#------------------------------------------------------------------------------ #$Date: 2019-12-16 11:43:06 +0200 (Mon, 16 Dec 2019) $ #$Revision: 245209 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/65/1556589.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556589 loop_ _publ_author_name 'Akasaka, N.' 'Tanaka, K.' 'Ishida, S.' 'Iwamoto, T.' _publ_section_title ; Synthesis and Functionalization of a 1,2-Bis(trimethylsilyl)-1,2-disilacyclohexene That Can Serve as a Unit of cis-1,2-Dialkyldisilene ; _journal_name_full Inorganics _journal_page_first 21 _journal_paper_doi 10.3390/inorganics6010021 _journal_volume 6 _journal_year 2018 _chemical_formula_sum 'C38 H98 O0 Si14' _chemical_formula_weight 948.42 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _cell_angle_alpha 84.8020(10) _cell_angle_beta 75.9110(10) _cell_angle_gamma 71.9750(10) _cell_formula_units_Z 2 _cell_length_a 11.4093(11) _cell_length_b 15.6821(15) _cell_length_c 19.5623(19) _cell_measurement_reflns_used 9890 _cell_measurement_temperature 173(2) _cell_measurement_theta_max 27.94 _cell_measurement_theta_min 2.41 _cell_volume 3227.8(5) _computing_cell_refinement 'APEX2 (Bruker AXS, 2006)' _computing_data_collection 'APEX2 (Bruker AXS, 2006)' _computing_data_reduction 'SAINT (Bruker AXS, 2004)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1997)' _diffrn_ambient_temperature 173(2) _diffrn_detector_area_resol_mean 8.333 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measurement_device_type 'Bruker APEXII CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator 'Bruker Helios multilayer confocal mirror' _diffrn_radiation_source 'Bruker TXS fine-focus rotating anode' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0150 _diffrn_reflns_av_unetI/netI 0.0172 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 37595 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.500 _diffrn_reflns_theta_min 1.723 _exptl_absorpt_coefficient_mu 0.300 _exptl_absorpt_correction_T_max 0.9706 _exptl_absorpt_correction_T_min 0.9564 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details ; SADABS Sheldrick 1996 ; _exptl_crystal_colour red _exptl_crystal_density_diffrn 0.976 _exptl_crystal_description block _exptl_crystal_F_000 1044 _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.338 _refine_diff_density_min -0.190 _refine_diff_density_rms 0.040 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.039 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 500 _refine_ls_number_reflns 14622 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.039 _refine_ls_R_factor_all 0.0309 _refine_ls_R_factor_gt 0.0266 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0390P)^2^+0.7796P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0716 _refine_ls_wR_factor_ref 0.0759 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 13006 _reflns_number_total 14622 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file Cpd8_si358a_r171216_sq_final.cif _cod_data_source_block si358a_r171214_sq _cod_database_code 1556589 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.956 _shelx_estimated_absorpt_t_max 0.971 _shelx_res_file ; si358a_r171214_sq.res created by SHELXL-2014/7 TITL REM Yadorkari-X generated CELL 0.71073 11.4093 15.6821 19.5623 84.8020 75.9110 71.9750 ZERR 2.0 0.0011 0.0015 0.0019 0.0010 0.0010 0.0010 LATT 1 REM SPGR P-1 triclinic SFAC C H O Si UNIT 76 196 0 28 SIZE 0.15 0.10 0.10 TEMP -100.0 L.S. 10 FMAP 2 PLAN -25 ACTA CONF 2.5 LIST 4 MERG 2 OMIT -10.000000 55.000000 OMIT 0 -2 6 OMIT -3 3 3 OMIT 1 9 6 OMIT 3 3 1 OMIT -3 -1 5 OMIT -2 2 4 OMIT 4 -1 3 OMIT 3 0 2 OMIT -4 -1 5 OMIT -2 4 2 OMIT 0 -2 3 OMIT 0 -1 2 ABIN WGHT 0.039000 0.779600 FVAR 0.45364 0.63769 SI1 4 -0.120835 0.903102 0.241227 11.00000 0.02202 0.02790 = 0.02374 0.00164 -0.00816 -0.00764 SI2 4 0.034815 0.803816 0.277257 11.00000 0.02083 0.02864 = 0.02051 -0.00092 -0.00721 -0.00645 SI3 4 0.133166 0.669095 0.216550 11.00000 0.01957 0.02742 = 0.02157 -0.00010 -0.00253 -0.00909 SI4 4 0.057201 0.555434 0.247791 11.00000 0.02294 0.02898 = 0.02513 0.00201 -0.00426 -0.01087 SI5 4 -0.205566 0.881344 0.148085 11.00000 0.02726 0.04162 = 0.02854 0.00139 -0.01353 -0.00796 SI6 4 -0.134523 0.561902 0.329963 11.00000 0.02688 0.03817 = 0.03705 0.00683 -0.00098 -0.01449 C1 1 -0.184379 1.012541 0.292113 11.00000 0.02235 0.02822 = 0.02806 0.00064 -0.00579 -0.00667 C2 1 -0.083974 1.009465 0.336023 11.00000 0.02582 0.03193 = 0.03394 -0.00488 -0.00792 -0.00828 AFIX 23 H1 2 -0.003865 1.010703 0.302653 11.00000 -1.20000 H2 2 -0.114586 1.064496 0.364368 11.00000 -1.20000 AFIX 0 C3 1 -0.055127 0.927439 0.386092 11.00000 0.02506 0.03824 = 0.02430 -0.00677 -0.00623 -0.00569 AFIX 23 H3 2 -0.129874 0.904967 0.398336 11.00000 -1.20000 H4 2 -0.046245 0.948590 0.430202 11.00000 -1.20000 AFIX 0 C4 1 0.065239 0.845538 0.359406 11.00000 0.02267 0.03477 = 0.02193 -0.00368 -0.00758 -0.00665 C5 1 0.158163 0.448023 0.198522 11.00000 0.02576 0.02614 = 0.02780 0.00246 -0.00950 -0.00856 C6 1 0.287541 0.465141 0.160682 11.00000 0.02418 0.03038 = 0.02989 -0.00091 -0.00829 -0.00685 AFIX 23 H5 2 0.330159 0.472266 0.197311 11.00000 -1.20000 H6 2 0.342017 0.411119 0.133585 11.00000 -1.20000 AFIX 0 C7 1 0.279023 0.547375 0.110250 11.00000 0.02524 0.03191 = 0.02289 -0.00262 -0.00346 -0.00942 AFIX 23 H7 2 0.200056 0.559958 0.093495 11.00000 -1.20000 H8 2 0.350461 0.530494 0.068615 11.00000 -1.20000 AFIX 0 C8 1 0.280742 0.637359 0.139567 11.00000 0.02076 0.03118 = 0.02175 -0.00171 -0.00215 -0.01005 C9 1 -0.124050 0.924875 0.062991 11.00000 0.05585 0.06869 = 0.03287 0.01250 -0.01639 -0.01517 AFIX 137 H9 2 -0.139387 0.989565 0.066278 11.00000 -1.50000 H10 2 -0.157427 0.913313 0.024250 11.00000 -1.50000 H11 2 -0.032847 0.894435 0.054095 11.00000 -1.50000 AFIX 0 C10 1 -0.380826 0.935728 0.165504 11.00000 0.03189 0.06460 = 0.05654 -0.00706 -0.02211 -0.00383 AFIX 137 H12 2 -0.421905 0.910646 0.209099 11.00000 -1.50000 H13 2 -0.412936 0.924500 0.126129 11.00000 -1.50000 H14 2 -0.399345 1.000496 0.170398 11.00000 -1.50000 AFIX 0 C11 1 -0.181343 0.759467 0.138493 11.00000 0.03931 0.04838 = 0.04793 -0.00649 -0.01863 -0.01458 AFIX 137 H15 2 -0.196953 0.749616 0.093171 11.00000 -1.50000 H16 2 -0.240197 0.739139 0.176897 11.00000 -1.50000 H17 2 -0.094149 0.725597 0.140371 11.00000 -1.50000 AFIX 0 SI7 4 -0.181559 1.113967 0.230546 11.00000 0.03202 0.02835 = 0.04092 0.00535 -0.00499 -0.00840 C12 1 -0.018728 1.097365 0.173622 11.00000 0.04177 0.04012 = 0.05726 0.01194 0.00115 -0.01454 AFIX 137 H18 2 -0.022027 1.141508 0.134782 11.00000 -1.50000 H19 2 0.013749 1.036742 0.154471 11.00000 -1.50000 H20 2 0.037326 1.105155 0.201815 11.00000 -1.50000 AFIX 0 C13 1 -0.289116 1.141105 0.167784 11.00000 0.05016 0.04855 = 0.05024 0.01858 -0.01646 -0.00940 AFIX 137 H21 2 -0.269699 1.089317 0.137970 11.00000 -1.50000 H22 2 -0.276624 1.192798 0.138110 11.00000 -1.50000 H23 2 -0.377287 1.155395 0.194444 11.00000 -1.50000 AFIX 0 C14 1 -0.224927 1.216815 0.284638 11.00000 0.05636 0.03220 = 0.06925 -0.00298 -0.00365 -0.01458 AFIX 137 H24 2 -0.226703 1.269408 0.253307 11.00000 -1.50000 H25 2 -0.162077 1.209857 0.312721 11.00000 -1.50000 H26 2 -0.308634 1.224855 0.316115 11.00000 -1.50000 AFIX 0 SI8 4 -0.346322 1.024983 0.354722 11.00000 0.02204 0.03743 = 0.03038 0.00072 -0.00430 -0.00507 C15 1 -0.484350 1.100019 0.321368 11.00000 0.02761 0.05225 = 0.05055 0.00474 -0.00849 -0.00212 AFIX 137 H27 2 -0.474126 1.160031 0.311571 11.00000 -1.50000 H28 2 -0.562641 1.103807 0.357083 11.00000 -1.50000 H29 2 -0.488537 1.075500 0.277991 11.00000 -1.50000 AFIX 0 C16 1 -0.354186 1.075209 0.439346 11.00000 0.03863 0.07499 = 0.03834 -0.01677 -0.00137 -0.00540 AFIX 137 H30 2 -0.293145 1.033777 0.463735 11.00000 -1.50000 H31 2 -0.439713 1.086172 0.469246 11.00000 -1.50000 H32 2 -0.333827 1.132031 0.429452 11.00000 -1.50000 AFIX 0 C17 1 -0.382782 0.915749 0.376284 11.00000 0.02942 0.04943 = 0.05153 0.00860 -0.00123 -0.01442 AFIX 137 H33 2 -0.469189 0.926796 0.405047 11.00000 -1.50000 H34 2 -0.322890 0.876738 0.402546 11.00000 -1.50000 H35 2 -0.375339 0.886575 0.332538 11.00000 -1.50000 AFIX 0 SI9 4 0.212597 0.885578 0.340642 11.00000 0.02427 0.03888 = 0.03424 -0.00753 -0.01024 -0.00959 C18 1 0.251851 0.934711 0.250088 11.00000 0.02976 0.05564 = 0.04689 0.00033 -0.00553 -0.01881 AFIX 137 H36 2 0.236666 0.899774 0.215855 11.00000 -1.50000 H37 2 0.341060 0.933080 0.238156 11.00000 -1.50000 H38 2 0.198352 0.996972 0.248902 11.00000 -1.50000 AFIX 0 C19 1 0.188644 0.978736 0.401400 11.00000 0.04477 0.05233 = 0.05573 -0.01759 -0.01733 -0.01570 AFIX 137 H39 2 0.268402 0.992876 0.395646 11.00000 -1.50000 H40 2 0.161226 0.959858 0.450286 11.00000 -1.50000 H41 2 0.123812 1.032057 0.389955 11.00000 -1.50000 AFIX 0 C20 1 0.357444 0.793888 0.352237 11.00000 0.02741 0.05267 = 0.05534 -0.00481 -0.01482 -0.00817 AFIX 137 H42 2 0.347526 0.774913 0.401907 11.00000 -1.50000 H43 2 0.431502 0.815931 0.337632 11.00000 -1.50000 H44 2 0.369147 0.742810 0.323243 11.00000 -1.50000 AFIX 0 SI10 4 0.062277 0.762848 0.437698 11.00000 0.03109 0.04327 = 0.02061 0.00071 -0.00910 -0.00825 C21 1 -0.102866 0.756219 0.474030 11.00000 0.04035 0.06222 = 0.03235 0.01068 -0.00696 -0.01803 AFIX 137 H45 2 -0.100920 0.705828 0.507685 11.00000 -1.50000 H46 2 -0.138490 0.747222 0.435404 11.00000 -1.50000 H47 2 -0.155425 0.812145 0.497974 11.00000 -1.50000 AFIX 0 C22 1 0.105904 0.803041 0.513216 11.00000 0.04907 0.06484 = 0.02641 -0.00441 -0.01528 -0.01214 AFIX 137 H48 2 0.193042 0.806030 0.498581 11.00000 -1.50000 H49 2 0.099059 0.761242 0.553337 11.00000 -1.50000 H50 2 0.048308 0.862761 0.527018 11.00000 -1.50000 AFIX 0 C23 1 0.168303 0.646427 0.418660 11.00000 0.04596 0.04318 = 0.03004 0.00658 -0.01141 -0.00853 AFIX 137 H51 2 0.150616 0.623719 0.378402 11.00000 -1.50000 H52 2 0.153290 0.607756 0.460047 11.00000 -1.50000 H53 2 0.256762 0.646578 0.407519 11.00000 -1.50000 AFIX 0 C24 1 -0.102559 0.529070 0.419901 11.00000 0.05663 0.06109 = 0.03638 0.01486 0.00083 -0.01841 AFIX 137 H54 2 -0.182288 0.531468 0.453920 11.00000 -1.50000 H55 2 -0.064092 0.570634 0.433902 11.00000 -1.50000 H56 2 -0.044615 0.467973 0.418822 11.00000 -1.50000 AFIX 0 C25 1 -0.219294 0.487497 0.307089 11.00000 0.03702 0.05640 = 0.08028 0.00274 -0.00748 -0.02607 AFIX 137 H57 2 -0.235468 0.503636 0.259942 11.00000 -1.50000 H58 2 -0.299894 0.495028 0.341603 11.00000 -1.50000 H59 2 -0.166921 0.424855 0.307741 11.00000 -1.50000 AFIX 0 C26 1 -0.246698 0.677335 0.332682 11.00000 0.03241 0.04648 = 0.05294 0.00468 0.00062 -0.00960 AFIX 137 H60 2 -0.311590 0.684819 0.376805 11.00000 -1.50000 H61 2 -0.287125 0.686705 0.292658 11.00000 -1.50000 H62 2 -0.200410 0.721225 0.330015 11.00000 -1.50000 AFIX 0 SI11 4 0.205708 0.349674 0.261383 11.00000 0.04040 0.03310 = 0.03627 0.00952 -0.01851 -0.01102 C27 1 0.287032 0.378370 0.324299 11.00000 0.08273 0.06524 = 0.05564 0.02458 -0.04655 -0.03499 AFIX 137 H63 2 0.297233 0.331535 0.360988 11.00000 -1.50000 H64 2 0.236083 0.436006 0.346077 11.00000 -1.50000 H65 2 0.370423 0.382617 0.298821 11.00000 -1.50000 AFIX 0 C28 1 0.318624 0.251594 0.208137 11.00000 0.06200 0.04023 = 0.06245 0.00753 -0.02329 0.00758 AFIX 137 H66 2 0.338814 0.199219 0.239323 11.00000 -1.50000 H67 2 0.396474 0.266174 0.184635 11.00000 -1.50000 H68 2 0.279555 0.238165 0.172644 11.00000 -1.50000 AFIX 0 C29 1 0.076412 0.307921 0.318243 11.00000 0.06346 0.04616 = 0.05302 0.02163 -0.01919 -0.02351 AFIX 137 H69 2 0.013651 0.357210 0.346640 11.00000 -1.50000 H70 2 0.112351 0.259638 0.349461 11.00000 -1.50000 H71 2 0.035591 0.285073 0.288375 11.00000 -1.50000 AFIX 0 SI12 4 0.081788 0.419952 0.129690 11.00000 0.03032 0.02772 = 0.03153 0.00164 -0.01262 -0.01102 C30 1 0.205329 0.374464 0.048749 11.00000 0.04340 0.04255 = 0.03601 -0.00722 -0.01210 -0.00844 AFIX 137 H72 2 0.166182 0.356098 0.015503 11.00000 -1.50000 H73 2 0.270591 0.322540 0.061664 11.00000 -1.50000 H74 2 0.243942 0.420923 0.026672 11.00000 -1.50000 AFIX 0 C31 1 -0.002489 0.333145 0.158550 11.00000 0.05938 0.04511 = 0.05612 0.00809 -0.02551 -0.03143 AFIX 137 H75 2 0.057449 0.276961 0.170029 11.00000 -1.50000 H76 2 -0.038432 0.323022 0.120421 11.00000 -1.50000 H77 2 -0.070610 0.353998 0.200311 11.00000 -1.50000 AFIX 0 C32 1 -0.039535 0.519100 0.102111 11.00000 0.03531 0.03851 = 0.04228 0.00121 -0.02041 -0.00967 AFIX 137 H78 2 -0.079365 0.499847 0.069672 11.00000 -1.50000 H79 2 0.001403 0.563716 0.078438 11.00000 -1.50000 H80 2 -0.104156 0.545641 0.143786 11.00000 -1.50000 AFIX 0 SI13 4 0.269790 0.718130 0.060176 11.00000 0.02837 0.03628 = 0.02194 0.00177 -0.00107 -0.01190 C33 1 0.229562 0.839075 0.080339 11.00000 0.05093 0.03851 = 0.03362 0.00426 -0.00402 -0.01457 AFIX 137 H81 2 0.151615 0.856136 0.117320 11.00000 -1.50000 H82 2 0.217112 0.875379 0.037740 11.00000 -1.50000 H83 2 0.298801 0.849316 0.096563 11.00000 -1.50000 AFIX 0 C34 1 0.422478 0.690209 -0.008882 11.00000 0.03845 0.05600 = 0.02886 0.00142 0.00495 -0.01482 AFIX 137 H84 2 0.489283 0.700073 0.009942 11.00000 -1.50000 H85 2 0.411441 0.728768 -0.050580 11.00000 -1.50000 H86 2 0.446230 0.627246 -0.021972 11.00000 -1.50000 AFIX 0 C35 1 0.150703 0.705192 0.013695 11.00000 0.04199 0.05313 = 0.03219 0.00940 -0.01354 -0.01757 AFIX 137 H87 2 0.135419 0.753674 -0.021359 11.00000 -1.50000 H88 2 0.071259 0.707885 0.048078 11.00000 -1.50000 H89 2 0.183222 0.647258 -0.009916 11.00000 -1.50000 AFIX 0 SI14 4 0.437208 0.616927 0.167152 11.00000 0.01960 0.04032 = 0.03128 -0.00436 -0.00367 -0.01079 C36 1 0.486357 0.721105 0.161077 11.00000 0.04202 0.06015 = 0.05897 -0.00053 -0.01482 -0.03039 AFIX 137 H90 2 0.561080 0.709120 0.180868 11.00000 -1.50000 H91 2 0.417004 0.768871 0.187616 11.00000 -1.50000 H92 2 0.506742 0.739920 0.111561 11.00000 -1.50000 AFIX 0 C37 1 0.567693 0.530094 0.109906 11.00000 0.02532 0.06107 = 0.04664 -0.01131 -0.00201 -0.00468 AFIX 137 H93 2 0.648749 0.525828 0.120812 11.00000 -1.50000 H94 2 0.570951 0.547364 0.060220 11.00000 -1.50000 H95 2 0.551395 0.471829 0.118847 11.00000 -1.50000 AFIX 0 C38 1 0.435963 0.571737 0.259296 11.00000 0.03280 0.05675 = 0.03687 -0.00242 -0.01514 -0.01457 AFIX 137 H96 2 0.352853 0.598934 0.289984 11.00000 -1.50000 H97 2 0.501327 0.586141 0.276487 11.00000 -1.50000 H98 2 0.453057 0.506510 0.259589 11.00000 -1.50000 AFIX 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM REM R1 = 0.0266 for 13006 Fo > 4sig(Fo) and 0.0309 for all 14622 data REM 500 parameters refined using 0 restraints END WGHT 0.0390 0.7795 REM Highest difference peak 0.338, deepest hole -0.190, 1-sigma level 0.040 Q1 1 -0.1853 0.6149 0.3354 11.00000 0.05 0.34 Q2 1 0.1217 0.7021 0.4272 11.00000 0.05 0.33 Q3 1 0.0180 0.4782 0.1151 11.00000 0.05 0.33 Q4 1 0.1533 0.3989 0.0844 11.00000 0.05 0.32 Q5 1 0.1680 0.4092 0.2297 11.00000 0.05 0.31 Q6 1 0.1181 0.4909 0.2228 11.00000 0.05 0.31 Q7 1 0.2481 0.7778 0.0755 11.00000 0.05 0.30 Q8 1 0.2783 0.6776 0.0994 11.00000 0.05 0.30 Q9 1 0.2026 0.7068 0.0391 11.00000 0.05 0.30 Q10 1 -0.1539 0.9543 0.2661 11.00000 0.05 0.30 Q11 1 -0.1989 1.1682 0.2570 11.00000 0.05 0.29 Q12 1 -0.2960 0.9142 0.1593 11.00000 0.05 0.29 Q13 1 -0.3481 1.0572 0.3878 11.00000 0.05 0.29 Q14 1 -0.0707 0.9703 0.3611 11.00000 0.05 0.29 Q15 1 0.4600 0.6757 0.1627 11.00000 0.05 0.29 Q16 1 0.3575 0.6940 0.0238 11.00000 0.05 0.29 Q17 1 0.2129 0.9307 0.3683 11.00000 0.05 0.28 Q18 1 0.5045 0.5696 0.1362 11.00000 0.05 0.28 Q19 1 0.4370 0.5894 0.2111 11.00000 0.05 0.28 Q20 1 0.1186 0.4451 0.1627 11.00000 0.05 0.28 Q21 1 0.0426 0.3710 0.1513 11.00000 0.05 0.27 Q22 1 -0.1657 0.5199 0.3134 11.00000 0.05 0.27 Q23 1 -0.2359 1.1289 0.1973 11.00000 0.05 0.27 Q24 1 -0.1631 0.8880 0.1993 11.00000 0.05 0.27 Q25 1 -0.1892 0.8107 0.1359 11.00000 0.05 0.27 ; _shelx_res_checksum 89008 _shelx_hkl_file ; 1 0 0 3858.31 63.99 1 0 0 3810.32 56.09 1 0 0 3778.32 53.99 1 0 0 3854.21 68.59 2 0 0 364.66 5.70 2 0 0 365.16 5.50 2 0 0 361.76 5.30 2 0 0 374.56 5.40 3 0 0 1755.52 25.80 3 0 0 1751.42 26.30 3 0 0 1753.72 26.50 3 0 0 1808.62 25.90 4 0 0 5.90 0.50 4 0 0 5.80 0.60 4 0 0 5.50 0.50 4 0 0 4.50 0.50 5 0 0 1.00 0.40 5 0 0 0.40 0.40 5 0 0 0.90 0.40 5 0 0 0.60 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1.80 1.20 10 -8 0 59.59 3.70 9 -8 0 44.00 2.50 9 -8 0 48.40 3.30 -9 8 0 43.50 2.10 8 -8 0 132.99 4.80 8 -8 0 127.49 4.00 -8 8 0 128.59 3.50 7 -8 0 33.40 2.00 7 -8 0 31.80 2.50 -7 8 0 35.60 1.70 6 -8 0 139.59 3.80 6 -8 0 143.59 4.40 -6 8 0 141.19 3.40 5 -8 0 311.67 6.20 5 -8 0 316.37 7.00 -5 8 0 307.97 5.80 4 -8 0 334.47 7.00 4 -8 0 324.27 6.20 -4 8 0 336.07 6.00 3 -8 0 84.59 2.80 3 -8 0 79.09 2.30 -3 8 0 82.89 2.20 2 -8 0 92.69 2.80 2 -8 0 95.89 2.50 -2 8 0 99.69 2.40 1 -8 0 999.50 16.00 1 -8 0 1012.20 15.10 -1 8 0 1012.10 15.00 -1 8 0 1014.90 13.90 0 -8 0 43.60 1.60 0 -8 0 43.70 1.40 0 8 0 43.70 1.10 0 8 0 43.30 1.40 -1 -8 0 9.80 0.70 -1 -8 0 9.30 0.70 1 8 0 9.40 0.60 1 8 0 8.60 0.70 -2 -8 0 1606.74 23.20 -2 -8 0 1600.24 23.70 2 8 0 1617.74 23.10 2 8 0 1610.64 22.70 -3 -8 0 546.45 8.70 -3 -8 0 555.44 8.50 3 8 0 544.15 8.60 3 8 0 553.34 8.70 -4 -8 0 30.30 1.40 -4 -8 0 29.60 0.90 4 8 0 31.80 1.40 4 8 0 31.40 1.30 -5 -8 0 277.67 5.30 -5 -8 0 280.17 4.40 5 8 0 275.07 5.10 5 8 0 279.87 5.30 -6 -8 0 19.90 1.40 6 8 0 19.40 1.30 6 8 0 20.20 1.20 -7 -8 0 368.96 7.00 7 8 0 367.26 6.60 7 8 0 362.16 7.00 -8 -8 0 572.94 10.00 8 8 0 543.25 9.30 8 8 0 560.74 10.00 -9 -8 0 122.69 3.70 9 8 0 117.39 3.70 9 8 0 117.59 3.20 -10 -8 0 396.86 8.20 10 8 0 409.26 8.30 -11 -8 0 169.18 4.90 11 8 0 165.28 4.90 -12 -8 0 75.69 3.50 12 8 0 74.59 3.50 -13 -8 0 21.30 2.30 13 8 0 19.40 2.10 -14 -8 0 4.10 1.50 14 8 0 2.80 1.30 10 -9 0 73.49 4.20 9 -9 0 10.80 1.80 -9 9 0 11.20 1.30 8 -9 0 6.40 1.60 8 -9 0 6.20 1.20 -8 9 0 8.20 1.10 7 -9 0 1.30 0.80 7 -9 0 1.90 1.20 -7 9 0 1.10 0.70 6 -9 0 154.48 4.10 6 -9 0 157.98 4.80 -6 9 0 147.19 3.70 5 -9 0 108.39 3.20 5 -9 0 109.89 3.80 -5 9 0 109.39 2.90 4 -9 0 366.86 6.90 4 -9 0 369.56 7.70 -4 9 0 363.26 6.60 3 -9 0 910.71 14.30 3 -9 0 902.31 15.40 -3 9 0 927.41 14.00 2 -9 0 120.29 3.00 2 -9 0 118.19 3.30 -2 9 0 123.09 2.90 1 -9 0 626.34 9.90 1 -9 0 620.34 10.60 -1 9 0 608.94 9.80 0 -9 0 2041.30 30.30 0 -9 0 2007.40 29.00 0 9 0 2004.10 28.80 0 9 0 2030.80 27.90 -1 -9 0 1764.42 26.20 -1 -9 0 1719.53 25.20 1 9 0 1776.52 24.50 1 9 0 1752.82 25.20 -2 -9 0 1.10 0.40 -2 -9 0 0.50 0.40 2 9 0 0.60 0.30 2 9 0 0.40 0.40 -3 -9 0 124.59 2.80 -3 -9 0 124.09 2.50 3 9 0 125.09 2.90 3 9 0 127.39 2.80 -4 -9 0 0.30 0.50 -4 -9 0 -0.10 0.20 4 9 0 0.20 0.40 4 9 0 0.20 0.40 -5 -9 0 9.10 1.00 5 9 0 6.50 0.80 5 9 0 9.40 0.90 -6 -9 0 57.99 2.20 6 9 0 58.09 2.20 6 9 0 59.69 2.00 -7 -9 0 395.86 7.50 7 9 0 402.76 7.20 7 9 0 402.36 7.60 -8 -9 0 138.69 3.80 8 9 0 138.49 3.50 8 9 0 140.59 3.90 -9 -9 0 3.00 1.00 9 9 0 4.10 0.80 9 9 0 3.30 1.00 -10 -9 0 14.20 1.60 10 9 0 15.30 1.70 -11 -9 0 358.26 7.90 11 9 0 361.86 8.00 -12 -9 0 200.08 5.70 12 9 0 210.58 5.90 -13 -9 0 22.10 2.30 13 9 0 16.00 2.00 -14 -9 0 4.80 1.60 14 9 0 7.70 1.70 9 -10 0 25.50 2.70 -9 10 0 25.40 1.90 8 -10 0 22.60 2.00 8 -10 0 16.10 2.30 -8 10 0 18.50 1.60 7 -10 0 31.00 2.70 7 -10 0 28.90 2.10 -7 10 0 33.10 1.80 6 -10 0 30.10 2.40 6 -10 0 33.10 2.10 -6 10 0 33.90 1.80 5 -10 0 228.48 6.00 5 -10 0 224.18 5.20 -5 10 0 226.78 4.90 4 -10 0 0.50 0.60 4 -10 0 2.00 0.90 -4 10 0 0.70 0.60 3 -10 0 102.59 3.40 3 -10 0 100.49 2.90 -3 10 0 97.39 2.70 2 -10 0 7.30 0.90 2 -10 0 5.50 1.00 -2 10 0 5.70 0.70 1 -10 0 138.49 3.60 1 -10 0 137.39 3.20 -1 10 0 134.49 3.20 0 -10 0 35.10 1.40 0 -10 0 33.80 1.60 0 10 0 33.10 1.40 -1 -10 0 3.00 0.70 -1 -10 0 3.70 0.60 1 10 0 4.50 0.70 1 10 0 4.20 0.50 -2 -10 0 119.99 2.70 -2 -10 0 118.59 2.70 2 10 0 123.49 2.70 2 10 0 118.99 2.90 -3 -10 0 17.50 0.90 -3 -10 0 19.20 1.10 3 10 0 17.40 1.10 3 10 0 18.30 1.00 -4 -10 0 7.70 0.60 -4 -10 0 6.70 0.80 4 10 0 6.50 0.80 4 10 0 5.00 0.70 -5 -10 0 51.49 2.00 5 10 0 51.59 2.00 5 10 0 50.49 1.90 -6 -10 0 132.39 3.50 6 10 0 135.09 3.40 6 10 0 130.39 3.50 -7 -10 0 94.49 3.00 7 10 0 92.19 2.70 7 10 0 87.49 2.90 -8 -10 0 14.60 1.50 8 10 0 13.60 1.30 8 10 0 12.10 1.40 -9 -10 0 85.59 3.10 9 10 0 80.89 2.70 9 10 0 79.29 3.10 -10 -10 0 95.89 3.40 10 10 0 95.59 3.60 -11 -10 0 40.40 2.70 11 10 0 47.70 2.70 -12 -10 0 8.70 1.70 12 10 0 10.50 1.80 -13 -10 0 95.79 4.10 13 10 0 102.09 4.30 -14 -10 0 91.79 4.20 14 10 0 89.59 4.30 9 -11 0 5.10 1.80 -9 11 0 5.20 1.10 8 -11 0 18.10 2.30 -8 11 0 19.30 1.70 7 -11 0 1.80 1.00 7 -11 0 -2.60 1.10 -7 11 0 -1.00 0.70 6 -11 0 5.10 1.50 6 -11 0 8.20 1.30 -6 11 0 7.70 1.10 5 -11 0 2.40 0.90 5 -11 0 5.10 1.30 -5 11 0 3.90 0.90 4 -11 0 114.99 3.90 4 -11 0 115.19 3.40 -4 11 0 115.49 3.20 3 -11 0 0.80 0.90 3 -11 0 1.60 0.60 -3 11 0 1.30 0.60 2 -11 0 1.30 0.60 2 -11 0 -0.20 0.60 -2 11 0 0.80 0.60 1 -11 0 298.97 6.30 1 -11 0 308.67 5.80 0 -11 0 314.77 6.20 0 -11 0 303.77 5.70 0 11 0 313.27 5.90 -1 -11 0 369.06 6.80 -1 -11 0 356.76 6.40 1 11 0 358.06 6.50 -2 -11 0 0.60 0.50 -2 -11 0 0.80 0.50 2 11 0 0.50 0.40 2 11 0 0.50 0.50 -3 -11 0 17.80 1.00 -3 -11 0 18.90 1.20 3 11 0 14.20 1.10 3 11 0 16.90 1.20 -4 -11 0 77.69 2.40 4 11 0 74.39 2.40 4 11 0 77.39 2.40 -5 -11 0 67.09 2.30 5 11 0 67.59 2.30 5 11 0 64.49 2.30 -6 -11 0 107.69 3.10 6 11 0 101.79 3.10 6 11 0 101.29 3.00 -7 -11 0 328.67 6.50 7 11 0 323.87 6.40 7 11 0 308.37 6.50 -8 -11 0 0.40 0.80 8 11 0 -1.00 0.70 8 11 0 0.80 0.60 -9 -11 0 63.59 2.70 9 11 0 64.09 2.60 9 11 0 65.79 2.80 -10 -11 0 2.00 1.10 10 11 0 0.20 0.90 -11 -11 0 -1.50 1.10 11 11 0 1.40 1.00 -12 -11 0 3.90 1.50 12 11 0 7.50 1.60 -13 -11 0 19.50 2.30 13 11 0 18.80 2.30 -14 -11 0 -2.40 1.30 8 -12 0 3.40 1.50 -8 12 0 2.90 1.10 7 -12 0 79.29 4.10 -7 12 0 79.79 3.00 6 -12 0 105.49 4.40 6 -12 0 100.89 3.60 -6 12 0 102.99 3.30 5 -12 0 168.48 4.60 5 -12 0 173.18 5.40 -5 12 0 184.78 4.50 4 -12 0 325.47 6.80 4 -12 0 324.77 7.70 -4 12 0 340.97 6.70 3 -12 0 3.20 0.80 3 -12 0 2.00 0.90 -3 12 0 1.90 0.70 2 -12 0 256.47 5.50 2 -12 0 262.17 6.10 -2 12 0 264.57 5.40 1 -12 0 24.40 1.50 1 -12 0 29.80 1.80 -1 12 0 24.90 1.50 0 -12 0 14.80 1.30 0 -12 0 12.70 1.10 0 12 0 13.90 1.20 -1 -12 0 131.69 3.20 -1 -12 0 135.89 3.50 1 12 0 130.69 3.30 -2 -12 0 48.10 1.70 -2 -12 0 46.20 1.80 2 12 0 43.40 1.90 -3 -12 0 29.80 1.40 3 12 0 28.00 1.40 3 12 0 28.80 1.50 -4 -12 0 11.60 1.10 4 12 0 10.50 1.10 4 12 0 11.40 1.10 -5 -12 0 20.50 1.50 5 12 0 16.60 1.30 5 12 0 17.40 1.30 -6 -12 0 86.99 2.80 6 12 0 85.99 2.80 6 12 0 85.09 2.80 -7 -12 0 129.09 3.70 7 12 0 128.19 3.60 7 12 0 120.79 3.70 -8 -12 0 269.67 6.00 8 12 0 273.57 5.90 8 12 0 271.57 6.20 -9 -12 0 22.10 2.00 9 12 0 27.70 1.90 9 12 0 23.10 1.90 -10 -12 0 94.09 3.60 10 12 0 93.99 3.70 -11 -12 0 18.00 1.90 11 12 0 20.40 2.10 -12 -12 0 131.89 4.60 12 12 0 134.39 4.80 -13 -12 0 215.98 6.20 13 12 0 213.38 6.40 -8 13 0 6.20 1.30 7 -13 0 8.20 1.80 -7 13 0 5.30 1.10 6 -13 0 99.19 3.70 6 -13 0 100.09 4.50 -6 13 0 96.79 3.30 5 -13 0 11.70 1.50 5 -13 0 8.50 1.60 -5 13 0 10.90 1.40 4 -13 0 36.00 2.10 4 -13 0 33.50 2.70 -4 13 0 30.40 1.90 3 -13 0 44.30 2.20 3 -13 0 47.50 2.70 -3 13 0 43.60 2.20 2 -13 0 44.20 2.30 2 -13 0 46.30 2.10 -2 13 0 43.00 2.00 1 -13 0 69.69 2.50 1 -13 0 69.69 2.80 -1 13 0 66.69 2.40 0 -13 0 108.89 3.10 0 -13 0 113.19 3.50 0 13 0 117.39 3.30 -1 -13 0 175.48 4.00 -1 -13 0 171.18 4.20 1 13 0 170.68 4.10 -2 -13 0 229.68 4.70 -2 -13 0 225.28 4.80 2 13 0 214.38 4.80 -3 -13 0 97.89 2.70 3 13 0 92.59 2.90 -4 -13 0 256.37 5.20 4 13 0 268.17 5.30 4 13 0 262.37 5.60 -5 -13 0 745.13 12.10 5 13 0 742.03 12.40 5 13 0 734.03 12.10 -6 -13 0 57.09 2.40 6 13 0 58.59 2.40 6 13 0 54.49 2.40 -7 -13 0 246.18 5.50 7 13 0 238.08 5.60 7 13 0 239.78 5.40 -8 -13 0 64.19 2.70 8 13 0 70.29 2.70 8 13 0 69.19 2.90 -9 -13 0 15.60 1.70 9 13 0 15.10 1.70 -10 -13 0 -0.30 0.90 10 13 0 1.40 1.10 -11 -13 0 0.70 1.20 11 13 0 0.00 1.00 -12 -13 0 -1.60 1.10 12 13 0 0.30 1.10 -13 -13 0 7.40 1.80 13 13 0 8.10 1.70 7 -14 0 18.60 2.80 -7 14 0 22.90 2.00 6 -14 0 114.09 4.90 -6 14 0 114.49 3.80 5 -14 0 124.09 4.10 5 -14 0 124.19 4.80 -5 14 0 129.69 4.00 4 -14 0 3.50 1.40 4 -14 0 4.50 1.10 -4 14 0 4.40 1.10 3 -14 0 0.50 0.80 3 -14 0 -0.60 0.90 -3 14 0 -0.80 0.80 2 -14 0 35.70 2.00 2 -14 0 32.30 2.30 -2 14 0 38.00 2.10 1 -14 0 1.80 0.70 1 -14 0 -0.10 0.80 -1 14 0 0.00 0.60 0 -14 0 6.20 1.00 0 -14 0 6.50 1.00 0 14 0 8.70 1.10 -1 -14 0 -0.80 0.60 -1 -14 0 0.60 0.60 1 14 0 -0.20 0.60 -2 -14 0 50.59 2.00 2 14 0 51.79 2.20 -3 -14 0 51.69 2.00 3 14 0 54.09 2.30 -4 -14 0 117.09 3.20 4 14 0 123.29 3.50 -5 -14 0 72.59 2.50 5 14 0 71.69 2.70 5 14 0 69.79 2.60 -6 -14 0 22.10 1.60 6 14 0 27.90 1.80 6 14 0 23.50 1.70 -7 -14 0 14.00 1.50 7 14 0 11.50 1.40 7 14 0 12.50 1.40 -8 -14 0 41.70 2.30 8 14 0 43.40 2.40 8 14 0 37.80 2.20 -9 -14 0 477.05 9.30 9 14 0 487.35 9.70 -10 -14 0 91.49 3.70 10 14 0 94.99 3.80 -11 -14 0 79.79 3.40 11 14 0 79.09 3.60 -12 -14 0 5.00 1.50 12 14 0 9.40 1.80 6 -15 0 8.60 1.90 -6 15 0 15.40 1.70 5 -15 0 57.69 3.70 -5 15 0 65.29 3.00 4 -15 0 7.20 1.30 4 -15 0 5.10 1.40 -4 15 0 7.70 1.40 3 -15 0 161.08 5.20 3 -15 0 145.79 4.40 -3 15 0 160.58 4.50 2 -15 0 35.80 2.60 2 -15 0 39.30 2.20 -2 15 0 37.80 2.10 1 -15 0 10.90 1.30 1 -15 0 9.70 1.40 -1 15 0 9.70 1.30 0 -15 0 31.40 1.90 0 -15 0 30.70 2.10 0 15 0 32.80 1.90 -1 -15 0 6.10 1.00 1 15 0 5.70 1.10 -2 -15 0 36.20 1.90 2 15 0 33.90 1.90 -3 -15 0 67.09 2.40 3 15 0 67.69 2.70 -4 -15 0 54.59 2.20 4 15 0 53.69 2.40 -5 -15 0 35.60 1.90 5 15 0 38.50 2.10 -6 -15 0 25.60 1.80 6 15 0 22.70 1.80 6 15 0 20.50 1.80 -7 -15 0 0.60 0.90 7 15 0 1.40 0.90 7 15 0 1.80 0.90 -8 -15 0 22.60 1.90 8 15 0 23.50 2.00 8 15 0 20.60 1.80 -9 -15 0 50.29 2.80 9 15 0 46.40 2.90 -10 -15 0 3.60 1.20 10 15 0 3.70 1.20 -11 -15 0 -1.10 0.90 11 15 0 -1.10 0.90 -12 -15 0 0.40 1.30 12 15 0 -0.90 1.10 5 -16 0 8.40 1.80 -5 16 0 4.90 1.20 4 -16 0 12.10 1.70 4 -16 0 12.70 2.00 -4 16 0 14.90 1.70 3 -16 0 67.09 3.60 3 -16 0 75.19 3.20 -3 16 0 75.39 3.10 2 -16 0 -1.10 0.90 2 -16 0 0.00 0.70 -2 16 0 0.70 0.80 1 -16 0 -2.00 0.90 1 -16 0 -0.10 0.70 -1 16 0 0.80 0.70 0 -16 0 3.30 1.00 0 16 0 3.80 1.00 -1 -16 0 55.79 2.50 1 16 0 51.99 2.50 -2 -16 0 74.89 2.70 2 16 0 73.99 2.90 -3 -16 0 58.19 2.40 3 16 0 51.49 2.50 -4 -16 0 52.39 2.40 4 16 0 60.19 2.70 -5 -16 0 47.50 2.20 5 16 0 51.09 2.60 -6 -16 0 7.30 1.20 6 16 0 5.90 1.30 -7 -16 0 1.60 0.90 7 16 0 2.00 1.00 7 16 0 0.30 0.90 -8 -16 0 160.58 4.50 8 16 0 160.88 4.80 8 16 0 161.38 4.80 -9 -16 0 2.30 1.10 9 16 0 2.20 1.10 -10 -16 0 1.20 1.00 10 16 0 2.00 1.10 -11 -16 0 8.40 1.50 11 16 0 8.00 1.60 4 -17 0 30.20 3.00 3 -17 0 29.50 2.30 3 -17 0 22.60 2.50 -3 17 0 24.70 2.20 2 -17 0 14.20 1.70 2 -17 0 12.60 2.00 -2 17 0 17.60 1.80 1 -17 0 22.20 1.90 -1 17 0 21.30 2.00 0 -17 0 2.30 0.90 0 17 0 2.40 1.00 -1 -17 0 4.30 1.00 1 17 0 6.60 1.30 -2 -17 0 144.09 4.00 2 17 0 132.09 4.10 -3 -17 0 24.00 1.80 3 17 0 30.10 2.20 -4 -17 0 27.10 2.00 4 17 0 29.10 2.20 -5 -17 0 8.00 1.20 5 17 0 8.50 1.40 -6 -17 0 2.30 1.00 6 17 0 -0.70 0.90 -7 -17 0 73.69 2.90 7 17 0 71.09 3.20 -8 -17 0 76.09 3.10 8 17 0 78.79 3.30 8 17 0 72.19 3.20 -9 -17 0 5.40 1.30 9 17 0 8.10 1.50 -10 -17 0 232.98 5.90 10 17 0 228.98 6.40 11 17 0 69.69 3.70 2 -18 0 59.39 3.00 -2 18 0 59.09 2.90 1 -18 0 -0.20 0.80 -1 18 0 1.00 1.00 0 -18 0 24.80 2.00 0 18 0 19.60 1.90 -1 -18 0 15.90 1.70 1 18 0 12.70 1.70 -2 -18 0 0.50 0.80 2 18 0 1.90 1.00 -3 -18 0 71.09 2.90 3 18 0 68.69 3.00 -4 -18 0 68.59 2.80 4 18 0 68.79 3.20 -5 -18 0 1.70 0.90 5 18 0 1.50 1.00 -6 -18 0 11.10 1.40 6 18 0 14.10 1.70 -7 -18 0 0.40 0.90 7 18 0 0.40 0.90 -8 -18 0 13.50 1.60 8 18 0 12.90 1.70 -9 -18 0 5.90 1.40 9 18 0 6.10 1.60 10 18 0 30.80 2.70 1 -19 0 45.60 2.80 0 -19 0 3.10 1.20 0 19 0 3.20 1.10 -1 -19 0 48.80 2.60 1 19 0 42.70 2.70 -2 -19 0 7.30 1.30 2 19 0 8.20 1.50 -3 -19 0 8.20 1.30 3 19 0 7.70 1.40 -4 -19 0 27.60 2.10 4 19 0 22.20 2.10 -5 -19 0 2.40 0.90 5 19 0 2.80 1.20 -6 -19 0 36.40 2.20 6 19 0 30.50 2.50 -7 -19 0 10.80 1.50 7 19 0 9.90 1.60 -8 -19 0 20.40 1.90 8 19 0 17.50 2.00 -2 -20 0 13.80 1.70 2 20 0 11.20 1.90 -3 -20 0 25.90 2.10 3 20 0 18.30 2.10 -4 -20 0 32.60 2.30 4 20 0 39.40 2.80 -5 -20 0 33.90 2.30 5 20 0 40.10 2.80 -6 -20 0 5.80 1.30 6 20 0 8.20 1.60 7 20 0 0.00 1.10 7 20 -1 83.29 3.80 6 20 -1 199.68 5.90 -6 -20 1 180.78 5.00 5 20 -1 2.00 1.20 -5 -20 1 1.10 1.00 4 20 -1 9.50 1.70 -4 -20 1 9.00 1.40 3 20 -1 8.00 1.50 -3 -20 1 14.60 1.70 2 20 -1 -0.10 1.10 -2 -20 1 0.30 0.90 -8 -19 1 6.90 1.40 7 19 -1 54.99 3.10 -7 -19 1 53.69 2.70 6 19 -1 11.50 1.70 -6 -19 1 9.90 1.50 5 19 -1 2.30 1.00 -5 -19 1 3.10 1.00 4 19 -1 1.20 0.90 -4 -19 1 -0.30 0.90 3 19 -1 31.20 2.40 -3 -19 1 34.40 2.20 2 19 -1 -1.70 0.80 -2 -19 1 0.30 0.80 1 19 -1 6.70 1.50 -1 -19 1 7.00 1.30 0 19 -1 1.20 1.10 0 -19 1 0.70 1.00 1 -19 1 22.90 2.20 10 18 -1 6.80 1.70 9 18 -1 51.79 3.00 -9 -18 1 48.30 2.70 -8 -18 1 12.90 1.60 7 18 -1 1.20 0.90 -7 -18 1 0.80 0.80 6 18 -1 -0.10 0.90 -6 -18 1 1.60 0.80 5 18 -1 0.00 0.90 -5 -18 1 2.10 0.80 4 18 -1 4.50 1.20 -4 -18 1 4.80 1.10 3 18 -1 3.50 1.10 -3 -18 1 4.80 1.00 2 18 -1 27.50 2.10 -2 -18 1 30.30 2.00 1 18 -1 0.50 0.90 -1 -18 1 2.60 0.90 0 18 -1 56.69 3.10 0 -18 1 59.69 2.80 -1 18 -1 2.70 1.20 1 -18 1 5.10 1.20 -2 18 -1 2.00 1.20 2 -18 1 3.70 1.10 11 17 -1 20.20 2.40 10 17 -1 18.20 2.20 -10 -17 1 20.50 2.10 9 17 -1 4.30 1.30 -9 -17 1 2.10 1.00 8 17 -1 3.40 1.20 -8 -17 1 4.80 1.20 7 17 -1 107.29 3.90 -7 -17 1 103.89 3.40 6 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3.20 -7 -15 4 78.29 3.10 6 15 -4 52.99 2.50 6 15 -4 52.49 2.40 -6 -15 4 53.59 2.40 5 15 -4 99.39 3.20 5 15 -4 99.69 3.30 -5 -15 4 106.09 3.30 4 15 -4 41.80 2.10 -4 -15 4 38.60 2.00 3 15 -4 3.80 0.90 -3 -15 4 1.70 0.80 2 15 -4 146.19 4.00 -2 -15 4 144.59 3.70 1 15 -4 16.10 1.50 -1 -15 4 16.70 1.40 -1 -15 4 15.80 1.50 0 15 -4 8.90 1.30 0 -15 4 7.20 1.00 0 -15 4 6.20 1.20 -1 15 -4 86.29 3.10 1 -15 4 85.99 3.40 1 -15 4 85.49 2.90 -2 15 -4 2.10 0.90 2 -15 4 0.20 1.10 -3 15 -4 39.50 2.20 3 -15 4 41.80 2.60 -4 15 -4 43.40 2.40 4 -15 4 40.20 2.90 -5 15 -4 -0.20 0.80 5 -15 4 -0.70 1.00 -6 15 -4 70.99 3.30 6 -15 4 71.19 4.00 11 14 -4 1.00 1.10 -11 -14 4 0.20 1.30 10 14 -4 44.70 2.80 -10 -14 4 38.50 2.80 9 14 -4 8.00 1.40 -9 -14 4 6.00 1.50 8 14 -4 49.80 2.70 -8 -14 4 47.40 2.60 7 14 -4 70.39 2.90 -7 -14 4 65.29 2.80 6 14 -4 18.40 1.70 6 14 -4 18.50 1.50 -6 -14 4 20.40 1.60 5 14 -4 280.67 5.90 5 14 -4 280.17 6.00 -5 -14 4 284.37 5.90 4 14 -4 337.97 6.70 4 14 -4 338.27 6.60 -4 -14 4 331.27 6.50 3 14 -4 18.70 1.40 -3 -14 4 17.20 1.40 2 14 -4 204.08 4.70 -2 -14 4 193.28 4.30 1 14 -4 171.28 4.20 -1 -14 4 171.48 3.90 -1 -14 4 175.18 4.40 0 14 -4 61.59 2.50 0 -14 4 60.29 2.60 0 -14 4 62.99 2.30 -1 14 -4 1.10 0.80 1 -14 4 0.60 0.90 1 -14 4 2.10 0.80 -2 14 -4 158.88 4.20 2 -14 4 152.68 4.60 2 -14 4 157.08 4.00 -3 14 -4 115.09 3.50 3 -14 4 112.39 4.10 -4 14 -4 85.79 3.10 4 -14 4 80.19 3.60 -5 14 -4 12.10 1.40 5 -14 4 11.30 1.90 -6 14 -4 0.90 0.90 6 -14 4 0.20 1.20 -7 14 -4 26.00 2.00 7 -14 4 25.30 3.00 12 13 -4 3.70 1.40 -12 -13 4 1.90 1.50 11 13 -4 0.90 1.20 -11 -13 4 -0.20 1.30 10 13 -4 75.49 3.50 -10 -13 4 72.19 3.40 9 13 -4 4.30 1.10 -9 -13 4 4.70 1.40 8 13 -4 104.59 3.70 -8 -13 4 105.49 3.60 7 13 -4 55.29 2.60 -7 -13 4 51.09 2.60 6 13 -4 112.89 3.20 6 13 -4 114.89 3.50 -6 -13 4 116.69 3.50 5 13 -4 622.44 10.60 5 13 -4 625.04 10.80 -5 -13 4 621.84 10.70 4 13 -4 178.28 4.20 4 13 -4 184.38 4.30 -4 -13 4 184.88 4.20 3 13 -4 112.59 3.00 3 13 -4 115.99 3.20 -3 -13 4 113.39 3.00 2 13 -4 82.39 2.60 -2 -13 4 78.59 2.60 -2 -13 4 75.79 2.40 1 13 -4 30.30 1.60 -1 -13 4 31.30 1.50 -1 -13 4 33.70 1.80 0 13 -4 50.99 2.00 0 -13 4 49.50 2.20 0 -13 4 51.79 1.90 -1 13 -4 164.78 4.00 1 -13 4 165.18 4.50 1 -13 4 172.18 3.90 -2 13 -4 15.20 1.40 2 -13 4 16.70 1.70 2 -13 4 14.20 1.30 -3 13 -4 3.20 0.90 3 -13 4 3.30 0.80 3 -13 4 2.10 0.90 -4 13 -4 44.60 2.20 4 -13 4 42.00 2.80 -5 13 -4 1.10 0.80 5 -13 4 2.00 1.20 -6 13 -4 23.80 2.00 6 -13 4 28.70 2.70 -7 13 -4 1.80 1.00 7 -13 4 4.00 1.60 -8 13 -4 9.10 1.50 12 12 -4 22.20 2.40 -12 -12 4 21.00 2.40 11 12 -4 42.90 2.90 -11 -12 4 38.60 2.90 10 12 -4 21.90 2.20 -10 -12 4 17.20 1.90 9 12 -4 72.99 3.20 -9 -12 4 76.19 3.20 8 12 -4 142.99 4.30 -8 -12 4 140.19 4.30 7 12 -4 76.99 2.90 6 12 -4 64.99 2.50 6 12 -4 66.49 2.30 -6 -12 4 65.09 2.60 5 12 -4 19.40 1.30 5 12 -4 17.60 1.40 -5 -12 4 15.20 1.40 4 12 -4 0.80 0.60 4 12 -4 1.20 0.60 -4 -12 4 0.10 0.60 3 12 -4 38.40 1.70 3 12 -4 37.00 1.70 -3 -12 4 38.60 1.70 -3 -12 4 37.40 1.60 2 12 -4 381.36 6.90 2 12 -4 382.96 6.70 -2 -12 4 384.66 7.10 -2 -12 4 388.16 6.80 1 12 -4 1518.65 22.50 -1 -12 4 1495.45 23.40 -1 -12 4 1526.45 22.30 0 12 -4 65.49 2.20 0 -12 4 71.39 2.20 0 -12 4 67.99 2.50 -1 12 -4 1.10 0.60 1 -12 4 0.70 0.60 1 -12 4 1.70 0.60 -2 12 -4 47.50 2.00 2 -12 4 44.00 2.20 2 -12 4 52.29 1.90 -3 12 -4 182.78 4.30 3 -12 4 179.38 4.20 3 -12 4 177.78 4.90 -4 12 -4 1.20 0.70 4 -12 4 1.00 0.90 -5 12 -4 31.00 2.00 5 -12 4 34.40 2.60 -6 12 -4 34.70 2.00 6 -12 4 41.20 3.00 -7 12 -4 2.60 0.90 7 -12 4 3.50 1.30 -8 12 -4 -0.40 0.70 8 -12 4 -1.40 1.10 12 11 -4 45.90 3.10 -12 -11 4 38.60 2.80 11 11 -4 41.10 2.70 -11 -11 4 40.40 2.80 10 11 -4 -1.00 0.90 -10 -11 4 -0.80 0.90 9 11 -4 61.49 2.90 -9 -11 4 70.69 3.20 8 11 -4 10.60 1.40 -8 -11 4 9.50 1.50 7 11 -4 30.00 1.80 -7 -11 4 28.50 2.10 6 11 -4 107.09 2.90 6 11 -4 106.79 3.30 -6 -11 4 109.29 3.40 5 11 -4 75.19 2.30 5 11 -4 76.69 2.60 -5 -11 4 79.49 2.70 4 11 -4 87.39 2.50 4 11 -4 88.59 2.60 -4 -11 4 86.49 2.30 -4 -11 4 89.19 2.70 3 11 -4 388.66 6.90 3 11 -4 402.06 6.90 -3 -11 4 381.56 6.90 -3 -11 4 382.46 6.80 2 11 -4 111.39 2.70 2 11 -4 106.49 2.80 -2 -11 4 113.29 2.80 -2 -11 4 105.99 2.70 1 11 -4 106.39 2.50 1 11 -4 106.79 2.80 -1 -11 4 106.59 2.60 -1 -11 4 104.19 2.90 0 11 -4 182.78 4.00 0 -11 4 181.48 4.20 0 -11 4 187.18 3.80 -1 11 -4 -0.10 0.50 1 -11 4 -0.40 0.50 1 -11 4 0.40 0.50 -2 11 -4 4.60 0.80 2 -11 4 4.30 1.00 2 -11 4 4.50 0.70 -3 11 -4 79.89 2.50 3 -11 4 73.19 2.90 3 -11 4 77.09 2.40 -4 11 -4 9.70 1.10 4 -11 4 13.10 1.60 4 -11 4 11.30 1.10 -5 11 -4 96.19 3.00 5 -11 4 100.89 3.80 -6 11 -4 72.49 2.70 6 -11 4 71.49 3.40 -7 11 -4 105.09 3.40 7 -11 4 106.39 4.50 -8 11 -4 62.09 2.70 8 -11 4 60.09 3.40 -9 11 -4 62.99 2.90 9 -11 4 73.19 4.10 13 10 -4 159.58 5.50 -13 -10 4 157.08 5.50 12 10 -4 10.10 1.80 -12 -10 4 10.90 1.90 11 10 -4 3.10 1.30 -11 -10 4 0.00 1.20 10 10 -4 8.60 1.40 -10 -10 4 4.20 1.40 9 10 -4 61.29 2.80 -9 -10 4 62.19 2.90 8 10 -4 331.97 7.10 -8 -10 4 343.57 7.30 7 10 -4 251.97 5.60 -7 -10 4 245.48 5.60 6 10 -4 3.20 0.70 6 10 -4 2.20 0.70 -6 -10 4 4.00 1.00 5 10 -4 145.29 3.60 5 10 -4 148.39 3.40 -5 -10 4 150.48 3.80 4 10 -4 114.29 3.00 4 10 -4 114.19 2.80 -4 -10 4 111.19 2.60 -4 -10 4 111.99 3.10 3 10 -4 307.17 5.50 3 10 -4 300.57 5.50 -3 -10 4 295.87 5.40 -3 -10 4 286.27 5.50 2 10 -4 640.14 10.10 2 10 -4 637.64 10.00 -2 -10 4 643.64 10.40 -2 -10 4 630.74 10.10 1 10 -4 728.83 11.50 1 10 -4 754.12 11.20 -1 -10 4 748.23 11.50 -1 -10 4 743.63 12.10 0 10 -4 79.89 1.90 0 10 -4 74.09 2.20 0 -10 4 75.39 2.00 0 -10 4 75.49 2.40 1 -10 4 61.29 1.80 1 -10 4 62.09 2.30 -2 10 -4 639.84 10.60 2 -10 4 663.23 10.50 2 -10 4 673.03 11.60 -3 10 -4 6.80 0.80 3 -10 4 9.20 1.00 3 -10 4 5.50 1.10 -4 10 -4 1.20 0.60 4 -10 4 3.40 0.70 4 -10 4 2.80 0.90 -5 10 -4 70.79 2.50 5 -10 4 67.89 3.00 -6 10 -4 57.79 2.30 6 -10 4 55.29 3.00 -7 10 -4 33.10 2.00 7 -10 4 35.20 2.80 -8 10 -4 -0.40 0.80 8 -10 4 -0.20 1.10 -9 10 -4 14.40 1.50 9 -10 4 16.80 2.30 -10 10 -4 8.90 1.40 13 9 -4 21.20 2.30 -13 -9 4 17.80 2.20 12 9 -4 3.40 1.30 -12 -9 4 4.80 1.50 11 9 -4 36.90 2.70 -11 -9 4 34.50 2.70 10 9 -4 3.80 1.20 -10 -9 4 1.00 1.10 9 9 -4 184.88 5.00 -9 -9 4 188.18 5.10 8 9 -4 244.48 5.70 -8 -9 4 240.78 5.70 7 9 -4 11.00 1.20 -7 -9 4 14.70 1.50 6 9 -4 15.20 1.30 6 9 -4 15.40 1.00 -6 -9 4 15.50 1.40 5 9 -4 1.50 0.60 5 9 -4 1.40 0.50 -5 -9 4 1.50 0.50 -5 -9 4 2.20 0.70 4 9 -4 1062.79 15.80 4 9 -4 1047.80 15.50 -4 -9 4 1005.90 16.00 -4 -9 4 1044.10 15.80 3 9 -4 326.07 5.60 3 9 -4 323.07 5.70 -3 -9 4 314.77 5.60 -3 -9 4 327.17 5.90 2 9 -4 16.80 0.90 2 9 -4 17.90 1.00 -2 -9 4 14.80 0.90 -2 -9 4 14.80 1.00 1 9 -4 66.39 1.80 1 9 -4 68.89 1.90 -1 -9 4 65.29 2.00 -1 -9 4 64.49 1.80 0 9 -4 965.00 14.40 0 9 -4 951.20 13.90 0 -9 4 967.60 15.20 0 -9 4 971.20 14.30 -1 9 -4 1781.52 25.00 -1 9 -4 1674.53 24.10 1 -9 4 1747.43 24.90 1 -9 4 1729.63 26.40 -2 9 -4 385.46 6.70 2 -9 4 396.96 7.40 2 -9 4 384.06 6.60 -3 9 -4 9.40 0.90 3 -9 4 4.60 0.90 3 -9 4 6.80 0.80 -4 9 -4 129.39 3.20 4 -9 4 125.39 3.80 4 -9 4 128.59 3.10 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1.60 -5 -19 -4 2.50 0.90 5 19 4 1.10 1.10 -6 -19 -4 4.10 1.10 6 19 4 2.60 1.20 -7 -19 -4 1.80 1.00 7 19 4 0.00 1.10 -8 -19 -4 68.79 3.00 8 19 4 70.79 3.60 -9 -19 -4 2.30 1.00 9 19 4 2.10 1.20 -3 -20 -4 17.90 1.90 3 20 4 20.90 2.60 -4 -20 -4 23.00 2.20 4 20 4 23.90 2.50 -5 -20 -4 1.40 1.10 5 20 4 0.90 1.20 -6 -20 -4 10.80 1.60 6 20 4 14.00 2.00 7 20 4 62.29 3.40 8 20 4 63.99 3.60 -7 -19 5 3.50 1.10 -6 -19 5 8.50 1.30 -5 -19 5 2.50 1.00 4 19 -5 25.80 2.20 -4 -19 5 25.90 2.00 3 19 -5 27.90 2.30 -3 -19 5 26.20 2.00 2 19 -5 14.10 1.80 -2 -19 5 14.70 1.70 1 19 -5 25.10 2.30 -8 -18 5 6.10 1.40 -7 -18 5 59.29 2.80 -6 -18 5 1.80 1.00 -5 -18 5 36.40 2.20 4 18 -5 9.90 1.50 -4 -18 5 9.30 1.20 3 18 -5 26.70 2.10 -3 -18 5 30.50 1.90 2 18 -5 65.39 3.00 -2 -18 5 69.09 2.80 1 18 -5 49.90 2.80 0 18 -5 26.60 2.30 -1 18 -5 28.10 2.30 2 -18 5 5.20 1.50 9 17 -5 69.89 3.50 -9 -17 5 70.79 3.50 8 17 -5 6.20 1.40 -8 -17 5 5.50 1.40 7 17 -5 8.20 1.50 -7 -17 5 7.00 1.30 -6 -17 5 2.30 0.90 5 17 -5 3.80 1.00 -5 -17 5 3.00 0.90 4 17 -5 6.00 1.10 -4 -17 5 4.20 1.00 3 17 -5 12.30 1.40 -3 -17 5 14.00 1.40 2 17 -5 33.00 2.10 -2 -17 5 29.70 1.90 1 17 -5 -0.30 0.70 -1 -17 5 -0.10 0.70 0 17 -5 1.10 0.90 -1 17 -5 1.90 1.00 1 -17 5 2.30 1.20 -2 17 -5 0.10 1.00 2 -17 5 0.90 1.10 -3 17 -5 3.80 1.20 3 -17 5 2.30 1.40 4 -17 5 18.20 2.30 10 16 -5 27.10 2.60 -10 -16 5 26.70 2.40 9 16 -5 24.80 2.40 -9 -16 5 24.00 2.20 8 16 -5 19.50 2.00 -8 -16 5 18.90 1.90 7 16 -5 36.40 2.40 -7 -16 5 37.40 2.40 6 16 -5 250.87 6.10 -6 -16 5 258.67 5.90 5 16 -5 30.00 2.00 -5 -16 5 30.40 2.00 4 16 -5 3.80 1.00 -4 -16 5 5.40 1.00 3 16 -5 38.10 2.20 -3 -16 5 40.30 2.00 2 16 -5 106.79 3.50 -2 -16 5 104.29 3.20 1 16 -5 133.89 4.00 -1 -16 5 133.49 3.60 0 16 -5 37.30 2.10 0 -16 5 38.60 2.40 0 -16 5 32.00 1.90 -1 16 -5 19.50 1.80 1 -16 5 23.60 2.20 -2 16 -5 0.80 0.90 2 -16 5 2.80 1.20 -3 16 -5 6.10 1.30 3 -16 5 5.30 1.40 -4 16 -5 2.50 1.10 4 -16 5 1.60 1.40 5 -16 5 3.80 1.40 11 15 -5 7.40 1.60 10 15 -5 0.00 1.10 -10 -15 5 -0.10 1.20 9 15 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14 -5 20.50 1.50 -3 -14 5 22.00 1.50 2 14 -5 58.69 2.30 -2 -14 5 56.89 2.30 -2 -14 5 56.79 2.10 1 14 -5 6.20 0.90 -1 -14 5 6.60 1.00 -1 -14 5 5.90 0.80 0 14 -5 248.68 5.40 0 -14 5 249.58 5.80 0 -14 5 247.68 5.10 -1 14 -5 185.68 4.50 1 -14 5 190.18 5.00 1 -14 5 181.28 4.20 -2 14 -5 31.40 1.90 2 -14 5 33.60 2.30 -3 14 -5 33.10 1.90 3 -14 5 27.20 2.40 -4 14 -5 39.60 2.20 4 -14 5 48.50 3.00 -5 14 -5 31.60 2.10 5 -14 5 36.30 2.90 -6 14 -5 0.50 0.80 6 -14 5 1.30 1.20 11 13 -5 9.80 1.70 -11 -13 5 8.20 1.80 10 13 -5 161.58 5.10 -10 -13 5 158.98 5.00 9 13 -5 165.18 5.00 -9 -13 5 179.18 5.20 8 13 -5 104.89 3.70 -8 -13 5 110.79 3.90 7 13 -5 9.70 1.30 -7 -13 5 11.10 1.40 6 13 -5 41.80 2.20 -6 -13 5 40.00 2.20 5 13 -5 49.10 2.20 5 13 -5 48.90 2.00 -5 -13 5 46.50 2.20 4 13 -5 400.26 7.60 4 13 -5 417.76 7.60 -4 -13 5 418.46 7.60 3 13 -5 169.38 4.00 3 13 -5 171.58 4.10 -3 -13 5 182.08 4.00 2 13 -5 207.18 4.60 -2 -13 5 204.88 4.60 -2 -13 5 208.78 4.40 1 13 -5 10.90 1.20 -1 -13 5 10.30 1.20 -1 -13 5 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6 -6 5 15.70 1.10 -7 6 -5 612.64 10.10 7 -6 5 590.74 11.30 -8 6 -5 518.85 9.20 8 -6 5 544.55 10.70 -9 6 -5 -0.60 0.60 9 -6 5 -0.10 0.90 -10 6 -5 30.90 1.80 10 -6 5 29.40 2.50 -11 6 -5 0.40 0.80 11 -6 5 0.20 1.20 -12 6 -5 22.60 1.90 12 -6 5 19.70 2.50 13 5 -5 41.40 2.80 -13 -5 5 40.20 2.90 12 5 -5 2.10 1.20 -12 -5 5 2.30 1.40 11 5 -5 -0.80 0.90 -11 -5 5 0.30 1.00 10 5 -5 62.39 2.80 -10 -5 5 66.09 3.20 9 5 -5 47.70 2.30 -9 -5 5 45.90 2.00 -9 -5 5 46.70 2.50 8 5 -5 65.79 2.50 -8 -5 5 64.29 2.30 -8 -5 5 62.49 2.70 7 5 -5 594.04 10.10 -7 -5 5 585.94 10.00 -7 -5 5 602.44 10.70 6 5 -5 629.14 10.30 -6 -5 5 619.24 10.30 -6 -5 5 623.04 10.80 5 5 -5 133.79 2.50 5 5 -5 135.39 3.20 -5 -5 5 136.99 3.00 4 5 -5 145.89 3.10 4 5 -5 139.99 2.50 -4 -5 5 139.89 3.30 -4 -5 5 135.39 3.00 3 5 -5 435.06 6.40 3 5 -5 428.96 6.90 -3 -5 5 424.16 7.20 -3 -5 5 417.46 7.00 2 5 -5 691.63 9.80 2 5 -5 672.33 10.10 -2 -5 5 683.23 10.50 -2 -5 5 670.23 10.60 1 5 -5 2996.30 43.60 1 5 -5 3031.40 43.90 -1 -5 5 3040.00 44.90 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5 36.40 2.50 2 -16 -5 12.40 1.70 -2 16 5 15.10 1.70 -2 16 5 9.20 1.70 1 -16 -5 -1.00 0.80 -1 16 5 -1.40 0.80 0 -16 -5 11.00 1.40 0 16 5 13.10 1.60 -1 -16 -5 10.00 1.50 1 16 5 10.00 1.40 -2 -16 -5 487.75 9.40 2 16 5 499.55 9.70 -3 -16 -5 172.28 4.60 3 16 5 177.68 5.00 -4 -16 -5 2.50 0.80 4 16 5 1.60 1.00 -5 -16 -5 28.90 1.90 5 16 5 28.30 2.20 -6 -16 -5 1.10 0.80 6 16 5 2.00 1.00 -7 -16 -5 70.09 2.80 7 16 5 67.99 3.20 -8 -16 -5 80.89 3.00 8 16 5 78.69 3.20 8 16 5 81.19 3.40 -9 -16 -5 1.60 0.80 9 16 5 0.50 1.00 9 16 5 0.10 0.90 -10 -16 -5 53.29 2.60 10 16 5 47.30 2.90 10 16 5 47.60 2.80 -11 -16 -5 3.40 1.10 11 16 5 1.70 1.20 11 16 5 2.20 1.10 -12 -16 -5 3.70 1.20 12 16 5 2.80 1.30 3 -17 -5 6.90 1.60 -3 17 5 6.60 1.40 -3 17 5 9.70 1.80 2 -17 -5 2.80 1.20 -2 17 5 1.00 0.90 1 -17 -5 0.70 0.90 -1 17 5 1.20 1.00 0 -17 -5 6.80 1.30 0 17 5 7.00 1.30 -1 -17 -5 13.10 1.60 1 17 5 15.90 1.80 -2 -17 -5 14.90 1.60 2 17 5 11.80 1.70 -3 -17 -5 1.80 0.90 3 17 5 1.60 1.00 -4 -17 -5 77.09 3.00 4 17 5 76.29 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0 -14 6 1.30 0.70 0 -14 6 0.80 0.80 -1 14 -6 13.50 1.30 1 -14 6 13.30 1.50 -2 14 -6 86.99 3.00 2 -14 6 86.89 3.40 -3 14 -6 0.10 0.70 3 -14 6 -1.00 0.90 -4 14 -6 80.69 3.00 4 -14 6 79.39 3.70 -5 14 -6 43.80 2.40 5 -14 6 42.00 2.90 -6 14 -6 1.00 0.90 6 -14 6 5.70 1.50 11 13 -6 33.30 2.60 -11 -13 6 33.40 2.80 10 13 -6 0.80 1.10 -10 -13 6 -0.40 1.20 9 13 -6 0.50 0.90 -9 -13 6 1.50 1.20 8 13 -6 75.39 3.20 -8 -13 6 75.59 3.30 7 13 -6 82.99 3.20 -7 -13 6 83.69 3.30 6 13 -6 1.10 0.80 -6 -13 6 2.00 1.00 5 13 -6 7.80 1.10 -5 -13 6 7.10 1.10 4 13 -6 114.79 3.10 4 13 -6 113.29 3.30 -4 -13 6 114.29 3.30 3 13 -6 359.36 6.70 3 13 -6 350.76 6.70 -3 -13 6 355.26 6.60 -3 -13 6 352.96 7.10 2 13 -6 103.09 2.80 2 13 -6 101.99 2.90 -2 -13 6 101.89 3.00 -2 -13 6 100.39 2.80 1 13 -6 0.80 0.60 -1 -13 6 1.00 0.60 -1 -13 6 1.00 0.70 0 13 -6 6.20 0.90 0 -13 6 7.60 0.90 0 -13 6 6.60 1.00 -1 13 -6 287.57 5.90 1 -13 6 287.37 5.50 1 -13 6 287.17 6.40 -2 13 -6 71.59 2.60 2 -13 6 73.39 3.00 -3 13 -6 22.80 1.70 3 -13 6 22.50 2.10 -4 13 -6 1.40 0.80 4 -13 6 0.30 1.10 -5 13 -6 6.30 1.10 5 -13 6 7.30 1.60 -6 13 -6 7.40 1.30 6 -13 6 8.50 1.60 -7 13 -6 -0.50 0.80 7 -13 6 0.10 1.20 -12 -12 6 29.30 3.10 11 12 -6 77.39 3.80 -11 -12 6 76.19 3.90 10 12 -6 2.30 1.10 -10 -12 6 -0.20 1.30 9 12 -6 6.10 1.30 -9 -12 6 4.00 1.30 8 12 -6 39.50 2.40 -8 -12 6 34.70 2.40 7 12 -6 5.10 1.10 -7 -12 6 3.10 1.00 6 12 -6 34.90 2.00 -6 -12 6 36.70 2.00 5 12 -6 70.89 2.60 -5 -12 6 71.39 2.60 4 12 -6 17.70 1.40 4 12 -6 17.40 1.20 -4 -12 6 18.30 1.50 3 12 -6 13.30 1.20 3 12 -6 15.00 1.20 -3 -12 6 16.40 1.20 -3 -12 6 16.60 1.30 2 12 -6 1.10 0.60 2 12 -6 1.20 0.50 -2 -12 6 1.30 0.60 -2 -12 6 1.20 0.60 1 12 -6 13.30 1.20 1 12 -6 14.00 1.10 -1 -12 6 13.60 1.20 -1 -12 6 13.70 1.10 0 12 -6 18.20 1.30 0 -12 6 17.40 1.20 0 -12 6 16.60 1.40 -1 12 -6 18.30 1.30 1 -12 6 16.40 1.50 1 -12 6 16.20 1.20 -2 12 -6 114.79 3.20 2 -12 6 107.49 3.50 -3 12 -6 208.98 4.70 3 -12 6 212.08 5.50 -4 12 -6 2.00 0.80 4 -12 6 1.60 1.00 -5 12 -6 88.89 3.10 5 -12 6 84.89 3.70 -6 12 -6 41.00 2.30 6 -12 6 41.40 3.00 -7 12 -6 1.60 0.80 7 -12 6 2.20 1.30 -8 12 -6 20.20 1.80 8 -12 6 14.90 2.10 12 11 -6 2.40 1.40 -12 -11 6 2.10 1.50 11 11 -6 274.17 7.20 -11 -11 6 284.17 7.20 10 11 -6 0.50 1.00 -10 -11 6 -1.90 1.10 9 11 -6 9.10 1.40 -9 -11 6 6.70 1.50 8 11 -6 59.09 2.70 -8 -11 6 61.19 2.80 7 11 -6 51.99 2.40 -7 -11 6 53.19 2.60 6 11 -6 7.70 1.10 -6 -11 6 8.70 1.30 5 11 -6 33.70 1.80 -5 -11 6 27.80 1.80 4 11 -6 0.00 0.40 4 11 -6 -0.50 0.50 -4 -11 6 0.00 0.50 -4 -11 6 -0.30 0.70 3 11 -6 414.76 7.10 3 11 -6 410.76 7.20 -3 -11 6 403.76 7.30 -3 -11 6 411.76 7.30 2 11 -6 134.69 3.10 2 11 -6 133.79 3.20 -2 -11 6 131.19 3.30 -2 -11 6 131.29 3.10 1 11 -6 50.09 1.80 1 11 -6 51.49 1.70 -1 -11 6 47.70 1.70 -1 -11 6 52.69 2.00 0 11 -6 0.50 0.50 0 11 -6 1.40 0.50 0 -11 6 0.50 0.50 0 -11 6 0.20 0.40 -1 11 -6 33.10 1.60 1 -11 6 35.80 1.80 1 -11 6 33.30 1.40 -2 11 -6 123.49 3.20 2 -11 6 125.19 3.70 2 -11 6 120.09 2.90 -3 11 -6 348.67 6.60 3 -11 6 352.36 7.50 -4 11 -6 71.49 2.50 4 -11 6 64.39 2.90 -5 11 -6 -0.70 0.60 5 -11 6 -0.10 0.80 -6 11 -6 93.79 3.20 6 -11 6 88.59 3.90 -7 11 -6 1.90 0.80 7 -11 6 1.80 1.30 -8 11 -6 15.10 1.50 8 -11 6 16.20 2.20 -9 11 -6 0.80 0.90 9 -11 6 0.70 1.30 12 10 -6 29.10 2.70 -12 -10 6 22.60 2.30 11 10 -6 15.40 2.00 -11 -10 6 13.60 2.00 10 10 -6 107.69 4.00 -10 -10 6 110.29 4.20 9 10 -6 12.20 1.50 -9 -10 6 11.60 1.60 8 10 -6 373.96 7.80 -8 -10 6 367.86 7.80 7 10 -6 647.24 11.40 -7 -10 6 663.83 11.70 6 10 -6 0.70 0.60 -6 -10 6 1.40 0.90 5 10 -6 233.98 5.00 -5 -10 6 226.78 5.10 -5 -10 6 224.18 4.50 4 10 -6 304.17 5.40 4 10 -6 287.47 5.70 -4 -10 6 301.37 5.50 -4 -10 6 296.77 5.90 3 10 -6 757.82 11.80 3 10 -6 744.13 11.50 -3 -10 6 755.22 12.00 -3 -10 6 727.63 11.90 2 10 -6 945.41 14.10 2 10 -6 933.21 14.10 -2 -10 6 928.61 14.30 -2 -10 6 933.51 14.80 1 10 -6 149.49 3.30 1 10 -6 149.29 3.20 -1 -10 6 148.89 3.50 -1 -10 6 151.38 3.20 0 10 -6 194.58 3.90 0 10 -6 186.08 3.60 0 -10 6 189.08 4.30 0 -10 6 193.38 3.70 -1 10 -6 27.40 1.40 -1 10 -6 26.10 1.10 1 -10 6 27.50 1.20 1 -10 6 25.40 1.50 -2 10 -6 333.27 6.20 2 -10 6 335.17 5.90 2 -10 6 334.47 6.80 -3 10 -6 640.94 10.60 3 -10 6 648.74 11.60 3 -10 6 646.94 10.40 -4 10 -6 41.50 1.90 4 -10 6 46.30 2.40 -5 10 -6 84.19 2.70 5 -10 6 77.69 3.20 -6 10 -6 38.60 2.00 6 -10 6 35.60 2.50 -7 10 -6 84.79 3.00 7 -10 6 77.89 3.60 -8 10 -6 26.90 1.90 8 -10 6 30.00 2.60 -9 10 -6 -0.40 0.70 9 -10 6 -0.50 1.10 -10 10 -6 9.30 1.40 12 9 -6 2.70 1.20 -12 -9 6 0.70 1.30 11 9 -6 19.10 2.10 -11 -9 6 16.90 2.10 10 9 -6 181.08 5.20 -10 -9 6 175.48 5.30 9 9 -6 105.59 3.80 -9 -9 6 108.49 3.90 8 9 -6 96.29 3.40 -8 -9 6 91.59 3.40 7 9 -6 36.80 2.00 -7 -9 6 38.50 2.20 6 9 -6 2.30 0.70 -6 -9 6 1.90 0.70 -6 -9 6 1.90 0.90 5 9 -6 203.18 4.60 -5 -9 6 208.28 4.70 -5 -9 6 209.88 4.20 4 9 -6 106.49 2.90 4 9 -6 108.69 2.50 -4 -9 6 104.19 3.00 -4 -9 6 104.39 2.60 3 9 -6 19.70 1.10 3 9 -6 18.80 1.00 -3 -9 6 18.80 1.10 -3 -9 6 18.20 1.30 2 9 -6 328.37 5.60 2 9 -6 319.97 5.70 -2 -9 6 328.57 5.90 -2 -9 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37.90 2.40 6 15 -7 94.89 3.50 -6 -15 7 98.49 3.40 5 15 -7 24.40 1.90 -5 -15 7 26.80 1.90 4 15 -7 110.79 3.50 4 15 -7 114.69 3.80 -4 -15 7 115.99 3.40 3 15 -7 37.70 2.10 -3 -15 7 38.00 1.90 2 15 -7 6.70 1.10 -2 -15 7 3.90 0.90 1 15 -7 29.60 1.90 -1 -15 7 28.30 2.00 -1 -15 7 31.20 1.70 0 15 -7 9.70 1.30 0 -15 7 9.00 1.40 -1 15 -7 5.00 1.10 1 -15 7 3.40 1.10 -2 15 -7 4.80 1.10 2 -15 7 3.10 1.10 -3 15 -7 7.80 1.20 3 -15 7 10.20 1.60 -4 15 -7 67.49 2.90 4 -15 7 74.69 3.80 -5 15 -7 65.29 3.00 5 -15 7 62.59 3.60 10 14 -7 0.30 1.00 -10 -14 7 -0.40 1.20 9 14 -7 3.70 1.10 -9 -14 7 0.20 1.00 8 14 -7 1.90 1.00 -8 -14 7 1.80 1.10 7 14 -7 300.47 6.90 -7 -14 7 304.47 6.80 6 14 -7 0.40 0.80 -6 -14 7 0.00 0.90 5 14 -7 0.40 0.70 -5 -14 7 -0.40 0.80 4 14 -7 45.50 2.10 4 14 -7 44.70 2.20 -4 -14 7 43.80 2.10 3 14 -7 97.19 3.00 3 14 -7 101.79 3.00 -3 -14 7 96.09 2.90 2 14 -7 32.60 1.80 -2 -14 7 31.00 1.70 -2 -14 7 30.00 1.80 1 14 -7 57.39 2.30 -1 -14 7 57.19 2.50 -1 -14 7 57.19 2.10 0 14 -7 298.67 6.10 0 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79.79 2.90 -4 10 -7 0.00 0.50 4 -10 7 -1.60 0.70 -5 10 -7 57.89 2.30 5 -10 7 55.09 2.70 -6 10 -7 64.19 2.50 6 -10 7 60.39 3.00 -7 10 -7 184.98 4.70 7 -10 7 178.78 5.60 -8 10 -7 48.20 2.40 8 -10 7 47.10 3.20 -9 10 -7 0.70 0.90 9 -10 7 1.50 1.40 -10 10 -7 7.20 1.30 12 9 -7 3.20 1.30 -12 -9 7 3.30 1.40 11 9 -7 67.99 3.40 -11 -9 7 58.89 3.40 10 9 -7 35.50 2.50 -10 -9 7 34.60 2.50 9 9 -7 319.07 7.20 -9 -9 7 317.57 7.40 8 9 -7 101.49 3.50 -8 -9 7 100.49 3.60 7 9 -7 140.29 4.00 -7 -9 7 148.19 4.30 6 9 -7 115.89 3.40 -6 -9 7 116.69 3.00 -6 -9 7 114.29 3.50 5 9 -7 104.79 3.10 -5 -9 7 109.49 2.90 -5 -9 7 107.99 3.20 4 9 -7 250.67 4.50 4 9 -7 252.67 5.10 -4 -9 7 244.88 5.20 -4 -9 7 250.97 4.90 3 9 -7 40.80 1.40 3 9 -7 37.60 1.60 -3 -9 7 39.00 1.60 -3 -9 7 40.90 1.80 2 9 -7 90.49 2.40 2 9 -7 91.49 2.20 -2 -9 7 91.79 2.50 -2 -9 7 90.79 2.50 1 9 -7 195.78 3.80 1 9 -7 190.88 3.80 -1 -9 7 192.68 3.80 -1 -9 7 195.48 4.10 0 9 -7 15.90 0.90 0 9 -7 14.50 0.90 0 -9 7 16.00 0.90 0 -9 7 13.80 1.10 -1 9 -7 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75.89 2.20 -2 -8 7 71.79 2.10 1 8 -7 43.40 1.40 1 8 -7 40.50 1.40 -1 -8 7 42.40 1.60 -1 -8 7 42.30 1.50 0 8 -7 87.39 2.10 0 8 -7 85.29 2.00 0 -8 7 78.99 1.90 0 -8 7 80.29 2.30 -1 8 -7 159.98 3.00 -1 8 -7 159.48 3.30 1 -8 7 151.08 2.90 1 -8 7 150.68 3.60 -2 8 -7 831.72 12.00 -2 8 -7 839.52 12.70 2 -8 7 828.02 12.30 2 -8 7 804.12 13.60 -3 8 -7 333.27 5.30 -3 8 -7 319.67 5.90 3 -8 7 334.87 5.50 3 -8 7 324.07 6.60 -4 8 -7 430.96 7.60 4 -8 7 434.16 8.40 -5 8 -7 119.59 3.20 5 -8 7 127.89 3.80 -6 8 -7 9.40 1.00 6 -8 7 9.80 1.40 -7 8 -7 92.29 3.00 7 -8 7 89.59 3.60 -8 8 -7 57.39 2.50 8 -8 7 57.09 3.10 -9 8 -7 12.50 1.50 9 -8 7 12.30 1.90 -10 8 -7 17.00 1.70 10 -8 7 16.30 2.10 -11 8 -7 8.60 1.40 11 -8 7 7.90 1.80 12 7 -7 50.09 3.10 -12 -7 7 46.60 3.30 11 7 -7 140.29 4.60 -11 -7 7 154.48 5.20 10 7 -7 0.60 1.00 -10 -7 7 0.40 1.10 9 7 -7 12.80 1.50 -9 -7 7 18.10 2.00 8 7 -7 168.78 4.50 -8 -7 7 176.28 4.90 7 7 -7 8.90 1.10 -7 -7 7 8.30 1.20 -7 -7 7 11.30 1.10 6 7 -7 158.88 4.00 -6 -7 7 163.08 4.20 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35.50 2.20 11 -7 7 38.60 3.10 13 6 -7 25.60 2.50 12 6 -7 1.30 1.30 -12 -6 7 1.80 1.40 11 6 -7 11.70 1.60 -11 -6 7 11.70 1.80 10 6 -7 26.10 2.20 -10 -6 7 22.70 2.30 9 6 -7 53.79 2.60 -9 -6 7 58.69 2.90 8 6 -7 266.47 6.00 -8 -6 7 272.97 6.50 -8 -6 7 280.87 5.80 7 6 -7 166.48 4.20 -7 -6 7 167.08 4.50 -7 -6 7 167.58 3.90 6 6 -7 457.55 8.10 -6 -6 7 443.66 8.50 -6 -6 7 454.85 8.00 5 6 -7 1397.76 20.50 -5 -6 7 1392.96 21.10 -5 -6 7 1346.47 21.10 4 6 -7 413.16 6.30 4 6 -7 414.36 7.10 -4 -6 7 412.66 7.20 -4 -6 7 407.56 7.40 3 6 -7 214.48 4.20 3 6 -7 211.78 3.60 -3 -6 7 216.48 4.20 -3 -6 7 209.38 4.40 2 6 -7 251.07 4.50 2 6 -7 251.97 4.10 -2 -6 7 254.47 4.70 -2 -6 7 253.07 4.80 1 6 -7 36.50 1.10 1 6 -7 38.80 1.30 -1 -6 7 37.90 1.30 -1 -6 7 38.30 1.50 0 6 -7 43.70 1.30 0 6 -7 44.50 1.30 0 -6 7 42.90 1.30 0 -6 7 42.70 1.50 -1 6 -7 15.30 0.80 -1 6 -7 16.60 0.80 1 -6 7 14.30 0.90 1 -6 7 16.20 0.70 -2 6 -7 1549.24 21.20 -2 6 -7 1510.75 21.70 2 -6 7 1482.95 23.00 2 -6 7 1500.55 21.30 -3 6 -7 157.18 3.30 -3 6 -7 154.28 2.80 3 -6 7 154.98 3.70 3 -6 7 157.78 2.80 -4 6 -7 46.60 1.70 -4 6 -7 48.80 1.30 4 -6 7 47.30 1.40 4 -6 7 47.60 1.90 -5 6 -7 37.70 1.60 -5 6 -7 38.30 1.20 5 -6 7 40.30 1.90 -6 6 -7 91.29 2.60 6 -6 7 92.39 3.20 -7 6 -7 5.20 0.90 7 -6 7 5.30 1.10 -8 6 -7 -0.40 0.60 8 -6 7 -0.50 0.80 -9 6 -7 10.10 1.30 9 -6 7 9.60 1.50 -10 6 -7 155.38 4.30 10 -6 7 153.98 5.20 -11 6 -7 2.00 0.90 11 -6 7 0.70 1.30 -12 6 -7 3.80 1.10 12 -6 7 3.10 1.50 13 5 -7 77.29 3.70 12 5 -7 175.98 5.40 -12 -5 7 179.38 5.90 11 5 -7 1.90 1.10 -11 -5 7 -0.10 1.20 10 5 -7 16.60 1.80 -10 -5 7 13.10 1.80 9 5 -7 42.30 2.20 -9 -5 7 41.90 2.60 -9 -5 7 42.90 2.10 8 5 -7 363.46 7.20 -8 -5 7 376.96 7.90 -8 -5 7 346.97 7.10 7 5 -7 7.50 1.00 -7 -5 7 8.10 0.90 -7 -5 7 8.40 1.20 6 5 -7 46.50 1.90 -6 -5 7 42.60 2.20 -6 -5 7 48.20 1.90 5 5 -7 184.28 4.00 -5 -5 7 192.48 4.10 -5 -5 7 185.98 4.50 4 5 -7 3.30 0.60 4 5 -7 2.50 0.30 -4 -5 7 2.00 0.60 -4 -5 7 2.70 0.70 3 5 -7 239.98 4.40 3 5 -7 242.08 3.70 -3 -5 7 237.68 4.60 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150.98 4.70 -4 13 -9 36.30 2.20 4 -13 9 36.80 2.60 -5 13 -9 13.90 1.50 5 -13 9 14.80 2.00 -6 13 -9 6.00 1.20 6 -13 9 6.40 1.50 -7 13 -9 29.90 2.10 7 -13 9 31.50 2.90 10 12 -9 70.19 3.60 -10 -12 9 62.99 3.40 9 12 -9 101.19 4.00 -9 -12 9 103.99 4.10 8 12 -9 82.69 3.30 -8 -12 9 87.89 3.70 7 12 -9 32.10 2.20 -7 -12 9 31.10 2.40 6 12 -9 48.30 2.50 -6 -12 9 47.30 2.50 5 12 -9 7.50 1.10 -5 -12 9 8.20 1.30 4 12 -9 186.78 4.50 -4 -12 9 180.68 4.20 -4 -12 9 177.98 4.40 3 12 -9 129.29 3.40 -3 -12 9 129.69 3.40 -3 -12 9 126.69 3.40 2 12 -9 121.59 3.20 2 12 -9 118.69 3.10 -2 -12 9 121.19 3.10 -2 -12 9 117.79 3.30 1 12 -9 2.10 0.60 1 12 -9 1.50 0.60 -1 -12 9 0.40 0.60 -1 -12 9 1.20 0.50 0 12 -9 92.39 2.70 0 -12 9 94.29 3.10 -1 12 -9 9.00 1.00 1 -12 9 9.90 1.20 -2 12 -9 4.40 0.90 2 -12 9 4.90 1.10 -3 12 -9 120.99 3.50 3 -12 9 112.19 3.80 -4 12 -9 115.89 3.50 4 -12 9 113.19 4.00 -5 12 -9 29.00 2.00 5 -12 9 27.60 2.40 -6 12 -9 70.89 2.80 6 -12 9 71.49 3.50 -7 12 -9 24.10 2.00 7 -12 9 18.00 2.30 -8 12 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3.00 7 -7 10 90.29 3.40 -8 7 -10 3.70 1.00 8 -7 10 3.50 1.20 -9 7 -10 64.89 2.70 9 -7 10 67.69 3.50 -10 7 -10 4.10 1.00 10 -7 10 2.60 1.20 -11 7 -10 16.70 1.80 11 -7 10 14.60 2.10 11 6 -10 62.59 3.30 -11 -6 10 65.39 3.60 10 6 -10 38.80 2.50 -10 -6 10 39.60 2.90 9 6 -10 118.09 4.00 -9 -6 10 119.09 4.50 8 6 -10 175.58 4.80 -8 -6 10 179.38 5.20 -8 -6 10 178.98 4.60 7 6 -10 253.97 5.70 -7 -6 10 255.17 5.70 -7 -6 10 257.87 6.30 6 6 -10 374.36 7.30 -6 -6 10 380.66 7.40 -6 -6 10 386.36 7.90 5 6 -10 199.28 4.50 -5 -6 10 204.28 4.60 -5 -6 10 207.18 5.00 4 6 -10 585.84 9.80 -4 -6 10 595.34 10.20 -4 -6 10 584.14 10.20 3 6 -10 250.67 4.90 -3 -6 10 253.37 5.20 -3 -6 10 252.47 5.20 2 6 -10 575.04 8.50 2 6 -10 580.54 9.20 -2 -6 10 560.24 9.40 -2 -6 10 572.44 9.80 1 6 -10 323.57 5.70 1 6 -10 332.97 5.30 -1 -6 10 332.77 6.30 -1 -6 10 326.77 5.80 0 6 -10 977.80 14.40 0 6 -10 977.70 14.30 0 -6 10 981.00 14.40 0 -6 10 954.40 15.40 -1 6 -10 201.48 3.80 -1 6 -10 202.58 3.80 1 -6 10 196.98 3.40 1 -6 10 202.38 4.40 -2 6 -10 15.60 1.00 -2 6 -10 15.10 0.90 2 -6 10 13.80 1.10 -3 6 -10 1.70 0.50 -3 6 -10 1.20 0.40 3 -6 10 2.00 0.60 -4 6 -10 37.30 1.60 -4 6 -10 38.40 1.30 4 -6 10 36.60 1.90 -5 6 -10 26.60 1.40 -5 6 -10 27.70 1.20 5 -6 10 25.40 1.60 -6 6 -10 1.10 0.60 -6 6 -10 0.70 0.40 6 -6 10 1.10 0.70 -7 6 -10 58.49 2.30 7 -6 10 59.29 2.70 -8 6 -10 42.60 2.10 8 -6 10 41.00 2.50 -9 6 -10 1.00 0.80 9 -6 10 1.40 1.00 -10 6 -10 24.30 1.80 10 -6 10 18.20 2.00 -11 6 -10 98.29 3.60 11 -6 10 99.69 4.40 12 5 -10 0.80 1.10 11 5 -10 54.29 3.10 -11 -5 10 51.29 3.20 10 5 -10 3.90 1.10 -10 -5 10 2.90 1.20 9 5 -10 63.79 2.90 -9 -5 10 62.89 2.80 -9 -5 10 66.99 3.40 8 5 -10 51.69 2.50 -8 -5 10 52.89 2.40 -8 -5 10 53.49 2.90 7 5 -10 116.19 3.50 -7 -5 10 114.09 3.90 -7 -5 10 117.99 3.50 6 5 -10 183.98 4.40 -6 -5 10 177.98 4.40 -6 -5 10 183.68 4.80 5 5 -10 18.30 1.30 -5 -5 10 18.50 1.40 -5 -5 10 17.20 1.40 4 5 -10 55.99 2.00 -4 -5 10 54.39 2.10 -4 -5 10 53.19 2.20 3 5 -10 671.53 10.70 -3 -5 10 676.13 11.30 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119.69 2.50 1 -3 10 121.09 2.30 -2 3 -10 45.90 1.40 2 -3 10 46.00 1.50 2 -3 10 45.90 1.70 2 -3 10 46.40 0.90 -3 3 -10 370.66 6.10 3 -3 10 369.86 6.40 3 -3 10 376.46 6.70 -4 3 -10 378.96 6.30 4 -3 10 381.06 6.70 4 -3 10 388.06 7.00 -5 3 -10 374.76 6.30 5 -3 10 385.96 7.20 5 -3 10 389.06 6.90 -6 3 -10 4.90 0.60 6 -3 10 5.00 0.80 6 -3 10 4.10 0.80 -7 3 -10 55.59 1.80 7 -3 10 54.09 2.30 7 -3 10 57.59 2.20 -8 3 -10 536.75 8.80 8 -3 10 525.25 9.40 8 -3 10 534.95 10.00 -9 3 -10 323.47 6.00 9 -3 10 319.47 7.10 10 -3 10 1.20 0.90 -11 3 -10 72.79 3.00 11 -3 10 77.89 3.50 -12 3 -10 16.90 1.70 12 -3 10 20.20 2.20 -13 3 -10 58.69 2.90 11 2 -10 1.00 1.20 -11 -2 10 -0.40 1.20 10 2 -10 7.00 1.30 10 2 -10 7.70 1.60 -10 -2 10 6.90 1.50 9 2 -10 200.38 5.50 9 2 -10 197.58 5.10 -9 -2 10 197.08 5.50 8 2 -10 110.09 3.70 8 2 -10 103.89 3.30 -8 -2 10 105.19 3.70 7 2 -10 42.30 2.20 7 2 -10 39.00 1.90 -7 -2 10 38.70 2.10 6 2 -10 246.98 5.60 6 2 -10 246.48 5.10 -6 -2 10 243.78 5.60 5 2 -10 596.84 9.90 5 2 -10 601.54 10.50 -5 -2 10 606.74 10.70 4 2 -10 214.88 4.70 4 2 -10 221.38 4.40 -4 -2 10 216.78 4.80 3 2 -10 170.78 3.50 3 2 -10 177.78 3.90 -3 -2 10 178.38 4.00 2 2 -10 518.45 8.40 2 2 -10 540.85 8.80 -2 -2 10 541.95 9.20 1 2 -10 10.30 0.80 1 2 -10 9.20 0.80 -1 -2 10 8.00 0.80 0 2 -10 40.20 1.20 0 2 -10 40.10 1.30 0 -2 10 39.20 1.60 0 -2 10 38.20 1.10 -1 2 -10 456.45 7.10 1 -2 10 454.75 7.10 1 -2 10 450.55 7.80 -2 2 -10 60.79 1.60 2 -2 10 55.59 1.90 2 -2 10 57.19 1.10 2 -2 10 58.59 1.70 -3 2 -10 261.07 4.50 3 -2 10 249.38 4.70 3 -2 10 254.87 4.90 -4 2 -10 127.49 2.70 4 -2 10 119.39 3.00 4 -2 10 125.09 3.00 -5 2 -10 5.00 0.60 5 -2 10 4.30 0.70 5 -2 10 6.00 0.90 -6 2 -10 101.79 2.50 6 -2 10 99.39 2.80 6 -2 10 98.79 2.90 -7 2 -10 0.70 0.50 7 -2 10 2.30 0.70 7 -2 10 0.50 0.60 -8 2 -10 15.80 1.20 8 -2 10 14.70 1.50 8 -2 10 11.30 1.20 -9 2 -10 425.86 7.60 9 -2 10 427.96 8.60 9 -2 10 437.86 8.20 -10 2 -10 3.50 0.80 10 -2 10 1.10 0.90 10 -2 10 2.40 1.00 11 -2 10 19.10 2.00 11 -2 10 20.00 1.80 -12 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2.70 1 -6 13 111.99 3.20 -2 6 -13 14.40 1.00 -2 6 -13 13.40 1.00 2 -6 13 14.10 1.30 -3 6 -13 63.19 2.10 -3 6 -13 64.19 2.00 3 -6 13 63.89 2.40 -4 6 -13 15.20 1.00 -4 6 -13 15.20 1.10 4 -6 13 11.60 1.30 -5 6 -13 83.69 2.70 -5 6 -13 83.29 2.30 5 -6 13 80.09 2.90 -6 6 -13 4.10 0.70 -6 6 -13 6.00 1.00 6 -6 13 5.30 1.10 -7 6 -13 54.39 1.90 -7 6 -13 53.69 2.30 7 -6 13 54.89 2.70 -8 6 -13 176.78 4.60 8 -6 13 172.78 5.20 -9 6 -13 66.59 2.90 9 -6 13 68.59 3.30 -10 6 -13 5.10 1.20 10 -6 13 5.30 1.50 -11 6 -13 180.48 5.10 11 -6 13 173.18 5.90 10 5 -13 35.50 2.60 -10 -5 13 28.50 2.70 9 5 -13 24.30 2.20 -9 -5 13 23.30 2.40 -9 -5 13 21.60 2.10 8 5 -13 -0.10 0.90 -8 -5 13 -0.80 0.90 -8 -5 13 1.70 1.00 7 5 -13 0.80 0.80 -7 -5 13 1.00 1.00 -7 -5 13 1.90 1.10 6 5 -13 289.77 6.30 -6 -5 13 292.57 6.80 -6 -5 13 294.17 6.50 5 5 -13 31.40 1.80 -5 -5 13 34.50 2.10 -5 -5 13 31.10 2.00 4 5 -13 61.49 2.30 -4 -5 13 63.69 2.60 -4 -5 13 60.39 2.60 3 5 -13 2.20 0.60 -3 -5 13 3.30 1.00 -3 -5 13 3.10 0.80 2 5 -13 22.40 1.40 -2 -5 13 22.60 1.50 -2 -5 13 25.10 1.80 1 5 -13 530.65 8.70 -1 -5 13 519.25 8.70 -1 -5 13 513.55 9.40 0 5 -13 1931.61 27.00 0 5 -13 1898.11 27.30 0 -5 13 1888.01 29.10 -1 5 -13 366.96 6.20 -1 5 -13 369.26 6.30 1 -5 13 357.26 7.00 -2 5 -13 37.00 1.40 -2 5 -13 36.90 1.40 2 -5 13 34.70 1.80 -3 5 -13 30.70 1.40 -3 5 -13 32.20 1.40 3 -5 13 29.40 1.70 -4 5 -13 512.55 8.30 -4 5 -13 512.85 8.70 4 -5 13 498.75 9.30 -5 5 -13 42.00 1.60 -5 5 -13 40.80 1.80 5 -5 13 41.70 2.10 -6 5 -13 15.50 1.10 -6 5 -13 15.50 1.40 6 -5 13 13.80 1.40 -7 5 -13 40.50 1.60 -7 5 -13 36.90 1.90 7 -5 13 37.40 2.20 -8 5 -13 44.90 1.90 -8 5 -13 48.70 2.40 8 -5 13 46.10 2.50 -9 5 -13 13.80 1.50 9 -5 13 11.20 1.70 -10 5 -13 6.80 1.30 10 -5 13 6.90 1.40 -11 5 -13 22.40 2.10 11 -5 13 21.40 2.30 10 4 -13 1.30 1.10 -10 -4 13 -0.60 1.00 -10 -4 13 1.80 1.20 9 4 -13 5.30 1.20 -9 -4 13 3.60 1.20 8 4 -13 48.90 2.60 8 4 -13 50.49 2.80 -8 -4 13 43.80 2.60 7 4 -13 45.50 2.60 7 4 -13 47.70 2.40 -7 -4 13 48.00 2.60 6 4 -13 140.79 3.90 6 4 -13 140.99 4.20 -6 -4 13 147.39 4.20 5 4 -13 122.99 3.70 5 4 -13 130.69 3.50 -5 -4 13 124.99 3.70 4 4 -13 20.10 1.50 4 4 -13 21.70 1.40 -4 -4 13 18.70 1.70 3 4 -13 163.08 3.70 -3 -4 13 160.68 4.20 2 4 -13 0.80 0.50 -2 -4 13 0.40 0.50 -2 -4 13 0.90 0.80 1 4 -13 12.50 1.00 -1 -4 13 11.20 1.10 -1 -4 13 9.90 1.10 0 4 -13 1.90 0.50 0 4 -13 1.40 0.40 0 -4 13 2.00 0.90 0 -4 13 1.20 0.60 -1 4 -13 131.19 2.80 -1 4 -13 126.29 2.90 1 -4 13 134.89 3.50 -2 4 -13 3.90 0.60 -2 4 -13 3.90 0.60 2 -4 13 4.70 0.90 -3 4 -13 65.49 1.90 3 -4 13 63.99 2.30 -4 4 -13 30.10 1.30 4 -4 13 29.80 1.70 -5 4 -13 22.60 1.20 5 -4 13 23.30 1.60 5 -4 13 23.40 1.50 -6 4 -13 28.80 1.40 6 -4 13 30.80 1.80 -7 4 -13 1.80 0.60 7 -4 13 2.90 0.90 -8 4 -13 58.59 2.10 8 -4 13 54.19 2.60 -9 4 -13 69.89 2.90 -9 4 -13 67.59 2.30 9 -4 13 67.39 3.10 -10 4 -13 15.40 1.70 10 -4 13 16.30 1.80 -11 4 -13 53.09 2.70 11 -4 13 53.09 3.10 -12 4 -13 3.20 1.10 12 -4 13 2.60 1.40 10 3 -13 27.20 2.30 10 3 -13 26.80 2.60 -10 -3 13 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180.18 5.40 -9 -7 14 190.28 6.00 8 7 -14 3.50 1.10 -8 -7 14 4.30 1.40 -8 -7 14 1.10 1.10 7 7 -14 46.80 2.60 -7 -7 14 47.60 2.80 -7 -7 14 39.20 2.50 6 7 -14 0.20 0.80 -6 -7 14 1.30 1.10 -6 -7 14 2.60 1.20 5 7 -14 112.29 3.50 -5 -7 14 108.69 3.60 -5 -7 14 113.09 3.70 4 7 -14 25.10 1.60 -4 -7 14 28.80 1.90 -4 -7 14 29.30 2.10 3 7 -14 45.60 2.00 -3 -7 14 47.70 2.10 -3 -7 14 46.00 2.40 2 7 -14 4.60 0.80 -2 -7 14 4.50 1.10 1 7 -14 -0.10 0.50 -1 -7 14 0.20 0.70 0 7 -14 34.60 1.60 0 -7 14 34.50 1.90 -1 7 -14 162.58 3.60 -1 7 -14 154.28 3.40 1 -7 14 144.29 3.90 -2 7 -14 16.60 1.20 -2 7 -14 17.70 1.20 2 -7 14 19.70 1.60 -3 7 -14 0.00 0.50 -3 7 -14 -0.70 0.50 3 -7 14 0.50 0.60 -4 7 -14 178.18 3.90 -4 7 -14 180.98 4.20 4 -7 14 182.48 4.80 -5 7 -14 63.79 2.10 -5 7 -14 65.29 2.40 5 -7 14 63.89 2.70 -6 7 -14 256.67 5.60 -6 7 -14 245.08 4.90 6 -7 14 254.47 6.20 -7 7 -14 74.99 2.90 7 -7 14 73.49 3.30 -8 7 -14 0.60 0.80 8 -7 14 1.70 1.00 -9 7 -14 11.60 1.40 9 -7 14 15.70 2.00 -10 7 -14 52.99 2.80 10 -7 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2 -14 143.49 3.60 4 2 -14 145.89 4.00 -4 -2 14 148.09 4.20 3 2 -14 6.50 0.90 3 2 -14 8.00 1.00 -3 -2 14 5.90 1.00 2 2 -14 298.87 5.90 2 2 -14 305.67 5.70 1 2 -14 270.47 5.20 1 2 -14 253.77 5.00 -1 -2 14 275.47 5.80 0 2 -14 104.49 2.60 0 2 -14 103.69 2.50 0 -2 14 104.89 3.20 1 -2 14 18.30 1.60 1 -2 14 18.00 1.00 -2 2 -14 26.10 1.20 2 -2 14 25.00 1.60 2 -2 14 22.60 1.20 -3 2 -14 314.97 5.60 3 -2 14 314.07 6.20 3 -2 14 309.77 5.80 -4 2 -14 212.68 4.10 4 -2 14 200.18 4.30 4 -2 14 199.48 4.60 -5 2 -14 6.10 0.80 5 -2 14 5.60 0.90 5 -2 14 6.30 1.00 -6 2 -14 101.89 2.70 6 -2 14 95.99 3.00 6 -2 14 104.59 3.10 -7 2 -14 301.67 5.80 7 -2 14 299.57 6.40 7 -2 14 312.07 6.40 -8 2 -14 224.58 4.80 8 -2 14 231.28 5.50 8 -2 14 232.88 5.40 -9 2 -14 40.30 1.90 9 -2 14 39.20 2.20 9 -2 14 42.40 2.30 -10 2 -14 33.40 1.90 10 -2 14 31.90 2.10 10 -2 14 35.20 2.30 -11 2 -14 180.38 4.50 11 -2 14 190.68 5.20 11 -2 14 185.98 5.40 -10 -1 14 30.00 2.70 9 1 -14 0.70 1.10 -9 -1 14 2.50 1.20 8 1 -14 11.40 1.70 8 1 -14 11.30 1.40 -8 -1 14 11.60 1.70 7 1 -14 41.90 2.20 7 1 -14 40.40 2.50 -7 -1 14 43.00 2.70 6 1 -14 16.00 1.50 6 1 -14 13.40 1.60 -6 -1 14 15.30 1.80 5 1 -14 159.28 4.00 5 1 -14 160.98 4.50 -5 -1 14 161.98 4.60 4 1 -14 537.35 9.30 4 1 -14 557.94 10.00 -4 -1 14 554.44 10.40 3 1 -14 137.59 3.40 3 1 -14 140.19 3.70 -3 -1 14 137.09 4.00 2 1 -14 0.40 0.60 2 1 -14 0.50 0.50 -2 -1 14 0.00 0.70 1 1 -14 16.80 1.20 1 1 -14 18.60 1.20 -1 -1 14 17.60 1.60 0 1 -14 195.48 4.00 0 1 -14 196.78 4.00 0 -1 14 196.98 4.60 -1 1 -14 64.29 1.90 1 -1 14 61.99 2.30 1 -1 14 62.79 1.80 -2 1 -14 388.76 6.60 2 -1 14 392.56 7.30 2 -1 14 395.16 6.70 -3 1 -14 21.90 1.10 3 -1 14 19.30 1.40 3 -1 14 18.50 1.20 -4 1 -14 20.60 1.10 4 -1 14 21.40 1.40 4 -1 14 21.30 1.50 -5 1 -14 67.09 2.10 5 -1 14 67.29 2.40 5 -1 14 66.69 2.30 -6 1 -14 78.79 2.40 6 -1 14 79.59 2.60 6 -1 14 78.89 2.70 -7 1 -14 28.60 1.50 7 -1 14 27.50 1.60 7 -1 14 31.80 1.90 -8 1 -14 78.59 2.50 8 -1 14 78.29 2.90 8 -1 14 73.49 2.80 -9 1 -14 43.50 2.00 9 -1 14 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115.39 4.10 -4 -6 21 116.59 4.60 3 6 -21 7.10 1.40 -3 -6 21 5.50 1.70 2 6 -21 32.10 2.20 -2 -6 21 30.80 2.80 1 6 -21 19.00 1.70 -1 -6 21 17.00 2.10 0 6 -21 3.80 1.00 0 -6 21 2.70 1.40 -1 6 -21 -0.80 0.70 1 -6 21 -0.60 0.90 -2 6 -21 13.60 1.50 2 -6 21 16.80 1.90 -3 6 -21 29.20 1.80 3 -6 21 34.30 2.40 -4 6 -21 100.79 3.30 4 -6 21 107.69 4.00 -5 6 -21 50.69 2.30 5 -6 21 49.99 2.90 -6 6 -21 5.50 1.10 -6 6 -21 8.40 1.20 6 -6 21 6.60 1.40 -7 6 -21 23.00 2.00 -7 6 -21 22.40 1.70 7 -6 21 25.50 2.40 -5 -5 21 -0.70 1.60 4 5 -21 3.20 1.20 -4 -5 21 1.20 1.50 3 5 -21 9.50 1.60 -3 -5 21 9.80 1.90 2 5 -21 12.80 1.60 -2 -5 21 12.90 1.90 1 5 -21 70.69 2.90 -1 -5 21 72.59 3.60 0 5 -21 135.89 4.00 0 -5 21 135.69 4.60 -1 5 -21 24.40 1.70 1 -5 21 24.00 2.20 -2 5 -21 7.50 1.10 2 -5 21 5.50 1.30 -3 5 -21 60.79 2.50 3 -5 21 61.49 3.00 -4 5 -21 0.00 0.70 4 -5 21 2.40 1.10 -5 5 -21 -0.40 0.70 5 -5 21 1.10 1.00 -6 5 -21 116.19 3.50 -6 5 -21 115.09 3.70 6 -5 21 111.19 4.10 -7 5 -21 48.80 2.30 -7 5 -21 41.90 2.50 7 -5 21 54.49 2.90 -8 5 -21 16.30 1.80 -8 5 -21 18.40 1.70 8 -5 21 16.10 2.00 5 4 -21 7.90 1.40 -5 -4 21 4.70 1.70 4 4 -21 2.80 1.10 -4 -4 21 -0.30 1.40 3 4 -21 0.80 0.90 -3 -4 21 -1.40 1.30 2 4 -21 149.09 4.30 -2 -4 21 149.19 5.00 1 4 -21 17.10 1.70 -1 -4 21 19.20 2.20 0 4 -21 12.90 1.50 0 -4 21 13.00 1.90 -1 4 -21 19.40 1.70 1 -4 21 17.90 1.90 -2 4 -21 92.59 3.10 2 -4 21 91.69 3.70 -3 4 -21 18.50 1.60 3 -4 21 13.70 1.60 -4 4 -21 9.50 1.20 4 -4 21 8.10 1.30 -5 4 -21 26.40 1.80 5 -4 21 26.00 2.10 -6 4 -21 14.00 1.50 -6 4 -21 12.10 1.30 6 -4 21 13.10 1.60 -7 4 -21 -0.40 0.80 -7 4 -21 0.20 0.80 7 -4 21 3.20 1.10 -8 4 -21 82.19 3.30 -8 4 -21 77.09 2.90 8 -4 21 80.09 3.60 5 3 -21 0.60 1.00 -5 -3 21 -1.30 1.30 4 3 -21 21.30 2.00 -4 -3 21 19.40 2.20 3 3 -21 2.90 1.00 -3 -3 21 0.00 1.30 2 3 -21 21.60 1.90 -2 -3 21 23.00 2.30 1 3 -21 223.08 5.30 -1 -3 21 226.68 6.10 0 3 -21 294.37 6.30 0 -3 21 309.37 7.30 -1 3 -21 8.70 1.20 1 -3 21 5.40 1.50 -2 3 -21 -0.40 0.60 2 -3 21 -1.80 1.00 -3 3 -21 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10.40 1.40 -4 -1 21 11.90 1.90 3 1 -21 119.69 3.70 -3 -1 21 110.29 4.30 2 1 -21 -0.50 0.70 -2 -1 21 -0.40 1.30 1 1 -21 50.99 2.40 -1 -1 21 55.19 3.20 0 1 -21 -0.40 0.70 0 -1 21 -0.60 1.20 -1 1 -21 37.90 2.10 1 -1 21 42.60 2.60 -2 1 -21 52.09 2.30 2 -1 21 55.69 3.00 -3 1 -21 0.50 0.70 3 -1 21 -1.20 0.90 -4 1 -21 0.60 0.70 4 -1 21 0.50 1.00 -5 1 -21 0.70 0.70 5 -1 21 1.80 1.00 -6 1 -21 33.00 1.90 6 -1 21 33.90 2.10 6 -1 21 39.10 2.30 -7 1 -21 7.50 1.20 7 -1 21 5.00 1.20 7 -1 21 6.30 1.10 -8 1 -21 9.90 1.30 8 -1 21 8.70 1.50 8 -1 21 8.40 1.30 -9 1 -21 221.18 5.40 9 -1 21 231.78 6.10 9 -1 21 252.07 6.20 -10 1 -21 92.09 3.30 10 -1 21 92.79 3.80 5 0 -21 10.70 1.50 4 0 -21 2.40 1.00 -4 0 21 1.20 1.30 3 0 -21 82.89 3.00 -3 0 21 78.59 3.60 2 0 -21 0.30 0.80 -2 0 21 -2.20 1.00 1 0 -21 176.98 4.50 -1 0 21 181.08 5.30 0 0 -21 4.90 0.90 0 0 21 8.20 1.70 -1 0 -21 75.09 2.70 1 0 21 81.29 3.50 -2 0 -21 0.60 0.70 2 0 21 1.80 1.20 -3 0 -21 13.30 1.40 3 0 21 11.60 1.50 -4 0 -21 1.00 0.70 4 0 21 1.20 0.90 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0.19 0.00 9 -11 9 0.07 0.00 10 -10 9 0.10 0.00 -12 -9 9 -0.57 0.00 13 -4 9 -0.27 0.00 -12 -3 9 0.01 0.00 -12 -2 9 -0.04 0.00 -12 -1 9 0.02 0.00 13 -1 9 -0.07 0.00 14 -1 9 -0.05 0.00 -12 0 9 -0.34 0.00 14 0 9 0.24 0.00 15 5 9 0.16 0.00 -10 6 9 -0.36 0.00 15 6 9 -0.23 0.00 15 7 9 0.10 0.00 15 8 9 0.13 0.00 -8 10 9 0.10 0.00 -7 12 9 -0.15 0.00 -6 13 9 -0.16 0.00 14 13 9 0.40 0.00 -1 18 9 0.28 0.00 1 19 9 -0.36 0.00 9 19 9 -0.29 0.00 4 20 9 0.13 0.00 5 20 9 -0.04 0.00 6 20 9 0.07 0.00 -5 -18 10 -0.27 0.00 -4 -18 10 0.39 0.00 -3 -18 10 -0.21 0.00 -2 -18 10 0.09 0.00 0 -18 10 0.09 0.00 -7 -17 10 0.23 0.00 -5 -17 10 0.25 0.00 -4 -17 10 0.00 0.00 -3 -17 10 -0.17 0.00 -2 -17 10 0.14 0.00 -4 -16 10 0.41 0.00 -3 -16 10 -0.45 0.00 -2 -16 10 0.45 0.00 4 -16 10 -0.23 0.00 -3 -15 10 -0.17 0.00 -2 -15 10 0.58 0.00 7 -13 10 0.23 0.00 8 -12 10 0.05 0.00 -11 -11 10 0.08 0.00 9 -11 10 0.05 0.00 11 -8 10 -0.33 0.00 -12 -7 10 -0.31 0.00 -12 -6 10 -0.01 0.00 12 -6 10 0.24 0.00 -12 -4 10 0.03 0.00 -12 -3 10 0.00 0.00 13 -1 10 -0.42 0.00 14 0 10 0.03 0.00 -9 8 10 -0.05 0.00 -7 11 10 0.13 0.00 -5 14 10 -0.10 0.00 -4 15 10 0.28 0.00 13 15 10 0.23 0.00 -3 16 10 -0.12 0.00 2 19 10 0.10 0.00 9 19 10 0.04 0.00 -6 -17 11 0.14 0.00 -5 -17 11 -0.27 0.00 -4 -17 11 0.38 0.00 -3 -17 11 -0.36 0.00 -2 -17 11 0.26 0.00 -1 -17 11 -0.30 0.00 -4 -16 11 -0.22 0.00 -3 -16 11 -0.20 0.00 -2 -16 11 0.47 0.00 -1 -16 11 -0.57 0.00 -3 -15 11 0.13 0.00 -2 -15 11 0.07 0.00 5 -15 11 0.00 0.00 6 -14 11 -0.19 0.00 7 -13 11 -0.15 0.00 8 -12 11 -0.13 0.00 -11 -10 11 0.23 0.00 -11 -9 11 0.41 0.00 10 -9 11 0.15 0.00 13 -1 11 -0.10 0.00 14 0 11 0.11 0.00 -11 1 11 0.54 0.00 -9 7 11 -0.10 0.00 -8 9 11 0.12 0.00 -6 12 11 -0.07 0.00 14 12 11 0.45 0.00 10 18 11 0.02 0.00 3 19 11 -0.29 0.00 4 19 11 0.37 0.00 8 19 11 0.35 0.00 -5 -17 12 0.26 0.00 -4 -17 12 -0.11 0.00 -3 -17 12 -0.18 0.00 -2 -17 12 0.27 0.00 -1 -17 12 -0.24 0.00 0 -17 12 0.17 0.00 -4 -16 12 0.17 0.00 -3 -16 12 -0.09 0.00 -2 -16 12 0.05 0.00 -1 -16 12 -0.21 0.00 3 -16 12 -0.49 0.00 -3 -15 12 0.15 0.00 -2 -15 12 0.28 0.00 9 -10 12 -0.12 0.00 10 -9 12 0.01 0.00 -11 -8 12 0.41 0.00 -11 -3 12 -0.04 0.00 13 -3 12 -0.24 0.00 12 -2 12 0.20 0.00 -11 -1 12 0.06 0.00 -10 3 12 -0.20 0.00 -9 6 12 -0.07 0.00 -8 8 12 0.09 0.00 -7 10 12 -0.22 0.00 -5 13 12 -0.08 0.00 13 14 12 0.11 0.00 -2 16 12 -0.04 0.00 11 17 12 -0.08 0.00 1 18 12 -0.26 0.00 4 19 12 0.07 0.00 5 19 12 -0.02 0.00 6 19 12 -0.19 0.00 7 19 12 0.11 0.00 -2 -17 13 -0.01 0.00 -4 -16 13 -0.26 0.00 -3 -16 13 0.04 0.00 -2 -16 13 0.28 0.00 -1 -16 13 -0.53 0.00 2 -16 13 0.21 0.00 -7 -15 13 -0.02 0.00 -2 -15 13 -0.19 0.00 4 -15 13 0.50 0.00 -8 -14 13 -0.17 0.00 5 -14 13 -0.29 0.00 7 -12 13 0.02 0.00 8 -11 13 0.14 0.00 -10 -10 13 -0.28 0.00 9 -10 13 -0.15 0.00 11 -7 13 0.02 0.00 12 -5 13 0.09 0.00 12 -2 13 0.26 0.00 13 -2 13 -0.24 0.00 14 1 13 0.07 0.00 -10 2 13 -0.05 0.00 -9 5 13 0.08 0.00 -8 7 13 0.09 0.00 -7 9 13 -0.09 0.00 -6 11 13 0.20 0.00 14 11 13 0.11 0.00 -2 15 13 -0.06 0.00 -1 16 13 0.01 0.00 0 17 13 0.20 0.00 2 18 13 -0.29 0.00 9 18 13 -0.08 0.00 -4 -16 14 0.06 0.00 -3 -16 14 0.08 0.00 -2 -16 14 -0.12 0.00 -1 -16 14 0.01 0.00 1 -16 14 -0.18 0.00 -6 -15 14 -0.17 0.00 -2 -15 14 -0.07 0.00 3 -15 14 -0.23 0.00 -7 -14 14 0.24 0.00 -8 -13 14 0.11 0.00 6 -13 14 0.22 0.00 7 -12 14 -0.01 0.00 -9 -11 14 -0.09 0.00 8 -11 14 -0.06 0.00 -10 -8 14 -0.47 0.00 10 -8 14 0.02 0.00 -10 -7 14 -0.22 0.00 12 -2 14 0.14 0.00 13 -1 14 -0.21 0.00 -10 0 14 -0.46 0.00 -9 4 14 0.24 0.00 -8 6 14 0.11 0.00 -7 8 14 -0.02 0.00 14 9 14 0.66 0.00 -6 10 14 0.14 0.00 14 10 14 0.19 0.00 -4 13 14 0.19 0.00 13 13 14 0.04 0.00 -3 14 14 -0.17 0.00 -2 15 14 0.34 0.00 12 15 14 -0.08 0.00 11 16 14 -0.20 0.00 10 17 14 0.10 0.00 3 18 14 -0.30 0.00 4 18 14 0.54 0.00 8 18 14 0.31 0.00 -2 -15 15 -0.24 0.00 2 -15 15 0.22 0.00 -6 -14 15 -0.18 0.00 4 -14 15 0.35 0.00 -7 -13 15 -0.15 0.00 8 -10 15 0.03 0.00 9 -9 15 -0.12 0.00 11 -6 15 -0.09 0.00 12 -3 15 0.25 0.00 12 -2 15 0.18 0.00 13 -1 15 -0.01 0.00 -9 2 15 0.11 0.00 14 4 15 -0.03 0.00 -8 5 15 0.02 0.00 14 5 15 0.23 0.00 14 6 15 0.23 0.00 -7 7 15 -0.04 0.00 14 7 15 0.65 0.00 14 8 15 0.50 0.00 -6 9 15 -0.04 0.00 -5 11 15 -0.14 0.00 13 11 15 0.24 0.00 13 12 15 0.00 0.00 -1 15 15 0.07 0.00 0 16 15 -0.08 0.00 10 16 15 0.39 0.00 9 17 15 -0.19 0.00 6 18 15 0.06 0.00 -2 -15 16 -0.07 0.00 -1 -15 16 0.09 0.00 0 -15 16 0.04 0.00 -5 -14 16 -0.27 0.00 3 -14 16 -0.11 0.00 -6 -13 16 -0.10 0.00 -7 -12 16 -0.43 0.00 6 -12 16 0.17 0.00 -7 -11 16 -0.29 0.00 7 -11 16 -0.10 0.00 -8 -10 16 0.13 0.00 -9 -7 16 0.29 0.00 10 -7 16 0.13 0.00 12 -3 16 0.18 0.00 12 -2 16 -0.19 0.00 -9 -1 16 -0.15 0.00 -9 0 16 0.30 0.00 13 0 16 0.02 0.00 -8 3 16 -0.17 0.00 -8 4 16 -0.15 0.00 -7 6 16 -0.04 0.00 -6 8 16 -0.13 0.00 -5 10 16 -0.21 0.00 13 10 16 0.13 0.00 13 11 16 -0.03 0.00 12 13 16 -0.12 0.00 11 15 16 -0.22 0.00 1 16 16 -0.02 0.00 9 16 16 -0.37 0.00 10 16 16 0.35 0.00 3 17 16 0.17 0.00 8 17 16 0.19 0.00 -3 -14 17 0.07 0.00 1 -14 17 0.08 0.00 -5 -13 17 -0.09 0.00 -6 -12 17 0.03 0.00 -6 -11 17 0.37 0.00 -7 -10 17 -0.23 0.00 8 -9 17 0.24 0.00 -8 -8 17 -0.19 0.00 9 -8 17 -0.22 0.00 12 -2 17 0.00 0.00 -8 2 17 -0.13 0.00 -7 5 17 0.03 0.00 -6 7 17 -0.11 0.00 13 7 17 0.13 0.00 13 8 17 0.22 0.00 -5 9 17 -0.12 0.00 13 9 17 0.15 0.00 13 10 17 -0.05 0.00 -3 12 17 -0.25 0.00 12 12 17 -0.12 0.00 -2 13 17 0.37 0.00 -1 14 17 -0.26 0.00 11 14 17 -0.14 0.00 2 16 17 -0.06 0.00 8 16 17 0.37 0.00 9 16 17 -0.34 0.00 -3 -13 18 -0.14 0.00 2 -13 18 0.03 0.00 4 -12 18 0.18 0.00 9 -7 18 -0.23 0.00 -8 -4 18 0.18 0.00 -8 -3 18 0.43 0.00 -8 -2 18 0.18 0.00 12 -1 18 -0.11 0.00 -7 3 18 0.21 0.00 13 4 18 0.05 0.00 13 5 18 -0.06 0.00 -6 6 18 -0.08 0.00 13 6 18 0.11 0.00 13 7 18 0.16 0.00 -5 8 18 0.04 0.00 13 8 18 0.21 0.00 -3 11 18 -0.22 0.00 12 11 18 -0.03 0.00 -1 13 18 -0.22 0.00 0 14 18 0.04 0.00 9 15 18 -0.65 0.00 4 16 18 0.34 0.00 5 16 18 -0.28 0.00 7 16 18 0.00 0.00 -3 -12 19 -0.11 0.00 2 -12 19 -0.07 0.00 4 -11 19 0.17 0.00 7 -9 19 -0.13 0.00 -7 -6 19 0.49 0.00 -7 -5 19 0.31 0.00 -7 0 19 -0.21 0.00 -6 4 19 -0.26 0.00 12 8 19 0.20 0.00 3 9 19 -0.51 0.00 12 9 19 0.24 0.00 -3 10 19 -0.07 0.00 3 10 19 0.02 0.00 12 10 19 0.14 0.00 11 12 19 0.33 0.00 0 13 19 -0.06 0.00 3 15 19 -0.11 0.00 8 15 19 0.02 0.00 3 -11 20 -0.01 0.00 -4 -10 20 0.03 0.00 4 -10 20 0.17 0.00 5 -9 20 -0.14 0.00 6 -9 20 -0.04 0.00 7 -8 20 -0.03 0.00 -6 -6 20 -0.19 0.00 11 -1 20 -0.05 0.00 12 3 20 -0.01 0.00 12 4 20 0.04 0.00 -5 5 20 0.29 0.00 12 5 20 0.00 0.00 12 6 20 -0.08 0.00 -4 7 20 -0.23 0.00 12 7 20 0.05 0.00 12 8 20 0.13 0.00 3 9 20 0.33 0.00 -2 10 20 -0.02 0.00 2 10 20 0.40 0.00 3 10 20 -0.15 0.00 11 10 20 0.17 0.00 2 11 20 0.08 0.00 3 11 20 -0.30 0.00 11 11 20 0.31 0.00 3 12 20 -0.09 0.00 4 12 20 0.05 0.00 1 13 20 0.18 0.00 3 13 20 0.02 0.00 4 13 20 0.08 0.00 3 14 20 0.08 0.00 4 14 20 0.36 0.00 8 14 20 0.20 0.00 -2 -10 21 0.36 0.00 3 -10 21 -0.11 0.00 -4 -8 21 0.26 0.00 6 -8 21 0.06 0.00 7 -7 21 -0.11 0.00 -5 -6 21 -0.06 0.00 9 -4 21 0.03 0.00 10 -2 21 0.13 0.00 -5 1 21 -0.18 0.00 11 1 21 -0.06 0.00 -5 2 21 -0.26 0.00 11 2 21 -0.02 0.00 11 3 21 -0.14 0.00 -4 5 21 0.01 0.00 11 6 21 -0.10 0.00 11 7 21 -0.26 0.00 11 8 21 -0.14 0.00 2 9 21 0.58 0.00 3 9 21 -0.40 0.00 11 9 21 0.02 0.00 -1 10 21 0.14 0.00 1 10 21 0.20 0.00 2 10 21 0.01 0.00 3 10 21 -0.04 0.00 4 10 21 -0.13 0.00 0 11 21 -0.14 0.00 1 11 21 0.15 0.00 2 11 21 -0.06 0.00 3 11 21 0.03 0.00 4 11 21 -0.17 0.00 10 11 21 0.18 0.00 1 12 21 0.26 0.00 2 12 21 -0.20 0.00 3 12 21 -0.10 0.00 4 12 21 0.09 0.00 9 12 21 -0.88 0.00 3 13 21 0.15 0.00 4 13 21 0.14 0.00 8 13 21 0.33 0.00 -1 -9 22 -0.25 0.00 0 -9 22 0.37 0.00 2 -9 22 0.00 0.00 -2 -8 22 -0.15 0.00 -3 -7 22 -0.41 0.00 -4 -5 22 0.27 0.00 -4 -4 22 0.06 0.00 10 0 22 0.41 0.00 -4 2 22 0.23 0.00 -3 4 22 -0.12 0.00 -3 5 22 -0.14 0.00 -2 7 22 -0.05 0.00 2 9 22 -0.06 0.00 3 9 22 0.05 0.00 10 9 22 0.03 0.00 1 10 22 -0.29 0.00 2 10 22 0.26 0.00 3 10 22 -0.08 0.00 4 10 22 -0.09 0.00 5 10 22 0.15 0.00 2 11 22 -0.04 0.00 3 11 22 -0.12 0.00 4 11 22 0.06 0.00 5 11 22 0.15 0.00 9 11 22 -0.90 0.00 3 12 22 0.08 0.00 4 12 22 -0.07 0.00 5 12 22 0.15 0.00 -1 -7 23 0.12 0.00 0 -7 23 0.03 0.00 1 -7 23 -0.22 0.00 4 -7 23 0.00 0.00 -2 -6 23 0.40 0.00 -1 -6 23 -0.23 0.00 -2 -5 23 0.07 0.00 -3 -4 23 -0.34 0.00 -3 -3 23 -0.16 0.00 -3 2 23 -0.03 0.00 10 3 23 0.45 0.00 -2 4 23 0.12 0.00 10 4 23 0.16 0.00 -2 5 23 -0.10 0.00 10 5 23 0.19 0.00 10 6 23 0.02 0.00 -1 7 23 -0.01 0.00 0 8 23 0.16 0.00 3 8 23 -0.07 0.00 1 9 23 -0.43 0.00 2 9 23 0.35 0.00 3 9 23 -0.21 0.00 4 9 23 0.08 0.00 9 9 23 -0.55 0.00 2 10 23 0.07 0.00 3 10 23 -0.08 0.00 4 10 23 0.01 0.00 5 10 23 0.09 0.00 8 10 23 0.72 0.00 4 11 23 -0.10 0.00 5 11 23 0.24 0.00 6 11 23 -0.21 0.00 1 -6 24 -0.14 0.00 2 -6 24 0.26 0.00 3 -6 24 -0.22 0.00 0 -5 24 -0.01 0.00 1 -5 24 0.07 0.00 2 -5 24 0.00 0.00 3 -5 24 -0.05 0.00 4 -5 24 0.01 0.00 -1 -4 24 -0.12 0.00 0 -4 24 0.03 0.00 5 -4 24 -0.33 0.00 -1 -3 24 -0.08 0.00 -2 -2 24 0.25 0.00 7 -2 24 -0.31 0.00 -2 -1 24 -0.05 0.00 -2 0 24 0.36 0.00 -2 1 24 -0.03 0.00 -1 4 24 0.21 0.00 9 4 24 -0.15 0.00 9 5 24 -0.10 0.00 0 6 24 -0.17 0.00 2 8 24 0.14 0.00 3 8 24 -0.19 0.00 8 8 24 0.68 0.00 3 9 24 -0.08 0.00 4 9 24 0.06 0.00 6 9 24 -0.06 0.00 7 9 24 -0.08 0.00 1 -3 25 0.02 0.00 2 -3 25 -0.23 0.00 3 -3 25 0.19 0.00 4 -3 25 0.10 0.00 0 -2 25 0.02 0.00 1 -2 25 -0.01 0.00 2 -2 25 -0.17 0.00 5 -2 25 -0.21 0.00 0 -1 25 0.26 0.00 1 -1 25 -0.26 0.00 6 -1 25 0.26 0.00 0 0 25 -0.07 0.00 0 1 25 0.18 0.00 7 1 25 -0.33 0.00 0 2 25 0.09 0.00 7 2 25 -0.01 0.00 6 3 25 0.12 0.00 7 3 25 -0.24 0.00 1 4 25 0.06 0.00 6 4 25 0.17 0.00 7 4 25 -0.21 0.00 7 5 25 -0.07 0.00 2 6 25 -0.01 0.00 6 6 25 -0.06 0.00 7 6 25 -0.06 0.00 4 7 25 0.10 0.00 5 7 25 -0.05 0.00 6 7 25 0.19 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 211117) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.500 0.000 0.000 190 41 ' ' 2 0.500 0.500 0.500 249 40 ' ' 3 0.267 0.643 0.854 7 0 ' ' 4 0.435 0.661 0.790 13 0 ' ' 5 0.571 0.340 0.207 13 0 ' ' 6 0.742 0.358 0.142 6 0 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 0 1 0 1.366 0 0 1 1.073 3 3 1 5.867 0 -1 2 2.564 3 0 2 5.701 -2 4 2 8.102 0 -2 3 4.260 4 -1 3 8.200 -3 3 3 9.133 -2 2 4 7.379 -4 -1 5 10.197 -3 -1 5 8.620 0 -2 6 7.054 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL si358a_R17P -1 R = 0.07 CELL 11.4093 15.6821 19.5623 84.80 75.91 71.97 SPGR P-1 # Solvent Accessible Volume = 478 # Electrons Found in S.A.V. = 81 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.500 1.000 0.000 ! 8.17 eA-3 C102 0.500 0.500 0.500 ! 4.57 eA-3 C103 0.408 0.100 0.027 ! 3.96 eA-3 C104 0.407 0.017 0.027 ! 3.90 eA-3 C105 0.311 0.093 0.074 ! 3.30 eA-3 C106 0.483 0.442 0.451 ! 2.72 eA-3 C107 0.516 0.378 0.453 ! 2.52 eA-3 ) ; _shelx_fab_checksum 76860 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si1 Si -0.12083(3) 0.90310(2) 0.24123(2) 0.02410(7) Uani 1 1 d . . . . . Si2 Si 0.03482(3) 0.80382(2) 0.27726(2) 0.02305(7) Uani 1 1 d . . . . . Si3 Si 0.13317(3) 0.66909(2) 0.21655(2) 0.02277(7) Uani 1 1 d . . . . . Si4 Si 0.05720(3) 0.55543(2) 0.24779(2) 0.02532(7) Uani 1 1 d . . . . . Si5 Si -0.20557(3) 0.88134(2) 0.14809(2) 0.03184(8) Uani 1 1 d . . . . . Si6 Si -0.13452(3) 0.56190(2) 0.32996(2) 0.03454(8) Uani 1 1 d . . . . . C1 C -0.18438(11) 1.01254(8) 0.29211(6) 0.0265(2) Uani 1 1 d . . . . . C2 C -0.08397(11) 1.00947(8) 0.33602(6) 0.0301(2) Uani 1 1 d . . . . . H1 H -0.0039 1.0107 0.3027 0.036 Uiso 1 1 calc R U . . . H2 H -0.1146 1.0645 0.3644 0.036 Uiso 1 1 calc R U . . . C3 C -0.05513(11) 0.92744(8) 0.38609(6) 0.0296(2) Uani 1 1 d . . . . . H3 H -0.1299 0.9050 0.3983 0.035 Uiso 1 1 calc R U . . . H4 H -0.0462 0.9486 0.4302 0.035 Uiso 1 1 calc R U . . . C4 C 0.06524(10) 0.84554(8) 0.35941(6) 0.0262(2) Uani 1 1 d . . . . . C5 C 0.15816(11) 0.44802(7) 0.19852(6) 0.0259(2) Uani 1 1 d . . . . . C6 C 0.28754(11) 0.46514(8) 0.16068(6) 0.0280(2) Uani 1 1 d . . . . . H5 H 0.3302 0.4723 0.1973 0.034 Uiso 1 1 calc R U . . . H6 H 0.3420 0.4111 0.1336 0.034 Uiso 1 1 calc R U . . . C7 C 0.27902(11) 0.54737(8) 0.11025(6) 0.0267(2) Uani 1 1 d . . . . . H7 H 0.2001 0.5600 0.0935 0.032 Uiso 1 1 calc R U . . . H8 H 0.3505 0.5305 0.0686 0.032 Uiso 1 1 calc R U . . . C8 C 0.28074(10) 0.63736(8) 0.13957(6) 0.0244(2) Uani 1 1 d . . . . . C9 C -0.12405(16) 0.92487(12) 0.06299(8) 0.0530(4) Uani 1 1 d . . . . . H9 H -0.1394 0.9896 0.0663 0.079 Uiso 1 1 calc R U . . . H10 H -0.1574 0.9133 0.0243 0.079 Uiso 1 1 calc R U . . . H11 H -0.0328 0.8944 0.0541 0.079 Uiso 1 1 calc R U . . . C10 C -0.38083(14) 0.93573(12) 0.16550(9) 0.0509(4) Uani 1 1 d . . . . . H12 H -0.4219 0.9106 0.2091 0.076 Uiso 1 1 calc R U . . . H13 H -0.4129 0.9245 0.1261 0.076 Uiso 1 1 calc R U . . . H14 H -0.3993 1.0005 0.1704 0.076 Uiso 1 1 calc R U . . . C11 C -0.18134(14) 0.75947(10) 0.13849(8) 0.0429(3) Uani 1 1 d . . . . . H15 H -0.1970 0.7496 0.0932 0.064 Uiso 1 1 calc R U . . . H16 H -0.2402 0.7391 0.1769 0.064 Uiso 1 1 calc R U . . . H17 H -0.0941 0.7256 0.1404 0.064 Uiso 1 1 calc R U . . . Si7 Si -0.18156(3) 1.11397(2) 0.23055(2) 0.03488(8) Uani 1 1 d . . . . . C12 C -0.01873(14) 1.09736(10) 0.17362(9) 0.0489(4) Uani 1 1 d . . . . . H18 H -0.0220 1.1415 0.1348 0.073 Uiso 1 1 calc R U . . . H19 H 0.0137 1.0367 0.1545 0.073 Uiso 1 1 calc R U . . . H20 H 0.0373 1.1052 0.2018 0.073 Uiso 1 1 calc R U . . . C13 C -0.28912(16) 1.14110(11) 0.16778(8) 0.0512(4) Uani 1 1 d . . . . . H21 H -0.2697 1.0893 0.1380 0.077 Uiso 1 1 calc R U . . . H22 H -0.2766 1.1928 0.1381 0.077 Uiso 1 1 calc R U . . . H23 H -0.3773 1.1554 0.1944 0.077 Uiso 1 1 calc R U . . . C14 C -0.22493(17) 1.21682(10) 0.28464(10) 0.0541(4) Uani 1 1 d . . . . . H24 H -0.2267 1.2694 0.2533 0.081 Uiso 1 1 calc R U . . . H25 H -0.1621 1.2099 0.3127 0.081 Uiso 1 1 calc R U . . . H26 H -0.3086 1.2249 0.3161 0.081 Uiso 1 1 calc R U . . . Si8 Si -0.34632(3) 1.02498(2) 0.35472(2) 0.03122(8) Uani 1 1 d . . . . . C15 C -0.48435(13) 1.10002(11) 0.32137(8) 0.0462(3) Uani 1 1 d . . . . . H27 H -0.4741 1.1600 0.3116 0.069 Uiso 1 1 calc R U . . . H28 H -0.5626 1.1038 0.3571 0.069 Uiso 1 1 calc R U . . . H29 H -0.4885 1.0755 0.2780 0.069 Uiso 1 1 calc R U . . . C16 C -0.35419(15) 1.07521(13) 0.43935(8) 0.0536(4) Uani 1 1 d . . . . . H30 H -0.2931 1.0338 0.4637 0.080 Uiso 1 1 calc R U . . . H31 H -0.4397 1.0862 0.4692 0.080 Uiso 1 1 calc R U . . . H32 H -0.3338 1.1320 0.4295 0.080 Uiso 1 1 calc R U . . . C17 C -0.38278(13) 0.91575(10) 0.37628(8) 0.0449(3) Uani 1 1 d . . . . . H33 H -0.4692 0.9268 0.4050 0.067 Uiso 1 1 calc R U . . . H34 H -0.3229 0.8767 0.4025 0.067 Uiso 1 1 calc R U . . . H35 H -0.3753 0.8866 0.3325 0.067 Uiso 1 1 calc R U . . . Si9 Si 0.21260(3) 0.88558(2) 0.34064(2) 0.03131(8) Uani 1 1 d . . . . . C18 C 0.25185(13) 0.93471(11) 0.25009(8) 0.0433(3) Uani 1 1 d . . . . . H36 H 0.2367 0.8998 0.2159 0.065 Uiso 1 1 calc R U . . . H37 H 0.3411 0.9331 0.2382 0.065 Uiso 1 1 calc R U . . . H38 H 0.1984 0.9970 0.2489 0.065 Uiso 1 1 calc R U . . . C19 C 0.18864(15) 0.97874(11) 0.40140(9) 0.0485(4) Uani 1 1 d . . . . . H39 H 0.2684 0.9929 0.3956 0.073 Uiso 1 1 calc R U . . . H40 H 0.1612 0.9599 0.4503 0.073 Uiso 1 1 calc R U . . . H41 H 0.1238 1.0321 0.3900 0.073 Uiso 1 1 calc R U . . . C20 C 0.35744(13) 0.79389(10) 0.35224(8) 0.0448(3) Uani 1 1 d . . . . . H42 H 0.3475 0.7749 0.4019 0.067 Uiso 1 1 calc R U . . . H43 H 0.4315 0.8159 0.3376 0.067 Uiso 1 1 calc R U . . . H44 H 0.3691 0.7428 0.3232 0.067 Uiso 1 1 calc R U . . . Si10 Si 0.06228(3) 0.76285(2) 0.43770(2) 0.03182(8) Uani 1 1 d . . . . . C21 C -0.10287(14) 0.75622(11) 0.47403(7) 0.0453(3) Uani 1 1 d . . . . . H45 H -0.1009 0.7058 0.5077 0.068 Uiso 1 1 calc R U . . . H46 H -0.1385 0.7472 0.4354 0.068 Uiso 1 1 calc R U . . . H47 H -0.1554 0.8121 0.4980 0.068 Uiso 1 1 calc R U . . . C22 C 0.10590(15) 0.80304(11) 0.51322(7) 0.0464(3) Uani 1 1 d . . . . . H48 H 0.1930 0.8060 0.4986 0.070 Uiso 1 1 calc R U . . . H49 H 0.0991 0.7612 0.5533 0.070 Uiso 1 1 calc R U . . . H50 H 0.0483 0.8628 0.5270 0.070 Uiso 1 1 calc R U . . . C23 C 0.16830(14) 0.64643(9) 0.41866(7) 0.0408(3) Uani 1 1 d . . . . . H51 H 0.1506 0.6237 0.3784 0.061 Uiso 1 1 calc R U . . . H52 H 0.1533 0.6078 0.4600 0.061 Uiso 1 1 calc R U . . . H53 H 0.2568 0.6466 0.4075 0.061 Uiso 1 1 calc R U . . . C24 C -0.10256(16) 0.52907(12) 0.41990(8) 0.0542(4) Uani 1 1 d . . . . . H54 H -0.1823 0.5315 0.4539 0.081 Uiso 1 1 calc R U . . . H55 H -0.0641 0.5706 0.4339 0.081 Uiso 1 1 calc R U . . . H56 H -0.0446 0.4680 0.4188 0.081 Uiso 1 1 calc R U . . . C25 C -0.21929(15) 0.48750(12) 0.30709(10) 0.0564(4) Uani 1 1 d . . . . . H57 H -0.2355 0.5036 0.2599 0.085 Uiso 1 1 calc R U . . . H58 H -0.2999 0.4950 0.3416 0.085 Uiso 1 1 calc R U . . . H59 H -0.1669 0.4249 0.3077 0.085 Uiso 1 1 calc R U . . . C26 C -0.24670(14) 0.67734(10) 0.33268(8) 0.0467(3) Uani 1 1 d . . . . . H60 H -0.3116 0.6848 0.3768 0.070 Uiso 1 1 calc R U . . . H61 H -0.2871 0.6867 0.2927 0.070 Uiso 1 1 calc R U . . . H62 H -0.2004 0.7212 0.3300 0.070 Uiso 1 1 calc R U . . . Si11 Si 0.20571(4) 0.34967(2) 0.26138(2) 0.03546(8) Uani 1 1 d . . . . . C27 C 0.28703(19) 0.37837(12) 0.32430(9) 0.0609(5) Uani 1 1 d . . . . . H63 H 0.2972 0.3315 0.3610 0.091 Uiso 1 1 calc R U . . . H64 H 0.2361 0.4360 0.3461 0.091 Uiso 1 1 calc R U . . . H65 H 0.3704 0.3826 0.2988 0.091 Uiso 1 1 calc R U . . . C28 C 0.31862(17) 0.25159(11) 0.20814(10) 0.0591(4) Uani 1 1 d . . . . . H66 H 0.3388 0.1992 0.2393 0.089 Uiso 1 1 calc R U . . . H67 H 0.3965 0.2662 0.1846 0.089 Uiso 1 1 calc R U . . . H68 H 0.2796 0.2382 0.1726 0.089 Uiso 1 1 calc R U . . . C29 C 0.07641(17) 0.30792(11) 0.31824(9) 0.0529(4) Uani 1 1 d . . . . . H69 H 0.0137 0.3572 0.3466 0.079 Uiso 1 1 calc R U . . . H70 H 0.1124 0.2596 0.3495 0.079 Uiso 1 1 calc R U . . . H71 H 0.0356 0.2851 0.2884 0.079 Uiso 1 1 calc R U . . . Si12 Si 0.08179(3) 0.41995(2) 0.12969(2) 0.02843(7) Uani 1 1 d . . . . . C30 C 0.20533(14) 0.37446(10) 0.04875(7) 0.0407(3) Uani 1 1 d . . . . . H72 H 0.1662 0.3561 0.0155 0.061 Uiso 1 1 calc R U . . . H73 H 0.2706 0.3225 0.0617 0.061 Uiso 1 1 calc R U . . . H74 H 0.2439 0.4209 0.0267 0.061 Uiso 1 1 calc R U . . . C31 C -0.00249(16) 0.33314(10) 0.15855(9) 0.0482(4) Uani 1 1 d . . . . . H75 H 0.0574 0.2770 0.1700 0.072 Uiso 1 1 calc R U . . . H76 H -0.0384 0.3230 0.1204 0.072 Uiso 1 1 calc R U . . . H77 H -0.0706 0.3540 0.2003 0.072 Uiso 1 1 calc R U . . . C32 C -0.03953(13) 0.51910(9) 0.10211(7) 0.0370(3) Uani 1 1 d . . . . . H78 H -0.0794 0.4998 0.0697 0.056 Uiso 1 1 calc R U . . . H79 H 0.0014 0.5637 0.0784 0.056 Uiso 1 1 calc R U . . . H80 H -0.1042 0.5456 0.1438 0.056 Uiso 1 1 calc R U . . . Si13 Si 0.26979(3) 0.71813(2) 0.06018(2) 0.02931(7) Uani 1 1 d . . . . . C33 C 0.22956(15) 0.83907(9) 0.08034(7) 0.0421(3) Uani 1 1 d . . . . . H81 H 0.1516 0.8561 0.1173 0.063 Uiso 1 1 calc R U . . . H82 H 0.2171 0.8754 0.0377 0.063 Uiso 1 1 calc R U . . . H83 H 0.2988 0.8493 0.0966 0.063 Uiso 1 1 calc R U . . . C34 C 0.42248(13) 0.69021(11) -0.00888(7) 0.0433(3) Uani 1 1 d . . . . . H84 H 0.4893 0.7001 0.0099 0.065 Uiso 1 1 calc R U . . . H85 H 0.4114 0.7288 -0.0506 0.065 Uiso 1 1 calc R U . . . H86 H 0.4462 0.6272 -0.0220 0.065 Uiso 1 1 calc R U . . . C35 C 0.15070(14) 0.70519(10) 0.01369(7) 0.0414(3) Uani 1 1 d . . . . . H87 H 0.1354 0.7537 -0.0214 0.062 Uiso 1 1 calc R U . . . H88 H 0.0713 0.7079 0.0481 0.062 Uiso 1 1 calc R U . . . H89 H 0.1832 0.6473 -0.0099 0.062 Uiso 1 1 calc R U . . . Si14 Si 0.43721(3) 0.61693(2) 0.16715(2) 0.03010(7) Uani 1 1 d . . . . . C36 C 0.48636(15) 0.72111(11) 0.16108(9) 0.0496(4) Uani 1 1 d . . . . . H90 H 0.5611 0.7091 0.1809 0.074 Uiso 1 1 calc R U . . . H91 H 0.4170 0.7689 0.1876 0.074 Uiso 1 1 calc R U . . . H92 H 0.5067 0.7399 0.1116 0.074 Uiso 1 1 calc R U . . . C37 C 0.56769(13) 0.53009(11) 0.10991(8) 0.0467(3) Uani 1 1 d . . . . . H93 H 0.6487 0.5258 0.1208 0.070 Uiso 1 1 calc R U . . . H94 H 0.5710 0.5474 0.0602 0.070 Uiso 1 1 calc R U . . . H95 H 0.5514 0.4718 0.1188 0.070 Uiso 1 1 calc R U . . . C38 C 0.43596(13) 0.57174(10) 0.25930(7) 0.0404(3) Uani 1 1 d . . . . . H96 H 0.3529 0.5989 0.2900 0.061 Uiso 1 1 calc R U . . . H97 H 0.5013 0.5861 0.2765 0.061 Uiso 1 1 calc R U . . . H98 H 0.4531 0.5065 0.2596 0.061 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.02202(15) 0.02790(15) 0.02374(15) 0.00164(12) -0.00816(11) -0.00764(12) Si2 0.02083(14) 0.02864(15) 0.02051(14) -0.00092(11) -0.00721(11) -0.00645(12) Si3 0.01957(14) 0.02742(15) 0.02157(14) -0.00010(11) -0.00253(11) -0.00909(12) Si4 0.02294(15) 0.02898(16) 0.02513(15) 0.00201(12) -0.00426(12) -0.01087(12) Si5 0.02726(17) 0.04162(19) 0.02854(16) 0.00139(14) -0.01353(13) -0.00796(14) Si6 0.02688(17) 0.03817(19) 0.03705(18) 0.00683(15) -0.00098(14) -0.01449(14) C1 0.0224(5) 0.0282(5) 0.0281(5) 0.0006(4) -0.0058(4) -0.0067(4) C2 0.0258(6) 0.0319(6) 0.0339(6) -0.0049(5) -0.0079(5) -0.0083(5) C3 0.0251(6) 0.0382(6) 0.0243(5) -0.0068(5) -0.0062(4) -0.0057(5) C4 0.0227(5) 0.0348(6) 0.0219(5) -0.0037(4) -0.0076(4) -0.0067(5) C5 0.0258(5) 0.0261(5) 0.0278(5) 0.0025(4) -0.0095(4) -0.0086(4) C6 0.0242(6) 0.0304(6) 0.0299(6) -0.0009(5) -0.0083(4) -0.0069(4) C7 0.0252(5) 0.0319(6) 0.0229(5) -0.0026(4) -0.0035(4) -0.0094(5) C8 0.0208(5) 0.0312(6) 0.0217(5) -0.0017(4) -0.0021(4) -0.0101(4) C9 0.0558(10) 0.0687(11) 0.0329(7) 0.0125(7) -0.0164(7) -0.0152(8) C10 0.0319(7) 0.0646(10) 0.0565(9) -0.0071(8) -0.0221(7) -0.0038(7) C11 0.0393(7) 0.0484(8) 0.0479(8) -0.0065(6) -0.0186(6) -0.0146(6) Si7 0.03202(18) 0.02835(17) 0.04092(19) 0.00535(14) -0.00499(15) -0.00840(14) C12 0.0418(8) 0.0401(8) 0.0573(9) 0.0119(7) 0.0012(7) -0.0145(6) C13 0.0502(9) 0.0486(9) 0.0502(9) 0.0186(7) -0.0165(7) -0.0094(7) C14 0.0564(10) 0.0322(7) 0.0693(11) -0.0030(7) -0.0036(8) -0.0146(7) Si8 0.02204(16) 0.03743(18) 0.03038(17) 0.00072(14) -0.00430(13) -0.00507(13) C15 0.0276(7) 0.0523(9) 0.0505(8) 0.0047(7) -0.0085(6) -0.0021(6) C16 0.0386(8) 0.0750(11) 0.0383(8) -0.0168(7) -0.0014(6) -0.0054(7) C17 0.0294(7) 0.0494(8) 0.0515(8) 0.0086(7) -0.0012(6) -0.0144(6) Si9 0.02427(16) 0.03888(18) 0.03424(17) -0.00753(14) -0.01024(13) -0.00959(14) C18 0.0298(7) 0.0556(9) 0.0469(8) 0.0003(7) -0.0055(6) -0.0188(6) C19 0.0448(8) 0.0523(9) 0.0557(9) -0.0176(7) -0.0173(7) -0.0157(7) C20 0.0274(7) 0.0527(8) 0.0553(9) -0.0048(7) -0.0148(6) -0.0082(6) Si10 0.03109(17) 0.04327(19) 0.02061(15) 0.00071(13) -0.00910(13) -0.00825(14) C21 0.0403(8) 0.0622(9) 0.0323(7) 0.0107(6) -0.0070(6) -0.0180(7) C22 0.0491(8) 0.0648(10) 0.0264(6) -0.0044(6) -0.0153(6) -0.0121(7) C23 0.0460(8) 0.0432(7) 0.0300(6) 0.0066(5) -0.0114(6) -0.0085(6) C24 0.0566(10) 0.0611(10) 0.0364(8) 0.0149(7) 0.0008(7) -0.0184(8) C25 0.0370(8) 0.0564(9) 0.0803(12) 0.0027(8) -0.0075(8) -0.0261(7) C26 0.0324(7) 0.0465(8) 0.0529(9) 0.0047(7) 0.0006(6) -0.0096(6) Si11 0.0404(2) 0.03310(18) 0.03627(18) 0.00952(14) -0.01851(15) -0.01102(15) C27 0.0827(13) 0.0652(11) 0.0556(10) 0.0246(8) -0.0465(9) -0.0350(10) C28 0.0620(11) 0.0402(8) 0.0625(10) 0.0075(7) -0.0233(8) 0.0076(7) C29 0.0635(10) 0.0462(8) 0.0530(9) 0.0216(7) -0.0192(8) -0.0235(8) Si12 0.03032(17) 0.02772(16) 0.03153(17) 0.00164(13) -0.01262(13) -0.01102(13) C30 0.0434(8) 0.0426(7) 0.0360(7) -0.0072(6) -0.0121(6) -0.0084(6) C31 0.0594(10) 0.0451(8) 0.0561(9) 0.0081(7) -0.0255(8) -0.0314(7) C32 0.0353(7) 0.0385(7) 0.0423(7) 0.0012(6) -0.0204(6) -0.0097(5) Si13 0.02837(17) 0.03628(17) 0.02194(15) 0.00177(13) -0.00107(12) -0.01190(14) C33 0.0509(8) 0.0385(7) 0.0336(7) 0.0043(6) -0.0040(6) -0.0146(6) C34 0.0385(7) 0.0560(9) 0.0289(6) 0.0014(6) 0.0050(5) -0.0148(6) C35 0.0420(8) 0.0531(8) 0.0322(7) 0.0094(6) -0.0135(6) -0.0176(6) Si14 0.01960(15) 0.04032(18) 0.03128(17) -0.00436(14) -0.00367(12) -0.01079(13) C36 0.0420(8) 0.0602(9) 0.0590(9) -0.0005(7) -0.0148(7) -0.0304(7) C37 0.0253(6) 0.0611(9) 0.0466(8) -0.0113(7) -0.0020(6) -0.0047(6) C38 0.0328(7) 0.0568(8) 0.0369(7) -0.0024(6) -0.0151(5) -0.0146(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C1 Si1 Si2 113.89(4) . . C1 Si1 Si5 121.67(4) . . Si2 Si1 Si5 124.439(19) . . C4 Si2 Si1 110.70(4) . . C4 Si2 Si3 130.58(4) . . Si1 Si2 Si3 118.712(17) . . C8 Si3 Si4 110.80(4) . . C8 Si3 Si2 129.90(4) . . Si4 Si3 Si2 119.284(18) . . C5 Si4 Si3 113.50(4) . . C5 Si4 Si6 121.52(4) . . Si3 Si4 Si6 124.925(19) . . C11 Si5 C10 105.79(7) . . C11 Si5 C9 108.37(8) . . C10 Si5 C9 110.65(8) . . C11 Si5 Si1 110.14(5) . . C10 Si5 Si1 111.73(5) . . C9 Si5 Si1 110.03(6) . . C26 Si6 C25 105.48(8) . . C26 Si6 C24 109.28(8) . . C25 Si6 C24 108.86(8) . . C26 Si6 Si4 110.51(5) . . C25 Si6 Si4 112.99(6) . . C24 Si6 Si4 109.60(6) . . C2 C1 Si7 103.65(8) . . C2 C1 Si1 105.71(7) . . Si7 C1 Si1 111.62(6) . . C2 C1 Si8 109.56(8) . . Si7 C1 Si8 112.92(6) . . Si1 C1 Si8 112.70(6) . . C3 C2 C1 115.69(10) . . C2 C3 C4 118.08(10) . . C3 C4 Si9 108.71(8) . . C3 C4 Si10 103.03(7) . . Si9 C4 Si10 111.66(5) . . C3 C4 Si2 104.97(7) . . Si9 C4 Si2 114.06(6) . . Si10 C4 Si2 113.45(6) . . C6 C5 Si4 105.91(7) . . C6 C5 Si11 103.58(7) . . Si4 C5 Si11 112.06(6) . . C6 C5 Si12 109.57(8) . . Si4 C5 Si12 112.52(6) . . Si11 C5 Si12 112.57(6) . . C7 C6 C5 116.03(9) . . C6 C7 C8 117.90(9) . . C7 C8 Si14 108.81(7) . . C7 C8 Si13 103.19(7) . . Si14 C8 Si13 111.41(5) . . C7 C8 Si3 105.04(7) . . Si14 C8 Si3 113.87(6) . . Si13 C8 Si3 113.62(6) . . C12 Si7 C13 105.15(8) . . C12 Si7 C14 108.67(8) . . C13 Si7 C14 106.34(8) . . C12 Si7 C1 109.83(6) . . C13 Si7 C1 117.34(6) . . C14 Si7 C1 109.17(7) . . C16 Si8 C15 105.23(7) . . C16 Si8 C17 107.82(8) . . C15 Si8 C17 104.90(7) . . C16 Si8 C1 110.22(6) . . C15 Si8 C1 114.99(6) . . C17 Si8 C1 113.11(6) . . C20 Si9 C18 106.84(7) . . C20 Si9 C19 107.81(7) . . C18 Si9 C19 104.29(7) . . C20 Si9 C4 112.50(6) . . C18 Si9 C4 114.42(6) . . C19 Si9 C4 110.47(6) . . C23 Si10 C21 107.69(7) . . C23 Si10 C22 106.89(7) . . C21 Si10 C22 104.78(7) . . C23 Si10 C4 115.45(6) . . C21 Si10 C4 110.14(6) . . C22 Si10 C4 111.27(6) . . C27 Si11 C29 105.00(8) . . C27 Si11 C28 108.35(9) . . C29 Si11 C28 106.21(8) . . C27 Si11 C5 110.91(6) . . C29 Si11 C5 117.43(6) . . C28 Si11 C5 108.54(6) . . C30 Si12 C31 105.52(7) . . C30 Si12 C32 107.66(6) . . C31 Si12 C32 104.68(7) . . C30 Si12 C5 110.25(6) . . C31 Si12 C5 114.93(6) . . C32 Si12 C5 113.24(5) . . C33 Si13 C35 108.01(7) . . C33 Si13 C34 106.71(7) . . C35 Si13 C34 103.98(7) . . C33 Si13 C8 115.44(6) . . C35 Si13 C8 110.62(6) . . C34 Si13 C8 111.38(6) . . C36 Si14 C38 106.39(7) . . C36 Si14 C37 108.02(7) . . C38 Si14 C37 104.60(7) . . C36 Si14 C8 112.43(6) . . C38 Si14 C8 114.34(5) . . C37 Si14 C8 110.57(6) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Si1 C1 1.9105(12) . Si1 Si2 2.1850(4) . Si1 Si5 2.3548(5) . Si2 C4 1.9323(11) . Si2 Si3 2.3392(5) . Si3 C8 1.9322(11) . Si3 Si4 2.1915(5) . Si4 C5 1.9095(12) . Si4 Si6 2.3578(5) . Si5 C11 1.8648(15) . Si5 C10 1.8728(15) . Si5 C9 1.8802(16) . Si6 C26 1.8623(15) . Si6 C25 1.8711(16) . Si6 C24 1.8777(16) . C1 C2 1.5779(16) . C1 Si7 1.9098(12) . C1 Si8 1.9158(12) . C2 C3 1.5456(17) . C3 C4 1.5777(16) . C4 Si9 1.9149(12) . C4 Si10 1.9159(12) . C5 C6 1.5736(16) . C5 Si11 1.9101(11) . C5 Si12 1.9189(12) . C6 C7 1.5442(16) . C7 C8 1.5779(16) . C8 Si14 1.9143(11) . C8 Si13 1.9163(12) . Si7 C12 1.8722(15) . Si7 C13 1.8735(16) . Si7 C14 1.8779(16) . Si8 C16 1.8679(15) . Si8 C15 1.8721(14) . Si8 C17 1.8735(15) . Si9 C20 1.8716(14) . Si9 C18 1.8741(15) . Si9 C19 1.8791(14) . Si10 C23 1.8634(15) . Si10 C21 1.8767(15) . Si10 C22 1.8837(14) . Si11 C27 1.8690(16) . Si11 C29 1.8732(16) . Si11 C28 1.8765(17) . Si12 C30 1.8704(14) . Si12 C31 1.8716(14) . Si12 C32 1.8720(13) . Si13 C33 1.8634(14) . Si13 C35 1.8760(14) . Si13 C34 1.8817(13) . Si14 C36 1.8700(15) . Si14 C38 1.8745(14) . Si14 C37 1.8801(14) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C1 Si1 Si2 C4 4.87(6) . . . . Si5 Si1 Si2 C4 -175.50(4) . . . . C1 Si1 Si2 Si3 -176.21(4) . . . . Si5 Si1 Si2 Si3 3.42(3) . . . . C4 Si2 Si3 C8 -88.58(7) . . . . Si1 Si2 Si3 C8 92.75(5) . . . . C4 Si2 Si3 Si4 90.31(5) . . . . Si1 Si2 Si3 Si4 -88.36(2) . . . . C8 Si3 Si4 C5 4.57(5) . . . . Si2 Si3 Si4 C5 -174.51(4) . . . . C8 Si3 Si4 Si6 -172.75(4) . . . . Si2 Si3 Si4 Si6 8.16(3) . . . . C1 Si1 Si5 C11 -153.57(7) . . . . Si2 Si1 Si5 C11 26.83(6) . . . . C1 Si1 Si5 C10 -36.30(8) . . . . Si2 Si1 Si5 C10 144.10(6) . . . . C1 Si1 Si5 C9 87.03(7) . . . . Si2 Si1 Si5 C9 -92.58(6) . . . . C5 Si4 Si6 C26 -150.13(7) . . . . Si3 Si4 Si6 C26 26.99(6) . . . . C5 Si4 Si6 C25 -32.21(8) . . . . Si3 Si4 Si6 C25 144.91(6) . . . . C5 Si4 Si6 C24 89.38(7) . . . . Si3 Si4 Si6 C24 -93.50(6) . . . . Si2 Si1 C1 C2 12.89(8) . . . . Si5 Si1 C1 C2 -166.75(6) . . . . Si2 Si1 C1 Si7 124.93(5) . . . . Si5 Si1 C1 Si7 -54.72(7) . . . . Si2 Si1 C1 Si8 -106.75(5) . . . . Si5 Si1 C1 Si8 73.60(6) . . . . Si7 C1 C2 C3 -174.10(8) . . . . Si1 C1 C2 C3 -56.57(11) . . . . Si8 C1 C2 C3 65.12(11) . . . . C1 C2 C3 C4 97.17(12) . . . . C2 C3 C4 Si9 61.07(11) . . . . C2 C3 C4 Si10 179.66(8) . . . . C2 C3 C4 Si2 -61.35(11) . . . . Si1 Si2 C4 C3 14.25(8) . . . . Si3 Si2 C4 C3 -164.50(6) . . . . Si1 Si2 C4 Si9 -104.64(5) . . . . Si3 Si2 C4 Si9 76.61(7) . . . . Si1 Si2 C4 Si10 125.99(5) . . . . Si3 Si2 C4 Si10 -52.77(8) . . . . Si3 Si4 C5 C6 13.03(8) . . . . Si6 Si4 C5 C6 -169.55(6) . . . . Si3 Si4 C5 Si11 125.29(5) . . . . Si6 Si4 C5 Si11 -57.29(7) . . . . Si3 Si4 C5 Si12 -106.65(5) . . . . Si6 Si4 C5 Si12 70.77(6) . . . . Si4 C5 C6 C7 -56.84(11) . . . . Si11 C5 C6 C7 -174.91(8) . . . . Si12 C5 C6 C7 64.76(11) . . . . C5 C6 C7 C8 97.03(12) . . . . C6 C7 C8 Si14 61.16(11) . . . . C6 C7 C8 Si13 179.58(8) . . . . C6 C7 C8 Si3 -61.14(11) . . . . Si4 Si3 C8 C7 14.50(8) . . . . Si2 Si3 C8 C7 -166.54(5) . . . . Si4 Si3 C8 Si14 -104.46(5) . . . . Si2 Si3 C8 Si14 74.51(7) . . . . Si4 Si3 C8 Si13 126.54(5) . . . . Si2 Si3 C8 Si13 -54.49(7) . . . . C2 C1 Si7 C12 59.68(10) . . . . Si1 C1 Si7 C12 -53.64(9) . . . . Si8 C1 Si7 C12 178.16(7) . . . . C2 C1 Si7 C13 179.62(8) . . . . Si1 C1 Si7 C13 66.30(9) . . . . Si8 C1 Si7 C13 -61.90(9) . . . . C2 C1 Si7 C14 -59.38(10) . . . . Si1 C1 Si7 C14 -172.70(7) . . . . Si8 C1 Si7 C14 59.10(9) . . . . C2 C1 Si8 C16 22.96(10) . . . . Si7 C1 Si8 C16 -92.01(8) . . . . Si1 C1 Si8 C16 140.36(8) . . . . C2 C1 Si8 C15 141.69(9) . . . . Si7 C1 Si8 C15 26.71(9) . . . . Si1 C1 Si8 C15 -100.92(8) . . . . C2 C1 Si8 C17 -97.82(9) . . . . Si7 C1 Si8 C17 147.21(7) . . . . Si1 C1 Si8 C17 19.57(9) . . . . C3 C4 Si9 C20 151.70(8) . . . . Si10 C4 Si9 C20 38.71(8) . . . . Si2 C4 Si9 C20 -91.56(8) . . . . C3 C4 Si9 C18 -86.13(9) . . . . Si10 C4 Si9 C18 160.87(7) . . . . Si2 C4 Si9 C18 30.61(9) . . . . C3 C4 Si9 C19 31.17(10) . . . . Si10 C4 Si9 C19 -81.82(8) . . . . Si2 C4 Si9 C19 147.91(7) . . . . C3 C4 Si10 C23 166.12(8) . . . . Si9 C4 Si10 C23 -77.37(8) . . . . Si2 C4 Si10 C23 53.21(8) . . . . C3 C4 Si10 C21 43.91(9) . . . . Si9 C4 Si10 C21 160.42(7) . . . . Si2 C4 Si10 C21 -69.00(8) . . . . C3 C4 Si10 C22 -71.83(9) . . . . Si9 C4 Si10 C22 44.68(8) . . . . Si2 C4 Si10 C22 175.26(7) . . . . C6 C5 Si11 C27 58.81(11) . . . . Si4 C5 Si11 C27 -54.90(10) . . . . Si12 C5 Si11 C27 177.07(8) . . . . C6 C5 Si11 C29 179.50(9) . . . . Si4 C5 Si11 C29 65.79(9) . . . . Si12 C5 Si11 C29 -62.24(9) . . . . C6 C5 Si11 C28 -60.11(10) . . . . Si4 C5 Si11 C28 -173.82(8) . . . . Si12 C5 Si11 C28 58.15(9) . . . . C6 C5 Si12 C30 23.84(9) . . . . Si4 C5 Si12 C30 141.37(7) . . . . Si11 C5 Si12 C30 -90.84(7) . . . . C6 C5 Si12 C31 142.91(9) . . . . Si4 C5 Si12 C31 -99.55(8) . . . . Si11 C5 Si12 C31 28.23(9) . . . . C6 C5 Si12 C32 -96.84(9) . . . . Si4 C5 Si12 C32 20.69(8) . . . . Si11 C5 Si12 C32 148.48(7) . . . . C7 C8 Si13 C33 165.55(8) . . . . Si14 C8 Si13 C33 -77.86(8) . . . . Si3 C8 Si13 C33 52.38(8) . . . . C7 C8 Si13 C35 42.54(9) . . . . Si14 C8 Si13 C35 159.14(6) . . . . Si3 C8 Si13 C35 -70.63(8) . . . . C7 C8 Si13 C34 -72.58(9) . . . . Si14 C8 Si13 C34 44.02(8) . . . . Si3 C8 Si13 C34 174.26(7) . . . . C7 C8 Si14 C36 152.37(8) . . . . Si13 C8 Si14 C36 39.26(8) . . . . Si3 C8 Si14 C36 -90.85(8) . . . . C7 C8 Si14 C38 -86.18(9) . . . . Si13 C8 Si14 C38 160.71(6) . . . . Si3 C8 Si14 C38 30.60(9) . . . . C7 C8 Si14 C37 31.55(10) . . . . Si13 C8 Si14 C37 -81.56(8) . . . . Si3 C8 Si14 C37 148.33(7) . . . .