#------------------------------------------------------------------------------ #$Date: 2019-12-16 11:41:32 +0200 (Mon, 16 Dec 2019) $ #$Revision: 245206 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/65/1556586.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556586 loop_ _publ_author_name 'Akasaka, N.' 'Tanaka, K.' 'Ishida, S.' 'Iwamoto, T.' _publ_section_title ; Synthesis and Functionalization of a 1,2-Bis(trimethylsilyl)-1,2-disilacyclohexene That Can Serve as a Unit of cis-1,2-Dialkyldisilene ; _journal_name_full Inorganics _journal_page_first 21 _journal_paper_doi 10.3390/inorganics6010021 _journal_volume 6 _journal_year 2018 _chemical_formula_moiety 'C33 H57 Br Si7' _chemical_formula_sum 'C33 H57 Br Si7' _chemical_formula_weight 730.32 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _cell_angle_alpha 93.9480(10) _cell_angle_beta 90.1810(10) _cell_angle_gamma 109.1330(10) _cell_formula_units_Z 2 _cell_length_a 9.0529(3) _cell_length_b 11.9109(4) _cell_length_c 19.1793(7) _cell_measurement_reflns_used 9865 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 33.44 _cell_measurement_theta_min 2.38 _cell_volume 1948.47(12) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014 (Sheldrick 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 8.333 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEXII CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator 'Bruker Helios multilayer confocal mirror' _diffrn_radiation_source 'Bruker TXS fine-focus rotating anode' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0259 _diffrn_reflns_av_unetI/netI 0.0182 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 37185 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.500 _diffrn_reflns_theta_min 1.065 _exptl_absorpt_coefficient_mu 1.292 _exptl_absorpt_correction_T_max 0.7467 _exptl_absorpt_correction_T_min 0.7010 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details 'SADABS Sheldrick 1996' _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.245 _exptl_crystal_description plate _exptl_crystal_F_000 776 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.030 _refine_diff_density_max 0.689 _refine_diff_density_min -0.503 _refine_diff_density_rms 0.055 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 385 _refine_ls_number_reflns 7235 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.043 _refine_ls_R_factor_all 0.0306 _refine_ls_R_factor_gt 0.0263 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0359P)^2^+1.3295P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0679 _refine_ls_wR_factor_ref 0.0701 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 6547 _reflns_number_total 7235 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file Cpd6Br_NA133a_a.cif _cod_data_source_block NA133a_a _cod_database_code 1556586 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.782 _shelx_estimated_absorpt_t_max 0.962 _shelxl_version_number 2014-3 _shelx_res_file ; TITL NA133a_a.res in P-1 REM Yadorkari-X generated CELL 0.71073 9.0529 11.9109 19.1793 93.9480 90.1810 109.1330 ZERR 2.0 0.0003 0.0004 0.0007 0.0010 0.0010 0.0010 LATT 1 REM SPGR P-1 triclinic SFAC C H Si Br UNIT 66 114 14 2 SIZE 0.20 0.10 0.03 TEMP -173.0 L.S. 30 FMAP 2 PLAN -20 ACTA CONF LIST 4 MERG 2 OMIT -10.000000 51.000000 WGHT 0.035900 1.329500 FVAR 0.39456 C4 1 0.557111 0.744837 0.645007 11.00000 0.02356 0.02461 = 0.01819 -0.00209 0.00122 0.01404 AFIX 43 H1 2 0.460043 0.745488 0.663383 11.00000 -1.20000 AFIX 0 C5 1 0.634591 0.829039 0.597565 11.00000 0.03550 0.02093 = 0.02317 0.00156 0.00067 0.01895 AFIX 43 H2 2 0.589960 0.886821 0.584730 11.00000 -1.20000 AFIX 0 C6 1 0.772215 0.828136 0.570155 11.00000 0.03244 0.01494 = 0.01840 0.00390 0.00254 0.01026 AFIX 43 H3 2 0.823120 0.886037 0.538706 11.00000 -1.20000 AFIX 0 C12 1 1.140926 0.448370 0.594816 11.00000 0.02418 0.02642 = 0.01931 0.00562 0.00243 0.01538 AFIX 43 H4 2 1.171791 0.380530 0.600450 11.00000 -1.20000 AFIX 0 C10 1 1.178994 0.631607 0.540402 11.00000 0.01783 0.02685 = 0.01611 0.00766 0.00554 0.00560 AFIX 43 H5 2 1.237042 0.689910 0.510598 11.00000 -1.20000 AFIX 0 C13 1 1.014266 0.460195 0.628428 11.00000 0.01989 0.01933 = 0.01331 0.00577 0.00232 0.00837 AFIX 43 H6 2 0.959340 0.400566 0.658143 11.00000 -1.20000 AFIX 0 C16 1 0.767371 0.348231 0.875898 11.00000 0.01280 0.01252 = 0.01296 0.00250 -0.00059 0.00246 AFIX 23 H7 2 0.769032 0.323341 0.924010 11.00000 -1.20000 H8 2 0.861033 0.339552 0.852760 11.00000 -1.20000 AFIX 0 SI1 3 0.773585 0.487061 0.738566 11.00000 0.01141 0.01053 = 0.00991 0.00222 0.00102 0.00202 SI2 3 0.585693 0.321227 0.750782 11.00000 0.01254 0.01140 = 0.01127 0.00178 0.00032 0.00112 SI3 3 0.440641 0.227498 0.893324 11.00000 0.01345 0.01245 = 0.01360 0.00330 0.00413 0.00290 SI4 3 0.856920 0.714674 0.843609 11.00000 0.01654 0.01025 = 0.01558 0.00008 -0.00043 0.00296 SI5 3 1.095430 0.570443 0.828795 11.00000 0.01102 0.01686 = 0.01550 0.00206 -0.00113 0.00250 SI6 3 0.675139 0.118609 0.813830 11.00000 0.01661 0.01010 = 0.02031 0.00209 0.00298 0.00500 SI7 3 0.444094 0.226742 0.648137 11.00000 0.01550 0.01664 = 0.01424 -0.00073 0.00023 0.00618 BR1 4 1.093133 0.854346 0.499782 11.00000 0.03141 0.02323 = 0.03196 0.01644 0.01220 0.00768 C1 1 0.830803 0.571252 0.657382 11.00000 0.01333 0.01058 = 0.01025 0.00051 -0.00034 0.00061 C2 1 0.765136 0.656752 0.637182 11.00000 0.01789 0.01178 = 0.01100 -0.00120 -0.00109 0.00385 C7 1 0.842174 0.741803 0.587645 11.00000 0.02097 0.01326 = 0.01347 0.00060 -0.00149 0.00545 C9 1 1.042932 0.644891 0.572819 11.00000 0.01631 0.01667 = 0.01230 0.00272 0.00031 0.00341 C3 1 0.621206 0.662752 0.664461 11.00000 0.01913 0.01748 = 0.01427 0.00040 0.00123 0.00607 AFIX 43 H9 2 0.568578 0.607828 0.697166 11.00000 -1.20000 AFIX 0 C8 1 0.982175 0.735381 0.560024 11.00000 0.02061 0.01284 = 0.01385 0.00679 0.00327 0.00088 C14 1 0.960895 0.558911 0.620679 11.00000 0.01381 0.01557 = 0.01053 0.00104 -0.00157 0.00383 C15 1 0.618564 0.257675 0.836001 11.00000 0.01161 0.01066 = 0.01195 0.00170 0.00082 0.00249 C17 1 0.784900 0.482419 0.881385 11.00000 0.01443 0.01253 = 0.01007 0.00204 0.00084 0.00164 AFIX 23 H10 2 0.835187 0.517442 0.927329 11.00000 -1.20000 H11 2 0.678653 0.488932 0.881267 11.00000 -1.20000 AFIX 0 C18 1 0.880301 0.561224 0.823430 11.00000 0.01153 0.01046 = 0.01026 0.00117 -0.00039 0.00100 C11 1 1.226768 0.537258 0.551414 11.00000 0.02004 0.03454 = 0.02005 0.00693 0.00589 0.01435 AFIX 43 H12 2 1.318315 0.530891 0.529863 11.00000 -1.20000 AFIX 0 C19 1 0.227642 0.162232 0.659218 11.00000 0.01841 0.03137 = 0.02344 0.00314 -0.00193 0.00266 AFIX 137 H13 2 0.189973 0.221799 0.684098 11.00000 -1.50000 H14 2 0.204766 0.091812 0.686182 11.00000 -1.50000 H15 2 0.175019 0.139356 0.613166 11.00000 -1.50000 AFIX 0 C20 1 0.508415 0.105959 0.603921 11.00000 0.04062 0.02804 = 0.02321 -0.00667 -0.00191 0.01766 AFIX 137 H16 2 0.446666 0.075072 0.560534 11.00000 -1.50000 H17 2 0.492762 0.041324 0.635005 11.00000 -1.50000 H18 2 0.619452 0.138320 0.593104 11.00000 -1.50000 AFIX 0 C21 1 0.485999 0.350227 0.588331 11.00000 0.02159 0.02368 = 0.01482 0.00066 -0.00092 0.00635 AFIX 137 H19 2 0.598594 0.380877 0.580357 11.00000 -1.50000 H20 2 0.451911 0.414470 0.609648 11.00000 -1.50000 H21 2 0.429467 0.320092 0.543624 11.00000 -1.50000 AFIX 0 C22 1 0.252939 0.147712 0.844004 11.00000 0.01314 0.02434 = 0.02848 -0.00111 0.00435 0.00050 AFIX 137 H22 2 0.166775 0.127485 0.876698 11.00000 -1.50000 H23 2 0.259683 0.074556 0.819634 11.00000 -1.50000 H24 2 0.233935 0.199257 0.809817 11.00000 -1.50000 AFIX 0 C23 1 0.417976 0.367447 0.935213 11.00000 0.01789 0.02069 = 0.01854 0.00230 0.00765 0.00738 AFIX 137 H25 2 0.413033 0.420315 0.898965 11.00000 -1.50000 H26 2 0.507601 0.407648 0.966960 11.00000 -1.50000 H27 2 0.321432 0.347614 0.961634 11.00000 -1.50000 AFIX 0 C24 1 0.453636 0.136513 0.967765 11.00000 0.03114 0.02181 = 0.02229 0.01114 0.00938 0.00948 AFIX 137 H28 2 0.367754 0.132292 0.999557 11.00000 -1.50000 H29 2 0.553836 0.173844 0.993140 11.00000 -1.50000 H30 2 0.446105 0.055893 0.949469 11.00000 -1.50000 AFIX 0 C25 1 0.501545 -0.015696 0.789114 11.00000 0.02724 0.01313 = 0.03874 -0.00259 0.00650 0.00244 AFIX 137 H31 2 0.438137 0.003233 0.753129 11.00000 -1.50000 H32 2 0.438564 -0.039543 0.830399 11.00000 -1.50000 H33 2 0.536952 -0.081166 0.770859 11.00000 -1.50000 AFIX 0 C26 1 0.778721 0.083417 0.890211 11.00000 0.02941 0.02419 = 0.03067 0.01040 0.00415 0.01574 AFIX 137 H34 2 0.711210 0.072393 0.930771 11.00000 -1.50000 H35 2 0.875969 0.149339 0.901451 11.00000 -1.50000 H36 2 0.802979 0.010175 0.878225 11.00000 -1.50000 AFIX 0 C27 1 0.816788 0.138217 0.740942 11.00000 0.02200 0.02190 = 0.02563 0.00032 0.00500 0.01188 AFIX 137 H37 2 0.838866 0.063732 0.730275 11.00000 -1.50000 H38 2 0.914176 0.202089 0.755128 11.00000 -1.50000 H39 2 0.771384 0.159083 0.699313 11.00000 -1.50000 AFIX 0 C28 1 1.220329 0.693612 0.778531 11.00000 0.01371 0.02579 = 0.03906 0.01046 0.00220 -0.00045 AFIX 137 H40 2 1.213085 0.769734 0.798174 11.00000 -1.50000 H41 2 1.184343 0.680330 0.729468 11.00000 -1.50000 H42 2 1.329227 0.695530 0.781523 11.00000 -1.50000 AFIX 0 C29 1 1.141617 0.433413 0.796542 11.00000 0.01688 0.02720 = 0.02348 0.00322 0.00069 0.01048 AFIX 137 H43 2 1.085222 0.400905 0.752066 11.00000 -1.50000 H44 2 1.109335 0.373649 0.831069 11.00000 -1.50000 H45 2 1.254381 0.454222 0.789672 11.00000 -1.50000 AFIX 0 C30 1 1.167872 0.595377 0.922144 11.00000 0.02629 0.04416 = 0.02195 -0.00544 -0.00823 0.01852 AFIX 137 H46 2 1.279032 0.603199 0.923914 11.00000 -1.50000 H47 2 1.108397 0.527543 0.948004 11.00000 -1.50000 H48 2 1.154051 0.668422 0.943306 11.00000 -1.50000 AFIX 0 C31 1 0.933734 0.825028 0.775868 11.00000 0.02580 0.01134 = 0.02694 0.00389 -0.00050 0.00200 AFIX 137 H49 2 0.845885 0.838079 0.751685 11.00000 -1.50000 H50 2 0.993959 0.793815 0.741952 11.00000 -1.50000 H51 2 1.001363 0.900663 0.798686 11.00000 -1.50000 AFIX 0 C32 1 0.958134 0.789523 0.928567 11.00000 0.03021 0.02037 = 0.02134 -0.00515 -0.00516 0.00792 AFIX 137 H52 2 0.922244 0.856578 0.943008 11.00000 -1.50000 H53 2 1.071457 0.818830 0.922332 11.00000 -1.50000 H54 2 0.933386 0.732122 0.964583 11.00000 -1.50000 AFIX 0 C33 1 0.644239 0.694825 0.856086 11.00000 0.02280 0.01921 = 0.02207 0.00055 0.00163 0.01065 AFIX 137 H55 2 0.626279 0.770552 0.850565 11.00000 -1.50000 H56 2 0.614798 0.669417 0.903058 11.00000 -1.50000 H57 2 0.580744 0.634155 0.821140 11.00000 -1.50000 AFIX 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM NA133a_a.res in P-1 REM R1 = 0.0263 for 6547 Fo > 4sig(Fo) and 0.0306 for all 7235 data REM 385 parameters refined using 0 restraints END WGHT 0.0359 1.3295 REM Highest difference peak 0.689, deepest hole -0.503, 1-sigma level 0.055 Q1 1 0.5808 0.4406 0.7536 11.00000 0.05 0.69 Q2 1 0.7721 0.3558 0.7196 11.00000 0.05 0.49 Q3 1 0.3793 0.1757 0.6200 11.00000 0.05 0.47 Q4 1 1.1809 0.8801 0.5334 11.00000 0.05 0.40 Q5 1 0.8293 0.5240 0.7800 11.00000 0.05 0.39 Q6 1 1.0335 0.7817 0.4780 11.00000 0.05 0.37 Q7 1 0.6817 0.4060 0.7418 11.00000 0.05 0.36 Q8 1 0.5785 0.0569 0.7970 11.00000 0.05 0.36 Q9 1 0.4596 0.2970 0.6189 11.00000 0.05 0.36 Q10 1 0.5081 0.2623 0.7035 11.00000 0.05 0.36 Q11 1 0.7790 0.4113 0.8768 11.00000 0.05 0.34 Q12 1 0.6896 0.3040 0.8524 11.00000 0.05 0.34 Q13 1 0.9289 0.7542 0.8824 11.00000 0.05 0.34 Q14 1 0.6162 0.2925 0.7988 11.00000 0.05 0.33 Q15 1 0.4559 0.1770 0.9287 11.00000 0.05 0.33 Q16 1 1.1481 0.6267 0.8002 11.00000 0.05 0.33 Q17 1 0.7256 0.0995 0.8568 11.00000 0.05 0.31 Q18 1 0.3491 0.1915 0.8607 11.00000 0.05 0.30 Q19 1 0.6943 0.6636 0.6476 11.00000 0.05 0.30 Q20 1 0.9984 0.6039 0.5989 11.00000 0.05 0.30 ; _shelx_res_checksum 46463 _shelx_hkl_file ; -1 0 0 244.88 4.60 -1 0 0 246.48 4.80 -1 0 0 246.08 4.60 -1 0 0 237.18 4.40 1 0 0 232.58 4.40 1 0 0 230.88 4.40 1 0 0 231.18 4.60 1 0 0 236.88 4.40 1 0 0 230.18 4.60 1 0 0 240.68 4.80 -2 0 0 60.29 2.60 -2 0 0 59.49 2.70 -2 0 0 57.99 2.20 -2 0 0 58.49 1.70 2 0 0 57.59 2.00 2 0 0 62.09 2.40 2 0 0 55.39 1.80 2 0 0 61.59 1.80 2 0 0 61.19 1.70 -3 0 0 1979.60 35.00 -3 0 0 1938.71 36.20 -3 0 0 1980.70 35.70 -3 0 0 2003.60 36.00 3 0 0 1897.01 34.30 3 0 0 1944.71 34.30 3 0 0 1954.80 34.90 3 0 0 1940.01 34.80 -4 0 0 127.49 5.10 -4 0 0 130.69 4.20 -4 0 0 124.59 3.40 -4 0 0 129.59 5.00 4 0 0 130.09 3.50 4 0 0 141.29 4.20 -5 0 0 31.60 3.50 -5 0 0 25.80 3.10 -5 0 0 33.50 2.00 -5 0 0 35.50 2.80 5 0 0 34.50 2.70 5 0 0 29.70 2.00 -6 0 0 429.06 12.10 -6 0 0 423.56 9.00 -6 0 0 440.26 10.60 6 0 0 426.36 9.20 6 0 0 427.66 10.50 -7 0 0 10.40 3.50 -7 0 0 15.20 1.90 -7 0 0 18.30 2.90 7 0 0 16.30 2.70 7 0 0 18.50 2.10 7 0 0 13.20 3.30 -8 0 0 12.20 4.00 -8 0 0 11.80 1.90 -8 0 0 13.80 3.10 8 0 0 14.90 2.20 8 0 0 11.40 2.90 8 0 0 12.90 3.70 -9 0 0 321.97 12.80 -9 0 0 318.27 10.30 9 0 0 335.47 10.70 9 0 0 343.77 12.60 -10 0 0 7.70 5.20 -10 0 0 3.90 3.50 10 0 0 9.60 4.80 10 0 0 6.50 3.50 -11 0 0 16.70 4.60 -11 0 0 14.60 6.00 11 0 0 11.20 4.50 11 0 0 19.50 5.90 -12 0 0 24.20 7.70 -12 0 0 22.30 5.20 12 0 0 23.50 6.70 12 0 0 19.60 5.40 -13 0 0 8.20 9.50 13 -1 0 121.29 11.70 -13 1 0 132.89 12.00 -13 1 0 105.29 8.50 12 -1 0 11.50 6.00 12 -1 0 11.40 4.60 -12 1 0 10.10 6.50 -12 1 0 11.80 4.60 11 -1 0 -3.60 3.40 11 -1 0 -0.80 4.60 -11 1 0 -3.90 3.80 -11 1 0 2.40 5.30 10 -1 0 20.90 5.30 10 -1 0 15.60 3.90 -10 1 0 15.80 4.10 -10 1 0 8.30 5.10 9 -1 0 291.17 11.60 9 -1 0 292.47 9.70 -9 1 0 319.37 11.30 -9 1 0 303.47 12.20 -9 1 0 287.37 9.80 8 -1 0 12.70 2.80 8 -1 0 7.00 1.70 8 -1 0 8.90 3.60 -8 1 0 11.20 3.90 -8 1 0 7.20 1.90 -8 1 0 9.10 3.00 7 -1 0 90.09 6.00 7 -1 0 95.19 3.50 7 -1 0 96.59 4.70 -7 1 0 97.99 5.10 -7 1 0 91.09 3.80 -7 1 0 97.09 6.30 6 -1 0 63.19 3.50 6 -1 0 57.19 4.20 6 -1 0 58.49 2.60 -6 1 0 59.09 4.90 -6 1 0 56.99 3.70 -6 1 0 61.79 2.90 5 -1 0 152.58 4.70 5 -1 0 158.68 5.90 5 -1 0 157.98 4.00 -5 1 0 159.78 4.40 -5 1 0 158.18 6.20 -5 1 0 162.38 5.30 4 -1 0 587.84 13.10 4 -1 0 615.14 12.00 4 -1 0 605.14 11.70 4 -1 0 586.94 11.30 -4 1 0 597.54 11.70 -4 1 0 609.64 13.50 -4 1 0 601.04 12.40 3 -1 0 444.56 9.90 3 -1 0 462.75 9.10 3 -1 0 458.85 8.60 -3 1 0 470.25 8.60 -3 1 0 459.05 9.10 -3 1 0 473.95 9.60 -3 1 0 469.35 10.30 2 -1 0 27.60 1.10 2 -1 0 25.30 1.40 2 -1 0 24.70 1.80 2 -1 0 26.00 1.20 -2 1 0 26.00 1.40 -2 1 0 25.60 1.70 -2 1 0 27.80 1.10 -2 1 0 26.60 2.00 -2 1 0 29.50 1.20 1 -1 0 377.76 7.20 1 -1 0 390.06 7.40 1 -1 0 382.86 7.10 1 -1 0 371.96 6.80 1 -1 0 379.96 6.70 -1 1 0 383.76 6.70 -1 1 0 377.06 7.10 -1 1 0 382.76 7.20 -1 1 0 376.86 6.80 -1 1 0 374.16 7.10 0 -1 0 923.61 17.30 0 -1 0 935.91 16.50 0 -1 0 925.41 16.30 0 -1 0 916.41 16.80 0 -1 0 947.81 17.40 0 -1 0 903.01 16.60 0 1 0 934.01 16.90 0 1 0 910.41 16.40 0 1 0 958.10 16.80 0 1 0 899.01 17.00 0 1 0 949.31 17.10 -1 -1 0 966.10 17.40 -1 -1 0 995.50 17.00 -1 -1 0 963.30 17.20 -1 -1 0 971.00 16.80 -1 -1 0 983.90 17.50 1 1 0 948.71 17.00 1 1 0 978.00 17.30 1 1 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100.89 5.60 8 4 0 113.09 7.40 8 4 0 120.89 6.20 -9 -4 0 24.30 6.50 -9 -4 0 16.20 5.80 9 4 0 24.90 5.30 -10 -4 0 5.50 5.60 10 4 0 5.60 4.50 -11 -4 0 21.90 7.20 11 4 0 26.70 7.40 11 4 0 21.00 6.10 13 -5 0 -4.50 5.90 13 -5 0 10.90 6.30 -13 5 0 3.40 5.10 12 -5 0 34.20 6.90 12 -5 0 41.90 7.50 -12 5 0 28.20 5.60 11 -5 0 36.30 6.40 11 -5 0 43.10 6.90 -11 5 0 37.00 5.50 -11 5 0 40.80 4.40 10 -5 0 7.70 4.70 10 -5 0 1.80 4.00 -10 5 0 8.70 3.90 -10 5 0 0.20 2.40 9 -5 0 71.69 6.90 9 -5 0 102.49 7.50 9 -5 0 84.59 4.30 -9 5 0 83.39 6.10 -9 5 0 82.69 5.20 8 -5 0 1.70 1.60 8 -5 0 0.30 2.90 8 -5 0 -1.00 3.10 -8 5 0 2.60 2.70 -8 5 0 4.50 2.20 7 -5 0 299.87 9.70 7 -5 0 283.27 6.90 7 -5 0 303.87 10.30 -7 5 0 302.47 9.10 -7 5 0 292.87 8.40 -7 5 0 290.77 6.50 6 -5 0 525.35 13.20 6 -5 0 523.05 13.70 6 -5 0 525.45 10.50 -6 5 0 540.65 12.30 -6 5 0 523.75 12.50 -6 5 0 522.15 10.50 5 -5 0 48.90 1.70 5 -5 0 48.00 3.60 5 -5 0 47.50 1.80 5 -5 0 51.89 4.10 -5 5 0 55.09 2.40 -5 5 0 52.69 3.40 -5 5 0 50.79 3.50 4 -5 0 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4.20 -5 -5 0 24.60 4.10 -5 -5 0 32.70 2.70 5 5 0 28.00 3.50 5 5 0 35.50 3.50 -6 -5 0 89.99 7.10 -6 -5 0 100.89 4.50 -6 -5 0 86.09 6.90 6 5 0 94.39 6.00 6 5 0 94.49 5.40 -7 -5 0 39.60 5.90 -7 -5 0 27.80 5.50 -7 -5 0 27.50 3.20 7 5 0 30.10 4.70 7 5 0 27.70 3.80 -8 -5 0 107.59 9.10 -8 -5 0 122.89 9.20 8 5 0 110.39 7.90 8 5 0 116.19 6.50 -9 -5 0 6.30 5.40 -9 -5 0 7.50 5.80 9 5 0 2.30 4.50 -10 -5 0 39.10 7.90 10 5 0 30.00 6.20 -11 -5 0 115.39 11.50 11 5 0 99.89 10.90 11 5 0 119.99 10.10 14 -6 0 10.30 10.90 13 -6 0 14.20 6.70 13 -6 0 10.50 6.30 -13 6 0 13.30 5.60 12 -6 0 27.70 7.30 12 -6 0 27.10 6.60 -12 6 0 23.50 5.40 11 -6 0 73.59 7.90 11 -6 0 74.89 8.30 -11 6 0 55.39 5.10 -11 6 0 63.99 6.40 10 -6 0 143.09 9.10 10 -6 0 148.79 9.40 -10 6 0 131.09 6.70 -10 6 0 139.59 7.80 9 -6 0 299.67 12.10 9 -6 0 305.17 11.40 -9 6 0 282.97 10.10 -9 6 0 294.87 9.40 8 -6 0 186.38 8.10 8 -6 0 173.28 8.50 8 -6 0 172.18 5.00 -8 6 0 161.28 6.70 -8 6 0 178.38 7.40 7 -6 0 696.63 16.80 7 -6 0 677.63 13.20 7 -6 0 699.73 17.60 -7 6 0 666.03 15.60 -7 6 0 692.83 16.10 -7 6 0 687.53 13.40 6 -6 0 357.76 10.90 6 -6 0 347.57 6.90 6 -6 0 369.56 10.30 6 -6 0 334.87 6.90 -6 6 0 355.56 7.80 -6 6 0 350.86 9.50 -6 6 0 363.26 9.70 5 -6 0 627.74 14.90 5 -6 0 630.44 14.20 -5 6 0 606.34 12.40 -5 6 0 619.34 13.90 -5 6 0 604.84 13.60 4 -6 0 99.19 5.00 4 -6 0 112.49 4.60 -4 6 0 114.39 4.60 -4 6 0 100.49 3.60 -4 6 0 114.99 4.40 3 -6 0 313.77 8.20 3 -6 0 321.47 8.70 -3 6 0 320.87 6.00 -3 6 0 334.37 7.60 -3 6 0 327.67 7.60 -3 6 0 320.47 8.20 -3 6 0 325.37 6.00 2 -6 0 847.62 17.20 2 -6 0 821.02 16.60 -2 6 0 829.52 16.40 -2 6 0 818.62 15.80 -2 6 0 812.72 16.60 1 -6 0 304.97 8.10 1 -6 0 301.37 7.60 1 -6 0 301.37 6.60 -1 6 0 313.67 7.70 -1 6 0 303.67 6.80 -1 6 0 316.97 7.50 0 -6 0 213.58 6.60 0 -6 0 209.88 4.60 0 -6 0 201.68 6.00 0 6 0 206.48 5.50 0 6 0 212.38 6.10 0 6 0 194.18 5.40 -1 -6 0 108.19 4.60 -1 -6 0 115.19 2.90 -1 -6 0 112.49 3.00 -1 -6 0 106.89 4.80 1 6 0 119.19 4.60 1 6 0 115.39 3.80 1 6 0 109.79 4.30 -2 -6 0 1.50 1.00 -2 -6 0 1.60 2.10 -2 -6 0 3.00 2.20 2 6 0 0.50 1.20 2 6 0 3.10 1.80 2 6 0 0.50 1.50 -3 -6 0 81.79 3.00 -3 -6 0 87.29 5.50 -3 -6 0 73.99 5.00 3 6 0 87.29 3.00 3 6 0 89.39 4.60 3 6 0 79.09 4.50 -4 -6 0 29.30 4.20 -4 -6 0 22.90 3.90 -4 -6 0 23.60 2.10 4 6 0 25.50 3.40 4 6 0 23.00 3.10 -5 -6 0 104.29 6.90 -5 -6 0 104.49 6.80 -5 -6 0 96.39 4.00 5 6 0 100.59 5.90 5 6 0 103.69 5.70 -6 -6 0 102.69 7.70 -6 -6 0 108.89 7.70 6 6 0 104.89 6.10 6 6 0 110.39 6.70 -7 -6 0 105.99 8.70 -7 -6 0 104.59 8.70 7 6 0 112.69 6.60 7 6 0 107.19 7.40 -8 -6 0 324.37 14.20 -8 -6 0 299.67 13.70 8 6 0 309.97 12.20 8 6 0 328.37 10.70 -9 -6 0 132.19 11.10 -9 -6 0 137.09 11.40 9 6 0 157.68 9.90 -10 -6 0 5.10 6.20 -10 -6 0 1.50 6.90 10 6 0 2.70 5.30 14 -7 0 3.90 8.40 13 -7 0 3.20 6.20 13 -7 0 6.00 6.30 -13 7 0 12.50 5.40 12 -7 0 13.60 6.10 12 -7 0 8.80 5.80 -12 7 0 14.90 5.20 -12 7 0 15.30 4.10 11 -7 0 95.39 9.00 11 -7 0 90.89 8.50 -11 7 0 82.29 7.10 -11 7 0 90.89 6.50 10 -7 0 4.90 4.50 10 -7 0 17.00 5.30 -10 7 0 5.70 3.90 -10 7 0 3.30 2.90 9 -7 0 21.40 4.70 9 -7 0 24.80 5.30 -9 7 0 21.70 3.50 -9 7 0 20.80 4.00 8 -7 0 61.19 6.30 8 -7 0 63.99 5.80 -8 7 0 56.99 4.70 -8 7 0 55.19 5.00 7 -7 0 7.90 3.30 7 -7 0 8.50 3.60 -7 7 0 9.80 2.70 -7 7 0 6.80 1.50 -7 7 0 10.10 2.90 6 -7 0 94.29 5.50 6 -7 0 100.09 6.20 -6 7 0 92.39 5.00 -6 7 0 87.69 3.60 -6 7 0 84.39 4.80 5 -7 0 2130.79 40.90 5 -7 0 2113.69 40.20 -5 7 0 2101.39 40.10 -5 7 0 2111.69 38.50 -5 7 0 2143.99 39.60 4 -7 0 123.99 5.70 4 -7 0 118.89 5.20 -4 7 0 111.99 4.10 -4 7 0 107.99 4.80 -4 7 0 105.69 4.40 3 -7 0 179.18 6.00 3 -7 0 171.98 6.60 -3 7 0 165.08 5.20 -3 7 0 164.18 3.70 -3 7 0 163.98 3.70 -3 7 0 162.88 5.00 -3 7 0 175.48 5.80 2 -7 0 12.80 2.80 2 -7 0 10.30 2.30 -2 7 0 15.80 1.70 -2 7 0 13.60 2.10 -2 7 0 15.20 1.40 -2 7 0 13.70 2.10 1 -7 0 1021.00 19.20 1 -7 0 1018.80 20.50 1 -7 0 1063.69 21.20 -1 7 0 1052.39 20.70 -1 7 0 1035.50 19.60 -1 7 0 1028.60 20.30 0 -7 0 417.26 10.20 0 -7 0 422.86 8.50 0 -7 0 447.46 10.80 0 7 0 416.06 9.60 0 7 0 412.46 9.60 0 7 0 437.16 10.30 -1 -7 0 782.62 14.60 -1 -7 0 773.72 16.90 -1 -7 0 814.82 17.30 1 7 0 795.22 16.50 1 7 0 784.52 15.70 1 7 0 793.82 16.90 -2 -7 0 -1.60 2.30 -2 -7 0 1.40 1.00 -2 -7 0 -3.40 2.30 2 7 0 1.00 1.80 2 7 0 0.50 1.30 2 7 0 2.00 2.00 -3 -7 0 11.80 3.20 -3 -7 0 10.00 3.30 -3 -7 0 15.90 1.60 3 7 0 13.60 2.80 3 7 0 10.90 2.70 3 7 0 9.70 1.60 -4 -7 0 1466.95 26.60 -4 -7 0 1454.05 30.80 -4 -7 0 1401.76 30.50 4 7 0 1496.65 29.40 4 7 0 1455.25 29.80 -5 -7 0 63.09 6.20 -5 -7 0 57.29 6.00 5 7 0 52.29 4.80 5 7 0 52.59 5.00 -6 -7 0 -0.80 3.90 -6 -7 0 1.30 4.20 6 7 0 5.30 3.20 6 7 0 3.60 3.60 -7 -7 0 10.80 5.30 -7 -7 0 14.80 5.40 7 7 0 18.10 4.60 7 7 0 18.30 4.00 -8 -7 0 38.80 7.60 -8 -7 0 39.50 7.30 8 7 0 42.90 6.30 8 7 0 43.70 5.30 -9 -7 0 39.50 8.00 -9 -7 0 34.00 7.80 9 7 0 37.00 6.60 -10 -7 0 67.89 10.00 -10 -7 0 77.39 10.40 10 7 0 86.69 9.00 14 -8 0 39.70 11.20 13 -8 0 7.80 6.40 13 -8 0 -0.80 5.90 -13 8 0 -6.70 4.70 12 -8 0 109.59 9.80 12 -8 0 99.19 9.80 -12 8 0 107.99 8.60 -12 8 0 99.39 7.30 11 -8 0 5.60 5.00 11 -8 0 2.70 5.20 -11 8 0 3.00 3.50 -11 8 0 -0.40 4.00 10 -8 0 64.59 7.20 10 -8 0 48.90 6.80 -10 8 0 47.30 5.60 -10 8 0 48.20 5.00 9 -8 0 253.17 11.60 9 -8 0 241.48 10.10 -9 8 0 254.67 9.60 -9 8 0 250.47 9.30 8 -8 0 2.10 3.30 8 -8 0 5.10 3.80 -8 8 0 6.60 2.80 -8 8 0 5.10 3.00 7 -8 0 4.00 3.50 7 -8 0 4.20 3.10 -7 8 0 3.90 1.60 -7 8 0 3.80 2.50 -7 8 0 7.70 2.80 6 -8 0 223.08 8.20 6 -8 0 216.78 8.80 -6 8 0 228.18 7.90 -6 8 0 215.68 7.40 -6 8 0 229.18 6.40 5 -8 0 161.78 7.30 5 -8 0 159.88 6.50 -5 8 0 167.28 6.40 -5 8 0 152.68 5.90 -5 8 0 164.88 5.40 4 -8 0 11.30 2.90 4 -8 0 15.50 3.50 -4 8 0 11.60 2.00 -4 8 0 9.40 2.10 -4 8 0 11.70 2.50 3 -8 0 893.31 19.40 3 -8 0 858.91 18.50 -3 8 0 904.71 18.20 -3 8 0 873.81 16.20 -3 8 0 890.31 18.70 -3 8 0 891.51 17.60 2 -8 0 4.30 1.60 2 -8 0 2.40 2.30 2 -8 0 7.10 2.90 -2 8 0 4.70 1.20 -2 8 0 1.80 1.70 -2 8 0 2.60 1.70 1 -8 0 9.50 2.60 1 -8 0 15.70 1.80 1 -8 0 14.60 3.20 -1 8 0 10.40 1.80 -1 8 0 14.00 2.40 -1 8 0 14.00 2.20 0 -8 0 80.09 4.70 0 -8 0 81.89 2.90 0 -8 0 86.29 5.40 0 8 0 83.89 4.50 0 8 0 89.79 4.00 0 8 0 78.99 3.90 -1 -8 0 140.49 3.80 -1 -8 0 147.59 6.80 -1 -8 0 144.19 6.10 1 8 0 146.39 5.90 1 8 0 139.89 5.40 1 8 0 146.89 5.00 -2 -8 0 3.20 2.80 -2 -8 0 3.90 1.10 -2 -8 0 7.00 3.00 2 8 0 -2.50 2.10 2 8 0 3.60 2.30 2 8 0 1.90 1.60 -3 -8 0 348.07 11.10 -3 -8 0 371.16 11.60 3 8 0 366.16 10.50 3 8 0 365.06 8.20 3 8 0 366.66 10.60 -4 -8 0 128.39 7.50 -4 -8 0 114.89 7.40 4 8 0 124.29 6.70 4 8 0 130.99 6.70 -5 -8 0 19.00 4.90 -5 -8 0 20.60 4.80 5 8 0 13.30 3.80 5 8 0 18.30 3.80 -6 -8 0 35.90 6.00 -6 -8 0 14.50 5.30 6 8 0 22.10 4.80 6 8 0 26.20 4.40 -7 -8 0 4.40 5.30 -7 -8 0 6.20 5.90 7 8 0 11.60 4.10 7 8 0 8.90 4.40 -8 -8 0 60.49 8.70 -8 -8 0 56.89 8.30 8 8 0 66.19 6.50 8 8 0 76.59 7.70 -9 -8 0 -2.70 6.70 -9 -8 0 0.10 6.40 9 8 0 1.10 5.50 13 -9 0 3.00 6.00 13 -9 0 19.20 7.50 -13 9 0 8.40 5.50 -13 9 0 13.20 4.70 12 -9 0 11.10 5.80 12 -9 0 13.20 6.40 -12 9 0 13.60 5.20 -12 9 0 10.30 4.20 11 -9 0 16.00 5.50 11 -9 0 -2.20 5.50 -11 9 0 8.20 3.90 -11 9 0 5.80 4.70 10 -9 0 4.20 4.40 10 -9 0 1.30 4.80 -10 9 0 2.50 3.30 -10 9 0 -3.80 3.50 9 -9 0 41.50 5.50 9 -9 0 32.70 5.60 -9 9 0 32.90 4.60 -9 9 0 37.60 4.90 8 -9 0 1.50 3.50 8 -9 0 -5.90 3.60 -8 9 0 0.50 2.80 -8 9 0 -1.60 2.70 7 -9 0 161.78 7.60 7 -9 0 163.18 8.60 -7 9 0 158.48 5.40 -7 9 0 148.49 7.20 -7 9 0 144.79 6.70 6 -9 0 44.50 5.00 6 -9 0 45.50 4.60 -6 9 0 48.40 3.40 -6 9 0 44.20 4.20 -6 9 0 47.20 4.20 5 -9 0 49.10 4.60 5 -9 0 44.50 5.10 -5 9 0 37.20 3.90 -5 9 0 43.80 3.70 -5 9 0 40.70 3.30 4 -9 0 167.38 6.90 4 -9 0 166.08 7.70 -4 9 0 155.68 5.80 -4 9 0 157.28 6.40 -4 9 0 154.08 5.50 3 -9 0 15.50 3.20 3 -9 0 11.60 3.60 -3 9 0 17.10 2.80 -3 9 0 20.10 2.70 -3 9 0 15.70 2.20 -3 9 0 17.30 1.60 2 -9 0 4.50 1.80 2 -9 0 3.70 2.70 2 -9 0 5.70 3.40 -2 9 0 5.80 2.20 -2 9 0 3.80 1.40 -2 9 0 6.40 2.20 1 -9 0 767.32 15.30 1 -9 0 794.52 17.30 1 -9 0 808.42 18.10 -1 9 0 819.62 16.40 -1 9 0 796.82 17.50 -1 9 0 790.32 17.00 0 -9 0 143.19 4.10 0 -9 0 146.29 7.00 0 -9 0 148.39 6.40 0 9 0 146.59 6.30 0 9 0 153.88 5.60 0 9 0 147.49 5.50 -1 -9 0 44.00 2.30 -1 -9 0 35.10 4.10 -1 -9 0 45.10 4.70 1 9 0 40.40 4.00 1 9 0 44.40 3.80 1 9 0 43.80 3.30 -2 -9 0 655.33 16.30 -2 -9 0 653.03 16.70 2 9 0 651.83 16.00 2 9 0 674.73 15.80 2 9 0 676.23 14.00 -3 -9 0 7.40 3.80 -3 -9 0 3.70 3.50 3 9 0 8.30 3.10 3 9 0 3.30 2.80 -4 -9 0 89.69 7.30 -4 -9 0 70.89 6.60 4 9 0 74.99 6.10 4 9 0 71.99 5.80 -5 -9 0 45.50 6.20 -5 -9 0 37.80 6.00 5 9 0 37.60 5.00 5 9 0 56.49 6.00 -6 -9 0 3.90 5.10 -6 -9 0 2.40 5.20 6 9 0 3.60 3.80 6 9 0 15.80 4.90 -7 -9 0 20.10 6.70 -7 -9 0 15.60 6.50 7 9 0 15.00 4.70 7 9 0 29.00 5.90 -8 -9 0 98.29 10.40 -8 -9 0 82.49 9.60 8 9 0 98.79 8.70 8 9 0 99.39 7.90 -9 -9 0 7.80 7.10 13 -10 0 97.79 10.00 13 -10 0 81.89 10.20 -13 10 0 93.59 8.80 -13 10 0 117.29 8.70 12 -10 0 -1.40 5.10 12 -10 0 6.40 6.30 -12 10 0 -0.50 3.80 -12 10 0 -4.20 4.60 11 -10 0 77.59 8.50 11 -10 0 70.79 7.90 -11 10 0 57.39 6.20 -11 10 0 70.29 6.90 10 -10 0 4.60 4.60 10 -10 0 1.00 4.80 -10 10 0 -2.50 3.70 -10 10 0 3.10 3.70 9 -10 0 13.70 4.80 9 -10 0 23.10 5.50 -9 10 0 13.50 4.10 -9 10 0 12.80 3.90 8 -10 0 15.70 4.30 8 -10 0 9.60 4.80 -8 10 0 10.90 3.50 -8 10 0 12.80 3.50 7 -10 0 55.69 5.60 7 -10 0 49.30 5.90 -7 10 0 42.70 4.70 -7 10 0 45.70 4.50 -7 10 0 49.30 3.80 6 -10 0 200.48 9.40 6 -10 0 206.48 8.50 -6 10 0 192.08 6.70 -6 10 0 203.58 7.40 -6 10 0 214.58 8.30 5 -10 0 393.16 11.50 5 -10 0 401.16 12.50 -5 10 0 410.66 10.50 -5 10 0 391.36 10.40 -5 10 0 385.96 11.40 4 -10 0 69.79 6.10 4 -10 0 76.99 5.60 -4 10 0 70.69 4.50 -4 10 0 70.39 4.10 -4 10 0 76.59 5.30 3 -10 0 23.50 4.40 3 -10 0 24.60 2.90 3 -10 0 31.30 4.10 -3 10 0 27.30 3.50 -3 10 0 28.50 2.10 -3 10 0 24.00 3.10 2 -10 0 245.28 8.30 2 -10 0 265.77 9.40 2 -10 0 256.77 6.80 -2 10 0 241.78 8.10 -2 10 0 259.37 8.20 -2 10 0 244.28 6.70 1 -10 0 253.87 9.40 1 -10 0 237.58 8.20 1 -10 0 234.78 6.10 -1 10 0 260.27 8.50 -1 10 0 227.68 7.60 -1 10 0 246.58 7.10 0 -10 0 247.38 5.90 0 -10 0 250.57 9.30 0 -10 0 243.98 8.80 0 10 0 254.97 7.70 0 10 0 251.97 7.70 0 10 0 256.07 8.80 -1 -10 0 44.30 5.00 -1 -10 0 37.50 4.50 1 10 0 41.00 4.10 1 10 0 36.70 3.40 1 10 0 39.00 4.30 -2 -10 0 13.00 3.80 -2 -10 0 8.00 3.70 2 10 0 10.30 2.30 2 10 0 9.80 3.40 2 10 0 9.00 3.00 -3 -10 0 67.39 6.80 -3 -10 0 65.69 6.30 3 10 0 66.29 5.70 3 10 0 58.69 5.40 -4 -10 0 241.18 10.80 -4 -10 0 235.28 10.90 4 10 0 226.38 9.70 4 10 0 236.98 9.70 -5 -10 0 15.20 5.40 -5 -10 0 13.10 5.20 5 10 0 13.00 4.40 5 10 0 6.50 4.10 -6 -10 0 31.80 6.60 -6 -10 0 24.70 6.60 6 10 0 27.80 5.50 6 10 0 29.20 5.80 -7 -10 0 7.30 6.10 -7 -10 0 8.20 6.50 7 10 0 19.20 5.90 7 10 0 12.50 5.10 -8 -10 0 2.50 6.10 -8 -10 0 10.40 7.20 8 10 0 -3.30 5.40 8 10 0 -6.00 4.50 13 -11 0 -4.30 6.00 -13 11 0 13.90 5.00 12 -11 0 -6.80 5.40 12 -11 0 9.80 6.70 -12 11 0 4.20 4.90 -12 11 0 5.80 4.50 11 -11 0 28.50 6.50 11 -11 0 39.70 7.60 -11 11 0 44.10 6.30 -11 11 0 43.50 6.00 10 -11 0 55.09 7.00 10 -11 0 61.39 7.90 -10 11 0 52.99 6.10 -10 11 0 74.09 6.90 9 -11 0 252.27 12.00 9 -11 0 251.47 10.90 -9 11 0 266.67 10.30 -9 11 0 281.67 11.10 8 -11 0 164.98 8.80 8 -11 0 164.48 10.30 -8 11 0 162.18 8.40 -8 11 0 168.38 7.90 7 -11 0 109.99 8.30 7 -11 0 97.49 7.30 -7 11 0 93.59 6.00 -7 11 0 109.69 7.10 -7 11 0 105.49 5.40 6 -11 0 98.79 7.60 6 -11 0 103.09 7.10 -6 11 0 112.19 6.70 -6 11 0 112.29 6.00 -6 11 0 103.39 5.50 5 -11 0 -1.40 3.90 5 -11 0 4.60 3.50 -5 11 0 0.70 2.40 -5 11 0 3.50 2.80 -5 11 0 5.20 2.50 4 -11 0 139.59 6.90 4 -11 0 145.79 8.20 -4 11 0 154.18 7.20 -4 11 0 143.39 6.60 3 -11 0 373.06 12.20 3 -11 0 362.46 9.40 3 -11 0 360.66 10.90 -3 11 0 377.46 10.80 -3 11 0 377.06 8.50 -3 11 0 365.26 10.70 2 -11 0 17.00 3.70 2 -11 0 19.60 2.50 2 -11 0 20.50 4.40 -2 11 0 16.80 3.20 -2 11 0 22.90 2.60 -2 11 0 22.60 3.40 1 -11 0 5.50 3.60 1 -11 0 7.00 3.20 1 -11 0 8.30 2.00 -1 11 0 5.30 2.20 -1 11 0 5.30 2.90 -1 11 0 10.00 2.80 0 -11 0 183.68 8.00 0 -11 0 168.48 8.00 0 11 0 175.98 7.90 0 11 0 171.88 6.70 0 11 0 178.98 6.80 -1 -11 0 189.68 8.80 -1 -11 0 199.08 8.90 1 11 0 190.78 7.70 1 11 0 205.98 7.00 1 11 0 197.48 8.60 -2 -11 0 116.89 8.10 -2 -11 0 120.99 7.90 2 11 0 107.09 7.30 2 11 0 106.09 6.40 -3 -11 0 112.29 8.40 -3 -11 0 118.19 8.90 3 11 0 100.99 7.00 3 11 0 111.49 7.80 -4 -11 0 12.00 5.20 -4 -11 0 2.90 4.90 4 11 0 -0.10 3.80 4 11 0 0.60 3.80 -5 -11 0 -0.20 5.10 -5 -11 0 0.30 5.30 5 11 0 0.30 4.30 5 11 0 0.30 4.20 -6 -11 0 187.68 12.00 -6 -11 0 187.18 12.70 6 11 0 179.58 10.60 6 11 0 184.48 10.50 -7 -11 0 18.30 7.00 -7 -11 0 23.70 7.50 7 11 0 10.10 5.20 7 11 0 5.80 5.70 8 11 0 27.80 6.20 13 -12 0 19.80 7.60 -13 12 0 28.60 6.20 12 -12 0 26.10 7.70 12 -12 0 31.90 7.30 -12 12 0 30.00 5.80 -12 12 0 33.50 6.40 11 -12 0 27.00 7.30 11 -12 0 7.50 5.70 -11 12 0 28.30 5.70 -11 12 0 14.10 5.30 10 -12 0 10.60 5.40 10 -12 0 23.50 6.90 -10 12 0 27.50 5.20 -10 12 0 23.00 5.20 9 -12 0 3.40 4.60 9 -12 0 3.70 5.50 -9 12 0 3.40 3.80 -9 12 0 4.20 3.90 8 -12 0 34.00 5.50 8 -12 0 32.70 6.20 -8 12 0 31.40 4.60 -8 12 0 23.50 4.90 7 -12 0 316.57 12.80 7 -12 0 301.47 11.40 -7 12 0 324.57 11.60 -7 12 0 319.07 9.60 -7 12 0 320.17 10.40 6 -12 0 28.70 5.70 6 -12 0 36.50 5.20 -6 12 0 31.00 3.90 -6 12 0 32.80 4.40 -6 12 0 38.00 4.10 5 -12 0 2.50 3.70 5 -12 0 3.00 4.40 -5 12 0 3.10 3.10 -5 12 0 4.50 2.70 4 -12 0 25.20 4.50 4 -12 0 20.30 4.90 4 -12 0 20.40 3.30 -4 12 0 18.60 3.60 -4 12 0 28.70 4.20 3 -12 0 1.50 2.40 3 -12 0 9.40 4.40 3 -12 0 2.00 3.50 -3 12 0 3.90 2.80 -3 12 0 1.20 2.90 2 -12 0 258.17 9.40 2 -12 0 259.97 10.50 -2 12 0 245.88 7.40 -2 12 0 254.07 9.40 -2 12 0 261.67 9.10 1 -12 0 61.19 5.60 1 -12 0 59.39 6.00 -1 12 0 56.79 5.40 -1 12 0 67.59 5.20 -1 12 0 64.29 4.60 0 -12 0 6.00 4.00 0 -12 0 9.20 3.90 0 12 0 10.60 3.80 0 12 0 11.10 3.10 0 12 0 5.00 2.90 -1 -12 0 104.69 7.90 -1 -12 0 95.79 7.20 1 12 0 108.29 6.50 1 12 0 93.79 6.70 1 12 0 111.59 7.60 -2 -12 0 253.07 11.10 -2 -12 0 222.88 10.40 2 12 0 257.17 10.70 2 12 0 250.67 9.60 -3 -12 0 13.50 5.30 -3 -12 0 9.70 5.20 3 12 0 6.60 4.30 3 12 0 10.30 4.30 -4 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139.79 5.90 4 5 -3 125.69 5.10 -4 -5 3 140.49 6.60 -4 -5 3 138.29 5.00 -4 -5 3 135.89 6.60 3 5 -3 34.50 3.10 3 5 -3 37.70 3.00 -3 -5 3 37.20 2.70 -3 -5 3 35.40 3.50 -3 -5 3 40.60 4.00 2 5 -3 -0.60 1.50 2 5 -3 1.60 0.70 2 5 -3 0.40 1.40 -2 -5 3 4.70 1.80 -2 -5 3 2.10 0.80 -2 -5 3 5.50 2.10 -2 -5 3 1.70 1.30 1 5 -3 483.85 9.30 1 5 -3 476.05 10.30 1 5 -3 482.75 10.50 -1 -5 3 452.85 9.60 -1 -5 3 460.25 10.90 -1 -5 3 469.35 10.30 0 5 -3 113.89 4.00 0 5 -3 114.79 3.40 0 5 -3 110.29 3.60 0 -5 3 109.49 3.40 0 -5 3 107.09 3.60 0 -5 3 116.09 4.60 -1 5 -3 62.49 2.70 -1 5 -3 63.09 2.90 -1 5 -3 55.89 2.20 1 -5 3 62.79 2.60 1 -5 3 57.99 2.50 1 -5 3 61.09 3.60 -2 5 -3 468.85 9.90 -2 5 -3 461.05 9.90 -2 5 -3 438.76 8.40 2 -5 3 442.86 8.40 2 -5 3 433.16 9.50 2 -5 3 460.35 9.30 2 -5 3 460.45 10.50 -3 5 -3 26.80 2.10 -3 5 -3 39.10 2.70 -3 5 -3 33.90 2.60 3 -5 3 32.10 2.40 3 -5 3 28.50 2.90 -4 5 -3 213.48 6.10 -4 5 -3 222.18 5.80 -4 5 -3 223.38 6.40 4 -5 3 221.78 6.20 4 -5 3 225.08 7.20 -5 5 -3 8.00 1.50 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103.19 6.90 -10 4 -3 115.29 6.10 10 -4 3 112.09 5.70 10 -4 3 118.99 8.40 -11 4 -3 38.50 4.40 -11 4 -3 39.60 5.50 11 -4 3 38.90 6.40 -12 4 -3 -0.30 4.20 12 -4 3 2.20 5.70 12 -4 3 5.30 5.70 -13 4 -3 73.69 7.40 13 -4 3 87.19 9.90 13 -4 3 69.89 9.10 12 3 -3 -3.30 4.90 11 3 -3 20.90 5.90 11 3 -3 22.20 6.70 -11 -3 3 28.90 7.70 10 3 -3 24.20 6.20 10 3 -3 28.70 5.60 -10 -3 3 31.10 4.90 -10 -3 3 29.30 6.90 9 3 -3 219.38 11.20 9 3 -3 245.28 10.30 -9 -3 3 229.88 9.00 -9 -3 3 230.48 11.90 8 3 -3 156.18 6.00 8 3 -3 172.58 8.20 -8 -3 3 161.28 9.50 -8 -3 3 149.39 7.10 7 3 -3 32.60 4.10 7 3 -3 37.30 3.20 -7 -3 3 32.70 5.20 -7 -3 3 33.90 3.80 -7 -3 3 30.20 4.90 6 3 -3 207.78 7.60 6 3 -3 195.38 6.10 -6 -3 3 197.18 6.90 -6 -3 3 186.48 8.60 -6 -3 3 199.88 8.60 5 3 -3 53.09 3.10 5 3 -3 57.79 4.10 -5 -3 3 48.30 4.50 -5 -3 3 46.90 4.60 -5 -3 3 48.40 3.60 4 3 -3 627.04 13.90 4 3 -3 614.74 12.80 -4 -3 3 608.44 14.50 -4 -3 3 629.04 14.70 -4 -3 3 617.14 13.20 3 3 -3 260.87 6.40 3 3 -3 269.27 7.10 -3 -3 3 243.38 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7.30 8 -11 4 113.39 9.10 8 -11 4 112.09 7.10 -9 11 -4 4.80 3.80 -9 11 -4 7.10 3.90 9 -11 4 0.50 4.80 9 -11 4 8.00 4.20 -10 11 -4 53.39 6.10 -10 11 -4 61.39 6.40 10 -11 4 55.79 6.60 10 -11 4 59.49 8.10 -11 11 -4 75.79 7.40 -11 11 -4 59.59 6.90 11 -11 4 58.39 8.50 -12 11 -4 -1.40 4.20 -12 11 -4 1.40 5.20 12 -11 4 0.10 6.60 -13 11 -4 -3.40 4.30 8 10 -4 10.50 5.90 -8 -10 4 12.00 7.50 -8 -10 4 9.50 7.20 7 10 -4 -0.30 4.80 7 10 -4 2.50 4.20 -7 -10 4 -3.10 5.90 -7 -10 4 5.30 6.60 6 10 -4 57.19 6.20 6 10 -4 66.19 7.30 -6 -10 4 45.10 7.50 -6 -10 4 44.20 7.40 5 10 -4 539.35 16.20 5 10 -4 569.04 15.90 -5 -10 4 540.95 17.40 -5 -10 4 538.25 18.20 4 10 -4 12.90 4.20 4 10 -4 11.60 3.90 -4 -10 4 7.00 4.50 -4 -10 4 10.10 5.10 3 10 -4 243.98 9.60 3 10 -4 256.27 9.60 -3 -10 4 270.77 11.40 -3 -10 4 247.28 10.10 2 10 -4 537.55 14.10 2 10 -4 561.74 14.60 -2 -10 4 544.85 15.40 -2 -10 4 545.35 14.70 -2 -10 4 513.65 13.50 1 10 -4 28.30 2.80 1 10 -4 31.20 4.10 1 10 -4 24.70 3.40 -1 -10 4 28.90 4.00 -1 -10 4 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2.40 -8 8 -4 12.00 3.30 8 -8 4 8.90 3.40 8 -8 4 7.80 4.20 -9 8 -4 5.70 3.10 -9 8 -4 3.60 3.30 9 -8 4 16.90 4.90 9 -8 4 8.40 3.90 -10 8 -4 49.60 5.20 -10 8 -4 40.20 5.20 10 -8 4 41.50 6.60 10 -8 4 59.79 6.40 -11 8 -4 6.10 4.30 -11 8 -4 2.70 3.60 11 -8 4 2.90 4.80 11 -8 4 2.80 5.40 -12 8 -4 2.70 4.80 -12 8 -4 -0.60 3.70 12 -8 4 -11.50 4.60 12 -8 4 -2.90 5.50 -13 8 -4 2.20 4.30 -13 8 -4 -3.10 5.20 13 -8 4 -4.00 6.00 13 -8 4 0.20 6.00 10 7 -4 12.60 6.60 10 7 -4 -1.60 5.60 -10 -7 4 -2.70 6.40 9 7 -4 -0.50 4.90 -9 -7 4 -3.70 6.30 -9 -7 4 -5.70 5.70 8 7 -4 58.29 7.70 8 7 -4 48.50 6.60 -8 -7 4 64.79 8.80 -8 -7 4 57.49 8.30 7 7 -4 30.40 4.30 7 7 -4 40.20 5.50 -7 -7 4 37.40 6.80 -7 -7 4 34.40 6.70 6 7 -4 105.69 7.20 6 7 -4 98.79 6.30 -6 -7 4 98.99 8.30 -6 -7 4 115.39 8.70 -6 -7 4 110.09 8.50 5 7 -4 2.00 2.70 5 7 -4 2.40 3.00 -5 -7 4 1.70 3.60 -5 -7 4 2.90 3.60 -5 -7 4 1.20 2.20 4 7 -4 20.10 3.20 4 7 -4 16.60 3.50 -4 -7 4 26.90 4.30 -4 -7 4 28.40 3.00 -4 -7 4 26.20 4.30 3 7 -4 3.40 2.40 3 7 -4 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56.39 3.40 -4 6 -4 50.99 3.40 -4 6 -4 49.50 3.10 4 -6 4 48.20 3.90 4 -6 4 50.19 3.10 -5 6 -4 60.09 3.90 -5 6 -4 62.29 3.40 -5 6 -4 59.09 3.80 5 -6 4 58.69 4.70 5 -6 4 62.79 3.60 -6 6 -4 209.08 7.00 -6 6 -4 217.18 6.30 -6 6 -4 216.38 7.10 6 -6 4 201.78 4.40 6 -6 4 227.78 8.50 6 -6 4 216.78 7.20 -7 6 -4 238.38 6.70 -7 6 -4 227.68 7.80 -7 6 -4 221.98 7.60 7 -6 4 212.38 5.10 7 -6 4 225.68 9.10 7 -6 4 229.98 8.10 -8 6 -4 20.50 3.50 -8 6 -4 26.40 3.50 -8 6 -4 27.50 2.80 8 -6 4 25.70 4.80 8 -6 4 25.50 4.10 -9 6 -4 2.70 2.70 -9 6 -4 1.40 3.00 9 -6 4 2.00 4.00 9 -6 4 -1.20 3.40 -10 6 -4 19.10 3.70 -10 6 -4 22.60 4.50 10 -6 4 22.30 5.50 10 -6 4 29.00 5.30 -11 6 -4 16.40 3.90 -11 6 -4 14.90 4.60 11 -6 4 8.70 5.30 11 -6 4 12.00 5.10 -12 6 -4 1.30 4.40 -12 6 -4 -1.50 3.50 12 -6 4 1.10 5.80 12 -6 4 4.20 5.20 -13 6 -4 25.60 6.10 13 -6 4 31.60 7.30 13 -6 4 34.60 7.70 14 -6 4 0.90 6.40 11 5 -4 15.00 5.90 11 5 -4 16.30 7.10 -11 -5 4 10.60 7.30 10 5 -4 9.60 5.70 10 5 -4 -2.30 4.80 -10 -5 4 7.10 6.50 9 5 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17.30 9 -5 4 738.43 20.00 9 -5 4 784.32 19.40 -10 5 -4 95.99 7.10 -10 5 -4 95.69 5.90 10 -5 4 81.69 7.80 10 -5 4 99.49 8.10 -11 5 -4 4.80 3.20 -11 5 -4 5.00 4.10 11 -5 4 5.50 4.90 11 -5 4 5.10 5.20 -12 5 -4 1.70 4.40 12 -5 4 6.30 6.20 12 -5 4 2.60 5.40 -13 5 -4 6.20 5.10 13 -5 4 14.30 6.50 13 -5 4 11.00 6.30 14 -5 4 -2.60 7.10 11 4 -4 45.90 7.10 11 4 -4 23.50 7.30 -11 -4 4 31.60 8.30 10 4 -4 38.30 7.00 10 4 -4 59.79 7.30 -10 -4 4 55.49 8.50 9 4 -4 1.30 3.90 9 4 -4 4.40 4.80 -9 -4 4 0.50 3.30 -9 -4 4 4.80 5.20 8 4 -4 88.69 6.30 8 4 -4 102.59 7.40 -8 -4 4 84.19 8.10 -8 -4 4 95.89 6.10 7 4 -4 256.27 9.50 7 4 -4 239.68 7.50 -7 -4 4 235.08 10.80 -7 -4 4 254.77 8.50 -7 -4 4 245.18 10.70 6 4 -4 3.50 2.40 6 4 -4 1.30 2.00 -6 -4 4 2.70 3.50 -6 -4 4 1.10 3.40 -6 -4 4 0.00 2.20 5 4 -4 33.50 3.80 5 4 -4 29.90 2.80 -5 -4 4 31.30 4.10 -5 -4 4 33.30 3.30 -5 -4 4 36.00 4.60 4 4 -4 523.35 12.60 4 4 -4 523.35 11.60 -4 -4 4 523.05 13.40 -4 -4 4 513.45 11.80 -4 -4 4 525.15 13.20 3 4 -4 4.00 1.40 3 4 -4 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13.30 4 -4 8 592.54 12.10 4 -4 8 623.44 13.70 4 -4 8 583.44 13.20 -5 4 -8 6.70 2.10 -5 4 -8 8.80 2.10 -5 4 -8 5.60 1.60 5 -4 8 7.40 2.30 5 -4 8 8.40 2.80 5 -4 8 4.80 1.80 -6 4 -8 414.66 9.40 -6 4 -8 403.06 10.50 -6 4 -8 417.66 10.50 -6 4 -8 400.66 10.50 6 -4 8 403.16 11.50 6 -4 8 407.06 10.40 -7 4 -8 77.29 4.00 -7 4 -8 70.79 4.70 -7 4 -8 77.39 4.70 -7 4 -8 71.49 4.80 7 -4 8 68.59 5.80 7 -4 8 69.79 5.00 -8 4 -8 107.49 5.50 -8 4 -8 110.59 5.90 -8 4 -8 111.89 6.00 8 -4 8 107.09 6.40 8 -4 8 110.59 5.00 8 -4 8 111.89 7.50 -9 4 -8 10.00 2.90 -9 4 -8 5.90 3.30 -9 4 -8 6.00 2.90 9 -4 8 7.90 2.70 9 -4 8 2.20 4.00 9 -4 8 7.10 3.80 -10 4 -8 218.48 8.60 -10 4 -8 213.58 9.30 10 -4 8 224.08 11.30 10 -4 8 214.58 10.40 -11 4 -8 15.30 4.60 -11 4 -8 21.90 4.20 11 -4 8 19.90 5.90 11 -4 8 14.00 5.60 -12 4 -8 2.50 4.30 12 -4 8 -0.10 5.20 12 -4 8 12.40 6.10 -13 4 -8 3.60 4.70 13 -4 8 -0.50 8.50 13 -4 8 8.90 6.30 11 3 -8 68.09 8.90 11 3 -8 83.49 8.60 -11 -3 8 81.79 7.70 -11 -3 8 83.89 10.00 10 3 -8 -3.10 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7.70 -3 14 -9 74.79 5.90 3 -14 9 72.79 7.90 3 -14 9 88.39 6.50 -4 14 -9 -0.90 4.00 -4 14 -9 -0.40 3.30 4 -14 9 7.10 4.30 4 -14 9 8.30 5.60 -5 14 -9 520.95 15.20 -5 14 -9 513.15 15.80 5 -14 9 479.45 16.90 5 -14 9 504.45 14.80 -6 14 -9 4.80 3.90 -6 14 -9 -2.00 3.80 6 -14 9 3.00 4.90 6 -14 9 3.00 6.10 -7 14 -9 3.60 4.10 -7 14 -9 3.50 4.20 7 -14 9 7.80 5.20 7 -14 9 0.40 6.20 -8 14 -9 2.80 4.00 -8 14 -9 3.50 4.30 8 -14 9 -6.20 4.90 8 -14 9 -4.60 6.80 -9 14 -9 174.08 10.70 9 -14 9 161.58 10.90 9 -14 9 160.88 12.60 -10 14 -9 41.70 6.50 10 -14 9 48.50 7.70 10 -14 9 27.40 8.30 6 13 -9 19.20 9.60 5 13 -9 23.30 6.10 5 13 -9 17.10 5.50 -5 -13 9 43.50 9.10 4 13 -9 86.09 8.10 4 13 -9 91.29 8.20 -4 -13 9 111.59 10.70 3 13 -9 19.60 5.40 3 13 -9 21.30 5.20 -3 -13 9 22.30 6.60 2 13 -9 -0.30 3.80 2 13 -9 -0.70 4.30 -2 -13 9 12.30 5.90 1 13 -9 97.89 7.00 1 13 -9 108.19 8.20 -1 -13 9 120.69 9.60 0 13 -9 47.40 5.90 0 13 -9 44.70 4.90 0 -13 9 45.30 6.40 -1 13 -9 49.40 6.10 -1 13 -9 38.20 4.00 1 -13 9 45.10 6.20 1 -13 9 47.30 4.90 -2 13 -9 27.60 4.00 -2 13 -9 40.60 5.50 2 -13 9 41.00 6.30 2 -13 9 35.30 4.60 -3 13 -9 36.00 4.50 -3 13 -9 29.20 5.10 3 -13 9 28.90 4.60 3 -13 9 28.30 5.90 -4 13 -9 -0.10 3.10 -4 13 -9 -4.00 3.40 4 -13 9 5.60 5.10 4 -13 9 5.80 3.90 -5 13 -9 30.90 4.70 -5 13 -9 32.80 5.10 5 -13 9 21.40 6.00 5 -13 9 34.30 5.30 -6 13 -9 18.00 4.50 -6 13 -9 12.80 4.10 6 -13 9 17.00 4.90 6 -13 9 3.70 5.70 -7 13 -9 -1.10 3.40 -7 13 -9 3.60 3.70 7 -13 9 1.50 4.90 7 -13 9 -13.60 5.40 -8 13 -9 5.00 3.70 -8 13 -9 -3.40 3.80 8 -13 9 -7.50 5.80 8 -13 9 -1.90 5.10 -9 13 -9 284.37 12.30 -9 13 -9 256.07 10.80 9 -13 9 274.87 12.50 9 -13 9 280.17 14.50 -10 13 -9 -1.60 4.50 10 -13 9 -5.90 6.80 10 -13 9 -4.10 5.60 -11 13 -9 6.10 5.10 11 -13 9 6.40 6.30 11 -13 9 -5.90 7.20 6 12 -9 12.60 5.90 6 12 -9 10.30 5.20 -6 -12 9 17.20 7.80 -6 -12 9 12.50 6.50 5 12 -9 118.59 8.70 5 12 -9 97.99 8.50 -5 -12 9 111.39 9.60 -5 -12 9 115.99 11.10 4 12 -9 0.00 4.20 4 12 -9 4.10 4.50 -4 -12 9 -0.80 5.60 -4 -12 9 2.10 4.90 3 12 -9 47.40 6.10 3 12 -9 48.90 5.90 -3 -12 9 49.00 7.70 -3 -12 9 54.69 6.60 2 12 -9 -3.70 3.50 2 12 -9 4.40 4.10 -2 -12 9 11.20 5.30 -2 -12 9 13.10 4.40 1 12 -9 53.59 5.30 1 12 -9 53.29 5.90 -1 -12 9 55.49 4.80 -1 -12 9 52.99 5.90 -1 -12 9 47.60 6.40 0 12 -9 245.28 9.00 0 12 -9 254.77 10.40 0 -12 9 266.87 11.30 0 -12 9 260.97 8.90 -1 12 -9 188.78 7.10 -1 12 -9 180.78 9.00 -1 12 -9 177.88 7.20 1 -12 9 167.88 9.30 1 -12 9 194.78 7.80 -2 12 -9 5.50 3.60 -2 12 -9 5.60 2.70 2 -12 9 8.50 4.60 2 -12 9 4.30 3.60 -3 12 -9 306.17 9.90 -3 12 -9 309.77 11.20 3 -12 9 300.37 11.90 3 -12 9 303.37 10.00 -4 12 -9 6.80 3.50 -4 12 -9 6.50 3.20 4 -12 9 10.60 4.00 4 -12 9 2.20 4.70 -5 12 -9 38.40 5.00 -5 12 -9 45.20 5.00 5 -12 9 35.10 5.00 5 -12 9 42.00 6.50 -6 12 -9 80.19 6.60 -6 12 -9 73.39 6.20 6 -12 9 73.19 6.40 6 -12 9 63.39 7.50 -7 12 -9 52.19 5.50 -7 12 -9 51.79 5.50 7 -12 9 56.29 6.40 7 -12 9 39.70 7.10 -8 12 -9 5.00 3.90 -8 12 -9 7.30 3.50 8 -12 9 16.00 6.20 8 -12 9 -2.90 4.60 -9 12 -9 55.29 5.60 -9 12 -9 54.79 6.40 9 -12 9 44.80 6.60 9 -12 9 47.30 8.20 -10 12 -9 80.89 7.60 10 -12 9 94.59 10.30 10 -12 9 101.19 8.90 -11 12 -9 22.70 5.80 11 -12 9 8.70 7.50 11 -12 9 18.00 6.60 -12 12 -9 0.90 5.50 12 -12 9 -12.40 7.10 7 11 -9 46.60 8.30 6 11 -9 45.50 6.20 6 11 -9 54.69 7.50 -6 -11 9 41.30 7.60 -6 -11 9 58.39 9.00 5 11 -9 87.49 8.10 5 11 -9 82.69 7.30 -5 -11 9 76.89 8.90 -5 -11 9 75.59 8.20 4 11 -9 -2.50 4.10 4 11 -9 -2.00 3.70 -4 -11 9 1.30 5.40 -4 -11 9 2.60 4.50 3 11 -9 270.77 10.90 3 11 -9 270.97 10.80 -3 -11 9 281.27 12.70 -3 -11 9 255.77 10.80 2 11 -9 36.30 4.70 2 11 -9 35.50 5.00 -2 -11 9 53.69 4.80 -2 -11 9 34.70 6.20 -2 -11 9 40.40 5.10 1 11 -9 265.27 10.30 1 11 -9 261.67 9.40 -1 -11 9 233.38 10.60 -1 -11 9 265.67 9.20 -1 -11 9 256.37 8.80 0 11 -9 74.29 5.40 0 11 -9 62.29 4.30 0 11 -9 67.69 6.00 0 -11 9 67.89 5.20 0 -11 9 77.29 5.30 0 -11 9 79.89 7.00 -1 11 -9 72.59 4.70 -1 11 -9 77.49 6.00 -1 11 -9 83.49 5.00 1 -11 9 74.39 4.70 1 -11 9 77.49 5.70 1 -11 9 72.29 6.30 -2 11 -9 295.77 8.30 -2 11 -9 298.07 10.60 -2 11 -9 303.67 9.20 2 -11 9 282.57 10.90 2 -11 9 293.07 9.30 -3 11 -9 74.29 5.80 -3 11 -9 83.99 5.50 3 -11 9 76.99 5.60 3 -11 9 70.29 6.60 -4 11 -9 160.38 7.70 -4 11 -9 144.29 7.00 4 -11 9 144.69 8.90 4 -11 9 167.58 7.90 -5 11 -9 124.19 7.10 -5 11 -9 121.79 6.90 5 -11 9 134.69 8.80 5 -11 9 129.09 7.30 -6 11 -9 41.60 4.70 -6 11 -9 41.70 4.80 6 -11 9 43.00 5.30 6 -11 9 26.60 5.70 -7 11 -9 89.19 6.90 -7 11 -9 91.19 6.40 7 -11 9 78.19 7.70 7 -11 9 82.79 6.90 -8 11 -9 20.70 3.90 -8 11 -9 10.50 4.00 8 -11 9 21.20 5.00 8 -11 9 11.70 5.70 -9 11 -9 7.50 3.50 -9 11 -9 14.40 4.40 9 -11 9 5.10 5.70 9 -11 9 6.60 4.90 -10 11 -9 106.39 8.10 10 -11 9 116.69 9.10 10 -11 9 122.69 10.80 -11 11 -9 0.00 4.40 11 -11 9 -2.50 6.70 11 -11 9 4.30 5.50 -12 11 -9 10.40 5.30 12 -11 9 0.80 7.00 12 -11 9 18.40 6.70 8 10 -9 8.70 5.70 7 10 -9 120.19 9.70 -7 -10 9 107.29 11.00 6 10 -9 17.40 5.50 6 10 -9 17.80 4.80 -6 -10 9 19.00 6.80 -6 -10 9 15.50 6.20 5 10 -9 75.69 7.10 5 10 -9 88.09 7.10 -5 -10 9 80.39 8.70 -5 -10 9 82.29 8.10 4 10 -9 7.10 4.20 4 10 -9 12.80 4.20 -4 -10 9 15.10 4.90 -4 -10 9 8.90 5.30 3 10 -9 48.00 5.50 3 10 -9 55.09 5.70 -3 -10 9 48.00 5.60 -3 -10 9 52.29 4.80 -3 -10 9 57.29 6.90 2 10 -9 20.90 4.00 2 10 -9 14.20 3.70 -2 -10 9 21.10 5.00 -2 -10 9 18.40 3.40 -2 -10 9 23.80 4.10 1 10 -9 41.10 4.70 1 10 -9 45.20 3.20 1 10 -9 49.99 4.70 -1 -10 9 43.10 4.40 -1 -10 9 40.20 5.30 -1 -10 9 41.60 4.20 0 10 -9 46.50 4.80 0 10 -9 52.69 3.80 0 10 -9 55.29 4.50 0 -10 9 49.30 4.00 0 -10 9 52.69 5.60 0 -10 9 55.39 4.50 -1 10 -9 502.35 12.00 -1 10 -9 507.15 13.60 -1 10 -9 502.75 12.10 1 -10 9 495.95 14.10 1 -10 9 488.05 12.30 1 -10 9 488.65 11.50 -2 10 -9 9.70 2.30 -2 10 -9 8.70 3.10 -2 10 -9 10.30 2.60 2 -10 9 8.90 4.10 2 -10 9 10.80 2.10 2 -10 9 7.40 3.10 -3 10 -9 468.75 12.70 -3 10 -9 423.76 11.40 -3 10 -9 425.76 9.70 3 -10 9 423.46 11.60 3 -10 9 412.36 12.90 3 -10 9 421.86 10.40 -4 10 -9 21.20 3.60 -4 10 -9 22.70 3.40 4 -10 9 12.60 4.30 4 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7.00 -3 -9 9 116.79 6.40 -3 -9 9 134.99 8.50 -3 -9 9 130.99 7.40 2 9 -9 2.90 2.80 2 9 -9 -0.90 2.70 -2 -9 9 0.40 3.50 -2 -9 9 -1.20 2.80 -2 -9 9 -0.60 2.70 1 9 -9 427.26 12.00 1 9 -9 413.26 11.40 1 9 -9 377.66 9.30 -1 -9 9 414.86 10.90 -1 -9 9 407.36 12.60 -1 -9 9 412.66 10.80 0 9 -9 46.20 4.50 0 9 -9 44.70 3.90 0 9 -9 50.29 3.60 0 -9 9 54.59 4.40 0 -9 9 51.99 3.80 0 -9 9 48.50 5.00 -1 9 -9 10.10 2.40 -1 9 -9 13.40 3.00 -1 9 -9 9.00 2.20 1 -9 9 8.80 3.70 1 -9 9 8.20 2.10 1 -9 9 11.40 3.10 -2 9 -9 61.99 4.30 -2 9 -9 65.09 3.70 -2 9 -9 74.09 5.20 2 -9 9 62.89 4.60 2 -9 9 71.59 5.90 2 -9 9 65.29 3.20 -3 9 -9 4.60 2.40 -3 9 -9 4.50 1.70 -3 9 -9 4.70 2.30 3 -9 9 3.10 3.70 3 -9 9 8.50 3.10 3 -9 9 7.30 1.70 -4 9 -9 4.40 2.40 -4 9 -9 5.50 1.50 -4 9 -9 7.30 2.80 4 -9 9 7.10 3.10 4 -9 9 8.40 1.70 4 -9 9 4.00 3.80 -5 9 -9 4.50 2.60 -5 9 -9 2.30 2.60 5 -9 9 3.90 2.70 5 -9 9 5.40 4.00 5 -9 9 2.10 3.00 -6 9 -9 168.58 7.50 -6 9 -9 167.28 7.40 6 -9 9 164.88 9.10 6 -9 9 168.38 7.70 -7 9 -9 87.59 5.90 -7 9 -9 97.69 6.50 7 -9 9 100.59 7.90 7 -9 9 95.59 6.80 -8 9 -9 212.18 9.00 -8 9 -9 217.18 8.30 8 -9 9 201.38 10.30 8 -9 9 204.58 9.30 -9 9 -9 -2.50 3.20 -9 9 -9 0.60 2.80 9 -9 9 -1.40 3.80 9 -9 9 -5.10 4.60 -10 9 -9 8.50 4.00 10 -9 9 0.40 5.60 -11 9 -9 0.50 4.20 11 -9 9 -1.90 5.90 -12 9 -9 6.10 4.40 12 -9 9 12.80 7.00 -13 9 -9 4.80 4.60 13 -9 9 -0.90 8.20 9 8 -9 56.59 8.40 9 8 -9 61.19 9.10 -9 -8 9 41.20 9.30 8 8 -9 9.50 5.40 8 8 -9 4.10 4.90 -8 -8 9 -5.10 6.10 7 8 -9 133.89 9.40 -7 -8 9 119.79 10.70 6 8 -9 0.90 4.10 6 8 -9 1.00 3.10 -6 -8 9 3.70 3.30 -6 -8 9 -0.90 5.10 -6 -8 9 0.20 4.80 5 8 -9 43.20 4.70 5 8 -9 26.30 4.80 -5 -8 9 32.30 5.60 -5 -8 9 31.30 6.00 -5 -8 9 32.40 4.30 4 8 -9 173.58 7.60 4 8 -9 181.58 8.30 -4 -8 9 172.98 7.50 -4 -8 9 183.18 8.90 -4 -8 9 154.68 9.00 3 8 -9 185.28 7.60 3 8 -9 185.18 7.80 -3 -8 9 199.38 7.50 -3 -8 9 176.38 9.20 -3 -8 9 189.68 8.20 2 8 -9 5.60 2.70 2 8 -9 3.90 2.50 2 8 -9 3.50 1.30 -2 -8 9 3.80 3.50 -2 -8 9 6.10 2.70 -2 -8 9 0.80 2.50 1 8 -9 71.89 3.40 1 8 -9 75.69 5.10 1 8 -9 81.79 5.00 -1 -8 9 66.99 4.60 -1 -8 9 76.39 4.60 -1 -8 9 66.09 5.60 0 8 -9 5.10 1.70 0 8 -9 5.70 2.50 0 8 -9 9.10 2.40 0 -8 9 5.80 2.10 0 -8 9 2.00 3.20 0 -8 9 8.70 2.70 -1 8 -9 147.49 5.40 -1 8 -9 158.38 6.60 -1 8 -9 154.38 5.60 1 -8 9 160.58 4.80 1 -8 9 148.89 7.20 1 -8 9 152.98 6.20 -2 8 -9 629.34 13.30 -2 8 -9 638.94 15.00 -2 8 -9 617.04 14.00 2 -8 9 603.44 12.20 2 -8 9 624.64 14.40 2 -8 9 644.34 15.50 -3 8 -9 221.08 5.80 -3 8 -9 237.68 8.00 -3 8 -9 229.58 7.30 3 -8 9 212.38 5.10 3 -8 9 221.28 8.90 3 -8 9 223.38 7.60 -4 8 -9 199.88 7.30 -4 8 -9 201.48 5.20 -4 8 -9 208.68 7.60 4 -8 9 209.58 5.10 4 -8 9 220.98 8.80 4 -8 9 215.28 7.60 -5 8 -9 7.40 2.50 -5 8 -9 4.60 2.40 5 -8 9 1.90 2.80 5 -8 9 8.30 2.10 5 -8 9 3.70 3.80 -6 8 -9 2.10 2.50 -6 8 -9 4.70 2.50 6 -8 9 3.20 3.70 6 -8 9 2.10 2.90 6 -8 9 0.30 2.10 -7 8 -9 60.59 5.20 -7 8 -9 60.39 4.80 7 -8 9 57.19 5.10 7 -8 9 58.89 4.30 7 -8 9 65.99 6.50 -8 8 -9 20.50 3.50 -8 8 -9 26.40 4.10 8 -8 9 22.20 5.30 8 -8 9 25.50 4.60 -9 8 -9 29.70 4.40 -9 8 -9 35.60 4.10 9 -8 9 31.60 6.00 -10 8 -9 30.10 4.80 10 -8 9 26.50 6.00 -11 8 -9 3.70 4.10 11 -8 9 1.00 5.90 -12 8 -9 17.00 4.90 12 -8 9 9.30 6.80 -13 8 -9 17.70 5.10 13 -8 9 9.90 7.20 9 7 -9 52.39 7.50 9 7 -9 45.30 7.60 -9 -7 9 60.59 9.50 8 7 -9 69.39 7.80 8 7 -9 71.79 8.00 -8 -7 9 79.19 9.60 7 7 -9 37.50 6.00 7 7 -9 40.00 6.10 7 7 -9 45.80 5.60 -7 -7 9 40.30 5.10 -7 -7 9 40.80 7.40 6 7 -9 86.59 7.40 6 7 -9 77.69 5.60 -6 -7 9 74.39 8.20 -6 -7 9 73.29 5.80 5 7 -9 32.30 4.90 5 7 -9 28.70 3.80 -5 -7 9 27.70 5.50 -5 -7 9 31.20 5.20 -5 -7 9 22.50 3.90 4 7 -9 138.99 6.50 4 7 -9 126.09 6.90 -4 -7 9 145.89 7.80 -4 -7 9 129.89 6.20 -4 -7 9 131.59 7.90 3 7 -9 174.58 7.00 3 7 -9 164.48 7.10 -3 -7 9 155.98 8.10 -3 -7 9 185.08 7.00 -3 -7 9 171.18 7.40 2 7 -9 81.29 3.10 2 7 -9 89.89 5.10 2 7 -9 93.29 5.10 -2 -7 9 74.69 4.80 -2 -7 9 87.99 5.10 -2 -7 9 76.49 5.90 1 7 -9 48.90 4.00 1 7 -9 52.69 4.10 1 7 -9 51.09 2.80 -1 -7 9 49.00 4.90 -1 -7 9 52.39 4.10 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2.40 2.20 -2 -6 9 -3.10 2.50 -2 -6 9 1.70 2.10 -2 -6 9 2.00 2.40 1 6 -9 66.69 2.90 1 6 -9 65.69 4.10 1 6 -9 63.69 4.10 -1 -6 9 62.19 4.70 -1 -6 9 65.49 3.60 -1 -6 9 54.19 4.00 0 6 -9 136.09 4.40 0 6 -9 133.99 5.00 0 6 -9 132.99 5.40 0 -6 9 130.49 5.40 0 -6 9 133.89 4.20 0 -6 9 131.29 5.80 -1 6 -9 108.49 4.30 -1 6 -9 112.69 4.90 -1 6 -9 109.89 3.10 -1 6 -9 123.79 4.40 1 -6 9 123.09 5.00 1 -6 9 110.89 3.10 1 -6 9 110.29 5.40 -2 6 -9 42.60 2.70 -2 6 -9 39.80 3.30 -2 6 -9 40.40 3.00 2 -6 9 41.50 4.00 2 -6 9 41.40 3.40 -3 6 -9 49.20 3.80 -3 6 -9 43.60 3.30 -3 6 -9 50.69 2.70 3 -6 9 52.09 4.40 3 -6 9 60.19 4.20 -4 6 -9 25.70 3.00 -4 6 -9 34.10 3.20 -4 6 -9 34.00 2.40 4 -6 9 32.70 2.30 4 -6 9 28.70 2.10 4 -6 9 30.30 3.30 4 -6 9 33.00 3.90 -5 6 -9 3.80 1.40 -5 6 -9 4.00 2.00 -5 6 -9 5.60 2.20 5 -6 9 5.40 1.70 5 -6 9 9.00 3.10 5 -6 9 8.00 2.60 -6 6 -9 96.39 3.60 -6 6 -9 104.89 5.30 -6 6 -9 98.89 5.30 6 -6 9 93.89 5.80 6 -6 9 94.89 4.40 6 -6 9 108.69 6.70 -7 6 -9 2.90 2.40 -7 6 -9 5.80 2.60 -7 6 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6.20 2.40 -6 5 -9 -0.20 2.00 -6 5 -9 4.00 1.60 6 -5 9 3.20 2.00 6 -5 9 2.50 3.00 6 -5 9 2.70 2.80 -7 5 -9 62.09 3.60 -7 5 -9 73.59 4.90 -7 5 -9 69.99 4.80 7 -5 9 64.19 4.50 7 -5 9 65.99 5.80 -8 5 -9 5.10 2.50 -8 5 -9 0.50 3.00 -8 5 -9 9.10 3.00 8 -5 9 7.40 3.20 8 -5 9 -0.30 3.70 8 -5 9 3.80 2.00 -9 5 -9 3.50 2.90 -9 5 -9 -2.30 2.50 -9 5 -9 0.40 3.40 9 -5 9 -1.20 3.90 9 -5 9 -2.10 3.20 -10 5 -9 22.50 4.10 -10 5 -9 21.60 4.60 -10 5 -9 23.50 4.80 10 -5 9 19.90 4.80 10 -5 9 19.50 5.60 -11 5 -9 49.80 5.40 -11 5 -9 43.50 5.80 11 -5 9 47.70 6.70 11 -5 9 45.90 7.50 -12 5 -9 2.90 4.70 -12 5 -9 9.50 4.30 12 -5 9 11.80 6.20 13 -5 9 12.30 7.20 11 4 -9 26.60 6.50 11 4 -9 24.20 7.10 -11 -4 9 33.70 8.80 10 4 -9 25.30 5.80 10 4 -9 25.90 6.60 -10 -4 9 22.10 7.40 -10 -4 9 14.20 4.90 9 4 -9 33.90 6.40 9 4 -9 49.30 6.50 -9 -4 9 44.50 5.80 -9 -4 9 34.10 7.50 8 4 -9 291.07 12.30 8 4 -9 299.37 11.60 -8 -4 9 281.77 10.70 -8 -4 9 293.77 13.30 7 4 -9 101.79 7.10 7 4 -9 100.19 7.40 -7 -4 9 113.89 8.60 -7 -4 9 97.69 6.70 6 4 -9 175.18 7.80 6 4 -9 174.98 8.30 6 4 -9 173.28 6.10 -6 -4 9 188.08 9.50 -6 -4 9 161.78 7.40 5 4 -9 268.47 9.30 5 4 -9 274.77 7.70 5 4 -9 272.87 9.20 -5 -4 9 287.07 10.30 -5 -4 9 264.47 8.90 4 4 -9 -1.80 2.10 4 4 -9 0.90 1.60 4 4 -9 0.00 2.10 -4 -4 9 1.70 2.40 -4 -4 9 -0.10 2.70 3 4 -9 -0.70 1.40 3 4 -9 -0.20 1.70 3 4 -9 0.60 1.90 -3 -4 9 1.60 2.10 -3 -4 9 1.30 1.00 -3 -4 9 1.30 2.30 2 4 -9 569.04 12.30 2 4 -9 561.64 12.30 2 4 -9 539.15 12.80 -2 -4 9 559.24 13.10 -2 -4 9 559.54 11.10 -2 -4 9 525.15 12.50 1 4 -9 516.35 10.80 1 4 -9 520.45 11.80 1 4 -9 516.45 11.60 -1 -4 9 518.25 11.70 -1 -4 9 524.45 12.00 0 4 -9 964.30 17.90 0 4 -9 986.10 17.60 0 4 -9 997.10 19.50 0 4 -9 977.20 18.80 0 4 -9 988.60 19.70 0 -4 9 1004.00 19.60 0 -4 9 970.30 19.50 -1 4 -9 576.24 12.10 -1 4 -9 554.44 12.00 -1 4 -9 556.14 12.70 1 -4 9 586.04 12.40 1 -4 9 596.04 12.60 -2 4 -9 -0.50 1.50 -2 4 -9 1.20 1.30 -2 4 -9 -0.70 1.30 2 -4 9 3.70 1.90 2 -4 9 1.70 2.00 -3 4 -9 62.19 3.70 -3 4 -9 71.59 3.10 -3 4 -9 67.29 3.60 3 -4 9 71.49 4.00 3 -4 9 70.09 4.00 -4 4 -9 -0.40 1.70 -4 4 -9 1.50 1.40 -4 4 -9 1.60 1.60 4 -4 9 4.30 2.30 4 -4 9 1.70 2.00 4 -4 9 3.60 1.30 -5 4 -9 364.46 8.40 -5 4 -9 369.36 9.70 -5 4 -9 349.87 9.50 5 -4 9 363.96 10.10 5 -4 9 358.66 8.70 5 -4 9 366.06 9.80 -6 4 -9 2.30 1.70 -6 4 -9 1.80 2.10 -6 4 -9 3.80 2.20 6 -4 9 0.30 2.60 6 -4 9 1.90 2.10 6 -4 9 4.00 2.90 -7 4 -9 -0.50 2.10 -7 4 -9 -0.40 2.20 -7 4 -9 -2.20 1.70 -7 4 -9 -3.20 2.30 7 -4 9 0.90 2.50 7 -4 9 -0.30 3.10 -8 4 -9 95.49 5.70 -8 4 -9 97.49 5.90 -8 4 -9 94.99 5.50 8 -4 9 106.89 7.30 8 -4 9 110.49 6.30 -9 4 -9 372.46 10.70 -9 4 -9 357.96 11.20 -9 4 -9 344.27 10.90 9 -4 9 352.66 10.20 9 -4 9 377.96 12.40 9 -4 9 378.76 13.20 -10 4 -9 -2.30 3.50 -10 4 -9 -0.90 2.70 -10 4 -9 4.90 3.30 10 -4 9 7.00 4.40 10 -4 9 7.40 5.00 -11 4 -9 186.88 8.80 -11 4 -9 200.48 9.60 11 -4 9 203.68 11.80 11 -4 9 206.68 11.20 -12 4 -9 18.30 5.20 12 -4 9 19.00 6.20 12 -4 9 8.20 6.20 13 -4 9 -4.30 5.90 11 3 -9 2.70 5.20 11 3 -9 0.50 5.40 -11 -3 9 0.30 4.80 -11 -3 9 12.50 6.80 10 3 -9 173.98 10.70 10 3 -9 161.78 11.10 -10 -3 9 187.28 9.70 -10 -3 9 182.48 13.00 9 3 -9 46.90 6.70 9 3 -9 56.09 6.50 -9 -3 9 43.90 5.60 -9 -3 9 47.60 7.60 8 3 -9 51.29 5.60 8 3 -9 52.79 6.50 -8 -3 9 50.69 7.10 -8 -3 9 61.39 6.00 7 3 -9 8.00 3.80 7 3 -9 2.60 3.30 -7 -3 9 3.30 3.10 -7 -3 9 1.60 4.20 6 3 -9 19.60 2.30 6 3 -9 19.00 3.80 6 3 -9 20.60 3.60 -6 -3 9 16.60 3.50 -6 -3 9 21.70 4.50 5 3 -9 16.70 2.30 5 3 -9 11.80 2.90 5 3 -9 10.40 3.10 -5 -3 9 15.10 3.00 -5 -3 9 9.80 3.40 4 3 -9 433.46 11.40 4 3 -9 432.26 11.30 4 3 -9 415.86 9.80 -4 -3 9 440.16 11.30 -4 -3 9 429.26 11.80 -4 -3 9 424.26 8.40 3 3 -9 207.58 6.80 3 3 -9 204.08 6.60 3 3 -9 211.08 5.90 -3 -3 9 202.18 4.90 -3 -3 9 199.08 6.70 -3 -3 9 200.88 7.20 2 3 -9 759.42 16.10 2 3 -9 741.63 15.30 2 3 -9 759.92 15.50 -2 -3 9 736.43 15.80 -2 -3 9 753.02 14.50 -2 -3 9 764.32 16.10 1 3 -9 258.97 7.10 1 3 -9 257.17 6.90 1 3 -9 262.87 6.30 -1 -3 9 258.07 6.40 -1 -3 9 267.67 7.20 -1 -3 9 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10 6.10 6.60 7 7 -10 124.49 9.00 7 7 -10 123.39 8.80 -7 -7 10 113.49 7.80 -7 -7 10 135.99 10.80 6 7 -10 110.19 6.50 6 7 -10 107.39 7.70 6 7 -10 106.09 7.70 -6 -7 10 93.39 6.70 -6 -7 10 94.99 8.80 5 7 -10 17.70 4.30 5 7 -10 16.70 3.40 -5 -7 10 10.10 4.50 -5 -7 10 16.20 3.80 4 7 -10 18.10 3.80 4 7 -10 20.70 3.30 -4 -7 10 22.30 4.90 -4 -7 10 24.60 4.00 -4 -7 10 21.00 4.30 3 7 -10 4.20 2.80 3 7 -10 4.90 2.50 -3 -7 10 5.30 3.60 -3 -7 10 1.90 2.90 -3 -7 10 2.10 2.70 2 7 -10 232.78 7.80 2 7 -10 212.18 7.70 -2 -7 10 229.38 7.70 -2 -7 10 222.18 7.80 -2 -7 10 204.18 8.50 1 7 -10 8.70 2.60 1 7 -10 14.40 2.70 1 7 -10 17.70 2.00 -1 -7 10 15.80 2.60 -1 -7 10 5.50 3.30 -1 -7 10 14.30 3.10 0 7 -10 155.18 6.20 0 7 -10 132.19 4.80 0 7 -10 140.99 5.50 0 -7 10 145.29 6.00 0 -7 10 141.19 4.70 0 -7 10 146.79 6.70 -1 7 -10 235.18 7.00 -1 7 -10 237.68 6.90 -1 7 -10 242.68 7.90 1 -7 10 232.68 8.30 1 -7 10 241.78 7.90 1 -7 10 242.78 5.60 -2 7 -10 37.20 3.60 -2 7 -10 41.30 3.30 -2 7 -10 36.10 2.90 2 -7 10 41.00 3.80 2 -7 10 43.00 4.40 -3 7 -10 2.20 1.90 -3 7 -10 0.70 2.10 -3 7 -10 1.50 1.60 3 -7 10 1.50 3.00 3 -7 10 0.70 2.60 -4 7 -10 84.29 3.50 -4 7 -10 77.79 4.70 -4 7 -10 83.49 5.10 4 -7 10 81.19 6.30 4 -7 10 83.49 5.40 -5 7 -10 77.29 3.20 -5 7 -10 80.19 5.10 -5 7 -10 68.49 4.60 5 -7 10 72.09 5.90 5 -7 10 79.19 5.50 5 -7 10 68.39 3.20 -6 7 -10 261.37 8.70 -6 7 -10 270.27 8.80 -6 7 -10 250.17 6.20 6 -7 10 268.67 10.00 6 -7 10 259.67 9.00 6 -7 10 242.78 6.80 -7 7 -10 31.70 4.00 -7 7 -10 31.50 3.90 7 -7 10 32.20 3.50 7 -7 10 32.00 4.40 7 -7 10 41.30 5.30 -8 7 -10 6.20 2.90 -8 7 -10 10.30 3.20 8 -7 10 5.60 4.30 8 -7 10 6.10 3.80 -9 7 -10 20.90 3.70 -9 7 -10 18.20 3.90 9 -7 10 20.60 5.20 9 -7 10 15.30 4.40 -10 7 -10 145.39 11.10 -10 7 -10 131.79 8.10 10 -7 10 137.59 10.20 -11 7 -10 0.40 3.70 11 -7 10 13.00 6.20 -12 7 -10 15.00 4.70 12 -7 10 5.00 6.60 12 -7 10 8.80 5.40 -13 7 -10 -6.90 6.30 13 -7 10 9.40 5.80 13 -7 10 -4.50 6.50 10 6 -10 25.20 7.20 10 6 -10 25.30 6.80 -10 -6 10 29.80 9.00 9 6 -10 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76.79 6.00 4 8 -14 75.59 6.10 4 8 -14 84.69 7.20 -4 -8 14 75.19 6.50 -4 -8 14 96.89 8.50 3 8 -14 89.09 6.90 3 8 -14 102.59 6.80 -3 -8 14 89.39 7.80 -3 -8 14 96.99 6.90 2 8 -14 299.07 10.60 2 8 -14 280.67 10.10 -2 -8 14 308.67 10.50 -2 -8 14 292.47 11.10 1 8 -14 195.08 8.10 1 8 -14 198.38 8.30 -1 -8 14 176.08 6.40 -1 -8 14 178.08 8.70 -1 -8 14 172.68 8.00 0 8 -14 6.90 2.90 0 8 -14 11.80 2.50 0 8 -14 5.80 3.00 0 -8 14 12.20 3.70 0 -8 14 13.40 4.00 -1 8 -14 112.29 6.60 -1 8 -14 109.89 5.30 -1 8 -14 119.19 5.90 1 -8 14 110.99 6.80 1 -8 14 112.19 6.70 -2 8 -14 222.18 7.60 -2 8 -14 220.28 8.70 -2 8 -14 219.48 7.50 2 -8 14 219.08 8.90 2 -8 14 228.48 8.80 -3 8 -14 99.19 5.10 -3 8 -14 99.29 5.60 -3 8 -14 100.09 6.30 3 -8 14 106.79 6.80 3 -8 14 122.59 7.20 -4 8 -14 368.86 10.90 -4 8 -14 368.16 11.50 -4 8 -14 379.16 9.50 4 -8 14 368.26 11.90 4 -8 14 374.06 11.50 -5 8 -14 126.69 6.70 -5 8 -14 120.69 7.10 5 -8 14 116.49 7.90 5 -8 14 117.39 7.40 -6 8 -14 73.59 5.60 -6 8 -14 74.69 6.00 6 -8 14 70.79 6.70 6 -8 14 64.39 6.00 -7 8 -14 232.08 9.60 -7 8 -14 230.88 9.50 7 -8 14 233.78 10.60 7 -8 14 226.08 10.00 -8 8 -14 67.39 6.20 -8 8 -14 60.29 5.90 8 -8 14 64.09 6.80 8 -8 14 57.59 7.00 -9 8 -14 11.10 4.40 -9 8 -14 8.50 4.00 9 -8 14 13.40 5.30 9 -8 14 6.60 5.60 -10 8 -14 86.19 7.40 -10 8 -14 88.59 7.00 10 -8 14 80.19 7.90 10 -8 14 80.99 8.80 -11 8 -14 1.00 4.50 11 -8 14 -10.70 5.80 11 -8 14 -0.80 5.60 -12 8 -14 5.90 4.90 12 -8 14 -15.60 6.20 12 -8 14 14.40 7.30 9 7 -14 58.99 8.10 8 7 -14 10.80 5.60 8 7 -14 2.30 5.50 -8 -7 14 7.70 6.70 -8 -7 14 5.00 4.60 7 7 -14 44.20 6.40 7 7 -14 51.69 7.00 -7 -7 14 35.70 7.70 -7 -7 14 46.40 6.30 6 7 -14 68.99 7.10 6 7 -14 74.59 7.00 -6 -7 14 65.59 6.60 -6 -7 14 70.89 8.60 5 7 -14 53.89 6.10 5 7 -14 62.39 5.90 5 7 -14 53.19 5.10 -5 -7 14 65.29 7.40 -5 -7 14 55.99 6.10 4 7 -14 4.00 3.70 4 7 -14 7.80 3.20 4 7 -14 2.90 2.90 -4 -7 14 4.40 4.40 -4 -7 14 4.10 3.90 3 7 -14 256.27 8.50 3 7 -14 258.87 9.80 3 7 -14 279.17 9.50 -3 -7 14 244.98 10.70 -3 -7 14 270.47 10.00 2 7 -14 1.60 2.00 2 7 -14 2.10 2.60 2 7 -14 5.30 3.10 -2 -7 14 1.30 3.30 -2 -7 14 0.60 1.90 -2 -7 14 -0.30 3.50 1 7 -14 199.78 8.00 1 7 -14 190.08 7.70 -1 -7 14 198.18 6.70 -1 -7 14 205.78 8.60 -1 -7 14 195.68 8.20 0 7 -14 173.78 7.00 0 7 -14 177.88 6.20 0 7 -14 170.48 7.40 0 -7 14 176.78 7.60 0 -7 14 173.38 7.80 -1 7 -14 66.19 4.80 -1 7 -14 68.89 4.40 -1 7 -14 67.59 5.30 1 -7 14 71.49 5.50 1 -7 14 72.39 5.50 -2 7 -14 208.58 7.10 -2 7 -14 206.98 8.20 -2 7 -14 212.88 7.30 2 -7 14 223.48 8.50 2 -7 14 226.58 8.30 -3 7 -14 71.09 5.50 -3 7 -14 74.49 4.60 -3 7 -14 73.19 4.80 3 -7 14 79.19 6.00 3 -7 14 79.09 5.70 -4 7 -14 14.50 2.70 -4 7 -14 14.00 3.00 -4 7 -14 20.20 3.60 4 -7 14 16.30 4.10 4 -7 14 17.10 3.80 -5 7 -14 55.59 4.70 -5 7 -14 62.59 5.30 -5 7 -14 53.69 3.90 5 -7 14 49.90 5.00 5 -7 14 60.09 5.80 -6 7 -14 97.79 6.70 -6 7 -14 109.29 6.50 6 -7 14 102.69 7.20 6 -7 14 104.39 7.40 -7 7 -14 86.89 6.40 -7 7 -14 92.79 6.60 7 -7 14 85.19 7.10 7 -7 14 89.69 6.90 -8 7 -14 19.60 4.20 -8 7 -14 18.60 4.20 8 -7 14 17.60 5.20 8 -7 14 18.30 4.80 -9 7 -14 33.70 5.00 -9 7 -14 36.10 5.20 9 -7 14 34.90 5.90 9 -7 14 26.70 6.00 -10 7 -14 19.70 4.90 -10 7 -14 14.10 4.30 10 -7 14 1.10 5.40 10 -7 14 13.00 6.20 -11 7 -14 24.50 5.40 11 -7 14 24.00 6.80 11 -7 14 27.00 6.30 -12 7 -14 17.00 5.50 12 -7 14 3.20 5.80 9 6 -14 -1.60 5.60 9 6 -14 -3.20 4.70 -9 -6 14 -2.90 4.60 -9 -6 14 2.30 6.60 8 6 -14 39.60 6.60 8 6 -14 18.80 5.60 -8 -6 14 20.90 7.20 -8 -6 14 26.70 5.60 7 6 -14 1.10 4.10 7 6 -14 -0.40 4.60 -7 -6 14 -0.50 3.90 -7 -6 14 6.60 5.80 6 6 -14 109.39 7.80 6 6 -14 99.59 7.90 -6 -6 14 113.89 9.60 -6 -6 14 107.59 8.00 5 6 -14 313.67 9.90 5 6 -14 315.37 11.50 5 6 -14 277.77 10.50 -5 -6 14 280.17 11.20 -5 -6 14 311.87 12.50 4 6 -14 5.30 3.50 4 6 -14 3.80 2.70 4 6 -14 4.30 2.70 -4 -6 14 1.80 3.40 -4 -6 14 -1.90 3.70 3 6 -14 4.40 3.20 3 6 -14 8.00 2.80 3 6 -14 3.80 2.40 -3 -6 14 12.00 3.70 -3 -6 14 9.30 3.70 2 6 -14 3.30 2.40 2 6 -14 5.80 2.90 2 6 -14 6.10 2.10 -2 -6 14 7.70 3.20 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502.25 13.50 -2 -5 14 551.14 13.90 1 5 -14 28.00 3.40 1 5 -14 23.40 2.20 1 5 -14 26.40 3.60 -1 -5 14 28.70 3.10 -1 -5 14 25.50 3.80 -1 -5 14 21.40 3.40 0 5 -14 113.39 5.50 0 5 -14 114.39 5.70 0 -5 14 92.49 5.90 0 -5 14 100.59 5.60 0 -5 14 107.79 5.20 -1 5 -14 15.30 3.00 -1 5 -14 13.60 2.40 -1 5 -14 11.30 2.80 1 -5 14 15.60 3.40 1 -5 14 18.80 3.10 -2 5 -14 452.35 11.90 -2 5 -14 418.76 10.80 -2 5 -14 413.86 10.70 2 -5 14 427.76 11.30 2 -5 14 408.76 10.80 -3 5 -14 340.07 10.30 -3 5 -14 353.16 9.40 -3 5 -14 340.17 9.60 3 -5 14 343.27 9.80 3 -5 14 347.77 10.30 -4 5 -14 195.68 7.30 -4 5 -14 199.48 7.90 -4 5 -14 195.98 6.60 4 -5 14 196.88 7.80 4 -5 14 190.98 7.50 -5 5 -14 1.10 2.30 -5 5 -14 -1.70 2.10 -5 5 -14 0.70 2.60 5 -5 14 -4.70 2.80 5 -5 14 0.80 3.10 -6 5 -14 124.79 6.50 -6 5 -14 130.59 5.70 -6 5 -14 144.59 7.20 6 -5 14 134.89 7.40 6 -5 14 133.89 7.20 -7 5 -14 9.40 3.20 -7 5 -14 10.40 3.60 -7 5 -14 14.50 2.90 7 -5 14 14.70 4.20 7 -5 14 13.30 4.10 -8 5 -14 13.80 3.90 -8 5 -14 13.80 3.80 8 -5 14 14.10 4.50 8 -5 14 13.20 4.60 -9 5 -14 5.70 3.70 -9 5 -14 5.40 3.70 9 -5 14 2.60 4.70 9 -5 14 8.80 4.70 -10 5 -14 104.09 7.60 -10 5 -14 116.39 8.20 10 -5 14 90.19 8.40 10 -5 14 112.09 8.50 -11 5 -14 22.00 4.90 11 -5 14 13.20 5.70 12 -5 14 3.00 5.80 10 4 -14 49.99 7.60 10 4 -14 50.49 7.80 -10 -4 14 39.20 8.60 -10 -4 14 62.69 7.70 9 4 -14 3.30 4.80 9 4 -14 1.10 4.90 -9 -4 14 1.20 4.70 -9 -4 14 2.80 6.00 8 4 -14 6.40 4.50 8 4 -14 1.30 4.50 -8 -4 14 -4.90 3.90 -8 -4 14 -1.20 5.10 7 4 -14 215.18 10.20 7 4 -14 215.08 10.20 -7 -4 14 222.68 11.80 -7 -4 14 201.08 9.80 6 4 -14 423.86 13.40 6 4 -14 421.36 13.50 -6 -4 14 431.76 14.70 -6 -4 14 411.16 13.40 5 4 -14 -1.70 1.90 5 4 -14 -0.50 3.10 5 4 -14 1.20 2.70 -5 -4 14 -0.10 3.30 -5 -4 14 6.90 3.90 4 4 -14 114.69 6.50 4 4 -14 111.39 5.90 4 4 -14 104.09 5.30 -4 -4 14 106.59 4.50 -4 -4 14 96.59 6.60 -4 -4 14 95.09 6.80 3 4 -14 5.40 2.20 3 4 -14 4.30 2.30 3 4 -14 2.90 2.70 -3 -4 14 0.60 1.80 -3 -4 14 0.40 2.80 -3 -4 14 2.40 2.90 2 4 -14 2.90 1.80 2 4 -14 1.50 2.00 2 4 -14 2.10 2.50 -2 -4 14 5.20 2.10 -2 -4 14 3.10 2.50 -2 -4 14 0.40 2.70 1 4 -14 302.17 7.20 1 4 -14 297.47 9.20 1 4 -14 304.57 8.90 -1 -4 14 302.67 8.80 -1 -4 14 299.57 9.50 -1 -4 14 296.07 8.30 0 4 -14 71.99 4.70 0 4 -14 79.09 4.60 0 -4 14 80.69 4.70 0 -4 14 80.09 5.00 0 -4 14 78.89 4.50 -1 4 -14 185.58 6.60 -1 4 -14 170.98 6.80 1 -4 14 171.48 6.00 1 -4 14 168.08 6.90 1 -4 14 181.38 6.60 -2 4 -14 1.20 2.30 -2 4 -14 2.00 2.30 -2 4 -14 4.50 2.10 2 -4 14 2.10 3.00 2 -4 14 2.30 2.30 -3 4 -14 14.80 3.00 -3 4 -14 20.40 3.10 -3 4 -14 19.30 2.80 3 -4 14 27.40 3.70 3 -4 14 22.50 3.20 -4 4 -14 15.50 3.10 -4 4 -14 11.00 2.70 -4 4 -14 11.70 2.60 4 -4 14 14.80 3.50 4 -4 14 15.90 3.20 -5 4 -14 52.09 4.30 -5 4 -14 51.19 4.00 -5 4 -14 58.19 4.90 5 -4 14 53.89 4.50 5 -4 14 57.39 5.00 -6 4 -14 441.06 12.20 -6 4 -14 444.76 11.40 -6 4 -14 456.15 12.90 6 -4 14 450.95 12.50 6 -4 14 435.06 12.20 -7 4 -14 14.40 3.50 -7 4 -14 14.50 3.80 -7 4 -14 18.20 3.20 7 -4 14 15.40 4.10 7 -4 14 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7.10 -6 11 -22 12.40 5.60 -6 11 -22 7.20 4.70 6 -11 22 13.50 6.60 -7 11 -22 2.00 6.80 -4 -10 22 99.99 11.30 3 10 -22 109.79 8.90 3 10 -22 95.09 8.90 -3 -10 22 110.29 10.70 -3 -10 22 93.39 9.10 2 10 -22 2.40 4.50 2 10 -22 -1.80 5.10 -2 -10 22 13.20 6.10 -2 -10 22 7.50 6.20 1 10 -22 35.60 6.40 1 10 -22 30.40 5.90 -1 -10 22 47.40 7.50 0 10 -22 134.79 9.40 0 10 -22 126.09 9.20 0 -10 22 147.89 10.50 -1 10 -22 96.39 7.90 -1 10 -22 95.99 8.50 1 -10 22 100.79 9.10 -2 10 -22 -0.10 4.40 2 -10 22 1.40 4.70 2 -10 22 5.40 5.90 -3 10 -22 33.00 6.10 3 -10 22 20.00 5.70 3 -10 22 36.80 7.00 -4 10 -22 -0.80 4.50 4 -10 22 5.60 5.90 4 -10 22 4.30 5.10 -5 10 -22 69.19 7.80 5 -10 22 74.79 8.20 -6 10 -22 18.20 5.80 6 -10 22 16.60 6.50 -7 10 -22 9.30 5.50 7 -10 22 10.60 6.30 4 9 -22 34.20 7.10 -4 -9 22 42.70 7.30 3 9 -22 5.40 5.40 3 9 -22 17.00 5.00 -3 -9 22 15.50 6.20 2 9 -22 77.29 7.90 2 9 -22 70.79 7.10 -2 -9 22 72.89 8.50 1 9 -22 109.29 8.70 1 9 -22 110.89 8.50 -1 -9 22 121.09 9.60 0 9 -22 14.50 5.30 0 9 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2.40 5.30 3 -8 -22 13.60 5.90 3 -8 -22 5.90 5.10 -3 8 22 10.60 5.70 2 -8 -22 101.99 8.60 2 -8 -22 82.89 8.00 -2 8 22 94.59 7.60 -2 8 22 101.89 9.10 1 -8 -22 51.39 6.80 1 -8 -22 71.09 7.50 -1 8 22 61.09 8.00 -1 8 22 55.59 6.60 0 -8 -22 55.19 7.30 0 -8 -22 43.90 6.80 0 8 22 43.30 7.40 0 8 22 44.90 6.60 -1 -8 -22 51.49 7.00 -1 -8 -22 53.29 7.20 1 8 22 47.50 7.00 1 8 22 50.89 7.70 -2 -8 -22 29.90 6.70 -2 -8 -22 44.90 7.00 2 8 22 23.80 6.90 2 8 22 35.50 6.90 -3 -8 -22 7.70 5.80 -3 -8 -22 13.80 5.90 3 8 22 -3.70 6.20 3 8 22 0.10 5.90 -4 -8 -22 7.00 5.90 4 8 22 -1.30 6.80 7 -9 -22 8.70 6.60 -7 9 22 27.10 6.30 6 -9 -22 72.89 8.80 6 -9 -22 83.09 7.90 -6 9 22 71.79 8.30 5 -9 -22 8.70 6.40 5 -9 -22 13.60 5.40 -5 9 22 12.70 5.90 4 -9 -22 1.00 5.80 4 -9 -22 -1.90 4.60 -4 9 22 2.20 5.30 3 -9 -22 1.20 5.80 3 -9 -22 12.40 4.80 -3 9 22 4.00 5.60 2 -9 -22 4.60 5.10 2 -9 -22 16.90 6.00 -2 9 22 9.00 6.00 -2 9 22 4.90 4.50 1 -9 -22 9.00 5.30 1 -9 -22 15.90 5.90 -1 9 22 6.00 4.80 -1 9 22 3.00 5.90 0 -9 -22 22.40 6.20 0 -9 -22 15.10 5.60 0 9 22 15.30 6.70 0 9 22 17.70 5.60 -1 -9 -22 5.90 5.70 -1 -9 -22 0.60 5.20 1 9 22 9.40 5.60 1 9 22 10.30 6.60 -2 -9 -22 28.40 6.40 -2 -9 -22 14.00 7.90 2 9 22 9.90 6.80 2 9 22 16.90 6.30 -3 -9 -22 24.60 7.10 6 -10 -22 -5.90 6.10 -6 10 22 1.10 7.30 5 -10 -22 1.40 6.10 5 -10 -22 -6.30 4.40 -5 10 22 4.40 5.60 4 -10 -22 13.70 5.50 4 -10 -22 10.70 6.20 -4 10 22 4.30 5.70 3 -10 -22 5.70 6.00 3 -10 -22 20.50 5.50 -3 10 22 5.80 5.90 2 -10 -22 24.60 6.00 2 -10 -22 28.50 6.70 -2 10 22 24.40 5.50 -2 10 22 24.20 7.10 1 -10 -22 -4.80 5.00 1 -10 -22 12.30 5.90 -1 10 22 -0.50 6.20 -1 10 22 -5.30 4.60 0 -10 -22 2.00 5.20 0 -10 -22 8.80 5.80 0 10 22 1.80 5.30 0 10 22 -11.50 5.70 -1 -10 -22 16.30 6.20 1 10 22 1.70 8.30 1 10 22 2.10 8.90 4 -11 -22 14.10 7.60 4 -11 -22 -4.20 5.00 3 -11 -22 14.70 6.50 3 -11 -22 7.00 5.10 2 -11 -22 30.50 7.40 2 -11 -22 29.10 6.40 -2 11 22 31.60 7.20 1 -11 -22 25.90 6.40 -1 11 22 29.90 6.30 3 -12 -22 10.90 7.00 4 -13 23 -0.60 6.10 1 -12 23 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45.20 7.10 6 -10 23 47.80 7.50 6 -10 23 54.49 8.00 3 9 -23 233.88 12.20 3 9 -23 225.18 11.50 -3 -9 23 248.58 13.70 2 9 -23 10.70 4.80 2 9 -23 6.20 5.50 -2 -9 23 4.90 6.00 1 9 -23 18.60 5.00 1 9 -23 13.20 5.30 -1 -9 23 23.60 6.50 0 9 -23 -4.10 4.70 0 9 -23 1.10 4.30 0 -9 23 4.80 6.10 -1 9 -23 36.50 6.20 -1 9 -23 40.40 6.30 1 -9 23 54.79 6.30 1 -9 23 45.10 7.40 -2 9 -23 -0.50 4.80 -2 9 -23 8.70 4.80 2 -9 23 13.60 6.40 2 -9 23 21.10 5.50 -3 9 -23 49.50 6.80 3 -9 23 44.30 7.40 3 -9 23 38.40 6.50 -4 9 -23 8.60 5.00 4 -9 23 0.30 6.00 4 -9 23 3.50 5.50 -5 9 -23 3.20 4.90 5 -9 23 0.40 5.60 5 -9 23 -3.10 5.90 -6 9 -23 2.60 5.20 6 -9 23 9.00 6.20 6 -9 23 1.10 5.80 -7 9 -23 8.10 5.50 7 -9 23 0.90 6.20 7 -9 23 12.40 6.40 4 8 -23 0.10 5.10 -4 -8 23 -2.60 6.00 3 8 -23 0.60 5.30 3 8 -23 12.60 4.70 -3 -8 23 10.30 6.00 2 8 -23 17.50 5.90 2 8 -23 10.70 4.60 -2 -8 23 10.10 6.30 1 8 -23 37.30 5.70 1 8 -23 42.00 6.30 -1 -8 23 49.40 7.50 0 8 -23 15.50 5.00 0 8 -23 5.90 4.70 0 -8 23 1.30 4.20 0 -8 23 5.30 5.80 -1 8 -23 30.10 5.30 -1 8 -23 37.40 6.10 1 -8 23 41.40 7.10 1 -8 23 30.70 5.50 -2 8 -23 44.70 6.20 -2 8 -23 38.20 5.90 2 -8 23 41.80 7.00 2 -8 23 40.00 6.20 -3 8 -23 52.29 6.20 -3 8 -23 65.29 7.40 3 -8 23 65.79 7.80 3 -8 23 67.79 7.20 -4 8 -23 92.39 8.30 4 -8 23 84.69 8.30 4 -8 23 92.99 8.30 -5 8 -23 74.99 8.00 5 -8 23 83.19 8.50 5 -8 23 73.69 8.20 -6 8 -23 29.10 6.10 6 -8 23 36.00 7.10 6 -8 23 43.90 7.30 -7 8 -23 15.10 5.90 7 -8 23 27.10 7.00 7 -8 23 26.70 6.90 -8 8 -23 49.50 9.80 8 -8 23 35.30 9.10 5 7 -23 72.09 8.40 -5 -7 23 68.69 8.70 4 7 -23 3.80 5.10 -4 -7 23 1.80 5.80 3 7 -23 -2.30 3.60 3 7 -23 -8.80 4.40 -3 -7 23 8.10 6.20 2 7 -23 38.50 5.50 2 7 -23 33.60 6.30 -2 -7 23 26.40 6.50 1 7 -23 35.50 5.40 1 7 -23 36.90 6.20 -1 -7 23 58.09 7.40 0 7 -23 8.50 4.10 0 7 -23 1.70 4.50 0 -7 23 8.80 5.70 0 -7 23 9.90 4.50 -1 7 -23 122.79 8.50 -1 7 -23 116.49 8.50 1 -7 23 123.39 8.30 1 -7 23 116.19 9.10 -2 7 -23 11.50 5.00 -2 7 -23 18.30 4.90 2 -7 23 21.80 6.40 2 -7 23 13.70 5.10 -3 7 -23 4.10 4.50 -3 7 -23 -0.50 4.20 3 -7 23 3.20 4.90 3 -7 23 7.00 5.80 -4 7 -23 1.90 4.50 -4 7 -23 3.70 4.20 4 -7 23 5.20 5.60 4 -7 23 1.20 5.10 -5 7 -23 -0.90 4.50 5 -7 23 -4.40 5.10 5 -7 23 5.10 5.70 -6 7 -23 -0.20 4.70 6 -7 23 4.10 5.60 6 -7 23 -0.40 5.70 -7 7 -23 -8.90 4.70 7 -7 23 6.00 5.70 7 -7 23 2.00 6.00 -8 7 -23 2.80 5.20 8 -7 23 0.50 5.90 8 -7 23 -12.80 8.90 5 6 -23 42.10 7.00 -5 -6 23 44.00 7.80 4 6 -23 79.39 8.20 -4 -6 23 85.29 9.10 3 6 -23 38.90 6.50 3 6 -23 40.40 5.40 -3 -6 23 51.49 7.60 2 6 -23 89.49 7.90 2 6 -23 73.29 6.50 -2 -6 23 104.69 9.10 1 6 -23 -0.60 3.50 1 6 -23 2.80 4.80 -1 -6 23 -2.30 5.30 -1 -6 23 4.40 4.00 0 6 -23 38.30 5.40 0 6 -23 39.70 6.00 0 -6 23 22.90 5.00 0 -6 23 29.10 6.50 -1 6 -23 7.20 4.10 -1 6 -23 6.30 4.80 1 -6 23 3.10 5.40 1 -6 23 0.30 4.20 -2 6 -23 90.89 7.50 -2 6 -23 104.29 8.10 2 -6 23 115.79 8.20 2 -6 23 79.79 7.90 -3 6 -23 12.90 4.60 -3 6 -23 9.50 4.70 3 -6 23 13.10 5.20 3 -6 23 12.40 5.70 -4 6 -23 2.40 4.20 -4 6 -23 3.70 4.40 4 -6 23 0.40 5.50 4 -6 23 8.70 5.20 -5 6 -23 2.00 4.50 -5 6 -23 -2.30 4.10 5 -6 23 3.10 5.30 5 -6 23 1.80 5.20 -6 6 -23 20.40 5.70 6 -6 23 14.60 5.90 6 -6 23 14.70 6.00 -7 6 -23 -4.10 4.90 7 -6 23 -1.80 5.60 7 -6 23 13.40 6.20 -8 6 -23 5.30 5.40 8 -6 23 0.00 5.90 8 -6 23 0.40 6.10 6 5 -23 9.40 5.90 -6 -5 23 6.00 6.00 5 5 -23 27.40 6.40 -5 -5 23 26.30 6.90 4 5 -23 4.60 5.20 -4 -5 23 8.90 6.00 3 5 -23 116.19 7.80 3 5 -23 161.68 9.80 -3 -5 23 159.18 10.90 2 5 -23 133.89 9.10 2 5 -23 137.89 8.30 -2 -5 23 133.69 8.50 -2 -5 23 146.79 10.40 1 5 -23 116.29 7.80 1 5 -23 136.59 9.30 -1 -5 23 117.29 8.10 -1 -5 23 130.09 9.50 0 5 -23 -1.80 4.30 0 5 -23 3.40 3.50 0 -5 23 1.60 5.30 0 -5 23 -0.10 4.00 -1 5 -23 7.00 4.10 -1 5 -23 4.00 4.40 1 -5 23 12.10 5.50 1 -5 23 6.40 4.40 -2 5 -23 127.59 8.60 -2 5 -23 137.09 8.80 2 -5 23 128.99 9.00 2 -5 23 137.09 9.50 -3 5 -23 25.90 5.20 -3 5 -23 43.30 5.80 3 -5 23 31.70 5.80 3 -5 23 28.20 5.90 -4 5 -23 40.10 6.00 -4 5 -23 41.50 5.70 4 -5 23 44.10 6.70 4 -5 23 37.50 6.40 -5 5 -23 13.20 5.20 -5 5 -23 9.00 4.50 5 -5 23 9.60 5.50 5 -5 23 5.50 5.20 -6 5 -23 26.90 5.90 -6 5 -23 20.00 5.70 6 -5 23 21.40 6.40 6 -5 23 18.00 5.90 -7 5 -23 49.50 7.10 7 -5 23 43.80 6.80 7 -5 23 52.39 7.90 -8 5 -23 0.10 5.20 8 -5 23 1.60 5.60 8 -5 23 1.90 6.40 9 -5 23 2.80 5.80 6 4 -23 89.19 8.70 -6 -4 23 82.49 9.20 5 4 -23 -2.20 4.80 -5 -4 23 5.00 6.10 4 4 -23 -4.80 4.40 -4 -4 23 -5.10 5.20 3 4 -23 0.60 3.20 3 4 -23 -2.20 4.30 -3 -4 23 -7.00 5.10 2 4 -23 39.60 5.10 2 4 -23 29.60 5.80 -2 -4 23 39.30 5.30 -2 -4 23 47.20 7.30 1 4 -23 17.20 4.20 1 4 -23 14.20 5.00 -1 -4 23 1.30 5.10 -1 -4 23 5.30 3.90 0 4 -23 106.89 8.00 0 4 -23 117.49 8.00 0 -4 23 128.99 9.20 0 -4 23 113.59 8.10 -1 4 -23 8.20 4.70 -1 4 -23 13.10 4.30 1 -4 23 12.60 5.30 1 -4 23 15.00 4.80 -2 4 -23 -0.80 4.40 -2 4 -23 3.00 3.80 2 -4 23 1.00 4.80 2 -4 23 4.20 4.50 -3 4 -23 0.90 4.10 -3 4 -23 2.50 4.10 3 -4 23 -1.50 4.50 3 -4 23 3.90 5.00 -4 4 -23 6.00 4.50 -4 4 -23 6.70 4.50 4 -4 23 1.90 5.00 4 -4 23 10.20 5.20 -5 4 -23 15.90 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-27 5.60 9.60 -4 5 27 -1.20 5.80 3 -5 -27 14.60 6.50 -3 5 27 15.10 6.30 2 -5 -27 -0.80 5.70 -2 5 27 9.60 6.30 1 -5 -27 19.30 6.50 -1 5 27 17.90 6.70 -1 5 27 13.40 5.30 0 -5 -27 33.40 8.80 0 5 27 19.70 6.10 1 5 27 5.00 5.60 -1 6 27 10.80 5.30 0 6 27 10.20 5.60 -1 7 27 10.20 5.70 -1 8 -28 10.40 6.30 2 -8 28 6.20 10.40 1 7 -28 6.40 5.80 0 7 -28 -2.40 4.80 0 7 -28 -9.20 5.60 -1 7 -28 7.00 6.20 1 -7 28 4.80 5.60 -2 7 -28 -1.80 5.70 2 -7 28 2.00 5.70 1 6 -28 1.50 4.50 1 6 -28 2.30 6.10 0 6 -28 40.90 6.40 0 6 -28 40.50 7.50 0 -6 28 40.80 7.00 -1 6 -28 -6.90 5.50 -1 6 -28 11.40 5.30 1 -6 28 8.70 5.80 1 -6 28 18.00 11.30 -2 6 -28 4.60 5.50 -2 6 -28 6.50 5.60 2 -6 28 -0.90 5.50 2 -6 28 9.70 10.80 -3 6 -28 108.69 9.10 3 -6 28 92.29 11.50 1 5 -28 48.40 6.70 1 5 -28 47.80 7.70 -1 -5 28 35.30 11.90 0 5 -28 -2.70 4.40 0 5 -28 -11.30 5.60 0 -5 28 9.70 6.90 0 -5 28 1.10 5.40 -1 5 -28 21.50 6.60 -1 5 -28 19.00 5.60 1 -5 28 33.10 7.60 1 -5 28 33.70 6.90 -2 5 -28 -2.40 5.50 -2 5 -28 -3.80 4.70 2 -5 28 -8.20 5.30 2 -5 28 1.10 6.60 -3 5 -28 2.70 6.50 -3 5 -28 2.00 5.20 3 -5 28 10.50 6.40 3 -5 28 3.70 6.20 -4 5 -28 0.00 5.30 4 -5 28 12.50 8.20 2 4 -28 -0.20 5.60 -2 -4 28 8.20 8.80 1 4 -28 3.00 4.60 1 4 -28 1.90 5.90 -1 -4 28 6.40 6.50 -1 -4 28 4.90 5.60 0 4 -28 -3.10 5.30 0 4 -28 3.40 4.60 0 -4 28 8.50 6.40 0 -4 28 4.10 5.40 -1 4 -28 16.80 5.40 -1 4 -28 16.80 6.40 1 -4 28 25.30 7.00 1 -4 28 10.80 5.90 -2 4 -28 4.90 5.40 -2 4 -28 -2.10 4.80 2 -4 28 6.40 5.80 2 -4 28 9.30 6.60 -3 4 -28 -0.10 5.10 -3 4 -28 -6.20 5.10 3 -4 28 0.00 5.80 3 -4 28 7.40 6.00 -4 4 -28 81.49 8.00 4 -4 28 76.69 8.70 -5 4 -28 18.30 6.00 5 -4 28 25.50 8.60 2 3 -28 6.20 5.70 -2 -3 28 7.50 5.40 -2 -3 28 11.80 7.00 1 3 -28 18.70 6.40 1 3 -28 19.60 5.10 -1 -3 28 13.70 5.90 -1 -3 28 22.70 7.00 0 3 -28 87.09 8.70 0 3 -28 84.19 8.00 0 -3 28 83.39 8.30 0 -3 28 74.09 9.10 -1 3 -28 3.40 5.80 -1 3 -28 7.40 4.80 1 -3 28 16.20 6.60 1 -3 28 -0.20 5.50 -2 3 -28 3.90 5.40 -2 3 -28 3.80 5.10 2 -3 28 6.00 5.80 2 -3 28 10.70 6.30 -3 3 -28 14.30 6.00 -3 3 -28 6.50 5.40 3 -3 28 4.20 6.10 3 -3 28 19.60 6.50 -4 3 -28 12.00 5.70 4 -3 28 12.00 6.40 -5 3 -28 18.70 6.20 5 -3 28 28.30 6.80 3 2 -28 38.50 8.00 -3 -2 28 38.90 8.10 2 2 -28 16.30 6.40 -2 -2 28 18.90 5.70 -2 -2 28 19.90 6.90 1 2 -28 49.90 6.50 1 2 -28 54.99 7.70 -1 -2 28 63.39 7.40 -1 -2 28 68.79 8.50 0 2 -28 25.60 5.60 0 2 -28 21.10 6.30 0 -2 28 38.40 7.40 0 -2 28 24.90 6.60 -1 2 -28 12.10 5.00 -1 2 -28 14.60 6.10 1 -2 28 20.30 6.70 1 -2 28 17.50 6.40 -2 2 -28 6.80 5.90 -2 2 -28 11.70 5.50 2 -2 28 12.70 6.20 2 -2 28 15.10 6.40 -3 2 -28 20.10 6.10 -3 2 -28 43.60 7.10 3 -2 28 38.20 7.20 3 -2 28 26.50 7.10 -4 2 -28 38.50 6.80 4 -2 28 50.99 7.40 3 1 -28 -3.00 5.50 -3 -1 28 1.10 5.20 -3 -1 28 13.20 6.50 2 1 -28 29.90 6.80 -2 -1 28 29.90 6.30 -2 -1 28 32.40 7.20 1 1 -28 -3.60 3.80 1 1 -28 -1.20 5.20 -1 -1 28 3.20 6.30 -1 -1 28 -4.90 5.00 0 1 -28 55.29 6.90 0 1 -28 40.40 7.20 0 -1 28 38.90 7.00 0 -1 28 71.79 8.40 -1 1 -28 -3.50 4.30 -1 1 -28 1.90 5.70 1 -1 28 4.30 5.90 1 -1 28 8.10 5.90 -2 1 -28 -1.40 5.50 -2 1 -28 3.50 5.00 2 -1 28 -0.90 6.00 2 -1 28 14.40 5.70 -3 1 -28 28.70 6.70 -3 1 -28 29.60 6.50 3 -1 28 32.90 9.00 3 -1 28 45.80 7.50 -4 1 -28 5.70 6.10 -4 0 28 31.00 8.00 3 0 -28 -1.00 5.60 -3 0 28 0.80 5.20 -3 0 28 -4.40 6.30 2 0 -28 44.00 7.10 -2 0 28 51.29 8.10 -2 0 28 49.40 7.40 1 0 -28 11.70 5.80 1 0 -28 13.50 4.90 -1 0 28 21.10 6.60 -1 0 28 12.20 6.00 0 0 -28 28.20 5.90 0 0 -28 24.20 6.50 0 0 28 28.00 6.60 0 0 28 27.20 6.50 -1 0 -28 105.59 9.50 -1 0 -28 111.89 9.00 1 0 28 123.59 9.60 1 0 28 115.69 9.90 -2 0 -28 48.40 7.20 -2 0 -28 29.80 6.80 2 0 28 26.50 7.10 -3 0 -28 -1.80 5.50 -3 0 -28 -2.90 4.90 -4 1 28 6.20 5.40 -4 1 28 12.10 6.80 3 -1 -28 1.30 5.40 -3 1 28 8.90 6.60 -3 1 28 5.80 5.60 2 -1 -28 93.09 9.20 -2 1 28 94.59 8.70 -2 1 28 100.59 9.40 1 -1 -28 0.20 4.10 1 -1 -28 -4.20 5.30 -1 1 28 6.00 5.80 -1 1 28 12.40 6.00 0 -1 -28 4.30 5.70 0 -1 -28 -2.40 4.30 0 1 28 -0.30 5.90 0 1 28 7.50 5.60 -1 -1 -28 33.50 6.80 -1 -1 -28 44.60 6.60 1 1 28 53.79 7.90 -2 -1 -28 26.60 6.80 -2 -1 -28 21.80 5.90 2 1 28 23.60 7.40 -4 2 28 34.60 7.40 -4 2 28 30.40 6.60 3 -2 -28 -6.40 5.50 -3 2 28 -5.40 5.70 -3 2 28 -1.30 5.40 2 -2 -28 33.20 6.90 -2 2 28 53.09 7.60 -2 2 28 28.80 6.70 1 -2 -28 -0.10 5.60 1 -2 -28 -4.10 4.10 -1 2 28 7.50 6.10 -1 2 28 -3.10 5.40 0 -2 -28 13.60 6.30 0 -2 -28 14.10 5.30 0 2 28 26.70 7.00 -1 -2 -28 -5.40 4.50 -1 -2 -28 -4.70 5.40 1 2 28 0.70 6.40 -5 3 28 8.30 7.00 -4 3 28 18.20 6.20 -4 3 28 26.80 7.00 -3 3 28 1.50 5.80 -3 3 28 5.50 5.90 2 -3 -28 -1.20 5.70 -2 3 28 0.00 5.80 1 -3 -28 12.50 6.00 -1 3 28 10.50 6.50 -1 3 28 13.20 5.50 0 -3 -28 40.40 7.90 0 3 28 38.20 7.00 0 3 28 25.40 7.60 1 3 28 9.50 5.80 -4 4 28 23.90 6.70 -1 4 28 71.19 7.50 0 4 28 50.69 7.30 -1 5 28 1.00 5.10 0 5 28 18.40 7.90 1 -6 29 25.60 8.70 -2 6 -29 -0.90 7.20 -3 6 -29 6.30 6.90 1 5 -29 -4.60 4.30 0 5 -29 43.40 6.90 0 -5 29 46.60 7.40 -1 5 -29 -1.70 6.10 1 -5 29 -2.60 5.60 -2 5 -29 59.19 7.80 -3 5 -29 0.40 5.90 1 4 -29 6.10 4.90 -1 -4 29 -11.10 5.00 0 4 -29 -6.70 7.20 0 4 -29 3.10 4.90 0 -4 29 3.70 5.70 -1 4 -29 5.10 5.00 -1 4 -29 2.60 5.90 1 -4 29 -2.30 5.50 1 -4 29 -1.00 9.90 -2 4 -29 0.70 5.40 2 -4 29 11.90 8.20 -3 4 -29 -5.80 5.70 1 3 -29 0.20 4.50 -1 -3 29 6.60 5.80 0 3 -29 35.40 7.80 0 3 -29 40.30 6.50 0 -3 29 50.49 8.30 0 -3 29 36.70 7.10 -1 3 -29 10.60 5.80 -1 3 -29 2.70 4.90 1 -3 29 19.90 7.00 1 -3 29 4.90 6.10 -2 3 -29 46.90 7.40 -2 3 -29 39.10 9.00 2 -3 29 50.79 8.10 -3 3 -29 27.90 8.40 3 -3 29 27.90 7.30 -2 -2 29 5.00 5.50 1 2 -29 11.70 5.00 -1 -2 29 12.00 6.10 -1 -2 29 8.90 6.60 0 2 -29 -5.60 4.30 0 2 -29 -0.80 5.90 0 -2 29 -9.30 5.40 0 -2 29 11.90 6.30 -1 2 -29 19.60 6.60 -1 2 -29 14.90 5.40 1 -2 29 21.40 7.20 1 -2 29 31.30 7.00 -2 2 -29 15.30 6.50 -2 2 -29 3.80 5.60 2 -2 29 20.90 6.70 3 -2 29 2.40 6.00 -2 -1 29 25.00 7.10 -2 -1 29 22.90 6.50 1 1 -29 -5.80 4.20 1 1 -29 4.30 9.80 -1 -1 29 3.20 5.80 -1 -1 29 0.40 5.70 0 1 -29 28.70 7.50 0 1 -29 42.30 6.50 0 -1 29 43.70 7.70 0 -1 29 36.50 7.00 -1 1 -29 -4.40 4.50 -1 1 -29 0.80 6.00 1 -1 29 -1.60 6.50 1 -1 29 3.70 6.30 -2 1 -29 51.19 9.50 2 -1 29 45.80 7.50 -3 0 29 -3.70 5.40 -2 0 29 45.60 7.40 -2 0 29 39.50 7.90 1 0 -29 11.50 5.20 -1 0 29 15.10 6.40 -1 0 29 19.60 6.50 0 0 -29 2.80 4.60 0 0 -29 2.20 9.70 0 0 29 7.30 6.30 0 0 29 12.20 6.10 -1 0 -29 2.80 5.00 1 0 29 20.10 6.30 -4 1 29 20.50 7.30 -3 1 29 3.30 7.30 -3 1 29 1.90 5.70 -2 1 29 10.80 6.10 -2 1 29 8.80 6.10 1 -1 -29 8.10 4.70 -1 1 29 10.80 7.00 -1 1 29 10.80 6.10 0 -1 -29 -3.30 4.30 0 1 29 14.10 8.50 -1 -1 -29 64.49 7.50 -3 2 29 36.80 7.70 -2 2 29 5.80 6.00 -3 3 29 23.00 7.20 -1 3 29 2.00 5.70 0 3 29 -0.20 5.40 1 3 -30 -0.90 5.10 1 2 -30 -2.20 4.40 1 1 -30 6.70 5.60 0 1 -30 -1.50 5.70 1 -1 30 13.40 8.30 0 0 -30 -0.40 5.90 0 0 30 9.50 6.40 -1 1 30 3.80 6.90 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 98460 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C4 C 0.5571(2) 0.74484(17) 0.64501(10) 0.0208(4) Uani 1 1 d . . . . . H1 H 0.4600 0.7455 0.6634 0.025 Uiso 1 1 calc R U . . . C5 C 0.6346(3) 0.82904(18) 0.59756(10) 0.0242(4) Uani 1 1 d . . . . . H2 H 0.5900 0.8868 0.5847 0.029 Uiso 1 1 calc R U . . . C6 C 0.7722(2) 0.82814(17) 0.57015(10) 0.0212(4) Uani 1 1 d . . . . . H3 H 0.8231 0.8860 0.5387 0.025 Uiso 1 1 calc R U . . . C12 C 1.1409(2) 0.44837(18) 0.59482(10) 0.0214(4) Uani 1 1 d . . . . . H4 H 1.1718 0.3805 0.6005 0.026 Uiso 1 1 calc R U . . . C10 C 1.1790(2) 0.63161(18) 0.54040(10) 0.0204(4) Uani 1 1 d . . . . . H5 H 1.2370 0.6899 0.5106 0.024 Uiso 1 1 calc R U . . . C13 C 1.0143(2) 0.46019(16) 0.62843(9) 0.0168(4) Uani 1 1 d . . . . . H6 H 0.9593 0.4006 0.6581 0.020 Uiso 1 1 calc R U . . . C16 C 0.7674(2) 0.34823(15) 0.87590(9) 0.0131(3) Uani 1 1 d . . . . . H7 H 0.7690 0.3233 0.9240 0.016 Uiso 1 1 calc R U . . . H8 H 0.8610 0.3396 0.8528 0.016 Uiso 1 1 calc R U . . . Si1 Si 0.77359(5) 0.48706(4) 0.73857(2) 0.01093(10) Uani 1 1 d . . . . . Si2 Si 0.58569(6) 0.32123(4) 0.75078(2) 0.01238(10) Uani 1 1 d . . . . . Si3 Si 0.44064(6) 0.22750(4) 0.89332(2) 0.01337(11) Uani 1 1 d . . . . . Si4 Si 0.85692(6) 0.71467(4) 0.84361(3) 0.01452(11) Uani 1 1 d . . . . . Si5 Si 1.09543(6) 0.57044(4) 0.82879(3) 0.01493(11) Uani 1 1 d . . . . . Si6 Si 0.67514(6) 0.11861(4) 0.81383(3) 0.01547(11) Uani 1 1 d . . . . . Si7 Si 0.44409(6) 0.22674(4) 0.64814(3) 0.01533(11) Uani 1 1 d . . . . . Br1 Br 1.09313(3) 0.85435(2) 0.49978(2) 0.02846(7) Uani 1 1 d . . . . . C1 C 0.8308(2) 0.57125(15) 0.65738(9) 0.0122(3) Uani 1 1 d . . . . . C2 C 0.7651(2) 0.65675(15) 0.63718(9) 0.0139(4) Uani 1 1 d . . . . . C7 C 0.8422(2) 0.74180(16) 0.58765(9) 0.0160(4) Uani 1 1 d . . . . . C9 C 1.0429(2) 0.64489(16) 0.57282(9) 0.0155(4) Uani 1 1 d . . . . . C3 C 0.6212(2) 0.66275(16) 0.66446(9) 0.0170(4) Uani 1 1 d . . . . . H9 H 0.5686 0.6078 0.6972 0.020 Uiso 1 1 calc R U . . . C8 C 0.9822(2) 0.73538(16) 0.56002(9) 0.0166(4) Uani 1 1 d . . . . . C14 C 0.9609(2) 0.55891(16) 0.62068(9) 0.0136(4) Uani 1 1 d . . . . . C15 C 0.6186(2) 0.25768(15) 0.83600(9) 0.0116(3) Uani 1 1 d . . . . . C17 C 0.7849(2) 0.48242(15) 0.88139(9) 0.0130(3) Uani 1 1 d . . . . . H10 H 0.8352 0.5174 0.9273 0.016 Uiso 1 1 calc R U . . . H11 H 0.6787 0.4889 0.8813 0.016 Uiso 1 1 calc R U . . . C18 C 0.8803(2) 0.56122(15) 0.82343(9) 0.0114(3) Uani 1 1 d . . . . . C11 C 1.2268(2) 0.53726(19) 0.55141(10) 0.0233(4) Uani 1 1 d . . . . . H12 H 1.3183 0.5309 0.5299 0.028 Uiso 1 1 calc R U . . . C19 C 0.2276(2) 0.16223(19) 0.65922(11) 0.0257(4) Uani 1 1 d . . . . . H13 H 0.1900 0.2218 0.6841 0.039 Uiso 1 1 calc R U . . . H14 H 0.2048 0.0918 0.6862 0.039 Uiso 1 1 calc R U . . . H15 H 0.1750 0.1394 0.6132 0.039 Uiso 1 1 calc R U . . . C20 C 0.5084(3) 0.10596(19) 0.60392(11) 0.0295(5) Uani 1 1 d . . . . . H16 H 0.4467 0.0751 0.5605 0.044 Uiso 1 1 calc R U . . . H17 H 0.4928 0.0413 0.6350 0.044 Uiso 1 1 calc R U . . . H18 H 0.6195 0.1383 0.5931 0.044 Uiso 1 1 calc R U . . . C21 C 0.4860(2) 0.35023(17) 0.58833(10) 0.0203(4) Uani 1 1 d . . . . . H19 H 0.5986 0.3809 0.5804 0.031 Uiso 1 1 calc R U . . . H20 H 0.4519 0.4145 0.6096 0.031 Uiso 1 1 calc R U . . . H21 H 0.4295 0.3201 0.5436 0.031 Uiso 1 1 calc R U . . . C22 C 0.2529(2) 0.14771(18) 0.84400(11) 0.0235(4) Uani 1 1 d . . . . . H22 H 0.1668 0.1275 0.8767 0.035 Uiso 1 1 calc R U . . . H23 H 0.2597 0.0746 0.8196 0.035 Uiso 1 1 calc R U . . . H24 H 0.2339 0.1993 0.8098 0.035 Uiso 1 1 calc R U . . . C23 C 0.4180(2) 0.36745(17) 0.93521(10) 0.0187(4) Uani 1 1 d . . . . . H25 H 0.4130 0.4203 0.8990 0.028 Uiso 1 1 calc R U . . . H26 H 0.5076 0.4076 0.9670 0.028 Uiso 1 1 calc R U . . . H27 H 0.3214 0.3476 0.9616 0.028 Uiso 1 1 calc R U . . . C24 C 0.4536(3) 0.13651(18) 0.96776(10) 0.0244(4) Uani 1 1 d . . . . . H28 H 0.3678 0.1323 0.9996 0.037 Uiso 1 1 calc R U . . . H29 H 0.5538 0.1738 0.9931 0.037 Uiso 1 1 calc R U . . . H30 H 0.4461 0.0559 0.9495 0.037 Uiso 1 1 calc R U . . . C25 C 0.5015(2) -0.01570(17) 0.78911(12) 0.0276(5) Uani 1 1 d . . . . . H31 H 0.4381 0.0032 0.7531 0.041 Uiso 1 1 calc R U . . . H32 H 0.4386 -0.0395 0.8304 0.041 Uiso 1 1 calc R U . . . H33 H 0.5370 -0.0812 0.7709 0.041 Uiso 1 1 calc R U . . . C26 C 0.7787(3) 0.08342(18) 0.89021(11) 0.0260(4) Uani 1 1 d . . . . . H34 H 0.7112 0.0724 0.9308 0.039 Uiso 1 1 calc R U . . . H35 H 0.8760 0.1493 0.9015 0.039 Uiso 1 1 calc R U . . . H36 H 0.8030 0.0102 0.8782 0.039 Uiso 1 1 calc R U . . . C27 C 0.8168(2) 0.13822(18) 0.74094(10) 0.0221(4) Uani 1 1 d . . . . . H37 H 0.8389 0.0637 0.7303 0.033 Uiso 1 1 calc R U . . . H38 H 0.9142 0.2021 0.7551 0.033 Uiso 1 1 calc R U . . . H39 H 0.7714 0.1591 0.6993 0.033 Uiso 1 1 calc R U . . . C28 C 1.2203(2) 0.69361(19) 0.77853(12) 0.0275(5) Uani 1 1 d . . . . . H40 H 1.2131 0.7697 0.7982 0.041 Uiso 1 1 calc R U . . . H41 H 1.1843 0.6803 0.7295 0.041 Uiso 1 1 calc R U . . . H42 H 1.3292 0.6955 0.7815 0.041 Uiso 1 1 calc R U . . . C29 C 1.1416(2) 0.43341(18) 0.79654(10) 0.0217(4) Uani 1 1 d . . . . . H43 H 1.0852 0.4009 0.7521 0.032 Uiso 1 1 calc R U . . . H44 H 1.1093 0.3736 0.8311 0.032 Uiso 1 1 calc R U . . . H45 H 1.2544 0.4542 0.7897 0.032 Uiso 1 1 calc R U . . . C30 C 1.1679(3) 0.5954(2) 0.92214(11) 0.0295(5) Uani 1 1 d . . . . . H46 H 1.2790 0.6032 0.9239 0.044 Uiso 1 1 calc R U . . . H47 H 1.1084 0.5275 0.9480 0.044 Uiso 1 1 calc R U . . . H48 H 1.1541 0.6684 0.9433 0.044 Uiso 1 1 calc R U . . . C31 C 0.9337(2) 0.82503(16) 0.77587(10) 0.0223(4) Uani 1 1 d . . . . . H49 H 0.8459 0.8381 0.7517 0.033 Uiso 1 1 calc R U . . . H50 H 0.9940 0.7938 0.7420 0.033 Uiso 1 1 calc R U . . . H51 H 1.0014 0.9007 0.7987 0.033 Uiso 1 1 calc R U . . . C32 C 0.9581(2) 0.78952(18) 0.92857(10) 0.0244(4) Uani 1 1 d . . . . . H52 H 0.9222 0.8566 0.9430 0.037 Uiso 1 1 calc R U . . . H53 H 1.0715 0.8188 0.9223 0.037 Uiso 1 1 calc R U . . . H54 H 0.9334 0.7321 0.9646 0.037 Uiso 1 1 calc R U . . . C33 C 0.6442(2) 0.69482(17) 0.85609(10) 0.0205(4) Uani 1 1 d . . . . . H55 H 0.6263 0.7706 0.8506 0.031 Uiso 1 1 calc R U . . . H56 H 0.6148 0.6694 0.9031 0.031 Uiso 1 1 calc R U . . . H57 H 0.5807 0.6342 0.8211 0.031 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C4 0.0236(10) 0.0246(10) 0.0182(9) -0.0021(8) 0.0012(8) 0.0140(8) C5 0.0355(12) 0.0209(10) 0.0232(10) 0.0016(8) 0.0007(9) 0.0190(9) C6 0.0324(11) 0.0149(9) 0.0184(10) 0.0039(7) 0.0025(8) 0.0103(8) C12 0.0242(10) 0.0264(10) 0.0193(10) 0.0056(8) 0.0024(8) 0.0154(9) C10 0.0178(10) 0.0268(10) 0.0161(9) 0.0077(8) 0.0055(7) 0.0056(8) C13 0.0199(9) 0.0193(9) 0.0133(9) 0.0058(7) 0.0023(7) 0.0084(8) C16 0.0128(8) 0.0125(8) 0.0130(8) 0.0025(7) -0.0006(7) 0.0025(7) Si1 0.0114(2) 0.0105(2) 0.0099(2) 0.00222(17) 0.00102(17) 0.00202(18) Si2 0.0125(2) 0.0114(2) 0.0113(2) 0.00178(18) 0.00032(18) 0.00112(19) Si3 0.0134(2) 0.0125(2) 0.0136(2) 0.00330(18) 0.00413(19) 0.00290(19) Si4 0.0165(2) 0.0102(2) 0.0156(2) 0.00008(18) -0.00043(19) 0.00296(19) Si5 0.0110(2) 0.0169(2) 0.0155(2) 0.00206(19) -0.00113(19) 0.0025(2) Si6 0.0166(3) 0.0101(2) 0.0203(3) 0.00209(19) 0.0030(2) 0.0050(2) Si7 0.0155(2) 0.0166(2) 0.0142(2) -0.00073(19) 0.00023(19) 0.0062(2) Br1 0.03141(12) 0.02323(11) 0.03196(12) 0.01644(9) 0.01220(9) 0.00768(9) C1 0.0133(8) 0.0106(8) 0.0102(8) 0.0005(6) -0.0003(7) 0.0006(7) C2 0.0179(9) 0.0118(8) 0.0110(8) -0.0012(7) -0.0011(7) 0.0038(7) C7 0.0210(9) 0.0133(9) 0.0135(9) 0.0006(7) -0.0015(7) 0.0055(7) C9 0.0163(9) 0.0167(9) 0.0123(8) 0.0027(7) 0.0003(7) 0.0034(7) C3 0.0191(9) 0.0175(9) 0.0143(9) 0.0004(7) 0.0012(7) 0.0061(8) C8 0.0206(9) 0.0128(9) 0.0139(9) 0.0068(7) 0.0033(7) 0.0009(7) C14 0.0138(9) 0.0156(9) 0.0105(8) 0.0010(7) -0.0016(7) 0.0038(7) C15 0.0116(8) 0.0107(8) 0.0119(8) 0.0017(6) 0.0008(7) 0.0025(7) C17 0.0144(9) 0.0125(8) 0.0101(8) 0.0020(6) 0.0008(7) 0.0016(7) C18 0.0115(8) 0.0105(8) 0.0103(8) 0.0012(6) -0.0004(6) 0.0010(7) C11 0.0200(10) 0.0345(11) 0.0200(10) 0.0069(8) 0.0059(8) 0.0144(9) C19 0.0184(10) 0.0314(11) 0.0234(10) 0.0031(9) -0.0019(8) 0.0027(9) C20 0.0406(13) 0.0280(11) 0.0232(11) -0.0067(9) -0.0019(9) 0.0177(10) C21 0.0216(10) 0.0237(10) 0.0148(9) 0.0007(8) -0.0009(7) 0.0063(8) C22 0.0131(9) 0.0243(10) 0.0285(11) -0.0011(8) 0.0044(8) 0.0005(8) C23 0.0179(9) 0.0207(9) 0.0185(9) 0.0023(7) 0.0077(7) 0.0074(8) C24 0.0311(11) 0.0218(10) 0.0223(10) 0.0111(8) 0.0094(9) 0.0095(9) C25 0.0272(11) 0.0131(9) 0.0387(12) -0.0026(8) 0.0065(9) 0.0024(8) C26 0.0294(11) 0.0242(10) 0.0307(11) 0.0104(9) 0.0041(9) 0.0157(9) C27 0.0220(10) 0.0219(10) 0.0256(10) 0.0003(8) 0.0050(8) 0.0119(8) C28 0.0137(10) 0.0258(11) 0.0391(12) 0.0105(9) 0.0022(9) -0.0004(8) C29 0.0169(9) 0.0272(10) 0.0235(10) 0.0032(8) 0.0007(8) 0.0105(8) C30 0.0263(11) 0.0442(13) 0.0220(11) -0.0054(9) -0.0082(9) 0.0185(10) C31 0.0258(11) 0.0113(9) 0.0269(11) 0.0039(8) -0.0005(8) 0.0020(8) C32 0.0302(11) 0.0204(10) 0.0213(10) -0.0052(8) -0.0052(8) 0.0079(9) C33 0.0228(10) 0.0192(10) 0.0221(10) 0.0005(8) 0.0016(8) 0.0106(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C3 C4 C5 120.14(18) . . C6 C5 C4 120.58(18) . . C5 C6 C7 121.33(18) . . C13 C12 C11 119.93(18) . . C11 C10 C9 121.29(17) . . C12 C13 C14 122.36(17) . . C17 C16 C15 118.41(14) . . C1 Si1 C18 117.05(8) . . C1 Si1 Si2 128.72(6) . . C18 Si1 Si2 113.99(6) . . C15 Si2 Si1 109.52(6) . . C15 Si2 Si7 130.65(6) . . Si1 Si2 Si7 115.87(3) . . C22 Si3 C23 106.02(9) . . C22 Si3 C24 107.53(10) . . C23 Si3 C24 105.24(9) . . C22 Si3 C15 112.95(8) . . C23 Si3 C15 112.60(8) . . C24 Si3 C15 111.97(9) . . C33 Si4 C31 108.61(9) . . C33 Si4 C32 105.24(9) . . C31 Si4 C32 105.95(9) . . C33 Si4 C18 109.13(8) . . C31 Si4 C18 115.45(8) . . C32 Si4 C18 111.92(8) . . C28 Si5 C30 109.03(11) . . C28 Si5 C29 105.97(10) . . C30 Si5 C29 103.04(9) . . C28 Si5 C18 111.16(8) . . C30 Si5 C18 110.43(9) . . C29 Si5 C18 116.70(8) . . C25 Si6 C27 108.03(9) . . C25 Si6 C26 107.64(10) . . C27 Si6 C26 104.88(9) . . C25 Si6 C15 112.38(9) . . C27 Si6 C15 112.55(8) . . C26 Si6 C15 110.97(9) . . C21 Si7 C20 107.43(10) . . C21 Si7 C19 109.45(9) . . C20 Si7 C19 106.92(10) . . C21 Si7 Si2 102.93(6) . . C20 Si7 Si2 115.45(7) . . C19 Si7 Si2 114.32(7) . . C2 C1 C14 118.48(16) . . C2 C1 Si1 123.49(13) . . C14 C1 Si1 117.46(13) . . C1 C2 C3 121.70(16) . . C1 C2 C7 120.75(16) . . C3 C2 C7 117.55(16) . . C8 C7 C6 123.75(17) . . C8 C7 C2 117.83(16) . . C6 C7 C2 118.42(17) . . C8 C9 C10 123.96(17) . . C8 C9 C14 117.44(16) . . C10 C9 C14 118.60(16) . . C4 C3 C2 121.95(18) . . C9 C8 C7 123.35(16) . . C9 C8 Br1 118.37(14) . . C7 C8 Br1 118.26(13) . . C1 C14 C13 121.61(16) . . C1 C14 C9 121.13(16) . . C13 C14 C9 117.25(16) . . C16 C15 Si3 110.50(11) . . C16 C15 Si6 104.45(11) . . Si3 C15 Si6 112.67(9) . . C16 C15 Si2 108.87(11) . . Si3 C15 Si2 111.48(9) . . Si6 C15 Si2 108.57(8) . . C16 C17 C18 117.71(14) . . C17 C18 Si1 104.18(11) . . C17 C18 Si5 110.33(11) . . Si1 C18 Si5 114.70(9) . . C17 C18 Si4 104.61(11) . . Si1 C18 Si4 110.80(8) . . Si5 C18 Si4 111.49(8) . . C10 C11 C12 120.38(18) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 C4 C3 1.361(3) . C4 C5 1.412(3) . C5 C6 1.357(3) . C6 C7 1.430(3) . C12 C13 1.359(3) . C12 C11 1.416(3) . C10 C11 1.358(3) . C10 C9 1.431(3) . C13 C14 1.426(3) . C16 C17 1.550(2) . C16 C15 1.578(2) . Si1 C1 1.8916(17) . Si1 C18 1.8962(17) . Si1 Si2 2.1711(7) . Si2 C15 1.9099(17) . Si2 Si7 2.3492(7) . Si3 C22 1.869(2) . Si3 C23 1.8727(19) . Si3 C24 1.8768(19) . Si3 C15 1.9022(18) . Si4 C33 1.880(2) . Si4 C31 1.8818(19) . Si4 C32 1.883(2) . Si4 C18 1.9214(18) . Si5 C28 1.864(2) . Si5 C30 1.875(2) . Si5 C29 1.879(2) . Si5 C18 1.9164(18) . Si6 C25 1.870(2) . Si6 C27 1.874(2) . Si6 C26 1.880(2) . Si6 C15 1.9098(18) . Si7 C21 1.8688(19) . Si7 C20 1.874(2) . Si7 C19 1.874(2) . Br1 C8 1.9109(17) . C1 C2 1.411(2) . C1 C14 1.417(2) . C2 C3 1.427(3) . C2 C7 1.445(2) . C7 C8 1.398(3) . C9 C8 1.396(3) . C9 C14 1.442(2) . C17 C18 1.575(2) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C3 C4 C5 C6 0.9(3) . . . . C4 C5 C6 C7 0.7(3) . . . . C11 C12 C13 C14 1.3(3) . . . . C18 Si1 C1 C2 -86.27(16) . . . . Si2 Si1 C1 C2 87.75(15) . . . . C18 Si1 C1 C14 84.95(15) . . . . Si2 Si1 C1 C14 -101.03(13) . . . . C14 C1 C2 C3 170.75(16) . . . . Si1 C1 C2 C3 -18.1(2) . . . . C14 C1 C2 C7 -9.2(2) . . . . Si1 C1 C2 C7 161.96(13) . . . . C5 C6 C7 C8 178.80(19) . . . . C5 C6 C7 C2 -1.8(3) . . . . C1 C2 C7 C8 0.8(3) . . . . C3 C2 C7 C8 -179.17(16) . . . . C1 C2 C7 C6 -178.67(17) . . . . C3 C2 C7 C6 1.4(2) . . . . C11 C10 C9 C8 -175.63(19) . . . . C11 C10 C9 C14 3.1(3) . . . . C5 C4 C3 C2 -1.3(3) . . . . C1 C2 C3 C4 -179.81(17) . . . . C7 C2 C3 C4 0.1(3) . . . . C10 C9 C8 C7 174.64(18) . . . . C14 C9 C8 C7 -4.2(3) . . . . C10 C9 C8 Br1 -3.7(3) . . . . C14 C9 C8 Br1 177.50(13) . . . . C6 C7 C8 C9 -174.47(18) . . . . C2 C7 C8 C9 6.1(3) . . . . C6 C7 C8 Br1 3.9(3) . . . . C2 C7 C8 Br1 -175.51(13) . . . . C2 C1 C14 C13 -167.53(16) . . . . Si1 C1 C14 C13 20.8(2) . . . . C2 C1 C14 C9 11.3(3) . . . . Si1 C1 C14 C9 -160.40(13) . . . . C12 C13 C14 C1 -178.51(18) . . . . C12 C13 C14 C9 2.7(3) . . . . C8 C9 C14 C1 -4.8(3) . . . . C10 C9 C14 C1 176.36(16) . . . . C8 C9 C14 C13 174.06(16) . . . . C10 C9 C14 C13 -4.8(2) . . . . C17 C16 C15 Si3 -77.61(16) . . . . C17 C16 C15 Si6 160.96(12) . . . . C17 C16 C15 Si2 45.13(18) . . . . C15 C16 C17 C18 -92.71(19) . . . . C16 C17 C18 Si1 58.11(16) . . . . C16 C17 C18 Si5 -65.48(17) . . . . C16 C17 C18 Si4 174.50(12) . . . . C1 Si1 C18 C17 169.29(11) . . . . Si2 Si1 C18 C17 -5.60(12) . . . . C1 Si1 C18 Si5 -70.01(11) . . . . Si2 Si1 C18 Si5 115.11(8) . . . . C1 Si1 C18 Si4 57.30(11) . . . . Si2 Si1 C18 Si4 -117.58(7) . . . . C9 C10 C11 C12 0.9(3) . . . . C13 C12 C11 C10 -3.2(3) . . . .