#------------------------------------------------------------------------------ #$Date: 2019-12-13 11:04:13 +0200 (Fri, 13 Dec 2019) $ #$Revision: 245052 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/65/1556556.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556556 loop_ _publ_author_name 'Sunada, Y.' 'Taniyama, N.' 'Shimamoto, K.' 'Kyushin, S.' 'Nagashima, H.' _publ_section_title ; Construction of a Planar Tetrapalladium Cluster by the Reaction of Palladium(0) Bis(isocyanide) with Cyclic Tetrasilane ; _journal_name_full Inorganics _journal_page_first 84 _journal_paper_doi 10.3390/inorganics5040084 _journal_volume 5 _journal_year 2017 _chemical_formula_moiety 'C36 H75 O9 P3 Pd3 Si3' _chemical_formula_sum 'C36 H75 O9 P3 Pd3 Si3' _chemical_formula_weight 1148.36 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 81.516(6) _cell_angle_beta 85.854(6) _cell_angle_gamma 64.096(5) _cell_formula_units_Z 2 _cell_length_a 11.2891(18) _cell_length_b 12.711(2) _cell_length_c 19.549(3) _cell_measurement_reflns_used 31166 _cell_measurement_temperature 103 _cell_measurement_theta_max 11.37 _cell_measurement_theta_min 0.83 _cell_volume 2495.6(7) _computing_cell_refinement 'RAPID AUTO' _computing_data_collection 'RAPID AUTO (Rigaku, ????)' _computing_data_reduction 'RAPID AUTO' _computing_molecular_graphics 'CrystalStructure 4.2.5' _computing_publication_material 'CrystalStructure 4.2.5 (Rigaku, 2017)' _computing_structure_refinement 'SHELXL97 (Sheldrick, 2008)' _computing_structure_solution 'SIR2011 (Burla, et al., 2012)' _diffrn_ambient_temperature 103 _diffrn_detector_area_resol_mean 14.706 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Rigaku R-AXIS IV' _diffrn_measurement_method \w _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.71075 _diffrn_reflns_av_R_equivalents 0.0682 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 44577 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.485 _diffrn_reflns_theta_min 2.896 _diffrn_standards_interval_count . _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.000 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.834 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'ABSCOR (Rigaku, 1995)' _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.528 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1176.00 _exptl_crystal_size_max 0.120 _exptl_crystal_size_mid 0.120 _exptl_crystal_size_min 0.080 _refine_diff_density_max 2.32 _refine_diff_density_min -0.94 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.023 _refine_ls_hydrogen_treatment constr _refine_ls_number_parameters 507 _refine_ls_number_reflns 11457 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0523 _refine_ls_R_factor_gt 0.0370 _refine_ls_shift/su_max 0.002 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w = 1/[\s^2^(Fo^2^)+(0.0264P)^2^+4.7817P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0774 _refine_ls_wR_factor_ref 0.0830 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 9364 _reflns_number_total 11457 _reflns_threshold_expression F^2^>2.0\s(F^2^) _cod_data_source_file Inorganics-2017-5-84.cif _cod_data_source_block Pd4Si3POR3 _cod_database_code 1556556 _shelxl_version_number 2014-1 _shelx_res_file ; TITL Pd4Si3POR3 CELL 0.71075 11.28906 12.71067 19.54930 81.51620 85.85410 64.09610 ZERR 2 0.00176 0.00198 0.00320 0.00570 0.00600 0.00450 LATT 1 SFAC C H O PD SI P UNIT 72 150 18 6 6 6 OMIT 1 -1 1 OMIT -1 0 1 OMIT 0 1 0 OMIT 1 0 0 OMIT 0 0 2 OMIT 0 1 1 OMIT 1 1 2 OMIT 0 1 2 OMIT 1 1 0 OMIT -1 -1 1 OMIT 1 1 1 OMIT 0 -1 1 OMIT 0 0 1 OMIT 1 0 1 OMIT -1 0 2 OMIT 0 1 3 OMIT 2 1 0 OMIT 0 -1 2 OMIT 1 2 2 OMIT 1 1 3 OMIT 1 2 0 OMIT 1 0 3 L.S. 20 FMAP 2 PLAN 21 WPDB -2 HTAB BOND $H CONF LIST 4 TEMP -170.0 ACTA SIZE 0.120 0.120 0.080 WGHT 0.026400 4.781700 FVAR 0.82342 PD1 4 0.405452 0.646875 0.690840 11.00000 0.00651 0.00985 = 0.01099 0.00000 0.00090 -0.00282 PD2 4 0.158948 0.693646 0.739882 11.00000 0.00667 0.01099 = 0.00944 0.00049 0.00021 -0.00339 PD3 4 0.367748 0.500089 0.795822 11.00000 0.00642 0.01122 = 0.01048 0.00084 -0.00063 -0.00403 P1 6 0.540796 0.688515 0.618619 11.00000 0.01125 0.01449 = 0.01535 -0.00066 0.00094 -0.00518 P2 6 -0.051054 0.813291 0.737822 11.00000 0.01030 0.01582 = 0.01291 -0.00198 0.00075 -0.00515 P3 6 0.451768 0.363521 0.883961 11.00000 0.01193 0.01582 = 0.01452 -0.00115 -0.00054 -0.00658 SI1 5 0.214403 0.817327 0.653831 11.00000 0.01183 0.01558 = 0.01047 0.00045 -0.00046 -0.00458 SI2 5 0.145088 0.544213 0.824090 11.00000 0.01176 0.01900 = 0.01237 -0.00046 0.00004 -0.00824 SI3 5 0.573653 0.469957 0.742856 11.00000 0.00896 0.01485 = 0.01416 -0.00077 -0.00088 -0.00409 O1 3 0.691445 0.641058 0.642409 11.00000 0.01246 0.02402 = 0.01342 0.00217 0.00003 -0.00874 O2 3 0.560522 0.637868 0.546117 11.00000 0.01883 0.02809 = 0.01639 -0.00611 0.00311 -0.01538 O3 3 0.508539 0.825701 0.592123 11.00000 0.01825 0.01416 = 0.02990 -0.00016 0.00751 -0.00496 O4 3 -0.109139 0.907723 0.669613 11.00000 0.01344 0.02339 = 0.01843 0.00464 0.00269 -0.00255 O5 3 -0.158253 0.760109 0.747482 11.00000 0.01367 0.01485 = 0.02663 0.00001 -0.00172 -0.00589 O6 3 -0.096425 0.899376 0.796942 11.00000 0.01292 0.02622 = 0.02143 -0.01106 -0.00270 -0.00386 O7 3 0.358338 0.318467 0.934227 11.00000 0.01303 0.02561 = 0.01638 0.00248 -0.00280 -0.01000 O8 3 0.512346 0.409538 0.938925 11.00000 0.02120 0.01553 = 0.01661 -0.00116 -0.00427 -0.00904 O9 3 0.573899 0.238063 0.873866 11.00000 0.01900 0.01638 = 0.01171 -0.00090 0.00128 -0.00523 C1 1 0.779724 0.671083 0.594284 11.00000 0.01390 0.02455 = 0.01368 0.00040 -0.00052 -0.00878 AFIX 23 H1A 2 0.859931 0.598588 0.587025 11.00000 -1.20000 H1B 2 0.806645 0.724685 0.613982 11.00000 -1.20000 AFIX 0 C2 1 0.662078 0.649548 0.499744 11.00000 0.02123 0.02414 = 0.01240 -0.00170 0.00383 -0.01294 AFIX 23 H2A 2 0.625700 0.682498 0.452713 11.00000 -1.20000 H2B 2 0.736115 0.570849 0.497152 11.00000 -1.20000 AFIX 0 C3 1 0.593918 0.844075 0.538010 11.00000 0.01793 0.01783 = 0.02002 0.00344 0.00070 -0.00664 AFIX 23 H3A 2 0.624781 0.900526 0.550623 11.00000 -1.20000 H3B 2 0.543290 0.879510 0.494663 11.00000 -1.20000 AFIX 0 C4 1 0.712272 0.730554 0.525539 11.00000 0.01514 0.01672 = 0.01449 0.00046 -0.00125 -0.00570 C5 1 0.804076 0.760094 0.472649 11.00000 0.01850 0.02394 = 0.01604 0.00304 0.00177 -0.01077 AFIX 23 H5A 2 0.752569 0.805973 0.430772 11.00000 -1.20000 H5B 2 0.834412 0.811471 0.492317 11.00000 -1.20000 AFIX 0 C6 1 0.924162 0.654899 0.451019 11.00000 0.02641 0.03496 = 0.02323 -0.00901 0.01098 -0.01772 AFIX 33 H6A 2 0.895814 0.604209 0.430158 11.00000 -1.20000 H6B 2 0.978015 0.610009 0.491694 11.00000 -1.20000 H6C 2 0.976177 0.682571 0.417242 11.00000 -1.20000 AFIX 0 C7 1 -0.243584 0.995280 0.673089 11.00000 0.01348 0.01893 = 0.01867 0.00199 0.00098 -0.00381 AFIX 23 H7A 2 -0.293100 0.994838 0.633436 11.00000 -1.20000 H7B 2 -0.245414 1.074424 0.669984 11.00000 -1.20000 AFIX 0 C8 1 -0.296329 0.845271 0.747105 11.00000 0.01054 0.01853 = 0.02754 -0.00232 0.00191 -0.00527 AFIX 23 H8A 2 -0.339732 0.828498 0.790404 11.00000 -1.20000 H8B 2 -0.341259 0.837386 0.707835 11.00000 -1.20000 AFIX 0 C9 1 -0.234975 0.978276 0.800223 11.00000 0.01448 0.02170 = 0.02035 -0.00975 0.00023 -0.00401 AFIX 23 H9A 2 -0.245737 1.060242 0.798297 11.00000 -1.20000 H9B 2 -0.272492 0.957777 0.844716 11.00000 -1.20000 AFIX 0 C10 1 -0.309484 0.970480 0.740750 11.00000 0.01005 0.01413 = 0.01628 -0.00423 0.00165 -0.00295 C11 1 -0.454866 1.061101 0.744965 11.00000 0.01109 0.02364 = 0.02051 -0.00331 0.00093 -0.00334 AFIX 23 H11A 2 -0.496100 1.034381 0.786028 11.00000 -1.20000 H11B 2 -0.457194 1.137403 0.752303 11.00000 -1.20000 AFIX 0 C12 1 -0.538134 1.081777 0.681750 11.00000 0.01506 0.02045 = 0.03462 -0.00331 -0.00514 -0.00352 AFIX 33 H12A 2 -0.630709 1.131648 0.691745 11.00000 -1.20000 H12B 2 -0.529279 1.005900 0.670739 11.00000 -1.20000 H12C 2 -0.507802 1.121041 0.642234 11.00000 -1.20000 AFIX 0 C13 1 0.412924 0.252741 1.000844 11.00000 0.01894 0.02365 = 0.01103 0.00057 0.00070 -0.01030 AFIX 23 H13A 2 0.394148 0.182789 1.010258 11.00000 -1.20000 H13B 2 0.371084 0.303014 1.037916 11.00000 -1.20000 AFIX 0 C14 1 0.585905 0.322974 0.995853 11.00000 0.02130 0.01869 = 0.01527 -0.00349 -0.00463 -0.01011 AFIX 23 H14A 2 0.558770 0.357711 1.039729 11.00000 -1.20000 H14B 2 0.681139 0.300779 0.988648 11.00000 -1.20000 AFIX 0 C15 1 0.619387 0.154447 0.936362 11.00000 0.01802 0.01240 = 0.01490 -0.00094 -0.00073 -0.00208 AFIX 23 H15A 2 0.716672 0.120048 0.938178 11.00000 -1.20000 H15B 2 0.593853 0.089485 0.935160 11.00000 -1.20000 AFIX 0 C16 1 0.561166 0.213549 1.000668 11.00000 0.01576 0.01695 = 0.01103 -0.00211 -0.00075 -0.00817 C17 1 0.624364 0.132960 1.066940 11.00000 0.02146 0.02534 = 0.01732 -0.00104 -0.00246 -0.01119 AFIX 23 H17A 2 0.715498 0.124496 1.069108 11.00000 -1.20000 H17B 2 0.575236 0.172205 1.106988 11.00000 -1.20000 AFIX 0 C18 1 0.629209 0.009831 1.074562 11.00000 0.04528 0.02826 = 0.02757 0.01175 -0.01059 -0.02140 AFIX 33 H18A 2 0.679325 -0.031063 1.035844 11.00000 -1.20000 H18B 2 0.539400 0.016458 1.074553 11.00000 -1.20000 H18C 2 0.672010 -0.034915 1.118179 11.00000 -1.20000 AFIX 0 C19 1 0.145606 0.849328 0.563608 11.00000 0.01434 0.03359 = 0.01222 0.00100 -0.00192 -0.00764 AFIX 13 H19 2 0.053317 0.912248 0.564952 11.00000 -1.20000 AFIX 0 C20 1 0.137992 0.740682 0.543606 11.00000 0.06696 0.08147 = 0.01857 -0.01137 0.00094 -0.05880 AFIX 33 H20A 2 0.227207 0.679647 0.537085 11.00000 -1.20000 H20B 2 0.088882 0.762293 0.500462 11.00000 -1.20000 H20C 2 0.093005 0.710433 0.580444 11.00000 -1.20000 AFIX 0 C21 1 0.219597 0.895319 0.508081 11.00000 0.02634 0.03796 = 0.01747 0.00157 0.00101 -0.01242 AFIX 33 H21A 2 0.174667 0.915007 0.463727 11.00000 -1.20000 H21B 2 0.309788 0.834478 0.503829 11.00000 -1.20000 H21C 2 0.221881 0.966024 0.521007 11.00000 -1.20000 AFIX 0 C22 1 0.208698 0.959788 0.676747 11.00000 0.01969 0.01313 = 0.02006 0.00075 0.00003 -0.00772 AFIX 13 H22 2 0.267569 0.982075 0.643140 11.00000 -1.20000 AFIX 0 C23 1 0.266031 0.937767 0.748559 11.00000 0.04238 0.03131 = 0.02694 -0.00742 -0.00415 -0.01953 AFIX 33 H23A 2 0.264376 1.010929 0.759976 11.00000 -1.20000 H23B 2 0.357104 0.876831 0.749164 11.00000 -1.20000 H23C 2 0.213457 0.911390 0.782687 11.00000 -1.20000 AFIX 0 C24 1 0.072157 1.064312 0.671639 11.00000 0.02527 0.01842 = 0.04479 -0.00665 0.00248 -0.00586 AFIX 33 H24A 2 0.078763 1.134988 0.681418 11.00000 -1.20000 H24B 2 0.012469 1.046851 0.705328 11.00000 -1.20000 H24C 2 0.037857 1.077989 0.624904 11.00000 -1.20000 AFIX 0 C25 1 0.077685 0.446368 0.793255 11.00000 0.01578 0.02255 = 0.02406 -0.00280 -0.00275 -0.01067 AFIX 13 H25 2 -0.016379 0.475173 0.808756 11.00000 -1.20000 AFIX 0 C26 1 0.079570 0.454545 0.714823 11.00000 0.05621 0.04460 = 0.02387 -0.00623 -0.01020 -0.03174 AFIX 33 H26A 2 0.061148 0.391891 0.701411 11.00000 -1.20000 H26B 2 0.166476 0.445486 0.697043 11.00000 -1.20000 H26C 2 0.012299 0.531529 0.695469 11.00000 -1.20000 AFIX 0 C27 1 0.149636 0.317749 0.824770 11.00000 0.03479 0.02325 = 0.04345 0.00245 -0.01368 -0.01843 AFIX 33 H27A 2 0.241426 0.285537 0.808691 11.00000 -1.20000 H27B 2 0.106623 0.272223 0.810551 11.00000 -1.20000 H27C 2 0.147082 0.312856 0.875315 11.00000 -1.20000 AFIX 0 C28 1 0.076291 0.566213 0.915331 11.00000 0.02071 0.02340 = 0.01425 -0.00042 0.00005 -0.01049 AFIX 13 H28 2 0.084475 0.487829 0.938598 11.00000 -1.20000 AFIX 0 C29 1 -0.069517 0.651595 0.917044 11.00000 0.01771 0.04096 = 0.01719 -0.00269 0.00157 -0.01118 AFIX 33 H29A 2 -0.080958 0.731179 0.897982 11.00000 -1.20000 H29B 2 -0.101928 0.651794 0.964924 11.00000 -1.20000 H29C 2 -0.119270 0.626623 0.889324 11.00000 -1.20000 AFIX 0 C30 1 0.155432 0.603706 0.957533 11.00000 0.02394 0.04468 = 0.03091 -0.01818 -0.00502 -0.00573 AFIX 33 H30A 2 0.138534 0.685571 0.940924 11.00000 -1.20000 H30B 2 0.249466 0.552392 0.952604 11.00000 -1.20000 H30C 2 0.129430 0.597381 1.006337 11.00000 -1.20000 AFIX 0 C31 1 0.650518 0.341978 0.689879 11.00000 0.01908 0.01495 = 0.01846 -0.00221 0.00083 -0.00406 AFIX 13 H31 2 0.680395 0.267530 0.722980 11.00000 -1.20000 AFIX 0 C32 1 0.548355 0.342079 0.642810 11.00000 0.03358 0.02107 = 0.02658 -0.00734 -0.00527 -0.01154 AFIX 33 H32A 2 0.587002 0.270850 0.619738 11.00000 -1.20000 H32B 2 0.520575 0.411981 0.607976 11.00000 -1.20000 H32C 2 0.471877 0.343472 0.670488 11.00000 -1.20000 AFIX 0 C33 1 0.770728 0.339259 0.647385 11.00000 0.02934 0.02132 = 0.02555 -0.00902 0.01195 -0.00638 AFIX 33 H33A 2 0.812210 0.266048 0.626264 11.00000 -1.20000 H33B 2 0.833945 0.343017 0.677633 11.00000 -1.20000 H33C 2 0.743085 0.406970 0.611019 11.00000 -1.20000 AFIX 0 C34 1 0.711127 0.475858 0.789971 11.00000 0.01455 0.03080 = 0.01573 0.00095 -0.00147 -0.01445 AFIX 13 H34 2 0.768148 0.496220 0.754093 11.00000 -1.20000 AFIX 0 C35 1 0.798358 0.359065 0.831154 11.00000 0.01663 0.04732 = 0.02302 0.00883 -0.00388 -0.01577 AFIX 33 H35A 2 0.746573 0.338293 0.868485 11.00000 -1.20000 H35B 2 0.871480 0.366121 0.850953 11.00000 -1.20000 H35C 2 0.833310 0.297416 0.800599 11.00000 -1.20000 AFIX 0 C36 1 0.654012 0.574885 0.835129 11.00000 0.04183 0.04646 = 0.02706 -0.01228 0.00348 -0.03263 AFIX 33 H36A 2 0.596486 0.648292 0.807288 11.00000 -1.20000 H36B 2 0.725791 0.585234 0.853983 11.00000 -1.20000 H36C 2 0.602977 0.554900 0.873197 11.00000 -1.20000 AFIX 0 C37 1 0.008576 1.061090 0.885086 10.50000 0.02447 C38 1 0.001034 0.949843 0.934339 10.50000 0.04742 C39 1 -0.000197 1.024581 0.945869 10.50000 0.04171 C40 1 -0.010522 0.918321 0.984581 10.50000 0.02083 C41 1 -0.020627 0.887399 1.039736 10.50000 0.04896 HKLF 4 REM Pd4Si3POR3 REM R1 = 0.0370 for 9364 Fo > 4sig(Fo) and 0.0523 for all 11457 data REM 507 parameters refined using 0 restraints END WGHT 0.0264 4.8156 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 2.320, deepest hole -0.936, 1-sigma level 0.121 Q1 1 0.0208 1.0538 0.9127 11.00000 0.05 2.32 Q2 1 -0.0009 1.0664 0.8620 11.00000 0.05 1.82 Q3 1 -0.0261 0.9192 0.9595 11.00000 0.05 1.71 Q4 1 0.0050 0.9086 1.0096 11.00000 0.05 1.59 Q5 1 0.0000 1.0000 1.0000 10.50000 0.05 1.32 Q6 1 0.0142 0.9638 0.9176 11.00000 0.05 0.88 Q7 1 -0.0464 0.8573 1.0332 11.00000 0.05 0.57 Q8 1 0.0973 0.4895 0.8099 11.00000 0.05 0.56 Q9 1 0.3051 0.5142 0.7820 11.00000 0.05 0.55 Q10 1 0.5010 0.4198 0.7815 11.00000 0.05 0.54 Q11 1 0.0271 0.2010 0.7702 11.00000 0.05 0.48 Q12 1 0.6056 0.4197 0.6934 11.00000 0.05 0.47 Q13 1 0.2892 0.6204 0.7285 11.00000 0.05 0.47 Q14 1 0.2255 0.6020 0.5817 11.00000 0.05 0.47 Q15 1 0.3419 0.5603 0.7305 11.00000 0.05 0.46 Q16 1 -0.0876 0.8887 0.7613 11.00000 0.05 0.45 Q17 1 0.5605 0.2715 1.0026 11.00000 0.05 0.45 Q18 1 0.4084 0.4342 0.8513 11.00000 0.05 0.44 Q19 1 0.7579 0.1111 0.9018 11.00000 0.05 0.44 Q20 1 0.4798 0.6498 0.7044 11.00000 0.05 0.43 Q21 1 0.4116 0.5864 0.7497 11.00000 0.05 0.43 ; _shelx_res_checksum 68182 _shelx_hkl_file ; 0 0 1 -0.46 3.13 0 0 -1 -6.64 3.46 0 0 -1 0.65 3.37 0 0 2 -3.02 8.78 0 0 2 6.40 12.56 0 0 -2 -7.38 9.68 0 0 -2 0.50 8.52 0 0 3 2765.76 105.76 0 0 416194.22 631.91 0 0 418456.21 726.76 0 0 -417868.27 691.09 0 0 -419251.65 741.29 0 0 5 2124.56 120.06 0 0 5 2309.50 134.43 0 0 -5 2027.78 118.76 0 0 -5 2505.73 131.76 0 0 6 106.73 54.92 0 0 6 -15.17 59.06 0 0 -6 32.86 55.19 0 0 -6 -74.11 60.79 0 0 7 2684.40 148.46 0 0 7 2544.54 149.73 0 0 -7 2501.92 110.61 0 0 -7 2537.27 153.30 0 0 8 1210.66 82.75 0 0 8 1408.65 120.97 0 0 -8 1335.52 117.22 0 0 -8 1462.23 128.84 0 0 9 37.04 71.85 0 0 9 107.30 77.02 0 0 -9 10.34 45.46 0 0 -9 137.86 78.03 0 0 10 105.39 50.08 0 0 10 211.40 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79.73 11 -3 -3 1096.58 220.28 -11 3 3 852.07 206.13 11 -3 -2 1045.69 98.53 11 -3 -2 752.44 107.31 11 -3 -2 1303.86 241.69 -11 3 2 936.91 227.16 11 -3 -1 2202.12 162.64 11 -3 -1 1812.27 146.07 11 -3 -1 2083.06 293.85 -11 3 1 1807.76 187.24 11 -3 0 1338.12 144.17 11 -3 0 1029.28 131.24 11 -3 0 1253.68 255.35 -11 3 0 1598.59 251.73 11 -3 1 2107.91 186.93 11 -3 1 2064.22 178.19 11 -3 1 2828.81 312.41 -11 3 -1 2132.75 290.63 11 -3 2 1785.52 189.32 11 -3 2 1706.88 145.67 11 -3 2 1973.05 204.82 -11 3 -2 1812.55 263.02 11 -3 3 667.05 149.03 11 -3 3 759.31 150.11 11 -3 3 637.77 235.88 -11 3 -3 885.89 210.01 11 -3 4 841.06 169.09 11 -3 4 829.69 164.68 11 -3 4 882.13 238.91 -11 3 -4 674.46 220.56 11 -3 5 142.81 105.16 11 -3 5 265.73 143.47 11 -3 5 540.94 190.48 -11 3 -5 66.38 112.58 11 -3 6 138.77 118.88 11 -3 6 251.82 120.29 11 -3 6 540.90 210.18 -11 3 -6 428.72 190.46 11 -3 7 811.60 157.17 11 -3 7 868.41 160.08 11 -3 7 1024.47 170.76 -11 3 -7 936.71 228.94 11 -3 8 806.96 216.90 11 -3 8 812.63 220.59 11 -3 8 850.71 264.79 -11 3 -8 1556.45 233.34 11 -2 -11 1566.84 247.98 -11 2 11 1435.57 239.45 11 -2 -10 1849.63 270.34 -11 2 10 1720.08 267.44 11 -2 -9 4142.50 382.22 -11 2 9 4017.18 381.76 11 -2 -8 3197.77 337.16 -11 2 8 3039.10 339.48 11 -2 -7 248.23 184.15 -11 2 7 252.88 174.70 11 -2 -6 2459.35 293.83 -11 2 6 2310.45 284.37 11 -2 -5 20.34 32.72 11 -2 -5 34.18 27.86 11 -2 -5 -15.34 162.32 -11 2 5 240.69 154.22 11 -2 -4 159.65 40.99 11 -2 -4 304.69 45.43 11 -2 -4 443.72 177.80 -11 2 4 392.64 172.89 11 -2 -3 240.66 50.70 11 -2 -3 309.56 47.42 11 -2 -3 180.13 176.66 -11 2 3 240.80 164.56 11 -2 -2 84.80 53.16 11 -2 -2 101.26 47.89 11 -2 -2 -116.45 167.56 -11 2 2 263.90 157.96 11 -2 -1 1143.05 110.44 11 -2 -1 987.17 87.21 11 -2 -1 1410.61 243.63 -11 2 1 1108.12 227.62 11 -2 0 501.49 102.45 11 -2 0 481.20 91.74 11 -2 0 586.08 136.79 -11 2 0 622.45 192.91 11 -2 1 2544.81 159.34 11 -2 1 2554.79 179.78 11 -2 1 2793.77 311.63 -11 2 -1 2579.68 286.91 11 -2 2 167.06 100.48 11 -2 2 19.96 94.58 11 -2 2 148.70 180.59 -11 2 -2 158.90 163.31 11 -2 3 1976.32 197.22 11 -2 3 1954.88 182.79 11 -2 3 2018.89 305.59 -11 2 -3 2459.63 273.70 11 -2 4 427.59 112.45 11 -2 4 533.67 137.99 11 -2 4 403.99 136.88 -11 2 -4 845.19 122.94 11 -2 5 450.71 150.50 11 -2 5 556.22 113.31 11 -2 5 653.89 213.95 -11 2 -5 493.98 188.83 11 -2 6 47.22 94.98 11 -2 6 -17.21 127.88 11 -2 6 177.48 177.04 -11 2 -6 -4.26 152.80 11 -2 7 192.67 150.33 11 -2 7 -52.16 157.14 11 -2 7 517.78 194.93 -11 2 -7 291.94 175.08 11 -2 8 1355.67 180.14 11 -2 8 1433.48 184.85 11 -2 8 1294.17 177.74 -11 2 -8 1011.08 245.49 11 -2 9 543.46 144.46 11 -2 9 319.07 145.12 11 -2 9 456.98 219.91 -11 2 -9 228.74 195.91 11 -2 10 3221.66 289.80 11 -2 10 3163.75 390.76 11 -2 10 4181.48 425.16 -11 2 -10 4110.45 381.86 11 -1 -12 706.48 192.27 -11 1 12 603.68 36.81 -11 1 12 657.12 199.88 11 -1 -11 302.09 165.60 -11 1 11 217.52 103.76 11 -1 -10 287.55 152.15 -11 1 10 74.64 102.15 11 -1 -9 2987.18 328.90 -11 1 9 3243.54 328.20 11 -1 -8 826.28 188.86 -11 1 8 464.00 201.46 11 -1 -7 4909.25 322.51 -11 1 7 4988.12 410.33 11 -1 -6 2369.82 290.19 -11 1 6 2439.78 280.13 11 -1 -5 996.06 223.54 -11 1 5 975.91 141.41 11 -1 -4 1816.33 266.25 -11 1 4 2103.82 243.44 11 -1 -3 351.86 42.67 11 -1 -3 462.39 44.97 11 -1 -3 735.17 186.75 -11 1 3 -97.91 178.43 11 -1 -2 744.30 63.49 11 -1 -2 715.66 66.14 11 -1 -2 546.01 209.11 -11 1 2 718.70 128.97 11 -1 -1 752.04 71.00 11 -1 -1 556.14 62.11 11 -1 -1 527.06 133.40 -11 1 1 910.45 182.12 11 -1 0 28.75 67.28 11 -1 0 174.85 160.40 -11 1 0 29.24 140.80 11 -1 1 1778.37 143.64 11 -1 1 1498.67 121.27 11 -1 1 1735.57 173.91 -11 1 -1 1461.94 235.76 11 -1 2 246.65 95.10 11 -1 2 46.31 87.07 11 -1 2 -250.93 170.32 -11 1 -2 179.51 155.09 11 -1 3 3641.43 239.69 11 -1 3 3026.89 219.99 11 -1 3 3896.60 357.40 -11 1 -3 2964.92 230.99 11 -1 4 76.58 80.18 11 -1 4 75.04 106.70 11 -1 4 46.84 103.85 -11 1 -4 93.04 143.70 11 -1 5 1077.09 141.07 11 -1 5 1232.46 136.86 11 -1 5 1463.43 230.12 -11 1 -5 1230.21 214.22 11 -1 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826.27 153.71 -11 -2 -12 1050.38 181.43 -11 -2 -12 1122.54 148.69 11 2 13 394.70 159.79 11 2 13 485.01 189.22 -11 -2 -13 435.68 161.68 -11 -2 -13 272.03 197.65 11 2 14 472.03 166.95 11 2 14 513.46 141.96 -11 -2 -14 662.62 182.39 -11 -2 -14 485.19 206.86 11 2 15 2463.84 283.83 11 2 15 2039.44 319.48 -11 -2 -15 2433.74 283.52 -11 -2 -15 2143.62 318.62 11 2 16 2049.31 276.89 11 2 16 2484.82 322.07 -11 -2 -16 1851.48 272.27 -11 -2 -16 1706.28 307.86 11 3 -15 -8.00 122.68 -11 -3 15 39.57 83.79 -11 -3 15 35.31 75.11 -11 -3 15 -61.84 129.87 11 3 -14 4993.93 360.33 -11 -3 14 4856.57 250.01 -11 -3 14 4884.36 252.25 -11 -3 14 4855.00 355.62 11 3 -13 165.08 119.43 -11 -3 13 -34.83 53.13 -11 -3 13 12.28 61.41 -11 -3 13 -104.20 141.16 11 3 -12 3947.56 384.11 -11 -3 12 4403.42 194.19 -11 -3 12 4038.93 194.46 -11 -3 12 4208.10 307.69 11 3 -11 88.37 120.55 -11 -3 11 43.52 44.19 -11 -3 11 81.93 45.99 -11 -3 11 15.48 121.94 11 3 -1010390.27 538.84 -11 -3 10 7135.06 273.88 -11 -3 10 7817.86 285.60 -11 -3 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1921.62 223.79 -12 -5 -7 1657.45 180.61 -12 -5 -7 1931.90 228.94 12 5 8 825.28 194.02 12 5 8 1025.19 208.24 -12 -5 -8 956.43 154.79 -12 -5 -8 839.39 124.53 12 5 9 1921.50 211.94 12 5 9 2289.19 270.90 -12 -5 -9 2204.61 218.89 -12 -5 -9 2143.39 264.30 12 5 10 2938.99 330.51 12 5 10 3183.49 341.28 -12 -5 -10 3023.41 270.76 -12 -5 -10 3919.84 259.76 12 5 11 3490.31 306.15 12 5 11 3961.33 367.14 -12 -5 -11 3589.58 299.73 -12 -5 -11 3950.22 364.11 12 5 12 2992.98 300.04 12 5 12 3289.52 349.06 -12 -5 -12 3196.66 303.66 -12 -5 -12 3958.33 359.94 12 5 13 2943.02 298.34 12 5 13 2992.61 343.97 -12 -5 -13 3502.65 307.06 -12 -5 -13 3220.35 349.02 12 5 14 192.29 162.65 12 5 14 338.70 124.67 -12 -5 -14 264.51 162.81 -12 -5 -14 155.39 116.00 12 5 15 1583.46 239.52 12 5 15 1507.23 278.81 -12 -5 -15 1437.36 252.44 12 6 -12 259.53 109.11 12 6 -12 149.48 109.58 -12 -6 12 185.53 100.77 -12 -6 12 219.27 108.79 12 6 -11 1381.42 158.15 12 6 -11 1243.49 154.95 -12 -6 11 1265.17 146.85 -12 -6 11 1096.57 142.50 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195.52 112.84 12 6 1 117.77 79.66 12 6 1 62.98 171.46 -12 -6 -1 173.27 78.72 -12 -6 -1 276.45 113.81 12 6 2 760.58 140.48 12 6 2 797.87 164.79 -12 -6 -2 644.31 107.90 -12 -6 -2 607.52 146.35 12 6 3 -11.43 85.83 12 6 3 244.06 126.97 -12 -6 -3 158.75 83.64 -12 -6 -3 -110.26 111.74 12 6 4 -133.89 110.82 12 6 4 93.67 113.58 -12 -6 -4 116.06 106.50 -12 -6 -4 -15.65 109.29 12 6 5 167.96 99.81 12 6 5 -112.46 135.54 -12 -6 -5 167.78 98.12 -12 -6 -5 224.22 124.40 12 6 6 693.31 171.26 12 6 6 403.87 171.78 -12 -6 -6 609.51 134.23 -12 -6 -6 991.63 163.96 12 6 7 604.65 181.06 12 6 7 753.86 171.77 -12 -6 -7 620.44 140.94 -12 -6 -7 616.04 166.20 12 6 8 -5.68 109.81 12 6 8 60.61 124.33 -12 -6 -8 52.24 109.94 -12 -6 -8 38.07 128.68 12 6 9 166.28 133.30 12 6 9 320.91 165.82 -12 -6 -9 518.37 135.51 -12 -6 -9 350.99 158.90 12 6 10 2356.71 229.63 12 6 10 2416.91 280.39 -12 -6 -10 1996.26 234.58 -12 -6 -10 2301.33 275.53 12 6 11 -146.05 130.21 12 6 11 72.90 159.21 -12 -6 -11 -128.01 133.30 -12 -6 -11 -59.52 157.31 12 6 12 7956.01 534.93 12 6 12 8476.40 497.83 -12 -6 -12 8831.55 554.35 -12 -6 -12 8442.17 602.19 12 6 13 -93.05 139.43 12 6 13 357.82 169.26 -12 -6 -13 -36.61 144.24 -12 -6 -13 57.22 161.99 12 6 14 5936.14 456.26 12 6 14 7333.02 551.54 -12 -6 -14 7243.21 491.93 -12 -6 -14 6088.70 405.40 12 6 15 367.81 195.02 12 6 15 575.73 147.06 -12 -6 -15 785.20 192.18 -12 -6 -15 676.47 220.96 12 7 -12 306.22 138.41 12 7 -12 261.61 132.02 -12 -7 12 275.20 129.44 -12 -7 12 433.40 138.09 12 7 -11 133.98 103.49 12 7 -11 -87.73 86.41 -12 -7 11 0.85 102.50 -12 -7 11 38.73 111.16 12 7 -10 266.90 112.10 12 7 -10 205.77 95.64 -12 -7 10 148.96 111.54 -12 -7 10 137.75 94.38 12 7 -9 907.78 106.74 12 7 -9 552.40 155.13 -12 -7 9 839.70 134.89 -12 -7 9 753.82 156.41 12 7 -8 144.60 77.19 12 7 -8 74.88 90.64 -12 -7 8 218.97 102.47 -12 -7 8 67.41 90.74 12 7 -7 2788.53 207.88 12 7 -7 2786.42 206.27 -12 -7 7 2767.95 203.63 -12 -7 7 2956.67 241.39 12 7 -6 93.35 71.00 12 7 -6 -63.21 124.36 -12 -7 6 125.98 95.58 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295.07 -12 -7 -16 1685.28 279.60 -12 -7 -16 1773.93 200.89 12 8 -12 9.47 116.35 12 8 -12 -62.71 93.98 -12 -8 12 41.89 89.41 -12 -8 12 11.38 100.52 12 8 -11 2134.70 177.32 12 8 -11 2168.11 158.80 -12 -8 11 2444.06 196.88 -12 -8 11 2227.90 167.71 12 8 -10 28.25 87.26 12 8 -10 87.66 99.60 -12 -8 10 148.21 119.53 -12 -8 10 64.89 106.02 12 8 -9 217.10 92.06 12 8 -9 251.56 107.19 -12 -8 9 141.40 128.18 -12 -8 9 143.66 110.93 12 8 -8 24.98 99.44 12 8 -8 -92.33 90.95 -12 -8 8 48.44 104.78 12 8 -7 50.49 77.99 12 8 -7 27.09 72.19 -12 -8 7 127.56 104.12 -12 -8 7 -99.87 96.31 12 8 -6 1140.87 130.79 12 8 -6 980.43 150.86 -12 -8 6 1049.14 162.82 -12 -8 6 1030.37 152.60 12 8 -5 227.69 96.01 12 8 -5 196.19 88.19 -12 -8 5 217.99 87.84 -12 -8 5 216.68 112.10 12 8 -4 1246.56 174.65 12 8 -4 1008.63 168.46 -12 -8 4 1278.75 132.80 -12 -8 4 1188.16 161.31 12 8 -3 4381.36 266.83 12 8 -3 4810.83 304.54 -12 -8 3 4463.20 298.48 -12 -8 3 4383.00 249.26 12 8 -2 -9.18 98.23 12 8 -2 116.06 125.75 -12 -8 2 146.36 106.67 -12 -8 2 12.42 105.05 12 8 -1 5283.60 307.06 12 8 -1 5237.29 303.76 -12 -8 1 4630.84 318.81 -12 -8 1 4661.83 274.90 12 8 0 377.27 107.42 12 8 0 377.28 114.97 -12 -8 0 250.28 129.63 -12 -8 0 84.99 100.38 12 8 1 36.77 89.87 12 8 1 -103.59 99.13 -12 -8 -1 -57.14 85.86 -12 -8 -1 146.90 87.12 12 8 2 632.54 159.64 12 8 2 741.18 143.18 -12 -8 -2 759.93 167.72 -12 -8 -2 691.09 164.71 12 8 3 826.69 186.64 12 8 3 1007.43 192.47 -12 -8 -3 1080.81 178.74 -12 -8 -3 952.00 145.69 12 8 4 1252.33 210.83 12 8 4 1709.22 180.55 -12 -8 -4 1651.50 179.65 -12 -8 -4 1380.82 170.07 12 8 5 2741.72 232.26 12 8 5 2846.54 242.34 -12 -8 -5 2603.74 280.71 -12 -8 -5 2898.59 289.32 12 8 6 3623.00 265.05 12 8 6 3734.29 357.71 -12 -8 -6 3582.82 275.46 -12 -8 -6 4176.77 358.51 12 8 7 1034.18 178.63 12 8 7 1314.52 192.47 -12 -8 -7 1292.51 185.87 -12 -8 -7 1486.98 240.62 12 8 8 2530.53 231.12 12 8 8 2490.69 243.47 -12 -8 -8 2076.01 227.97 -12 -8 -8 1659.48 226.26 12 8 9 585.24 152.41 12 8 9 322.74 163.87 -12 -8 -9 465.89 155.16 -12 -8 -9 311.81 163.28 12 8 10 513.81 159.75 12 8 10 349.93 168.94 -12 -8 -10 362.75 157.13 -12 -8 -10 398.72 168.01 12 8 11 370.10 152.99 12 8 11 528.54 170.68 -12 -8 -11 248.82 158.85 -12 -8 -11 147.71 165.79 12 8 12 -53.60 133.47 12 8 12 -108.56 148.29 -12 -8 -12 138.18 138.90 -12 -8 -12 215.67 149.74 12 8 13 1797.69 252.37 12 8 13 2101.19 275.89 -12 -8 -13 2107.09 264.32 -12 -8 -13 2215.66 271.87 12 8 14 1110.59 217.82 12 8 14 1240.45 240.83 -12 -8 -14 1102.50 153.48 -12 -8 -14 911.85 237.44 12 8 15 2390.86 281.23 12 8 15 1948.95 290.14 -12 -8 -15 2129.12 279.37 -12 -8 -15 1992.99 283.87 12 9 -11 5283.53 326.98 12 9 -11 4887.42 274.88 -12 -9 11 5237.53 343.43 -12 -9 11 4801.90 284.94 12 9 -10 98.81 100.59 12 9 -10 -18.62 83.32 -12 -9 10 85.29 108.04 -12 -9 10 36.85 89.08 12 9 -9 1441.83 208.56 12 9 -9 1590.87 146.24 -12 -9 9 1323.80 215.73 -12 -9 9 1611.37 153.34 12 9 -8 35.38 119.68 12 9 -8 71.70 80.15 -12 -9 8 127.05 96.37 -12 -9 8 -112.02 82.48 12 9 -7 63.58 87.15 12 9 -7 120.43 83.71 -12 -9 7 -27.33 122.76 -12 -9 7 -82.22 81.73 12 9 -6 207.56 100.71 12 9 -6 197.72 93.81 -12 -9 6 44.50 96.05 -12 -9 6 121.96 91.45 12 9 -5 467.79 122.33 12 9 -5 428.70 113.16 -12 -9 5 551.88 112.16 -12 -9 5 503.35 106.70 12 9 -4 1178.93 192.81 12 9 -4 1279.38 116.60 -12 -9 4 1118.89 182.79 -12 -9 4 1097.74 142.64 12 9 -3 -54.10 97.38 12 9 -3 57.03 75.24 -12 -9 3 137.94 119.33 -12 -9 3 47.08 93.04 12 9 -2 2093.01 255.13 12 9 -2 2412.08 213.95 -12 -9 2 2396.43 197.54 -12 -9 2 2300.52 156.82 12 9 -1 3029.10 242.33 12 9 -1 3335.53 208.38 -12 -9 1 2678.75 217.94 -12 -9 1 3046.43 190.21 12 9 0 2384.47 275.65 12 9 0 3020.58 210.24 -12 -9 0 2631.41 219.12 -12 -9 0 3056.57 190.08 12 9 1 280.99 125.83 12 9 1 465.54 146.99 -12 -9 -1 414.99 121.56 -12 -9 -1 447.29 104.76 12 9 2 2159.43 205.97 12 9 2 2458.03 234.40 -12 -9 -2 2676.90 222.42 -12 -9 -2 2342.75 230.57 12 9 3 61.34 116.46 12 9 3 -114.27 141.62 -12 -9 -3 138.42 120.32 -12 -9 -3 354.78 104.02 12 9 4 2059.49 198.17 12 9 4 1860.55 184.94 -12 -9 -4 1748.92 196.02 -12 -9 -4 2026.30 187.68 12 9 5 3893.46 296.08 12 9 5 3840.46 282.88 -12 -9 -5 4953.01 316.49 -12 -9 -5 3890.13 282.26 12 9 6 622.32 159.11 12 9 6 760.36 158.26 -12 -9 -6 667.10 149.29 -12 -9 -6 911.81 152.73 12 9 7 6481.64 414.91 12 9 7 5357.18 373.98 -12 -9 -7 5800.30 387.49 -12 -9 -7 5360.34 443.90 12 9 8 810.93 177.54 12 9 8 929.02 178.22 -12 -9 -8 790.69 223.92 -12 -9 -8 660.03 167.48 12 9 9 3299.17 298.78 12 9 9 3704.05 308.96 -12 -9 -9 3522.16 307.72 -12 -9 -9 3528.14 355.39 12 9 10 1042.91 187.73 12 9 10 718.11 192.54 -12 -9 -10 737.39 186.19 -12 -9 -10 810.93 189.37 12 9 11 1083.12 205.48 12 9 11 1092.63 216.44 -12 -9 -11 1174.90 200.14 -12 -9 -11 1205.45 213.74 12 9 12 354.02 109.57 12 9 12 587.55 118.50 -12 -9 -12 246.69 177.05 -12 -9 -12 308.31 168.51 12 9 13 404.94 173.80 12 9 13 683.50 190.86 -12 -9 -13 347.81 114.55 -12 -9 -13 537.75 184.94 12 9 14 29.65 148.91 12 9 14 -147.96 162.48 -12 -9 -14 134.96 146.38 -12 -9 -14 31.38 149.48 12 9 15 3376.85 347.71 12 9 15 3381.41 369.13 -12 -9 -15 3180.90 328.58 -12 -9 -15 3113.92 348.53 12 10 -10 4176.73 302.84 12 10 -10 3812.45 210.64 -12 -10 10 4514.81 314.89 -12 -10 10 3924.04 217.62 12 10 -9 4092.86 327.96 12 10 -9 3539.44 182.46 -12 -10 9 3496.77 270.71 -12 -10 9 3547.69 196.78 12 10 -8 905.01 156.43 12 10 -8 764.11 94.70 -12 -10 8 1052.87 162.27 -12 -10 8 750.75 92.21 12 10 -7 521.21 129.44 12 10 -7 570.44 86.59 -12 -10 7 290.15 137.56 -12 -10 7 383.16 77.36 12 10 -6 392.65 126.86 12 10 -6 336.49 75.15 -12 -10 6 358.99 125.65 -12 -10 6 359.31 78.34 12 10 -5 400.17 120.63 12 10 -5 298.40 87.17 -12 -10 5 86.49 158.15 -12 -10 5 225.87 78.69 12 10 -4 200.35 110.66 12 10 -4 66.46 77.44 -12 -10 4 103.37 102.56 -12 -10 4 -7.42 79.66 12 10 -3 316.28 128.08 12 10 -3 261.20 103.44 -12 -10 3 443.48 123.27 -12 -10 3 272.47 96.55 12 10 -2 261.70 122.82 12 10 -2 131.95 103.67 -12 -10 2 270.59 114.81 -12 -10 2 186.96 96.09 12 10 -1 89.88 118.25 12 10 -1 101.30 104.48 -12 -10 1 85.20 115.30 -12 -10 1 124.54 96.43 12 10 0 822.59 156.57 12 10 0 1101.23 156.48 -12 -10 0 764.93 190.17 -12 -10 0 905.71 137.73 12 10 1 498.90 153.64 12 10 1 710.56 112.20 -12 -10 -1 733.90 143.44 -12 -10 -1 496.89 108.42 12 10 2 945.53 168.75 12 10 2 889.49 160.86 -12 -10 -2 995.68 166.14 -12 -10 -2 803.07 166.20 12 10 3 249.74 173.92 12 10 3 309.21 140.21 -12 -10 -3 106.08 120.72 -12 -10 -3 327.63 101.97 12 10 4 453.28 139.06 12 10 4 469.96 120.52 -12 -10 -4 88.22 144.96 -12 -10 -4 622.61 119.59 12 10 5 1856.30 207.74 12 10 5 1690.78 235.86 -12 -10 -5 1856.62 214.31 -12 -10 -5 1842.33 182.48 12 10 6 90.34 120.17 12 10 6 -44.51 104.00 -12 -10 -6 -74.09 121.95 -12 -10 -6 -32.14 105.36 12 10 7 6570.91 426.80 12 10 7 5441.62 374.41 -12 -10 -7 5979.28 409.56 -12 -10 -7 5380.36 363.92 12 10 8 918.67 182.41 12 10 8 574.17 159.81 -12 -10 -8 785.65 185.90 -12 -10 -8 758.66 163.99 12 10 9 5535.94 403.17 12 10 9 5461.17 402.13 -12 -10 -9 5904.49 417.17 -12 -10 -9 5268.85 389.50 12 10 10 214.41 143.23 12 10 10 64.01 138.30 -12 -10 -10 -22.80 138.00 -12 -10 -10 -90.23 136.19 12 10 11 3868.98 343.71 12 10 11 4593.18 372.41 -12 -10 -11 4500.12 292.34 -12 -10 -11 4144.11 357.89 12 10 12 360.83 113.75 12 10 12 158.41 176.11 -12 -10 -12 320.12 115.91 -12 -10 -12 165.78 168.35 12 10 13 1852.79 269.50 12 10 13 1928.54 273.57 -12 -10 -13 1913.08 270.78 -12 -10 -13 1935.83 271.92 12 10 14 388.07 159.65 12 10 14 -174.72 161.87 -12 -10 -14 177.71 170.36 -12 -10 -14 89.14 169.67 12 10 15 652.25 131.17 12 10 15 488.71 200.78 -12 -10 -15 469.44 200.17 -12 -10 -15 671.94 199.76 12 11 -8 5038.02 349.42 12 11 -8 4848.32 198.57 -12 -11 8 5026.98 364.90 -12 -11 8 5693.69 231.55 12 11 -7 -63.68 114.36 12 11 -7 -5.63 41.35 -12 -11 7 142.22 114.75 -12 -11 7 47.89 46.82 12 11 -6 2160.40 220.37 12 11 -6 1758.23 111.06 -12 -11 6 2207.90 220.69 -12 -11 6 2159.89 125.08 12 11 -5 608.25 159.44 12 11 -5 471.11 76.92 -12 -11 5 510.32 150.28 -12 -11 5 517.09 70.25 12 11 -4 606.19 163.21 12 11 -4 555.65 85.12 -12 -11 4 692.13 152.07 -12 -11 4 656.89 89.85 12 11 -3 156.35 130.55 12 11 -3 126.17 77.68 -12 -11 3 182.11 121.55 -12 -11 3 30.59 66.92 12 11 -2 -3.92 122.84 12 11 -2 21.23 65.36 -12 -11 2 51.98 112.13 -12 -11 2 59.54 74.14 12 11 -1 -60.77 130.97 12 11 -1 92.18 95.73 -12 -11 1 168.04 114.30 -12 -11 1 66.38 86.71 12 11 0 385.81 154.68 12 11 0 460.10 114.92 -12 -11 0 470.40 140.18 -12 -11 0 344.57 108.46 12 11 1 650.05 166.85 12 11 1 853.67 140.71 -12 -11 -1 858.58 164.28 -12 -11 -1 732.37 139.28 12 11 2 627.04 157.55 12 11 2 383.52 97.43 -12 -11 -2 225.79 141.17 -12 -11 -2 512.54 107.75 12 11 3 397.76 154.59 12 11 3 500.21 106.50 -12 -11 -3 288.37 146.50 -12 -11 -3 368.52 138.83 12 11 4 601.28 155.85 12 11 4 386.22 111.95 -12 -11 -4 334.62 149.34 -12 -11 -4 319.30 112.62 12 11 5 302.63 148.74 12 11 5 106.32 115.35 -12 -11 -5 161.48 146.71 -12 -11 -5 367.49 118.20 12 11 6 414.61 155.15 12 11 6 147.96 130.18 -12 -11 -6 557.59 156.47 -12 -11 -6 421.92 163.09 12 11 7 2581.70 264.09 12 11 7 2290.41 222.37 -12 -11 -7 2478.43 262.83 -12 -11 -7 1850.32 281.99 12 11 8 2812.96 271.62 12 11 8 1910.92 227.00 -12 -11 -8 2474.82 261.83 -12 -11 -8 2111.25 230.85 12 11 9 1286.13 219.35 12 11 9 1226.40 198.37 -12 -11 -9 1252.82 216.36 -12 -11 -9 1146.49 202.29 12 11 10 4138.77 354.89 12 11 10 3600.44 321.41 -12 -11 -10 3989.63 364.66 -12 -11 -10 3882.03 326.24 12 11 11 1792.96 263.89 12 11 11 1953.22 250.76 -12 -11 -11 1969.91 263.18 -12 -11 -11 2261.32 321.61 12 11 12 1588.49 256.91 12 11 12 2184.80 257.84 -12 -11 -12 1527.25 260.91 -12 -11 -12 1867.15 258.98 12 11 13 2804.47 306.44 12 11 13 2320.40 300.65 -12 -11 -13 2925.14 315.28 -12 -11 -13 2675.92 299.27 12 11 14 1191.64 234.94 12 11 14 1300.16 224.00 -12 -11 -14 832.83 240.00 -12 -11 -14 752.10 229.79 12 12 -7 899.74 177.54 12 12 -7 686.60 55.22 -12 -12 7 1163.65 240.63 -12 -12 7 716.43 47.89 12 12 -6 1317.92 262.64 12 12 -6 1315.00 65.56 -12 -12 6 1311.36 205.93 -12 -12 6 1361.18 84.62 12 12 -5 3215.01 267.42 12 12 -5 2180.93 100.35 -12 -12 5 2670.65 252.22 12 12 -4 551.61 154.75 -12 -12 4 445.91 194.75 -12 -12 4 295.39 57.81 12 12 -3 1900.95 297.37 12 12 -3 1824.64 106.54 -12 -12 3 1741.57 218.27 -12 -12 3 1857.86 124.44 12 12 -2 996.05 189.23 12 12 -2 739.06 94.51 -12 -12 2 599.24 168.05 -12 -12 2 699.02 91.44 12 12 -1 275.60 151.23 12 12 -1 196.62 78.56 -12 -12 1 318.09 139.28 -12 -12 1 195.72 90.00 12 12 0 1569.39 216.13 12 12 0 1350.31 137.40 -12 -12 0 1197.60 195.42 -12 -12 0 1062.74 142.44 12 12 1 1447.97 226.05 12 12 1 1432.69 151.33 -12 -12 -1 1107.44 205.96 -12 -12 -1 1296.97 160.36 12 12 2 2683.61 278.90 12 12 2 2494.15 206.29 -12 -12 -2 2458.01 265.09 -12 -12 -2 2819.09 232.26 12 12 3 1272.92 209.53 12 12 3 1030.41 128.83 -12 -12 -3 1008.57 199.09 -12 -12 -3 1259.67 180.46 12 12 4 1646.07 230.45 12 12 4 1435.38 185.70 -12 -12 -4 1415.06 211.67 -12 -12 -4 1515.16 205.42 12 12 5 2471.52 257.91 12 12 5 2343.31 196.55 -12 -12 -5 1621.90 245.93 -12 -12 -5 1955.51 189.06 12 12 6 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1311.69 218.52 13 2 -3 3415.69 356.51 -13 -2 3 3957.37 339.80 13 2 -2 2149.35 89.20 13 2 -2 2007.77 84.01 13 2 -2 2422.78 303.63 -13 -2 2 2069.07 272.19 13 2 -1 1841.54 96.65 13 2 -1 1414.78 82.38 13 2 -1 1524.46 261.00 -13 -2 1 1987.11 253.80 13 2 0 3347.79 168.29 13 2 0 2798.38 145.91 13 2 0 3777.65 361.26 -13 -2 0 3748.57 322.16 13 2 1 8.09 73.29 13 2 1 23.47 60.68 13 2 1 64.45 165.55 -13 -2 -1 202.92 143.57 13 2 2 152.19 91.03 13 2 2 460.64 171.69 -13 -2 -2 -218.01 157.62 13 2 3 597.22 123.05 13 2 3 775.28 217.20 -13 -2 -3 604.77 182.11 13 2 4 285.64 125.89 13 2 4 277.95 199.98 -13 -2 -4 346.13 127.46 -13 -2 -4 438.98 179.96 13 2 5 2088.59 179.86 13 2 5 2209.33 299.55 -13 -2 -5 2201.49 177.33 -13 -2 -5 1941.04 272.49 13 2 6 -14.95 100.18 13 2 6 47.95 177.45 -13 -2 -6 130.33 103.94 -13 -2 -6 319.43 160.79 13 2 7 2209.78 206.51 13 2 7 2711.53 334.51 -13 -2 -7 2486.21 266.18 -13 -2 -7 2293.26 286.09 13 2 8 199.59 113.58 13 2 8 257.78 203.32 -13 -2 -8 290.97 132.69 -13 -2 -8 -15.55 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388.89 135.58 13 5 -4 15.65 55.54 13 5 -4 -177.92 119.31 -13 -5 4 -28.49 49.86 -13 -5 4 94.05 110.28 13 5 -3 127.50 57.47 13 5 -3 168.54 126.23 -13 -5 3 93.01 52.76 -13 -5 3 152.57 116.12 13 5 -2 2198.79 142.51 13 5 -2 2218.03 256.57 -13 -5 2 2526.25 147.25 -13 -5 2 2374.37 223.92 13 5 -1 -27.84 75.25 13 5 -1 4.35 135.39 -13 -5 1 -40.31 68.44 -13 -5 1 221.80 112.04 13 5 0 7346.44 368.76 13 5 0 7171.66 488.85 -13 -5 0 7327.53 359.24 -13 -5 0 7171.24 436.97 13 5 1 256.49 101.77 13 5 1 44.73 159.83 -13 -5 -1 377.32 102.16 -13 -5 -1 166.97 139.79 13 5 2 4724.49 304.83 13 5 2 4616.96 387.80 -13 -5 -2 5317.65 298.72 -13 -5 -2 4544.13 352.64 13 5 3 1412.01 140.28 13 5 3 1568.17 236.06 -13 -5 -3 1486.27 167.20 -13 -5 -3 1574.31 209.04 13 5 4 2600.45 204.94 13 5 4 2936.42 302.83 -13 -5 -4 3124.01 200.40 -13 -5 -4 2835.94 275.49 13 5 5 669.81 120.54 13 5 5 382.32 182.22 -13 -5 -5 476.59 154.46 -13 -5 -5 563.60 162.75 13 5 6 2832.31 212.77 13 5 6 2459.54 279.39 -13 -5 -6 1949.46 203.34 -13 -5 -6 2504.68 271.44 13 5 7 -22.19 109.21 13 5 7 234.90 148.92 -13 -5 -7 189.29 109.08 -13 -5 -7 45.47 158.24 13 5 8 498.58 142.72 13 5 8 855.73 178.82 -13 -5 -8 457.75 136.07 -13 -5 -8 193.22 184.80 13 5 9 581.69 136.09 13 5 9 288.35 191.08 -13 -5 -9 417.37 138.73 -13 -5 -9 469.03 193.07 13 5 10 129.71 119.94 13 5 10 269.58 160.11 -13 -5 -10 97.43 124.75 -13 -5 -10 -132.15 156.85 13 5 11 634.64 212.69 13 5 11 559.27 135.42 -13 -5 -11 704.20 158.03 -13 -5 -11 508.52 129.17 13 5 12 -193.13 131.78 13 5 12 199.37 166.60 -13 -5 -12 152.72 134.86 -13 -5 -12 106.94 166.47 13 6 -10 1163.18 133.35 13 6 -10 1249.89 173.52 -13 -6 10 1270.00 112.48 -13 -6 10 1139.30 167.23 13 6 -9 588.82 99.71 13 6 -9 683.71 134.39 -13 -6 9 457.65 97.18 -13 -6 9 495.65 137.54 13 6 -8 3603.13 206.75 13 6 -8 4128.23 359.65 -13 -6 8 4302.33 206.62 -13 -6 8 4317.70 295.45 13 6 -7 1344.39 122.26 13 6 -7 1379.96 181.53 -13 -6 7 1308.01 107.51 -13 -6 7 1519.88 177.74 13 6 -6 3454.25 190.22 13 6 -6 3013.33 258.19 -13 -6 6 3223.61 167.10 -13 -6 6 3042.58 249.04 13 6 -5 1350.09 124.91 13 6 -5 1605.07 197.71 -13 -6 5 1564.38 126.51 -13 -6 5 1496.49 226.60 13 6 -4 3274.32 198.43 13 6 -4 3146.49 277.44 -13 -6 4 3088.95 192.60 -13 -6 4 3434.99 298.30 13 6 -3 619.38 108.80 13 6 -3 918.44 201.19 -13 -6 3 659.11 93.51 -13 -6 3 855.24 148.99 13 6 -2 402.18 99.10 13 6 -2 -106.75 145.23 -13 -6 2 232.70 89.78 -13 -6 2 227.28 125.71 13 6 -1 1836.47 172.97 13 6 -1 1858.43 232.10 -13 -6 1 1966.49 164.54 -13 -6 1 2041.06 208.25 13 6 0 1672.08 177.03 13 6 0 2387.37 238.57 -13 -6 0 1994.79 168.13 -13 -6 0 2151.29 216.48 13 6 1 1562.74 137.04 13 6 1 1610.32 216.90 -13 -6 -1 1326.27 135.65 -13 -6 -1 1697.38 200.51 13 6 2 2438.67 226.65 13 6 2 2890.34 261.44 -13 -6 -2 2686.87 210.32 -13 -6 -2 2505.64 241.01 13 6 3 1232.12 138.14 13 6 3 934.17 195.98 -13 -6 -3 1024.98 124.09 -13 -6 -3 953.90 178.91 13 6 4 1878.48 203.41 13 6 4 1635.27 217.59 -13 -6 -4 1337.38 196.54 -13 -6 -4 1356.16 205.37 13 6 5 510.00 122.37 13 6 5 318.45 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-6 5 481.06 85.51 -14 -6 5 590.34 148.90 14 6 -4 1215.90 120.10 14 6 -4 1299.52 250.40 -14 -6 4 1451.99 118.38 -14 -6 4 1297.74 187.12 14 6 -3 64.75 84.81 14 6 -3 282.48 137.49 -14 -6 3 122.23 78.32 -14 -6 3 0.74 133.85 14 6 -2 212.32 95.95 14 6 -2 220.97 148.86 -14 -6 2 80.53 85.37 -14 -6 2 277.45 126.73 14 6 -1 287.14 106.64 14 6 -1 501.70 169.36 -14 -6 1 405.60 102.87 -14 -6 1 343.07 143.36 14 6 0 767.95 131.55 14 6 0 653.57 197.65 -14 -6 0 828.68 121.91 -14 -6 0 866.66 169.26 14 6 1 805.04 110.69 14 6 1 984.74 200.48 -14 -6 -1 1048.15 112.83 -14 -6 -1 845.86 175.75 14 6 2 2147.89 200.76 14 6 2 1933.61 256.29 -14 -6 -2 1780.26 196.48 -14 -6 -2 1866.17 229.95 14 6 3 3507.32 237.47 14 6 3 3563.14 333.46 -14 -6 -3 3269.49 215.72 -14 -6 -3 3403.55 306.41 14 6 4 1320.54 153.00 14 6 4 1637.84 247.23 -14 -6 -4 1616.81 159.99 -14 -6 -4 1424.97 285.30 14 6 5 6226.93 440.08 14 6 5 6538.22 495.36 -14 -6 -5 6639.40 435.01 -14 -6 -5 6154.74 444.29 14 6 6 102.81 107.83 14 6 6 37.36 156.16 -14 -6 -6 9.99 106.00 -14 -6 -6 272.12 149.74 14 6 7 1453.54 187.75 14 6 7 1649.25 250.03 -14 -6 -7 1208.65 224.96 -14 -6 -7 1065.81 216.89 14 6 8 51.66 120.74 14 6 8 238.74 160.81 -14 -6 -8 39.49 124.19 -14 -6 -8 116.09 98.02 14 7 -5 3461.96 222.78 -14 -7 5 3651.75 222.72 -14 -7 5 3872.24 330.72 14 7 -4 567.41 129.99 14 7 -4 788.45 166.80 -14 -7 4 908.82 126.09 -14 -7 4 1057.95 155.26 14 7 -3 595.68 118.52 14 7 -3 496.64 154.67 -14 -7 3 549.02 116.41 -14 -7 3 389.14 134.17 14 7 -2 94.77 109.45 14 7 -2 257.94 144.29 -14 -7 2 256.85 106.65 -14 -7 2 162.19 163.22 14 7 -1 349.73 123.42 14 7 -1 235.27 160.23 -14 -7 1 364.80 115.65 -14 -7 1 564.98 130.33 14 7 0 419.87 132.09 14 7 0 395.29 150.57 -14 -7 0 489.18 94.81 -14 -7 0 199.67 140.04 14 7 1 315.38 123.06 14 7 1 -136.09 152.37 -14 -7 -1 179.63 88.07 -14 -7 -1 169.48 130.74 14 7 2 3845.04 292.81 14 7 2 4160.01 348.25 -14 -7 -2 3739.90 283.31 -14 -7 -2 3830.65 300.00 14 7 3 52.04 92.75 14 7 3 -58.62 138.74 -14 -7 -3 -120.14 93.37 -14 -7 -3 30.14 124.17 14 7 4 4139.55 273.39 14 7 4 3714.59 343.90 -14 -7 -4 3861.66 252.01 -14 -7 -4 4190.45 332.51 14 7 5 211.32 118.33 14 7 5 279.40 160.67 -14 -7 -5 98.88 114.80 -14 -7 -5 251.80 149.04 14 7 6 4547.62 327.05 14 7 6 4272.89 375.87 -14 -7 -6 4779.95 315.99 -14 -7 -6 5477.89 389.74 14 7 7 637.13 150.38 14 7 7 819.53 199.27 -14 -7 -7 471.16 148.90 -14 -7 -7 536.06 184.76 14 7 8 1958.08 287.58 14 7 8 1973.00 275.25 -14 -7 -8 2233.79 221.82 -14 -7 -8 1898.93 262.67 14 7 9 194.74 136.05 14 7 9 179.52 169.68 -14 -7 -9 15.68 133.89 -14 -7 -9 233.86 158.65 14 8 -5 1115.95 149.27 14 8 -5 1388.78 175.33 -14 -8 5 932.22 143.86 -14 -8 5 1123.59 153.37 14 8 -4 3832.89 234.98 14 8 -4 3695.05 276.24 -14 -8 4 3605.67 256.65 -14 -8 4 3877.97 322.14 14 8 -3 1456.31 187.15 14 8 -3 1722.88 203.80 -14 -8 3 1704.63 180.29 -14 -8 3 1603.74 223.47 14 8 -2 4094.47 256.85 14 8 -2 4260.08 302.11 -14 -8 2 3924.56 290.16 -14 -8 2 3896.17 285.80 14 8 -1 900.20 177.25 14 8 -1 1246.65 238.41 -14 -8 1 1046.78 130.05 -14 -8 1 1221.32 167.40 14 8 0 1024.34 184.28 14 8 0 1165.22 192.79 -14 -8 0 1130.36 181.27 -14 -8 0 1616.60 224.27 14 8 1 1953.35 234.84 14 8 1 2186.38 307.76 -14 -8 -1 2315.33 234.32 -14 -8 -1 2408.49 215.77 14 8 2 545.10 124.00 14 8 2 252.99 161.71 -14 -8 -2 478.64 122.04 -14 -8 -2 428.44 144.31 14 8 3 1750.97 175.31 14 8 3 1595.44 227.50 -14 -8 -3 1410.74 171.03 -14 -8 -3 1701.31 253.83 14 8 4 885.71 154.75 14 8 4 1144.92 252.72 -14 -8 -4 865.99 143.25 -14 -8 -4 841.03 178.09 14 8 5 1038.79 165.94 14 8 5 1409.73 195.57 -14 -8 -5 1194.57 220.17 -14 -8 -5 1209.42 181.89 14 8 6 1523.28 246.91 14 8 6 1477.28 224.73 -14 -8 -6 1777.86 190.99 -14 -8 -6 1702.55 272.06 14 8 7 370.47 181.90 14 8 7 156.58 169.34 -14 -8 -7 304.02 180.50 -14 -8 -7 358.72 155.74 14 8 8 1482.55 209.94 14 8 8 1449.42 239.52 -14 -8 -8 1037.97 190.45 -14 -8 -8 1413.35 221.17 14 8 9 296.25 208.11 14 8 9 562.80 193.44 -14 -8 -9 249.42 159.42 -14 -8 -9 570.93 173.32 14 9 -4 2941.62 261.88 14 9 -4 3194.11 232.20 -14 -9 4 2475.31 244.60 -14 -9 4 3166.25 213.57 14 9 -3 86.79 115.10 14 9 -3 242.51 163.47 -14 -9 3 453.09 108.43 -14 -9 3 220.26 110.06 14 9 -2 6151.13 376.40 14 9 -2 6703.17 470.54 -14 -9 2 6394.81 413.10 -14 -9 2 6606.94 369.86 14 9 -1 1342.06 213.45 14 9 -1 1285.15 243.80 -14 -9 1 1514.70 162.45 -14 -9 1 1318.52 210.62 14 9 0 5053.34 334.78 14 9 0 5413.48 438.05 -14 -9 0 5064.15 319.74 -14 -9 0 5533.11 326.45 14 9 1 153.71 145.53 14 9 1 1.76 119.88 -14 -9 -1 54.66 98.81 -14 -9 -1 87.57 143.08 14 9 2 3956.94 347.94 14 9 2 3593.00 373.87 -14 -9 -2 4361.08 293.80 -14 -9 -2 4299.01 353.08 14 9 3 1244.42 165.28 14 9 3 1125.92 191.32 -14 -9 -3 890.92 162.04 -14 -9 -3 1067.17 173.88 14 9 4 -3.02 108.55 -14 -9 -4 12.92 109.36 -14 -9 -4 -157.58 114.78 14 9 5 1301.67 176.87 14 9 5 1324.91 245.92 -14 -9 -5 979.06 176.97 -14 -9 -5 1104.32 187.93 14 9 6 32.72 180.83 14 9 6 59.07 152.77 -14 -9 -6 333.51 132.49 -14 -9 -6 380.27 148.28 14 9 7 689.48 168.87 14 9 7 835.61 240.37 -14 -9 -7 819.57 168.66 -14 -9 -7 605.09 180.52 14 9 8 61.79 141.17 14 9 8 357.40 155.50 -14 -9 -8 56.12 141.54 -14 -9 -8 297.13 148.35 14 10 -2 85.57 138.69 14 10 -2 74.94 129.44 -14 -10 2 10.03 97.82 -14 -10 2 -35.74 85.29 14 10 -1 3258.05 264.91 14 10 -1 3619.74 308.46 -14 -10 1 3580.42 262.87 -14 -10 1 3033.76 226.44 14 10 0 170.22 138.99 14 10 0 530.67 136.63 -14 -10 0 341.13 132.83 -14 -10 0 416.46 119.93 14 10 1 5344.57 371.69 14 10 1 6119.74 383.74 -14 -10 -1 5342.26 368.01 -14 -10 -1 5674.81 394.37 14 10 2 1109.28 239.51 14 10 2 1363.84 230.24 -14 -10 -2 1206.73 176.80 -14 -10 -2 1041.50 161.95 14 10 3 1157.88 179.89 14 10 3 1016.52 167.83 -14 -10 -3 996.93 220.43 -14 -10 -3 1010.07 158.44 14 10 4 364.19 194.25 14 10 4 577.85 154.27 -14 -10 -4 348.98 152.86 -14 -10 -4 696.31 189.42 14 10 5 60.67 126.97 14 10 5 -104.28 121.52 -14 -10 -5 231.18 127.42 -14 -10 -5 333.58 160.23 14 10 6 -49.86 123.79 14 10 6 -151.67 113.92 -14 -10 -6 121.25 124.33 -14 -10 -6 218.12 128.02 14 10 7 115.37 193.97 14 10 7 210.65 146.58 -14 -10 -7 179.52 131.24 -14 -10 -7 105.69 141.74 14 11 0 -36.68 135.93 14 11 0 -8.07 138.52 -14 -11 0 144.26 118.85 -14 -11 0 213.74 121.12 14 11 1 2851.60 331.21 14 11 1 2410.13 267.31 -14 -11 -1 2751.38 247.43 -14 -11 -1 2478.15 244.77 14 11 2 55.90 123.01 14 11 2 241.90 134.18 -14 -11 -2 -83.97 122.29 -14 -11 -2 -106.68 128.14 14 11 3 2558.02 261.64 14 11 3 2534.18 227.96 -14 -11 -3 2722.73 259.21 -14 -11 -3 2654.12 262.39 14 11 4 137.73 179.52 14 11 4 38.36 157.68 -14 -11 -4 275.75 132.29 -14 -11 -4 19.39 116.20 14 11 5 322.19 194.60 14 11 5 353.39 176.97 -14 -11 -5 205.33 156.71 -14 -11 -5 312.91 133.07 ; _shelx_hkl_checksum 2222 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 +X,+Y,+Z 2 -X,-Y,-Z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pd1 Pd 0.40545(2) 0.64688(2) 0.69084(2) 0.00958(6) Uani 1 1 d . . . . . Pd2 Pd 0.15895(2) 0.69365(2) 0.73988(2) 0.00940(6) Uani 1 1 d . . . . . Pd3 Pd 0.36775(2) 0.50009(2) 0.79582(2) 0.00951(6) Uani 1 1 d . . . . . P1 P 0.54080(9) 0.68852(8) 0.61862(5) 0.01404(18) Uani 1 1 d . . . . . P2 P -0.05105(8) 0.81329(8) 0.73782(5) 0.01322(18) Uani 1 1 d . . . . . P3 P 0.45177(9) 0.36352(8) 0.88396(5) 0.01395(18) Uani 1 1 d . . . . . Si1 Si 0.21440(9) 0.81733(9) 0.65383(5) 0.0133(2) Uani 1 1 d . . . . . Si2 Si 0.14509(9) 0.54421(9) 0.82409(5) 0.0140(2) Uani 1 1 d . . . . . Si3 Si 0.57365(9) 0.46996(9) 0.74286(5) 0.01312(19) Uani 1 1 d . . . . . O1 O 0.6914(2) 0.6411(2) 0.64241(13) 0.0168(5) Uani 1 1 d . . . . . O2 O 0.5605(3) 0.6379(2) 0.54612(14) 0.0190(6) Uani 1 1 d . . . . . O3 O 0.5085(3) 0.8257(2) 0.59212(15) 0.0222(6) Uani 1 1 d . . . . . O4 O -0.1091(2) 0.9077(2) 0.66961(14) 0.0214(6) Uani 1 1 d . . . . . O5 O -0.1583(2) 0.7601(2) 0.74748(14) 0.0187(6) Uani 1 1 d . . . . . O6 O -0.0964(2) 0.8994(2) 0.79694(14) 0.0208(6) Uani 1 1 d . . . . . O7 O 0.3583(2) 0.3185(2) 0.93423(14) 0.0182(6) Uani 1 1 d . . . . . O8 O 0.5123(3) 0.4095(2) 0.93893(14) 0.0173(5) Uani 1 1 d . . . . . O9 O 0.5739(2) 0.2381(2) 0.87387(13) 0.0167(5) Uani 1 1 d . . . . . C1 C 0.7797(3) 0.6711(4) 0.59428(19) 0.0175(8) Uani 1 1 d . . . . . H1A H 0.8599 0.5986 0.5870 0.021 Uiso 1 1 calc R U . . . H1B H 0.8066 0.7247 0.6140 0.021 Uiso 1 1 calc R U . . . C2 C 0.6621(4) 0.6495(4) 0.49974(19) 0.0184(8) Uani 1 1 d . . . . . H2A H 0.6257 0.6825 0.4527 0.022 Uiso 1 1 calc R U . . . H2B H 0.7361 0.5708 0.4972 0.022 Uiso 1 1 calc R U . . . C3 C 0.5939(4) 0.8441(3) 0.5380(2) 0.0197(8) Uani 1 1 d . . . . . H3A H 0.6248 0.9005 0.5506 0.024 Uiso 1 1 calc R U . . . H3B H 0.5433 0.8795 0.4947 0.024 Uiso 1 1 calc R U . . . C4 C 0.7123(3) 0.7306(3) 0.52554(19) 0.0161(7) Uani 1 1 d . . . . . C5 C 0.8041(4) 0.7601(3) 0.4726(2) 0.0196(8) Uani 1 1 d . . . . . H5A H 0.7526 0.8060 0.4308 0.024 Uiso 1 1 calc R U . . . H5B H 0.8344 0.8115 0.4923 0.024 Uiso 1 1 calc R U . . . C6 C 0.9242(4) 0.6549(4) 0.4510(2) 0.0266(9) Uani 1 1 d . . . . . H6A H 0.8958 0.6042 0.4302 0.032 Uiso 1 1 calc R U . . . H6B H 0.9780 0.6100 0.4917 0.032 Uiso 1 1 calc R U . . . H6C H 0.9762 0.6826 0.4172 0.032 Uiso 1 1 calc R U . . . C7 C -0.2436(3) 0.9953(3) 0.6731(2) 0.0187(8) Uani 1 1 d . . . . . H7A H -0.2931 0.9948 0.6334 0.022 Uiso 1 1 calc R U . . . H7B H -0.2454 1.0744 0.6700 0.022 Uiso 1 1 calc R U . . . C8 C -0.2963(3) 0.8453(3) 0.7471(2) 0.0194(8) Uani 1 1 d . . . . . H8A H -0.3397 0.8285 0.7904 0.023 Uiso 1 1 calc R U . . . H8B H -0.3413 0.8374 0.7078 0.023 Uiso 1 1 calc R U . . . C9 C -0.2350(3) 0.9783(4) 0.8002(2) 0.0195(8) Uani 1 1 d . . . . . H9A H -0.2457 1.0602 0.7983 0.023 Uiso 1 1 calc R U . . . H9B H -0.2725 0.9578 0.8447 0.023 Uiso 1 1 calc R U . . . C10 C -0.3095(3) 0.9705(3) 0.74075(19) 0.0142(7) Uani 1 1 d . . . . . C11 C -0.4549(3) 1.0611(4) 0.7450(2) 0.0199(8) Uani 1 1 d . . . . . H11A H -0.4961 1.0344 0.7860 0.024 Uiso 1 1 calc R U . . . H11B H -0.4572 1.1374 0.7523 0.024 Uiso 1 1 calc R U . . . C12 C -0.5381(4) 1.0818(4) 0.6817(2) 0.0246(9) Uani 1 1 d . . . . . H12A H -0.6307 1.1316 0.6917 0.030 Uiso 1 1 calc R U . . . H12B H -0.5293 1.0059 0.6707 0.030 Uiso 1 1 calc R U . . . H12C H -0.5078 1.1210 0.6422 0.030 Uiso 1 1 calc R U . . . C13 C 0.4129(4) 0.2527(3) 1.00084(19) 0.0178(8) Uani 1 1 d . . . . . H13A H 0.3941 0.1828 1.0103 0.021 Uiso 1 1 calc R U . . . H13B H 0.3711 0.3030 1.0379 0.021 Uiso 1 1 calc R U . . . C14 C 0.5859(4) 0.3230(3) 0.99585(19) 0.0175(7) Uani 1 1 d . . . . . H14A H 0.5588 0.3577 1.0397 0.021 Uiso 1 1 calc R U . . . H14B H 0.6811 0.3008 0.9886 0.021 Uiso 1 1 calc R U . . . C15 C 0.6194(4) 0.1544(3) 0.93636(19) 0.0168(7) Uani 1 1 d . . . . . H15A H 0.7167 0.1200 0.9382 0.020 Uiso 1 1 calc R U . . . H15B H 0.5939 0.0895 0.9352 0.020 Uiso 1 1 calc R U . . . C16 C 0.5612(3) 0.2135(3) 1.00067(18) 0.0141(7) Uani 1 1 d . . . . . C17 C 0.6244(4) 0.1330(4) 1.0669(2) 0.0210(8) Uani 1 1 d . . . . . H17A H 0.7155 0.1245 1.0691 0.025 Uiso 1 1 calc R U . . . H17B H 0.5752 0.1722 1.1070 0.025 Uiso 1 1 calc R U . . . C18 C 0.6292(5) 0.0098(4) 1.0746(2) 0.0329(10) Uani 1 1 d . . . . . H18A H 0.6793 -0.0311 1.0358 0.039 Uiso 1 1 calc R U . . . H18B H 0.5394 0.0165 1.0746 0.039 Uiso 1 1 calc R U . . . H18C H 0.6720 -0.0349 1.1182 0.039 Uiso 1 1 calc R U . . . C19 C 0.1456(4) 0.8493(4) 0.5636(2) 0.0214(8) Uani 1 1 d . . . . . H19 H 0.0533 0.9122 0.5650 0.026 Uiso 1 1 calc R U . . . C20 C 0.1380(6) 0.7407(5) 0.5436(2) 0.0455(14) Uani 1 1 d . . . . . H20A H 0.2272 0.6796 0.5371 0.055 Uiso 1 1 calc R U . . . H20B H 0.0889 0.7623 0.5005 0.055 Uiso 1 1 calc R U . . . H20C H 0.0930 0.7104 0.5804 0.055 Uiso 1 1 calc R U . . . C21 C 0.2196(4) 0.8953(4) 0.5081(2) 0.0284(10) Uani 1 1 d . . . . . H21A H 0.1747 0.9150 0.4637 0.034 Uiso 1 1 calc R U . . . H21B H 0.3098 0.8345 0.5038 0.034 Uiso 1 1 calc R U . . . H21C H 0.2219 0.9660 0.5210 0.034 Uiso 1 1 calc R U . . . C22 C 0.2087(4) 0.9598(3) 0.6767(2) 0.0177(8) Uani 1 1 d . . . . . H22 H 0.2676 0.9821 0.6431 0.021 Uiso 1 1 calc R U . . . C23 C 0.2660(5) 0.9378(4) 0.7486(2) 0.0316(10) Uani 1 1 d . . . . . H23A H 0.2644 1.0109 0.7600 0.038 Uiso 1 1 calc R U . . . H23B H 0.3571 0.8768 0.7492 0.038 Uiso 1 1 calc R U . . . H23C H 0.2135 0.9114 0.7827 0.038 Uiso 1 1 calc R U . . . C24 C 0.0722(4) 1.0643(4) 0.6716(3) 0.0307(10) Uani 1 1 d . . . . . H24A H 0.0788 1.1350 0.6814 0.037 Uiso 1 1 calc R U . . . H24B H 0.0125 1.0469 0.7053 0.037 Uiso 1 1 calc R U . . . H24C H 0.0379 1.0780 0.6249 0.037 Uiso 1 1 calc R U . . . C25 C 0.0777(4) 0.4464(3) 0.7933(2) 0.0198(8) Uani 1 1 d . . . . . H25 H -0.0164 0.4752 0.8088 0.024 Uiso 1 1 calc R U . . . C26 C 0.0796(5) 0.4545(5) 0.7148(2) 0.0372(11) Uani 1 1 d . . . . . H26A H 0.0611 0.3919 0.7014 0.045 Uiso 1 1 calc R U . . . H26B H 0.1665 0.4455 0.6970 0.045 Uiso 1 1 calc R U . . . H26C H 0.0123 0.5315 0.6955 0.045 Uiso 1 1 calc R U . . . C27 C 0.1496(5) 0.3177(4) 0.8248(3) 0.0317(10) Uani 1 1 d . . . . . H27A H 0.2414 0.2855 0.8087 0.038 Uiso 1 1 calc R U . . . H27B H 0.1066 0.2722 0.8106 0.038 Uiso 1 1 calc R U . . . H27C H 0.1471 0.3129 0.8753 0.038 Uiso 1 1 calc R U . . . C28 C 0.0763(4) 0.5662(4) 0.9153(2) 0.0193(8) Uani 1 1 d . . . . . H28 H 0.0845 0.4878 0.9386 0.023 Uiso 1 1 calc R U . . . C29 C -0.0695(4) 0.6516(4) 0.9170(2) 0.0260(9) Uani 1 1 d . . . . . H29A H -0.0810 0.7312 0.8980 0.031 Uiso 1 1 calc R U . . . H29B H -0.1019 0.6518 0.9649 0.031 Uiso 1 1 calc R U . . . H29C H -0.1193 0.6266 0.8893 0.031 Uiso 1 1 calc R U . . . C30 C 0.1554(4) 0.6037(5) 0.9575(2) 0.0347(11) Uani 1 1 d . . . . . H30A H 0.1385 0.6856 0.9409 0.042 Uiso 1 1 calc R U . . . H30B H 0.2495 0.5524 0.9526 0.042 Uiso 1 1 calc R U . . . H30C H 0.1294 0.5974 1.0063 0.042 Uiso 1 1 calc R U . . . C31 C 0.6505(4) 0.3420(3) 0.6899(2) 0.0187(8) Uani 1 1 d . . . . . H31 H 0.6804 0.2675 0.7230 0.022 Uiso 1 1 calc R U . . . C32 C 0.5484(4) 0.3421(4) 0.6428(2) 0.0264(9) Uani 1 1 d . . . . . H32A H 0.5870 0.2708 0.6197 0.032 Uiso 1 1 calc R U . . . H32B H 0.5206 0.4120 0.6080 0.032 Uiso 1 1 calc R U . . . H32C H 0.4719 0.3435 0.6705 0.032 Uiso 1 1 calc R U . . . C33 C 0.7707(4) 0.3393(4) 0.6474(2) 0.0270(9) Uani 1 1 d . . . . . H33A H 0.8122 0.2660 0.6263 0.032 Uiso 1 1 calc R U . . . H33B H 0.8339 0.3430 0.6776 0.032 Uiso 1 1 calc R U . . . H33C H 0.7431 0.4070 0.6110 0.032 Uiso 1 1 calc R U . . . C34 C 0.7111(4) 0.4759(4) 0.7900(2) 0.0190(8) Uani 1 1 d . . . . . H34 H 0.7681 0.4962 0.7541 0.023 Uiso 1 1 calc R U . . . C35 C 0.7984(4) 0.3591(4) 0.8312(2) 0.0296(10) Uani 1 1 d . . . . . H35A H 0.7466 0.3383 0.8685 0.035 Uiso 1 1 calc R U . . . H35B H 0.8715 0.3661 0.8510 0.035 Uiso 1 1 calc R U . . . H35C H 0.8333 0.2974 0.8006 0.035 Uiso 1 1 calc R U . . . C36 C 0.6540(5) 0.5749(4) 0.8351(2) 0.0329(11) Uani 1 1 d . . . . . H36A H 0.5965 0.6483 0.8073 0.039 Uiso 1 1 calc R U . . . H36B H 0.7258 0.5852 0.8540 0.039 Uiso 1 1 calc R U . . . H36C H 0.6030 0.5549 0.8732 0.039 Uiso 1 1 calc R U . . . C37 C 0.0086(8) 1.0611(7) 0.8851(4) 0.0245(17) Uiso 0.5 1 d . . P . . C38 C 0.0010(11) 0.9498(11) 0.9343(6) 0.047(3) Uiso 0.5 1 d . . P . . C39 C -0.0002(10) 1.0246(10) 0.9459(6) 0.042(2) Uiso 0.5 1 d . . P . . C40 C -0.0105(8) 0.9183(7) 0.9846(4) 0.0208(16) Uiso 0.5 1 d . . P . . C41 C -0.0206(11) 0.8874(11) 1.0397(6) 0.049(3) Uiso 0.5 1 d . . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pd1 0.00651(11) 0.00985(13) 0.01099(13) 0.00000(10) 0.00090(9) -0.00282(10) Pd2 0.00667(11) 0.01099(13) 0.00944(13) 0.00049(10) 0.00021(9) -0.00339(10) Pd3 0.00642(11) 0.01122(13) 0.01048(13) 0.00084(10) -0.00063(9) -0.00403(10) P1 0.0113(4) 0.0145(4) 0.0154(5) -0.0007(4) 0.0009(3) -0.0052(4) P2 0.0103(4) 0.0158(5) 0.0129(4) -0.0020(4) 0.0007(3) -0.0052(4) P3 0.0119(4) 0.0158(5) 0.0145(5) -0.0011(4) -0.0005(3) -0.0066(4) Si1 0.0118(4) 0.0156(5) 0.0105(5) 0.0004(4) -0.0005(4) -0.0046(4) Si2 0.0118(4) 0.0190(5) 0.0124(5) -0.0005(4) 0.0000(4) -0.0082(4) Si3 0.0090(4) 0.0149(5) 0.0142(5) -0.0008(4) -0.0009(3) -0.0041(4) O1 0.0125(12) 0.0240(14) 0.0134(13) 0.0022(11) 0.0000(10) -0.0087(11) O2 0.0188(13) 0.0281(15) 0.0164(14) -0.0061(11) 0.0031(10) -0.0154(12) O3 0.0182(13) 0.0142(13) 0.0299(16) -0.0002(11) 0.0075(11) -0.0050(11) O4 0.0134(12) 0.0234(15) 0.0184(14) 0.0046(11) 0.0027(10) -0.0026(11) O5 0.0137(12) 0.0148(13) 0.0266(15) 0.0000(11) -0.0017(11) -0.0059(11) O6 0.0129(12) 0.0262(15) 0.0214(14) -0.0111(12) -0.0027(10) -0.0039(11) O7 0.0130(12) 0.0256(15) 0.0164(13) 0.0025(11) -0.0028(10) -0.0100(11) O8 0.0212(13) 0.0155(13) 0.0166(13) -0.0012(10) -0.0043(10) -0.0090(11) O9 0.0190(13) 0.0164(13) 0.0117(13) -0.0009(10) 0.0013(10) -0.0052(11) C1 0.0139(16) 0.025(2) 0.0137(18) 0.0004(15) -0.0005(13) -0.0088(15) C2 0.0212(18) 0.024(2) 0.0124(18) -0.0017(15) 0.0038(14) -0.0129(16) C3 0.0179(18) 0.0178(19) 0.020(2) 0.0034(15) 0.0007(15) -0.0066(15) C4 0.0151(16) 0.0167(18) 0.0145(18) 0.0005(14) -0.0013(14) -0.0057(14) C5 0.0185(18) 0.024(2) 0.0160(19) 0.0030(15) 0.0018(14) -0.0108(16) C6 0.026(2) 0.035(2) 0.023(2) -0.0090(18) 0.0110(17) -0.0177(19) C7 0.0135(17) 0.0189(19) 0.0187(19) 0.0020(15) 0.0010(14) -0.0038(15) C8 0.0105(16) 0.0185(19) 0.028(2) -0.0023(16) 0.0019(14) -0.0053(15) C9 0.0145(17) 0.022(2) 0.020(2) -0.0098(16) 0.0002(14) -0.0040(15) C10 0.0100(15) 0.0141(17) 0.0163(18) -0.0042(14) 0.0016(13) -0.0030(13) C11 0.0111(16) 0.024(2) 0.021(2) -0.0033(16) 0.0009(14) -0.0033(15) C12 0.0151(18) 0.020(2) 0.035(2) -0.0033(18) -0.0051(16) -0.0035(16) C13 0.0189(18) 0.024(2) 0.0110(17) 0.0006(15) 0.0007(14) -0.0103(16) C14 0.0213(18) 0.0187(19) 0.0153(18) -0.0035(15) -0.0046(14) -0.0101(15) C15 0.0180(17) 0.0124(17) 0.0149(18) -0.0009(14) -0.0007(14) -0.0021(14) C16 0.0158(16) 0.0170(18) 0.0110(17) -0.0021(14) -0.0008(13) -0.0082(14) C17 0.0215(19) 0.025(2) 0.0173(19) -0.0010(16) -0.0025(15) -0.0112(17) C18 0.045(3) 0.028(2) 0.028(2) 0.0118(19) -0.011(2) -0.021(2) C19 0.0143(17) 0.034(2) 0.0122(18) 0.0010(16) -0.0019(14) -0.0076(16) C20 0.067(4) 0.081(4) 0.019(2) -0.011(2) 0.001(2) -0.059(3) C21 0.026(2) 0.038(3) 0.017(2) 0.0016(18) 0.0010(17) -0.012(2) C22 0.0197(18) 0.0131(18) 0.020(2) 0.0008(15) 0.0000(15) -0.0077(15) C23 0.042(3) 0.031(2) 0.027(2) -0.0074(19) -0.004(2) -0.020(2) C24 0.025(2) 0.018(2) 0.045(3) -0.0067(19) 0.0025(19) -0.0059(17) C25 0.0158(17) 0.023(2) 0.024(2) -0.0028(16) -0.0028(15) -0.0107(16) C26 0.056(3) 0.045(3) 0.024(2) -0.006(2) -0.010(2) -0.032(3) C27 0.035(2) 0.023(2) 0.043(3) 0.002(2) -0.014(2) -0.018(2) C28 0.0207(18) 0.023(2) 0.0142(18) -0.0004(15) 0.0000(14) -0.0105(16) C29 0.0177(18) 0.041(3) 0.017(2) -0.0027(18) 0.0016(15) -0.0112(18) C30 0.024(2) 0.045(3) 0.031(3) -0.018(2) -0.0050(18) -0.006(2) C31 0.0191(18) 0.0150(18) 0.0185(19) -0.0022(15) 0.0008(15) -0.0041(15) C32 0.034(2) 0.021(2) 0.027(2) -0.0073(17) -0.0053(18) -0.0115(18) C33 0.029(2) 0.021(2) 0.026(2) -0.0090(17) 0.0119(18) -0.0064(18) C34 0.0146(17) 0.031(2) 0.0157(18) 0.0009(16) -0.0015(14) -0.0144(16) C35 0.0166(18) 0.047(3) 0.023(2) 0.009(2) -0.0039(16) -0.0158(19) C36 0.042(3) 0.046(3) 0.027(2) -0.012(2) 0.003(2) -0.033(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; H H 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Table 6.1.1.4) ; O O 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; Pd Pd 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; Si Si 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; P P 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 P1 Pd1 Si1 96.10(4) . . P1 Pd1 Si3 93.56(4) . . Si1 Pd1 Si3 170.27(3) . . P1 Pd1 Pd3 148.84(3) . . Si1 Pd1 Pd3 115.05(3) . . Si3 Pd1 Pd3 55.28(3) . . P1 Pd1 Pd2 151.20(3) . . Si1 Pd1 Pd2 55.25(3) . . Si3 Pd1 Pd2 115.16(3) . . Pd3 Pd1 Pd2 59.928(11) . . P2 Pd2 Si1 93.74(4) . . P2 Pd2 Si2 96.88(4) . . Si1 Pd2 Si2 169.30(3) . . P2 Pd2 Pd3 151.43(3) . . Si1 Pd2 Pd3 114.49(3) . . Si2 Pd2 Pd3 55.05(3) . . P2 Pd2 Pd1 148.47(3) . . Si1 Pd2 Pd1 54.73(2) . . Si2 Pd2 Pd1 114.65(3) . . Pd3 Pd2 Pd1 59.895(13) . . P3 Pd3 Si2 95.99(4) . . P3 Pd3 Si3 94.97(4) . . Si2 Pd3 Si3 167.66(4) . . P3 Pd3 Pd1 147.75(3) . . Si2 Pd3 Pd1 115.26(3) . . Si3 Pd3 Pd1 54.97(3) . . P3 Pd3 Pd2 148.42(3) . . Si2 Pd3 Pd2 55.38(3) . . Si3 Pd3 Pd2 115.09(3) . . Pd1 Pd3 Pd2 60.177(13) . . O2 P1 O1 101.45(14) . . O2 P1 O3 100.69(15) . . O1 P1 O3 99.44(14) . . O2 P1 Pd1 114.72(10) . . O1 P1 Pd1 117.91(10) . . O3 P1 Pd1 119.53(10) . . O6 P2 O5 101.59(14) . . O6 P2 O4 100.84(15) . . O5 P2 O4 99.63(14) . . O6 P2 Pd2 113.69(10) . . O5 P2 Pd2 119.70(10) . . O4 P2 Pd2 118.35(10) . . O8 P3 O9 101.01(14) . . O8 P3 O7 100.60(14) . . O9 P3 O7 99.83(14) . . O8 P3 Pd3 110.55(10) . . O9 P3 Pd3 121.16(10) . . O7 P3 Pd3 120.30(10) . . C19 Si1 C22 107.62(18) . . C19 Si1 Pd1 122.87(14) . . C22 Si1 Pd1 114.45(12) . . C19 Si1 Pd2 119.37(13) . . C22 Si1 Pd2 119.01(12) . . Pd1 Si1 Pd2 70.02(3) . . C25 Si2 C28 104.75(17) . . C25 Si2 Pd3 116.29(13) . . C28 Si2 Pd3 122.41(12) . . C25 Si2 Pd2 116.17(13) . . C28 Si2 Pd2 125.24(13) . . Pd3 Si2 Pd2 69.57(3) . . C34 Si3 C31 107.71(18) . . C34 Si3 Pd1 119.44(13) . . C31 Si3 Pd1 117.54(13) . . C34 Si3 Pd3 122.57(12) . . C31 Si3 Pd3 116.16(12) . . Pd1 Si3 Pd3 69.75(3) . . C1 O1 P1 117.3(2) . . C2 O2 P1 117.0(2) . . C3 O3 P1 115.3(2) . . C7 O4 P2 117.1(2) . . C8 O5 P2 116.6(2) . . C9 O6 P2 116.8(2) . . C13 O7 P3 116.5(2) . . C14 O8 P3 116.4(2) . . C15 O9 P3 115.7(2) . . O1 C1 C4 110.4(3) . . O1 C1 H1A 109.6 . . C4 C1 H1A 109.6 . . O1 C1 H1B 109.6 . . C4 C1 H1B 109.6 . . H1A C1 H1B 108.1 . . O2 C2 C4 110.4(3) . . O2 C2 H2A 109.6 . . C4 C2 H2A 109.6 . . O2 C2 H2B 109.6 . . C4 C2 H2B 109.6 . . H2A C2 H2B 108.1 . . O3 C3 C4 112.5(3) . . O3 C3 H3A 109.1 . . C4 C3 H3A 109.1 . . O3 C3 H3B 109.1 . . C4 C3 H3B 109.1 . . H3A C3 H3B 107.8 . . C3 C4 C1 108.2(3) . . C3 C4 C2 107.9(3) . . C1 C4 C2 108.0(3) . . C3 C4 C5 108.8(3) . . C1 C4 C5 111.9(3) . . C2 C4 C5 112.0(3) . . C6 C5 C4 115.5(3) . . C6 C5 H5A 108.4 . . C4 C5 H5A 108.4 . . C6 C5 H5B 108.4 . . C4 C5 H5B 108.4 . . H5A C5 H5B 107.5 . . C5 C6 H6A 109.5 . . C5 C6 H6B 109.5 . . H6A C6 H6B 109.5 . . C5 C6 H6C 109.5 . . H6A C6 H6C 109.5 . . H6B C6 H6C 109.5 . . O4 C7 C10 110.7(3) . . O4 C7 H7A 109.5 . . C10 C7 H7A 109.5 . . O4 C7 H7B 109.5 . . C10 C7 H7B 109.5 . . H7A C7 H7B 108.1 . . O5 C8 C10 111.0(3) . . O5 C8 H8A 109.4 . . C10 C8 H8A 109.4 . . O5 C8 H8B 109.4 . . C10 C8 H8B 109.4 . . H8A C8 H8B 108.0 . . O6 C9 C10 111.2(3) . . O6 C9 H9A 109.4 . . C10 C9 H9A 109.4 . . O6 C9 H9B 109.4 . . C10 C9 H9B 109.4 . . H9A C9 H9B 108.0 . . C8 C10 C9 108.1(3) . . C8 C10 C7 108.6(3) . . C9 C10 C7 107.9(3) . . C8 C10 C11 111.6(3) . . C9 C10 C11 108.7(3) . . C7 C10 C11 111.8(3) . . C12 C11 C10 115.5(3) . . C12 C11 H11A 108.4 . . C10 C11 H11A 108.4 . . C12 C11 H11B 108.4 . . C10 C11 H11B 108.4 . . H11A C11 H11B 107.5 . . C11 C12 H12A 109.5 . . C11 C12 H12B 109.5 . . H12A C12 H12B 109.5 . . C11 C12 H12C 109.5 . . H12A C12 H12C 109.5 . . H12B C12 H12C 109.5 . . O7 C13 C16 110.1(3) . . O7 C13 H13A 109.7 . . C16 C13 H13A 109.7 . . O7 C13 H13B 109.7 . . C16 C13 H13B 109.7 . . H13A C13 H13B 108.2 . . O8 C14 C16 110.4(3) . . O8 C14 H14A 109.6 . . C16 C14 H14A 109.6 . . O8 C14 H14B 109.6 . . C16 C14 H14B 109.6 . . H14A C14 H14B 108.1 . . O9 C15 C16 111.3(3) . . O9 C15 H15A 109.4 . . C16 C15 H15A 109.4 . . O9 C15 H15B 109.4 . . C16 C15 H15B 109.4 . . H15A C15 H15B 108.0 . . C15 C16 C14 108.0(3) . . C15 C16 C13 108.3(3) . . C14 C16 C13 108.2(3) . . C15 C16 C17 112.1(3) . . C14 C16 C17 108.5(3) . . C13 C16 C17 111.6(3) . . C18 C17 C16 115.7(3) . . C18 C17 H17A 108.3 . . C16 C17 H17A 108.3 . . C18 C17 H17B 108.3 . . C16 C17 H17B 108.3 . . H17A C17 H17B 107.4 . . C17 C18 H18A 109.5 . . C17 C18 H18B 109.5 . . H18A C18 H18B 109.5 . . C17 C18 H18C 109.5 . . H18A C18 H18C 109.5 . . H18B C18 H18C 109.5 . . C21 C19 C20 110.3(4) . . C21 C19 Si1 114.3(3) . . C20 C19 Si1 110.6(3) . . C21 C19 H19 107.1 . . C20 C19 H19 107.1 . . Si1 C19 H19 107.1 . . C19 C20 H20A 109.5 . . C19 C20 H20B 109.5 . . H20A C20 H20B 109.5 . . C19 C20 H20C 109.5 . . H20A C20 H20C 109.5 . . H20B C20 H20C 109.5 . . C19 C21 H21A 109.5 . . C19 C21 H21B 109.5 . . H21A C21 H21B 109.5 . . C19 C21 H21C 109.5 . . H21A C21 H21C 109.5 . . H21B C21 H21C 109.5 . . C23 C22 C24 110.8(4) . . C23 C22 Si1 109.6(3) . . C24 C22 Si1 114.7(3) . . C23 C22 H22 107.2 . . C24 C22 H22 107.2 . . Si1 C22 H22 107.2 . . C22 C23 H23A 109.5 . . C22 C23 H23B 109.5 . . H23A C23 H23B 109.5 . . C22 C23 H23C 109.5 . . H23A C23 H23C 109.5 . . H23B C23 H23C 109.5 . . C22 C24 H24A 109.5 . . C22 C24 H24B 109.5 . . H24A C24 H24B 109.5 . . C22 C24 H24C 109.5 . . H24A C24 H24C 109.5 . . H24B C24 H24C 109.5 . . C26 C25 C27 109.8(4) . . C26 C25 Si2 112.1(3) . . C27 C25 Si2 112.5(3) . . C26 C25 H25 107.4 . . C27 C25 H25 107.4 . . Si2 C25 H25 107.4 . . C25 C26 H26A 109.5 . . C25 C26 H26B 109.5 . . H26A C26 H26B 109.5 . . C25 C26 H26C 109.5 . . H26A C26 H26C 109.5 . . H26B C26 H26C 109.5 . . C25 C27 H27A 109.5 . . C25 C27 H27B 109.5 . . H27A C27 H27B 109.5 . . C25 C27 H27C 109.5 . . H27A C27 H27C 109.5 . . H27B C27 H27C 109.5 . . C30 C28 C29 110.4(4) . . C30 C28 Si2 112.1(3) . . C29 C28 Si2 113.2(3) . . C30 C28 H28 106.9 . . C29 C28 H28 106.9 . . Si2 C28 H28 106.9 . . C28 C29 H29A 109.5 . . C28 C29 H29B 109.5 . . H29A C29 H29B 109.5 . . C28 C29 H29C 109.5 . . H29A C29 H29C 109.5 . . H29B C29 H29C 109.5 . . C28 C30 H30A 109.5 . . C28 C30 H30B 109.5 . . H30A C30 H30B 109.5 . . C28 C30 H30C 109.5 . . H30A C30 H30C 109.5 . . H30B C30 H30C 109.5 . . C32 C31 C33 110.0(3) . . C32 C31 Si3 110.6(3) . . C33 C31 Si3 113.7(3) . . C32 C31 H31 107.4 . . C33 C31 H31 107.4 . . Si3 C31 H31 107.4 . . C31 C32 H32A 109.5 . . C31 C32 H32B 109.5 . . H32A C32 H32B 109.5 . . C31 C32 H32C 109.5 . . H32A C32 H32C 109.5 . . H32B C32 H32C 109.5 . . C31 C33 H33A 109.5 . . C31 C33 H33B 109.5 . . H33A C33 H33B 109.5 . . C31 C33 H33C 109.5 . . H33A C33 H33C 109.5 . . H33B C33 H33C 109.5 . . C35 C34 C36 111.6(4) . . C35 C34 Si3 113.5(3) . . C36 C34 Si3 109.8(3) . . C35 C34 H34 107.2 . . C36 C34 H34 107.2 . . Si3 C34 H34 107.2 . . C34 C35 H35A 109.5 . . C34 C35 H35B 109.5 . . H35A C35 H35B 109.5 . . C34 C35 H35C 109.5 . . H35A C35 H35C 109.5 . . H35B C35 H35C 109.5 . . C34 C36 H36A 109.5 . . C34 C36 H36B 109.5 . . H36A C36 H36B 109.5 . . C34 C36 H36C 109.5 . . H36A C36 H36C 109.5 . . H36B C36 H36C 109.5 . . C39 C37 C38 38.2(7) . . C39 C37 C41 49.1(7) . 2_577 C38 C37 C41 86.8(7) . 2_577 C39 C38 C40 94.9(13) . . C39 C38 C37 49.0(9) . . C40 C38 C37 143.8(12) . . C38 C39 C37 92.9(12) . . C38 C39 C41 170.0(14) . 2_577 C37 C39 C41 86.1(10) . 2_577 C38 C39 C40 43.2(9) . . C37 C39 C40 136.0(11) . . C41 C39 C40 137.4(11) 2_577 . C38 C39 C40 138.7(12) . 2_577 C37 C39 C40 127.6(10) . 2_577 C41 C39 C40 41.5(7) 2_577 2_577 C40 C39 C40 96.2(7) . 2_577 C38 C40 C41 176.8(13) . . C38 C40 C39 41.9(8) . . C41 C40 C39 135.1(11) . . C38 C40 C39 125.2(10) . 2_577 C41 C40 C39 51.7(8) . 2_577 C39 C40 C39 83.8(7) . 2_577 C40 C41 C39 86.8(10) . 2_577 C40 C41 C37 131.6(11) . 2_577 C39 C41 C37 44.8(7) 2_577 2_577 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Pd1 P1 2.1868(9) . Pd1 Si1 2.3557(10) . Pd1 Si3 2.3601(11) . Pd1 Pd3 2.7041(5) . Pd1 Pd2 2.7117(5) . Pd2 P2 2.1864(10) . Pd2 Si1 2.3708(10) . Pd2 Si2 2.3753(10) . Pd2 Pd3 2.7050(5) . Pd3 P3 2.1902(10) . Pd3 Si2 2.3658(10) . Pd3 Si3 2.3692(10) . P1 O2 1.604(3) . P1 O1 1.615(3) . P1 O3 1.627(3) . P2 O6 1.610(3) . P2 O5 1.613(3) . P2 O4 1.617(3) . P3 O8 1.614(3) . P3 O9 1.617(3) . P3 O7 1.618(3) . Si1 C19 1.895(4) . Si1 C22 1.902(4) . Si2 C25 1.898(4) . Si2 C28 1.903(4) . Si3 C34 1.895(4) . Si3 C31 1.899(4) . O1 C1 1.454(4) . O2 C2 1.455(4) . O3 C3 1.442(4) . O4 C7 1.442(4) . O5 C8 1.458(4) . O6 C9 1.446(4) . O7 C13 1.456(4) . O8 C14 1.454(4) . O9 C15 1.455(4) . C1 C4 1.517(5) . C1 H1A 0.9900 . C1 H1B 0.9900 . C2 C4 1.530(5) . C2 H2A 0.9900 . C2 H2B 0.9900 . C3 C4 1.516(5) . C3 H3A 0.9900 . C3 H3B 0.9900 . C4 C5 1.534(5) . C5 C6 1.518(5) . C5 H5A 0.9900 . C5 H5B 0.9900 . C6 H6A 0.9800 . C6 H6B 0.9800 . C6 H6C 0.9800 . C7 C10 1.530(5) . C7 H7A 0.9900 . C7 H7B 0.9900 . C8 C10 1.519(5) . C8 H8A 0.9900 . C8 H8B 0.9900 . C9 C10 1.522(5) . C9 H9A 0.9900 . C9 H9B 0.9900 . C10 C11 1.544(5) . C11 C12 1.528(6) . C11 H11A 0.9900 . C11 H11B 0.9900 . C12 H12A 0.9800 . C12 H12B 0.9800 . C12 H12C 0.9800 . C13 C16 1.523(5) . C13 H13A 0.9900 . C13 H13B 0.9900 . C14 C16 1.523(5) . C14 H14A 0.9900 . C14 H14B 0.9900 . C15 C16 1.518(5) . C15 H15A 0.9900 . C15 H15B 0.9900 . C16 C17 1.530(5) . C17 C18 1.527(6) . C17 H17A 0.9900 . C17 H17B 0.9900 . C18 H18A 0.9800 . C18 H18B 0.9800 . C18 H18C 0.9800 . C19 C21 1.525(5) . C19 C20 1.528(7) . C19 H19 1.0000 . C20 H20A 0.9800 . C20 H20B 0.9800 . C20 H20C 0.9800 . C21 H21A 0.9800 . C21 H21B 0.9800 . C21 H21C 0.9800 . C22 C23 1.525(6) . C22 C24 1.531(5) . C22 H22 1.0000 . C23 H23A 0.9800 . C23 H23B 0.9800 . C23 H23C 0.9800 . C24 H24A 0.9800 . C24 H24B 0.9800 . C24 H24C 0.9800 . C25 C26 1.521(6) . C25 C27 1.525(6) . C25 H25 1.0000 . C26 H26A 0.9800 . C26 H26B 0.9800 . C26 H26C 0.9800 . C27 H27A 0.9800 . C27 H27B 0.9800 . C27 H27C 0.9800 . C28 C30 1.517(6) . C28 C29 1.527(5) . C28 H28 1.0000 . C29 H29A 0.9800 . C29 H29B 0.9800 . C29 H29C 0.9800 . C30 H30A 0.9800 . C30 H30B 0.9800 . C30 H30C 0.9800 . C31 C32 1.526(6) . C31 C33 1.529(5) . C31 H31 1.0000 . C32 H32A 0.9800 . C32 H32B 0.9800 . C32 H32C 0.9800 . C33 H33A 0.9800 . C33 H33B 0.9800 . C33 H33C 0.9800 . C34 C35 1.519(6) . C34 C36 1.522(6) . C34 H34 1.0000 . C35 H35A 0.9800 . C35 H35B 0.9800 . C35 H35C 0.9800 . C36 H36A 0.9800 . C36 H36B 0.9800 . C36 H36C 0.9800 . C37 C39 1.224(13) . C37 C38 1.620(14) . C37 C41 1.731(15) 2_577 C38 C39 1.002(14) . C38 C40 1.026(13) . C39 C41 1.311(16) 2_577 C39 C40 1.495(13) . C39 C40 1.668(14) 2_577 C40 C41 1.107(14) . C40 C39 1.668(14) 2_577 C41 C39 1.311(16) 2_577 C41 C37 1.731(15) 2_577 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 O2 P1 O1 C1 54.8(3) . . . . O3 P1 O1 C1 -48.2(3) . . . . Pd1 P1 O1 C1 -179.0(2) . . . . O1 P1 O2 C2 -44.0(3) . . . . O3 P1 O2 C2 58.1(3) . . . . Pd1 P1 O2 C2 -172.2(2) . . . . O2 P1 O3 C3 -45.7(3) . . . . O1 P1 O3 C3 58.0(3) . . . . Pd1 P1 O3 C3 -172.3(2) . . . . O6 P2 O4 C7 -47.6(3) . . . . O5 P2 O4 C7 56.3(3) . . . . Pd2 P2 O4 C7 -172.2(2) . . . . O6 P2 O5 C8 52.5(3) . . . . O4 P2 O5 C8 -50.7(3) . . . . Pd2 P2 O5 C8 178.6(2) . . . . O5 P2 O6 C9 -48.0(3) . . . . O4 P2 O6 C9 54.3(3) . . . . Pd2 P2 O6 C9 -178.0(2) . . . . O8 P3 O7 C13 -42.4(3) . . . . O9 P3 O7 C13 60.8(3) . . . . Pd3 P3 O7 C13 -164.0(2) . . . . O9 P3 O8 C14 -43.1(3) . . . . O7 P3 O8 C14 59.2(3) . . . . Pd3 P3 O8 C14 -172.6(2) . . . . O8 P3 O9 C15 58.4(3) . . . . O7 P3 O9 C15 -44.5(3) . . . . Pd3 P3 O9 C15 -179.2(2) . . . . P1 O1 C1 C4 -7.2(4) . . . . P1 O2 C2 C4 -10.8(4) . . . . P1 O3 C3 C4 -10.3(4) . . . . O3 C3 C4 C1 -52.7(4) . . . . O3 C3 C4 C2 63.9(4) . . . . O3 C3 C4 C5 -174.4(3) . . . . O1 C1 C4 C3 62.0(4) . . . . O1 C1 C4 C2 -54.6(4) . . . . O1 C1 C4 C5 -178.2(3) . . . . O2 C2 C4 C3 -51.7(4) . . . . O2 C2 C4 C1 65.0(4) . . . . O2 C2 C4 C5 -171.4(3) . . . . C3 C4 C5 C6 -176.5(4) . . . . C1 C4 C5 C6 64.1(5) . . . . C2 C4 C5 C6 -57.3(5) . . . . P2 O4 C7 C10 -6.4(4) . . . . P2 O5 C8 C10 -2.7(4) . . . . P2 O6 C9 C10 -5.2(4) . . . . O5 C8 C10 C9 -56.9(4) . . . . O5 C8 C10 C7 59.9(4) . . . . O5 C8 C10 C11 -176.4(3) . . . . O6 C9 C10 C8 61.7(4) . . . . O6 C9 C10 C7 -55.7(4) . . . . O6 C9 C10 C11 -177.1(3) . . . . O4 C7 C10 C8 -54.9(4) . . . . O4 C7 C10 C9 62.1(4) . . . . O4 C7 C10 C11 -178.5(3) . . . . C8 C10 C11 C12 -72.1(4) . . . . C9 C10 C11 C12 168.9(3) . . . . C7 C10 C11 C12 49.9(5) . . . . P3 O7 C13 C16 -14.8(4) . . . . P3 O8 C14 C16 -13.9(4) . . . . P3 O9 C15 C16 -12.6(4) . . . . O9 C15 C16 C14 -51.3(4) . . . . O9 C15 C16 C13 65.7(4) . . . . O9 C15 C16 C17 -170.7(3) . . . . O8 C14 C16 C15 66.2(4) . . . . O8 C14 C16 C13 -50.9(4) . . . . O8 C14 C16 C17 -172.1(3) . . . . O7 C13 C16 C15 -49.9(4) . . . . O7 C13 C16 C14 66.9(4) . . . . O7 C13 C16 C17 -173.9(3) . . . . C15 C16 C17 C18 -51.2(4) . . . . C14 C16 C17 C18 -170.3(3) . . . . C13 C16 C17 C18 70.5(4) . . . . C22 Si1 C19 C21 58.8(3) . . . . Pd1 Si1 C19 C21 -77.5(3) . . . . Pd2 Si1 C19 C21 -161.5(3) . . . . C22 Si1 C19 C20 -176.0(3) . . . . Pd1 Si1 C19 C20 47.8(3) . . . . Pd2 Si1 C19 C20 -36.3(3) . . . . C28 Si2 C25 C26 159.3(3) . . . . Pd3 Si2 C25 C26 -62.2(3) . . . . Pd2 Si2 C25 C26 16.7(4) . . . . C28 Si2 C25 C27 -76.3(3) . . . . Pd3 Si2 C25 C27 62.1(3) . . . . Pd2 Si2 C25 C27 141.1(3) . . . . C34 Si3 C31 C32 -172.2(3) . . . . Pd1 Si3 C31 C32 -33.7(3) . . . . Pd3 Si3 C31 C32 46.0(3) . . . . C34 Si3 C31 C33 -47.8(3) . . . . Pd1 Si3 C31 C33 90.6(3) . . . . Pd3 Si3 C31 C33 170.3(3) . . . . C31 Si3 C34 C35 -52.5(3) . . . . Pd1 Si3 C34 C35 170.0(2) . . . . Pd3 Si3 C34 C35 86.3(3) . . . . C31 Si3 C34 C36 -178.2(3) . . . . Pd1 Si3 C34 C36 44.3(3) . . . . Pd3 Si3 C34 C36 -39.3(3) . . . . C41 C37 C38 C39 7.5(11) 2_577 . . . C39 C37 C38 C40 4.1(17) . . . . C41 C37 C38 C40 12(2) 2_577 . . . C40 C38 C39 C37 -177.6(10) . . . . C40 C38 C39 C41 99(8) . . . 2_577 C37 C38 C39 C41 -84(8) . . . 2_577 C37 C38 C39 C40 177.6(10) . . . . C40 C38 C39 C40 13(2) . . . 2_577 C37 C38 C39 C40 -169(2) . . . 2_577 C41 C37 C39 C38 -170.0(14) 2_577 . . . C38 C37 C39 C41 170.0(14) . . . 2_577 C38 C37 C39 C40 -2.4(10) . . . . C41 C37 C39 C40 -172.4(18) 2_577 . . . C38 C37 C39 C40 171.1(18) . . . 2_577 C41 C37 C39 C40 1.1(8) 2_577 . . 2_577 C37 C38 C40 C39 -3.1(13) . . . . C39 C38 C40 C39 -10.6(18) . . . 2_577 C37 C38 C40 C39 -14(3) . . . 2_577 C37 C39 C40 C38 3.5(15) . . . . C41 C39 C40 C38 -165(2) 2_577 . . . C40 C39 C40 C38 -171.3(15) 2_577 . . . C38 C39 C40 C41 178.1(18) . . . . C37 C39 C40 C41 -178.3(14) . . . . C41 C39 C40 C41 13(3) 2_577 . . . C40 C39 C40 C41 6.8(14) 2_577 . . . C38 C39 C40 C39 171.3(15) . . . 2_577 C37 C39 C40 C39 174.8(17) . . . 2_577 C41 C39 C40 C39 6.0(12) 2_577 . . 2_577 C40 C39 C40 C39 0.000(0) 2_577 . . 2_577 C39 C40 C41 C39 -8.7(18) . . . 2_577 C39 C40 C41 C37 -10(2) . . . 2_577 C39 C40 C41 C37 -1.2(9) 2_577 . . 2_577