 11 -6 -10 -2.16 9.45 11 -6 -10 6.62 6.40 -11 6 9 2956.89 128.22 11 6 -9 2990.63 152.36 11 -6 -9 2770.28 130.47 -11 6 8 26.15 8.87 11 6 -8 35.37 21.06 11 -6 -8 21.01 12.82 -11 6 7 68.51 15.51 11 6 -7 97.80 23.24 11 -6 -7 101.73 21.08 -11 -6 7 87.55 21.17 11 6 -6 75.41 20.81 -11 6 6 34.53 9.20 11 -6 -6 52.83 14.79 -11 -6 6 44.31 13.71 11 6 -5 114.21 18.77 -11 6 5 143.77 26.16 11 -6 -5 165.61 22.08 -11 -6 5 91.23 29.18 11 6 -4 817.95 119.89 -11 6 4 777.69 77.16 11 -6 -4 816.66 54.25 -11 -6 4 781.92 21.75 11 6 -3 1381.30 101.32 -11 6 3 1330.00 110.38 11 -6 -3 1235.40 40.68 -11 -6 3 1195.30 34.39 -11 6 2 140.77 29.38 11 6 -2 96.87 23.81 11 -6 -2 133.68 31.38 -11 -6 2 102.71 29.10 -11 6 1 3767.08 143.56 11 6 -1 3914.52 150.62 11 -6 -1 3743.30 139.71 -11 -6 1 3725.83 158.10 11 6 0 28.59 11.85 -11 6 0 8.29 12.22 11 -6 0 12.05 7.34 -11 -6 0 19.11 11.06 11 6 1 685.80 73.90 -11 6 -1 857.10 30.90 11 -6 1 796.78 37.42 -11 -6 -1 696.87 89.66 -11 6 -2 112.36 24.85 11 6 2 132.21 27.71 11 -6 2 108.81 28.12 -11 -6 -2 108.19 19.92 -11 6 -3 335.36 61.29 11 6 3 245.19 62.64 11 -6 3 246.93 58.38 -11 -6 -3 219.17 45.29 -11 6 -4 145.45 31.53 11 6 4 165.09 29.92 11 -6 4 110.73 30.05 -11 -6 -4 127.23 18.34 11 6 5 2953.43 132.45 -11 6 -5 3092.76 136.77 11 -6 5 3084.69 133.39 -11 -6 -5 2896.96 140.05 -11 6 -6 215.94 30.92 11 6 6 224.37 27.75 11 -6 6 150.04 44.84 -11 -6 -6 222.13 30.12 -11 6 -7 2053.83 82.10 11 6 7 2088.52 89.78 11 -6 7 1828.44 84.07 -11 -6 -7 1957.05 82.34 -11 6 -8 10.52 8.15 11 6 8 19.18 12.76 11 -6 8 22.73 8.83 -11 -6 -8 14.92 11.35 -11 6 -9 382.35 51.65 11 6 9 388.04 73.82 11 -6 9 350.95 63.32 -11 -6 -9 437.20 55.89 11 6 10 434.43 72.76 -11 6 -10 369.09 72.28 -11 -6 -10 481.72 87.17 11 6 11 1358.03 96.13 -11 6 -11 1178.43 155.33 11 -6 11 1263.17 84.89 -11 -6 -11 1343.02 93.14 11 6 12 94.42 26.21 -11 6 -12 95.43 18.45 11 -6 12 81.36 18.70 -11 -6 -12 73.22 25.48 11 6 13 1193.19 99.68 -11 6 -13 1130.99 113.55 11 -6 13 1242.30 107.01 -11 -6 -13 1184.23 107.53 -11 6 -14 299.32 91.44 11 6 14 483.37 93.38 11 -6 14 399.01 76.74 -11 -6 -14 418.38 99.99 -11 6 -15 81.38 22.31 11 6 15 31.12 20.13 11 -6 15 50.02 13.27 -11 -6 -15 38.05 23.42 11 6 16 -1.04 17.10 -11 6 -16 -3.25 17.45 -11 -6 -16 27.10 10.45 11 7 -17 37.61 10.88 11 7 -16 36.51 19.21 11 -7 -16 -4.06 14.76 11 7 -15 351.59 81.18 11 -7 -15 264.43 84.11 11 7 -14 206.43 46.64 11 -7 -14 160.61 45.57 11 7 -13 725.00 73.10 11 -7 -13 652.68 100.96 11 7 -12 2.51 12.63 11 -7 -12 15.21 10.88 11 7 -11 907.66 70.52 11 -7 -11 828.47 79.41 11 -7 -11 897.05 59.63 11 7 -10 1115.80 159.82 11 -7 -10 1092.26 65.21 11 7 -9 97.52 22.05 11 -7 -9 69.46 19.99 11 7 -8 9.49 17.90 -11 7 8 16.23 8.06 11 7 -7 2977.14 133.90 -11 7 7 3425.97 148.11 11 -7 -7 3217.47 139.07 -11 -7 7 3280.20 138.25 11 7 -6 340.98 72.39 -11 7 6 315.97 52.99 11 -7 -6 288.59 37.91 -11 -7 6 203.30 32.31 11 7 -5 1508.05 149.87 -11 7 5 1361.10 54.15 11 -7 -5 1379.32 81.73 -11 -7 5 1397.75 75.36 11 7 -4 325.52 104.08 -11 7 4 223.94 45.41 11 -7 -4 281.95 50.10 -11 -7 4 245.07 56.32 11 7 -3 713.48 75.11 -11 7 3 816.86 28.20 11 -7 -3 838.35 31.40 -11 -7 3 741.97 30.53 -11 7 2 71.04 18.72 11 7 -2 85.92 24.01 11 -7 -2 94.93 19.31 -11 -7 2 67.30 17.15 -11 7 1 569.29 72.14 11 7 -1 595.00 89.29 11 -7 -1 514.22 43.87 -11 -7 1 543.51 71.30 11 7 0 247.21 44.34 -11 7 0 259.19 40.35 11 -7 0 204.39 49.73 -11 -7 0 235.18 40.27 11 7 1 2004.66 170.12 -11 7 -1 2228.62 95.74 11 -7 1 2078.36 88.09 -11 -7 -1 2067.36 88.47 -11 7 -2 4.13 14.35 11 7 2 51.07 18.03 11 -7 2 26.19 12.36 -11 -7 -2 23.95 8.27 -11 7 -3 287.68 66.69 11 7 3 308.97 56.49 11 -7 3 245.32 39.13 -11 -7 -3 280.80 44.80 -11 7 -4 911.13 30.68 11 7 4 909.12 72.79 11 -7 4 925.54 27.47 -11 -7 -4 929.97 52.68 -11 7 -5 2364.10 92.38 11 7 5 2211.39 90.07 11 -7 5 2199.11 81.39 -11 -7 -5 2268.74 87.53 -11 7 -6 152.29 19.40 11 7 6 121.54 27.67 11 -7 6 136.87 60.52 -11 -7 -6 155.40 29.55 -11 7 -7 2380.18 109.46 11 7 7 2471.76 96.52 11 -7 7 2568.23 985.22 -11 -7 -7 2310.71 105.09 -11 7 -8 42.02 16.29 11 7 8 41.34 10.54 11 -7 8 38.61 13.02 -11 -7 -8 28.84 10.91 -11 7 -9 1138.76 149.74 11 7 9 1464.18 63.03 11 -7 9 1367.56 53.44 -11 -7 -9 1292.51 59.54 11 7 10 76.47 18.59 -11 7 -10 69.38 22.58 11 -7 10 87.11 25.75 -11 -7 -10 -4.56 18.68 11 7 11 309.54 71.90 -11 7 -11 303.97 82.29 -11 -7 -11 333.74 48.35 11 7 12 26.00 11.68 -11 7 -12 9.92 8.87 11 -7 12 -0.79 5.87 -11 -7 -12 -1.69 13.53 -11 7 -13 518.39 90.29 11 7 13 574.60 89.95 11 -7 13 471.51 76.05 -11 -7 -13 526.11 102.30 -11 7 -14 28.25 16.40 11 7 14 20.76 9.13 11 -7 14 24.15 12.46 -11 -7 -14 -33.75 16.30 -11 7 -15 2156.05 129.98 11 7 15 1978.31 119.75 11 -7 15 1957.57 114.86 -11 -7 -15 1940.07 120.50 -11 7 -16 570.40 82.23 11 7 16 582.22 97.99 11 -7 16 463.80 100.62 -11 -7 -16 604.24 75.58 11 8 -17 1745.34 148.66 11 -8 -17 1769.17 118.61 11 8 -16 83.18 24.76 11 8 -15 186.28 50.84 11 -8 -15 183.01 62.32 11 8 -14 325.11 65.05 11 8 -13 575.51 55.81 11 -8 -13 498.61 64.55 11 8 -12 276.21 33.28 11 -8 -12 143.83 46.42 11 -8 -12 126.39 41.28 11 8 -11 15.69 14.25 11 -8 -11 17.55 12.08 11 8 -10 166.69 53.24 11 -8 -10 140.36 34.80 11 -8 -10 113.02 32.82 11 8 -9 877.77 70.96 11 -8 -9 924.95 52.33 11 -8 -9 1000.41 50.63 -11 8 8 272.73 55.98 11 8 -8 401.62 65.15 11 -8 -8 257.26 73.73 -11 8 7 84.81 19.76 11 8 -7 54.94 17.24 11 -8 -7 62.87 24.54 11 8 -6 214.96 51.79 -11 8 6 190.29 36.47 11 -8 -6 196.34 87.53 -11 -8 6 137.37 65.43 11 8 -5 5271.64 226.49 -11 8 5 5021.51 211.05 11 -8 -5 4977.16 209.43 -11 -8 5 5010.31 214.43 11 8 -4 450.40 49.26 -11 8 4 384.75 51.41 11 -8 -4 329.79 61.73 -11 -8 4 234.13 47.14 -11 8 3 637.61 97.89 11 8 -3 805.66 90.05 11 -8 -3 685.31 24.98 -11 -8 3 735.30 24.60 -11 8 2 23.94 7.73 11 8 -2 9.72 14.27 11 -8 -2 -4.90 10.38 -11 -8 2 20.48 13.31 11 8 -1 699.13 79.40 -11 8 1 835.37 28.08 11 -8 -1 716.54 35.76 -11 -8 1 766.03 27.23 11 8 0 308.69 63.50 -11 8 0 289.52 57.53 11 -8 0 250.89 51.18 -11 -8 0 309.82 38.68 -11 8 -1 232.45 48.07 11 8 1 246.41 53.28 11 -8 1 236.92 60.35 -11 -8 -1 216.59 46.79 -11 8 -2 123.77 23.83 11 8 2 119.57 29.37 11 -8 2 111.04 31.10 -11 -8 -2 74.00 30.50 -11 8 -3 2257.12 88.89 11 8 3 2142.65 90.62 11 -8 3 2288.76 91.53 -11 -8 -3 2142.27 84.17 -11 8 -4 11.62 7.96 11 8 4 53.37 18.08 11 -8 4 50.72 19.13 -11 -8 -4 36.36 11.49 -11 8 -5 919.82 91.52 11 8 5 1032.66 89.27 11 -8 5 853.19 45.77 -11 -8 -5 881.52 30.68 -11 8 -6 1382.73 59.74 11 8 6 1464.66 138.44 11 -8 6 1217.42 50.12 -11 -8 -6 1305.15 54.31 -11 8 -7 2324.78 103.12 11 8 7 2287.27 104.19 11 -8 7 2213.03 93.43 -11 -8 -7 2058.58 102.26 -11 8 -8 1166.71 39.02 11 8 8 1223.35 471.70 11 -8 8 1168.00 29.23 -11 -8 -8 1051.94 34.21 11 8 9 557.12 67.58 -11 8 -9 449.91 61.24 -11 -8 -9 415.00 102.42 11 8 10 555.39 104.17 -11 8 -10 679.89 33.51 -11 -8 -10 589.51 92.66 11 8 11 165.56 44.42 -11 8 -11 203.06 37.83 11 -8 11 113.27 39.38 -11 -8 -11 169.98 47.75 11 8 12 68.17 20.82 -11 8 -12 92.28 15.89 11 -8 12 69.57 14.33 -11 -8 -12 66.64 17.45 -11 8 -13 700.25 73.75 11 8 13 630.01 91.19 11 -8 13 693.19 71.44 -11 -8 -13 670.14 113.28 -11 8 -14 219.10 51.65 11 8 14 266.03 50.89 11 -8 14 195.79 54.62 -11 -8 -14 140.49 78.40 -11 8 -15 1741.80 115.30 11 8 15 2057.59 125.62 11 -8 15 1761.15 104.08 -11 -8 -15 1737.11 113.36 11 9 -16 -4.95 21.70 11 9 -15 2294.22 116.30 11 -9 -15 2081.15 101.50 11 9 -14 36.40 13.02 11 -9 -14 6.18 9.79 11 9 -13 70.60 21.55 11 -9 -13 16.68 4.63 11 9 -12 123.23 19.32 11 -9 -12 106.94 30.83 11 -9 -12 72.13 22.73 11 9 -11 124.04 22.55 11 -9 -11 66.81 21.77 11 9 -10 456.32 108.97 11 9 -9 17.84 12.67 11 -9 -9 21.76 13.10 11 9 -8 586.16 47.74 11 -9 -8 584.87 27.98 -11 9 7 3344.80 118.10 11 9 -7 3339.72 129.70 11 -9 -7 3213.17 137.65 11 9 -6 706.85 75.31 -11 9 6 564.29 70.04 11 -9 -6 530.83 32.91 -11 -9 6 556.69 20.13 11 9 -5 341.33 69.61 -11 9 5 376.32 44.14 11 -9 -5 257.00 70.62 -11 -9 5 230.78 62.79 11 9 -4 631.53 127.55 -11 9 4 858.18 93.80 11 -9 -4 795.63 26.47 -11 -9 4 770.16 26.19 -11 9 3 1614.35 83.95 11 9 -3 1601.68 86.78 11 -9 -3 1428.23 84.73 -11 -9 3 1561.47 80.61 -11 9 2 349.92 48.39 11 9 -2 392.79 62.61 11 -9 -2 279.90 64.88 -11 -9 2 389.82 69.34 11 9 -1 319.41 61.44 -11 9 1 256.08 42.01 11 -9 -1 183.25 46.68 -11 -9 1 230.54 47.11 11 9 0 344.96 58.52 -11 9 0 277.97 118.69 11 -9 0 275.16 43.44 -11 -9 0 280.74 43.56 -11 9 -1 323.19 54.91 11 9 1 322.99 47.66 11 -9 1 285.44 61.10 -11 -9 -1 300.60 42.21 -11 9 -2 18.25 10.77 11 9 2 53.73 21.67 11 -9 2 8.45 8.79 -11 -9 -2 9.66 9.96 -11 9 -3 842.03 31.57 11 9 3 784.96 78.33 11 -9 3 836.37 24.63 -11 -9 -3 830.76 31.33 -11 9 -4 47.71 17.69 11 9 4 30.96 19.67 11 -9 4 57.86 13.23 -11 -9 -4 25.72 7.28 -11 9 -5 4186.22 149.66 11 9 5 3613.00 132.72 11 -9 5 3697.25 130.06 -11 -9 -5 3756.29 134.00 -11 9 -6 3009.77 112.96 11 9 6 3150.74 122.81 11 -9 6 2935.33 120.43 -11 -9 -6 2946.08 125.66 -11 9 -7 148.49 42.02 11 9 7 126.66 39.47 11 -9 7 169.38 34.34 -11 -9 -7 173.99 71.57 -11 9 -8 93.04 19.17 11 9 8 100.48 23.76 11 -9 8 82.54 22.07 -11 -9 -8 72.93 19.26 -11 9 -9 61.46 17.72 11 9 9 28.20 15.66 11 -9 9 37.18 13.86 -11 -9 -9 68.43 26.90 11 9 10 43.47 25.61 -11 9 -10 75.12 23.59 11 -9 10 46.86 22.34 -11 -9 -10 39.16 14.29 -11 9 -11 1762.20 98.80 11 9 11 1676.84 167.42 11 -9 11 1643.71 86.88 -11 -9 -11 1760.63 105.86 -11 9 -12 -1.76 20.29 11 9 12 71.05 12.87 11 -9 12 -8.05 9.32 11 9 13 1038.93 96.98 -11 9 -13 1133.32 105.53 -11 -9 -13 894.20 148.34 11 9 14 151.37 42.76 -11 9 -14 125.36 29.71 -11 -9 -14 208.85 32.31 11 9 15 70.68 28.98 -11 9 -15 85.87 21.18 -11 -9 -15 99.23 26.81 11 10 -16 887.76 196.58 11 -10 -16 1138.43 98.18 11 10 -15 -14.56 18.62 11 10 -14 66.70 24.62 11 -10 -14 41.71 15.53 11 10 -13 1934.80 99.66 11 -10 -13 1664.75 92.80 11 10 -12 175.22 48.18 11 -10 -12 97.37 37.85 11 -10 -12 80.31 26.75 11 10 -11 30.41 18.38 11 10 -10 22.16 14.47 11 -10 -10 1.28 8.19 11 10 -9 31.45 22.84 11 -10 -9 18.00 14.57 11 10 -8 647.61 105.48 11 -10 -8 508.52 82.40 11 10 -7 262.03 46.25 -11 10 7 217.79 49.79 11 -10 -7 261.40 37.41 11 10 -6 -7.67 13.44 -11 10 6 12.10 11.42 11 -10 -6 12.61 9.02 -11 -10 6 11.40 6.34 11 10 -5 4718.03 170.58 -11 10 5 4487.50 155.61 11 -10 -5 4121.67 142.21 -11 -10 5 4309.44 148.03 -11 10 4 2010.09 107.86 11 10 -4 2212.03 110.16 11 -10 -4 1988.95 84.96 -11 -10 4 1908.96 92.59 11 10 -3 76.47 24.16 -11 10 3 31.63 15.67 -11 -10 3 24.43 12.38 11 10 -2 165.18 34.12 -11 10 2 203.88 34.51 -11 -10 2 149.60 33.18 11 10 -1 96.45 32.09 -11 10 1 112.27 25.34 11 -10 -1 99.46 26.95 -11 -10 1 96.96 15.94 -11 10 0 36.75 10.52 11 10 0 1.45 12.40 11 -10 0 6.86 7.24 -11 -10 0 -1.51 11.44 -11 10 -1 1517.71 78.53 11 10 1 1688.72 89.78 11 -10 1 1587.98 85.37 -11 -10 -1 1691.47 88.37 -11 10 -2 176.20 26.50 11 10 2 198.59 27.96 11 -10 2 127.49 38.84 -11 -10 -2 174.59 71.20 -11 10 -3 1350.23 59.02 11 10 3 1260.35 59.37 11 -10 3 1145.55 25.88 -11 -10 -3 1208.05 35.89 -11 10 -4 1649.19 64.98 11 10 4 1623.93 118.68 11 -10 4 1503.96 59.14 -11 -10 -4 1635.20 64.41 -11 10 -5 56.47 16.79 11 10 5 41.17 18.62 11 -10 5 17.68 8.01 -11 -10 -5 28.32 14.33 -11 10 -6 72.71 17.18 11 10 6 121.23 21.70 11 -10 6 90.09 23.21 -11 -10 -6 93.28 26.26 11 10 7 918.82 84.11 -11 10 -7 901.78 56.40 -11 -10 -7 962.98 52.81 11 10 8 954.04 54.01 -11 10 -8 972.47 199.48 -11 -10 -8 905.36 49.38 11 10 9 983.07 200.76 -11 10 -9 1055.30 74.49 -11 -10 -9 958.73 52.59 11 10 10 36.96 12.97 -11 10 -10 100.41 25.33 -11 -10 -10 56.26 20.81 11 10 11 341.95 80.82 -11 10 -11 354.63 62.70 -11 -10 -11 232.55 76.99 11 10 12 8.79 12.45 -11 10 -12 13.33 14.83 -11 -10 -12 7.80 17.31 11 10 13 1160.75 154.28 -11 10 -13 1299.92 103.56 -11 -10 -13 1264.07 108.40 11 10 14 -16.18 16.88 -11 10 -14 18.33 10.90 -11 -10 -14 25.44 14.65 11 11 -15 1434.92 143.20 11 11 -14 949.35 151.56 11 -11 -14 865.08 108.90 11 11 -13 172.81 47.51 11 -11 -13 114.25 42.20 11 -11 -13 87.09 36.40 11 11 -12 126.49 30.79 11 -11 -12 79.74 29.00 11 -11 -12 119.06 22.95 11 11 -11 179.26 46.61 11 -11 -11 97.91 33.30 11 11 -10 73.87 45.95 11 -11 -10 113.51 31.15 11 11 -9 296.25 72.70 11 -11 -9 188.57 54.31 11 11 -8 27.71 18.49 11 -11 -8 18.50 13.03 11 11 -7 192.51 46.09 11 -11 -7 149.87 47.64 11 11 -6 3354.91 126.02 -11 11 6 3339.28 126.43 11 11 -5 465.33 86.70 -11 11 5 566.15 57.80 11 -11 -5 384.43 60.92 -11 -11 5 572.09 23.28 11 11 -4 38.34 19.23 -11 11 4 40.48 20.05 -11 -11 4 45.45 14.46 -11 11 3 1709.90 657.94 11 11 -3 1785.96 87.70 11 -11 -3 1451.59 70.75 -11 -11 3 1541.13 62.67 -11 11 2 388.17 65.97 11 11 -2 404.36 75.34 11 -11 -2 225.42 48.94 -11 -11 2 258.75 51.69 -11 11 1 33.13 13.99 11 11 -1 65.85 13.61 11 -11 -1 50.95 17.26 -11 -11 1 52.10 14.28 -11 11 0 163.60 30.30 11 11 0 186.82 28.59 11 -11 0 125.72 36.51 -11 -11 0 136.43 31.01 -11 11 -1 117.27 24.66 11 11 1 77.40 30.69 11 -11 1 69.65 19.51 -11 -11 -1 45.82 14.09 11 11 2 280.65 56.27 -11 11 -2 282.18 59.21 -11 -11 -2 317.98 133.54 11 11 3 960.34 96.47 -11 11 -3 791.08 81.58 -11 -11 -3 910.26 32.74 11 11 4 45.20 14.86 -11 11 -4 17.88 17.43 -11 -11 -4 40.96 20.06 11 11 5 655.83 94.15 -11 11 -5 808.93 44.80 -11 -11 -5 735.29 46.76 11 11 6 2684.56 116.96 -11 11 -6 2676.83 114.00 -11 -11 -6 2514.02 107.79 11 11 7 574.51 63.43 -11 11 -7 491.53 66.30 -11 -11 -7 426.95 96.38 11 11 8 124.40 39.84 -11 11 -8 117.97 25.13 -11 -11 -8 96.79 41.66 11 11 9 437.34 120.15 -11 11 -9 551.61 29.73 -11 -11 -9 372.42 98.92 11 11 10 69.35 26.11 -11 11 -10 76.66 19.49 -11 -11 -10 54.50 17.11 11 11 11 2048.18 102.14 -11 11 -11 1976.92 103.10 -11 -11 -11 2111.57 108.68 11 11 12 107.30 41.12 -11 11 -12 74.68 38.55 -11 -11 -12 46.15 27.71 11 11 13 892.84 79.51 -11 11 -13 889.05 65.89 -11 -11 -13 552.26 145.34 11 12 -14 231.11 51.01 11 12 -13 1241.17 108.26 11 -12 -13 977.23 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225.24 55.09 -11 13 3 295.86 56.85 11 13 -2 199.38 53.43 -11 13 2 309.93 55.47 -11 -13 2 113.79 42.08 11 13 -1 25.87 14.92 -11 13 1 72.82 15.66 -11 -13 1 21.40 10.15 11 13 0 772.08 99.09 -11 13 0 976.65 219.49 -11 -13 0 869.23 48.65 11 13 1 565.97 145.04 -11 13 -1 790.53 83.64 -11 -13 -1 603.68 38.89 11 13 2 1644.75 106.41 -11 13 -2 1749.71 91.91 -11 -13 -2 1626.86 85.69 11 13 3 23.40 13.43 -11 13 -3 31.22 9.77 -11 -13 -3 18.05 8.81 11 13 4 14.11 13.11 -11 13 -4 1.76 16.27 -11 -13 -4 4.87 12.08 11 13 5 33.09 10.93 -11 -13 -5 45.73 16.83 11 13 6 201.38 57.11 -11 13 -6 242.96 46.58 -11 -13 -6 145.25 50.56 11 13 7 17.68 9.98 -11 13 -7 44.27 10.14 -11 -13 -7 6.57 11.49 11 13 8 78.85 35.11 -11 13 -8 96.58 18.66 -11 -13 -8 100.27 41.01 11 13 9 454.35 128.14 -11 13 -9 377.64 93.84 -11 -13 -9 242.34 110.40 11 13 10 1404.01 89.00 -11 13 -10 1411.18 124.27 -11 -13 -10 1499.75 94.46 11 13 11 26.47 7.34 -11 13 -11 10.44 10.91 -11 -13 -11 19.85 13.22 11 14 -12 189.21 53.34 11 14 -11 228.35 71.36 11 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208.75 86.72 11 14 7 80.47 15.75 -11 14 -7 112.22 24.09 -11 -14 -7 67.68 16.35 11 14 8 14.23 20.84 -11 14 -8 10.47 14.00 -11 -14 -8 36.12 16.35 11 14 9 19.36 15.13 -11 14 -9 72.33 22.68 -11 -14 -9 15.66 13.26 11 14 10 20.91 8.81 -11 14 -10 21.62 10.90 -11 -14 -10 -0.73 11.07 11 15 -10 240.12 83.04 11 -15 -10 240.52 56.99 11 15 -9 1938.39 122.73 11 15 -8 97.24 28.08 11 -15 -8 11.83 15.78 11 -15 -7 125.19 43.88 11 15 -6 41.04 12.59 11 -15 -6 30.23 11.65 11 15 -5 -15.06 18.35 11 -15 -5 27.66 10.26 11 15 -4 291.23 84.37 11 -15 -4 201.55 96.78 11 15 -3 6.44 19.18 -11 15 3 23.76 11.02 -11 -15 3 17.04 6.00 11 15 -2 26.30 12.70 -11 15 2 12.81 12.22 -11 -15 2 2.33 4.88 11 15 -1 298.63 69.60 -11 15 1 425.08 79.14 -11 -15 1 187.99 65.61 11 15 0 11.89 15.42 -11 15 0 16.42 13.02 -11 -15 0 -3.98 11.50 11 15 1 648.75 84.72 -11 15 -1 729.54 128.28 -11 -15 -1 717.78 60.09 11 15 2 211.37 79.10 -11 15 -2 285.39 47.36 -11 -15 -2 193.72 54.07 11 15 3 1385.96 86.96 -11 15 -3 1465.11 87.50 -11 -15 -3 1355.89 78.83 11 15 4 -5.23 17.62 -11 15 -4 31.10 15.59 -11 -15 -4 6.72 11.29 11 15 5 138.73 39.86 -11 15 -5 108.94 26.27 -11 -15 -5 84.49 31.30 11 15 6 265.86 59.39 -11 15 -6 254.44 67.84 -11 -15 -6 193.09 64.39 11 15 7 342.64 70.72 -11 15 -7 266.00 81.32 -11 -15 -7 246.17 74.67 11 15 8 80.80 53.78 -11 15 -8 126.25 38.36 -11 -15 -8 112.63 34.10 11 15 9 48.50 15.93 -11 15 -9 41.43 20.92 -11 -15 -9 14.42 18.53 11 16 -8 15.20 20.33 11 -16 -8 12.10 9.11 11 16 -7 614.64 102.36 11 -16 -7 555.32 96.78 11 16 -6 27.42 11.01 11 -16 -6 57.78 17.25 11 16 -5 -1.61 18.24 11 -16 -5 24.16 15.02 11 16 -4 346.90 100.23 11 -16 -4 297.83 70.77 11 16 -3 267.28 86.82 11 16 -2 250.98 45.78 -11 16 2 160.39 54.82 -11 -16 2 71.07 34.41 11 16 -1 207.40 47.40 -11 16 1 223.35 62.35 11 16 0 48.20 22.61 -11 16 0 94.02 14.47 -11 -16 0 32.14 6.50 11 16 1 1899.62 826.67 -11 16 -1 2011.80 100.51 -11 -16 -1 1968.64 98.49 11 16 2 167.77 39.94 -11 16 -2 172.52 28.01 -11 -16 -2 116.23 45.00 11 16 3 88.27 26.46 -11 16 -3 95.76 23.91 -11 -16 -3 53.56 24.36 11 16 4 92.72 26.83 -11 16 -4 88.77 11.65 -11 -16 -4 32.73 20.20 11 16 5 123.04 42.32 -11 16 -5 116.67 15.52 -11 -16 -5 127.89 33.97 11 16 6 14.66 20.95 -11 16 -6 38.94 16.21 11 16 7 23.39 20.15 -11 16 -7 6.50 10.36 -11 -16 -7 4.12 9.75 11 17 -6 264.54 110.04 11 -17 -6 241.67 77.39 11 17 -5 76.99 40.58 11 -17 -5 114.04 41.02 11 17 -4 0.85 20.92 11 -17 -4 41.04 25.22 11 17 -3 78.54 38.90 11 17 -2 10.67 10.09 11 17 -1 27.31 10.86 -11 17 1 17.63 9.59 -11 -17 1 12.61 8.84 11 17 0 707.56 87.91 -11 17 0 785.20 99.09 -11 -17 0 441.41 131.09 11 17 1 33.00 10.45 -11 17 -1 34.77 7.62 -11 -17 -1 15.03 11.75 11 17 2 141.78 44.87 -11 17 -2 244.90 48.00 -11 -17 -2 155.94 46.17 11 17 3 316.00 81.86 -11 17 -3 423.93 89.60 -11 -17 -3 294.98 86.70 11 17 4 10.29 10.44 -11 17 -4 5.88 10.13 -11 -17 -4 -13.27 15.93 12 0 -15 16.06 11.73 12 0 -14 32.28 15.45 12 0 -13 16.58 13.89 12 0 -12 108.40 25.28 12 0 -11 13.85 8.83 12 0 -10 942.08 51.81 12 0 -9 -20.52 15.21 12 0 -8 71.08 19.91 12 0 -7 11.36 10.74 12 0 -6 902.52 49.48 -12 0 6 754.81 23.82 12 0 -5 5.24 11.74 -12 0 5 -0.59 8.15 12 0 -4 35.12 10.38 -12 0 4 34.02 6.92 12 0 -3 8.84 21.58 -12 0 3 -3.07 11.01 12 0 -2 4348.02 189.41 -12 0 2 4305.17 184.60 12 0 -1 6.90 7.33 -12 0 1 6.61 8.70 12 0 0 1788.47 686.86 -12 0 0 1717.33 86.99 12 0 1 -8.61 13.15 -12 0 -1 10.64 10.91 12 0 2 122.76 32.87 -12 0 -2 102.49 30.15 12 0 3 11.95 11.61 -12 0 -3 12.18 10.62 12 0 4 266.72 55.05 -12 0 -4 282.42 55.28 12 0 5 13.03 13.61 -12 0 -5 6.06 14.41 12 0 6 216.58 45.30 -12 0 -6 212.06 44.01 12 0 7 18.44 6.61 -12 0 -7 -10.55 17.23 12 0 8 2328.01 99.30 -12 0 -8 2272.75 461.64 12 0 9 26.68 6.67 -12 0 -9 -15.96 18.69 12 0 10 894.77 78.65 -12 0 -10 950.09 147.32 12 0 11 13.48 10.82 -12 0 -11 11.94 13.02 12 0 12 8.04 12.25 -12 0 -12 25.43 15.70 12 0 13 33.54 15.58 -12 0 -13 9.63 12.90 12 0 14 909.45 77.97 -12 0 -14 883.83 91.49 12 1 -16 141.08 60.58 12 -1 -16 188.40 66.65 12 1 -15 63.91 23.65 12 -1 -15 72.37 26.16 12 1 -14 40.14 16.14 12 -1 -14 64.71 27.04 12 1 -13 67.58 24.18 12 -1 -13 103.00 22.56 12 1 -12 751.33 114.44 12 -1 -12 710.75 109.69 12 1 -11 364.07 81.20 12 -1 -11 365.97 152.23 12 1 -10 219.59 75.02 12 -1 -10 191.56 67.53 12 1 -9 106.41 34.97 12 -1 -9 101.40 34.40 12 1 -8 95.96 26.77 -12 1 8 65.27 23.00 12 -1 -8 101.09 37.06 12 1 -7 162.58 45.03 12 -1 -7 120.58 36.59 -12 -1 7 98.29 32.43 12 1 -6 268.49 44.78 -12 1 6 208.08 44.95 12 -1 -6 243.62 51.52 -12 -1 6 212.67 54.18 12 1 -5 91.68 30.10 -12 1 5 87.61 22.62 12 -1 -5 130.64 25.04 -12 -1 5 107.28 28.48 12 1 -4 92.86 35.79 -12 1 4 94.92 28.13 -12 -1 4 124.28 26.95 12 -1 -4 180.68 27.79 12 1 -3 707.81 103.81 -12 1 3 718.36 64.53 -12 -1 3 612.21 22.39 12 -1 -3 634.15 100.59 12 1 -2 742.97 107.40 12 -1 -2 741.71 80.40 -12 -1 2 676.89 31.95 12 1 -1 1076.13 46.13 -12 1 1 1175.28 34.31 -12 -1 1 1217.22 34.95 12 -1 -1 1127.19 118.60 12 1 0 1437.86 80.60 -12 1 0 1445.10 77.63 -12 -1 0 1327.67 43.53 12 -1 0 1422.46 94.00 12 1 1 108.03 39.58 -12 1 -1 130.80 28.36 -12 -1 -1 129.89 30.55 12 -1 1 142.65 29.64 12 1 2 123.08 32.29 -12 1 -2 147.75 31.31 -12 -1 -2 163.73 22.56 12 -1 2 161.55 32.12 12 1 3 31.91 19.63 -12 1 -3 25.34 6.97 -12 -1 -3 15.92 12.55 12 -1 3 12.19 12.94 12 1 4 8.98 11.96 -12 1 -4 12.60 15.10 -12 -1 -4 27.12 7.99 12 -1 4 14.62 6.77 12 1 5 326.34 53.99 -12 1 -5 291.50 61.28 -12 -1 -5 288.80 57.92 12 -1 5 319.48 134.96 12 1 6 55.78 16.59 -12 1 -6 29.95 18.53 12 -1 6 64.98 18.54 12 1 7 246.51 67.75 -12 1 -7 216.64 56.06 -12 -1 -7 193.03 41.95 12 -1 7 204.64 55.25 12 1 8 567.01 25.78 -12 1 -8 501.85 85.13 -12 -1 -8 572.94 35.81 12 -1 8 469.20 88.64 12 1 9 -4.58 11.70 -12 1 -9 21.53 11.84 12 -1 9 4.78 11.54 -12 -1 -9 19.53 8.77 12 1 10 1986.11 106.26 -12 1 -10 1997.03 785.79 12 -1 10 1911.44 108.72 -12 -1 -10 1980.23 118.61 12 1 11 168.48 42.48 -12 1 -11 130.84 34.88 12 -1 11 142.39 45.34 -12 -1 -11 181.01 39.95 12 1 12 758.52 122.10 -12 1 -12 872.63 87.75 12 -1 12 809.82 86.21 -12 -1 -12 803.69 85.18 12 1 13 470.00 73.28 -12 1 -13 271.05 100.05 12 -1 13 416.31 111.97 -12 -1 -13 484.54 82.88 12 1 14 42.83 15.00 -12 1 -14 55.14 15.45 12 -1 14 35.92 13.08 -12 -1 -14 50.99 20.13 12 2 -16 34.97 19.88 12 -2 -16 -3.77 16.82 12 2 -15 270.85 91.21 12 -2 -15 303.39 90.96 12 2 -14 -15.13 15.53 12 -2 -14 24.74 7.95 12 2 -13 1258.64 80.02 12 -2 -13 1115.84 103.67 12 2 -12 -5.76 15.35 12 -2 -12 -6.75 14.43 12 2 -11 1736.37 99.97 12 -2 -11 1717.05 95.14 12 2 -10 50.12 20.91 12 -2 -10 61.07 21.79 12 2 -9 201.47 72.10 12 -2 -9 185.44 55.18 12 2 -8 229.36 37.63 12 -2 -8 215.04 38.35 12 2 -7 526.38 42.77 -12 2 7 462.22 18.87 12 -2 -7 508.10 61.96 -12 -2 7 409.90 29.69 12 2 -6 380.69 74.10 -12 2 6 227.23 49.88 12 -2 -6 254.44 49.72 12 2 -5 827.47 39.85 -12 2 5 791.59 23.76 12 -2 -5 953.34 95.43 -12 -2 5 845.35 34.40 12 2 -4 46.88 12.92 -12 2 4 28.65 10.34 -12 -2 4 42.45 14.08 12 -2 -4 129.91 26.94 12 2 -3 657.63 72.38 -12 2 3 432.62 76.89 -12 -2 3 622.84 63.54 12 -2 -3 674.79 95.90 12 2 -2 387.02 58.47 -12 2 2 475.27 43.23 12 -2 -2 463.96 80.42 -12 -2 2 315.29 62.18 12 2 -1 402.74 57.65 -12 2 1 441.77 61.53 -12 -2 1 368.57 158.73 12 -2 -1 374.73 62.99 12 2 0 298.11 53.22 -12 2 0 329.74 65.52 -12 -2 0 275.13 48.93 12 -2 0 220.56 65.61 12 2 1 1035.71 113.61 -12 2 -1 1052.16 104.31 -12 -2 -1 922.42 52.36 12 -2 1 1035.23 68.49 12 2 2 76.14 15.65 -12 2 -2 96.10 15.44 -12 -2 -2 72.70 20.67 12 -2 2 53.53 18.60 12 2 3 807.56 40.71 -12 2 -3 744.12 75.12 -12 -2 -3 799.84 54.01 12 -2 3 842.39 39.29 12 2 4 362.20 74.46 -12 2 -4 288.11 54.27 -12 -2 -4 293.51 57.43 12 -2 4 348.42 45.69 12 2 5 202.57 39.85 -12 2 -5 173.77 34.77 -12 -2 -5 131.59 63.68 12 -2 5 210.37 45.79 12 2 6 25.38 13.82 -12 2 -6 15.06 11.60 12 -2 6 20.24 11.92 -12 -2 -6 16.91 9.65 -12 2 -7 285.71 59.26 12 2 7 297.89 71.07 12 -2 7 247.24 73.12 -12 -2 -7 299.07 68.25 -12 2 -8 400.28 92.67 12 2 8 541.24 85.11 12 -2 8 480.82 84.33 -12 -2 -8 458.43 94.00 12 2 9 2473.09 105.77 -12 2 -9 2428.13 105.42 12 -2 9 2426.33 102.31 -12 -2 -9 2592.33 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5 7 50.98 27.96 13 -5 7 49.58 17.25 -13 -5 -7 18.00 11.01 -13 5 -8 209.07 87.67 13 5 8 292.86 91.34 13 -5 8 258.50 76.34 -13 -5 -8 241.10 75.00 13 5 9 22.11 9.44 -13 5 -9 43.22 12.76 13 6 -10 292.16 114.93 13 -6 -10 174.82 72.82 13 6 -9 426.28 92.63 13 6 -8 38.78 16.62 13 -6 -8 46.59 21.35 13 6 -7 474.39 128.63 -13 6 7 626.81 90.97 13 -6 -7 530.92 75.50 13 6 -6 264.96 86.70 13 -6 -6 209.63 46.92 13 6 -5 447.62 106.83 -13 6 5 429.80 74.53 13 -6 -5 449.31 69.14 -13 6 4 98.00 22.51 13 6 -4 133.60 20.72 13 -6 -4 126.81 38.17 -13 6 3 200.27 57.50 13 6 -3 263.92 56.83 13 -6 -3 160.78 42.57 -13 -6 3 157.65 51.46 13 6 -2 982.98 94.58 -13 6 2 1003.42 93.20 13 -6 -2 953.39 88.36 -13 -6 2 831.35 76.38 13 6 -1 41.52 14.41 13 -6 -1 35.22 18.47 -13 -6 1 53.65 12.45 13 6 0 163.47 33.86 -13 6 0 99.25 27.18 -13 -6 0 97.97 32.59 13 6 1 30.77 10.62 -13 6 -1 16.91 10.75 -13 -6 -1 -4.95 14.20 -13 6 -2 13.24 11.08 13 6 2 -0.73 11.99 13 -6 2 20.07 9.60 -13 -6 -2 21.58 9.08 -13 6 -3 1362.41 82.39 13 6 3 1386.96 81.81 13 -6 3 1390.99 79.15 -13 -6 -3 1336.79 81.26 13 6 4 32.18 15.00 -13 6 -4 32.80 14.58 13 -6 4 32.66 11.08 -13 -6 -4 13.85 8.73 -13 6 -5 1209.82 112.61 13 6 5 996.52 128.61 13 -6 5 972.60 98.16 -13 -6 -5 1234.43 74.18 -13 6 -6 95.50 36.00 13 6 6 114.66 36.56 13 -6 6 97.46 32.11 -13 -6 -6 105.96 36.69 -13 6 -7 33.30 12.57 13 6 7 32.95 17.54 13 -6 7 19.42 11.49 -13 -6 -7 49.19 17.49 -13 6 -8 235.15 68.73 13 6 8 252.75 66.87 13 -6 8 196.48 60.80 -13 -6 -8 196.15 72.20 13 7 -9 62.51 22.64 13 7 -8 27.19 16.54 13 -7 -8 18.16 11.26 13 7 -7 263.09 92.18 -13 7 7 320.93 71.51 13 -7 -7 388.61 66.81 13 7 -6 11.10 10.31 -13 7 6 18.56 7.74 13 -7 -6 -2.10 8.14 13 7 -5 1187.79 185.97 -13 7 5 1390.97 78.68 13 -7 -5 1229.15 537.36 -13 7 4 65.94 22.63 13 7 -4 125.18 31.96 13 -7 -4 57.76 32.16 13 7 -3 201.27 46.41 -13 7 3 186.40 56.50 13 -7 -3 158.05 52.75 13 7 -2 18.20 11.97 -13 7 2 39.88 12.98 13 -7 -2 29.23 12.90 -13 -7 2 23.42 7.19 13 7 -1 248.33 60.04 -13 7 1 263.53 76.42 13 -7 -1 209.98 69.05 -13 7 0 1264.82 74.19 13 7 0 1150.34 114.45 13 -7 0 1273.74 83.89 -13 -7 0 1189.82 111.38 -13 7 -1 1408.15 99.57 13 7 1 1566.46 99.63 13 -7 1 1529.09 93.19 -13 -7 -1 1519.61 86.67 -13 7 -2 126.12 32.53 13 7 2 123.30 37.80 13 -7 2 100.97 39.95 -13 -7 -2 81.21 27.34 -13 7 -3 134.11 50.27 13 7 3 149.06 29.59 13 -7 3 75.85 34.65 -13 -7 -3 113.29 35.91 -13 7 -4 1019.89 97.06 13 7 4 857.47 128.76 13 -7 4 882.10 80.66 -13 -7 -4 875.12 81.96 -13 7 -5 51.91 14.62 13 7 5 36.32 16.72 13 -7 5 17.95 11.91 -13 -7 -5 28.34 20.27 13 7 6 45.84 22.20 -13 7 -6 41.48 16.94 -13 -7 -6 32.13 15.19 13 7 7 186.22 73.98 -13 7 -7 185.45 59.85 -13 -7 -7 125.74 36.83 13 8 -8 238.35 49.52 13 -8 -8 127.04 47.53 13 8 -7 139.99 22.45 -13 8 7 82.33 20.57 13 8 -6 732.61 151.37 -13 8 6 950.85 80.02 13 -8 -6 818.25 102.55 -13 8 5 61.23 16.01 13 8 -5 33.41 18.04 13 -8 -5 28.48 14.78 -13 8 4 249.89 48.76 13 8 -4 248.30 81.89 13 -8 -4 150.16 48.62 13 8 -3 581.93 142.40 13 8 -2 50.33 23.12 -13 8 2 28.32 12.47 -13 -8 2 16.67 8.02 13 8 -1 2069.65 117.49 -13 8 1 1910.01 830.44 13 8 0 521.02 79.28 -13 8 0 353.67 83.02 -13 -8 0 317.57 70.93 13 8 1 300.52 164.27 -13 8 -1 198.38 75.20 -13 -8 -1 270.45 80.13 13 8 2 67.88 14.59 -13 8 -2 29.56 13.87 -13 -8 -2 29.04 8.83 13 8 3 243.95 76.51 -13 8 -3 156.20 58.77 -13 -8 -3 127.19 47.55 13 8 4 102.16 35.61 -13 8 -4 103.99 37.63 13 8 5 14.60 12.01 -13 8 -5 24.84 17.73 13 8 6 130.76 61.06 -13 8 -6 165.30 49.79 -13 -8 -6 100.96 41.86 13 9 -7 32.06 20.89 13 9 -6 203.24 51.27 -13 9 6 98.39 26.74 13 9 -5 21.11 18.15 -13 9 5 20.11 10.10 13 9 -4 329.43 109.12 -13 9 4 367.97 73.48 13 9 -3 288.55 54.40 -13 9 3 327.52 57.78 13 9 -2 41.80 18.63 13 9 -1 1303.73 87.97 -13 9 1 1374.85 87.09 -13 -9 1 1073.51 115.98 13 9 0 85.17 15.21 -13 9 0 91.05 19.74 -13 -9 0 50.60 16.14 13 9 1 913.00 108.16 -13 9 -1 992.64 98.64 -13 -9 -1 1196.81 99.52 13 9 2 220.57 70.84 -13 9 -2 134.71 43.60 13 9 3 59.05 18.61 -13 9 -3 22.63 18.58 -13 -9 -3 18.28 14.94 13 9 4 478.72 147.25 -13 9 -4 739.41 93.89 -13 -9 -4 345.63 113.17 13 9 5 13.05 12.18 -13 9 -5 6.90 13.12 -13 -9 -5 24.04 13.21 13 10 -5 40.23 14.43 -13 10 5 -4.67 10.88 13 10 -4 1019.40 121.55 -13 10 4 974.17 141.31 13 10 -3 23.27 10.28 -13 10 3 23.11 13.02 13 10 -2 445.45 132.51 -13 10 2 576.12 117.60 13 10 -1 720.63 152.04 -13 10 1 970.01 84.55 13 10 0 89.89 30.29 -13 10 0 84.35 29.09 -13 -10 0 102.99 24.77 13 10 1 1111.98 96.17 -13 10 -1 1042.84 99.92 -13 -10 -1 952.22 94.19 13 10 2 298.76 76.71 -13 10 -2 242.40 71.25 -13 -10 -2 214.41 69.01 13 10 3 -19.09 17.41 -13 10 -3 19.72 8.33 -13 -10 -3 -2.28 14.58 14 0 -3 3.03 9.78 14 0 -2 51.06 17.95 -14 0 2 49.42 11.04 14 0 -1 43.18 18.54 -14 0 1 -0.74 11.78 14 0 0 128.81 42.18 -14 0 0 101.36 36.99 14 0 1 -6.06 16.07 -14 0 -1 3.64 15.06 14 1 -3 11.35 13.66 -14 1 3 7.53 7.84 14 -1 -3 18.10 13.65 14 1 -2 246.26 78.91 -14 1 2 182.07 61.01 -14 -1 2 161.42 50.82 14 -1 -2 185.87 76.77 -14 1 1 40.13 13.17 -14 -1 1 6.01 8.53 14 -1 -1 23.70 11.98 14 1 0 22.22 12.72 -14 1 0 31.41 15.08 -14 -1 0 36.97 13.19 14 1 1 -3.30 16.95 -14 1 -1 19.80 10.30 -14 -1 -1 17.20 9.44 14 -1 1 5.78 10.92 14 2 -2 221.56 68.22 -14 2 2 184.75 62.92 -14 -2 2 153.93 49.97 14 -2 -2 210.83 51.80 14 2 -1 16.46 19.24 -14 2 1 30.04 19.27 14 -2 -1 38.50 18.33 14 2 0 1225.81 103.36 -14 2 0 1067.01 88.89 -14 -2 0 1100.59 90.76 14 -2 0 1010.59 85.98 ; _shelx_hkl_checksum 8119 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 +X,+Y,+Z 2 1/2-X,1/2+Y,1/2-Z 3 -X,-Y,-Z 4 -1/2+X,-1/2-Y,-1/2+Z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pd1 Pd 1.08441(3) 0.34714(2) 0.48005(2) 0.03188(10) Uani 1 1 d . . . . . Pd2 Pd 1.07048(3) 0.37266(2) 0.28340(2) 0.04022(11) Uani 1 1 d . . . . . Pd3 Pd 0.75754(3) 0.25373(2) 0.36938(2) 0.02496(9) Uani 1 1 d . . . . . Pd4 Pd 0.97266(3) 0.32031(2) 0.37665(2) 0.02494(9) Uani 1 1 d . . . . . Si1 Si 1.14663(10) 0.38090(5) 0.38460(5) 0.0280(2) Uani 1 1 d . . . . . Si2 Si 0.87993(10) 0.29843(5) 0.28888(4) 0.0251(2) Uani 1 1 d . . . . . Si3 Si 0.89677(10) 0.27737(5) 0.45803(5) 0.0260(2) Uani 1 1 d . . . . . N1 N 1.2643(3) 0.40595(18) 0.57413(17) 0.0367(8) Uani 1 1 d . . . . . N2 N 1.2512(4) 0.4418(2) 0.20325(17) 0.0410(9) Uani 1 1 d . . . . . N3 N 0.5613(3) 0.21551(17) 0.27061(15) 0.0313(7) Uani 1 1 d . . . . . N4 N 0.5904(4) 0.1868(2) 0.45846(17) 0.0388(9) Uani 1 1 d . . . . . C1 C 1.1964(4) 0.3839(2) 0.54121(19) 0.0371(10) Uani 1 1 d . . . . . C2 C 1.3567(4) 0.4352(2) 0.6120(2) 0.0378(10) Uani 1 1 d . . . . . C3 C 1.4753(5) 0.4003(3) 0.6076(3) 0.0605(16) Uani 1 1 d . . . . . H3A H 1.5012 0.4007 0.5670 0.073 Uiso 1 1 calc R U . . . H3B H 1.4625 0.3584 0.6201 0.073 Uiso 1 1 calc R U . . . H3C H 1.5397 0.4191 0.6329 0.073 Uiso 1 1 calc R U . . . C4 C 1.3670(6) 0.5002(3) 0.5925(3) 0.0607(16) Uani 1 1 d . . . . . H4A H 1.2865 0.5202 0.5953 0.073 Uiso 1 1 calc R U . . . H4B H 1.3928 0.5015 0.5519 0.073 Uiso 1 1 calc R U . . . H4C H 1.4284 0.5213 0.6177 0.073 Uiso 1 1 calc R U . . . C5 C 1.3108(5) 0.4322(3) 0.6742(2) 0.0478(12) Uani 1 1 d . . . . . H5A H 1.3008 0.3898 0.6857 0.057 Uiso 1 1 calc R U . . . H5B H 1.2311 0.4531 0.6758 0.057 Uiso 1 1 calc R U . . . H5C H 1.3711 0.4519 0.7010 0.057 Uiso 1 1 calc R U . . . C6 C 1.1821(5) 0.4173(3) 0.2315(2) 0.0452(12) Uani 1 1 d . . . . . C7 C 1.3455(4) 0.4732(2) 0.1715(2) 0.0375(10) Uani 1 1 d . . . . . C8 C 1.4327(6) 0.5030(3) 0.2170(3) 0.0649(18) Uani 1 1 d . . . . . H8A H 1.4701 0.4718 0.2425 0.078 Uiso 1 1 calc R U . . . H8B H 1.3862 0.5315 0.2406 0.078 Uiso 1 1 calc R U . . . H8C H 1.4980 0.5248 0.1971 0.078 Uiso 1 1 calc R U . . . C9 C 1.4125(6) 0.4268(3) 0.1353(3) 0.0607(15) Uani 1 1 d . . . . . H9A H 1.3534 0.4072 0.1078 0.073 Uiso 1 1 calc R U . . . H9B H 1.4506 0.3961 0.1612 0.073 Uiso 1 1 calc R U . . . H9C H 1.4769 0.4470 0.1134 0.073 Uiso 1 1 calc R U . . . C10 C 1.2828(6) 0.5200(3) 0.1327(3) 0.0574(14) Uani 1 1 d . . . . . H10A H 1.2387 0.5490 0.1569 0.069 Uiso 1 1 calc R U . . . H10B H 1.2238 0.5000 0.1055 0.069 Uiso 1 1 calc R U . . . H10C H 1.3450 0.5416 0.1106 0.069 Uiso 1 1 calc R U . . . C11 C 0.6409(4) 0.23184(19) 0.30199(17) 0.0283(8) Uani 1 1 d . . . . . C12 C 0.4588(4) 0.1966(2) 0.23119(19) 0.0340(9) Uani 1 1 d . . . . . C13 C 0.5142(5) 0.1652(3) 0.1790(2) 0.0485(12) Uani 1 1 d . . . . . H13A H 0.5412 0.1243 0.1903 0.058 Uiso 1 1 calc R U . . . H13B H 0.5854 0.1885 0.1661 0.058 Uiso 1 1 calc R U . . . H13C H 0.4518 0.1625 0.1469 0.058 Uiso 1 1 calc R U . . . C14 C 0.3880(5) 0.2531(3) 0.2112(2) 0.0466(12) Uani 1 1 d . . . . . H14A H 0.4434 0.2801 0.1904 0.056 Uiso 1 1 calc R U . . . H14B H 0.3568 0.2741 0.2454 0.056 Uiso 1 1 calc R U . . . H14C H 0.3184 0.2414 0.1850 0.056 Uiso 1 1 calc R U . . . C15 C 0.3769(5) 0.1541(3) 0.2650(3) 0.0489(12) Uani 1 1 d . . . . . H15A H 0.4275 0.1216 0.2826 0.059 Uiso 1 1 calc R U . . . H15B H 0.3137 0.1366 0.2383 0.059 Uiso 1 1 calc R U . . . H15C H 0.3368 0.1768 0.2959 0.059 Uiso 1 1 calc R U . . . C16 C 0.6572(4) 0.2139(2) 0.43111(18) 0.0330(9) Uani 1 1 d . . . . . C17 C 0.5060(5) 0.1501(3) 0.4923(2) 0.0448(12) Uani 1 1 d . . . . . C18 C 0.4323(7) 0.1109(4) 0.4480(3) 0.079(2) Uani 1 1 d . . . . . H18A H 0.4894 0.0857 0.4263 0.095 Uiso 1 1 calc R U . . . H18B H 0.3853 0.1371 0.4207 0.095 Uiso 1 1 calc R U . . . H18C H 0.3751 0.0848 0.4688 0.095 Uiso 1 1 calc R U . . . C19 C 0.4202(5) 0.1927(3) 0.5240(2) 0.0525(14) Uani 1 1 d . . . . . H19A H 0.3826 0.1711 0.5562 0.063 Uiso 1 1 calc R U . . . H19B H 0.3551 0.2072 0.4965 0.063 Uiso 1 1 calc R U . . . H19C H 0.4678 0.2273 0.5395 0.063 Uiso 1 1 calc R U . . . C20 C 0.5843(7) 0.1134(4) 0.5353(4) 0.077(2) Uani 1 1 d . . . . . H20A H 0.6319 0.1408 0.5613 0.093 Uiso 1 1 calc R U . . . H20B H 0.6412 0.0877 0.5140 0.093 Uiso 1 1 calc R U . . . H20C H 0.5307 0.0879 0.5586 0.093 Uiso 1 1 calc R U . . . C21 C 1.3134(4) 0.3531(2) 0.3779(2) 0.0358(9) Uani 1 1 d . . . . . H21 H 1.3447 0.3702 0.3408 0.043 Uiso 1 1 calc R U . . . C22 C 1.3147(5) 0.2841(2) 0.3721(2) 0.0464(12) Uani 1 1 d . . . . . H22A H 1.2906 0.2657 0.4090 0.056 Uiso 1 1 calc R U . . . H22B H 1.3981 0.2705 0.3631 0.056 Uiso 1 1 calc R U . . . H22C H 1.2563 0.2717 0.3406 0.056 Uiso 1 1 calc R U . . . C23 C 1.4036(5) 0.3724(3) 0.4273(3) 0.0512(13) Uani 1 1 d . . . . . H23A H 1.4873 0.3592 0.4184 0.061 Uiso 1 1 calc R U . . . H23B H 1.3793 0.3537 0.4640 0.061 Uiso 1 1 calc R U . . . H23C H 1.4021 0.4165 0.4313 0.061 Uiso 1 1 calc R U . . . C24 C 1.1519(4) 0.4673(2) 0.3996(2) 0.0371(9) Uani 1 1 d . . . . . H24 H 1.1977 0.4727 0.4381 0.045 Uiso 1 1 calc R U . . . C25 C 1.2219(5) 0.5038(2) 0.3549(3) 0.0484(12) Uani 1 1 d . . . . . H25A H 1.2286 0.5460 0.3678 0.058 Uiso 1 1 calc R U . . . H25B H 1.1772 0.5020 0.3168 0.058 Uiso 1 1 calc R U . . . H25C H 1.3049 0.4868 0.3512 0.058 Uiso 1 1 calc R U . . . C26 C 1.0224(5) 0.4931(2) 0.4070(3) 0.0546(14) Uani 1 1 d . . . . . H26A H 0.9857 0.4745 0.4412 0.065 Uiso 1 1 calc R U . . . H26B H 0.9707 0.4842 0.3719 0.065 Uiso 1 1 calc R U . . . H26C H 1.0277 0.5370 0.4126 0.065 Uiso 1 1 calc R U . . . C27 C 0.9335(4) 0.2356(2) 0.23814(19) 0.0337(9) Uani 1 1 d . . . . . H27 H 0.8587 0.2182 0.2173 0.040 Uiso 1 1 calc R U . . . C28 C 0.9978(5) 0.1844(2) 0.2728(2) 0.0447(11) Uani 1 1 d . . . . . H28A H 1.0725 0.2001 0.2930 0.054 Uiso 1 1 calc R U . . . H28B H 1.0203 0.1520 0.2460 0.054 Uiso 1 1 calc R U . . . H28C H 0.9415 0.1684 0.3017 0.054 Uiso 1 1 calc R U . . . C29 C 1.0200(6) 0.2602(3) 0.1919(2) 0.0522(14) Uani 1 1 d . . . . . H29A H 1.0421 0.2274 0.1653 0.063 Uiso 1 1 calc R U . . . H29B H 1.0951 0.2764 0.2113 0.063 Uiso 1 1 calc R U . . . H29C H 0.9778 0.2925 0.1695 0.063 Uiso 1 1 calc R U . . . C30 C 0.7910(4) 0.3554(2) 0.2406(2) 0.0367(10) Uani 1 1 d . . . . . H30 H 0.8560 0.3804 0.2221 0.044 Uiso 1 1 calc R U . . . C31 C 0.7205(7) 0.3989(3) 0.2763(3) 0.0679(18) Uani 1 1 d . . . . . H31A H 0.6477 0.3786 0.2914 0.081 Uiso 1 1 calc R U . . . H31B H 0.6940 0.4333 0.2518 0.081 Uiso 1 1 calc R U . . . H31C H 0.7734 0.4134 0.3091 0.081 Uiso 1 1 calc R U . . . C32 C 0.7120(6) 0.3297(3) 0.1892(3) 0.0592(16) Uani 1 1 d . . . . . H32A H 0.6854 0.3627 0.1630 0.071 Uiso 1 1 calc R U . . . H32B H 0.6392 0.3093 0.2042 0.071 Uiso 1 1 calc R U . . . H32C H 0.7611 0.3005 0.1676 0.071 Uiso 1 1 calc R U . . . C33 C 0.9588(4) 0.2028(2) 0.49051(18) 0.0329(9) Uani 1 1 d . . . . . H33 H 0.8873 0.1750 0.4960 0.039 Uiso 1 1 calc R U . . . C34 C 1.0469(5) 0.1728(2) 0.4481(2) 0.0435(11) Uani 1 1 d . . . . . H34A H 1.0737 0.1335 0.4638 0.052 Uiso 1 1 calc R U . . . H34B H 1.1192 0.1989 0.4433 0.052 Uiso 1 1 calc R U . . . H34C H 1.0039 0.1670 0.4100 0.052 Uiso 1 1 calc R U . . . C35 C 1.0273(5) 0.2115(2) 0.5501(2) 0.0431(11) Uani 1 1 d . . . . . H35A H 1.0966 0.2395 0.5457 0.052 Uiso 1 1 calc R U . . . H35B H 1.0588 0.1724 0.5643 0.052 Uiso 1 1 calc R U . . . H35C H 0.9702 0.2282 0.5782 0.052 Uiso 1 1 calc R U . . . C36 C 0.8187(4) 0.3210(2) 0.51913(18) 0.0317(9) Uani 1 1 d . . . . . H36 H 0.8874 0.3334 0.5470 0.038 Uiso 1 1 calc R U . . . C37 C 0.7628(4) 0.3800(2) 0.4959(2) 0.0393(10) Uani 1 1 d . . . . . H37A H 0.7409 0.4058 0.5288 0.047 Uiso 1 1 calc R U . . . H37B H 0.6884 0.3711 0.4716 0.047 Uiso 1 1 calc R U . . . H37C H 0.8232 0.4010 0.4723 0.047 Uiso 1 1 calc R U . . . C38 C 0.7269(5) 0.2874(2) 0.5561(2) 0.0422(11) Uani 1 1 d . . . . . H38A H 0.7596 0.2471 0.5660 0.051 Uiso 1 1 calc R U . . . H38B H 0.6480 0.2832 0.5339 0.051 Uiso 1 1 calc R U . . . H38C H 0.7138 0.3102 0.5921 0.051 Uiso 1 1 calc R U . . . C39 C 0.7199(10) 0.5209(5) 0.0845(5) 0.047(2) Uiso 0.5 1 d . . P . . C40 C 0.7284(10) 0.5698(5) 0.1230(5) 0.047(2) Uiso 0.5 1 d . . P . . C41 C 0.8062(11) 0.5670(5) 0.1715(5) 0.050(2) Uiso 0.5 1 d . . P . . C42 C 0.8842(12) 0.5173(6) 0.1833(6) 0.055(3) Uiso 0.5 1 d . . P . . C43 C 0.8749(13) 0.4710(7) 0.1412(6) 0.066(3) Uiso 0.5 1 d . . P . . C44 C 0.8008(9) 0.4701(4) 0.1045(4) 0.0386(19) Uiso 0.5 1 d . . P . . C45 C 0.6436(13) 0.5247(6) 0.0383(6) 0.064(3) Uiso 0.5 1 d . . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pd1 0.02821(18) 0.0446(2) 0.02250(16) -0.00255(12) -0.00339(12) -0.01021(13) Pd2 0.0398(2) 0.0565(2) 0.02411(17) 0.00626(14) -0.00301(14) -0.02397(16) Pd3 0.02163(16) 0.03306(17) 0.02005(15) -0.00019(10) -0.00122(11) -0.00557(11) Pd4 0.02231(16) 0.03282(17) 0.01951(15) -0.00014(10) -0.00139(11) -0.00602(11) Si1 0.0223(5) 0.0329(6) 0.0286(5) -0.0007(4) -0.0013(4) -0.0056(4) Si2 0.0238(5) 0.0316(5) 0.0196(5) 0.0001(4) -0.0017(4) -0.0030(4) Si3 0.0239(5) 0.0348(6) 0.0193(5) 0.0005(4) -0.0011(4) -0.0026(4) N1 0.0303(18) 0.043(2) 0.036(2) -0.0041(16) -0.0073(15) -0.0028(16) N2 0.039(2) 0.050(2) 0.0336(19) 0.0070(17) 0.0002(16) -0.0159(18) N3 0.0290(17) 0.0389(19) 0.0256(16) -0.0007(14) -0.0032(14) -0.0068(14) N4 0.0321(19) 0.055(2) 0.0292(18) 0.0011(16) 0.0041(15) -0.0143(17) C1 0.033(2) 0.050(3) 0.028(2) -0.0049(18) -0.0033(17) -0.0095(19) C2 0.032(2) 0.036(2) 0.044(3) -0.0079(19) -0.0133(19) -0.0033(17) C3 0.034(3) 0.080(4) 0.066(4) -0.016(3) -0.011(2) 0.008(3) C4 0.067(4) 0.048(3) 0.067(4) 0.009(3) -0.007(3) -0.018(3) C5 0.056(3) 0.048(3) 0.039(3) -0.006(2) -0.014(2) -0.006(2) C6 0.048(3) 0.063(3) 0.025(2) 0.007(2) -0.0035(19) -0.026(2) C7 0.033(2) 0.039(2) 0.040(2) 0.0093(19) 0.0076(18) -0.0065(18) C8 0.052(3) 0.081(4) 0.061(4) 0.008(3) -0.005(3) -0.033(3) C9 0.059(4) 0.056(3) 0.069(4) 0.006(3) 0.021(3) 0.009(3) C10 0.062(4) 0.055(3) 0.056(3) 0.020(3) 0.007(3) 0.007(3) C11 0.0280(19) 0.0332(19) 0.0236(18) 0.0017(15) 0.0003(15) -0.0029(16) C12 0.027(2) 0.046(2) 0.028(2) -0.0065(18) -0.0069(16) -0.0048(18) C13 0.045(3) 0.067(3) 0.033(2) -0.015(2) -0.004(2) 0.001(2) C14 0.039(3) 0.062(3) 0.038(3) 0.001(2) -0.010(2) 0.003(2) C15 0.035(2) 0.056(3) 0.055(3) -0.004(2) -0.005(2) -0.012(2) C16 0.027(2) 0.048(2) 0.0230(18) 0.0005(17) -0.0020(15) -0.0075(18) C17 0.041(3) 0.057(3) 0.037(2) 0.005(2) 0.011(2) -0.019(2) C18 0.080(5) 0.094(5) 0.065(4) -0.022(4) 0.030(4) -0.054(4) C19 0.044(3) 0.077(4) 0.037(3) 0.001(2) 0.012(2) -0.016(3) C20 0.059(4) 0.092(5) 0.082(5) 0.046(4) 0.018(4) 0.002(4) C21 0.024(2) 0.047(2) 0.036(2) 0.0022(18) 0.0026(17) -0.0037(17) C22 0.036(2) 0.053(3) 0.051(3) -0.008(2) 0.003(2) 0.009(2) C23 0.025(2) 0.071(4) 0.056(3) -0.005(3) -0.006(2) -0.005(2) C24 0.038(2) 0.035(2) 0.038(2) -0.0026(18) -0.0035(18) -0.0070(18) C25 0.049(3) 0.043(3) 0.054(3) 0.006(2) 0.005(2) -0.015(2) C26 0.050(3) 0.037(3) 0.077(4) -0.001(3) 0.011(3) 0.002(2) C27 0.034(2) 0.041(2) 0.027(2) -0.0089(17) 0.0033(16) -0.0056(18) C28 0.045(3) 0.043(3) 0.047(3) -0.013(2) 0.002(2) 0.006(2) C29 0.062(3) 0.058(3) 0.039(3) -0.012(2) 0.027(3) -0.009(3) C30 0.033(2) 0.041(2) 0.036(2) 0.0086(18) -0.0077(18) -0.0053(18) C31 0.066(4) 0.064(4) 0.074(4) 0.011(3) -0.004(3) 0.032(3) C32 0.055(3) 0.068(4) 0.052(3) 0.024(3) -0.026(3) -0.018(3) C33 0.030(2) 0.041(2) 0.0268(19) 0.0048(17) -0.0020(16) -0.0043(17) C34 0.046(3) 0.042(2) 0.042(3) 0.008(2) -0.001(2) 0.009(2) C35 0.048(3) 0.049(3) 0.032(2) 0.0071(19) -0.011(2) 0.000(2) C36 0.026(2) 0.046(2) 0.0221(18) -0.0044(16) -0.0012(15) -0.0063(17) C37 0.034(2) 0.042(2) 0.042(2) -0.0027(19) 0.0027(19) 0.0039(18) C38 0.042(3) 0.056(3) 0.030(2) -0.002(2) 0.0110(19) -0.006(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; H H 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Table 6.1.1.4) ; N N 0.0061 0.0033 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; Pd Pd -0.9988 1.0072 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; Si Si 0.0817 0.0704 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C1 Pd1 Si1 108.99(14) . . C1 Pd1 Si3 146.51(14) . . Si1 Pd1 Si3 104.50(4) . . C1 Pd1 Pd4 162.37(14) . . Si1 Pd1 Pd4 53.52(3) . . Si3 Pd1 Pd4 51.03(2) . . C6 Pd2 Si1 109.81(14) . . C6 Pd2 Si2 146.07(14) . . Si1 Pd2 Si2 103.80(4) . . C6 Pd2 Pd4 163.14(13) . . Si1 Pd2 Pd4 53.49(3) . . Si2 Pd2 Pd4 50.35(2) . . C11 Pd3 C16 95.32(16) . . C11 Pd3 Si2 82.28(12) . . C16 Pd3 Si2 176.83(13) . . C11 Pd3 Si3 176.62(12) . . C16 Pd3 Si3 81.33(12) . . Si2 Pd3 Si3 101.05(4) . . C11 Pd3 Pd4 132.74(11) . . C16 Pd3 Pd4 131.87(12) . . Si2 Pd3 Pd4 50.67(2) . . Si3 Pd3 Pd4 50.63(3) . . Si2 Pd4 Si3 118.44(4) . . Si2 Pd4 Si1 121.76(4) . . Si3 Pd4 Si1 119.73(4) . . Si2 Pd4 Pd2 63.97(3) . . Si3 Pd4 Pd2 177.56(3) . . Si1 Pd4 Pd2 57.85(3) . . Si2 Pd4 Pd1 179.32(3) . . Si3 Pd4 Pd1 62.24(3) . . Si1 Pd4 Pd1 57.56(3) . . Pd2 Pd4 Pd1 115.354(15) . . Si2 Pd4 Pd3 59.09(3) . . Si3 Pd4 Pd3 59.70(3) . . Si1 Pd4 Pd3 176.68(3) . . Pd2 Pd4 Pd3 122.739(14) . . Pd1 Pd4 Pd3 121.577(14) . . C21 Si1 C24 107.9(2) . . C21 Si1 Pd4 125.09(15) . . C24 Si1 Pd4 127.02(15) . . C21 Si1 Pd1 105.48(15) . . C24 Si1 Pd1 98.64(15) . . Pd4 Si1 Pd1 68.92(3) . . C21 Si1 Pd2 100.75(15) . . C24 Si1 Pd2 104.40(15) . . Pd4 Si1 Pd2 68.66(3) . . Pd1 Si1 Pd2 137.49(5) . . C30 Si2 C27 106.6(2) . . C30 Si2 Pd4 124.66(16) . . C27 Si2 Pd4 123.97(15) . . C30 Si2 Pd3 114.49(15) . . C27 Si2 Pd3 109.84(15) . . Pd4 Si2 Pd3 70.24(3) . . C30 Si2 Pd2 86.62(14) . . C27 Si2 Pd2 99.62(14) . . Pd4 Si2 Pd2 65.69(3) . . Pd3 Si2 Pd2 135.49(4) . . C33 Si3 C36 107.83(19) . . C33 Si3 Pd4 122.98(14) . . C36 Si3 Pd4 124.74(15) . . C33 Si3 Pd3 108.80(14) . . C36 Si3 Pd3 114.91(13) . . Pd4 Si3 Pd3 69.67(3) . . C33 Si3 Pd1 100.09(14) . . C36 Si3 Pd1 85.57(13) . . Pd4 Si3 Pd1 66.73(3) . . Pd3 Si3 Pd1 135.90(5) . . C1 N1 C2 175.4(5) . . C6 N2 C7 175.4(5) . . C11 N3 C12 178.3(5) . . C16 N4 C17 177.8(5) . . N1 C1 Pd1 176.6(4) . . N1 C2 C3 107.7(4) . . N1 C2 C4 107.7(4) . . C3 C2 C4 113.3(5) . . N1 C2 C5 107.3(4) . . C3 C2 C5 110.4(5) . . C4 C2 C5 110.2(5) . . C2 C3 H3A 109.5 . . C2 C3 H3B 109.5 . . H3A C3 H3B 109.5 . . C2 C3 H3C 109.5 . . H3A C3 H3C 109.5 . . H3B C3 H3C 109.5 . . C2 C4 H4A 109.5 . . C2 C4 H4B 109.5 . . H4A C4 H4B 109.5 . . C2 C4 H4C 109.5 . . H4A C4 H4C 109.5 . . H4B C4 H4C 109.5 . . C2 C5 H5A 109.5 . . C2 C5 H5B 109.5 . . H5A C5 H5B 109.5 . . C2 C5 H5C 109.5 . . H5A C5 H5C 109.5 . . H5B C5 H5C 109.5 . . N2 C6 Pd2 176.6(5) . . N2 C7 C10 108.2(4) . . N2 C7 C9 108.0(4) . . C10 C7 C9 110.8(5) . . N2 C7 C8 107.1(4) . . C10 C7 C8 111.0(5) . . C9 C7 C8 111.5(5) . . C7 C8 H8A 109.5 . . C7 C8 H8B 109.5 . . H8A C8 H8B 109.5 . . C7 C8 H8C 109.5 . . H8A C8 H8C 109.5 . . H8B C8 H8C 109.5 . . C7 C9 H9A 109.5 . . C7 C9 H9B 109.5 . . H9A C9 H9B 109.5 . . C7 C9 H9C 109.5 . . H9A C9 H9C 109.5 . . H9B C9 H9C 109.5 . . C7 C10 H10A 109.5 . . C7 C10 H10B 109.5 . . H10A C10 H10B 109.5 . . C7 C10 H10C 109.5 . . H10A C10 H10C 109.5 . . H10B C10 H10C 109.5 . . N3 C11 Pd3 168.3(4) . . N3 C12 C15 107.8(4) . . N3 C12 C13 107.5(4) . . C15 C12 C13 111.8(4) . . N3 C12 C14 108.1(4) . . C15 C12 C14 111.2(4) . . C13 C12 C14 110.2(4) . . C12 C13 H13A 109.5 . . C12 C13 H13B 109.5 . . H13A C13 H13B 109.5 . . C12 C13 H13C 109.5 . . H13A C13 H13C 109.5 . . H13B C13 H13C 109.5 . . C12 C14 H14A 109.5 . . C12 C14 H14B 109.5 . . H14A C14 H14B 109.5 . . C12 C14 H14C 109.5 . . H14A C14 H14C 109.5 . . H14B C14 H14C 109.5 . . C12 C15 H15A 109.5 . . C12 C15 H15B 109.5 . . H15A C15 H15B 109.5 . . C12 C15 H15C 109.5 . . H15A C15 H15C 109.5 . . H15B C15 H15C 109.5 . . N4 C16 Pd3 168.8(4) . . N4 C17 C20 107.2(5) . . N4 C17 C19 108.1(4) . . C20 C17 C19 111.1(5) . . N4 C17 C18 106.4(4) . . C20 C17 C18 113.2(6) . . C19 C17 C18 110.6(5) . . C17 C18 H18A 109.5 . . C17 C18 H18B 109.5 . . H18A C18 H18B 109.5 . . C17 C18 H18C 109.5 . . H18A C18 H18C 109.5 . . H18B C18 H18C 109.5 . . C17 C19 H19A 109.5 . . C17 C19 H19B 109.5 . . H19A C19 H19B 109.5 . . C17 C19 H19C 109.5 . . H19A C19 H19C 109.5 . . H19B C19 H19C 109.5 . . C17 C20 H20A 109.5 . . C17 C20 H20B 109.5 . . H20A C20 H20B 109.5 . . C17 C20 H20C 109.5 . . H20A C20 H20C 109.5 . . H20B C20 H20C 109.5 . . C23 C21 C22 109.5(4) . . C23 C21 Si1 115.5(4) . . C22 C21 Si1 109.7(3) . . C23 C21 H21 107.3 . . C22 C21 H21 107.3 . . Si1 C21 H21 107.3 . . C21 C22 H22A 109.5 . . C21 C22 H22B 109.5 . . H22A C22 H22B 109.5 . . C21 C22 H22C 109.5 . . H22A C22 H22C 109.5 . . H22B C22 H22C 109.5 . . C21 C23 H23A 109.5 . . C21 C23 H23B 109.5 . . H23A C23 H23B 109.5 . . C21 C23 H23C 109.5 . . H23A C23 H23C 109.5 . . H23B C23 H23C 109.5 . . C25 C24 C26 110.9(4) . . C25 C24 Si1 114.4(4) . . C26 C24 Si1 111.4(3) . . C25 C24 H24 106.5 . . C26 C24 H24 106.5 . . Si1 C24 H24 106.5 . . C24 C25 H25A 109.5 . . C24 C25 H25B 109.5 . . H25A C25 H25B 109.5 . . C24 C25 H25C 109.5 . . H25A C25 H25C 109.5 . . H25B C25 H25C 109.5 . . C24 C26 H26A 109.5 . . C24 C26 H26B 109.5 . . H26A C26 H26B 109.5 . . C24 C26 H26C 109.5 . . H26A C26 H26C 109.5 . . H26B C26 H26C 109.5 . . C28 C27 C29 109.9(4) . . C28 C27 Si2 111.3(3) . . C29 C27 Si2 111.5(3) . . C28 C27 H27 108.0 . . C29 C27 H27 108.0 . . Si2 C27 H27 108.0 . . C27 C28 H28A 109.5 . . C27 C28 H28B 109.5 . . H28A C28 H28B 109.5 . . C27 C28 H28C 109.5 . . H28A C28 H28C 109.5 . . H28B C28 H28C 109.5 . . C27 C29 H29A 109.5 . . C27 C29 H29B 109.5 . . H29A C29 H29B 109.5 . . C27 C29 H29C 109.5 . . H29A C29 H29C 109.5 . . H29B C29 H29C 109.5 . . C31 C30 C32 112.1(5) . . C31 C30 Si2 111.5(4) . . C32 C30 Si2 116.8(4) . . C31 C30 H30 105.1 . . C32 C30 H30 105.1 . . Si2 C30 H30 105.1 . . C30 C31 H31A 109.5 . . C30 C31 H31B 109.5 . . H31A C31 H31B 109.5 . . C30 C31 H31C 109.5 . . H31A C31 H31C 109.5 . . H31B C31 H31C 109.5 . . C30 C32 H32A 109.5 . . C30 C32 H32B 109.5 . . H32A C32 H32B 109.5 . . C30 C32 H32C 109.5 . . H32A C32 H32C 109.5 . . H32B C32 H32C 109.5 . . C34 C33 C35 108.9(4) . . C34 C33 Si3 110.0(3) . . C35 C33 Si3 112.7(3) . . C34 C33 H33 108.4 . . C35 C33 H33 108.4 . . Si3 C33 H33 108.4 . . C33 C34 H34A 109.5 . . C33 C34 H34B 109.5 . . H34A C34 H34B 109.5 . . C33 C34 H34C 109.5 . . H34A C34 H34C 109.5 . . H34B C34 H34C 109.5 . . C33 C35 H35A 109.5 . . C33 C35 H35B 109.5 . . H35A C35 H35B 109.5 . . C33 C35 H35C 109.5 . . H35A C35 H35C 109.5 . . H35B C35 H35C 109.5 . . C38 C36 C37 110.6(4) . . C38 C36 Si3 118.3(3) . . C37 C36 Si3 110.8(3) . . C38 C36 H36 105.4 . . C37 C36 H36 105.4 . . Si3 C36 H36 105.4 . . C36 C37 H37A 109.5 . . C36 C37 H37B 109.5 . . H37A C37 H37B 109.5 . . C36 C37 H37C 109.5 . . H37A C37 H37C 109.5 . . H37B C37 H37C 109.5 . . C36 C38 H38A 109.5 . . C36 C38 H38B 109.5 . . H38A C38 H38B 109.5 . . C36 C38 H38C 109.5 . . H38A C38 H38C 109.5 . . H38B C38 H38C 109.5 . . C45 C39 C40 118.7(11) . . C45 C39 C44 129.8(11) . . C40 C39 C44 111.5(9) . . C41 C40 C39 120.1(10) . . C40 C41 C42 122.6(11) . . C43 C42 C41 114.1(12) . . C44 C43 C42 123.2(14) . . C43 C44 C39 127.2(12) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Pd1 C1 1.988(4) . Pd1 Si1 2.4251(12) . Pd1 Si3 2.5828(11) . Pd1 Pd4 2.6812(4) . Pd2 C6 1.986(5) . Pd2 Si1 2.4339(12) . Pd2 Si2 2.6401(11) . Pd2 Pd4 2.6776(4) . Pd3 C11 2.014(4) . Pd3 C16 2.015(4) . Pd3 Si2 2.5094(11) . Pd3 Si3 2.5341(11) . Pd3 Pd4 2.7524(4) . Pd4 Si2 2.2622(11) . Pd4 Si3 2.2692(11) . Pd4 Si1 2.3106(11) . Si1 C21 1.917(5) . Si1 C24 1.938(5) . Si2 C30 1.910(5) . Si2 C27 1.913(4) . Si3 C33 1.917(5) . Si3 C36 1.919(4) . N1 C1 1.141(6) . N1 C2 1.449(5) . N2 C6 1.142(6) . N2 C7 1.449(6) . N3 C11 1.158(5) . N3 C12 1.464(5) . N4 C16 1.141(6) . N4 C17 1.465(6) . C2 C3 1.503(7) . C2 C4 1.510(7) . C2 C5 1.525(7) . C3 H3A 0.9800 . C3 H3B 0.9800 . C3 H3C 0.9800 . C4 H4A 0.9800 . C4 H4B 0.9800 . C4 H4C 0.9800 . C5 H5A 0.9800 . C5 H5B 0.9800 . C5 H5C 0.9800 . C7 C10 1.507(7) . C7 C9 1.520(8) . C7 C8 1.527(8) . C8 H8A 0.9800 . C8 H8B 0.9800 . C8 H8C 0.9800 . C9 H9A 0.9800 . C9 H9B 0.9800 . C9 H9C 0.9800 . C10 H10A 0.9800 . C10 H10B 0.9800 . C10 H10C 0.9800 . C12 C15 1.520(7) . C12 C13 1.523(7) . C12 C14 1.525(7) . C13 H13A 0.9800 . C13 H13B 0.9800 . C13 H13C 0.9800 . C14 H14A 0.9800 . C14 H14B 0.9800 . C14 H14C 0.9800 . C15 H15A 0.9800 . C15 H15B 0.9800 . C15 H15C 0.9800 . C17 C20 1.509(9) . C17 C19 1.524(8) . C17 C18 1.533(8) . C18 H18A 0.9800 . C18 H18B 0.9800 . C18 H18C 0.9800 . C19 H19A 0.9800 . C19 H19B 0.9800 . C19 H19C 0.9800 . C20 H20A 0.9800 . C20 H20B 0.9800 . C20 H20C 0.9800 . C21 C23 1.524(7) . C21 C22 1.531(7) . C21 H21 1.0000 . C22 H22A 0.9800 . C22 H22B 0.9800 . C22 H22C 0.9800 . C23 H23A 0.9800 . C23 H23B 0.9800 . C23 H23C 0.9800 . C24 C25 1.526(7) . C24 C26 1.527(7) . C24 H24 1.0000 . C25 H25A 0.9800 . C25 H25B 0.9800 . C25 H25C 0.9800 . C26 H26A 0.9800 . C26 H26B 0.9800 . C26 H26C 0.9800 . C27 C28 1.532(7) . C27 C29 1.538(6) . C27 H27 1.0000 . C28 H28A 0.9800 . C28 H28B 0.9800 . C28 H28C 0.9800 . C29 H29A 0.9800 . C29 H29B 0.9800 . C29 H29C 0.9800 . C30 C31 1.487(8) . C30 C32 1.537(7) . C30 H30 1.0000 . C31 H31A 0.9800 . C31 H31B 0.9800 . C31 H31C 0.9800 . C32 H32A 0.9800 . C32 H32B 0.9800 . C32 H32C 0.9800 . C33 C34 1.535(7) . C33 C35 1.538(6) . C33 H33 1.0000 . C34 H34A 0.9800 . C34 H34B 0.9800 . C34 H34C 0.9800 . C35 H35A 0.9800 . C35 H35B 0.9800 . C35 H35C 0.9800 . C36 C38 1.521(6) . C36 C37 1.523(6) . C36 H36 1.0000 . C37 H37A 0.9800 . C37 H37B 0.9800 . C37 H37C 0.9800 . C38 H38A 0.9800 . C38 H38B 0.9800 . C38 H38C 0.9800 . C39 C45 1.319(18) . C39 C40 1.394(15) . C39 C44 1.485(14) . C40 C41 1.369(16) . C41 C42 1.405(17) . C42 C43 1.406(19) . C43 C44 1.138(17) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C45 C39 C40 C41 179.7(12) . . . . C44 C39 C40 C41 1.0(15) . . . . C39 C40 C41 C42 3.1(18) . . . . C40 C41 C42 C43 0.0(18) . . . . C41 C42 C43 C44 -9(2) . . . . C42 C43 C44 C39 15(2) . . . . C45 C39 C44 C43 170.9(15) . . . . C40 C39 C44 C43 -10.7(18) . . . .