#------------------------------------------------------------------------------ #$Date: 2019-12-16 11:42:54 +0200 (Mon, 16 Dec 2019) $ #$Revision: 245208 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/65/1556588.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556588 loop_ _publ_author_name 'Akasaka, N.' 'Tanaka, K.' 'Ishida, S.' 'Iwamoto, T.' _publ_section_title ; Synthesis and Functionalization of a 1,2-Bis(trimethylsilyl)-1,2-disilacyclohexene That Can Serve as a Unit of cis-1,2-Dialkyldisilene ; _journal_name_full Inorganics _journal_page_first 21 _journal_paper_doi 10.3390/inorganics6010021 _journal_volume 6 _journal_year 2018 _chemical_formula_moiety 'C44 H58 Si6, C7 H8' _chemical_formula_sum 'C51 H66 Si6' _chemical_formula_weight 847.57 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _cell_angle_alpha 95.628(2) _cell_angle_beta 98.481(2) _cell_angle_gamma 90.755(2) _cell_formula_units_Z 2 _cell_length_a 11.9302(9) _cell_length_b 12.8081(10) _cell_length_c 15.7049(13) _cell_measurement_reflns_used 9887 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 31.51 _cell_measurement_theta_min 2.17 _cell_volume 2361.1(3) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 8.333 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEXII CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator 'Bruker Helios multilayer confocal mirror' _diffrn_radiation_source 'Bruker TXS fine-focus rotating anode' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0432 _diffrn_reflns_av_unetI/netI 0.0273 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 58976 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.500 _diffrn_reflns_theta_min 1.318 _exptl_absorpt_coefficient_mu 0.211 _exptl_absorpt_correction_T_max 0.7462 _exptl_absorpt_correction_T_min 0.6636 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details 'SADABS Sheldrick 1996' _exptl_crystal_colour purple _exptl_crystal_density_diffrn 1.192 _exptl_crystal_description block _exptl_crystal_F_000 912 _exptl_crystal_size_max 0.080 _exptl_crystal_size_mid 0.030 _exptl_crystal_size_min 0.020 _refine_diff_density_max 0.397 _refine_diff_density_min -0.269 _refine_diff_density_rms 0.050 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.028 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 568 _refine_ls_number_reflns 8802 _refine_ls_number_restraints 126 _refine_ls_restrained_S_all 1.025 _refine_ls_R_factor_all 0.0458 _refine_ls_R_factor_gt 0.0350 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0456P)^2^+1.5701P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0885 _refine_ls_wR_factor_ref 0.0954 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 7374 _reflns_number_total 8802 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file Cpd7_NA152a_a_final_171211.cif _cod_data_source_block NA152a_a _cod_database_code 1556588 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.983 _shelx_estimated_absorpt_t_max 0.996 _shelx_res_file ; NA152a_a.res created by SHELXL-2014/7 TITL NA152a_a.res in P-1 REM Yadorkari-X generated CELL 0.71073 11.9302 12.8081 15.7049 95.6280 98.4810 90.7550 ZERR 2.0 0.0009 0.0010 0.0013 0.0020 0.0020 0.0020 LATT 1 REM SPGR P-1 triclinic SFAC C H Si UNIT 102 132 12 SIZE 0.08 0.03 0.02 TEMP -173.0 L.S. 10 FMAP 2 PLAN -20 ACTA CONF LIST 4 MERG 2 OMIT -10.000000 51.000000 RIGU C45 C46 C47 C48 C49 C50 C51 RIGU C52 C53 C54 C55 C56 C57 C58 SIMU 0.01 0.02 2.0 C53 C54 C55 C56 C57 C58 WGHT 0.045600 1.570100 FVAR 0.47410 0.64807 SI1 3 0.300733 0.350015 0.675276 11.00000 0.01246 0.01507 = 0.01527 -0.00330 -0.00130 0.00296 SI2 3 0.443086 0.288613 0.753860 11.00000 0.01358 0.01755 = 0.01248 -0.00339 -0.00163 0.00324 SI3 3 0.092723 0.212709 0.575167 11.00000 0.01084 0.01863 = 0.01921 0.00031 -0.00177 -0.00056 SI4 3 0.254801 0.325920 0.470732 11.00000 0.01546 0.01722 = 0.01547 0.00154 -0.00158 0.00120 SI5 3 0.666867 0.215546 0.688895 11.00000 0.01097 0.02124 = 0.02023 -0.00139 -0.00025 0.00330 SI6 3 0.491552 0.042412 0.724742 11.00000 0.01884 0.01627 = 0.01630 -0.00007 -0.00038 0.00341 C1 1 0.213530 0.457435 0.721169 11.00000 0.01332 0.02068 = 0.01676 -0.00661 -0.00319 0.00309 C2 1 0.142230 0.439247 0.783166 11.00000 0.01565 0.02739 = 0.01620 -0.00905 -0.00262 0.00151 C3 1 0.138668 0.343238 0.821332 11.00000 0.02253 0.03149 = 0.01897 -0.00700 0.00073 -0.00086 AFIX 43 H1 2 0.188557 0.289386 0.806746 11.00000 -1.20000 AFIX 0 C5 1 -0.008772 0.404673 0.901426 11.00000 0.02904 0.05780 = 0.02592 -0.01333 0.01229 -0.00671 AFIX 43 H2 2 -0.060002 0.391829 0.940391 11.00000 -1.20000 AFIX 0 C6 1 -0.007571 0.497485 0.868614 11.00000 0.02558 0.05398 = 0.02980 -0.01514 0.00715 0.00816 AFIX 43 H3 2 -0.058093 0.549854 0.885060 11.00000 -1.20000 AFIX 0 C8 1 0.071618 0.616248 0.777619 11.00000 0.02503 0.03563 = 0.02649 -0.01236 -0.00287 0.01693 AFIX 43 H4 2 0.021326 0.668573 0.794546 11.00000 -1.20000 AFIX 0 C10 1 0.154137 0.741077 0.693985 11.00000 0.03265 0.02362 = 0.03257 -0.00853 -0.01177 0.01536 AFIX 43 H5 2 0.107930 0.794926 0.714529 11.00000 -1.20000 AFIX 0 C11 1 0.225962 0.762747 0.638921 11.00000 0.03381 0.01788 = 0.03721 -0.00262 -0.01214 0.00442 AFIX 43 H6 2 0.229629 0.831196 0.620850 11.00000 -1.20000 AFIX 0 C12 1 0.295913 0.683622 0.608005 11.00000 0.02603 0.02243 = 0.03413 -0.00039 -0.00475 0.00122 AFIX 43 H7 2 0.346127 0.698999 0.568964 11.00000 -1.20000 AFIX 0 C13 1 0.291428 0.585832 0.634000 11.00000 0.01974 0.01909 = 0.02742 -0.00419 -0.00235 0.00404 AFIX 43 H8 2 0.339264 0.533939 0.612659 11.00000 -1.20000 AFIX 0 C14 1 0.217528 0.558358 0.692127 11.00000 0.01607 0.02091 = 0.01767 -0.00695 -0.00755 0.00541 C7 1 0.067995 0.519429 0.809452 11.00000 0.01895 0.03819 = 0.02036 -0.01212 -0.00121 0.00559 C15 1 0.524044 0.365896 0.852997 11.00000 0.01357 0.02358 = 0.01556 -0.00680 -0.00008 0.00376 C16 1 0.566760 0.469271 0.851950 11.00000 0.01496 0.02346 = 0.02348 -0.00886 0.00136 0.00276 C17 1 0.544035 0.529146 0.779699 11.00000 0.02204 0.02514 = 0.02374 -0.00523 -0.00028 -0.00025 AFIX 43 H9 2 0.499036 0.497853 0.728346 11.00000 -1.20000 AFIX 0 C9 1 0.146104 0.639275 0.721956 11.00000 0.02216 0.02524 = 0.02194 -0.00950 -0.00822 0.01024 C4 1 0.066177 0.326035 0.878015 11.00000 0.02917 0.04208 = 0.02121 -0.00729 0.00390 -0.00705 AFIX 43 H10 2 0.065918 0.260785 0.902011 11.00000 -1.20000 AFIX 0 C18 1 0.584131 0.628904 0.781468 11.00000 0.03096 0.02578 = 0.03550 -0.00211 0.00222 -0.00317 AFIX 43 H11 2 0.565873 0.666327 0.732166 11.00000 -1.20000 AFIX 0 C19 1 0.653179 0.677908 0.856384 11.00000 0.03448 0.02534 = 0.04846 -0.00809 0.00124 -0.00777 AFIX 43 H12 2 0.681128 0.747862 0.857264 11.00000 -1.20000 AFIX 0 C20 1 0.678843 0.624943 0.926047 11.00000 0.02704 0.03195 = 0.03987 -0.01444 -0.00551 -0.00498 AFIX 43 H13 2 0.726107 0.657964 0.975616 11.00000 -1.20000 AFIX 0 C21 1 0.637028 0.520462 0.927578 11.00000 0.02013 0.03042 = 0.02576 -0.01177 -0.00164 0.00055 C22 1 0.661554 0.467814 1.000875 11.00000 0.02288 0.03959 = 0.02285 -0.01341 -0.00646 0.00033 AFIX 43 H14 2 0.710067 0.500994 1.049713 11.00000 -1.20000 AFIX 0 C23 1 0.617388 0.368456 1.004830 11.00000 0.02140 0.03836 = 0.01640 -0.00681 -0.00337 0.00659 C24 1 0.639523 0.316322 1.081142 11.00000 0.03559 0.05199 = 0.01647 -0.00465 -0.00727 0.00399 AFIX 43 H15 2 0.687262 0.349952 1.130199 11.00000 -1.20000 AFIX 0 C25 1 0.594497 0.220491 1.085584 11.00000 0.04751 0.05516 = 0.01688 0.00758 -0.00628 0.00740 AFIX 43 H16 2 0.611178 0.186795 1.137054 11.00000 -1.20000 AFIX 0 C26 1 0.521955 0.169923 1.013042 11.00000 0.04301 0.03855 = 0.02146 0.00389 0.00068 0.00257 AFIX 43 H17 2 0.489163 0.102743 1.016432 11.00000 -1.20000 AFIX 0 C27 1 0.499279 0.216783 0.939206 11.00000 0.02804 0.03070 = 0.01593 -0.00306 -0.00292 0.00344 AFIX 43 H18 2 0.450340 0.181495 0.891581 11.00000 -1.20000 AFIX 0 C28 1 0.546153 0.317085 0.930357 11.00000 0.01642 0.02758 = 0.01637 -0.00516 -0.00009 0.00581 C29 1 0.244002 0.260897 0.574111 11.00000 0.01043 0.01299 = 0.01462 -0.00227 -0.00242 0.00160 C30 1 0.320479 0.161732 0.577102 11.00000 0.01447 0.01421 = 0.01402 -0.00261 -0.00213 0.00240 AFIX 23 H19 2 0.299330 0.120255 0.622582 11.00000 -1.20000 H20 2 0.301143 0.117894 0.521172 11.00000 -1.20000 AFIX 0 C31 1 0.450868 0.180156 0.594263 11.00000 0.01442 0.01691 = 0.01187 -0.00145 0.00040 0.00316 AFIX 23 H21 2 0.468232 0.248624 0.574184 11.00000 -1.20000 H22 2 0.485006 0.125378 0.557996 11.00000 -1.20000 AFIX 0 C32 1 0.511658 0.179762 0.690700 11.00000 0.01236 0.01648 = 0.01316 -0.00146 -0.00110 0.00366 C33 1 0.088275 0.121497 0.660767 11.00000 0.01793 0.02993 = 0.02681 0.00441 0.00046 -0.00365 AFIX 137 H23 2 0.009682 0.111135 0.670216 11.00000 -1.50000 H24 2 0.133957 0.151785 0.714772 11.00000 -1.50000 H25 2 0.118856 0.053808 0.642139 11.00000 -1.50000 AFIX 0 C34 1 0.034913 0.132882 0.471721 11.00000 0.01943 0.02218 = 0.02530 0.00046 -0.00500 -0.00405 AFIX 137 H26 2 -0.036951 0.098625 0.477951 11.00000 -1.50000 H27 2 0.089265 0.079415 0.457929 11.00000 -1.50000 H28 2 0.022079 0.178705 0.424982 11.00000 -1.50000 AFIX 0 C35 1 -0.007864 0.320385 0.593541 11.00000 0.01340 0.02965 = 0.03127 -0.00098 0.00114 0.00254 AFIX 137 H29 2 -0.076754 0.308692 0.550943 11.00000 -1.50000 H30 2 0.028014 0.387935 0.587328 11.00000 -1.50000 H31 2 -0.027595 0.320989 0.651988 11.00000 -1.50000 AFIX 0 C36 1 0.141114 0.422258 0.448669 11.00000 0.02120 0.02388 = 0.03098 0.00777 -0.00285 0.00410 AFIX 137 H32 2 0.152733 0.457372 0.397829 11.00000 -1.50000 H33 2 0.143770 0.474570 0.498889 11.00000 -1.50000 H34 2 0.067043 0.385505 0.437683 11.00000 -1.50000 AFIX 0 C37 1 0.242682 0.227501 0.373385 11.00000 0.03810 0.02899 = 0.01792 -0.00074 0.00395 -0.00137 AFIX 137 H35 2 0.167935 0.192099 0.364400 11.00000 -1.50000 H36 2 0.301757 0.175572 0.382361 11.00000 -1.50000 H37 2 0.252004 0.263271 0.322396 11.00000 -1.50000 AFIX 0 C38 1 0.395135 0.393452 0.470838 11.00000 0.01979 0.02953 = 0.02312 0.00854 0.00128 -0.00051 AFIX 137 H38 2 0.386098 0.447313 0.430315 11.00000 -1.50000 H39 2 0.449386 0.341943 0.453071 11.00000 -1.50000 H40 2 0.423310 0.426414 0.529184 11.00000 -1.50000 AFIX 0 C39 1 0.758571 0.227652 0.796762 11.00000 0.01830 0.03553 = 0.03141 -0.00042 -0.00792 -0.00037 AFIX 137 H41 2 0.835411 0.250187 0.790276 11.00000 -1.50000 H42 2 0.761120 0.159524 0.820353 11.00000 -1.50000 H43 2 0.727301 0.279597 0.836257 11.00000 -1.50000 AFIX 0 C40 1 0.679072 0.344204 0.644166 11.00000 0.01682 0.02888 = 0.03108 0.00308 0.00551 0.00071 AFIX 137 H44 2 0.659962 0.400723 0.685872 11.00000 -1.50000 H45 2 0.626747 0.344012 0.589826 11.00000 -1.50000 H46 2 0.756918 0.355458 0.633306 11.00000 -1.50000 AFIX 0 C41 1 0.729854 0.114746 0.616369 11.00000 0.01483 0.03282 = 0.03509 -0.00585 0.00595 0.00418 AFIX 137 H47 2 0.683235 0.106591 0.559150 11.00000 -1.50000 H48 2 0.732296 0.047451 0.641289 11.00000 -1.50000 H49 2 0.806938 0.137533 0.610776 11.00000 -1.50000 AFIX 0 C42 1 0.358896 0.022902 0.773379 11.00000 0.02710 0.02461 = 0.02574 0.00476 0.00458 -0.00067 AFIX 137 H50 2 0.313227 -0.035573 0.740016 11.00000 -1.50000 H51 2 0.315054 0.087045 0.772061 11.00000 -1.50000 H52 2 0.379253 0.007065 0.833416 11.00000 -1.50000 AFIX 0 C43 1 0.610036 0.000342 0.804446 11.00000 0.03005 0.02751 = 0.02623 0.00716 -0.00376 0.00816 AFIX 137 H53 2 0.591959 -0.069532 0.819996 11.00000 -1.50000 H54 2 0.620271 0.050466 0.856477 11.00000 -1.50000 H55 2 0.680071 -0.001992 0.778701 11.00000 -1.50000 AFIX 0 C44 1 0.481342 -0.055655 0.627259 11.00000 0.03043 0.01929 = 0.02553 -0.00301 0.00184 0.00269 AFIX 137 H56 2 0.548231 -0.047949 0.598672 11.00000 -1.50000 H57 2 0.412878 -0.043692 0.586997 11.00000 -1.50000 H58 2 0.477568 -0.126694 0.645045 11.00000 -1.50000 PART 1 AFIX 0 C45 1 0.220257 0.996601 0.978921 21.00000 0.03020 0.12351 = 0.02815 -0.01213 0.00131 0.01313 AFIX 137 H59 2 0.211635 1.012840 1.039862 21.00000 -1.50000 H60 2 0.236972 1.061497 0.954376 21.00000 -1.50000 H61 2 0.282610 0.948249 0.974569 21.00000 -1.50000 AFIX 66 C46 1 0.113171 0.946767 0.930209 21.00000 0.03465 0.05212 = 0.02332 -0.00272 0.00271 0.02591 C47 1 0.058339 0.864087 0.959743 21.00000 0.04136 0.05370 = 0.01993 0.00111 -0.00224 0.01910 AFIX 43 H62 2 0.091175 0.835211 1.010799 21.00000 -1.20000 AFIX 65 C48 1 -0.044537 0.823656 0.914576 21.00000 0.05283 0.03719 = 0.02065 0.00414 0.00035 0.01459 AFIX 43 H63 2 -0.082012 0.767148 0.934762 21.00000 -1.20000 AFIX 65 C49 1 -0.092582 0.865906 0.839874 21.00000 0.04759 0.04263 = 0.01454 0.00237 0.00153 0.01118 AFIX 43 H64 2 -0.162894 0.838273 0.809005 21.00000 -1.20000 AFIX 65 C50 1 -0.037751 0.948586 0.810339 21.00000 0.03162 0.04640 = 0.01549 0.00260 0.00637 0.01330 AFIX 43 H65 2 -0.070588 0.977461 0.759283 21.00000 -1.20000 AFIX 65 C51 1 0.065125 0.989018 0.855505 21.00000 0.02586 0.03982 = 0.02406 0.00148 0.00743 0.01718 AFIX 43 H66 2 0.102600 1.045526 0.835319 21.00000 -1.20000 PART 2 AFIX 0 C52 1 0.231931 1.046040 0.974026 -21.00000 0.03779 0.07696 = 0.03236 -0.00506 0.00546 -0.00715 AFIX 137 H67 2 0.226383 1.067207 1.034909 -21.00000 -1.50000 H68 2 0.239434 1.108681 0.943912 -21.00000 -1.50000 H69 2 0.298464 1.002691 0.970374 -21.00000 -1.50000 AFIX 66 C53 1 0.123517 0.981995 0.931104 -21.00000 0.03197 0.02399 = 0.01668 -0.00035 0.01146 0.01521 C54 1 0.101662 0.889522 0.965981 -21.00000 0.04655 0.03025 = 0.02361 0.00233 0.00634 0.00830 AFIX 43 H70 2 0.151505 0.869030 1.014030 -21.00000 -1.20000 AFIX 65 C55 1 0.006878 0.827030 0.930557 -21.00000 0.05073 0.03543 = 0.02199 0.00175 0.00945 0.00306 AFIX 43 H71 2 -0.008059 0.763828 0.954395 -21.00000 -1.20000 AFIX 65 C56 1 -0.066052 0.857011 0.860255 -21.00000 0.04770 0.04314 = 0.02260 -0.00567 0.00758 0.00002 AFIX 43 H72 2 -0.130832 0.814300 0.836045 -21.00000 -1.20000 AFIX 65 C57 1 -0.044198 0.949485 0.825377 -21.00000 0.03739 0.04769 = 0.02172 0.00274 0.00441 0.00977 AFIX 43 H73 2 -0.094042 0.969975 0.777328 -21.00000 -1.20000 AFIX 65 C58 1 0.050586 1.011978 0.860800 -21.00000 0.02747 0.03575 = 0.02207 -0.00037 0.00956 0.02322 AFIX 43 H74 2 0.065522 1.075179 0.836962 -21.00000 -1.20000 PART 0 AFIX 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM NA152a_a.res in P-1 REM R1 = 0.0350 for 7374 Fo > 4sig(Fo) and 0.0458 for all 8802 data REM 568 parameters refined using 126 restraints END WGHT 0.0456 1.5673 REM Highest difference peak 0.397, deepest hole -0.269, 1-sigma level 0.050 Q1 1 0.2458 0.2701 0.4184 11.00000 0.05 0.40 Q2 1 0.4798 -0.0171 0.6808 11.00000 0.05 0.38 Q3 1 0.6957 0.1637 0.6505 11.00000 0.05 0.37 Q4 1 0.5033 0.1171 0.7135 11.00000 0.05 0.36 Q5 1 0.2710 0.2895 0.6365 11.00000 0.05 0.34 Q6 1 0.4836 0.3363 0.8026 11.00000 0.05 0.34 Q7 1 0.2616 0.2998 0.6193 11.00000 0.05 0.34 Q8 1 0.0670 0.1683 0.5222 11.00000 0.05 0.34 Q9 1 0.5481 0.0212 0.7704 11.00000 0.05 0.33 Q10 1 0.0372 0.2654 0.6012 11.00000 0.05 0.31 Q11 1 0.2536 0.4157 0.6961 11.00000 0.05 0.31 Q12 1 0.5979 0.4944 0.8920 11.00000 0.05 0.31 Q13 1 0.4744 0.2166 0.7205 11.00000 0.05 0.31 Q14 1 0.1845 0.6006 0.7072 11.00000 0.05 0.29 Q15 1 0.1896 0.2285 0.5760 11.00000 0.05 0.28 Q16 1 0.4232 0.0351 0.7533 11.00000 0.05 0.28 Q17 1 0.4997 0.2795 0.9453 11.00000 0.05 0.28 Q18 1 0.3538 -0.0433 0.7873 11.00000 0.05 0.27 Q19 1 0.7155 0.2276 0.7500 11.00000 0.05 0.26 Q20 1 0.6688 0.2814 0.6673 11.00000 0.05 0.26 ; _shelx_res_checksum 54221 _shelx_hkl_file ; -1 0 0 957.50 19.50 -1 0 0 966.10 19.60 -1 0 0 936.91 19.60 -1 0 0 988.90 20.40 -1 0 0 984.30 20.60 -1 0 0 964.70 19.70 -1 0 0 967.80 19.90 -1 0 0 946.11 20.00 1 0 0 974.10 20.40 1 0 0 957.60 19.90 1 0 0 926.11 20.00 1 0 0 1003.90 19.70 1 0 0 993.50 19.70 1 0 0 987.10 19.50 1 0 0 941.41 20.50 -2 0 0 734.23 17.10 -2 0 0 698.33 15.60 -2 0 0 710.13 16.30 -2 0 0 690.93 16.00 -2 0 0 689.53 14.90 -2 0 0 727.83 17.30 -2 0 0 713.13 15.70 -2 0 0 721.93 15.30 2 0 0 717.83 15.70 2 0 0 727.63 15.30 2 0 0 722.23 15.00 2 0 0 702.93 16.00 2 0 0 710.23 17.00 2 0 0 700.43 17.20 2 0 0 710.33 16.20 -3 0 0 430.36 11.20 -3 0 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11.90 1 -4 0 3.60 1.60 1 -4 0 5.10 2.50 1 -4 0 -0.90 2.20 1 -4 0 5.20 3.30 1 -4 0 3.70 1.40 1 -4 0 3.60 2.80 -1 4 0 3.30 1.60 -1 4 0 6.40 1.90 -1 4 0 2.30 1.30 -1 4 0 4.90 1.80 0 -4 0 13.40 2.00 0 -4 0 9.20 3.30 0 -4 0 6.80 2.80 0 -4 0 7.00 2.70 0 -4 0 8.10 1.90 0 -4 0 6.20 2.10 0 -4 0 8.60 2.50 0 -4 0 8.70 2.10 -1 -4 0 677.63 17.70 -1 -4 0 698.93 17.30 -1 -4 0 679.13 16.70 -1 -4 0 701.83 16.30 -1 -4 0 672.73 19.00 -1 -4 0 700.13 16.40 1 4 0 672.33 16.50 1 4 0 645.54 16.40 1 4 0 686.73 15.70 -2 -4 0 393.76 11.90 -2 -4 0 403.26 11.10 -2 -4 0 422.26 11.30 -2 -4 0 396.76 12.20 -2 -4 0 393.96 11.90 2 4 0 391.76 11.50 2 4 0 404.36 12.00 2 4 0 396.46 11.00 2 4 0 385.96 10.80 2 4 0 380.56 12.10 -3 -4 0 4.70 2.30 -3 -4 0 1.50 2.10 -3 -4 0 0.90 2.60 -3 -4 0 2.60 3.40 3 4 0 4.20 2.60 3 4 0 3.70 3.70 3 4 0 4.60 2.60 -4 -4 0 9.30 3.80 -4 -4 0 7.60 2.50 -4 -4 0 6.90 2.60 -4 -4 0 5.90 3.40 4 4 0 10.50 3.20 4 4 0 4.40 3.10 4 4 0 1.00 3.80 -5 -4 0 9.00 3.80 -5 -4 0 7.10 4.00 -5 -4 0 12.50 3.20 -5 -4 0 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88.79 11.70 -11 5 0 76.29 10.50 10 -5 0 27.10 9.50 10 -5 0 12.10 7.20 10 -5 0 20.70 5.10 -10 5 0 20.70 6.30 -10 5 0 18.50 6.40 -10 5 0 21.30 4.90 9 -5 0 73.69 4.00 9 -5 0 54.79 11.20 9 -5 0 61.29 10.60 9 -5 0 77.29 7.40 -9 5 0 78.39 10.50 -9 5 0 70.99 9.20 -9 5 0 72.79 7.40 8 -5 0 4.10 5.60 8 -5 0 6.20 1.70 8 -5 0 2.70 3.30 8 -5 0 8.10 5.90 -8 5 0 0.20 2.90 -8 5 0 6.40 4.20 -8 5 0 6.00 4.70 7 -5 0 226.58 14.30 7 -5 0 228.98 6.20 7 -5 0 226.08 9.50 7 -5 0 205.58 16.20 -7 5 0 219.98 9.80 -7 5 0 216.38 12.10 -7 5 0 219.68 12.90 -7 5 0 235.28 6.40 6 -5 0 111.99 6.30 6 -5 0 107.19 11.50 6 -5 0 109.79 9.80 -6 5 0 116.39 8.50 -6 5 0 105.59 9.00 -6 5 0 89.79 6.20 5 -5 0 13.60 4.30 5 -5 0 13.80 5.60 5 -5 0 19.50 3.20 5 -5 0 23.10 5.60 -5 5 0 19.40 3.30 -5 5 0 17.80 4.20 4 -5 0 1061.89 23.60 4 -5 0 1016.10 29.10 4 -5 0 1017.90 33.50 4 -5 0 1013.50 28.60 -4 5 0 1017.30 24.50 -4 5 0 1055.69 27.00 3 -5 0 55.39 3.80 3 -5 0 59.99 8.20 3 -5 0 58.59 6.20 3 -5 0 56.49 6.40 3 -5 0 61.69 2.60 -3 5 0 61.99 5.50 -3 5 0 57.89 4.30 -3 5 0 57.29 3.40 -3 5 0 59.39 2.70 2 -5 0 94.49 6.80 2 -5 0 92.89 3.70 2 -5 0 87.89 4.00 2 -5 0 91.49 6.70 2 -5 0 85.69 8.80 -2 5 0 85.19 4.20 -2 5 0 87.09 3.60 -2 5 0 87.99 4.80 1 -5 0 368.76 11.50 1 -5 0 340.77 11.90 1 -5 0 370.86 9.60 1 -5 0 388.66 16.00 1 -5 0 371.96 13.10 1 -5 0 366.36 9.30 -1 5 0 351.66 10.40 -1 5 0 364.26 10.10 0 -5 0 191.88 10.60 0 -5 0 198.38 9.10 0 -5 0 204.78 8.20 0 -5 0 211.18 6.40 0 -5 0 212.48 8.20 0 -5 0 206.28 7.30 -1 -5 0 119.39 6.70 -1 -5 0 122.09 5.80 -1 -5 0 128.59 6.70 -1 -5 0 110.29 5.90 -1 -5 0 128.19 5.80 -1 -5 0 120.09 7.90 1 5 0 119.99 5.20 1 5 0 118.49 5.90 -2 -5 0 30.60 4.40 -2 -5 0 33.20 3.60 -2 -5 0 31.10 4.20 -2 -5 0 24.70 3.40 -2 -5 0 33.90 4.50 2 5 0 33.80 4.00 2 5 0 35.50 3.70 2 5 0 33.70 4.50 -3 -5 0 235.18 9.90 -3 -5 0 216.98 8.50 -3 -5 0 214.58 8.20 -3 -5 0 217.78 9.00 -3 -5 0 207.48 8.30 3 5 0 226.58 9.10 3 5 0 218.78 9.90 3 5 0 202.88 8.20 3 5 0 204.48 8.40 -4 -5 0 23.20 3.70 -4 -5 0 29.20 4.10 -4 -5 0 22.40 4.80 -4 -5 0 24.50 4.40 4 5 0 21.10 4.20 4 5 0 29.30 5.40 4 5 0 25.40 4.10 -5 -5 0 73.69 6.80 -5 -5 0 81.69 7.70 -5 -5 0 74.59 5.80 -5 -5 0 76.99 6.20 5 5 0 71.29 7.90 5 5 0 87.39 6.50 5 5 0 67.39 6.20 -6 -5 0 26.40 4.30 -6 -5 0 22.70 5.40 -6 -5 0 33.70 6.40 -6 -5 0 28.10 4.40 6 5 0 30.80 6.40 6 5 0 28.80 4.90 6 5 0 25.10 4.90 -7 -5 0 157.68 10.40 -7 -5 0 150.58 11.10 -7 -5 0 142.99 8.20 -7 -5 0 150.48 9.00 7 5 0 136.09 9.30 7 5 0 158.88 11.20 7 5 0 134.39 9.20 -8 -5 0 151.98 9.60 -8 -5 0 138.89 10.90 -8 -5 0 147.99 8.70 -8 -5 0 157.98 12.00 8 5 0 124.69 9.80 8 5 0 126.79 9.50 8 5 0 149.19 11.90 -9 -5 0 195.88 10.50 -9 -5 0 218.58 11.90 -9 -5 0 201.68 13.10 -9 -5 0 206.38 14.00 9 5 0 204.48 11.70 9 5 0 203.28 12.20 9 5 0 200.08 14.00 -10 -5 0 545.15 20.60 -10 -5 0 569.84 19.00 -10 -5 0 558.34 23.00 -10 -5 0 569.14 20.40 10 5 0 566.04 20.80 10 5 0 594.24 21.40 10 5 0 546.85 23.80 -11 -5 0 268.57 18.30 -11 -5 0 306.57 18.10 -11 -5 0 268.57 13.20 -11 -5 0 274.57 14.80 11 5 0 301.87 15.90 11 5 0 294.47 15.20 11 5 0 293.07 18.40 -12 -5 0 25.60 7.10 -12 -5 0 30.20 6.40 -12 -5 0 41.30 10.50 12 5 0 33.00 8.10 12 5 0 32.50 7.70 12 5 0 22.90 9.10 -13 -5 0 8.80 5.50 -13 -5 0 6.30 6.00 -13 -5 0 -1.90 8.70 13 5 0 10.90 7.40 13 5 0 5.10 8.70 13 5 0 13.60 6.70 -14 -5 0 -4.40 10.30 -14 -5 0 10.70 5.70 -14 -5 0 5.00 6.30 14 5 0 18.90 8.70 14 5 0 5.40 6.50 -15 -5 0 -22.50 9.80 -15 -5 0 5.00 6.60 15 5 0 -0.80 6.70 15 5 0 8.60 8.40 -16 -5 0 16.50 8.20 -16 -5 0 -1.10 12.70 16 5 0 15.10 8.30 16 5 0 36.20 10.60 16 -6 0 1.30 6.40 16 -6 0 9.20 12.50 -16 6 0 0.20 8.70 -16 6 0 3.40 7.50 -16 6 0 -4.80 5.60 15 -6 0 38.30 8.50 15 -6 0 53.79 16.40 -15 6 0 29.40 10.20 -15 6 0 40.10 11.10 -15 6 0 34.70 8.20 14 -6 0 1.40 10.30 14 -6 0 0.70 14.20 14 -6 0 3.10 6.10 -14 6 0 0.30 6.60 -14 6 0 3.30 7.50 -14 6 0 0.60 5.10 13 -6 0 24.90 11.90 13 -6 0 7.00 5.70 13 -6 0 25.80 14.80 -13 6 0 18.70 6.10 -13 6 0 21.80 8.50 -13 6 0 24.80 8.60 12 -6 0 2.90 4.70 12 -6 0 16.50 12.50 12 -6 0 16.10 9.90 -12 6 0 6.00 4.80 -12 6 0 5.90 6.80 -12 6 0 1.50 5.90 11 -6 0 146.39 19.70 11 -6 0 168.28 10.80 11 -6 0 162.18 16.70 -11 6 0 145.49 10.70 -11 6 0 154.58 13.70 -11 6 0 163.38 14.30 10 -6 0 67.69 14.40 10 -6 0 50.09 6.70 10 -6 0 74.39 12.50 -10 6 0 79.19 11.50 -10 6 0 59.09 9.20 -10 6 0 59.09 7.50 9 -6 0 143.89 14.00 9 -6 0 147.39 17.40 9 -6 0 146.69 9.00 -9 6 0 149.99 12.60 -9 6 0 152.78 9.60 -9 6 0 164.78 12.20 8 -6 0 0.50 5.10 8 -6 0 6.60 6.60 8 -6 0 5.30 3.50 -8 6 0 -0.60 3.90 -8 6 0 1.40 4.40 -8 6 0 3.00 3.20 7 -6 0 7.00 6.00 7 -6 0 14.50 6.10 7 -6 0 5.10 3.30 -7 6 0 16.10 4.80 -7 6 0 10.50 3.50 -7 6 0 7.00 4.80 6 -6 0 34.00 7.50 6 -6 0 30.80 4.20 6 -6 0 40.80 8.60 -6 6 0 32.30 4.50 -6 6 0 35.80 6.00 5 -6 0 43.00 4.30 5 -6 0 48.00 7.30 5 -6 0 42.10 7.00 5 -6 0 48.30 8.90 -5 6 0 49.90 4.90 -5 6 0 41.70 5.90 4 -6 0 264.57 16.10 4 -6 0 239.18 12.30 4 -6 0 246.58 6.30 4 -6 0 257.07 8.30 4 -6 0 235.38 12.40 -4 6 0 237.28 9.10 -4 6 0 238.08 6.30 -4 6 0 246.38 7.40 -4 6 0 248.28 11.10 3 -6 0 286.17 16.00 3 -6 0 277.67 8.30 3 -6 0 277.17 7.40 3 -6 0 273.67 12.60 3 -6 0 273.97 12.50 -3 6 0 268.07 9.50 -3 6 0 281.77 11.30 -3 6 0 276.87 8.20 -3 6 0 253.27 7.50 2 -6 0 143.19 8.80 2 -6 0 155.58 5.60 2 -6 0 150.08 5.30 2 -6 0 139.69 8.30 2 -6 0 149.99 11.40 -2 6 0 145.69 5.90 -2 6 0 154.18 6.70 1 -6 0 291.87 14.70 1 -6 0 282.97 12.00 1 -6 0 273.67 8.00 1 -6 0 283.67 10.40 1 -6 0 259.37 10.70 -1 6 0 284.87 9.00 0 -6 0 1235.08 29.70 0 -6 0 1265.57 35.10 0 -6 0 1242.48 30.00 0 -6 0 1250.17 31.80 0 -6 0 1260.27 27.20 0 -6 0 1255.77 28.60 0 6 0 1278.67 28.50 -1 -6 0 60.69 5.70 -1 -6 0 53.79 6.60 -1 -6 0 52.89 5.60 -1 -6 0 53.99 5.10 -1 -6 0 47.30 4.50 -1 -6 0 56.59 4.70 1 6 0 55.39 4.30 1 6 0 56.19 4.90 -2 -6 0 50.89 4.70 -2 -6 0 52.99 5.80 -2 -6 0 44.90 5.70 -2 -6 0 47.90 4.70 -2 -6 0 58.19 5.90 2 6 0 51.79 5.90 2 6 0 48.10 5.00 2 6 0 47.70 4.30 -3 -6 0 493.45 16.00 -3 -6 0 498.85 14.80 -3 -6 0 503.55 15.50 -3 -6 0 490.55 15.60 -3 -6 0 505.85 14.80 3 6 0 502.15 14.40 3 6 0 513.45 15.50 3 6 0 485.05 15.90 -4 -6 0 45.30 5.00 -4 -6 0 50.99 5.20 -4 -6 0 50.89 6.30 -4 -6 0 51.59 5.80 4 6 0 48.90 5.80 4 6 0 48.70 5.30 4 6 0 52.29 7.00 -5 -6 0 86.39 8.30 -5 -6 0 85.89 7.40 -5 -6 0 94.29 7.10 -5 -6 0 85.79 6.60 5 6 0 79.19 6.90 5 6 0 81.99 7.00 5 6 0 79.69 9.00 -6 -6 0 47.80 5.50 -6 -6 0 47.20 6.30 -6 -6 0 48.60 5.90 -6 -6 0 40.00 7.20 6 6 0 45.20 7.30 6 6 0 54.69 6.70 6 6 0 50.09 6.30 -7 -6 0 41.80 5.70 -7 -6 0 69.69 9.00 -7 -6 0 45.30 6.20 -7 -6 0 59.79 7.20 7 6 0 49.00 6.80 7 6 0 51.39 6.70 7 6 0 54.39 8.30 -8 -6 0 65.39 9.60 -8 -6 0 59.99 7.60 -8 -6 0 61.89 7.00 -8 -6 0 57.69 7.10 8 6 0 51.99 7.40 8 6 0 73.09 9.60 8 6 0 66.49 8.00 -9 -6 0 66.09 8.00 -9 -6 0 66.59 9.80 -9 -6 0 79.49 8.10 -9 -6 0 99.59 9.50 9 6 0 68.69 8.20 9 6 0 85.49 10.70 9 6 0 86.09 9.30 -10 -6 0 21.60 6.00 -10 -6 0 11.90 4.80 -10 -6 0 3.70 7.30 -10 -6 0 17.40 5.90 10 6 0 12.80 6.40 10 6 0 12.00 6.80 10 6 0 6.50 5.30 -11 -6 0 12.50 8.50 -11 -6 0 22.60 6.00 -11 -6 0 12.80 5.70 11 6 0 14.60 7.10 11 6 0 17.40 6.50 11 6 0 21.70 8.10 -12 -6 0 -22.80 7.30 -12 -6 0 1.50 5.50 -12 -6 0 9.40 5.40 12 6 0 11.60 7.60 12 6 0 -0.30 6.70 12 6 0 1.20 5.60 -13 -6 0 -12.40 8.60 -13 -6 0 -1.50 4.90 -13 -6 0 -1.90 5.80 13 6 0 5.80 6.50 13 6 0 17.50 7.90 -14 -6 0 5.10 5.50 -14 -6 0 -7.60 10.30 -14 -6 0 1.90 6.30 14 6 0 10.90 7.70 14 6 0 14.70 8.60 -15 -6 0 0.70 7.00 -15 -6 0 -22.40 10.60 15 6 0 8.80 7.90 15 6 0 16.80 8.70 -16 -6 0 92.29 12.80 -16 -6 0 83.99 17.70 16 6 0 131.89 14.70 16 6 0 99.59 14.40 16 -7 0 7.50 13.00 16 -7 0 12.40 7.50 -16 7 0 12.00 9.30 -16 7 0 8.10 9.40 14 -7 0 22.50 6.90 14 -7 0 18.80 12.30 14 -7 0 -1.30 17.20 -14 7 0 8.40 8.00 -14 7 0 10.30 8.70 -14 7 0 2.80 5.40 13 -7 0 3.90 9.60 13 -7 0 -2.70 14.60 13 -7 0 1.80 5.10 -13 7 0 5.50 7.30 -13 7 0 1.90 7.10 -13 7 0 -1.90 4.30 12 -7 0 149.69 11.10 12 -7 0 179.28 26.50 12 -7 0 181.38 19.60 -12 7 0 170.28 12.10 -12 7 0 143.99 14.90 -12 7 0 159.48 16.20 11 -7 0 -4.90 10.10 11 -7 0 -0.70 4.20 11 -7 0 5.00 7.90 -11 7 0 -3.00 5.30 -11 7 0 1.80 4.40 -11 7 0 -4.90 5.10 10 -7 0 272.87 12.80 10 -7 0 291.37 19.90 10 -7 0 311.97 25.70 -10 7 0 285.87 13.80 -10 7 0 273.77 16.70 -10 7 0 285.87 18.20 9 -7 0 56.29 6.50 9 -7 0 56.19 10.60 9 -7 0 65.79 14.20 -9 7 0 52.29 8.80 -9 7 0 61.89 7.40 -9 7 0 53.99 9.80 8 -7 0 0.20 5.30 8 -7 0 6.00 6.80 8 -7 0 11.30 4.00 -8 7 0 6.40 5.40 -8 7 0 6.90 4.80 -8 7 0 6.80 3.60 7 -7 0 55.19 10.80 7 -7 0 64.79 9.90 7 -7 0 63.99 5.90 -7 7 0 62.29 8.10 -7 7 0 52.59 8.60 -7 7 0 56.19 6.20 6 -7 0 86.29 6.20 6 -7 0 89.89 10.10 6 -7 0 90.89 12.50 -6 7 0 87.39 6.80 -6 7 0 92.29 8.60 5 -7 0 609.54 22.80 5 -7 0 577.04 16.10 5 -7 0 615.84 27.60 5 -7 0 598.54 22.30 -5 7 0 645.24 20.90 -5 7 0 631.24 18.00 4 -7 0 1.60 2.30 4 -7 0 4.20 4.10 4 -7 0 2.40 4.50 4 -7 0 6.10 4.10 -4 7 0 3.80 2.10 -4 7 0 1.80 1.50 -4 7 0 6.80 3.60 -4 7 0 5.80 2.80 3 -7 0 237.68 15.70 3 -7 0 243.38 8.00 3 -7 0 248.28 12.60 3 -7 0 256.77 12.70 -3 7 0 242.98 9.50 -3 7 0 249.18 8.30 -3 7 0 259.47 11.30 2 -7 0 75.69 4.50 2 -7 0 83.49 7.80 2 -7 0 65.09 6.30 2 -7 0 74.39 7.20 2 -7 0 65.69 9.40 -2 7 0 77.69 5.60 -2 7 0 65.69 4.80 1 -7 0 502.65 16.60 1 -7 0 514.65 15.90 1 -7 0 507.35 13.00 1 -7 0 512.85 17.90 1 -7 0 506.95 21.40 -1 7 0 512.35 14.20 -1 7 0 496.55 14.50 -1 7 0 510.35 13.90 0 -7 0 497.35 17.40 0 -7 0 494.15 15.80 0 -7 0 515.95 15.70 0 -7 0 519.45 13.10 0 -7 0 521.45 14.70 0 -7 0 513.95 20.40 0 7 0 484.85 14.20 0 7 0 485.35 14.30 -1 -7 0 19.70 3.40 -1 -7 0 17.60 4.80 -1 -7 0 22.20 4.40 -1 -7 0 20.60 4.50 -1 -7 0 23.80 3.90 -1 -7 0 19.10 4.10 1 7 0 22.60 3.90 1 7 0 25.30 3.50 -2 -7 0 0.00 2.80 -2 -7 0 0.30 3.60 -2 -7 0 0.90 3.10 -2 -7 0 4.80 3.00 -2 -7 0 8.90 3.10 2 7 0 -0.90 2.80 2 7 0 3.00 3.80 2 7 0 5.90 3.00 -3 -7 0 3.80 3.40 -3 -7 0 8.00 4.50 -3 -7 0 5.60 3.10 -3 -7 0 7.30 3.20 -3 -7 0 9.00 3.40 3 7 0 3.90 3.30 3 7 0 -0.30 3.10 3 7 0 9.10 4.90 -4 -7 0 1.50 3.00 -4 -7 0 -0.10 2.80 -4 -7 0 -3.50 3.00 -4 -7 0 0.80 2.60 -4 -7 0 5.30 4.70 4 7 0 -1.50 3.40 4 7 0 3.80 5.60 4 7 0 2.50 3.50 -5 -7 0 168.08 11.70 -5 -7 0 189.38 9.70 -5 -7 0 181.38 9.40 -5 -7 0 185.18 10.10 5 7 0 177.88 11.90 5 7 0 187.58 10.30 5 7 0 193.38 10.20 -6 -7 0 19.80 4.50 -6 -7 0 20.80 5.10 -6 -7 0 33.60 7.50 -6 -7 0 25.60 5.10 6 7 0 18.40 5.30 6 7 0 20.80 5.20 6 7 0 20.70 6.50 -7 -7 0 95.89 8.60 -7 -7 0 74.59 9.70 -7 -7 0 91.59 8.50 -7 -7 0 95.59 8.10 7 7 0 79.39 8.40 7 7 0 77.59 8.30 7 7 0 89.99 10.20 -8 -7 0 10.50 4.90 -8 -7 0 11.60 4.50 -8 -7 0 13.00 4.90 -8 -7 0 6.50 6.90 8 7 0 2.80 5.10 8 7 0 12.00 6.00 8 7 0 9.00 4.90 -9 -7 0 68.09 8.10 -9 -7 0 82.39 10.90 -9 -7 0 92.59 8.80 -9 -7 0 94.39 9.30 9 7 0 97.99 10.80 9 7 0 70.19 8.90 9 7 0 91.09 9.90 -10 -7 0 26.20 9.00 -10 -7 0 34.80 6.80 -10 -7 0 28.70 6.90 10 7 0 26.20 6.90 10 7 0 30.20 8.30 10 7 0 29.10 6.90 -11 -7 0 41.70 10.60 -11 -7 0 34.30 7.40 -11 -7 0 53.59 7.90 11 7 0 45.20 9.80 11 7 0 38.10 8.00 11 7 0 42.30 8.90 -12 -7 0 107.39 14.80 -12 -7 0 108.89 11.70 -12 -7 0 121.99 11.70 12 7 0 98.69 11.60 12 7 0 107.59 12.20 -13 -7 0 -16.30 9.30 -13 -7 0 -6.90 5.60 -13 -7 0 -0.30 5.20 13 7 0 5.20 7.90 13 7 0 -5.70 6.10 -14 -7 0 10.30 7.70 -14 -7 0 1.30 11.60 14 7 0 27.30 9.10 14 7 0 12.30 8.30 -15 -7 0 -20.50 11.40 -15 -7 0 -9.80 6.30 15 7 0 3.20 7.70 15 7 0 -13.30 7.70 14 -8 0 51.49 23.40 14 -8 0 48.50 8.60 14 -8 0 58.69 16.10 -14 8 0 46.60 8.50 -14 8 0 48.00 11.50 -14 8 0 57.79 12.70 13 -8 0 92.99 24.90 13 -8 0 49.50 7.90 13 -8 0 55.99 14.50 -13 8 0 49.99 11.50 -13 8 0 44.60 10.70 -13 8 0 61.29 8.90 12 -8 0 0.80 4.50 12 -8 0 6.00 10.00 12 -8 0 3.10 15.70 -12 8 0 7.90 7.70 -12 8 0 -0.80 6.60 -12 8 0 2.10 4.70 11 -8 0 203.08 28.40 11 -8 0 151.08 18.90 11 -8 0 146.29 10.40 -11 8 0 151.38 11.50 -11 8 0 145.19 16.70 -11 8 0 160.68 14.70 10 -8 0 205.08 24.50 10 -8 0 187.18 10.60 10 -8 0 193.58 17.80 -10 8 0 182.38 16.00 -10 8 0 186.18 11.70 -10 8 0 158.88 14.30 9 -8 0 1.60 3.80 9 -8 0 -2.80 5.70 9 -8 0 2.40 7.70 -9 8 0 3.80 5.30 -9 8 0 -1.30 3.50 -9 8 0 -1.90 5.40 8 -8 0 71.89 13.50 8 -8 0 87.59 7.20 8 -8 0 75.29 11.50 -8 8 0 68.49 10.40 -8 8 0 74.39 9.60 -8 8 0 66.39 7.30 7 -8 0 178.18 17.50 7 -8 0 176.28 14.20 7 -8 0 189.68 8.90 -7 8 0 173.08 12.20 -7 8 0 197.28 10.10 -7 8 0 153.08 12.80 6 -8 0 2.00 2.70 6 -8 0 0.10 4.30 6 -8 0 1.30 5.00 6 -8 0 3.20 5.50 -6 8 0 0.00 2.90 -6 8 0 6.50 4.30 5 -8 0 14.50 3.30 5 -8 0 21.70 7.60 5 -8 0 17.80 5.80 5 -8 0 24.80 6.60 -5 8 0 11.50 3.70 -5 8 0 20.50 5.20 4 -8 0 406.36 17.90 4 -8 0 393.86 11.80 4 -8 0 421.46 17.90 4 -8 0 423.66 22.60 -4 8 0 400.56 16.00 -4 8 0 396.66 13.60 -4 8 0 386.96 11.60 3 -8 0 451.85 18.50 3 -8 0 441.76 17.60 3 -8 0 421.46 12.20 3 -8 0 444.66 22.80 -3 8 0 462.45 14.60 -3 8 0 466.35 12.20 -3 8 0 437.66 16.40 -3 8 0 444.36 12.90 2 -8 0 590.64 14.80 2 -8 0 581.94 25.10 2 -8 0 579.64 20.80 2 -8 0 577.34 18.40 2 -8 0 558.74 19.60 -2 8 0 563.14 15.70 -2 8 0 580.64 15.30 -2 8 0 579.34 16.80 1 -8 0 132.49 9.80 1 -8 0 124.89 5.90 1 -8 0 125.69 8.30 1 -8 0 127.99 11.80 1 -8 0 120.79 8.50 -1 8 0 120.39 7.10 -1 8 0 128.29 6.70 -1 8 0 117.39 6.70 0 -8 0 26.00 6.20 0 -8 0 39.70 4.80 0 -8 0 34.50 3.70 0 -8 0 33.20 5.60 0 -8 0 32.60 5.30 0 -8 0 39.30 6.20 0 8 0 27.60 4.30 0 8 0 32.50 4.40 -1 -8 0 95.39 9.40 -1 -8 0 90.39 7.00 -1 -8 0 82.89 7.80 -1 -8 0 92.49 7.90 -1 -8 0 96.39 7.60 1 8 0 90.99 6.60 1 8 0 102.89 6.40 -2 -8 0 159.28 8.50 -2 -8 0 151.68 10.70 -2 -8 0 153.88 9.90 -2 -8 0 154.48 8.20 -2 -8 0 152.38 9.70 2 8 0 150.98 8.10 2 8 0 160.38 8.90 2 8 0 144.29 9.70 -3 -8 0 1.30 3.40 -3 -8 0 3.20 3.20 -3 -8 0 3.80 3.70 -3 -8 0 2.70 4.60 -3 -8 0 0.80 3.30 3 8 0 -3.60 3.30 3 8 0 0.90 5.50 3 8 0 -1.60 3.50 -4 -8 0 3.50 3.80 -4 -8 0 3.30 3.20 -4 -8 0 4.40 5.50 -4 -8 0 5.90 3.70 -4 -8 0 4.10 3.40 4 8 0 2.80 4.00 4 8 0 1.00 4.00 4 8 0 1.40 6.20 -5 -8 0 107.89 8.00 -5 -8 0 95.59 8.30 -5 -8 0 97.29 9.70 -5 -8 0 98.59 8.40 5 8 0 109.19 8.90 5 8 0 94.69 10.90 5 8 0 84.69 7.90 -6 -8 0 110.49 8.50 -6 -8 0 108.49 10.50 -6 -8 0 104.59 8.70 -6 -8 0 109.39 9.10 6 8 0 91.89 9.00 6 8 0 107.59 11.00 6 8 0 107.59 9.20 -7 -8 0 134.19 10.10 -7 -8 0 145.49 13.30 -7 -8 0 136.79 9.80 -7 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123.59 25.60 -3 15 0 97.19 9.40 -3 15 0 104.49 10.80 -3 15 0 95.49 12.40 2 -15 0 0.00 14.20 2 -15 0 8.40 10.90 2 -15 0 -4.30 7.60 -2 15 0 -1.00 6.80 -2 15 0 2.60 5.30 -2 15 0 -4.40 4.70 1 -15 0 51.89 11.50 1 -15 0 106.09 18.60 1 -15 0 97.69 20.20 -1 15 0 54.49 8.50 -1 15 0 50.19 8.40 0 -15 0 -0.60 10.10 0 -15 0 7.30 5.90 0 -15 0 -2.20 10.80 0 15 0 -3.90 5.40 0 15 0 -3.00 5.50 0 15 0 -1.20 5.30 -1 -15 0 15.00 10.80 -1 -15 0 38.50 13.00 -1 -15 0 25.30 7.70 1 15 0 11.40 7.10 1 15 0 27.40 7.30 1 15 0 13.90 6.40 -2 -15 0 32.60 11.60 -2 -15 0 23.70 7.60 2 15 0 19.20 8.00 2 15 0 25.60 7.90 -3 -15 0 11.50 6.40 -3 -15 0 -7.70 8.00 -3 -15 0 7.20 6.30 3 15 0 2.90 6.70 3 15 0 -11.50 6.00 -4 -15 0 1.90 6.30 -4 -15 0 0.80 7.90 -4 -15 0 -7.10 5.90 4 15 0 -1.90 6.60 4 15 0 -2.50 6.70 -5 -15 0 6.00 6.60 -5 -15 0 1.90 7.10 5 15 0 -7.20 6.80 5 15 0 -8.30 6.60 -6 -15 0 -1.40 7.00 -6 -15 0 14.40 8.00 6 15 0 2.00 7.30 6 15 0 -1.50 7.80 -7 -15 0 2.10 7.80 -7 -15 0 1.40 7.40 7 15 0 -5.70 7.70 7 15 0 3.30 8.20 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16 0 83.19 10.50 0 -16 0 35.10 16.30 0 -16 0 68.89 16.30 0 -16 0 23.80 7.90 0 16 0 24.90 7.50 0 16 0 38.10 8.60 -1 -16 0 6.80 12.30 -1 -16 0 10.00 6.70 1 16 0 2.20 6.80 1 16 0 -2.80 6.10 1 16 0 -1.90 5.60 -2 -16 0 23.90 13.70 -2 -16 0 25.30 7.90 2 16 0 12.90 7.90 2 16 0 8.00 7.30 -3 -16 0 4.10 11.20 -3 -16 0 12.70 7.00 3 16 0 7.80 7.70 3 16 0 -3.70 7.30 -4 -16 0 24.40 8.20 -4 -16 0 -4.90 9.40 -4 -16 0 0.80 6.50 4 16 0 -9.00 7.30 4 16 0 3.60 7.70 -5 -16 0 -0.60 6.80 -5 -16 0 26.60 8.50 5 16 0 2.40 8.70 5 16 0 7.20 8.20 -6 -16 0 40.10 9.40 -6 -16 0 52.39 10.40 6 16 0 35.10 10.70 6 16 0 39.30 10.40 -7 -16 0 50.49 10.40 -7 -16 0 62.39 11.30 7 16 0 24.60 10.20 7 16 0 61.79 11.80 -8 -16 0 22.80 9.20 -8 -16 0 55.39 11.00 8 16 0 42.40 11.80 8 16 0 15.10 9.70 6 -17 0 60.29 14.70 -6 17 0 18.20 10.00 -6 17 0 17.10 10.90 -6 17 0 22.80 7.30 5 -17 0 51.29 18.50 4 -17 0 35.70 16.20 3 -17 0 27.00 15.60 -3 17 0 2.40 6.20 -3 17 0 8.30 8.10 2 -17 0 15.90 15.20 -2 17 0 15.50 7.20 -2 17 0 0.40 7.60 1 -17 0 150.18 23.70 -1 17 0 66.89 12.40 -1 17 0 93.19 11.50 -1 17 0 85.69 11.10 -1 -17 0 29.10 8.40 -1 -17 0 18.70 14.40 1 17 0 7.70 6.70 1 17 0 15.70 8.20 -2 -17 0 59.29 17.70 -2 -17 0 53.19 10.40 2 17 0 34.40 8.40 2 17 0 23.40 8.90 2 17 0 30.80 9.50 -3 -17 0 14.20 7.80 -3 -17 0 25.90 12.00 3 17 0 4.10 7.80 3 17 0 -5.30 7.40 -4 -17 0 8.60 7.30 4 17 0 -4.80 8.00 4 17 0 -4.60 8.00 -5 -17 0 12.00 8.00 -5 -17 0 26.00 8.30 5 17 0 7.40 9.20 5 17 0 -6.90 8.40 -6 -17 0 -2.90 7.10 -6 -17 0 15.00 7.40 6 17 0 0.30 9.00 6 17 0 5.00 9.10 0 18 0 22.10 9.10 0 18 0 12.40 7.20 -1 -18 0 24.60 7.90 1 18 0 -2.80 6.30 1 18 0 1.80 8.00 -2 -18 0 9.50 6.60 2 18 0 9.20 9.00 2 18 0 0.60 7.00 -3 -18 0 23.60 8.80 3 18 0 11.00 7.50 3 18 0 10.70 9.90 -4 -18 0 28.80 8.90 4 18 0 8.00 9.70 4 18 0 17.00 9.30 4 18 -1 37.60 10.50 4 18 -1 60.49 12.40 -4 -18 1 55.09 10.20 3 18 -1 22.10 8.40 3 18 -1 65.59 12.20 3 18 -1 40.50 11.60 -3 -18 1 58.49 10.60 2 18 -1 -1.90 8.20 2 18 -1 -0.60 6.40 -2 -18 1 11.80 7.30 1 18 -1 24.60 8.30 1 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5 -13 4 3.10 8.90 -6 13 -4 326.57 19.30 -6 13 -4 273.57 13.40 -6 13 -4 326.27 22.50 6 -13 4 330.97 31.30 6 -13 4 303.47 14.00 6 -13 4 302.87 22.80 -7 13 -4 144.19 18.30 -7 13 -4 117.09 13.90 7 -13 4 163.98 29.10 7 -13 4 174.28 21.40 7 -13 4 114.19 9.90 -8 13 -4 16.80 10.00 -8 13 -4 21.30 8.10 8 -13 4 7.90 20.20 8 -13 4 16.40 12.10 8 -13 4 9.80 5.60 -9 13 -4 24.00 9.50 -9 13 -4 21.90 10.70 9 -13 4 35.30 14.30 9 -13 4 13.10 22.20 9 -13 4 19.00 6.60 -10 13 -4 -4.60 7.10 -10 13 -4 2.60 9.00 10 -13 4 -3.30 11.00 10 -13 4 -3.30 5.40 10 -13 4 1.90 22.10 -11 13 -4 -3.40 8.10 -11 13 -4 -1.30 9.20 11 -13 4 -10.30 5.90 11 -13 4 -3.30 10.80 11 -13 4 14.70 22.30 13 12 -4 26.00 9.70 13 12 -4 9.60 9.40 -13 -12 4 5.20 8.20 -13 -12 4 15.50 8.60 -13 -12 4 21.70 10.40 12 12 -4 2.10 8.00 12 12 -4 3.50 9.00 -12 -12 4 -3.50 6.20 -12 -12 4 3.20 8.50 -12 -12 4 -11.40 6.60 11 12 -4 67.59 12.00 11 12 -4 70.39 12.00 -11 -12 4 77.89 11.70 -11 -12 4 57.39 10.20 -11 -12 4 104.19 13.20 10 12 -4 63.79 11.60 10 12 -4 72.29 11.90 -10 -12 4 55.59 10.40 -10 -12 4 50.79 9.50 -10 -12 4 48.60 9.60 9 12 -4 -0.20 8.10 9 12 -4 0.80 6.40 -9 -12 4 -2.70 5.80 -9 -12 4 4.30 7.10 -9 -12 4 -0.60 5.80 8 12 -4 171.88 27.70 8 12 -4 173.88 14.60 8 12 -4 130.29 13.50 -8 -12 4 145.79 13.80 -8 -12 4 154.78 13.00 -8 -12 4 144.69 13.40 7 12 -4 10.90 7.30 7 12 -4 -1.10 6.10 7 12 -4 4.80 11.20 -7 -12 4 10.00 6.30 -7 -12 4 -6.10 4.20 -7 -12 4 -0.40 5.20 6 12 -4 29.80 7.60 6 12 -4 27.80 8.20 6 12 -4 30.90 12.70 -6 -12 4 32.40 6.80 -6 -12 4 38.60 7.90 -6 -12 4 34.20 7.00 5 12 -4 128.89 12.10 5 12 -4 93.99 15.40 5 12 -4 117.69 11.40 -5 -12 4 113.29 9.50 -5 -12 4 101.09 9.90 -5 -12 4 109.19 9.80 -5 -12 4 107.29 10.70 4 12 -4 116.59 13.20 4 12 -4 122.09 16.30 4 12 -4 149.59 11.80 4 12 -4 129.59 11.30 -4 -12 4 143.99 10.80 -4 -12 4 133.39 10.20 -4 -12 4 96.49 9.20 -4 -12 4 143.59 11.40 3 12 -4 12.70 6.60 3 12 -4 14.90 6.00 3 12 -4 21.00 10.80 3 12 -4 23.30 6.70 -3 -12 4 12.30 4.90 -3 -12 4 20.60 5.50 -3 -12 4 16.60 5.30 -3 -12 4 15.30 5.80 2 12 -4 45.20 10.90 2 12 -4 30.50 8.40 2 12 -4 37.80 7.20 -2 -12 4 33.70 5.90 -2 -12 4 35.50 6.00 -2 -12 4 43.10 8.10 -2 -12 4 45.20 6.90 -1 -12 4 -0.40 3.70 -1 -12 4 -0.30 3.40 -1 -12 4 -1.80 4.90 -1 -12 4 2.20 4.30 -1 -12 4 5.30 4.70 0 -12 4 33.10 11.30 0 -12 4 39.50 5.70 0 -12 4 36.10 9.40 0 -12 4 39.80 6.00 0 -12 4 44.70 6.00 0 -12 4 44.50 8.90 -1 12 -4 127.99 8.80 -1 12 -4 103.39 10.20 1 -12 4 112.89 8.40 1 -12 4 128.59 8.50 1 -12 4 165.38 14.60 1 -12 4 136.19 18.40 -2 12 -4 20.90 6.20 -2 12 -4 28.00 8.10 -2 12 -4 29.00 5.20 -2 12 -4 22.70 4.60 2 -12 4 27.90 5.40 2 -12 4 30.50 11.50 2 -12 4 28.70 4.90 2 -12 4 22.40 8.40 -3 12 -4 23.80 4.40 -3 12 -4 15.80 7.30 -3 12 -4 13.40 5.70 -3 12 -4 18.70 4.70 3 -12 4 17.40 4.90 3 -12 4 21.70 4.30 3 -12 4 11.50 10.60 3 -12 4 26.10 8.70 -4 12 -4 63.59 6.90 -4 12 -4 62.79 11.20 -4 12 -4 56.29 8.70 4 -12 4 71.19 12.30 4 -12 4 71.69 16.40 4 -12 4 62.99 5.80 4 -12 4 55.99 6.70 -5 12 -4 60.39 9.60 -5 12 -4 63.59 11.70 -5 12 -4 57.09 6.60 5 -12 4 69.79 12.60 5 -12 4 53.29 6.80 5 -12 4 67.19 17.20 -6 12 -4 37.30 10.40 -6 12 -4 33.30 8.30 -6 12 -4 25.30 5.20 6 -12 4 35.40 11.60 6 -12 4 31.30 6.10 6 -12 4 34.70 16.20 -7 12 -4 24.90 7.90 -7 12 -4 14.60 5.10 -7 12 -4 16.70 8.90 7 -12 4 35.30 12.00 7 -12 4 15.40 16.90 7 -12 4 22.80 6.00 -8 12 -4 7.10 6.80 -8 12 -4 2.40 7.90 8 -12 4 11.30 5.50 8 -12 4 18.00 19.00 8 -12 4 2.10 9.50 -9 12 -4 22.70 9.00 -9 12 -4 11.90 9.40 9 -12 4 24.10 21.30 9 -12 4 30.80 12.40 9 -12 4 17.60 6.10 -10 12 -4 91.19 13.90 -10 12 -4 87.59 15.30 10 -12 4 132.09 30.70 10 -12 4 111.59 18.30 10 -12 4 78.39 9.40 -11 12 -4 19.10 11.00 -11 12 -4 36.90 10.80 11 -12 4 34.00 13.70 11 -12 4 21.60 7.00 11 -12 4 23.60 24.80 -12 12 -4 57.89 15.10 -12 12 -4 52.89 12.60 12 -12 4 59.39 9.20 12 -12 4 62.79 16.00 14 11 -4 5.10 9.50 14 11 -4 -1.10 8.10 -14 -11 4 -0.40 7.80 -14 -11 4 -2.80 10.20 -14 -11 4 6.00 7.50 13 11 -4 112.89 15.20 13 11 -4 80.89 13.30 -13 -11 4 90.59 14.10 -13 -11 4 94.59 12.80 -13 -11 4 93.79 12.50 12 11 -4 37.10 10.20 12 11 -4 26.50 9.40 -12 -11 4 39.30 9.00 -12 -11 4 25.80 8.70 -12 -11 4 46.90 11.50 11 11 -4 30.20 9.30 11 11 -4 49.20 10.70 -11 -11 4 53.09 11.00 -11 -11 4 44.50 9.10 -11 -11 4 39.10 8.80 10 11 -4 12.60 8.70 10 11 -4 -1.90 6.60 -10 -11 4 22.00 7.50 -10 -11 4 3.20 6.20 -10 -11 4 20.20 8.70 9 11 -4 206.78 19.00 9 11 -4 146.49 14.00 9 11 -4 160.28 14.30 -9 -11 4 169.38 13.40 -9 -11 4 168.68 15.20 -9 -11 4 158.88 13.00 8 11 -4 1.70 6.20 8 11 -4 14.30 10.30 8 11 -4 13.90 7.40 -8 -11 4 12.30 7.20 -8 -11 4 13.40 6.00 -8 -11 4 6.10 5.40 7 11 -4 -1.20 9.90 7 11 -4 6.70 5.90 7 11 -4 9.10 6.70 -7 -11 4 -3.10 4.90 -7 -11 4 0.10 4.80 -7 -11 4 7.20 6.30 6 11 -4 1.60 5.20 6 11 -4 -8.70 10.20 6 11 -4 0.90 5.80 -6 -11 4 2.30 4.60 -6 -11 4 1.70 4.70 -6 -11 4 10.40 5.70 5 11 -4 0.70 10.50 5 11 -4 2.40 5.50 5 11 -4 1.60 5.30 5 11 -4 8.10 5.40 -5 -11 4 3.80 3.90 -5 -11 4 7.10 5.50 -5 -11 4 7.10 4.50 -5 -11 4 1.50 4.60 4 11 -4 7.40 5.60 4 11 -4 7.80 6.10 4 11 -4 7.00 9.70 4 11 -4 7.40 5.20 -4 -11 4 11.60 5.60 -4 -11 4 5.00 4.50 -4 -11 4 7.40 4.30 -4 -11 4 4.30 4.10 3 11 -4 2.50 5.10 3 11 -4 7.70 5.50 3 11 -4 1.30 8.70 -3 -11 4 6.00 4.20 -3 -11 4 0.70 3.90 -3 -11 4 2.10 4.10 -3 -11 4 5.60 4.40 -3 -11 4 4.60 3.80 2 11 -4 67.29 7.70 2 11 -4 63.19 10.20 2 11 -4 70.89 11.10 -2 -11 4 54.39 6.90 -2 -11 4 52.69 7.90 -2 -11 4 63.29 7.30 -2 -11 4 56.49 6.50 -2 -11 4 58.09 6.60 -1 -11 4 6.30 5.00 -1 -11 4 5.00 6.70 -1 -11 4 8.10 4.10 -1 -11 4 1.20 3.60 -1 -11 4 6.80 4.30 -1 -11 4 0.70 3.80 -1 -11 4 4.60 3.40 0 -11 4 12.80 5.70 0 -11 4 12.30 7.90 0 -11 4 16.40 4.60 0 -11 4 11.90 4.10 0 -11 4 13.40 4.80 0 -11 4 11.40 7.30 0 -11 4 16.60 4.20 0 -11 4 15.00 4.60 -1 11 -4 31.50 4.90 -1 11 -4 25.10 5.80 1 -11 4 27.00 8.20 1 -11 4 32.10 9.80 1 -11 4 36.80 5.40 1 -11 4 35.90 5.30 -2 11 -4 209.08 10.10 -2 11 -4 222.88 12.70 -2 11 -4 236.98 15.40 2 -11 4 208.18 10.30 2 -11 4 226.18 15.50 2 -11 4 210.88 9.90 2 -11 4 211.98 20.40 -3 11 -4 177.48 8.50 -3 11 -4 170.18 9.30 -3 11 -4 170.78 11.70 -3 11 -4 191.48 15.10 3 -11 4 182.68 8.80 3 -11 4 190.28 15.10 3 -11 4 186.58 20.80 3 -11 4 168.38 9.50 -4 11 -4 220.28 16.30 -4 11 -4 203.78 10.20 -4 11 -4 208.78 13.60 4 -11 4 211.08 9.20 4 -11 4 231.48 17.20 4 -11 4 224.18 10.80 4 -11 4 230.78 22.50 -5 11 -4 3.30 6.60 -5 11 -4 6.10 3.50 -5 11 -4 2.50 5.10 5 -11 4 -3.20 8.40 5 -11 4 9.30 2.90 5 -11 4 -0.20 7.00 5 -11 4 5.20 4.20 -6 11 -4 188.98 16.60 -6 11 -4 218.28 14.90 -6 11 -4 199.18 10.30 6 -11 4 209.58 18.10 6 -11 4 196.68 10.80 6 -11 4 215.28 24.00 -7 11 -4 246.18 11.90 -7 11 -4 251.97 19.40 -7 11 -4 269.87 17.00 7 -11 4 250.77 12.40 7 -11 4 263.57 27.70 7 -11 4 256.27 20.20 -8 11 -4 5.00 6.50 -8 11 -4 13.40 4.80 -8 11 -4 25.20 9.40 8 -11 4 7.30 8.60 8 -11 4 6.60 5.00 8 -11 4 7.20 14.70 -9 11 -4 10.20 7.70 -9 11 -4 14.30 9.00 9 -11 4 21.10 6.30 9 -11 4 8.70 18.60 9 -11 4 19.00 10.50 -10 11 -4 84.49 14.70 -10 11 -4 78.69 12.60 10 -11 4 106.19 17.60 10 -11 4 72.99 8.90 10 -11 4 114.39 28.70 -11 11 -4 164.78 17.80 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91.09 14.30 7 10 -4 59.99 8.60 7 10 -4 77.59 9.80 -7 -10 4 75.99 9.40 -7 -10 4 64.19 8.40 -7 -10 4 73.89 8.60 6 10 -4 269.67 20.30 6 10 -4 286.57 14.50 6 10 -4 293.77 15.00 -6 -10 4 294.47 14.80 -6 -10 4 279.87 11.70 -6 -10 4 291.77 14.10 -6 -10 4 281.57 13.80 5 10 -4 147.19 16.10 5 10 -4 137.59 11.80 5 10 -4 144.99 11.40 5 10 -4 138.79 10.50 -5 -10 4 145.89 11.00 -5 -10 4 141.99 10.20 -5 -10 4 153.18 10.20 -5 -10 4 143.19 9.00 4 10 -4 42.60 7.60 4 10 -4 49.90 11.70 4 10 -4 52.09 7.50 -4 -10 4 42.00 6.10 -4 -10 4 37.30 6.60 -4 -10 4 47.60 6.50 -4 -10 4 39.60 6.00 3 10 -4 54.89 8.80 3 10 -4 64.79 11.30 3 10 -4 70.49 7.70 -3 -10 4 58.29 6.50 -3 -10 4 63.59 7.10 -3 -10 4 58.79 7.00 -3 -10 4 66.29 7.80 -3 -10 4 62.39 7.10 2 10 -4 33.60 8.90 2 10 -4 24.30 7.00 -2 -10 4 30.80 5.40 -2 -10 4 33.50 5.30 -2 -10 4 32.00 6.20 -2 -10 4 31.20 5.30 -2 -10 4 29.50 4.90 -1 -10 4 30.50 7.80 -1 -10 4 26.00 4.70 -1 -10 4 30.60 5.00 -1 -10 4 31.00 5.00 -1 -10 4 34.20 8.30 -1 -10 4 23.90 5.90 -1 -10 4 22.70 4.60 -1 -10 4 37.80 5.70 0 -10 4 92.99 6.90 0 -10 4 92.69 9.30 0 -10 4 84.69 10.40 0 -10 4 85.19 6.70 0 -10 4 92.29 13.00 0 -10 4 84.39 6.90 0 -10 4 76.19 7.80 0 -10 4 87.59 7.10 -1 10 -4 -1.80 2.60 -1 10 -4 0.00 3.30 1 -10 4 0.20 5.50 1 -10 4 1.60 2.80 1 -10 4 3.50 3.50 1 -10 4 -0.60 2.80 1 -10 4 -6.00 4.80 -2 10 -4 -0.60 4.70 -2 10 -4 1.10 2.70 -2 10 -4 -0.90 3.60 2 -10 4 -2.90 3.30 2 -10 4 4.10 6.40 2 -10 4 4.60 5.70 2 -10 4 2.50 2.60 -3 10 -4 205.48 14.50 -3 10 -4 179.38 8.90 -3 10 -4 192.08 11.70 -3 10 -4 198.38 8.10 3 -10 4 169.38 13.90 3 -10 4 198.28 9.70 3 -10 4 194.88 18.60 3 -10 4 182.28 8.50 -4 10 -4 63.69 10.20 -4 10 -4 65.19 8.30 -4 10 -4 59.09 5.80 4 -10 4 66.39 5.60 4 -10 4 78.89 11.20 4 -10 4 64.49 6.50 4 -10 4 57.49 12.30 -5 10 -4 -2.70 5.40 -5 10 -4 0.90 4.60 -5 10 -4 -1.70 2.80 5 -10 4 -5.20 6.30 5 -10 4 1.80 2.40 5 -10 4 0.90 3.60 5 -10 4 4.40 6.50 -6 10 -4 57.29 8.80 -6 10 -4 49.10 9.90 -6 10 -4 49.99 5.70 6 -10 4 54.99 4.60 6 -10 4 60.39 13.70 6 -10 4 77.29 12.20 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13 -5 10.10 13.20 7 13 -5 24.40 8.80 -7 -13 5 27.90 7.30 -7 -13 5 26.10 7.10 -7 -13 5 18.50 6.70 6 13 -5 -4.00 12.40 6 13 -5 -1.80 5.70 6 13 -5 -6.70 6.50 -6 -13 5 2.30 5.50 -6 -13 5 9.30 5.90 -6 -13 5 -4.00 4.60 5 13 -5 2.90 7.00 5 13 -5 5.90 6.50 5 13 -5 -2.10 12.10 -5 -13 5 14.20 5.80 -5 -13 5 9.50 5.80 -5 -13 5 13.30 5.80 4 13 -5 74.39 9.90 4 13 -5 74.19 15.30 4 13 -5 55.69 11.00 4 13 -5 70.89 9.60 -4 -13 5 85.69 8.90 -4 -13 5 71.29 8.20 -4 -13 5 78.39 8.90 3 13 -5 51.49 8.60 3 13 -5 64.39 14.10 3 13 -5 46.80 10.60 -3 -13 5 52.59 7.50 -3 -13 5 38.00 6.80 -3 -13 5 43.80 7.20 2 13 -5 71.09 12.60 2 13 -5 94.99 14.60 2 13 -5 74.89 9.30 -2 -13 5 68.79 7.80 -2 -13 5 69.59 8.30 -2 -13 5 67.59 8.00 -2 -13 5 72.29 8.50 1 13 -5 -0.10 6.30 1 13 -5 6.40 7.90 1 13 -5 9.60 6.00 -1 -13 5 0.50 4.30 -1 -13 5 -1.60 3.80 -1 -13 5 1.60 3.90 0 13 -5 184.18 12.70 0 13 -5 197.78 15.30 0 -13 5 185.98 10.60 0 -13 5 191.58 10.90 0 -13 5 177.58 10.90 0 -13 5 185.98 17.10 -1 13 -5 79.89 7.80 -1 13 -5 76.69 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39.40 7.50 -8 -11 5 27.80 7.20 -8 -11 5 40.50 8.40 7 11 -5 31.40 8.30 7 11 -5 24.60 7.00 7 11 -5 24.30 12.20 -7 -11 5 27.90 6.50 -7 -11 5 30.30 7.30 -7 -11 5 28.70 6.80 6 11 -5 63.59 8.80 6 11 -5 94.09 10.30 6 11 -5 93.49 15.70 -6 -11 5 85.29 9.10 -6 -11 5 69.59 8.60 -6 -11 5 76.29 8.60 5 11 -5 5.30 10.90 5 11 -5 11.30 6.30 5 11 -5 -2.40 5.50 -5 -11 5 9.80 5.50 -5 -11 5 7.10 4.70 -5 -11 5 2.60 4.60 4 11 -5 -5.20 10.00 4 11 -5 -4.90 5.00 4 11 -5 -3.90 5.00 -4 -11 5 0.50 3.80 -4 -11 5 -1.10 3.60 -4 -11 5 5.10 4.50 -4 -11 5 1.50 4.20 3 11 -5 38.00 8.90 3 11 -5 28.60 6.60 3 11 -5 24.60 10.30 -3 -11 5 21.30 5.20 -3 -11 5 33.20 5.90 -3 -11 5 30.30 5.50 -3 -11 5 24.00 5.20 2 11 -5 59.79 11.30 2 11 -5 57.59 10.40 -2 -11 5 54.89 6.50 -2 -11 5 66.49 7.10 -2 -11 5 55.59 7.00 -2 -11 5 57.99 7.00 1 11 -5 270.17 19.20 -1 -11 5 262.27 12.30 -1 -11 5 257.97 11.70 -1 -11 5 262.07 12.00 -1 -11 5 256.17 11.60 -1 -11 5 248.28 11.30 0 11 -5 -5.60 4.10 0 11 -5 -0.50 3.70 0 -11 5 0.90 3.50 0 -11 5 0.80 3.00 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9.20 5 11 -6 58.89 10.40 5 11 -6 76.79 15.60 -5 -11 6 61.69 8.30 -5 -11 6 71.59 8.00 -5 -11 6 71.79 8.40 -5 -11 6 57.19 7.20 4 11 -6 25.60 5.60 4 11 -6 26.10 7.80 4 11 -6 42.80 12.50 4 11 -6 28.40 7.00 -4 -11 6 29.30 5.40 -4 -11 6 30.50 6.10 -4 -11 6 30.40 5.70 -4 -11 6 24.80 5.70 3 11 -6 9.10 6.00 3 11 -6 11.80 6.90 3 11 -6 3.10 9.70 3 11 -6 6.30 4.70 -3 -11 6 7.90 4.40 -3 -11 6 5.80 3.90 -3 -11 6 8.60 4.40 -3 -11 6 10.00 4.20 2 11 -6 20.40 7.80 2 11 -6 18.80 9.50 2 11 -6 18.30 5.90 -2 -11 6 16.50 5.30 -2 -11 6 14.20 4.60 -2 -11 6 17.10 4.50 -2 -11 6 22.90 5.10 -2 -11 6 15.20 4.40 1 11 -6 302.17 15.80 1 11 -6 306.27 21.40 -1 -11 6 290.67 12.80 -1 -11 6 313.97 12.20 -1 -11 6 299.17 12.70 -1 -11 6 278.97 13.10 0 11 -6 107.39 14.60 0 11 -6 99.19 8.60 0 11 -6 104.99 10.90 0 -11 6 103.99 8.70 0 -11 6 100.79 7.50 0 -11 6 103.59 7.80 0 -11 6 99.99 12.80 0 -11 6 99.99 7.90 -1 11 -6 415.16 16.40 -1 11 -6 371.96 13.50 -1 11 -6 418.86 20.20 1 -11 6 400.26 14.90 1 -11 6 408.76 13.80 1 -11 6 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20.10 8.40 -9 -14 7 28.30 8.50 8 14 -7 43.60 11.10 8 14 -7 35.90 9.90 -8 -14 7 37.40 9.10 -8 -14 7 29.40 8.40 7 14 -7 10.90 15.40 7 14 -7 26.30 9.10 7 14 -7 19.70 9.50 -7 -14 7 13.80 6.80 -7 -14 7 34.30 8.50 6 14 -7 18.20 9.00 6 14 -7 4.80 7.30 6 14 -7 17.40 15.80 -6 -14 7 10.00 6.40 -6 -14 7 22.90 7.30 5 14 -7 41.10 9.60 5 14 -7 18.90 15.80 5 14 -7 29.80 9.00 -5 -14 7 32.80 7.60 -5 -14 7 25.00 7.00 4 14 -7 110.89 19.60 4 14 -7 94.09 11.50 -4 -14 7 106.19 11.00 -4 -14 7 96.69 11.50 -4 -14 7 98.19 9.60 3 14 -7 122.39 12.40 3 14 -7 136.79 18.50 3 14 -7 106.89 18.80 -3 -14 7 143.99 10.90 -3 -14 7 121.99 10.80 -3 -14 7 139.19 11.60 -3 -14 7 125.69 11.20 2 14 -7 -0.30 6.20 2 14 -7 5.90 11.80 2 14 -7 6.70 8.50 2 14 -7 5.70 7.20 2 14 -7 4.80 5.10 -2 -14 7 4.50 4.90 -2 -14 7 1.00 4.40 -2 -14 7 4.70 4.90 1 14 -7 28.40 8.60 1 14 -7 21.50 10.50 1 14 -7 15.60 6.00 1 14 -7 26.20 11.80 -1 -14 7 14.80 5.50 -1 -14 7 3.50 5.50 -1 -14 7 20.30 5.80 0 14 -7 1.70 4.10 0 14 -7 2.90 4.80 0 14 -7 2.80 8.70 0 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10 -7 75.39 16.30 8 10 -7 65.49 10.00 -8 -10 7 58.69 8.30 -8 -10 7 67.69 8.60 -8 -10 7 74.09 8.60 7 10 -7 10.80 12.60 7 10 -7 6.30 6.20 -7 -10 7 13.40 5.40 -7 -10 7 12.00 5.20 -7 -10 7 7.20 4.80 -7 -10 7 9.60 5.10 6 10 -7 47.30 14.10 6 10 -7 29.70 10.50 6 10 -7 31.20 7.70 -6 -10 7 44.30 6.80 -6 -10 7 46.10 7.20 -6 -10 7 49.30 7.10 -6 -10 7 46.90 6.50 5 10 -7 25.00 8.60 5 10 -7 40.80 13.40 5 10 -7 23.20 6.70 -5 -10 7 22.00 5.60 -5 -10 7 23.00 5.40 -5 -10 7 27.30 5.80 -5 -10 7 34.70 5.60 4 10 -7 40.30 5.90 4 10 -7 33.60 12.00 4 10 -7 38.80 6.90 4 10 -7 35.90 9.20 -4 -10 7 32.60 6.00 -4 -10 7 40.70 5.30 -4 -10 7 41.30 6.30 -4 -10 7 35.30 5.70 3 10 -7 10.10 6.60 3 10 -7 32.90 11.00 3 10 -7 25.30 5.70 -3 -10 7 25.60 4.50 -3 -10 7 27.00 5.40 -3 -10 7 27.60 5.10 -3 -10 7 19.30 5.10 2 10 -7 88.59 12.90 2 10 -7 79.49 8.90 2 10 -7 68.69 12.30 -2 -10 7 77.19 7.40 -2 -10 7 68.99 7.30 -2 -10 7 82.99 8.20 -2 -10 7 78.29 6.90 -2 -10 7 81.09 7.10 1 10 -7 505.25 20.10 1 10 -7 488.15 26.50 1 10 -7 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154.08 19.50 5 11 -9 171.68 12.90 -5 -11 9 157.88 11.70 -5 -11 9 164.28 10.90 -5 -11 9 183.38 12.20 4 11 -9 4.90 12.10 4 11 -9 6.50 8.40 4 11 -9 1.00 5.90 -4 -11 9 14.10 5.20 -4 -11 9 6.70 4.80 -4 -11 9 11.50 4.60 3 11 -9 81.49 15.40 3 11 -9 57.19 7.90 3 11 -9 70.19 13.10 -3 -11 9 57.59 6.40 -3 -11 9 66.19 8.10 -3 -11 9 77.99 8.70 -3 -11 9 73.99 8.20 2 11 -9 5.50 5.10 2 11 -9 5.20 10.00 2 11 -9 4.50 3.40 2 11 -9 6.10 7.70 -2 -11 9 6.80 5.30 -2 -11 9 2.40 3.60 -2 -11 9 2.40 4.00 -2 -11 9 2.10 4.00 1 11 -9 4.10 5.30 1 11 -9 -5.80 7.80 1 11 -9 1.00 7.40 1 11 -9 0.10 3.30 -1 -11 9 1.10 3.10 -1 -11 9 1.30 3.80 -1 -11 9 -1.70 4.60 -1 -11 9 1.20 3.30 0 11 -9 10.70 6.40 0 11 -9 8.40 8.50 0 11 -9 5.80 4.00 0 -11 9 10.80 5.20 0 -11 9 5.80 3.80 0 -11 9 11.10 4.40 -1 11 -9 9.50 6.50 -1 11 -9 4.20 8.00 -1 11 -9 4.50 4.00 1 -11 9 7.10 4.10 1 -11 9 9.50 3.90 1 -11 9 10.60 5.00 1 -11 9 4.20 8.10 -2 11 -9 77.79 15.00 -2 11 -9 86.39 8.70 -2 11 -9 86.19 12.10 2 -11 9 74.59 6.40 2 -11 9 78.29 8.20 2 -11 9 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24.30 12.80 11 -11 9 11.60 7.70 -12 11 -9 78.49 17.20 -12 11 -9 97.89 14.80 -12 11 -9 88.09 19.60 12 -11 9 105.29 12.70 12 -11 9 114.59 20.40 14 10 -9 2.90 7.90 14 10 -9 39.10 11.50 -14 -10 9 -5.80 7.30 -14 -10 9 15.20 8.20 13 10 -9 7.20 9.80 13 10 -9 6.50 7.90 -13 -10 9 3.00 7.40 -13 -10 9 6.50 7.50 12 10 -9 58.69 11.30 12 10 -9 82.69 13.30 12 10 -9 104.39 18.90 -12 -10 9 29.60 8.50 -12 -10 9 69.39 11.20 11 10 -9 25.60 8.80 11 10 -9 40.60 15.50 11 10 -9 31.60 10.90 -11 -10 9 32.20 8.10 -11 -10 9 19.20 7.90 10 10 -9 41.30 10.50 10 10 -9 58.89 10.10 10 10 -9 51.19 16.20 -10 -10 9 38.50 8.10 -10 -10 9 59.39 9.50 9 10 -9 43.10 10.00 9 10 -9 43.00 16.00 -9 -10 9 48.00 8.70 -9 -10 9 35.90 7.60 8 10 -9 19.40 7.40 8 10 -9 23.20 14.30 -8 -10 9 16.90 6.10 -8 -10 9 14.60 6.10 -8 -10 9 26.50 6.70 7 10 -9 82.59 10.20 7 10 -9 90.39 18.20 7 10 -9 53.99 21.40 -7 -10 9 74.99 9.30 -7 -10 9 81.89 8.80 -7 -10 9 80.59 9.20 6 10 -9 -14.10 10.40 6 10 -9 -4.80 5.70 6 10 -9 11.50 12.80 -6 -10 9 0.30 4.00 -6 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15.80 -7 8 -9 265.37 19.10 -7 8 -9 262.37 23.60 7 -8 9 264.57 13.40 7 -8 9 238.98 18.70 7 -8 9 254.57 11.90 -8 8 -9 25.60 7.40 -8 8 -9 13.50 8.40 -8 8 -9 24.50 10.40 8 -8 9 26.70 5.30 8 -8 9 24.60 6.40 8 -8 9 32.80 10.30 -9 8 -9 50.99 12.30 -9 8 -9 27.50 10.70 -9 8 -9 37.80 8.80 9 -8 9 31.10 10.70 9 -8 9 38.10 7.50 9 -8 9 43.30 6.30 -10 8 -9 268.97 26.00 -10 8 -9 274.07 18.70 -10 8 -9 295.57 22.50 10 -8 9 281.77 16.10 10 -8 9 245.28 21.80 -11 8 -9 122.29 18.00 -11 8 -9 97.19 18.30 -11 8 -9 112.99 14.40 11 -8 9 105.89 12.10 11 -8 9 129.39 19.50 -12 8 -9 -1.90 9.40 -12 8 -9 1.40 8.70 -12 8 -9 -8.30 6.80 12 -8 9 -1.90 9.70 12 -8 9 12.50 7.30 -13 8 -9 -9.10 8.00 -13 8 -9 2.10 9.20 -13 8 -9 -7.80 9.20 13 -8 9 -1.30 6.70 13 -8 9 -10.30 9.50 15 7 -9 43.00 10.80 15 7 -9 54.19 12.30 -15 -7 9 39.70 10.40 -15 -7 9 26.90 8.90 14 7 -9 99.29 13.00 14 7 -9 107.69 14.50 -14 -7 9 94.69 12.40 -14 -7 9 77.89 11.50 13 7 -9 12.60 7.60 13 7 -9 38.60 15.50 13 7 -9 0.90 8.20 -13 -7 9 5.00 6.60 -13 -7 9 13.80 7.20 12 7 -9 10.30 7.80 12 7 -9 -6.90 5.50 12 7 -9 6.00 11.20 -12 -7 9 -1.60 5.80 -12 -7 9 -1.90 5.40 11 7 -9 6.20 7.30 11 7 -9 -6.50 5.20 11 7 -9 22.10 12.00 -11 -7 9 -5.70 5.00 -11 -7 9 -0.50 5.20 10 7 -9 9.40 11.80 10 7 -9 -0.30 6.50 -10 -7 9 10.40 5.60 -10 -7 9 8.90 5.60 -10 -7 9 12.50 5.90 9 7 -9 54.99 11.20 9 7 -9 47.80 14.10 9 7 -9 48.10 8.80 -9 -7 9 49.10 7.40 -9 -7 9 46.70 7.40 -9 -7 9 52.39 7.70 -9 -7 9 37.90 7.00 8 7 -9 49.70 12.20 8 7 -9 52.99 14.60 8 7 -9 41.80 7.50 -8 -7 9 50.29 6.40 -8 -7 9 45.90 7.40 -8 -7 9 47.10 7.20 -8 -7 9 44.50 6.80 7 7 -9 32.30 6.70 7 7 -9 36.90 13.50 7 7 -9 28.20 13.00 -7 -7 9 36.90 6.70 -7 -7 9 35.60 6.10 -7 -7 9 40.00 6.50 -7 -7 9 35.90 5.10 6 7 -9 319.97 27.30 6 7 -9 318.47 14.80 6 7 -9 297.67 23.80 -6 -7 9 316.87 14.00 -6 -7 9 319.47 13.30 -6 -7 9 316.87 14.10 -6 -7 9 318.77 10.50 5 7 -9 280.47 22.10 5 7 -9 225.68 12.50 5 7 -9 262.17 23.30 -5 -7 9 256.47 12.20 -5 -7 9 245.18 11.10 -5 -7 9 257.67 12.30 -5 -7 9 249.08 8.10 4 7 -9 24.90 4.30 4 7 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12.20 -4 7 -9 77.19 7.90 -4 7 -9 72.29 10.60 4 -7 9 67.99 7.20 4 -7 9 64.69 6.80 4 -7 9 72.29 11.00 -5 7 -9 62.79 12.80 -5 7 -9 69.79 8.00 -5 7 -9 53.69 9.80 5 -7 9 51.49 6.60 5 -7 9 62.19 10.70 5 -7 9 61.89 6.80 -6 7 -9 3.50 4.50 -6 7 -9 7.90 6.20 -6 7 -9 -2.70 5.60 6 -7 9 2.60 3.40 6 -7 9 3.00 4.00 6 -7 9 2.40 6.10 -7 7 -9 0.50 6.50 -7 7 -9 0.60 4.60 -7 7 -9 1.20 6.30 7 -7 9 -4.80 5.60 7 -7 9 2.40 3.30 7 -7 9 -1.50 4.30 -8 7 -9 251.17 22.70 -8 7 -9 220.88 15.20 -8 7 -9 234.88 18.60 8 -7 9 245.18 13.30 8 -7 9 241.88 19.00 8 -7 9 234.48 11.70 -9 7 -9 185.48 21.10 -9 7 -9 185.48 14.90 -9 7 -9 183.08 17.70 9 -7 9 186.08 12.50 9 -7 9 187.98 18.10 9 -7 9 180.88 10.70 -10 7 -9 197.78 22.10 -10 7 -9 212.68 19.50 -10 7 -9 199.88 16.40 10 -7 9 217.28 13.80 10 -7 9 205.08 11.40 10 -7 9 172.08 18.50 -11 7 -9 -0.80 8.80 -11 7 -9 -2.90 6.80 -11 7 -9 0.60 7.80 11 -7 9 -4.90 8.70 11 -7 9 3.00 6.20 -12 7 -9 84.29 16.00 -12 7 -9 78.39 13.10 -12 7 -9 78.69 17.00 12 -7 9 105.89 18.70 12 -7 9 101.19 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38.30 11.60 -11 5 -9 37.70 11.10 -11 5 -9 30.10 9.30 11 -5 9 38.20 7.90 11 -5 9 41.20 12.10 11 -5 9 41.20 6.90 -12 5 -9 1.70 9.20 -12 5 -9 2.30 8.00 -12 5 -9 -4.10 7.20 12 -5 9 13.00 6.60 12 -5 9 6.60 6.20 12 -5 9 4.20 9.40 -13 5 -9 5.30 8.90 -13 5 -9 9.70 9.60 -13 5 -9 10.80 11.80 13 -5 9 19.80 7.70 13 -5 9 19.00 11.50 -14 5 -9 39.70 13.20 -14 5 -9 34.50 14.80 14 -5 9 44.20 9.80 14 -5 9 103.69 16.20 16 4 -9 33.50 15.90 16 4 -9 -0.70 8.00 -16 -4 9 4.80 6.60 -16 -4 9 2.40 7.50 15 4 -9 93.49 11.10 15 4 -9 130.09 14.50 15 4 -9 150.78 24.30 -15 -4 9 115.79 12.40 -15 -4 9 109.09 13.80 14 4 -9 0.40 5.80 14 4 -9 21.90 14.10 14 4 -9 -4.20 7.30 -14 -4 9 1.10 6.10 -14 -4 9 -0.20 5.50 13 4 -9 33.40 13.40 13 4 -9 -0.40 5.70 13 4 -9 9.30 7.50 -13 -4 9 -13.00 7.20 -13 -4 9 -0.90 6.00 -13 -4 9 2.30 5.30 12 4 -9 1.20 6.40 12 4 -9 0.10 10.10 12 4 -9 2.90 5.30 -12 -4 9 -1.20 5.60 -12 -4 9 -11.80 6.30 -12 -4 9 -4.20 4.50 11 4 -9 39.60 8.30 11 4 -9 52.19 13.40 11 4 -9 46.60 9.50 -11 -4 9 41.10 7.30 -11 -4 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4 -9 110.79 13.00 -3 -4 9 97.49 6.90 -3 -4 9 97.59 5.80 -3 -4 9 98.39 6.90 -3 -4 9 89.69 6.60 2 4 -9 93.79 11.70 2 4 -9 100.29 14.00 2 4 -9 80.29 7.40 -2 -4 9 88.79 6.40 -2 -4 9 73.79 6.10 -2 -4 9 78.09 6.40 -2 -4 9 75.49 4.70 1 4 -9 41.40 8.40 1 4 -9 42.70 9.10 1 4 -9 47.40 6.30 -1 -4 9 43.00 4.80 -1 -4 9 39.80 4.80 -1 -4 9 37.70 4.70 0 4 -9 400.46 18.40 0 4 -9 416.06 16.10 0 4 -9 419.46 22.20 0 -4 9 439.86 13.50 0 -4 9 390.36 13.60 0 -4 9 406.46 13.00 -1 4 -9 827.42 25.80 -1 4 -9 788.82 19.50 -1 4 -9 824.82 32.40 1 -4 9 812.92 20.80 1 -4 9 825.52 22.30 1 -4 9 808.62 21.40 1 -4 9 833.92 26.70 -2 4 -9 1421.66 46.20 -2 4 -9 1389.96 32.70 -2 4 -9 1403.96 38.70 2 -4 9 1467.55 34.60 2 -4 9 1393.36 33.40 2 -4 9 1427.26 32.10 2 -4 9 1396.46 38.90 -3 4 -9 92.29 12.60 -3 4 -9 84.59 6.50 -3 4 -9 89.99 10.20 3 -4 9 86.19 9.50 3 -4 9 106.09 7.00 3 -4 9 100.59 7.20 3 -4 9 78.49 5.00 -4 4 -9 71.29 7.00 -4 4 -9 67.39 11.70 -4 4 -9 69.89 9.60 4 -4 9 69.19 9.70 4 -4 9 60.09 6.30 4 -4 9 69.49 7.10 -5 4 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80.49 11.80 10 11 -10 -15.10 8.90 10 11 -10 -6.70 6.30 10 11 -10 26.10 15.50 -10 -11 10 -1.10 6.40 -10 -11 10 -6.00 5.60 9 11 -10 71.19 12.10 9 11 -10 75.09 18.80 -9 -11 10 54.89 9.30 -9 -11 10 44.80 9.10 -9 -11 10 52.49 8.70 8 11 -10 4.00 7.30 8 11 -10 5.80 14.80 -8 -11 10 -4.20 5.00 -8 -11 10 -0.20 4.90 -8 -11 10 0.30 5.60 7 11 -10 5.90 7.40 7 11 -10 24.70 16.00 -7 -11 10 2.30 5.10 -7 -11 10 0.60 5.10 -7 -11 10 -2.20 4.80 6 11 -10 -6.30 13.70 6 11 -10 -14.50 11.50 6 11 -10 1.90 6.50 -6 -11 10 3.80 4.70 -6 -11 10 4.50 5.00 -6 -11 10 5.70 5.10 5 11 -10 -4.60 10.30 5 11 -10 3.70 6.50 5 11 -10 7.70 14.40 -5 -11 10 2.60 5.10 -5 -11 10 12.40 5.70 -5 -11 10 15.60 5.20 4 11 -10 134.19 19.60 4 11 -10 127.49 12.00 4 11 -10 110.69 16.90 -4 -11 10 127.69 9.40 -4 -11 10 123.59 10.40 -4 -11 10 111.99 10.80 3 11 -10 -11.00 9.90 3 11 -10 -0.30 8.20 3 11 -10 -2.20 4.60 -3 -11 10 2.80 3.80 -3 -11 10 -3.00 4.80 -3 -11 10 -1.20 4.00 -3 -11 10 6.20 4.50 2 11 -10 2.90 10.10 2 11 -10 9.50 5.70 2 11 -10 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18.70 11 10 -10 26.80 8.90 -11 -10 10 33.30 8.30 -11 -10 10 28.60 8.40 10 10 -10 155.68 22.50 10 10 -10 109.99 13.60 -10 -10 10 114.39 12.20 -10 -10 10 106.89 11.10 9 10 -10 8.80 8.10 9 10 -10 7.70 14.00 -9 -10 10 1.30 5.50 -9 -10 10 7.30 6.20 -9 -10 10 6.10 5.80 8 10 -10 10.40 7.30 8 10 -10 36.00 16.20 -8 -10 10 11.00 5.70 -8 -10 10 18.20 6.10 -8 -10 10 11.70 6.20 7 10 -10 20.80 7.60 7 10 -10 18.30 15.10 7 10 -10 -7.40 14.70 -7 -10 10 16.10 5.50 -7 -10 10 8.80 5.60 -7 -10 10 22.20 6.30 6 10 -10 95.19 10.40 6 10 -10 131.49 20.30 6 10 -10 88.59 17.80 -6 -10 10 124.69 9.90 -6 -10 10 127.39 10.80 -6 -10 10 125.39 10.30 5 10 -10 10.10 11.40 5 10 -10 25.40 13.90 5 10 -10 18.30 6.80 -5 -10 10 20.40 5.70 -5 -10 10 19.60 5.10 -5 -10 10 19.50 5.50 4 10 -10 156.88 19.80 4 10 -10 174.18 19.90 -4 -10 10 152.18 10.70 -4 -10 10 166.18 9.70 -4 -10 10 162.88 11.30 3 10 -10 127.19 9.80 3 10 -10 115.99 17.00 3 10 -10 135.69 17.80 -3 -10 10 127.49 9.90 -3 -10 10 138.09 9.50 -3 -10 10 99.59 9.40 -3 -10 10 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13.90 11.20 6 3 -10 11.50 10.00 6 3 -10 12.30 4.70 -6 -3 10 14.60 4.10 -6 -3 10 17.80 4.60 -6 -3 10 17.10 4.20 5 3 -10 57.59 5.90 5 3 -10 55.09 12.00 5 3 -10 57.39 14.20 5 3 -10 58.49 6.40 -5 -3 10 48.60 6.30 -5 -3 10 60.19 6.00 -5 -3 10 40.80 5.30 4 3 -10 9.70 9.10 4 3 -10 16.00 11.50 4 3 -10 -1.10 4.90 -4 -3 10 -1.90 2.50 -4 -3 10 1.50 3.10 -4 -3 10 3.80 2.90 -4 -3 10 3.20 3.50 3 3 -10 59.19 11.30 3 3 -10 73.69 8.80 3 3 -10 68.69 14.20 -3 -3 10 64.09 5.10 -3 -3 10 61.09 6.40 -3 -3 10 62.89 6.00 -3 -3 10 56.49 5.90 2 3 -10 488.05 27.40 2 3 -10 479.85 18.30 2 3 -10 469.35 21.90 -2 -3 10 464.35 15.20 -2 -3 10 469.05 13.00 -2 -3 10 474.15 14.80 -2 -3 10 447.96 15.10 1 3 -10 21.60 8.70 1 3 -10 31.50 6.70 1 3 -10 20.00 7.70 -1 -3 10 24.10 4.30 -1 -3 10 27.40 4.40 -1 -3 10 26.70 4.30 0 3 -10 -6.20 5.10 0 3 -10 2.60 4.90 0 3 -10 0.80 6.30 0 -3 10 -3.50 2.80 0 -3 10 -3.20 2.20 0 -3 10 -1.60 2.60 -1 3 -10 523.95 26.30 -1 3 -10 504.65 13.90 -1 3 -10 506.25 20.00 1 -3 10 528.95 16.70 1 -3 10 512.35 15.50 1 -3 10 495.85 15.20 -2 3 -10 394.96 17.90 -2 3 -10 389.36 12.80 -2 3 -10 419.36 23.50 2 -3 10 391.36 14.30 2 -3 10 395.26 13.30 2 -3 10 385.26 12.50 2 -3 10 376.26 17.30 -3 3 -10 106.39 7.50 -3 3 -10 93.09 13.20 -3 3 -10 109.09 11.00 3 -3 10 96.09 5.90 3 -3 10 104.99 10.30 3 -3 10 96.99 7.70 3 -3 10 96.09 7.00 -4 3 -10 6.50 5.60 -4 3 -10 4.40 3.80 -4 3 -10 4.20 6.10 4 -3 10 5.90 3.60 4 -3 10 4.30 5.20 4 -3 10 4.60 2.40 4 -3 10 4.10 3.50 -5 3 -10 289.37 13.40 -5 3 -10 286.87 17.10 -5 3 -10 296.97 21.10 5 -3 10 288.57 12.60 5 -3 10 297.27 12.90 5 -3 10 279.07 9.70 5 -3 10 291.97 16.10 -6 3 -10 260.87 20.50 -6 3 -10 228.38 13.10 -6 3 -10 255.77 17.10 6 -3 10 240.88 15.20 6 -3 10 232.08 12.10 6 -3 10 258.37 12.40 -7 3 -10 2.00 6.20 -7 3 -10 0.70 4.70 -7 3 -10 3.80 6.80 7 -3 10 6.70 4.50 7 -3 10 1.10 5.60 7 -3 10 -0.20 4.00 -8 3 -10 146.89 13.60 -8 3 -10 125.09 15.90 -8 3 -10 117.19 16.00 8 -3 10 133.19 13.10 8 -3 10 130.89 10.00 8 -3 10 122.19 10.60 -9 3 -10 8.00 7.70 -9 3 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6 -14 114.09 20.40 -13 -6 14 74.39 11.70 -13 -6 14 88.09 12.50 12 6 -14 143.59 22.90 12 6 -14 89.59 13.50 -12 -6 14 104.39 11.90 -12 -6 14 103.99 12.40 -12 -6 14 104.79 12.20 11 6 -14 76.59 18.20 11 6 -14 49.90 10.80 -11 -6 14 47.30 8.80 -11 -6 14 40.00 8.40 -11 -6 14 43.90 9.10 10 6 -14 36.90 11.90 10 6 -14 8.50 13.30 10 6 -14 -0.50 7.40 -10 -6 14 -1.10 5.40 -10 -6 14 8.40 5.80 -10 -6 14 4.60 6.20 9 6 -14 20.40 6.90 9 6 -14 41.30 14.00 9 6 -14 27.80 14.60 -9 -6 14 20.60 6.70 -9 -6 14 20.90 6.80 -9 -6 14 21.10 6.40 8 6 -14 31.70 15.10 8 6 -14 36.30 14.50 8 6 -14 22.00 7.10 -8 -6 14 23.40 6.60 -8 -6 14 24.50 6.60 -8 -6 14 28.50 6.40 7 6 -14 3.80 5.50 7 6 -14 -12.30 11.10 7 6 -14 -8.40 14.60 -7 -6 14 -2.60 3.90 -7 -6 14 -1.80 4.60 -7 -6 14 -1.80 4.30 6 6 -14 -0.40 11.80 6 6 -14 19.20 6.20 6 6 -14 0.10 16.10 -6 -6 14 14.90 5.30 -6 -6 14 4.10 4.00 -6 -6 14 2.90 4.70 5 6 -14 2.70 15.50 5 6 -14 -5.50 10.70 -5 -6 14 -0.60 3.50 -5 -6 14 -1.90 3.70 -5 -6 14 1.60 4.50 4 6 -14 -5.80 7.80 4 6 -14 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33.50 8.50 -5 2 -21 9.00 21.80 9 1 -21 39.90 12.40 -9 -1 21 5.80 8.60 -9 -1 21 5.30 8.00 8 1 -21 61.49 18.00 8 1 -21 22.80 11.60 -8 -1 21 4.00 6.40 -8 -1 21 6.30 7.70 7 1 -21 44.20 18.10 7 1 -21 26.70 12.70 -7 -1 21 9.80 6.60 -7 -1 21 10.80 7.90 6 1 -21 83.09 20.90 6 1 -21 82.29 17.00 -6 -1 21 71.89 12.00 -6 -1 21 64.39 9.70 5 1 -21 55.29 15.50 5 1 -21 63.89 19.70 -5 -1 21 28.40 8.40 -5 -1 21 28.10 7.80 4 1 -21 96.99 23.60 4 1 -21 130.19 20.90 -4 -1 21 109.19 12.10 -4 -1 21 103.59 12.80 3 1 -21 42.80 19.90 3 1 -21 33.80 14.70 3 1 -21 54.39 11.40 -3 -1 21 36.20 8.60 -3 -1 21 15.10 7.30 2 1 -21 -6.60 12.10 2 1 -21 21.90 18.30 2 1 -21 25.60 11.10 -2 -1 21 -0.90 6.40 -2 -1 21 5.00 6.50 1 1 -21 13.60 14.10 1 1 -21 19.20 18.90 1 1 -21 19.90 12.40 -1 -1 21 9.90 6.30 -1 -1 21 11.70 6.90 0 1 -21 45.00 14.70 0 1 -21 4.80 18.10 0 -1 21 15.60 6.70 0 -1 21 13.80 7.40 -1 1 -21 140.19 28.80 -1 1 -21 181.38 23.60 1 -1 21 219.78 16.40 1 -1 21 190.38 14.40 -2 1 -21 -8.80 17.50 -2 1 -21 10.30 14.70 2 -1 21 7.70 5.90 2 -1 21 0.10 6.90 -3 1 -21 3.20 16.10 -3 1 -21 -0.30 18.30 3 -1 21 0.30 5.00 3 -1 21 -5.30 6.40 -4 1 -21 -7.90 17.60 -4 1 -21 -16.80 15.60 4 -1 21 1.30 6.80 8 0 -21 40.80 11.70 -8 0 21 -0.40 6.00 -8 0 21 7.10 7.40 7 0 -21 30.00 12.40 7 0 -21 44.30 17.90 -7 0 21 5.00 6.50 -7 0 21 4.20 6.90 6 0 -21 116.89 23.70 6 0 -21 112.29 18.90 -6 0 21 89.89 12.40 -6 0 21 79.09 10.40 5 0 -21 51.89 18.80 5 0 -21 60.29 14.60 -5 0 21 13.00 6.60 -5 0 21 28.90 9.10 4 0 -21 69.89 15.70 4 0 -21 85.69 21.20 4 0 -21 97.79 21.40 -4 0 21 66.69 10.10 -4 0 21 64.89 11.40 3 0 -21 34.50 17.30 3 0 -21 16.10 12.00 3 0 -21 30.10 9.40 -3 0 21 14.20 7.10 -3 0 21 16.20 7.40 2 0 -21 19.40 20.50 2 0 -21 11.10 16.60 2 0 -21 29.90 10.50 -2 0 21 -2.00 5.40 -2 0 21 -7.40 5.60 1 0 -21 32.10 12.10 1 0 -21 12.80 15.90 -1 0 21 29.00 8.30 -1 0 21 20.90 7.40 0 0 -21 33.70 13.30 0 0 -21 22.40 18.00 0 0 21 23.80 7.60 0 0 21 22.30 8.60 -1 0 -21 17.40 17.30 -1 0 -21 18.90 13.40 1 0 21 4.30 7.20 1 0 21 2.90 6.10 -2 0 -21 1.50 15.70 -2 0 -21 30.30 15.00 2 0 21 2.90 5.80 2 0 21 -8.90 6.00 -3 0 -21 1.20 16.80 -3 0 -21 18.20 15.20 3 0 21 8.90 5.50 3 0 21 -0.10 6.90 -4 0 -21 -5.10 15.50 -4 0 -21 -6.20 14.70 4 0 21 -6.60 6.60 8 -1 -21 193.68 20.40 -7 1 21 3.40 6.90 -7 1 21 -2.00 5.50 6 -1 -21 76.09 20.40 6 -1 -21 73.19 14.20 -6 1 21 30.60 7.50 -6 1 21 34.50 9.80 5 -1 -21 86.19 15.60 5 -1 -21 85.49 21.50 -5 1 21 47.70 8.70 -5 1 21 49.50 10.00 4 -1 -21 50.09 12.80 4 -1 -21 34.90 15.80 -4 1 21 14.70 6.80 -4 1 21 13.00 7.40 3 -1 -21 38.40 16.10 3 -1 -21 36.60 10.10 -3 1 21 4.00 6.40 -3 1 21 6.60 6.40 2 -1 -21 15.80 14.30 2 -1 -21 26.30 9.70 -2 1 21 2.10 6.20 -2 1 21 1.60 6.10 1 -1 -21 47.50 18.30 1 -1 -21 57.69 13.40 -1 1 21 50.29 9.80 -1 1 21 29.50 8.20 0 -1 -21 12.70 11.30 0 -1 -21 44.60 18.90 0 1 21 12.00 7.50 0 1 21 12.90 6.40 -1 -1 -21 78.69 21.20 -1 -1 -21 93.59 17.60 1 1 21 50.79 9.30 1 1 21 51.09 10.60 -2 -1 -21 53.79 18.90 -2 -1 -21 88.99 18.20 2 1 21 77.59 11.90 2 1 21 52.09 9.40 -3 -1 -21 5.30 14.30 -3 -1 -21 -2.90 12.60 3 1 21 -7.60 6.30 3 1 21 3.60 6.30 -4 -1 -21 10.40 14.80 -4 -1 -21 -8.40 13.30 4 1 21 2.30 6.90 4 1 21 10.30 6.40 7 -2 -21 124.99 24.20 -7 2 21 18.30 8.90 6 -2 -21 92.59 20.60 -6 2 21 35.20 7.80 -6 2 21 52.19 10.90 5 -2 -21 46.10 16.40 -5 2 21 -5.90 4.90 -5 2 21 -0.40 6.00 4 -2 -21 31.80 15.20 4 -2 -21 29.10 9.40 -4 2 21 2.90 5.90 -4 2 21 9.20 7.20 3 -2 -21 118.39 23.20 3 -2 -21 175.28 18.50 -3 2 21 115.99 12.20 -3 2 21 106.29 12.90 2 -2 -21 26.80 15.00 2 -2 -21 29.00 10.20 -2 2 21 1.90 6.00 -2 2 21 2.40 6.10 1 -2 -21 25.90 10.10 1 -2 -21 28.50 14.60 -1 2 21 8.90 7.00 -1 2 21 -4.80 5.80 0 -2 -21 35.40 12.50 0 -2 -21 27.40 15.10 0 2 21 4.80 7.00 0 2 21 5.00 6.60 -1 -2 -21 17.20 11.70 -1 -2 -21 26.50 14.20 1 2 21 13.60 6.70 1 2 21 4.50 6.80 -2 -2 -21 12.00 12.30 -2 -2 -21 25.30 12.60 2 2 21 -3.50 6.40 2 2 21 -3.10 5.20 -3 -2 -21 14.40 12.80 -3 -2 -21 16.80 13.10 3 2 21 -1.80 5.30 3 2 21 -2.00 6.50 -4 -2 -21 46.60 15.80 5 -3 -21 60.89 16.00 -5 3 21 12.80 6.60 -5 3 21 23.70 8.80 4 -3 -21 51.79 17.00 4 -3 -21 47.80 11.20 -4 3 21 10.90 7.80 3 -3 -21 26.50 9.50 3 -3 -21 40.90 17.10 -3 3 21 -0.40 6.00 -3 3 21 -0.10 6.30 2 -3 -21 18.20 10.00 2 -3 -21 24.70 13.50 -2 3 21 -4.80 6.00 -2 3 21 -3.40 6.10 1 -3 -21 70.29 14.00 1 -3 -21 80.39 19.10 -1 3 21 48.40 9.80 -1 3 21 45.00 9.80 0 -3 -21 37.40 11.10 0 -3 -21 44.70 14.50 0 3 21 -2.90 6.20 0 3 21 -5.30 6.30 -1 -3 -21 53.09 14.40 -1 -3 -21 32.00 11.40 1 3 21 22.90 8.50 1 3 21 6.10 6.70 -2 -3 -21 28.30 12.20 2 3 21 -1.30 5.90 2 3 21 8.70 7.30 -3 -3 -21 36.10 13.00 3 3 21 15.10 7.20 3 3 21 17.70 8.20 5 -4 -21 65.59 11.30 -5 4 21 15.60 8.50 4 -4 -21 165.58 17.00 3 -4 -21 35.20 10.40 -3 4 21 1.10 6.80 -3 4 21 8.00 6.60 2 -4 -21 10.60 8.30 -2 4 21 0.80 6.30 -2 4 21 1.50 7.10 1 -4 -21 26.10 10.60 1 -4 -21 68.49 18.50 -1 4 21 -2.20 6.60 0 -4 -21 24.50 10.80 0 4 21 -7.80 6.20 0 4 21 3.20 6.50 -1 -4 -21 36.10 11.70 1 4 21 6.00 6.90 1 4 21 2.90 7.20 -2 -4 -21 46.10 13.30 2 4 21 15.30 7.60 2 4 21 18.10 8.40 4 -5 -21 157.08 17.40 0 5 21 9.80 7.70 0 5 21 16.90 7.90 -1 -5 -21 36.00 11.90 1 5 21 0.70 6.80 1 5 21 2.10 7.00 2 -6 -21 194.58 18.50 4 7 -22 52.59 21.10 4 7 -22 17.50 26.40 -4 -7 22 53.79 9.90 -4 -7 22 51.89 10.20 3 7 -22 6.00 17.40 3 7 -22 -27.00 24.40 -3 -7 22 21.80 8.50 -3 -7 22 23.80 8.20 -3 -7 22 16.80 7.20 2 7 -22 -35.10 13.40 2 7 -22 -12.00 26.60 -2 -7 22 -2.10 6.10 -2 -7 22 5.00 6.40 -2 -7 22 3.40 7.10 1 7 -22 16.50 18.60 1 7 -22 -2.80 27.30 -1 -7 22 30.80 8.50 -1 -7 22 57.59 10.60 6 6 -22 19.90 21.70 5 6 -22 7.40 16.40 5 6 -22 -5.00 6.70 5 6 -22 4.90 22.20 -5 -6 22 -0.30 6.90 -5 -6 22 11.90 7.40 4 6 -22 -27.20 21.90 4 6 -22 -9.00 15.20 -4 -6 22 9.50 6.70 -4 -6 22 9.30 7.20 3 6 -22 -2.80 16.60 3 6 -22 -21.20 23.50 -3 -6 22 -1.20 6.30 -3 -6 22 -4.40 6.20 -3 -6 22 -0.70 6.20 2 6 -22 -37.40 22.30 2 6 -22 -11.50 15.10 -2 -6 22 5.70 6.80 -2 -6 22 -3.80 5.60 -2 -6 22 -4.10 6.10 1 6 -22 -4.60 15.90 1 6 -22 -22.40 24.60 -1 -6 22 12.70 6.50 -1 -6 22 20.90 7.70 -1 -6 22 30.00 8.50 0 6 -22 -31.20 23.70 0 6 -22 -7.40 15.70 0 -6 22 5.20 6.80 0 -6 22 9.60 7.30 -1 6 -22 -50.99 22.00 -1 6 -22 -31.10 17.40 -1 6 -22 -16.50 15.60 1 -6 22 5.30 7.30 1 -6 22 10.20 7.50 6 5 -22 -1.30 6.50 6 5 -22 3.70 15.10 6 5 -22 26.10 20.00 -6 -5 22 -2.10 6.60 -6 -5 22 4.50 6.90 5 5 -22 -8.60 6.30 5 5 -22 17.70 16.80 5 5 -22 10.40 21.80 -5 -5 22 -2.80 5.90 -5 -5 22 -5.70 6.30 4 5 -22 27.90 18.40 4 5 -22 31.40 24.00 -4 -5 22 24.10 8.30 -4 -5 22 33.40 8.40 3 5 -22 -1.00 15.30 3 5 -22 2.10 24.10 -3 -5 22 17.70 7.70 -3 -5 22 1.70 6.60 -3 -5 22 12.00 7.30 2 5 -22 10.70 16.50 2 5 -22 -13.20 23.20 -2 -5 22 26.80 8.60 -2 -5 22 15.40 7.40 -2 -5 22 22.70 7.60 1 5 -22 22.00 17.80 1 5 -22 -1.00 25.30 -1 -5 22 36.40 9.10 -1 -5 22 23.60 7.70 -1 -5 22 23.20 7.70 0 5 -22 4.80 16.60 0 5 -22 -14.80 24.10 0 5 -22 -5.30 15.10 0 -5 22 6.30 7.10 0 -5 22 -2.60 6.40 0 -5 22 23.10 7.40 -1 5 -22 -34.40 15.50 -1 5 -22 -28.40 13.80 1 -5 22 -9.20 6.30 1 -5 22 0.30 6.80 -2 5 -22 -41.50 21.80 -2 5 -22 -54.29 16.00 7 4 -22 38.70 16.10 7 4 -22 80.89 20.90 -7 -4 22 19.50 8.00 -7 -4 22 40.60 10.20 6 4 -22 26.70 15.60 6 4 -22 39.30 19.40 -6 -4 22 5.90 7.30 -6 -4 22 12.70 7.50 5 4 -22 -0.20 6.50 5 4 -22 2.00 14.40 5 4 -22 31.50 20.50 -5 -4 22 -7.00 6.00 -5 -4 22 12.20 7.40 4 4 -22 13.90 16.20 4 4 -22 30.30 22.10 -4 -4 22 19.30 7.60 -4 -4 22 6.30 7.00 3 4 -22 3.90 20.60 3 4 -22 5.50 15.90 -3 -4 22 6.90 6.80 -3 -4 22 -1.20 5.80 -3 -4 22 8.60 6.70 2 4 -22 2.20 15.80 2 4 -22 11.10 22.90 -2 -4 22 5.20 6.70 -2 -4 22 2.80 6.30 -2 -4 22 3.60 6.60 1 4 -22 0.50 16.00 1 4 -22 -9.40 21.70 -1 -4 22 12.70 6.60 -1 -4 22 20.60 7.50 -1 -4 22 17.40 7.80 0 4 -22 -8.50 14.90 0 4 -22 -6.40 23.60 0 4 -22 -0.80 14.90 0 -4 22 -2.80 5.20 0 -4 22 3.60 6.40 0 -4 22 -16.40 5.70 -1 4 -22 23.80 18.20 -1 4 -22 -4.50 23.50 -1 4 -22 20.60 17.10 1 -4 22 34.10 8.50 1 -4 22 26.50 8.90 -2 4 -22 -43.10 20.10 -2 4 -22 -45.50 15.10 -2 4 -22 -20.30 21.30 2 -4 22 4.60 7.10 2 -4 22 0.90 6.60 7 3 -22 82.89 19.10 7 3 -22 23.40 13.00 -7 -3 22 28.40 9.30 -7 -3 22 5.20 7.00 6 3 -22 56.09 19.90 6 3 -22 50.59 16.50 -6 -3 22 31.00 9.40 -6 -3 22 29.10 8.70 5 3 -22 38.10 19.80 5 3 -22 26.40 15.80 -5 -3 22 11.50 7.20 -5 -3 22 15.80 8.20 4 3 -22 35.20 20.40 4 3 -22 15.90 14.80 -4 -3 22 -2.30 6.00 -4 -3 22 -2.80 6.20 3 3 -22 -0.60 18.90 3 3 -22 6.00 14.90 -3 -3 22 -2.60 5.70 -3 -3 22 2.30 6.50 2 3 -22 6.90 15.20 2 3 -22 27.80 22.90 -2 -3 22 28.30 8.50 -2 -3 22 26.40 8.50 1 3 -22 -3.30 14.50 1 3 -22 -1.90 20.40 1 3 -22 33.20 13.80 -1 -3 22 19.10 7.60 -1 -3 22 14.10 7.70 -1 -3 22 5.60 6.70 0 3 -22 8.30 13.90 0 3 -22 0.10 14.20 0 3 -22 -10.60 19.80 0 -3 22 -3.20 5.90 0 -3 22 4.80 5.60 0 -3 22 5.20 6.70 -1 3 -22 13.90 15.90 -1 3 -22 -17.10 21.70 1 -3 22 1.70 6.90 1 -3 22 0.90 6.80 1 -3 22 6.80 6.00 -2 3 -22 -24.00 19.50 -2 3 -22 -19.70 15.40 2 -3 22 -1.50 6.60 2 -3 22 -2.90 6.60 7 2 -22 67.99 18.10 7 2 -22 25.00 12.90 -7 -2 22 -7.80 6.50 -7 -2 22 -1.40 5.80 6 2 -22 17.50 12.30 6 2 -22 55.39 18.00 -6 -2 22 -2.30 7.00 -6 -2 22 -3.30 5.70 5 2 -22 78.09 18.60 5 2 -22 83.29 23.00 -5 -2 22 35.70 9.10 -5 -2 22 37.50 8.70 4 2 -22 120.89 21.30 4 2 -22 114.09 26.00 -4 -2 22 84.19 11.10 -4 -2 22 119.19 14.20 3 2 -22 8.60 18.10 3 2 -22 -1.90 13.40 -3 -2 22 -0.90 6.20 -3 -2 22 -12.70 5.20 2 2 -22 53.09 12.70 2 2 -22 39.50 16.40 2 2 -22 33.00 21.20 -2 -2 22 37.40 9.40 -2 -2 22 44.80 9.60 1 2 -22 14.40 19.60 1 2 -22 24.80 16.90 1 2 -22 51.89 14.50 -1 -2 22 35.30 9.10 -1 -2 22 32.20 8.00 0 2 -22 80.19 17.00 0 2 -22 52.59 24.30 0 -2 22 56.79 10.30 0 -2 22 54.79 9.40 -1 2 -22 15.30 21.10 -1 2 -22 36.20 16.10 1 -2 22 52.39 10.60 1 -2 22 38.90 8.50 -2 2 -22 8.30 21.80 -2 2 -22 24.90 16.80 2 -2 22 12.80 8.10 2 -2 22 29.30 8.60 -3 2 -22 13.00 21.80 7 1 -22 63.29 15.20 -7 -1 22 22.00 9.30 -7 -1 22 40.20 8.60 6 1 -22 72.99 19.00 6 1 -22 45.00 14.00 -6 -1 22 17.80 8.60 -6 -1 22 15.00 7.10 5 1 -22 25.20 12.90 -5 -1 22 4.90 6.50 -5 -1 22 9.50 7.10 4 1 -22 53.89 15.50 4 1 -22 56.49 19.40 -4 -1 22 37.30 9.20 -4 -1 22 47.80 9.30 3 1 -22 23.40 13.50 3 1 -22 29.50 19.10 -3 -1 22 4.90 6.40 -3 -1 22 2.40 6.60 2 1 -22 19.50 21.00 2 1 -22 26.90 10.40 2 1 -22 17.60 17.90 -2 -1 22 0.30 6.00 -2 -1 22 -1.80 6.10 1 1 -22 17.90 19.50 1 1 -22 42.00 13.00 -1 -1 22 2.30 6.70 -1 -1 22 0.70 6.50 0 1 -22 32.70 14.00 0 1 -22 23.50 19.60 0 -1 22 10.70 6.80 0 -1 22 3.00 6.80 -1 1 -22 87.49 18.70 -1 1 -22 64.29 23.70 1 -1 22 57.59 9.60 1 -1 22 69.99 11.50 -2 1 -22 1.70 17.60 -2 1 -22 38.90 16.30 2 -1 22 11.80 6.40 2 -1 22 11.80 7.90 7 0 -22 181.18 20.40 6 0 -22 310.47 37.50 -6 0 22 201.08 17.20 -6 0 22 168.78 14.30 -5 0 22 3.80 7.10 -5 0 22 0.30 5.70 4 0 -22 49.90 18.00 4 0 -22 33.10 12.50 -4 0 22 7.90 6.70 -4 0 22 7.10 7.30 3 0 -22 42.30 9.50 3 0 -22 26.00 16.10 -3 0 22 0.70 6.10 -3 0 22 0.40 6.40 2 0 -22 29.50 17.20 2 0 -22 60.59 12.00 -2 0 22 9.40 6.90 -2 0 22 16.60 7.80 1 0 -22 33.40 11.70 1 0 -22 27.90 17.20 -1 0 22 9.30 6.90 -1 0 22 10.90 7.60 0 0 -22 23.60 17.30 0 0 -22 28.90 11.90 0 0 22 13.40 7.60 0 0 22 7.80 6.30 -1 0 -22 20.60 13.10 -1 0 -22 9.20 16.40 1 0 22 1.90 5.80 1 0 22 -0.40 7.00 -2 0 -22 2.70 15.90 -2 0 -22 20.90 14.20 2 0 22 -4.90 6.40 2 0 22 9.70 6.40 -7 1 22 6.90 7.80 6 -1 -22 76.99 18.30 -6 1 22 -4.90 6.60 -6 1 22 5.40 6.40 -5 1 22 21.70 7.20 -5 1 22 11.10 8.20 4 -1 -22 54.29 16.90 -4 1 22 0.70 6.80 -4 1 22 8.30 6.80 3 -1 -22 58.99 18.50 3 -1 -22 66.99 11.80 -3 1 22 34.50 9.20 -3 1 22 26.00 7.80 2 -1 -22 51.49 16.80 2 -1 -22 64.69 12.00 -2 1 22 24.40 8.20 -2 1 22 17.60 7.60 1 -1 -22 106.49 15.90 1 -1 -22 76.79 21.40 -1 1 22 67.69 10.90 -1 1 22 88.89 12.50 0 -1 -22 13.40 14.20 0 -1 -22 39.30 13.10 0 1 22 -1.60 6.40 0 1 22 -6.60 6.50 -1 -1 -22 32.70 12.80 -1 -1 -22 28.50 15.60 1 1 22 2.60 6.40 1 1 22 8.10 7.50 -2 -1 -22 47.80 15.20 -2 -1 -22 44.80 17.30 2 1 22 22.80 7.30 2 1 22 34.30 9.70 -5 2 22 3.90 7.10 -5 2 22 7.00 6.70 -4 2 22 0.60 7.10 -4 2 22 -0.80 5.70 3 -2 -22 34.70 14.90 3 -2 -22 43.70 10.40 -3 2 22 3.10 6.70 -3 2 22 0.40 6.50 2 -2 -22 45.90 10.60 -2 2 22 2.90 6.50 -2 2 22 9.90 7.20 1 -2 -22 57.39 16.80 1 -2 -22 44.80 11.10 -1 2 22 20.30 8.10 -1 2 22 10.40 7.00 0 -2 -22 64.19 16.30 0 -2 -22 60.79 12.80 0 2 22 21.90 8.40 0 2 22 14.90 7.30 -1 -2 -22 48.60 14.80 1 2 22 -4.80 5.60 1 2 22 -7.30 6.50 -5 3 22 6.30 7.40 -4 3 22 6.20 7.10 -4 3 22 -3.10 5.90 -3 3 22 34.30 9.60 -3 3 22 15.80 7.20 -2 3 22 -2.70 6.20 -2 3 22 -6.70 5.60 1 -3 -22 54.19 12.30 -1 3 22 12.50 7.70 -1 3 22 14.70 8.00 0 -3 -22 48.30 11.20 0 3 22 -9.30 6.00 0 3 22 -3.10 6.60 -3 4 22 6.60 7.50 3 4 -23 27.40 22.50 2 4 -23 -13.90 21.00 4 3 -23 42.20 20.40 3 3 -23 20.60 21.00 3 3 -23 9.50 14.90 -3 -3 23 2.50 6.70 -3 -3 23 2.80 7.10 2 3 -23 17.50 20.90 2 3 -23 18.60 15.60 -2 -3 23 16.80 7.60 -2 -3 23 19.30 8.40 1 3 -23 -6.70 18.90 -4 -2 23 10.50 7.80 -4 -2 23 12.70 7.30 3 2 -23 26.00 14.60 3 2 -23 22.20 17.90 -3 -2 23 -4.10 6.40 -3 -2 23 -3.40 6.40 2 2 -23 22.70 19.20 -2 -2 23 1.70 6.10 -2 -2 23 -4.30 6.50 1 2 -23 28.40 11.90 1 2 -23 1.20 18.80 -1 -2 23 -1.10 6.60 -1 -2 23 -0.20 6.00 4 1 -23 55.89 18.40 -4 -1 23 13.10 8.00 -4 -1 23 -6.00 5.60 3 1 -23 16.00 15.50 -3 -1 23 -9.70 5.80 -3 -1 23 4.10 7.30 2 1 -23 35.20 18.60 -2 -1 23 5.40 6.50 -2 -1 23 7.80 7.10 1 1 -23 70.09 22.90 -1 -1 23 52.09 9.90 3 0 -23 233.58 32.30 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 70214 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si1 Si 0.30073(4) 0.35001(4) 0.67528(3) 0.01491(11) Uani 1 1 d . . . . . Si2 Si 0.44309(4) 0.28861(4) 0.75386(3) 0.01520(11) Uani 1 1 d . . . . . Si3 Si 0.09272(4) 0.21271(4) 0.57517(3) 0.01675(12) Uani 1 1 d . . . . . Si4 Si 0.25480(4) 0.32592(4) 0.47073(3) 0.01644(12) Uani 1 1 d . . . . . Si5 Si 0.66687(4) 0.21555(4) 0.68890(3) 0.01795(12) Uani 1 1 d . . . . . Si6 Si 0.49155(4) 0.04241(4) 0.72474(3) 0.01753(12) Uani 1 1 d . . . . . C1 C 0.21353(15) 0.45744(14) 0.72117(12) 0.0180(4) Uani 1 1 d . . . . . C2 C 0.14223(15) 0.43925(15) 0.78317(12) 0.0210(4) Uani 1 1 d . . . . . C3 C 0.13867(17) 0.34324(16) 0.82133(12) 0.0252(4) Uani 1 1 d . . . . . H1 H 0.1886 0.2894 0.8067 0.030 Uiso 1 1 calc R U . . . C5 C -0.00877(19) 0.4047(2) 0.90143(15) 0.0380(6) Uani 1 1 d . . . . . H2 H -0.0600 0.3918 0.9404 0.046 Uiso 1 1 calc R U . . . C6 C -0.00757(19) 0.4975(2) 0.86861(14) 0.0374(6) Uani 1 1 d . . . . . H3 H -0.0581 0.5499 0.8851 0.045 Uiso 1 1 calc R U . . . C8 C 0.07162(18) 0.61625(17) 0.77762(13) 0.0306(5) Uani 1 1 d . . . . . H4 H 0.0213 0.6686 0.7945 0.037 Uiso 1 1 calc R U . . . C10 C 0.15414(19) 0.74108(16) 0.69398(14) 0.0319(5) Uani 1 1 d . . . . . H5 H 0.1079 0.7949 0.7145 0.038 Uiso 1 1 calc R U . . . C11 C 0.22596(19) 0.76275(16) 0.63892(15) 0.0317(5) Uani 1 1 d . . . . . H6 H 0.2296 0.8312 0.6209 0.038 Uiso 1 1 calc R U . . . C12 C 0.29591(18) 0.68362(16) 0.60800(14) 0.0287(5) Uani 1 1 d . . . . . H7 H 0.3461 0.6990 0.5690 0.034 Uiso 1 1 calc R U . . . C13 C 0.29143(16) 0.58583(15) 0.63400(13) 0.0231(4) Uani 1 1 d . . . . . H8 H 0.3393 0.5339 0.6127 0.028 Uiso 1 1 calc R U . . . C14 C 0.21753(15) 0.55836(15) 0.69213(12) 0.0198(4) Uani 1 1 d . . . . . C7 C 0.06799(17) 0.51943(17) 0.80945(13) 0.0272(5) Uani 1 1 d . . . . . C15 C 0.52404(15) 0.36590(15) 0.85300(12) 0.0184(4) Uani 1 1 d . . . . . C16 C 0.56676(15) 0.46927(15) 0.85195(12) 0.0215(4) Uani 1 1 d . . . . . C17 C 0.54404(17) 0.52915(15) 0.77970(13) 0.0245(4) Uani 1 1 d . . . . . H9 H 0.4990 0.4979 0.7283 0.029 Uiso 1 1 calc R U . . . C9 C 0.14610(17) 0.63927(16) 0.72196(13) 0.0250(4) Uani 1 1 d . . . . . C4 C 0.06618(18) 0.32603(19) 0.87802(13) 0.0316(5) Uani 1 1 d . . . . . H10 H 0.0659 0.2608 0.9020 0.038 Uiso 1 1 calc R U . . . C18 C 0.58413(18) 0.62890(17) 0.78147(15) 0.0314(5) Uani 1 1 d . . . . . H11 H 0.5659 0.6663 0.7322 0.038 Uiso 1 1 calc R U . . . C19 C 0.6532(2) 0.67791(18) 0.85638(16) 0.0375(6) Uani 1 1 d . . . . . H12 H 0.6811 0.7479 0.8573 0.045 Uiso 1 1 calc R U . . . C20 C 0.67884(19) 0.62494(18) 0.92605(15) 0.0353(5) Uani 1 1 d . . . . . H13 H 0.7261 0.6580 0.9756 0.042 Uiso 1 1 calc R U . . . C21 C 0.63703(17) 0.52046(16) 0.92758(13) 0.0269(5) Uani 1 1 d . . . . . C22 C 0.66155(17) 0.46781(18) 1.00088(13) 0.0305(5) Uani 1 1 d . . . . . H14 H 0.7101 0.5010 1.0497 0.037 Uiso 1 1 calc R U . . . C23 C 0.61739(17) 0.36846(17) 1.00483(12) 0.0266(5) Uani 1 1 d . . . . . C24 C 0.6395(2) 0.3163(2) 1.08114(13) 0.0363(5) Uani 1 1 d . . . . . H15 H 0.6873 0.3500 1.1302 0.044 Uiso 1 1 calc R U . . . C25 C 0.5945(2) 0.2205(2) 1.08558(14) 0.0407(6) Uani 1 1 d . . . . . H16 H 0.6112 0.1868 1.1371 0.049 Uiso 1 1 calc R U . . . C26 C 0.5220(2) 0.16992(19) 1.01304(14) 0.0347(5) Uani 1 1 d . . . . . H17 H 0.4892 0.1027 1.0164 0.042 Uiso 1 1 calc R U . . . C27 C 0.49928(17) 0.21678(16) 0.93921(12) 0.0259(4) Uani 1 1 d . . . . . H18 H 0.4503 0.1815 0.8916 0.031 Uiso 1 1 calc R U . . . C28 C 0.54615(15) 0.31709(15) 0.93036(12) 0.0208(4) Uani 1 1 d . . . . . C29 C 0.24400(14) 0.26090(13) 0.57411(11) 0.0133(3) Uani 1 1 d . . . . . C30 C 0.32048(14) 0.16173(13) 0.57710(11) 0.0149(4) Uani 1 1 d . . . . . H19 H 0.2993 0.1203 0.6226 0.018 Uiso 1 1 calc R U . . . H20 H 0.3011 0.1179 0.5212 0.018 Uiso 1 1 calc R U . . . C31 C 0.45087(14) 0.18016(14) 0.59426(11) 0.0147(4) Uani 1 1 d . . . . . H21 H 0.4682 0.2486 0.5742 0.018 Uiso 1 1 calc R U . . . H22 H 0.4850 0.1254 0.5580 0.018 Uiso 1 1 calc R U . . . C32 C 0.51166(14) 0.17976(14) 0.69070(11) 0.0145(4) Uani 1 1 d . . . . . C33 C 0.08827(16) 0.12150(16) 0.66077(13) 0.0251(4) Uani 1 1 d . . . . . H23 H 0.0097 0.1111 0.6702 0.038 Uiso 1 1 calc R U . . . H24 H 0.1340 0.1518 0.7148 0.038 Uiso 1 1 calc R U . . . H25 H 0.1189 0.0538 0.6421 0.038 Uiso 1 1 calc R U . . . C34 C 0.03491(16) 0.13288(15) 0.47172(13) 0.0233(4) Uani 1 1 d . . . . . H26 H -0.0370 0.0986 0.4780 0.035 Uiso 1 1 calc R U . . . H27 H 0.0893 0.0794 0.4579 0.035 Uiso 1 1 calc R U . . . H28 H 0.0221 0.1787 0.4250 0.035 Uiso 1 1 calc R U . . . C35 C -0.00786(16) 0.32039(16) 0.59354(14) 0.0252(4) Uani 1 1 d . . . . . H29 H -0.0768 0.3087 0.5509 0.038 Uiso 1 1 calc R U . . . H30 H 0.0280 0.3879 0.5873 0.038 Uiso 1 1 calc R U . . . H31 H -0.0276 0.3210 0.6520 0.038 Uiso 1 1 calc R U . . . C36 C 0.14111(17) 0.42226(16) 0.44867(14) 0.0257(4) Uani 1 1 d . . . . . H32 H 0.1527 0.4574 0.3978 0.039 Uiso 1 1 calc R U . . . H33 H 0.1438 0.4746 0.4989 0.039 Uiso 1 1 calc R U . . . H34 H 0.0670 0.3855 0.4377 0.039 Uiso 1 1 calc R U . . . C37 C 0.24268(19) 0.22750(16) 0.37339(13) 0.0286(5) Uani 1 1 d . . . . . H35 H 0.1679 0.1921 0.3644 0.043 Uiso 1 1 calc R U . . . H36 H 0.3018 0.1756 0.3824 0.043 Uiso 1 1 calc R U . . . H37 H 0.2520 0.2633 0.3224 0.043 Uiso 1 1 calc R U . . . C38 C 0.39514(16) 0.39345(16) 0.47084(13) 0.0240(4) Uani 1 1 d . . . . . H38 H 0.3861 0.4473 0.4303 0.036 Uiso 1 1 calc R U . . . H39 H 0.4494 0.3419 0.4531 0.036 Uiso 1 1 calc R U . . . H40 H 0.4233 0.4264 0.5292 0.036 Uiso 1 1 calc R U . . . C39 C 0.75857(17) 0.22765(17) 0.79676(14) 0.0299(5) Uani 1 1 d . . . . . H41 H 0.8354 0.2502 0.7903 0.045 Uiso 1 1 calc R U . . . H42 H 0.7611 0.1595 0.8204 0.045 Uiso 1 1 calc R U . . . H43 H 0.7273 0.2796 0.8363 0.045 Uiso 1 1 calc R U . . . C40 C 0.67907(16) 0.34420(16) 0.64417(14) 0.0254(4) Uani 1 1 d . . . . . H44 H 0.6600 0.4007 0.6859 0.038 Uiso 1 1 calc R U . . . H45 H 0.6267 0.3440 0.5898 0.038 Uiso 1 1 calc R U . . . H46 H 0.7569 0.3555 0.6333 0.038 Uiso 1 1 calc R U . . . C41 C 0.72985(16) 0.11475(17) 0.61637(14) 0.0279(5) Uani 1 1 d . . . . . H47 H 0.6832 0.1066 0.5591 0.042 Uiso 1 1 calc R U . . . H48 H 0.7323 0.0475 0.6413 0.042 Uiso 1 1 calc R U . . . H49 H 0.8069 0.1375 0.6108 0.042 Uiso 1 1 calc R U . . . C42 C 0.35890(17) 0.02290(16) 0.77338(13) 0.0256(4) Uani 1 1 d . . . . . H50 H 0.3132 -0.0356 0.7400 0.038 Uiso 1 1 calc R U . . . H51 H 0.3151 0.0870 0.7721 0.038 Uiso 1 1 calc R U . . . H52 H 0.3793 0.0071 0.8334 0.038 Uiso 1 1 calc R U . . . C43 C 0.61004(18) 0.00034(16) 0.80445(13) 0.0284(5) Uani 1 1 d . . . . . H53 H 0.5920 -0.0695 0.8200 0.043 Uiso 1 1 calc R U . . . H54 H 0.6203 0.0505 0.8565 0.043 Uiso 1 1 calc R U . . . H55 H 0.6801 -0.0020 0.7787 0.043 Uiso 1 1 calc R U . . . C44 C 0.48134(18) -0.05565(15) 0.62726(13) 0.0257(4) Uani 1 1 d . . . . . H56 H 0.5482 -0.0479 0.5987 0.038 Uiso 1 1 calc R U . . . H57 H 0.4129 -0.0437 0.5870 0.038 Uiso 1 1 calc R U . . . H58 H 0.4776 -0.1267 0.6450 0.038 Uiso 1 1 calc R U . . . C45 C 0.2203(6) 0.9966(10) 0.9789(5) 0.062(2) Uani 0.648(17) 1 d . U P A 1 H59 H 0.2116 1.0128 1.0399 0.093 Uiso 0.648(17) 1 calc R U P A 1 H60 H 0.2370 1.0615 0.9544 0.093 Uiso 0.648(17) 1 calc R U P A 1 H61 H 0.2826 0.9482 0.9746 0.093 Uiso 0.648(17) 1 calc R U P A 1 C46 C 0.1132(4) 0.9468(7) 0.9302(3) 0.0371(14) Uani 0.648(17) 1 d G U P A 1 C47 C 0.0583(7) 0.8641(6) 0.9597(3) 0.0390(16) Uani 0.648(17) 1 d G U P A 1 H62 H 0.0912 0.8352 1.0108 0.047 Uiso 0.648(17) 1 calc R U P A 1 C48 C -0.0445(7) 0.8237(3) 0.9146(4) 0.0372(14) Uani 0.648(17) 1 d G U P A 1 H63 H -0.0820 0.7671 0.9348 0.045 Uiso 0.648(17) 1 calc R U P A 1 C49 C -0.0926(5) 0.8659(4) 0.8399(4) 0.0352(12) Uani 0.648(17) 1 d G U P A 1 H64 H -0.1629 0.8383 0.8090 0.042 Uiso 0.648(17) 1 calc R U P A 1 C50 C -0.0378(4) 0.9486(5) 0.8103(4) 0.0308(13) Uani 0.648(17) 1 d G U P A 1 H65 H -0.0706 0.9775 0.7593 0.037 Uiso 0.648(17) 1 calc R U P A 1 C51 C 0.0651(5) 0.9890(6) 0.8555(4) 0.0295(14) Uani 0.648(17) 1 d G U P A 1 H66 H 0.1026 1.0455 0.8353 0.035 Uiso 0.648(17) 1 calc R U P A 1 C52 C 0.2319(13) 1.0460(13) 0.9740(10) 0.050(3) Uani 0.352(17) 1 d . U P A 2 H67 H 0.2264 1.0672 1.0349 0.075 Uiso 0.352(17) 1 calc R U P A 2 H68 H 0.2394 1.1087 0.9439 0.075 Uiso 0.352(17) 1 calc R U P A 2 H69 H 0.2985 1.0027 0.9704 0.075 Uiso 0.352(17) 1 calc R U P A 2 C53 C 0.1235(7) 0.9820(8) 0.9311(6) 0.0235(19) Uani 0.352(17) 1 d G U P A 2 C54 C 0.1017(11) 0.8895(7) 0.9660(5) 0.033(2) Uani 0.352(17) 1 d G U P A 2 H70 H 0.1515 0.8690 1.0140 0.040 Uiso 0.352(17) 1 calc R U P A 2 C55 C 0.0069(14) 0.8270(5) 0.9306(7) 0.036(2) Uani 0.352(17) 1 d G U P A 2 H71 H -0.0081 0.7638 0.9544 0.043 Uiso 0.352(17) 1 calc R U P A 2 C56 C -0.0661(9) 0.8570(8) 0.8603(8) 0.038(2) Uani 0.352(17) 1 d G U P A 2 H72 H -0.1308 0.8143 0.8360 0.046 Uiso 0.352(17) 1 calc R U P A 2 C57 C -0.0442(8) 0.9495(9) 0.8254(8) 0.036(3) Uani 0.352(17) 1 d G U P A 2 H73 H -0.0940 0.9700 0.7773 0.043 Uiso 0.352(17) 1 calc R U P A 2 C58 C 0.0506(10) 1.0120(7) 0.8608(8) 0.028(2) Uani 0.352(17) 1 d G U P A 2 H74 H 0.0655 1.0752 0.8370 0.033 Uiso 0.352(17) 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.0125(2) 0.0151(2) 0.0153(2) -0.00330(19) -0.00130(18) 0.00296(19) Si2 0.0136(2) 0.0175(2) 0.0125(2) -0.00339(19) -0.00163(18) 0.00324(19) Si3 0.0108(2) 0.0186(3) 0.0192(3) 0.0003(2) -0.00177(19) -0.00056(19) Si4 0.0155(2) 0.0172(3) 0.0155(2) 0.00154(19) -0.00158(19) 0.00120(19) Si5 0.0110(2) 0.0212(3) 0.0202(3) -0.0014(2) -0.00025(19) 0.0033(2) Si6 0.0188(3) 0.0163(3) 0.0163(3) -0.0001(2) -0.0004(2) 0.0034(2) C1 0.0133(9) 0.0207(9) 0.0168(9) -0.0066(7) -0.0032(7) 0.0031(7) C2 0.0156(9) 0.0274(10) 0.0162(9) -0.0091(8) -0.0026(7) 0.0015(8) C3 0.0225(10) 0.0315(11) 0.0190(10) -0.0070(8) 0.0007(8) -0.0009(8) C5 0.0290(12) 0.0578(16) 0.0259(11) -0.0133(11) 0.0123(9) -0.0067(11) C6 0.0256(11) 0.0540(15) 0.0298(12) -0.0151(11) 0.0072(9) 0.0082(11) C8 0.0250(11) 0.0356(12) 0.0265(11) -0.0124(9) -0.0029(9) 0.0169(9) C10 0.0326(12) 0.0236(11) 0.0326(12) -0.0085(9) -0.0118(10) 0.0154(9) C11 0.0338(12) 0.0179(10) 0.0372(12) -0.0026(9) -0.0121(10) 0.0044(9) C12 0.0260(11) 0.0224(10) 0.0341(12) -0.0004(9) -0.0048(9) 0.0012(8) C13 0.0197(10) 0.0191(10) 0.0274(10) -0.0042(8) -0.0024(8) 0.0040(8) C14 0.0161(9) 0.0209(10) 0.0177(9) -0.0069(8) -0.0076(7) 0.0054(7) C7 0.0190(10) 0.0382(12) 0.0204(10) -0.0121(9) -0.0012(8) 0.0056(9) C15 0.0136(9) 0.0236(10) 0.0156(9) -0.0068(7) -0.0001(7) 0.0038(7) C16 0.0150(9) 0.0235(10) 0.0235(10) -0.0089(8) 0.0014(8) 0.0028(8) C17 0.0220(10) 0.0251(10) 0.0237(10) -0.0052(8) -0.0003(8) -0.0002(8) C9 0.0222(10) 0.0252(10) 0.0219(10) -0.0095(8) -0.0082(8) 0.0102(8) C4 0.0292(11) 0.0421(13) 0.0212(10) -0.0073(9) 0.0039(9) -0.0070(10) C18 0.0310(12) 0.0258(11) 0.0355(12) -0.0021(9) 0.0022(9) -0.0032(9) C19 0.0345(13) 0.0253(11) 0.0485(15) -0.0081(10) 0.0012(11) -0.0078(10) C20 0.0270(11) 0.0319(12) 0.0399(13) -0.0144(10) -0.0055(10) -0.0050(9) C21 0.0201(10) 0.0304(11) 0.0258(11) -0.0118(9) -0.0016(8) 0.0006(8) C22 0.0229(10) 0.0396(13) 0.0228(11) -0.0134(9) -0.0065(8) 0.0003(9) C23 0.0214(10) 0.0384(12) 0.0164(10) -0.0068(9) -0.0034(8) 0.0066(9) C24 0.0356(13) 0.0520(15) 0.0165(10) -0.0047(10) -0.0073(9) 0.0040(11) C25 0.0475(14) 0.0552(16) 0.0169(11) 0.0076(10) -0.0063(10) 0.0074(12) C26 0.0430(13) 0.0386(13) 0.0215(11) 0.0039(9) 0.0007(9) 0.0026(11) C27 0.0280(11) 0.0307(11) 0.0159(10) -0.0031(8) -0.0029(8) 0.0034(9) C28 0.0164(9) 0.0276(10) 0.0164(9) -0.0052(8) -0.0001(7) 0.0058(8) C29 0.0104(8) 0.0130(8) 0.0146(9) -0.0023(7) -0.0024(7) 0.0016(7) C30 0.0145(9) 0.0142(8) 0.0140(9) -0.0026(7) -0.0021(7) 0.0024(7) C31 0.0144(9) 0.0169(9) 0.0119(8) -0.0015(7) 0.0004(7) 0.0032(7) C32 0.0124(8) 0.0165(9) 0.0132(9) -0.0015(7) -0.0011(7) 0.0037(7) C33 0.0179(10) 0.0299(11) 0.0268(11) 0.0044(9) 0.0005(8) -0.0037(8) C34 0.0194(10) 0.0222(10) 0.0253(10) 0.0005(8) -0.0050(8) -0.0040(8) C35 0.0134(9) 0.0297(11) 0.0313(11) -0.0010(9) 0.0011(8) 0.0025(8) C36 0.0212(10) 0.0239(10) 0.0310(11) 0.0078(9) -0.0029(8) 0.0041(8) C37 0.0381(12) 0.0290(11) 0.0179(10) -0.0007(8) 0.0039(9) -0.0014(9) C38 0.0198(10) 0.0295(11) 0.0231(10) 0.0085(8) 0.0013(8) -0.0005(8) C39 0.0183(10) 0.0355(12) 0.0314(12) -0.0004(9) -0.0079(9) -0.0004(9) C40 0.0168(9) 0.0289(11) 0.0311(11) 0.0031(9) 0.0055(8) 0.0007(8) C41 0.0148(9) 0.0328(11) 0.0351(12) -0.0059(9) 0.0060(8) 0.0042(8) C42 0.0271(11) 0.0246(10) 0.0257(11) 0.0048(8) 0.0046(8) -0.0007(8) C43 0.0300(11) 0.0275(11) 0.0262(11) 0.0072(9) -0.0038(9) 0.0082(9) C44 0.0304(11) 0.0193(10) 0.0255(11) -0.0030(8) 0.0018(9) 0.0027(8) C45 0.030(3) 0.124(7) 0.028(3) -0.012(4) 0.001(2) 0.013(4) C46 0.035(2) 0.052(4) 0.023(2) -0.003(2) 0.0027(17) 0.026(2) C47 0.041(4) 0.054(3) 0.020(2) 0.001(2) -0.002(2) 0.019(3) C48 0.053(4) 0.037(2) 0.021(2) 0.0041(17) 0.000(3) 0.015(2) C49 0.048(3) 0.043(3) 0.015(2) 0.0024(17) 0.0015(18) 0.011(2) C50 0.032(2) 0.046(3) 0.015(2) 0.0026(18) 0.0064(17) 0.013(2) C51 0.026(2) 0.040(3) 0.024(2) 0.001(2) 0.0074(17) 0.017(2) C52 0.038(4) 0.077(8) 0.032(5) -0.005(5) 0.005(3) -0.007(5) C53 0.032(3) 0.024(4) 0.017(3) 0.000(3) 0.011(3) 0.015(3) C54 0.047(5) 0.030(4) 0.024(3) 0.002(3) 0.006(3) 0.008(3) C55 0.051(6) 0.035(4) 0.022(4) 0.002(3) 0.009(4) 0.003(4) C56 0.048(4) 0.043(4) 0.023(5) -0.006(3) 0.008(4) 0.000(3) C57 0.037(4) 0.048(5) 0.022(4) 0.003(3) 0.004(3) 0.010(3) C58 0.027(3) 0.036(4) 0.022(4) 0.000(3) 0.010(3) 0.023(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C1 Si1 C29 121.94(8) . . C1 Si1 Si2 121.19(6) . . C29 Si1 Si2 113.97(6) . . C15 Si2 C32 121.38(8) . . C15 Si2 Si1 122.87(6) . . C32 Si2 Si1 111.46(6) . . C34 Si3 C35 107.76(9) . . C34 Si3 C33 104.78(9) . . C35 Si3 C33 108.08(10) . . C34 Si3 C29 111.32(8) . . C35 Si3 C29 113.84(8) . . C33 Si3 C29 110.59(8) . . C36 Si4 C37 107.03(10) . . C36 Si4 C38 108.38(9) . . C37 Si4 C38 103.16(10) . . C36 Si4 C29 111.96(9) . . C37 Si4 C29 111.89(9) . . C38 Si4 C29 113.85(8) . . C40 Si5 C39 106.43(10) . . C40 Si5 C41 107.19(10) . . C39 Si5 C41 107.66(10) . . C40 Si5 C32 110.27(8) . . C39 Si5 C32 115.00(9) . . C41 Si5 C32 109.96(9) . . C43 Si6 C44 106.20(9) . . C43 Si6 C42 105.69(10) . . C44 Si6 C42 106.12(9) . . C43 Si6 C32 114.63(9) . . C44 Si6 C32 109.12(9) . . C42 Si6 C32 114.46(8) . . C14 C1 C2 118.90(17) . . C14 C1 Si1 119.44(14) . . C2 C1 Si1 121.65(14) . . C1 C2 C3 123.22(17) . . C1 C2 C7 119.95(19) . . C3 C2 C7 116.83(18) . . C4 C3 C2 122.1(2) . . C6 C5 C4 120.0(2) . . C5 C6 C7 121.6(2) . . C9 C8 C7 122.13(18) . . C11 C10 C9 121.39(19) . . C10 C11 C12 120.1(2) . . C13 C12 C11 120.2(2) . . C12 C13 C14 122.28(19) . . C1 C14 C13 122.94(17) . . C1 C14 C9 120.29(18) . . C13 C14 C9 116.76(18) . . C8 C7 C6 121.6(2) . . C8 C7 C2 119.40(19) . . C6 C7 C2 119.0(2) . . C28 C15 C16 118.81(17) . . C28 C15 Si2 118.58(14) . . C16 C15 Si2 122.57(14) . . C15 C16 C17 124.00(17) . . C15 C16 C21 119.85(18) . . C17 C16 C21 116.14(18) . . C18 C17 C16 122.55(19) . . C8 C9 C10 121.65(19) . . C8 C9 C14 119.07(19) . . C10 C9 C14 119.3(2) . . C3 C4 C5 120.4(2) . . C17 C18 C19 120.5(2) . . C20 C19 C18 119.7(2) . . C19 C20 C21 121.7(2) . . C22 C21 C20 121.09(19) . . C22 C21 C16 119.52(19) . . C20 C21 C16 119.4(2) . . C23 C22 C21 121.82(18) . . C22 C23 C24 121.61(19) . . C22 C23 C28 119.21(19) . . C24 C23 C28 119.2(2) . . C25 C24 C23 121.6(2) . . C24 C25 C26 119.7(2) . . C27 C26 C25 120.4(2) . . C26 C27 C28 122.25(19) . . C15 C28 C27 122.56(17) . . C15 C28 C23 120.63(19) . . C27 C28 C23 116.81(18) . . C30 C29 Si1 105.27(11) . . C30 C29 Si3 106.88(11) . . Si1 C29 Si3 112.01(9) . . C30 C29 Si4 109.63(12) . . Si1 C29 Si4 112.12(9) . . Si3 C29 Si4 110.64(8) . . C31 C30 C29 117.88(14) . . C30 C31 C32 117.26(14) . . C31 C32 Si2 104.67(11) . . C31 C32 Si5 105.69(11) . . Si2 C32 Si5 110.20(9) . . C31 C32 Si6 107.73(11) . . Si2 C32 Si6 115.21(9) . . Si5 C32 Si6 112.56(9) . . C47 C46 C51 120.0 . . C47 C46 C45 122.0(4) . . C51 C46 C45 117.9(4) . . C46 C47 C48 120.0 . . C47 C48 C49 120.0 . . C50 C49 C48 120.0 . . C49 C50 C51 120.0 . . C50 C51 C46 120.0 . . C54 C53 C58 120.0 . . C54 C53 C52 116.5(7) . . C58 C53 C52 123.5(7) . . C53 C54 C55 120.0 . . C56 C55 C54 120.0 . . C57 C56 C55 120.0 . . C56 C57 C58 120.0 . . C57 C58 C53 120.0 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Si1 C1 1.8866(18) . Si1 C29 1.8952(17) . Si1 Si2 2.1525(7) . Si2 C15 1.8883(18) . Si2 C32 1.8961(17) . Si3 C34 1.8669(19) . Si3 C35 1.8690(19) . Si3 C33 1.871(2) . Si3 C29 1.9026(18) . Si4 C36 1.8632(19) . Si4 C37 1.871(2) . Si4 C38 1.874(2) . Si4 C29 1.9158(18) . Si5 C40 1.866(2) . Si5 C39 1.868(2) . Si5 C41 1.876(2) . Si5 C32 1.9066(18) . Si6 C43 1.867(2) . Si6 C44 1.871(2) . Si6 C42 1.880(2) . Si6 C32 1.9103(18) . C1 C14 1.415(3) . C1 C2 1.418(3) . C2 C3 1.423(3) . C2 C7 1.435(3) . C3 C4 1.360(3) . C5 C6 1.342(4) . C5 C4 1.413(3) . C6 C7 1.431(3) . C8 C9 1.383(3) . C8 C7 1.384(3) . C10 C11 1.349(3) . C10 C9 1.423(3) . C11 C12 1.416(3) . C12 C13 1.358(3) . C13 C14 1.424(3) . C14 C9 1.437(3) . C15 C28 1.413(3) . C15 C16 1.415(3) . C16 C17 1.426(3) . C16 C21 1.443(3) . C17 C18 1.355(3) . C18 C19 1.419(3) . C19 C20 1.343(3) . C20 C21 1.426(3) . C21 C22 1.387(3) . C22 C23 1.381(3) . C23 C24 1.421(3) . C23 C28 1.437(3) . C24 C25 1.346(4) . C25 C26 1.420(3) . C26 C27 1.351(3) . C27 C28 1.422(3) . C29 C30 1.574(2) . C30 C31 1.550(2) . C31 C32 1.580(2) . C45 C46 1.490(7) . C46 C47 1.3900 . C46 C51 1.3900 . C47 C48 1.3900 . C48 C49 1.3900 . C49 C50 1.3900 . C50 C51 1.3900 . C52 C53 1.551(13) . C53 C54 1.3900 . C53 C58 1.3900 . C54 C55 1.3900 . C55 C56 1.3900 . C56 C57 1.3900 . C57 C58 1.3900 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C29 Si1 C1 C14 -88.77(16) . . . . Si2 Si1 C1 C14 111.67(13) . . . . C29 Si1 C1 C2 90.11(16) . . . . Si2 Si1 C1 C2 -69.45(16) . . . . C14 C1 C2 C3 -175.04(17) . . . . Si1 C1 C2 C3 6.1(2) . . . . C14 C1 C2 C7 5.7(3) . . . . Si1 C1 C2 C7 -173.19(13) . . . . C1 C2 C3 C4 -177.23(18) . . . . C7 C2 C3 C4 2.0(3) . . . . C4 C5 C6 C7 0.3(3) . . . . C9 C10 C11 C12 -0.3(3) . . . . C10 C11 C12 C13 -0.4(3) . . . . C11 C12 C13 C14 0.2(3) . . . . C2 C1 C14 C13 176.17(17) . . . . Si1 C1 C14 C13 -4.9(2) . . . . C2 C1 C14 C9 -3.1(3) . . . . Si1 C1 C14 C9 175.86(13) . . . . C12 C13 C14 C1 -178.68(18) . . . . C12 C13 C14 C9 0.6(3) . . . . C9 C8 C7 C6 178.48(19) . . . . C9 C8 C7 C2 -1.0(3) . . . . C5 C6 C7 C8 -178.0(2) . . . . C5 C6 C7 C2 1.5(3) . . . . C1 C2 C7 C8 -3.8(3) . . . . C3 C2 C7 C8 176.95(18) . . . . C1 C2 C7 C6 176.71(18) . . . . C3 C2 C7 C6 -2.6(3) . . . . C32 Si2 C15 C28 -73.85(16) . . . . Si1 Si2 C15 C28 131.41(13) . . . . C32 Si2 C15 C16 103.86(16) . . . . Si1 Si2 C15 C16 -50.87(17) . . . . C28 C15 C16 C17 -175.81(17) . . . . Si2 C15 C16 C17 6.5(3) . . . . C28 C15 C16 C21 3.5(3) . . . . Si2 C15 C16 C21 -174.16(14) . . . . C15 C16 C17 C18 178.44(19) . . . . C21 C16 C17 C18 -0.9(3) . . . . C7 C8 C9 C10 -175.94(19) . . . . C7 C8 C9 C14 3.7(3) . . . . C11 C10 C9 C8 -179.22(19) . . . . C11 C10 C9 C14 1.1(3) . . . . C1 C14 C9 C8 -1.6(3) . . . . C13 C14 C9 C8 179.13(17) . . . . C1 C14 C9 C10 178.05(17) . . . . C13 C14 C9 C10 -1.2(3) . . . . C2 C3 C4 C5 -0.3(3) . . . . C6 C5 C4 C3 -0.9(3) . . . . C16 C17 C18 C19 1.0(3) . . . . C17 C18 C19 C20 -0.1(3) . . . . C18 C19 C20 C21 -1.0(4) . . . . C19 C20 C21 C22 -178.1(2) . . . . C19 C20 C21 C16 1.0(3) . . . . C15 C16 C21 C22 -0.3(3) . . . . C17 C16 C21 C22 179.09(18) . . . . C15 C16 C21 C20 -179.49(18) . . . . C17 C16 C21 C20 -0.1(3) . . . . C20 C21 C22 C23 176.9(2) . . . . C16 C21 C22 C23 -2.2(3) . . . . C21 C22 C23 C24 -177.7(2) . . . . C21 C22 C23 C28 1.5(3) . . . . C22 C23 C24 C25 178.5(2) . . . . C28 C23 C24 C25 -0.7(3) . . . . C23 C24 C25 C26 -0.7(4) . . . . C24 C25 C26 C27 1.0(4) . . . . C25 C26 C27 C28 0.2(3) . . . . C16 C15 C28 C27 175.01(18) . . . . Si2 C15 C28 C27 -7.2(2) . . . . C16 C15 C28 C23 -4.4(3) . . . . Si2 C15 C28 C23 173.45(14) . . . . C26 C27 C28 C15 179.12(19) . . . . C26 C27 C28 C23 -1.5(3) . . . . C22 C23 C28 C15 1.9(3) . . . . C24 C23 C28 C15 -178.88(18) . . . . C22 C23 C28 C27 -177.49(18) . . . . C24 C23 C28 C27 1.7(3) . . . . C1 Si1 C29 C30 -160.35(11) . . . . Si2 Si1 C29 C30 0.57(13) . . . . C1 Si1 C29 Si3 -44.56(13) . . . . Si2 Si1 C29 Si3 116.36(7) . . . . C1 Si1 C29 Si4 80.52(12) . . . . Si2 Si1 C29 Si4 -118.57(7) . . . . Si1 C29 C30 C31 -49.45(17) . . . . Si3 C29 C30 C31 -168.72(12) . . . . Si4 C29 C30 C31 71.33(16) . . . . C29 C30 C31 C32 95.83(18) . . . . C30 C31 C32 Si2 -59.10(17) . . . . C30 C31 C32 Si5 -175.47(12) . . . . C30 C31 C32 Si6 63.99(16) . . . . C15 Si2 C32 C31 -149.44(11) . . . . Si1 Si2 C32 C31 7.90(13) . . . . C15 Si2 C32 Si5 -36.23(13) . . . . Si1 Si2 C32 Si5 121.11(7) . . . . C15 Si2 C32 Si6 92.45(11) . . . . Si1 Si2 C32 Si6 -110.21(8) . . . . C51 C46 C47 C48 0.0 . . . . C45 C46 C47 C48 176.6(5) . . . . C46 C47 C48 C49 0.0 . . . . C47 C48 C49 C50 0.0 . . . . C48 C49 C50 C51 0.0 . . . . C49 C50 C51 C46 0.0 . . . . C47 C46 C51 C50 0.0 . . . . C45 C46 C51 C50 -176.7(5) . . . . C58 C53 C54 C55 0.0 . . . . C52 C53 C54 C55 -179.3(10) . . . . C53 C54 C55 C56 0.0 . . . . C54 C55 C56 C57 0.0 . . . . C55 C56 C57 C58 0.0 . . . . C56 C57 C58 C53 0.0 . . . . C54 C53 C58 C57 0.0 . . . . C52 C53 C58 C57 179.2(10) . . . .