#------------------------------------------------------------------------------ #$Date: 2019-12-21 02:10:17 +0200 (Sat, 21 Dec 2019) $ #$Revision: 245456 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/66/1556699.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556699 loop_ _publ_author_name 'Bangalore, Pavan K.' 'Vagolu, Siva K.' 'Bollikanda, Rakesh K.' 'Veeragoni, Dileep K.' 'Choudante, Pallavi C.' 'Misra, Sunil' 'Sriram, Dharmarajan' 'Sridhar, Balasubramanian' 'Kantevari, Srinivas' _publ_section_title ; Usnic Acid Enaminone-Coupled 1,2,3-Triazoles as Antibacterial and Antitubercular Agents ; _journal_name_full 'Journal of Natural Products' _journal_paper_doi 10.1021/acs.jnatprod.9b00475 _journal_year 2019 _chemical_absolute_configuration syn _chemical_formula_moiety 'C21 H19 N O6' _chemical_formula_sum 'C21 H19 N O6' _chemical_formula_weight 381.37 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 6.89532(9) _cell_length_b 12.63419(15) _cell_length_c 20.7068(2) _cell_measurement_reflns_used 9988 _cell_measurement_temperature 294(2) _cell_measurement_theta_max 30.59 _cell_measurement_theta_min 2.54 _cell_volume 1803.91(4) _computing_cell_refinement 'SAINT (Bruker, 2016)' _computing_data_collection 'APEX3 (Bruker, 2016)' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL2014 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_temperature 294(2) _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Bruker SMART APEX CCD area-detector' _diffrn_measurement_method \w _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0322 _diffrn_reflns_av_unetI/netI 0.0302 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 21931 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.591 _diffrn_reflns_theta_min 2.543 _exptl_absorpt_coefficient_mu 0.104 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.6458 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS, Bruker, 2016' _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.404 _exptl_crystal_description block _exptl_crystal_F_000 800 _exptl_crystal_size_max 0.250 _exptl_crystal_size_mid 0.220 _exptl_crystal_size_min 0.110 _refine_diff_density_max 0.209 _refine_diff_density_min -0.263 _refine_diff_density_rms 0.051 _refine_ls_abs_structure_details ; Flack x determined using 1920 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.2(2) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.052 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 269 _refine_ls_number_reflns 5516 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.052 _refine_ls_R_factor_all 0.0471 _refine_ls_R_factor_gt 0.0414 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0712P)^2^+0.0942P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1088 _refine_ls_wR_factor_ref 0.1128 _reflns_Friedel_coverage 0.757 _reflns_Friedel_fraction_full 0.996 _reflns_Friedel_fraction_max 0.992 _reflns_number_gt 4933 _reflns_number_total 5516 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file np9b00475_si_002.cif _cod_data_source_block KA812_0m _cod_database_code 1556699 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.975 _shelx_estimated_absorpt_t_max 0.989 _shelx_res_file ; TITL KA812_0m_a.res in P2(1)2(1)2(1) KA812_0m.res created by SHELXL-2018/3 at 16:12:32 on 25-Jul-2019 CELL 0.71073 6.89532 12.63419 20.70684 90.000 90.000 90.000 ZERR 4.00 0.00009 0.00015 0.00024 0.000 0.000 0.000 LATT -1 SYMM x+1/2, -y+1/2, -z SYMM -x, y+1/2, -z+1/2 SYMM -x+1/2, -y, z+1/2 SFAC C H N O UNIT 84 76 4 24 LIST 6 ! automatically inserted. Change 6 to 4 for CHECKCIF!! ACTA L.S. 10 FMAP 2 PLAN -5 HTAB N1 O6 HTAB O2 O1 HTAB O3 O5 SIZE 0.25 0.22 0.11 BOND $H CONF TEMP 21 WGHT 0.071200 0.094200 FVAR 0.85850 C1 1 0.502603 0.758477 0.646188 11.00000 0.03287 0.02620 = 0.03141 -0.00096 0.00187 -0.00141 C2 1 0.332930 0.749804 0.680636 11.00000 0.03208 0.02800 = 0.03303 0.00101 -0.00005 0.00068 C3 1 0.242961 0.834632 0.712223 11.00000 0.03512 0.03236 = 0.03597 -0.00119 0.00193 0.00431 C4 1 0.343326 0.932837 0.706252 11.00000 0.04260 0.03132 = 0.03900 -0.00380 -0.00053 0.00415 C5 1 0.516862 0.945046 0.672331 11.00000 0.04678 0.02816 = 0.03962 -0.00560 0.00043 -0.00333 C6 1 0.596260 0.856598 0.642084 11.00000 0.03735 0.02901 = 0.03282 -0.00169 0.00249 -0.00398 C7 1 0.062054 0.828660 0.748941 11.00000 0.03698 0.04316 = 0.04038 -0.00136 0.00560 0.00838 C8 1 -0.046020 0.727696 0.756668 11.00000 0.04526 0.04590 = 0.05458 0.00340 0.01648 0.00225 AFIX 137 H8A 2 -0.069939 0.697239 0.714947 11.00000 -1.50000 H8B 2 -0.167318 0.741225 0.777875 11.00000 -1.50000 H8C 2 0.029375 0.679395 0.782174 11.00000 -1.50000 AFIX 0 C9 1 0.615143 1.050684 0.669361 11.00000 0.07019 0.03348 = 0.06295 -0.01383 0.01307 -0.01644 AFIX 137 H9A 2 0.665635 1.061900 0.626701 11.00000 -1.50000 H9B 2 0.719497 1.052513 0.700030 11.00000 -1.50000 H9C 2 0.523278 1.105334 0.679447 11.00000 -1.50000 AFIX 0 C10 1 0.525960 0.657377 0.608058 11.00000 0.03001 0.02437 = 0.02790 0.00032 0.00206 -0.00357 C11 1 0.392213 0.587301 0.645299 11.00000 0.02826 0.02951 = 0.03193 0.00025 0.00475 -0.00229 C12 1 0.443481 0.675415 0.539118 11.00000 0.04395 0.03886 = 0.03206 0.00440 -0.00491 -0.00570 AFIX 137 H12A 2 0.522488 0.726125 0.516759 11.00000 -1.50000 H12B 2 0.313080 0.701567 0.542148 11.00000 -1.50000 H12C 2 0.443906 0.609700 0.515843 11.00000 -1.50000 AFIX 0 C13 1 0.723149 0.607748 0.597304 11.00000 0.03218 0.02889 = 0.02620 -0.00089 0.00250 -0.00291 C14 1 0.729283 0.494150 0.591925 11.00000 0.03207 0.02697 = 0.03113 -0.00104 0.00588 -0.00297 C15 1 0.571834 0.430578 0.618863 11.00000 0.04104 0.02763 = 0.03829 -0.00030 0.00996 -0.00400 C16 1 0.403076 0.482769 0.648385 11.00000 0.03574 0.03034 = 0.04309 0.00204 0.01337 -0.00414 AFIX 43 H16 2 0.306656 0.443460 0.668658 11.00000 -1.20000 AFIX 0 C17 1 0.889684 0.443721 0.561394 11.00000 0.03355 0.03236 = 0.03330 -0.00544 0.00300 -0.00312 C18 1 1.028622 0.501247 0.518706 11.00000 0.04273 0.04283 = 0.06260 -0.00234 0.02190 -0.00581 AFIX 137 H18A 2 1.049699 0.460983 0.480021 11.00000 -1.50000 H18B 2 1.149606 0.510535 0.540937 11.00000 -1.50000 H18C 2 0.975931 0.569228 0.507702 11.00000 -1.50000 AFIX 0 C19 1 1.066272 0.279456 0.536109 11.00000 0.04853 0.03744 = 0.07513 -0.01010 0.02296 0.00285 AFIX 23 H19A 2 1.053439 0.283473 0.489524 11.00000 -1.20000 H19B 2 1.191192 0.309006 0.547896 11.00000 -1.20000 AFIX 0 C20 1 1.056546 0.169110 0.556623 11.00000 0.05644 0.04153 = 0.06229 -0.01156 0.01520 0.00664 C21 1 1.047245 0.080868 0.573211 11.00000 0.10580 0.04611 = 0.07982 -0.00406 0.02962 0.01287 AFIX 163 H21 2 1.039842 0.010627 0.586416 11.00000 -1.20000 AFIX 0 N1 3 0.911455 0.340817 0.566631 11.00000 0.03924 0.03372 = 0.04677 -0.00569 0.01115 0.00143 H1N 2 0.818771 0.312090 0.590960 11.00000 0.05822 O1 4 -0.004176 0.909029 0.775137 11.00000 0.05276 0.05139 = 0.08145 -0.01874 0.02222 0.00704 O2 4 0.272044 1.020448 0.734420 11.00000 0.05649 0.03480 = 0.06473 -0.01288 0.01076 0.00571 H2O 2 0.181086 1.000074 0.752067 11.00000 0.07064 O3 4 0.764237 0.867561 0.609365 11.00000 0.04704 0.03146 = 0.05243 -0.00464 0.01573 -0.00986 H3O 2 0.803634 0.814015 0.603859 11.00000 0.08096 O4 4 0.258311 0.647482 0.678489 11.00000 0.03302 0.02901 = 0.04214 0.00025 0.00996 -0.00103 O5 4 0.863343 0.668124 0.589188 11.00000 0.03538 0.03356 = 0.05500 -0.00597 0.00823 -0.00859 O6 4 0.577432 0.332087 0.620141 11.00000 0.06086 0.02606 = 0.07677 0.00073 0.03124 -0.00191 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM KA812_0m_a.res in P2(1)2(1)2(1) REM wR2 = 0.1128, GooF = S = 1.052, Restrained GooF = 1.052 for all data REM R1 = 0.0414 for 4933 Fo > 4sig(Fo) and 0.0471 for all 5516 data REM 269 parameters refined using 0 restraints END WGHT 0.0712 0.0942 REM Highest difference peak 0.209, deepest hole -0.263, 1-sigma level 0.051 Q1 1 0.5548 0.8018 0.6475 11.00000 0.05 0.21 Q2 1 0.5659 0.8970 0.6628 11.00000 0.05 0.19 Q3 1 0.6130 1.0860 0.7173 11.00000 0.05 0.19 Q4 1 0.5219 0.7141 0.6250 11.00000 0.05 0.18 Q5 1 0.4628 0.6179 0.6239 11.00000 0.05 0.18 ; _shelx_res_checksum 4723 _shelx_hkl_file ; 1 0 0 0.59 0.20 1 0 0 0.40 0.16 -1 0 0 0.22 0.15 -1 0 0 0.49 0.20 -2 0 0 3976.35 173.13 2 0 0 3997.90 173.19 3 0 0 -0.09 0.65 3 0 0 0.42 0.55 -3 0 0 0.62 0.51 -3 0 0 0.19 0.43 4 0 0 1024.58 43.52 4 0 0 983.14 43.62 4 0 0 1015.14 43.40 -4 0 0 1014.55 43.56 -4 0 0 1014.14 43.60 5 0 0 1.69 0.98 -5 0 0 2.05 0.88 5 0 0 0.60 0.82 6 0 0 749.90 32.92 6 0 0 766.22 33.34 7 0 0 -0.91 1.23 7 0 0 1.42 1.18 8 0 0 80.30 4.63 8 0 0 66.48 4.55 9 0 0 0.12 2.35 9 0 0 0.06 2.05 1 -1 0 1650.06 71.71 -1 -1 0 1718.68 71.90 -1 1 0 1598.58 71.72 1 1 0 1611.29 71.83 -2 1 0 4196.69 179.81 2 1 0 4067.30 179.79 2 -1 0 4129.40 179.62 -2 -1 0 4174.25 179.76 -3 -1 0 37.97 2.25 3 1 0 42.82 2.33 -3 1 0 39.69 2.26 3 -1 0 40.26 2.30 3 -1 0 42.03 2.21 3 1 0 42.56 2.28 -3 1 0 42.47 2.27 3 -1 0 40.16 2.09 4 -1 0 9.78 1.21 -4 1 0 10.41 1.15 4 1 0 10.65 1.38 4 -1 0 14.14 1.20 4 -1 0 13.50 1.23 -4 -1 0 10.80 1.28 4 1 0 11.73 1.47 -4 1 0 10.96 1.31 -5 1 0 12.62 1.54 5 -1 0 11.83 1.59 5 1 0 14.14 1.71 5 -1 0 11.85 1.33 6 1 0 5.64 1.34 6 -1 0 7.03 1.21 6 -1 0 5.65 1.27 -6 1 0 6.13 1.49 6 1 0 7.58 1.44 7 -1 0 0.95 1.60 7 1 0 1.84 1.21 -7 1 0 1.96 1.52 7 -1 0 1.15 1.20 7 1 0 1.83 1.40 8 1 0 24.38 2.67 8 -1 0 26.23 2.87 8 1 0 18.39 2.54 8 -1 0 23.60 3.04 9 -1 0 0.15 1.79 9 -1 0 2.25 1.81 9 1 0 0.36 1.72 0 -2 0 114.00 4.80 0 -2 0 106.64 4.81 0 2 0 107.52 4.81 0 -2 0 114.74 4.81 1 2 0 152.28 6.97 -1 2 0 174.93 6.92 1 -2 0 156.49 6.90 1 2 0 156.30 7.02 -1 2 0 166.84 6.91 -1 2 0 155.39 6.94 -1 -2 0 161.42 7.05 1 -2 0 161.06 6.93 1 -2 0 155.34 6.93 -2 2 0 780.59 31.81 2 -2 0 761.04 31.77 -2 2 0 736.89 31.74 -2 2 0 714.39 31.82 2 -2 0 755.36 31.83 2 2 0 733.02 31.92 -2 -2 0 740.47 31.93 2 -2 0 712.94 31.69 3 -2 0 17.29 1.27 -3 2 0 18.14 1.35 3 2 0 18.87 1.41 3 -2 0 19.60 1.27 3 2 0 17.12 1.45 -3 -2 0 16.27 1.51 3 -2 0 18.88 1.18 -4 2 0 8.10 1.09 4 -2 0 9.17 1.21 4 2 0 7.51 1.08 4 -2 0 9.45 1.01 4 2 0 9.02 1.26 4 -2 0 7.64 1.03 -4 -2 0 8.68 1.15 -4 2 0 7.06 1.11 -5 2 0 189.74 8.65 5 -2 0 197.32 8.35 5 2 0 158.53 8.60 5 -2 0 184.53 8.60 6 2 0 13.36 1.77 -6 2 0 11.83 1.83 6 -2 0 14.09 1.48 6 -2 0 10.93 1.58 7 -2 0 60.20 4.10 7 -2 0 59.83 3.63 7 2 0 62.68 4.04 -7 2 0 61.10 4.09 7 2 0 63.06 4.02 8 2 0 52.19 4.25 8 2 0 50.06 4.16 -8 2 0 45.42 4.00 8 -2 0 48.91 3.44 9 2 0 49.51 4.07 9 2 0 49.86 4.81 9 -2 0 46.13 4.54 0 -3 0 0.03 0.18 0 3 0 0.16 0.18 0 3 0 0.15 0.18 0 -3 0 0.05 0.16 0 -3 0 0.41 0.19 1 -3 0 128.94 5.13 -1 3 0 116.06 5.13 1 3 0 112.95 5.19 1 -3 0 113.76 5.15 -1 -3 0 118.55 5.26 1 3 0 121.17 5.25 1 -3 0 114.07 5.13 -1 -3 0 117.23 5.22 1 3 0 112.89 5.20 -1 3 0 118.01 5.16 -2 3 0 25.09 1.32 2 3 0 22.99 1.45 -2 3 0 24.52 1.42 2 -3 0 26.02 1.36 2 -3 0 25.78 1.27 2 3 0 26.87 1.58 2 -3 0 26.83 1.39 -2 3 0 26.92 1.33 -2 -3 0 21.77 1.48 -3 -3 0 5239.58 223.33 4 3 0 7.46 1.13 4 3 0 6.84 1.12 -4 3 0 5.97 1.02 4 -3 0 5.92 0.92 4 -3 0 8.04 0.87 -4 3 0 6.47 0.94 4 -3 0 5.78 0.88 5 -3 0 19.98 1.78 5 -3 0 16.89 1.55 5 3 0 17.61 1.94 -5 3 0 17.83 1.85 6 -3 0 53.53 3.29 6 -3 0 44.51 2.81 -6 3 0 49.90 3.34 6 3 0 45.78 3.19 7 -3 0 66.64 3.48 7 3 0 51.01 3.83 -7 3 0 58.81 4.58 7 -3 0 62.08 3.84 8 3 0 3.79 2.07 8 -3 0 2.15 1.50 8 -3 0 -0.50 1.18 8 3 0 1.01 1.92 -8 3 0 -2.18 1.72 9 3 0 -0.05 2.60 9 -3 0 0.63 2.61 9 3 0 -2.82 1.97 -9 3 0 2.99 2.43 9 3 0 4.38 2.01 0 4 0 950.97 42.02 0 -4 0 965.66 42.04 0 -4 0 1004.03 42.02 0 4 0 1014.70 42.03 1 4 0 6.74 0.64 -1 -4 0 8.21 0.68 1 -4 0 9.61 0.60 -1 -4 0 7.88 0.73 1 -4 0 8.06 0.51 1 -4 0 7.31 0.58 1 4 0 6.89 0.64 -1 4 0 9.29 0.59 1 4 0 6.93 0.67 2 4 0 91.15 4.16 -2 4 0 92.34 3.91 -2 -4 0 86.90 4.18 2 -4 0 85.81 3.95 -2 4 0 84.20 4.01 2 4 0 86.77 4.04 -2 4 0 84.50 3.92 2 -4 0 82.33 3.90 2 -4 0 87.01 3.97 -3 4 0 352.86 15.46 -3 4 0 349.81 15.30 3 -4 0 362.35 15.32 -3 4 0 368.16 15.33 3 -4 0 361.78 15.42 3 4 0 373.99 15.48 3 4 0 338.90 15.56 3 -4 0 350.32 15.21 -3 -4 0 311.38 15.58 4 -4 0 5.93 0.77 4 4 0 4.74 0.92 -4 4 0 5.69 0.84 -4 4 0 5.15 0.79 -4 4 0 6.24 1.03 4 -4 0 4.27 0.87 4 -4 0 5.14 0.91 5 4 0 127.98 6.65 5 -4 0 130.78 6.44 5 -4 0 135.31 6.08 -5 4 0 134.45 6.57 6 -4 0 293.44 12.93 6 4 0 270.36 13.01 6 -4 0 276.00 12.36 -6 4 0 275.45 12.97 7 4 0 43.95 3.91 7 4 0 54.16 4.00 7 -4 0 48.87 2.97 -7 4 0 46.39 4.17 7 -4 0 52.84 3.67 8 -4 0 12.95 1.60 8 4 0 10.88 2.25 8 -4 0 11.94 2.41 8 4 0 12.64 2.58 8 4 0 8.59 2.08 -8 4 0 7.61 2.37 -9 4 0 33.97 3.87 9 4 0 42.14 5.09 9 -4 0 41.60 4.46 9 4 0 34.25 4.32 9 4 0 43.55 3.90 0 5 0 0.26 0.34 0 -5 0 0.30 0.35 0 5 0 1.35 0.34 0 -5 0 1.41 0.35 0 -5 0 0.50 0.34 -1 5 0 1112.18 46.69 1 5 0 1054.93 46.74 -1 -5 0 1106.98 46.81 1 -5 0 1075.19 46.69 -1 5 0 1124.33 46.72 -1 -5 0 1105.33 46.81 1 5 0 1129.94 46.77 -1 -5 0 1059.91 46.75 1 5 0 1072.11 46.75 1 -5 0 1085.87 46.69 -2 -5 0 420.24 18.63 -2 5 0 429.29 18.44 -2 5 0 439.45 18.36 2 -5 0 431.43 18.36 2 5 0 394.39 18.46 2 -5 0 449.74 18.39 2 5 0 421.44 18.48 2 -5 0 420.52 18.39 -3 5 0 166.71 7.47 3 -5 0 168.36 7.39 -3 5 0 163.47 7.40 3 -5 0 163.31 7.46 3 5 0 169.86 7.74 3 5 0 169.07 7.62 -3 5 0 169.78 7.61 3 5 0 170.48 7.59 -3 -5 0 161.39 7.79 3 -5 0 167.64 7.54 4 5 0 106.38 5.16 -4 5 0 105.18 5.01 -4 5 0 109.04 5.24 4 -5 0 100.68 4.95 -4 5 0 104.48 4.94 4 -5 0 105.59 5.11 4 -5 0 109.14 4.87 -5 5 0 45.88 3.03 -5 5 0 42.22 2.63 5 5 0 39.18 2.92 5 5 0 49.71 2.93 5 -5 0 48.06 2.50 5 -5 0 48.07 2.89 6 5 0 -0.31 1.39 6 5 0 1.88 1.27 6 -5 0 -0.68 1.15 -6 5 0 1.44 1.36 6 -5 0 -0.41 0.79 7 5 0 37.79 3.36 7 -5 0 35.34 2.79 7 5 0 33.22 2.96 -7 5 0 36.49 3.23 7 -5 0 35.72 2.42 8 -5 0 7.67 2.18 8 -5 0 6.07 1.23 -8 5 0 2.54 2.35 8 5 0 8.39 2.04 8 5 0 3.25 1.75 9 5 0 7.57 2.19 9 5 0 12.59 3.21 -9 5 0 17.74 2.96 9 -5 0 9.00 2.33 9 5 0 8.26 2.36 0 -6 0 2418.39 106.08 0 6 0 2559.00 106.10 1 -6 0 230.03 9.97 1 6 0 234.05 10.05 1 -6 0 225.10 9.98 1 6 0 235.35 10.03 -1 -6 0 225.86 10.09 -1 6 0 220.16 9.98 -1 6 0 228.73 9.96 -1 -6 0 228.48 10.11 1 6 0 224.49 10.01 -1 -6 0 221.76 10.03 2 -6 0 676.38 28.72 -2 6 0 656.98 28.77 2 6 0 694.02 28.84 2 -6 0 660.50 28.66 2 6 0 624.40 28.85 2 6 0 690.06 28.84 -2 6 0 684.05 28.68 -2 -6 0 658.95 28.98 2 -6 0 666.59 28.69 3 6 0 170.22 7.65 3 -6 0 172.53 7.40 -3 6 0 162.80 7.32 -3 6 0 161.35 7.46 3 -6 0 150.12 7.38 3 -6 0 164.11 7.32 3 6 0 159.72 7.45 -4 6 0 54.44 2.87 4 6 0 60.40 3.36 -4 6 0 60.30 3.03 -4 6 0 52.94 3.15 4 -6 0 55.64 3.02 4 -6 0 53.77 2.84 4 6 0 57.80 3.13 -5 6 0 164.24 8.71 5 6 0 203.20 9.11 5 6 0 184.22 9.24 5 -6 0 204.37 8.69 -5 6 0 196.02 9.24 5 -6 0 206.25 9.11 -5 6 0 198.53 8.90 6 6 0 530.47 24.10 -6 6 0 527.34 24.06 6 6 0 569.58 23.91 6 -6 0 548.36 23.87 6 -6 0 514.31 23.32 7 6 0 0.87 1.33 7 -6 0 1.45 0.93 -7 6 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16.73 -2 3 9 373.44 16.40 2 -3 9 361.34 16.64 2 3 -9 389.27 16.51 2 -3 9 396.08 16.64 -2 3 9 403.26 16.51 2 3 -9 393.03 16.54 2 3 9 380.08 16.62 -2 -3 9 391.64 16.79 -2 -3 9 380.10 16.60 2 3 9 394.97 16.91 -2 3 -9 367.48 16.77 -2 3 -9 379.47 16.72 -2 -3 9 359.65 16.53 -3 3 9 93.34 4.58 3 -3 9 100.22 4.98 3 -3 9 95.34 4.77 3 3 -9 101.86 4.51 3 3 -9 103.70 4.57 3 3 -9 97.95 4.76 -3 3 9 96.66 4.62 -3 -3 9 93.91 4.56 -3 -3 9 100.90 4.76 3 3 9 107.62 5.07 -3 3 -9 92.06 4.81 3 3 9 96.94 4.78 -4 3 9 195.45 8.92 4 -3 9 194.83 9.31 -4 3 9 194.32 8.90 4 3 -9 186.20 9.01 4 -3 9 203.01 9.02 4 3 -9 198.70 8.66 4 3 -9 203.81 8.78 4 3 9 188.39 9.31 4 3 9 193.38 9.24 -4 3 -9 199.01 9.13 4 -3 -9 195.73 8.46 4 -3 -9 190.58 8.44 -5 3 9 47.55 3.02 5 3 -9 48.84 2.69 5 -3 9 48.86 3.49 -5 3 9 47.53 3.12 5 -3 9 49.78 3.15 5 -3 -9 50.69 2.45 -5 3 -9 51.97 3.27 5 3 9 38.93 3.18 5 3 9 47.64 3.46 6 3 -9 74.30 3.98 -6 3 9 73.74 4.30 6 3 -9 66.88 4.11 6 -3 9 74.47 4.83 6 -3 9 76.92 4.35 6 3 9 80.33 4.73 6 -3 -9 75.52 3.70 -6 3 -9 76.49 4.52 6 -3 -9 71.59 3.92 6 3 9 71.41 4.78 7 3 -9 15.96 2.07 -7 3 9 13.12 2.69 7 -3 9 12.30 2.53 7 -3 9 16.05 2.20 7 3 -9 13.29 1.87 7 3 9 14.26 2.36 -7 3 -9 13.97 2.33 7 3 9 19.27 2.79 7 -3 -9 13.24 1.92 7 -3 -9 15.12 1.62 8 -3 9 14.57 2.70 8 -3 9 18.91 2.46 8 3 -9 14.22 2.52 8 3 -9 17.68 2.25 8 3 9 16.77 3.03 -8 3 -9 16.15 2.87 8 -3 -9 18.28 2.53 8 3 9 17.45 3.46 9 -3 9 1.38 3.11 9 -3 9 3.68 2.31 9 3 -9 3.67 2.12 9 3 9 4.08 2.36 9 -3 -9 -0.65 1.97 9 3 9 -0.77 3.02 0 4 -9 570.73 25.09 0 -4 9 614.77 25.12 0 -4 9 568.53 25.11 0 4 -9 586.01 25.11 0 4 9 572.91 25.08 1 -4 9 626.28 27.37 -1 4 9 630.23 27.19 1 -4 9 625.00 27.33 1 4 -9 646.39 27.31 -1 4 9 574.86 27.03 -1 -4 -9 631.58 27.35 1 4 -9 640.36 27.29 -1 4 -9 656.40 27.45 -1 -4 9 645.10 27.34 -1 4 -9 638.53 27.39 -1 -4 9 653.96 27.37 1 4 9 653.31 27.49 -2 -4 -9 16.72 1.40 -2 4 9 17.01 1.03 2 -4 9 17.31 1.32 2 -4 9 17.60 1.44 2 4 -9 17.89 1.19 -2 4 9 17.68 0.83 2 -4 9 18.57 1.32 2 4 -9 16.05 1.14 -2 4 9 16.50 0.96 2 4 9 16.27 1.36 -2 -4 9 16.91 1.31 -2 -4 9 17.77 1.28 -2 4 -9 18.76 1.39 -2 4 -9 17.82 1.52 -3 4 9 14.65 1.29 3 -4 9 16.10 1.42 3 4 -9 15.17 1.18 3 -4 9 18.44 1.60 3 4 -9 15.95 1.23 -3 4 9 15.81 1.14 3 4 9 13.43 1.40 3 4 9 15.50 1.43 -3 4 -9 17.45 1.53 -3 -4 9 13.34 1.33 4 4 -9 181.17 8.04 4 4 -9 194.58 8.20 -4 4 9 177.85 8.14 4 -4 9 189.79 8.68 4 -4 9 182.57 8.30 -4 4 9 178.80 8.25 4 -4 -9 157.28 7.67 4 4 9 161.51 8.60 -4 4 -9 183.81 8.53 4 -4 -9 188.27 7.69 -5 4 9 198.68 9.45 5 4 -9 220.10 9.42 -5 4 9 211.36 9.61 5 -4 9 205.20 9.54 5 -4 9 203.46 9.92 -5 4 -9 206.46 9.81 5 4 9 201.18 10.01 5 -4 -9 200.32 8.98 5 -4 -9 204.25 9.03 6 -4 9 6.92 1.41 6 -4 9 8.82 1.71 6 4 -9 9.70 1.36 -6 4 9 8.36 1.56 -6 4 -9 7.32 1.85 6 4 9 9.63 1.87 6 4 9 11.65 2.16 6 -4 -9 10.51 1.37 6 -4 -9 9.94 1.19 7 4 -9 4.48 1.37 7 4 -9 5.99 1.60 7 -4 9 3.99 2.03 7 4 9 2.68 1.65 7 -4 -9 4.07 1.03 -7 4 -9 4.52 2.24 7 -4 -9 4.35 1.45 7 4 9 3.43 2.08 8 4 -9 11.30 2.23 -8 4 9 11.21 2.86 8 -4 9 9.99 3.15 8 -4 9 13.90 2.25 -8 4 -9 18.02 2.84 8 -4 -9 11.68 1.97 8 4 9 11.84 3.04 8 4 9 16.01 3.20 9 -4 9 17.21 3.92 9 -4 9 12.79 2.48 9 4 -9 12.76 2.59 9 4 9 16.82 3.73 -9 4 -9 11.83 3.40 9 4 9 8.55 2.72 0 -5 9 767.05 34.07 0 5 -9 803.88 34.06 0 5 9 778.48 33.99 0 5 -9 811.00 34.05 0 -5 9 801.27 34.09 1 5 -9 191.41 8.37 -1 5 9 181.10 8.16 -1 5 9 192.41 8.23 1 5 -9 194.21 8.37 1 -5 9 182.43 8.43 -1 -5 -9 197.09 8.38 1 -5 9 180.91 8.40 -1 5 9 185.00 8.11 1 5 9 192.91 8.49 -1 5 -9 195.01 8.43 -1 -5 9 178.92 8.41 -1 5 -9 189.51 8.46 -1 -5 9 182.25 8.40 -2 5 9 73.85 3.26 -2 -5 -9 65.56 3.62 2 5 -9 74.96 3.55 -2 5 9 74.84 3.27 -2 5 9 73.26 3.33 2 -5 9 75.79 3.65 2 5 -9 77.93 3.58 -2 5 9 65.57 3.21 2 -5 9 81.13 3.80 -2 5 -9 75.11 3.72 -2 -5 9 75.04 3.64 2 5 9 75.30 3.84 -2 -5 9 67.27 3.64 -3 5 9 172.13 7.58 3 5 -9 176.00 7.74 3 5 -9 171.96 7.78 3 -5 9 165.21 7.85 3 -5 9 168.84 8.04 3 5 9 181.74 8.25 -3 -5 9 172.52 7.86 -3 5 -9 167.74 8.03 4 -5 9 372.49 16.60 -4 5 9 379.16 16.60 -4 5 9 371.45 16.39 4 -5 9 395.56 16.98 4 5 -9 394.68 16.57 4 5 9 338.09 16.95 -4 5 -9 380.21 16.91 5 -5 9 35.49 2.50 5 5 -9 31.48 2.16 -5 5 9 33.35 2.52 -5 5 9 30.11 2.20 5 -5 9 30.56 2.55 -5 5 -9 32.40 2.75 5 -5 -9 31.63 1.66 5 5 9 32.21 2.93 5 -5 -9 31.19 1.71 6 -5 9 44.43 3.59 -6 5 9 47.25 3.35 6 -5 9 46.07 3.11 6 5 -9 43.19 2.95 6 -5 -9 44.21 2.41 -6 5 -9 47.99 3.50 6 5 9 42.67 3.40 -7 5 9 60.55 4.24 7 -5 9 61.82 4.11 7 -5 9 69.58 4.80 7 5 9 59.06 4.46 7 -5 -9 60.43 3.58 -7 5 -9 56.89 4.52 7 5 9 62.01 5.17 -8 5 9 3.77 2.58 8 -5 9 0.85 1.83 8 -5 9 7.82 2.92 8 5 -9 1.08 1.94 8 5 9 1.60 2.65 8 5 9 1.68 2.52 -8 5 -9 0.64 2.39 0 6 9 171.79 7.80 0 6 9 173.67 7.71 0 -6 9 174.93 7.97 0 6 -9 177.95 7.92 0 -6 -9 176.47 7.70 0 -6 9 182.46 8.15 1 6 -9 138.48 6.49 -1 6 9 146.17 6.35 1 -6 9 136.89 6.55 -1 6 9 140.61 6.25 -1 -6 -9 147.74 6.47 -1 6 9 140.48 6.14 -1 6 -9 148.85 6.56 1 6 9 146.09 6.59 -1 -6 9 136.90 6.55 2 6 -9 122.28 5.89 -2 6 9 126.12 5.68 -2 6 9 131.93 5.62 2 -6 9 130.88 6.07 -2 -6 -9 127.81 6.06 2 -6 9 126.50 5.98 -2 -6 9 128.14 5.98 -2 6 -9 126.89 6.06 2 6 9 128.75 6.13 3 -6 9 280.73 12.72 3 6 -9 295.92 12.70 3 -6 9 271.18 12.88 -3 6 9 286.68 12.56 -3 6 -9 284.69 12.92 3 6 9 296.06 13.07 -3 -6 9 286.84 12.76 4 6 -9 113.29 5.49 4 -6 9 120.11 5.95 4 -6 9 114.35 5.55 -4 6 9 112.71 5.14 -4 6 9 112.10 5.50 4 6 9 101.41 5.82 -4 6 -9 123.33 5.91 5 6 -9 58.83 3.29 5 -6 9 49.44 3.46 -5 6 9 53.30 2.87 -5 6 9 53.26 3.36 5 -6 9 51.57 3.28 5 -6 -9 55.08 2.52 -5 6 -9 55.47 3.64 5 6 9 58.79 3.88 6 -6 9 21.09 2.35 6 6 -9 21.01 2.06 -6 6 9 22.27 2.66 6 -6 9 23.37 2.44 -6 6 -9 20.11 2.75 6 6 9 22.85 3.06 7 -6 9 3.01 2.18 7 6 -9 2.64 1.56 -7 6 9 5.30 2.12 7 -6 9 2.79 1.51 7 6 9 1.26 1.63 -7 6 -9 -0.88 1.99 7 6 9 1.61 2.49 8 -6 9 4.03 1.96 8 6 -9 7.68 2.10 8 -6 9 6.77 3.02 -8 6 9 3.42 2.41 8 6 9 7.52 2.85 -8 6 -9 4.74 2.54 8 6 9 2.52 2.76 0 7 9 104.36 4.84 0 -7 9 101.66 4.96 0 7 9 102.62 4.70 0 -7 -9 103.64 4.61 0 7 -9 102.70 4.89 0 7 9 104.11 4.69 -1 7 9 30.84 1.64 1 7 -9 26.27 1.75 -1 7 9 27.77 1.52 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8 9 92.55 4.50 0 8 9 95.30 4.36 0 8 9 93.64 4.26 0 -8 9 92.79 4.67 0 8 -9 96.66 4.58 0 -8 -9 92.32 4.21 1 8 -9 16.06 1.41 -1 -8 -9 16.15 1.38 1 -8 9 13.99 1.56 -1 8 9 16.07 1.15 -1 8 9 14.17 1.24 1 8 9 17.68 1.31 -1 -8 9 15.46 1.65 -1 8 -9 17.60 1.49 1 8 9 16.23 1.42 2 -8 9 10.80 1.41 2 -8 9 9.36 1.19 -2 8 9 9.58 1.00 -2 8 9 8.42 0.97 -2 -8 -9 9.99 1.45 2 8 -9 10.67 1.28 2 8 9 8.80 1.21 2 8 9 11.44 1.34 -2 -8 9 10.40 1.32 -2 8 -9 8.99 1.31 -3 8 9 100.28 4.45 3 8 -9 101.08 4.93 -3 8 9 97.51 4.69 3 -8 9 98.62 5.03 3 -8 9 96.12 4.98 3 8 9 92.40 5.03 -3 8 -9 102.68 5.17 -3 -8 9 95.58 5.08 3 8 9 105.13 5.01 -4 8 9 227.28 10.76 4 8 -9 240.71 10.86 4 -8 9 249.07 11.20 4 -8 9 230.76 10.86 -4 8 -9 237.80 11.16 4 8 9 240.25 11.26 5 -8 9 29.04 2.83 5 8 -9 29.23 2.37 -5 8 9 28.01 2.41 5 -8 9 30.84 2.58 5 8 9 25.28 2.51 6 8 -9 7.10 1.54 6 -8 9 7.57 2.09 -6 8 9 5.58 1.91 6 -8 9 5.23 1.99 6 8 9 5.09 1.67 -6 8 -9 5.17 1.99 -7 8 9 19.58 3.15 7 -8 9 21.44 3.18 7 8 -9 18.54 2.38 7 -8 9 18.42 2.27 7 8 9 28.65 3.68 -7 8 -9 23.17 3.20 7 8 9 22.43 3.06 8 -8 9 14.35 2.33 8 -8 9 15.56 3.78 -8 8 9 17.96 3.39 8 8 -9 15.61 2.74 8 8 9 12.96 3.20 8 8 9 12.74 2.84 8 8 9 18.76 3.72 -8 8 -9 16.79 3.26 0 9 9 7.01 0.88 0 9 9 7.94 0.69 0 9 -9 6.42 1.07 0 -9 -9 7.13 0.71 0 -9 9 6.37 1.11 1 9 -9 561.14 25.24 1 -9 9 575.91 25.28 -1 -9 -9 576.99 25.07 -1 9 9 587.94 25.01 -1 9 9 569.18 25.02 -1 9 -9 600.58 25.30 1 9 9 583.76 25.09 1 9 9 577.67 25.08 -1 -9 9 578.00 25.33 2 -9 9 191.17 8.66 -2 -9 -9 174.13 8.56 -2 9 9 187.40 8.25 2 9 -9 184.87 8.57 2 -9 9 184.04 8.64 -2 9 9 192.51 8.32 -2 9 -9 185.65 8.66 2 9 9 190.05 8.50 2 9 9 183.08 8.57 -2 -9 9 180.00 8.69 3 -9 9 78.35 4.33 3 -9 9 81.22 4.24 -3 9 9 78.89 3.68 -3 9 9 79.92 3.94 3 9 -9 77.43 4.24 3 9 9 76.04 4.12 -3 -9 9 77.35 4.39 -3 9 -9 76.08 4.36 3 9 9 84.77 4.35 4 -9 9 23.72 2.28 -4 9 9 21.39 1.94 4 9 -9 21.36 2.01 4 -9 9 27.23 2.46 4 9 9 22.17 2.09 -4 9 -9 23.88 2.46 4 9 9 21.50 2.28 -5 9 9 27.27 2.56 5 -9 9 33.33 2.78 5 -9 9 28.96 2.93 5 9 -9 27.91 2.80 -5 9 -9 37.12 3.16 5 9 9 24.14 2.94 5 9 9 36.97 3.13 6 9 -9 26.05 2.79 6 -9 9 21.30 2.81 6 -9 9 21.86 3.10 -6 9 -9 18.78 2.88 6 9 9 20.45 2.77 6 9 9 18.44 2.57 7 9 -9 23.19 2.81 7 -9 9 21.23 2.51 7 -9 9 19.34 3.35 -7 9 9 21.03 3.27 7 9 9 23.24 3.17 7 9 9 25.15 3.05 -7 9 -9 21.76 3.16 8 9 -9 33.23 3.39 8 -9 9 26.54 4.23 8 9 9 30.30 4.17 8 9 9 20.54 3.16 0 10 9 2.37 0.75 0 -10 -9 1.44 0.49 0 -10 9 3.40 1.14 0 10 -9 -0.28 0.89 1 10 -9 245.04 10.76 -1 10 9 234.13 10.47 1 -10 9 225.28 10.78 -1 -10 -9 239.83 10.54 1 10 9 231.21 10.54 -1 -10 9 232.76 10.86 -1 10 -9 238.84 10.78 -2 10 9 4.21 0.81 -2 10 9 3.59 0.79 2 -10 9 5.96 1.27 2 -10 9 3.35 1.22 2 10 -9 4.83 1.13 2 10 9 4.04 0.96 -2 -10 9 3.07 1.32 -2 10 -9 3.55 1.16 2 10 9 3.74 0.95 3 -10 9 23.49 2.31 -3 10 9 25.58 1.84 3 10 -9 25.66 2.13 3 -10 9 20.81 1.94 3 10 9 29.12 2.20 -3 -10 9 25.32 2.57 -3 10 -9 25.06 2.34 3 10 9 26.85 2.20 4 -10 9 13.02 1.91 4 -10 9 10.82 1.56 4 10 -9 14.05 1.99 -4 10 9 17.93 1.91 4 10 9 13.44 1.85 4 10 9 13.09 1.72 -4 10 -9 16.62 2.28 5 10 -9 22.15 2.36 -5 10 9 21.74 2.62 5 -10 9 19.58 2.67 5 -10 9 24.80 2.60 5 10 9 19.36 2.28 -5 10 -9 22.70 2.93 5 10 9 24.23 2.44 6 -10 9 -0.54 1.45 -6 10 9 4.51 2.19 6 10 -9 0.25 1.49 6 10 9 1.04 2.09 -6 10 -9 3.20 2.19 6 10 9 3.49 1.79 7 -10 9 14.66 3.23 7 10 -9 14.03 2.43 7 -10 9 10.60 2.05 -7 10 9 7.80 3.03 7 10 9 11.28 2.83 7 10 9 8.77 2.28 -7 10 -9 7.45 2.68 0 11 9 0.35 0.74 0 -11 9 -0.23 1.12 0 11 -9 1.49 0.98 1 -11 9 286.78 12.99 1 11 -9 297.60 12.93 -1 11 9 279.13 12.62 -1 -11 9 283.08 13.03 1 11 9 272.50 12.68 1 11 9 284.84 12.70 -1 11 -9 286.97 12.92 2 -11 9 1.64 1.13 2 11 -9 0.53 1.06 -2 11 9 3.30 0.87 2 -11 9 1.77 1.15 2 11 9 -0.24 0.71 2 11 9 1.12 0.87 -2 11 -9 1.98 1.15 -2 -11 9 -0.13 1.26 3 -11 9 124.58 6.21 3 -11 9 109.51 6.01 3 11 -9 117.32 7.31 -3 11 9 118.89 5.83 -3 -11 9 125.74 6.51 3 11 9 125.16 6.11 -3 11 -9 120.11 6.29 3 11 9 124.96 6.17 4 -11 9 3.78 1.47 4 -11 9 2.03 1.48 4 11 -9 5.35 1.60 -4 11 9 3.43 1.38 4 11 9 3.20 1.52 4 11 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35.28 3.59 5 12 9 33.35 3.36 5 12 9 28.49 3.07 6 -12 9 10.81 2.73 6 12 -9 9.32 2.26 6 -12 9 13.11 2.27 -6 12 9 10.08 2.58 -6 12 -9 10.05 2.55 6 12 9 10.07 2.19 6 12 9 9.48 2.55 0 13 9 39.49 2.68 0 -13 9 38.16 3.27 0 13 -9 37.67 2.79 1 -13 9 19.03 2.35 1 13 -9 17.73 2.08 -1 13 9 17.79 1.88 1 13 9 25.04 2.07 -1 -13 9 16.23 2.18 -1 13 -9 16.11 2.16 -2 13 9 10.29 1.47 2 13 -9 9.65 1.66 2 -13 9 11.05 1.78 2 -13 9 9.14 2.00 -2 -13 9 13.20 2.20 2 13 9 15.15 2.02 -2 13 -9 9.51 1.78 -3 13 9 81.21 4.48 3 13 -9 86.24 4.71 3 -13 9 82.43 4.74 3 -13 9 76.86 4.93 -3 13 -9 74.22 4.86 3 13 9 87.64 4.71 3 13 9 80.45 4.55 4 13 -9 15.77 2.18 4 -13 9 15.43 2.40 4 -13 9 18.28 2.35 -4 13 9 24.71 2.73 -4 13 -9 20.45 2.71 4 13 9 19.79 2.51 4 13 9 21.49 2.55 -5 13 9 2.92 2.22 5 13 -9 3.61 1.98 5 -13 9 2.86 1.86 -5 13 -9 0.63 2.03 5 13 9 3.89 2.03 5 13 9 1.61 2.00 -6 13 9 -0.29 2.88 6 13 -9 10.64 2.24 6 -13 9 8.37 2.28 -6 13 -9 3.06 2.59 6 13 9 3.02 2.40 6 13 9 7.41 2.17 0 -14 9 14.06 2.19 0 14 -9 14.04 1.88 0 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12 13 32.63 3.21 -4 12 -13 30.80 3.48 4 12 13 36.00 3.17 5 -12 13 14.60 2.41 5 -12 13 13.86 2.53 -5 12 13 14.42 2.33 5 12 -13 15.13 2.35 5 12 13 16.81 2.39 -5 12 -13 13.07 3.04 5 12 13 13.34 2.62 0 13 -13 3.89 1.43 0 -13 13 5.30 1.83 0 13 13 2.23 1.18 1 -13 13 9.34 1.71 -1 13 13 15.70 1.84 1 -13 13 15.12 2.21 1 13 -13 13.51 1.99 1 13 13 11.61 1.64 -1 13 -13 10.22 2.07 -1 -13 13 10.50 2.10 2 13 -13 3.80 1.67 -2 13 13 4.74 1.23 2 -13 13 4.97 1.77 2 -13 13 5.25 1.79 2 13 13 5.01 1.49 -2 13 -13 5.83 1.76 -2 -13 13 3.38 1.94 3 13 -13 20.71 2.44 -3 13 13 16.88 2.24 3 -13 13 15.52 2.29 3 -13 13 19.09 2.68 -3 13 -13 19.01 2.62 3 13 13 17.92 2.25 -3 -13 13 16.00 2.59 -4 13 13 9.44 1.99 4 -13 13 4.25 2.16 4 -13 13 4.72 2.47 4 13 -13 6.68 1.88 4 13 13 3.72 1.95 4 13 13 7.76 1.85 -4 13 -13 9.19 2.66 5 13 -13 0.39 1.76 5 -13 13 3.63 2.26 5 -13 13 -0.75 1.97 -5 13 -13 0.28 2.87 5 13 13 -0.11 2.11 5 13 13 -1.26 2.11 0 14 -13 30.65 2.84 0 -14 13 22.27 2.88 0 14 13 33.64 2.62 1 14 -13 15.31 2.16 -1 14 13 16.76 2.01 1 -14 13 15.36 2.41 1 -14 13 19.06 2.68 -1 14 -13 15.99 2.25 -1 -14 13 19.06 2.52 1 14 13 17.26 2.19 2 -14 13 1.25 1.96 2 -14 13 -3.36 1.94 2 14 -13 1.48 1.50 2 14 13 1.56 1.43 -2 -14 13 3.50 2.10 -2 14 -13 -1.19 1.94 3 -14 13 6.99 2.03 3 14 -13 8.75 1.94 -3 14 13 8.46 2.00 3 -14 13 10.34 2.15 3 14 13 6.82 1.96 -3 14 -13 8.44 2.35 4 14 -13 52.03 3.72 4 -14 13 35.45 4.48 4 -14 13 51.26 4.52 4 14 13 48.13 3.98 -4 14 -13 42.34 4.37 0 15 -13 8.36 2.00 0 -15 13 12.83 2.47 0 15 13 11.26 1.84 1 -15 13 10.36 2.60 1 -15 13 8.17 2.37 1 15 -13 10.77 2.03 -1 15 13 16.04 2.01 -1 15 -13 8.23 2.17 1 15 13 7.68 1.88 -1 -15 13 8.96 2.46 2 15 -13 2.95 1.86 2 -15 13 1.61 2.27 2 -15 13 5.82 2.39 -2 -15 13 5.80 2.45 2 15 13 2.45 1.74 -2 15 -13 3.54 1.98 3 -15 13 15.67 2.99 3 -15 13 20.15 3.17 3 15 -13 21.76 2.72 3 15 13 14.02 2.42 -3 15 -13 14.50 2.76 0 16 13 12.63 2.48 0 -16 13 11.07 2.81 0 16 -13 6.96 2.09 1 16 -13 4.33 1.87 1 -16 13 1.90 2.27 1 -16 13 1.70 2.23 1 16 13 0.20 1.70 -1 16 -13 1.57 1.98 -1 -16 13 2.66 2.49 0 0 14 310.84 13.09 0 0 14 313.23 13.45 0 0 -14 292.61 13.38 0 0 14 293.05 13.24 1 0 14 14.60 1.46 1 0 14 15.49 1.30 -1 0 -14 14.82 1.64 1 0 14 15.50 1.21 1 0 -14 15.75 1.42 -1 0 14 16.16 1.00 -1 0 14 14.55 1.04 2 0 -14 101.04 4.76 2 0 14 105.13 5.15 -2 0 14 104.34 4.68 -2 0 14 105.17 4.63 2 0 14 101.29 5.15 2 0 14 98.76 4.89 -3 0 14 157.60 6.98 3 0 14 164.86 7.70 -3 0 14 164.30 7.24 3 0 -14 159.74 7.06 3 0 14 150.32 7.72 4 0 14 446.70 19.58 4 0 14 411.75 19.20 5 0 14 55.71 3.90 5 0 14 49.76 3.64 6 0 14 10.37 2.02 6 0 14 6.72 2.04 7 0 14 -0.38 1.67 7 0 14 0.63 2.13 8 0 14 43.51 4.36 8 0 14 53.93 4.99 0 1 14 26.10 1.70 0 1 14 24.76 1.77 0 -1 14 26.81 1.69 0 1 14 29.08 1.46 0 1 -14 27.01 1.91 0 -1 14 29.57 1.53 -1 1 14 75.33 3.56 1 1 -14 76.04 3.79 -1 1 14 67.92 3.49 1 -1 14 77.35 3.84 1 -1 14 85.18 3.69 1 -1 14 74.35 3.92 -1 -1 14 76.78 3.66 1 1 14 80.26 3.69 -1 -1 14 82.37 3.61 1 1 14 76.11 3.92 1 1 14 74.88 3.93 2 -1 14 209.55 9.77 -2 1 14 211.26 9.49 2 -1 14 216.82 9.95 -2 1 14 224.01 9.54 2 1 -14 214.32 9.69 2 -1 14 232.10 10.18 -2 -1 14 229.23 9.65 2 1 14 211.49 10.03 -2 -1 14 214.98 9.58 2 1 14 209.63 9.79 2 1 14 233.84 10.20 3 1 -14 146.53 6.52 3 -1 14 146.47 7.04 3 -1 14 150.72 7.30 3 1 14 142.07 7.17 -3 -1 14 134.95 6.65 -3 -1 14 141.83 6.46 -3 1 -14 149.57 6.75 3 1 14 152.05 7.17 4 -1 14 74.68 4.32 4 1 -14 70.54 3.20 4 1 -14 73.90 3.43 4 -1 14 64.13 4.23 4 1 -14 76.31 3.19 4 1 14 69.74 4.39 4 1 14 73.00 4.36 -4 1 -14 77.39 3.94 5 -1 14 33.42 3.19 5 1 -14 32.68 1.82 5 -1 14 33.97 3.12 5 1 14 34.50 3.23 5 1 14 33.97 3.20 6 1 -14 24.55 1.60 6 -1 14 20.21 2.58 6 -1 14 25.38 3.19 6 1 14 22.91 2.69 6 1 14 24.23 2.92 7 -1 14 10.36 2.48 7 -1 14 4.22 2.60 7 1 14 8.59 2.36 7 1 14 6.85 2.18 8 -1 14 14.18 2.79 8 -1 14 8.70 3.27 8 1 14 5.40 2.35 8 1 14 7.36 2.98 0 2 -14 254.96 10.76 0 2 -14 247.09 11.19 0 2 14 249.19 11.16 0 -2 14 246.23 10.94 0 -2 14 252.57 11.04 0 2 14 241.82 11.08 0 2 14 256.18 10.79 -1 2 14 94.67 3.99 1 -2 14 85.12 4.43 1 -2 14 80.03 4.53 1 2 -14 96.43 4.46 -1 2 14 95.32 4.42 -1 2 14 93.35 4.22 1 -2 14 86.55 4.29 1 2 14 96.54 4.62 1 2 14 94.47 4.28 -1 2 -14 92.37 4.24 -1 -2 14 97.21 4.30 1 2 14 88.69 4.58 -1 -2 14 92.00 4.33 2 2 -14 50.74 2.68 2 -2 14 46.13 2.67 -2 2 14 51.47 2.40 2 -2 14 49.13 2.91 -2 2 14 49.56 2.34 2 -2 14 52.82 3.00 -2 2 14 52.51 2.47 2 2 14 52.26 2.76 2 2 14 50.57 2.97 -2 -2 14 51.69 2.63 -2 -2 14 51.22 2.61 2 2 14 50.06 3.09 3 -2 14 60.84 3.55 -3 2 14 61.89 3.19 3 2 -14 63.83 3.08 3 2 -14 53.59 2.96 3 2 -14 64.30 2.82 -3 2 14 61.44 3.32 -3 -2 14 62.29 3.31 3 2 14 62.21 3.49 3 2 14 69.70 3.87 3 2 14 56.73 3.61 -3 2 -14 63.60 3.36 -3 -2 14 64.93 3.27 4 -2 14 76.97 4.24 4 -2 14 67.76 4.25 -4 2 14 73.82 3.84 4 2 -14 70.39 3.57 4 2 -14 73.09 3.42 4 2 -14 73.74 3.49 4 2 14 70.82 4.47 4 2 14 78.31 4.60 -4 2 -14 72.94 4.02 5 2 -14 23.83 1.52 5 -2 14 23.13 2.42 5 -2 14 21.25 2.75 -5 2 -14 24.37 2.49 5 2 14 18.54 2.36 5 2 14 18.89 2.32 6 -2 14 16.89 2.68 6 -2 14 11.35 2.13 6 2 -14 16.48 1.42 -6 2 -14 14.03 2.20 6 2 14 12.72 2.26 6 2 14 12.05 2.49 7 -2 14 13.04 2.47 7 -2 14 8.75 2.26 7 2 14 11.12 2.69 7 2 14 9.89 2.37 8 -2 14 24.22 3.62 8 -2 14 28.83 3.30 8 2 14 25.45 3.65 8 2 14 28.44 3.67 0 -3 14 17.67 1.35 0 3 -14 18.55 1.33 0 -3 14 18.56 1.47 0 3 14 17.64 1.61 0 3 14 19.18 1.45 1 -3 14 309.15 13.40 1 -3 14 308.08 13.67 1 -3 14 300.53 13.32 -1 3 14 295.11 13.21 1 3 -14 302.52 13.38 1 3 -14 304.63 13.15 -1 3 14 308.49 13.35 -1 -3 14 302.65 13.32 -1 3 -14 292.57 13.32 1 3 14 287.66 13.54 -1 -3 14 320.61 13.31 1 3 14 298.64 13.55 1 3 14 313.02 13.21 2 3 -14 136.50 6.12 2 3 -14 139.78 6.32 -2 3 14 135.44 6.09 2 3 -14 141.51 6.25 2 -3 14 140.10 6.51 -2 3 14 116.89 6.25 -2 3 14 135.39 6.01 2 -3 14 147.21 6.81 2 3 14 140.07 6.75 2 3 14 146.35 6.80 2 3 14 137.01 6.38 -2 -3 14 141.00 6.32 -2 -3 14 140.93 6.37 -2 3 -14 139.65 6.47 3 3 -14 298.12 12.52 3 3 -14 287.27 12.66 -3 3 14 282.15 12.78 3 -3 14 306.72 13.29 -3 3 14 277.29 12.65 3 -3 14 283.31 12.94 3 3 -14 286.00 12.61 3 3 14 288.86 13.33 3 3 14 285.46 13.20 -3 -3 14 294.15 12.67 3 3 14 280.53 12.92 -3 3 -14 284.44 12.91 -4 3 14 5.88 1.08 -4 3 14 3.91 1.14 4 3 -14 5.47 0.80 4 -3 14 4.78 1.27 4 3 -14 4.73 0.80 4 3 -14 5.27 1.17 4 -3 14 5.69 1.37 4 3 14 3.30 1.47 4 3 14 6.83 1.46 -4 3 -14 6.71 1.33 5 3 -14 40.71 2.30 5 -3 14 37.63 3.14 5 -3 14 38.48 3.13 -5 3 14 42.40 2.79 5 3 14 41.12 3.48 5 3 14 44.15 3.69 -5 3 -14 41.04 3.02 -6 3 14 15.65 2.09 6 3 -14 15.87 1.55 6 -3 14 13.86 2.30 6 -3 14 13.19 2.11 6 3 14 13.81 2.75 6 3 14 11.94 2.46 -6 3 -14 18.53 2.48 7 -3 14 83.21 5.71 7 -3 14 72.37 4.92 7 3 14 54.24 4.80 -7 3 -14 67.38 5.15 7 3 14 77.56 5.73 8 -3 14 11.01 2.54 8 -3 14 15.48 2.95 8 3 14 18.67 3.55 8 3 14 13.48 2.84 0 4 14 0.18 0.78 0 4 14 0.66 0.61 0 -4 14 0.40 0.58 0 -4 14 2.36 0.72 0 4 -14 0.93 0.62 1 4 -14 256.60 12.44 -1 4 14 296.45 12.47 1 -4 14 292.18 12.57 1 -4 14 260.89 12.73 -1 4 14 283.45 12.38 -1 -4 14 300.94 12.68 1 4 14 279.10 12.71 1 4 14 283.90 12.71 -1 4 -14 286.24 12.52 -1 -4 14 286.05 12.49 -2 4 14 36.31 1.99 2 -4 14 36.36 2.40 2 -4 14 35.03 2.33 -2 4 14 35.13 1.73 2 4 -14 34.17 2.11 -2 4 14 34.78 1.68 2 4 -14 35.71 1.93 -2 4 14 36.19 1.96 2 4 14 33.78 2.64 2 4 14 36.86 2.36 2 4 14 36.21 2.20 -2 4 -14 35.13 2.28 -2 -4 14 35.55 2.14 3 -4 14 76.11 4.27 3 -4 14 73.20 3.97 3 4 -14 76.27 3.49 -3 4 14 71.26 3.60 3 4 -14 76.47 3.85 3 4 -14 69.60 3.59 -3 4 14 71.45 3.68 3 4 14 71.74 4.12 3 4 14 75.64 4.16 -3 -4 14 70.80 3.69 -3 4 -14 72.24 4.01 3 4 14 70.39 4.34 4 -4 14 195.18 10.27 4 4 -14 205.62 9.78 4 -4 14 217.33 10.01 -4 4 14 223.59 9.79 4 4 -14 220.09 9.57 -4 4 14 209.03 9.81 4 4 14 230.51 10.54 -4 4 -14 219.27 10.08 4 4 14 213.56 10.38 5 -4 14 2.57 1.27 5 4 -14 2.75 0.90 5 -4 14 0.69 1.26 -5 4 14 2.90 1.19 -5 4 -14 2.90 1.43 5 4 14 2.21 1.30 5 4 14 4.07 1.92 6 -4 14 2.70 2.15 -6 4 14 0.61 1.50 6 -4 14 -1.39 1.39 6 4 -14 0.74 1.01 6 4 14 2.45 2.05 6 4 14 -1.88 2.06 -6 4 -14 0.10 2.09 7 -4 14 5.21 2.63 7 4 -14 4.61 1.35 7 -4 14 3.97 1.95 -7 4 14 7.08 2.26 -7 4 -14 3.03 2.41 7 4 14 7.06 2.67 7 4 14 3.28 2.03 8 -4 14 21.28 3.87 8 -4 14 16.85 2.59 8 4 14 11.31 3.50 8 4 14 14.00 3.46 -8 4 -14 17.01 3.57 0 5 14 2.84 0.87 0 5 -14 4.31 0.80 0 5 14 2.85 0.97 0 -5 14 3.85 0.87 -1 5 14 52.15 2.79 1 -5 14 55.16 3.05 1 5 -14 56.03 2.80 1 -5 14 54.94 3.15 -1 5 14 55.91 2.84 -1 -5 14 57.10 2.98 1 5 14 50.55 3.21 -1 5 -14 51.92 2.96 1 5 14 58.43 3.11 2 -5 14 6.10 1.14 -2 5 14 8.40 0.68 -2 5 14 7.39 0.66 -2 5 14 7.36 0.63 -2 5 14 7.45 0.80 2 5 -14 6.81 0.93 2 -5 14 6.77 1.11 -2 5 14 7.21 0.88 -2 -5 14 6.24 0.98 2 5 14 7.14 1.23 -2 5 -14 8.41 1.17 2 5 14 6.86 1.37 3 5 -14 114.19 5.11 -3 5 14 105.64 5.09 3 -5 14 115.63 5.46 3 5 -14 110.71 5.42 3 -5 14 100.26 5.60 -3 5 14 109.63 5.07 3 5 14 104.27 5.80 -3 -5 14 105.32 5.24 -3 5 -14 105.12 5.47 3 5 14 114.92 5.79 -4 5 14 17.39 1.67 4 -5 14 12.63 1.86 4 -5 14 15.43 1.80 -4 5 14 13.64 1.54 4 5 -14 15.11 1.46 4 5 14 14.34 2.17 -4 5 -14 16.82 2.10 4 5 14 16.79 2.24 5 -5 14 0.80 1.25 5 -5 14 2.37 1.44 5 5 -14 2.81 0.97 -5 5 14 4.54 1.29 5 5 14 2.63 2.58 -5 5 -14 3.66 1.69 5 5 14 1.97 1.87 6 5 -14 0.60 1.15 6 -5 14 0.74 2.10 -6 5 14 -1.11 1.61 6 -5 14 1.60 1.61 6 5 14 1.04 1.57 -6 5 -14 3.46 2.13 6 5 14 0.33 2.01 7 -5 14 6.66 2.06 7 -5 14 4.54 2.03 7 5 -14 7.91 1.59 -7 5 14 11.19 2.44 -7 5 -14 7.91 2.47 7 5 14 8.43 2.89 7 5 14 10.03 2.84 8 -5 14 21.69 3.87 8 -5 14 20.68 2.83 -8 5 14 17.69 3.48 8 5 14 18.07 3.11 8 5 14 10.67 3.58 -8 5 -14 20.05 3.28 0 6 14 142.07 6.53 0 6 14 140.89 6.66 0 6 -14 140.51 6.46 0 -6 14 135.33 6.59 1 6 -14 0.85 0.69 -1 6 14 1.32 0.64 -1 6 14 0.77 0.30 1 -6 14 0.94 0.87 -1 6 14 -0.50 0.60 -1 -6 14 0.60 0.78 -1 6 -14 1.01 0.86 1 6 14 0.69 0.77 -2 6 14 89.64 4.09 2 -6 14 99.27 4.89 -2 6 14 88.83 4.12 2 6 -14 91.11 4.31 2 -6 14 85.50 4.58 -2 6 14 94.29 4.04 -2 6 14 86.44 4.00 -2 6 14 85.78 4.07 2 6 14 90.03 4.71 -2 -6 14 86.49 4.49 -2 6 -14 88.09 4.58 -3 6 14 6.64 0.72 -3 6 14 6.68 0.98 -3 6 14 5.60 0.84 3 -6 14 4.92 1.24 3 -6 14 5.78 1.20 3 6 -14 6.24 1.04 -3 -6 14 7.24 1.13 3 6 14 5.43 1.45 -3 6 -14 5.50 1.45 4 -6 14 93.34 5.61 4 -6 14 106.51 5.45 -4 6 14 105.24 5.15 4 6 -14 105.37 5.08 4 6 14 110.35 5.95 -4 6 -14 101.67 5.61 4 6 14 111.74 6.11 5 -6 14 5.83 1.48 -5 6 14 7.81 1.48 5 -6 14 7.48 1.97 5 6 -14 6.81 1.31 5 6 14 5.41 1.96 -5 6 -14 8.80 1.98 5 6 14 7.25 2.17 6 6 -14 6.22 1.43 6 -6 14 5.85 1.75 -6 6 14 7.83 1.97 6 -6 14 6.79 1.94 6 6 14 8.50 2.59 6 6 14 8.35 2.04 -6 6 -14 5.33 2.29 7 6 -14 7.69 2.07 7 -6 14 4.95 2.02 7 -6 14 9.90 2.92 -7 6 14 9.86 2.60 7 6 14 14.05 3.15 7 6 14 7.47 2.94 -7 6 -14 6.49 2.54 8 -6 14 5.34 3.25 -8 6 14 5.97 2.63 8 -6 14 4.69 2.26 8 6 14 3.41 3.43 8 6 14 5.96 3.39 -8 6 -14 4.94 2.78 0 7 14 134.33 6.21 0 -7 14 135.95 6.41 0 7 -14 128.98 6.25 0 7 14 131.95 5.92 -1 7 14 139.69 6.72 -1 7 14 149.55 6.64 -1 7 14 146.53 6.51 1 -7 14 151.43 7.06 1 7 -14 150.78 6.90 -1 -7 14 152.09 7.05 -1 7 -14 142.49 7.02 1 7 14 155.80 7.08 2 -7 14 42.20 2.87 -2 7 14 36.45 1.91 2 7 -14 35.86 2.30 -2 7 14 37.54 2.06 -2 7 14 36.10 1.90 2 -7 14 36.23 2.67 2 7 14 39.91 2.63 -2 -7 14 33.08 2.54 -2 7 -14 36.42 2.57 3 7 -14 183.68 8.79 3 -7 14 202.64 9.44 3 -7 14 199.37 9.09 -3 7 14 186.94 8.60 3 7 14 186.26 9.30 -3 7 -14 192.74 9.26 -3 -7 14 198.20 8.99 4 -7 14 6.08 1.35 4 -7 14 8.54 1.60 -4 7 14 9.22 1.30 4 7 -14 5.71 1.11 4 7 14 7.64 1.53 -4 7 -14 6.23 1.58 5 -7 14 28.28 2.88 5 -7 14 26.77 2.65 -5 7 14 28.41 2.55 5 7 -14 25.11 2.26 5 7 14 27.38 3.09 5 7 14 23.41 3.02 -5 7 -14 28.14 2.94 6 -7 14 21.76 3.02 -6 7 14 31.29 3.11 6 -7 14 31.30 3.26 6 7 -14 29.43 2.66 6 7 14 31.85 3.68 6 7 14 27.22 3.15 -6 7 -14 29.68 3.49 7 -7 14 10.09 2.48 7 -7 14 15.66 2.42 7 7 -14 15.42 2.23 -7 7 14 9.33 2.79 7 7 14 11.52 3.10 -7 7 -14 11.49 3.12 7 7 14 8.66 2.43 0 8 14 25.81 1.66 0 8 14 26.81 1.79 0 -8 14 25.40 2.30 0 8 -14 27.79 1.98 1 8 -14 86.24 4.25 -1 8 14 83.17 4.01 -1 8 14 72.06 3.65 -1 8 14 81.91 3.83 1 -8 14 85.64 4.46 -1 8 -14 84.86 4.35 -1 -8 14 85.75 4.45 1 8 14 84.21 4.02 1 8 14 84.83 4.29 2 8 -14 491.16 20.59 -2 8 14 460.19 20.28 2 -8 14 472.86 20.99 2 -8 14 474.68 20.78 -2 8 14 460.12 20.23 -2 8 -14 461.53 20.83 -2 -8 14 468.38 20.77 2 8 14 470.08 20.85 -3 8 14 9.38 1.24 3 8 -14 8.51 1.36 3 -8 14 6.71 1.40 3 -8 14 9.72 1.61 -3 8 -14 8.48 1.75 3 8 14 9.86 1.73 -3 -8 14 9.76 1.51 4 8 -14 3.38 1.03 -4 8 14 4.21 1.15 4 -8 14 3.24 1.32 4 -8 14 5.43 1.50 4 8 14 2.68 1.26 -4 8 -14 -0.96 1.66 5 8 -14 12.38 1.67 -5 8 14 13.76 1.84 5 -8 14 10.78 2.27 5 -8 14 12.68 2.05 -5 8 -14 10.01 2.20 6 -8 14 5.38 2.66 6 8 -14 5.79 1.68 -6 8 14 6.67 2.10 6 -8 14 4.95 1.84 6 8 14 3.91 2.71 -6 8 -14 7.84 2.47 6 8 14 0.67 2.47 -7 8 14 12.21 2.83 7 -8 14 13.03 3.30 7 -8 14 11.13 2.37 7 8 -14 11.79 2.31 7 8 14 6.22 2.87 -7 8 -14 9.52 2.94 7 8 14 13.32 3.28 0 -9 14 130.83 6.46 0 9 14 124.95 5.89 0 9 14 129.12 5.91 0 9 -14 133.18 6.28 -1 9 14 157.86 7.48 1 9 -14 164.12 7.72 -1 9 14 159.93 7.31 1 -9 14 165.56 7.91 -1 9 -14 161.94 7.79 -1 -9 14 165.09 7.91 1 9 14 162.18 7.44 1 9 14 173.90 7.71 2 9 -14 156.52 7.55 2 -9 14 175.14 8.06 2 -9 14 163.42 7.77 -2 9 14 154.49 7.17 2 9 14 164.56 7.75 -2 -9 14 156.97 7.76 2 9 14 152.60 7.43 -2 9 -14 158.47 7.78 3 -9 14 6.50 1.45 -3 9 14 9.30 1.18 3 9 -14 8.72 1.34 3 9 14 7.40 1.34 3 9 14 6.64 1.59 -3 9 -14 8.77 1.86 -3 -9 14 10.47 1.65 4 -9 14 7.32 1.58 4 9 -14 10.03 1.58 -4 9 14 8.29 1.37 -4 9 -14 6.42 1.97 4 9 14 8.57 1.90 5 9 -14 3.59 1.53 5 -9 14 1.32 1.59 -5 9 14 4.86 1.72 5 -9 14 3.42 1.64 5 9 14 4.13 2.13 -5 9 -14 6.00 2.07 6 -9 14 39.55 4.50 6 -9 14 44.48 3.78 6 9 -14 39.00 3.44 6 9 14 46.76 4.59 -6 9 -14 31.50 3.96 7 -9 14 34.08 3.95 7 -9 14 26.38 3.25 7 9 -14 36.82 3.67 -7 9 14 37.31 4.33 7 9 14 28.75 4.55 -7 9 -14 40.88 5.01 7 9 14 42.39 4.85 0 10 14 27.18 1.62 0 -10 14 35.53 2.80 0 10 14 34.40 1.97 0 10 -14 32.34 2.35 1 -10 14 22.64 2.54 1 10 -14 22.92 2.03 -1 10 14 25.38 1.62 -1 10 -14 23.86 2.18 1 10 14 24.63 1.80 -1 -10 14 27.22 2.62 1 10 14 21.07 1.76 -2 10 14 9.29 1.16 2 10 -14 9.71 1.52 2 -10 14 9.96 1.62 2 -10 14 13.27 1.88 -2 10 -14 11.80 1.71 -2 -10 14 10.56 1.77 2 10 14 10.31 1.42 2 10 14 11.12 1.47 3 10 -14 22.68 2.14 3 -10 14 28.68 2.78 -3 10 14 24.18 1.89 3 -10 14 22.27 2.64 3 10 14 23.45 2.25 -3 10 -14 30.53 2.97 -3 -10 14 24.29 2.92 3 10 14 20.00 2.64 4 -10 14 5.92 1.71 4 10 -14 4.59 1.50 -4 10 14 6.80 1.45 4 -10 14 7.80 2.07 4 10 14 5.58 1.51 -4 10 -14 6.91 2.02 4 10 14 2.02 1.77 5 -10 14 7.46 1.87 -5 10 14 8.77 2.01 5 -10 14 8.66 2.48 5 10 -14 9.00 1.74 5 10 14 5.84 2.35 5 10 14 8.04 2.13 -5 10 -14 9.74 2.67 6 -10 14 19.67 2.99 -6 10 14 25.19 2.88 6 -10 14 21.67 2.71 6 10 -14 25.29 3.16 -6 10 -14 20.17 3.30 6 10 14 20.00 3.02 6 10 14 17.76 3.24 0 -11 14 150.93 7.49 0 11 14 149.87 6.85 0 11 -14 141.81 7.49 1 -11 14 56.00 3.71 -1 11 14 54.04 2.83 1 11 -14 49.34 3.69 -1 -11 14 54.25 3.86 1 11 14 49.98 2.79 -1 11 -14 48.20 3.71 1 11 14 53.36 2.95 2 -11 14 14.67 2.44 2 11 -14 12.99 2.05 2 -11 14 13.10 1.93 -2 11 14 14.60 1.39 2 11 14 15.44 1.90 -2 11 -14 16.59 2.25 -2 -11 14 13.54 2.04 2 11 14 13.51 1.66 -3 11 14 39.63 2.53 3 -11 14 43.11 3.48 3 -11 14 35.60 3.33 3 11 -14 40.87 2.99 3 11 14 42.32 2.86 3 11 14 38.34 2.97 -3 11 -14 32.94 3.27 -3 -11 14 36.00 3.59 4 -11 14 14.01 2.54 4 -11 14 14.21 2.19 4 11 -14 15.10 2.13 -4 11 14 14.02 1.87 4 11 14 11.87 2.25 4 11 14 13.33 2.04 -4 11 -14 12.55 2.44 -5 11 14 2.43 1.71 5 -11 14 4.67 2.49 5 11 -14 2.02 1.88 5 -11 14 1.78 1.63 -5 11 -14 -1.40 2.17 5 11 14 1.55 2.18 5 11 14 3.34 1.90 6 11 -14 -0.35 2.10 6 -11 14 2.31 2.27 6 -11 14 4.51 2.06 6 11 14 1.31 2.14 -6 11 -14 1.96 2.64 6 11 14 -1.45 2.59 0 12 -14 32.07 2.68 0 12 14 33.73 2.25 0 -12 14 38.79 3.31 1 -12 14 5.22 1.67 1 12 -14 6.06 1.50 -1 12 14 8.12 1.15 -1 12 -14 3.39 1.48 1 12 14 7.59 1.25 -1 -12 14 6.07 1.68 -2 12 14 2.85 0.98 2 -12 14 7.48 1.81 2 -12 14 1.26 1.66 2 12 -14 3.71 1.49 2 12 14 4.63 1.31 -2 12 -14 3.62 1.88 -2 -12 14 0.97 1.58 -3 12 14 14.72 1.82 3 12 -14 15.55 2.13 3 -12 14 19.09 2.39 3 -12 14 17.70 2.58 -3 -12 14 14.58 2.41 3 12 14 17.11 2.29 -3 12 -14 14.70 2.47 3 12 14 17.64 2.13 4 12 -14 5.07 1.69 4 -12 14 1.49 1.77 4 -12 14 -1.11 2.17 -4 12 -14 4.81 2.41 4 12 14 2.01 1.74 4 12 14 5.67 1.80 5 -12 14 6.42 2.13 5 -12 14 10.35 2.96 5 12 -14 11.34 2.31 5 12 14 6.63 2.53 -5 12 -14 11.33 2.75 5 12 14 10.85 2.30 0 13 14 4.78 1.23 0 13 -14 7.31 1.67 0 -13 14 7.89 1.97 1 -13 14 1.82 1.75 1 -13 14 3.06 1.86 -1 13 14 4.16 1.17 1 13 -14 2.06 1.45 -1 13 -14 1.89 1.78 1 13 14 1.16 1.21 -1 -13 14 3.95 1.68 2 -13 14 2.67 1.66 -2 13 14 2.83 1.14 2 -13 14 4.17 1.50 2 13 -14 2.24 1.51 2 13 14 3.97 1.42 -2 -13 14 4.76 1.97 -2 13 -14 3.09 1.81 3 -13 14 27.70 3.51 3 13 -14 27.31 2.79 3 -13 14 30.08 3.70 -3 -13 14 31.81 3.94 3 13 14 34.52 2.95 -3 13 -14 29.86 3.78 4 -13 14 6.38 2.73 4 13 -14 7.41 1.96 4 -13 14 7.92 2.33 -4 13 -14 9.61 2.87 4 13 14 8.26 1.98 5 13 -14 2.53 2.14 5 13 14 2.50 1.98 0 -14 14 4.74 2.12 0 14 -14 5.99 1.93 0 14 14 6.61 1.46 1 -14 14 21.94 2.78 1 14 -14 17.89 2.38 1 -14 14 17.20 2.57 -1 14 -14 16.72 2.57 1 14 14 17.11 2.19 -1 -14 14 21.72 2.70 2 14 -14 -1.32 1.49 2 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6 0 15 10.67 2.35 7 0 15 14.87 2.80 7 0 15 17.53 2.95 8 0 15 -0.73 2.48 8 0 15 5.43 3.16 0 -1 15 252.45 10.85 0 -1 15 243.44 10.96 0 -1 15 243.25 11.20 0 1 15 250.26 10.77 0 1 15 239.55 10.98 0 1 15 260.64 11.15 0 1 -15 246.90 11.15 1 -1 15 94.67 4.40 -1 1 15 90.26 4.29 1 -1 15 100.17 4.81 1 -1 15 86.03 4.53 -1 1 15 96.84 4.18 1 1 -15 92.53 4.56 1 1 15 92.87 4.73 -1 -1 15 93.68 4.39 1 1 15 94.05 4.67 1 1 15 93.48 4.40 -1 -1 15 96.62 4.33 2 1 -15 90.72 4.39 2 -1 15 97.25 4.87 2 -1 15 90.29 4.47 -2 1 15 94.80 4.17 -2 1 15 94.84 4.13 2 -1 15 87.76 4.61 -2 -1 15 82.64 4.30 2 1 15 86.04 4.75 2 1 15 90.04 4.47 -2 -1 15 92.01 4.29 2 1 15 99.38 4.88 3 -1 15 95.38 5.08 -3 1 15 85.59 4.30 3 1 -15 88.69 4.27 -3 1 15 89.48 3.96 3 -1 15 93.72 4.84 -3 -1 15 89.28 4.15 3 1 15 84.53 4.97 -3 -1 15 89.12 4.41 3 1 15 94.32 4.97 4 1 -15 49.67 2.50 4 -1 15 46.29 3.30 4 -1 15 46.92 3.44 4 1 15 45.13 3.58 4 1 15 50.40 3.65 5 -1 15 10.99 1.95 5 -1 15 13.99 1.99 5 1 15 11.50 2.09 5 1 15 14.96 2.17 6 -1 15 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6 24 -0.67 1.91 1 6 24 0.76 1.76 2 -6 24 3.23 1.82 2 -6 24 2.47 1.74 2 6 24 5.75 2.54 -2 -6 24 0.41 1.95 2 6 24 3.02 2.23 3 -6 24 2.72 1.78 3 -6 24 2.09 1.81 3 6 24 -0.08 2.40 -3 -6 24 1.74 1.54 3 6 24 3.49 2.54 4 -6 24 2.60 2.00 4 -6 24 0.81 2.82 4 6 24 6.13 2.58 4 6 24 -2.54 2.76 0 -7 24 8.29 2.25 0 -7 24 6.38 1.93 1 -7 24 6.91 1.97 1 -7 24 4.42 1.76 -1 -7 24 6.54 1.81 1 7 24 4.13 2.04 1 7 24 6.89 2.02 2 -7 24 52.57 4.67 2 -7 24 56.24 4.32 2 7 24 53.47 4.89 2 7 24 55.86 4.26 -2 -7 24 61.93 4.27 3 -7 24 12.28 2.23 3 -7 24 16.46 2.99 -3 -7 24 13.96 2.22 3 7 24 15.11 3.06 3 7 24 11.20 2.70 4 -7 24 18.56 3.50 4 -7 24 13.08 2.54 4 7 24 8.64 2.81 4 7 24 13.08 3.28 0 -8 24 88.74 5.43 0 -8 24 87.13 5.33 1 -8 24 2.68 1.65 1 -8 24 3.14 1.80 -1 -8 24 1.69 1.80 2 -8 24 4.72 1.94 2 -8 24 5.87 2.58 2 8 24 3.39 2.27 -2 -8 24 6.47 2.03 3 -8 24 5.28 2.08 3 -8 24 4.17 2.13 3 8 24 5.68 2.52 -3 -8 24 4.83 2.15 3 8 24 2.53 2.82 0 -9 24 62.53 4.72 0 -9 24 60.12 4.50 1 -9 24 -1.09 1.48 1 -9 24 2.00 1.96 -1 -9 24 0.44 1.99 2 -9 24 1.88 2.47 2 -9 24 5.66 2.07 -2 -9 24 0.57 2.10 2 9 24 5.12 2.70 3 -9 24 19.50 3.46 0 -10 24 3.43 2.35 0 -10 24 2.39 1.97 1 -10 24 41.38 3.68 1 -10 24 41.96 4.31 -1 -10 24 47.61 4.30 0 0 25 2.27 1.78 0 0 25 0.94 1.26 1 0 25 27.23 2.69 1 0 25 18.83 2.44 -1 0 25 22.78 2.33 -1 0 25 24.59 2.64 2 0 25 8.48 1.97 2 0 25 10.36 2.50 -2 0 25 9.26 1.86 3 0 25 16.86 3.03 3 0 25 15.17 2.37 4 0 25 3.07 1.95 4 0 25 0.01 2.53 5 0 25 5.64 2.29 5 0 25 -0.10 2.25 0 -1 25 60.84 3.82 0 1 25 53.22 4.59 0 1 25 62.43 3.74 0 -1 25 68.67 4.40 -1 1 25 24.03 2.21 -1 1 25 27.12 2.76 1 -1 25 22.21 2.67 1 1 25 28.83 2.85 1 1 25 22.74 2.54 -1 -1 25 23.08 2.39 -1 -1 25 29.16 2.47 -2 1 25 11.61 1.98 2 -1 25 13.16 2.61 2 -1 25 11.25 1.93 2 1 25 10.11 2.03 -2 -1 25 10.13 2.00 2 1 25 9.61 2.09 3 -1 25 14.92 2.98 3 -1 25 20.46 2.55 3 1 25 16.31 2.42 3 1 25 13.22 2.44 4 -1 25 8.82 2.16 4 -1 25 10.64 2.36 4 1 25 11.34 2.39 4 1 25 10.96 3.07 5 -1 25 17.60 3.67 5 -1 25 10.33 2.63 5 1 25 14.56 3.48 5 1 25 15.47 2.91 0 2 25 1.00 1.64 0 2 25 1.19 1.13 0 -2 25 -0.11 1.28 0 -2 25 2.67 1.32 -1 2 25 29.06 2.23 -1 2 25 29.59 2.89 1 -2 25 28.34 3.39 1 -2 25 34.59 2.96 -1 -2 25 26.77 2.69 -1 -2 25 25.16 2.57 1 2 25 34.46 3.36 1 2 25 30.16 3.00 2 -2 25 4.81 1.65 2 -2 25 7.45 1.98 -2 2 25 6.93 1.64 -2 -2 25 6.62 1.35 2 2 25 4.85 1.92 2 2 25 5.75 2.36 -3 2 25 2.56 1.38 3 -2 25 3.98 2.61 3 -2 25 1.73 1.84 3 2 25 4.60 1.97 3 2 25 5.33 2.08 4 -2 25 9.48 2.20 4 -2 25 8.91 2.36 4 2 25 9.66 2.41 4 2 25 10.63 2.54 5 -2 25 18.32 3.12 5 -2 25 20.57 3.33 5 2 25 15.74 2.92 5 2 25 15.44 3.37 0 -3 25 0.84 1.36 0 3 25 -0.32 1.64 0 -3 25 2.12 1.67 0 3 25 -0.51 1.19 1 -3 25 7.20 2.23 1 -3 25 5.29 1.72 -1 3 25 5.91 1.91 -1 -3 25 7.13 1.59 1 3 25 5.60 1.74 -1 -3 25 10.49 2.11 -2 3 25 10.74 1.78 2 -3 25 9.77 1.90 2 -3 25 9.57 2.12 2 3 25 6.94 2.06 2 3 25 10.42 2.59 -2 -3 25 13.87 1.73 3 -3 25 1.96 1.81 3 -3 25 5.19 1.80 3 3 25 0.00 2.48 3 3 25 2.40 2.16 4 -3 25 1.55 2.08 4 -3 25 1.07 1.91 4 3 25 3.78 2.88 4 3 25 5.76 2.34 5 -3 25 7.16 3.36 5 -3 25 -0.69 2.26 5 3 25 0.57 3.12 5 3 25 4.14 2.67 0 -4 25 4.15 1.54 0 4 25 5.84 2.00 0 4 25 4.81 1.41 0 -4 25 3.63 1.55 -1 4 25 -2.91 1.35 1 -4 25 -1.49 1.94 1 -4 25 2.87 1.53 -1 -4 25 -1.13 1.39 1 4 25 -0.18 1.34 1 4 25 1.38 1.64 -1 -4 25 1.12 1.78 -2 4 25 6.83 1.43 2 -4 25 6.49 1.92 2 -4 25 9.14 2.09 2 4 25 10.00 2.15 2 4 25 8.93 2.52 -2 -4 25 7.99 1.69 3 -4 25 8.34 2.55 3 -4 25 7.26 1.93 3 4 25 5.39 2.13 3 4 25 6.72 2.37 4 -4 25 2.13 1.96 4 -4 25 7.12 2.27 4 4 25 1.81 2.79 4 4 25 3.94 2.50 0 5 25 -1.42 1.17 0 -5 25 1.08 1.88 0 -5 25 -0.49 1.51 0 5 25 3.56 1.65 -1 5 25 3.90 1.38 1 -5 25 2.77 1.72 1 -5 25 5.42 1.76 1 5 25 8.17 2.08 -1 -5 25 4.40 1.48 1 5 25 3.24 1.76 -1 -5 25 2.15 1.59 2 -5 25 20.62 2.94 2 -5 25 31.54 3.37 2 5 25 37.89 3.90 -2 -5 25 29.45 3.33 2 5 25 26.64 3.38 3 -5 25 0.42 1.78 3 -5 25 0.37 1.77 3 5 25 2.84 2.37 3 5 25 3.81 2.61 4 -5 25 0.22 2.00 4 -5 25 2.55 2.81 4 5 25 7.37 2.68 4 5 25 0.75 2.07 0 -6 25 3.37 1.74 0 -6 25 3.34 1.60 1 -6 25 15.50 2.85 1 -6 25 25.48 3.08 1 6 25 17.67 2.56 -1 -6 25 19.97 2.32 1 6 25 16.11 2.43 -1 -6 25 15.60 2.55 2 -6 25 55.03 4.25 2 -6 25 49.56 3.99 2 6 25 48.39 4.19 -2 -6 25 45.44 4.02 2 6 25 52.08 4.85 3 -6 25 0.93 1.77 3 -6 25 7.99 2.79 3 6 25 0.37 2.64 3 6 25 3.10 2.49 4 -6 25 22.71 3.82 4 -6 25 17.42 2.78 4 6 25 25.71 3.40 4 6 25 15.89 3.53 0 -7 25 66.66 4.82 0 -7 25 63.82 4.61 1 -7 25 12.14 2.23 1 -7 25 12.94 2.26 -1 -7 25 11.19 2.18 2 -7 25 2.24 2.42 2 -7 25 2.51 1.76 -2 -7 25 2.01 1.82 2 7 25 0.83 1.97 2 7 25 -0.69 2.25 3 -7 25 6.71 2.19 3 -7 25 0.03 1.95 3 7 25 -3.05 2.54 3 7 25 8.63 2.67 0 -8 25 6.55 2.43 0 -8 25 3.73 1.92 1 -8 25 9.92 2.13 1 -8 25 10.46 2.16 -1 -8 25 12.42 2.31 2 -8 25 -1.64 1.79 2 -8 25 -1.03 1.68 2 8 25 3.63 2.62 -2 -8 25 -1.42 2.02 0 -9 25 9.59 2.13 0 -9 25 13.96 2.26 1 -9 25 16.65 2.94 1 -9 25 13.72 2.46 -1 -9 25 15.20 2.58 0 0 26 53.42 3.80 0 0 26 57.15 3.69 1 0 26 4.85 1.70 -1 0 26 4.09 1.91 1 0 26 3.52 1.57 -1 0 26 4.81 1.26 2 0 26 45.96 3.75 -2 0 26 41.41 3.42 2 0 26 36.20 3.61 3 0 26 2.16 2.50 -3 0 26 3.31 1.35 3 0 26 -1.21 1.87 4 0 26 -3.52 1.80 4 0 26 0.84 2.02 0 -1 26 15.74 2.27 0 -1 26 18.24 2.05 0 1 26 17.87 2.39 0 1 26 19.95 2.40 1 -1 26 80.72 5.28 -1 1 26 99.33 5.33 1 -1 26 86.15 5.07 1 1 26 79.11 5.68 -1 -1 26 89.11 4.76 1 1 26 84.94 5.55 -1 -1 26 91.60 5.32 2 -1 26 10.75 1.96 2 -1 26 13.02 2.31 -2 1 26 8.15 1.86 2 1 26 9.42 2.68 2 1 26 8.98 2.10 -2 -1 26 12.00 2.20 -3 1 26 0.45 1.49 3 -1 26 4.19 2.11 3 -1 26 3.18 1.87 3 1 26 1.34 1.89 3 1 26 3.28 1.91 4 -1 26 10.46 2.36 4 -1 26 -0.89 2.74 4 1 26 4.25 2.26 4 1 26 6.79 2.36 0 2 26 8.83 1.50 0 2 26 6.33 1.96 0 -2 26 5.14 2.08 1 -2 26 1.93 1.59 1 -2 26 6.07 2.22 -1 -2 26 3.88 1.44 -1 -2 26 1.42 1.36 1 2 26 4.44 2.14 2 -2 26 1.17 1.73 2 -2 26 1.28 2.35 -2 2 26 0.81 2.97 2 2 26 5.26 2.42 2 2 26 0.71 1.80 -2 -2 26 1.32 1.77 -3 2 26 5.62 1.83 3 -2 26 11.36 2.21 3 -2 26 12.28 2.51 3 2 26 11.17 2.35 3 2 26 8.20 2.31 4 -2 26 5.12 2.08 4 -2 26 6.98 2.85 4 2 26 8.84 3.10 4 2 26 3.68 2.22 0 3 26 1.12 3.47 0 -3 26 0.26 1.45 0 -3 26 -1.48 1.31 0 3 26 -0.02 1.25 -1 3 26 7.46 1.85 1 -3 26 10.19 1.91 1 -3 26 9.06 1.98 1 3 26 8.08 2.28 -1 -3 26 8.24 2.13 -1 -3 26 8.28 1.72 2 -3 26 8.12 1.97 2 -3 26 12.26 2.29 -2 3 26 11.70 1.85 2 3 26 9.82 2.29 -2 -3 26 8.23 1.72 2 3 26 6.97 2.66 3 -3 26 2.19 1.78 3 -3 26 4.20 2.05 3 3 26 4.82 2.27 3 3 26 0.16 2.66 4 -3 26 37.38 3.89 4 -3 26 34.22 4.60 4 3 26 22.13 3.83 4 3 26 23.83 3.26 0 4 26 4.69 1.86 0 -4 26 4.25 1.64 0 -4 26 4.65 1.65 -1 4 26 15.35 2.11 1 -4 26 18.58 2.98 1 -4 26 16.37 2.26 -1 -4 26 15.25 2.19 -1 -4 26 19.50 2.65 1 4 26 18.74 2.73 2 -4 26 6.90 2.06 2 -4 26 7.34 1.95 -2 -4 26 6.89 1.66 2 4 26 8.95 2.25 2 4 26 8.80 2.66 3 -4 26 5.02 2.07 3 -4 26 0.91 1.79 3 4 26 2.60 2.71 3 4 26 3.28 2.25 4 -4 26 1.26 2.14 4 -4 26 1.27 2.17 4 4 26 3.42 2.90 4 4 26 1.99 2.58 0 -5 26 0.71 1.74 0 5 26 2.96 2.06 0 -5 26 1.75 2.16 1 -5 26 3.63 1.81 1 -5 26 1.59 1.62 -1 -5 26 2.49 1.75 1 5 26 10.97 2.37 1 5 26 5.26 2.29 -1 -5 26 3.64 2.13 2 -5 26 4.50 1.90 2 -5 26 3.15 1.85 2 5 26 5.86 2.50 2 5 26 6.64 2.29 -2 -5 26 5.34 1.79 3 -5 26 7.33 2.14 3 -5 26 10.23 2.87 3 5 26 9.44 2.58 3 5 26 9.37 3.05 0 -6 26 2.24 1.88 0 -6 26 -2.28 2.04 1 -6 26 2.14 1.73 1 -6 26 -2.65 1.45 -1 -6 26 1.80 1.80 1 6 26 1.57 1.83 -1 -6 26 -0.30 1.93 2 -6 26 0.42 1.77 2 -6 26 3.30 1.93 -2 -6 26 4.20 1.89 2 6 26 5.11 2.38 2 6 26 2.31 2.28 3 -6 26 15.20 2.76 3 -6 26 12.13 2.37 3 6 26 8.69 3.16 3 6 26 17.40 2.99 0 -7 26 3.77 1.74 0 -7 26 1.06 1.89 1 -7 26 1.89 1.96 1 -7 26 2.09 2.33 -1 -7 26 -2.40 1.97 -1 -7 26 -1.46 1.91 2 -7 26 4.13 2.74 2 -7 26 2.91 2.02 -2 -7 26 2.60 2.05 2 7 26 0.43 2.59 0 -8 26 -1.79 2.19 0 -8 26 -1.83 1.93 1 -8 26 3.74 2.54 1 -8 26 1.09 2.07 -1 -8 26 -2.08 1.45 -1 -8 26 3.68 2.07 0 0 27 1.28 1.49 0 0 27 -0.41 2.06 -1 0 27 2.22 2.00 1 0 27 -1.58 1.53 1 0 27 -2.30 1.55 2 0 27 8.43 2.13 2 0 27 9.30 2.88 -2 0 27 8.13 1.71 3 0 27 2.31 1.95 -3 0 27 3.73 1.88 3 0 27 2.88 2.05 4 0 27 2.16 2.28 4 0 27 0.33 2.16 0 -1 27 31.33 3.77 0 1 27 45.59 3.95 0 1 27 43.26 3.27 0 -1 27 44.60 4.05 -1 1 27 37.02 3.65 1 -1 27 37.15 3.50 1 -1 27 47.44 3.71 1 1 27 45.91 3.57 -1 -1 27 38.57 3.74 1 1 27 44.53 4.15 2 -1 27 30.64 3.99 2 -1 27 31.89 3.52 -2 1 27 29.68 3.07 -2 -1 27 25.29 2.69 2 1 27 29.94 3.32 2 1 27 33.20 3.72 3 -1 27 3.40 2.80 3 -1 27 0.52 2.01 -3 1 27 3.92 2.10 -3 -1 27 4.37 2.00 3 1 27 2.76 2.11 3 1 27 3.21 2.06 4 -1 27 8.52 3.35 4 1 27 5.52 2.44 0 -2 27 8.54 2.36 0 2 27 5.35 1.43 0 -2 27 6.34 1.83 0 2 27 3.76 2.15 -1 2 27 25.09 3.12 1 -2 27 19.70 2.79 1 -2 27 29.44 3.33 1 2 27 22.04 3.25 1 2 27 28.35 3.23 -1 -2 27 22.96 3.15 -1 -2 27 28.53 2.77 2 -2 27 5.20 2.56 -2 2 27 2.01 1.71 2 -2 27 5.57 1.79 -2 -2 27 1.69 1.42 2 2 27 1.96 1.97 2 2 27 1.61 2.48 -3 2 27 1.60 1.83 3 -2 27 -1.36 1.77 3 -2 27 3.65 2.04 3 2 27 -2.03 1.92 3 2 27 3.01 2.13 0 -3 27 12.07 2.02 0 3 27 9.57 2.36 0 -3 27 11.07 2.57 1 -3 27 0.32 1.72 1 -3 27 2.43 1.78 -1 3 27 1.80 1.72 -1 -3 27 1.22 1.65 -1 -3 27 3.97 2.09 1 3 27 -1.17 2.27 1 3 27 -0.84 1.80 2 -3 27 7.73 2.13 2 -3 27 5.34 1.94 -2 3 27 5.02 2.08 -2 -3 27 5.31 2.13 2 3 27 5.66 2.15 2 3 27 2.96 2.00 3 -3 27 1.43 2.76 3 -3 27 2.58 1.97 3 3 27 5.49 2.34 3 3 27 -1.76 2.79 0 4 27 6.60 2.14 0 -4 27 5.44 1.90 0 -4 27 4.45 2.25 -1 4 27 0.34 1.82 1 -4 27 2.34 1.91 1 -4 27 1.95 1.71 1 4 27 1.56 2.29 1 4 27 0.86 1.84 -1 -4 27 1.45 1.73 -1 -4 27 1.02 1.50 2 -4 27 1.89 2.40 2 -4 27 1.93 1.83 2 4 27 3.80 2.73 -2 -4 27 2.46 1.51 2 4 27 4.62 2.27 3 -4 27 -4.59 1.90 3 -4 27 4.21 2.86 3 4 27 0.82 2.86 3 4 27 -1.03 2.34 0 -5 27 -0.11 1.94 0 -5 27 2.01 1.63 1 -5 27 -1.71 1.72 1 -5 27 1.45 2.27 -1 -5 27 3.45 2.09 1 5 27 3.00 2.50 1 5 27 -0.38 1.91 -1 -5 27 -1.56 1.77 2 -5 27 3.04 1.91 2 -5 27 -0.53 1.74 2 5 27 1.50 2.55 2 5 27 5.86 2.42 0 -6 27 8.81 2.34 0 -6 27 6.87 2.17 1 -6 27 9.75 2.70 1 -6 27 13.14 2.32 -1 -6 27 7.11 1.89 -1 -6 27 12.19 2.18 2 -6 27 1.14 2.13 2 -6 27 4.04 1.95 2 6 27 -3.74 2.29 2 6 27 0.59 2.41 0 -7 27 -0.05 1.95 0 -7 27 -1.75 1.61 1 -7 27 4.34 2.20 1 -7 27 10.14 2.21 -1 -7 27 6.19 2.19 -1 -7 27 6.40 2.42 0 0 28 128.55 6.63 0 0 28 130.18 7.47 1 0 28 10.66 2.08 -1 0 28 8.43 2.40 1 0 28 9.48 2.68 -2 0 28 10.78 2.42 2 0 28 14.24 3.05 2 0 28 13.33 2.31 3 0 28 -1.12 1.98 3 0 28 5.19 3.00 -3 0 28 3.34 1.92 0 -1 28 7.68 1.89 0 1 28 4.31 1.83 0 -1 28 11.90 2.66 1 -1 28 31.66 3.50 -1 1 28 30.37 3.50 1 -1 28 33.16 3.93 1 1 28 22.06 3.42 -1 -1 28 26.16 3.48 1 1 28 25.60 3.26 -2 1 28 17.89 2.54 2 -1 28 13.93 2.34 2 -1 28 14.62 3.20 2 1 28 16.76 2.50 2 1 28 5.78 2.91 -2 -1 28 13.46 2.54 -3 1 28 0.37 1.71 3 -1 28 0.44 2.76 3 -1 28 1.97 2.08 -3 -1 28 0.14 2.06 3 1 28 1.63 2.14 3 1 28 -1.78 2.84 0 -2 28 45.00 3.93 0 -2 28 62.21 4.17 0 2 28 51.83 4.42 1 -2 28 15.86 2.55 1 -2 28 16.26 2.45 -1 2 28 15.95 2.68 1 2 28 16.77 2.35 -1 -2 28 16.27 2.66 1 2 28 19.40 3.18 2 -2 28 14.54 2.29 -2 2 28 15.48 2.36 -2 -2 28 13.18 2.58 2 2 28 13.22 2.54 2 2 28 16.32 3.37 3 -2 28 1.50 2.99 3 2 28 1.89 2.20 -3 -2 28 4.15 2.16 0 3 28 -2.29 2.09 0 -3 28 1.12 1.75 0 -3 28 -1.29 2.14 -1 3 28 10.81 2.20 1 -3 28 12.29 2.21 1 -3 28 8.77 2.82 1 3 28 7.67 2.82 1 3 28 8.86 1.95 -1 -3 28 9.12 1.97 2 -3 28 -0.95 1.87 2 -3 28 0.17 2.03 -2 -3 28 4.29 2.20 2 3 28 1.16 2.18 2 3 28 6.25 2.93 0 4 28 22.17 3.17 0 -4 28 24.14 2.72 0 -4 28 26.57 3.34 1 -4 28 21.84 3.25 1 -4 28 16.39 2.44 1 4 28 13.88 2.95 -1 -4 28 15.65 2.26 -1 -4 28 13.36 2.31 2 -4 28 5.06 2.05 2 -4 28 8.47 2.92 2 4 28 4.47 2.33 2 4 28 12.90 3.05 -2 -4 28 4.10 2.23 0 -5 28 1.01 2.04 0 -5 28 4.34 1.73 1 -5 28 5.88 1.98 1 -5 28 4.65 2.02 -1 -5 28 5.07 1.96 -1 -5 28 1.32 1.55 0 0 29 2.28 1.84 1 0 29 52.51 4.32 -1 0 29 50.87 4.41 1 0 29 50.71 4.79 -2 0 29 6.56 2.26 2 0 29 2.08 2.14 0 1 29 19.68 3.06 0 -1 29 15.26 2.56 -1 1 29 16.22 2.76 1 -1 29 10.54 2.93 1 -1 29 16.53 2.51 -1 -1 29 20.87 2.70 1 1 29 15.70 2.28 1 1 29 16.28 2.63 0 2 29 0.86 2.28 0 -2 29 2.62 1.80 0 -2 29 -0.21 1.68 -1 2 29 -1.49 2.09 1 -2 29 2.53 1.98 1 -2 29 0.81 2.46 -1 -2 29 3.86 2.40 1 2 29 5.83 2.73 1 2 29 5.37 2.48 0 -3 29 23.11 2.71 0 3 29 27.12 3.62 0 -3 29 23.48 3.35 1 -3 29 2.20 2.17 1 -3 29 4.58 2.02 1 3 29 2.02 2.69 -1 -3 29 2.02 2.23 0 0 0 0.00 0.00 _exptl_absorpt_process_details 'SADABS 2014/5' _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.6458 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 0.71073 6.893 12.646 20.722 89.977 90.031 89.943 ) _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 60354 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp C1 C 0.5026(2) 0.75848(12) 0.64619(8) 0.0302(3) Uani 1 1 d . . C2 C 0.3329(2) 0.74980(13) 0.68064(8) 0.0310(3) Uani 1 1 d . . C3 C 0.2430(3) 0.83463(13) 0.71222(8) 0.0345(3) Uani 1 1 d . . C4 C 0.3433(3) 0.93284(14) 0.70625(9) 0.0376(4) Uani 1 1 d . . C5 C 0.5169(3) 0.94505(13) 0.67233(9) 0.0382(4) Uani 1 1 d . . C6 C 0.5963(3) 0.85660(13) 0.64208(8) 0.0331(3) Uani 1 1 d . . C7 C 0.0621(3) 0.82866(15) 0.74894(9) 0.0402(4) Uani 1 1 d . . C8 C -0.0460(3) 0.72770(16) 0.75667(11) 0.0486(5) Uani 1 1 d . . H8A H -0.069939 0.697239 0.714947 0.073 Uiso 1 1 calc R U H8B H -0.167318 0.741225 0.777875 0.073 Uiso 1 1 calc R U H8C H 0.029375 0.679395 0.782174 0.073 Uiso 1 1 calc R U C9 C 0.6151(4) 1.05068(17) 0.66936(12) 0.0555(6) Uani 1 1 d . . H9A H 0.665635 1.061900 0.626701 0.083 Uiso 1 1 calc R U H9B H 0.719497 1.052513 0.700030 0.083 Uiso 1 1 calc R U H9C H 0.523278 1.105334 0.679447 0.083 Uiso 1 1 calc R U C10 C 0.5260(2) 0.65738(11) 0.60806(7) 0.0274(3) Uani 1 1 d . . C11 C 0.3922(2) 0.58730(12) 0.64530(8) 0.0299(3) Uani 1 1 d . . C12 C 0.4435(3) 0.67542(15) 0.53912(8) 0.0383(4) Uani 1 1 d . . H12A H 0.522488 0.726125 0.516759 0.057 Uiso 1 1 calc R U H12B H 0.313080 0.701567 0.542148 0.057 Uiso 1 1 calc R U H12C H 0.443906 0.609700 0.515843 0.057 Uiso 1 1 calc R U C13 C 0.7231(2) 0.60775(12) 0.59730(7) 0.0291(3) Uani 1 1 d . . C14 C 0.7293(2) 0.49415(12) 0.59193(8) 0.0301(3) Uani 1 1 d . . C15 C 0.5718(3) 0.43058(13) 0.61886(8) 0.0357(3) Uani 1 1 d . . C16 C 0.4031(3) 0.48277(14) 0.64838(9) 0.0364(4) Uani 1 1 d . . H16 H 0.306656 0.443460 0.668658 0.044 Uiso 1 1 calc R U C17 C 0.8897(3) 0.44372(14) 0.56139(8) 0.0331(3) Uani 1 1 d . . C18 C 1.0286(3) 0.50125(16) 0.51871(11) 0.0494(5) Uani 1 1 d . . H18A H 1.049699 0.460983 0.480021 0.074 Uiso 1 1 calc R U H18B H 1.149606 0.510535 0.540937 0.074 Uiso 1 1 calc R U H18C H 0.975931 0.569228 0.507702 0.074 Uiso 1 1 calc R U C19 C 1.0663(3) 0.27946(16) 0.53611(13) 0.0537(6) Uani 1 1 d . . H19A H 1.053439 0.283473 0.489524 0.064 Uiso 1 1 calc R U H19B H 1.191192 0.309006 0.547896 0.064 Uiso 1 1 calc R U C20 C 1.0565(4) 0.16911(18) 0.55662(12) 0.0534(5) Uani 1 1 d . . C21 C 1.0472(6) 0.0809(2) 0.57321(15) 0.0772(9) Uani 1 1 d . . H21 H 1.039842 0.010627 0.586416 0.093 Uiso 1 1 calc R U N1 N 0.9115(2) 0.34082(12) 0.56663(8) 0.0399(3) Uani 1 1 d . . H1N H 0.819(5) 0.312(2) 0.5910(14) 0.058(8) Uiso 1 1 d . . O1 O -0.0042(3) 0.90903(13) 0.77514(10) 0.0619(5) Uani 1 1 d . . O2 O 0.2720(3) 1.02045(12) 0.73442(9) 0.0520(4) Uani 1 1 d . . H2O H 0.181(6) 1.000(3) 0.7521(16) 0.071(10) Uiso 1 1 d . . O3 O 0.7642(2) 0.86756(11) 0.60936(7) 0.0436(3) Uani 1 1 d . . H3O H 0.804(6) 0.814(3) 0.6039(18) 0.081(11) Uiso 1 1 d . . O4 O 0.25831(18) 0.64748(9) 0.67849(6) 0.0347(3) Uani 1 1 d . . O5 O 0.86334(19) 0.66812(10) 0.58919(7) 0.0413(3) Uani 1 1 d . . O6 O 0.5774(2) 0.33209(11) 0.62014(9) 0.0546(4) Uani 1 1 d . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0329(7) 0.0262(6) 0.0314(7) -0.0010(5) 0.0019(6) -0.0014(6) C2 0.0321(7) 0.0280(7) 0.0330(7) 0.0010(6) -0.0001(6) 0.0007(6) C3 0.0351(8) 0.0324(7) 0.0360(8) -0.0012(6) 0.0019(7) 0.0043(6) C4 0.0426(9) 0.0313(8) 0.0390(8) -0.0038(6) -0.0005(7) 0.0041(7) C5 0.0468(9) 0.0282(7) 0.0396(8) -0.0056(6) 0.0004(8) -0.0033(7) C6 0.0374(8) 0.0290(7) 0.0328(7) -0.0017(6) 0.0025(6) -0.0040(6) C7 0.0370(8) 0.0432(9) 0.0404(8) -0.0014(7) 0.0056(7) 0.0084(7) C8 0.0453(10) 0.0459(10) 0.0546(11) 0.0034(8) 0.0165(9) 0.0023(8) C9 0.0702(14) 0.0335(9) 0.0630(12) -0.0138(9) 0.0131(11) -0.0164(9) C10 0.0300(7) 0.0244(6) 0.0279(6) 0.0003(5) 0.0021(6) -0.0036(5) C11 0.0283(7) 0.0295(7) 0.0319(7) 0.0002(6) 0.0048(6) -0.0023(5) C12 0.0439(9) 0.0389(8) 0.0321(7) 0.0044(6) -0.0049(7) -0.0057(7) C13 0.0322(7) 0.0289(7) 0.0262(6) -0.0009(5) 0.0025(6) -0.0029(6) C14 0.0321(7) 0.0270(7) 0.0311(7) -0.0010(5) 0.0059(6) -0.0030(5) C15 0.0410(9) 0.0276(7) 0.0383(8) -0.0003(6) 0.0100(7) -0.0040(6) C16 0.0357(8) 0.0303(7) 0.0431(8) 0.0020(6) 0.0134(7) -0.0041(6) C17 0.0336(7) 0.0324(7) 0.0333(7) -0.0054(6) 0.0030(6) -0.0031(6) C18 0.0427(10) 0.0428(10) 0.0626(12) -0.0023(9) 0.0219(10) -0.0058(8) C19 0.0485(11) 0.0374(10) 0.0751(15) -0.0101(9) 0.0230(11) 0.0029(8) C20 0.0564(12) 0.0415(10) 0.0623(12) -0.0116(9) 0.0152(10) 0.0066(9) C21 0.106(2) 0.0461(13) 0.0798(17) -0.0041(12) 0.0296(18) 0.0129(14) N1 0.0392(8) 0.0337(7) 0.0468(8) -0.0057(6) 0.0112(7) 0.0014(6) O1 0.0528(9) 0.0514(8) 0.0815(11) -0.0187(8) 0.0222(9) 0.0070(7) O2 0.0565(9) 0.0348(7) 0.0647(9) -0.0129(6) 0.0108(8) 0.0057(7) O3 0.0470(7) 0.0315(6) 0.0524(8) -0.0046(5) 0.0157(6) -0.0099(5) O4 0.0330(6) 0.0290(5) 0.0421(6) 0.0002(4) 0.0100(5) -0.0010(4) O5 0.0354(6) 0.0336(6) 0.0550(7) -0.0060(6) 0.0082(6) -0.0086(5) O6 0.0609(9) 0.0261(6) 0.0768(10) 0.0007(6) 0.0312(8) -0.0019(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C2 C1 C6 119.64(15) C2 C1 C10 107.14(13) C6 C1 C10 131.90(15) C1 C2 O4 111.84(14) C1 C2 C3 123.94(15) O4 C2 C3 124.18(14) C2 C3 C4 114.23(15) C2 C3 C7 125.52(16) C4 C3 C7 120.25(15) O2 C4 C5 116.15(17) O2 C4 C3 120.09(17) C5 C4 C3 123.76(15) C6 C5 C4 118.32(16) C6 C5 C9 121.22(18) C4 C5 C9 120.45(17) O3 C6 C5 118.74(15) O3 C6 C1 121.15(15) C5 C6 C1 120.10(16) O1 C7 C3 119.99(19) O1 C7 C8 118.15(17) C3 C7 C8 121.86(16) C7 C8 H8A 109.5 C7 C8 H8B 109.5 H8A C8 H8B 109.5 C7 C8 H8C 109.5 H8A C8 H8C 109.5 H8B C8 H8C 109.5 C5 C9 H9A 109.5 C5 C9 H9B 109.5 H9A C9 H9B 109.5 C5 C9 H9C 109.5 H9A C9 H9C 109.5 H9B C9 H9C 109.5 C11 C10 C1 99.53(12) C11 C10 C13 112.65(13) C1 C10 C13 121.53(13) C11 C10 C12 109.60(13) C1 C10 C12 108.50(13) C13 C10 C12 104.74(13) C16 C11 O4 124.30(14) C16 C11 C10 125.55(15) O4 C11 C10 110.12(13) C10 C12 H12A 109.5 C10 C12 H12B 109.5 H12A C12 H12B 109.5 C10 C12 H12C 109.5 H12A C12 H12C 109.5 H12B C12 H12C 109.5 O5 C13 C14 125.34(15) O5 C13 C10 117.67(14) C14 C13 C10 116.78(13) C17 C14 C13 120.19(14) C17 C14 C15 120.03(14) C13 C14 C15 119.77(14) O6 C15 C14 122.30(16) O6 C15 C16 117.63(15) C14 C15 C16 120.01(15) C11 C16 C15 118.16(15) C11 C16 H16 120.9 C15 C16 H16 120.9 N1 C17 C14 119.67(15) N1 C17 C18 117.24(16) C14 C17 C18 122.92(16) C17 C18 H18A 109.5 C17 C18 H18B 109.5 H18A C18 H18B 109.5 C17 C18 H18C 109.5 H18A C18 H18C 109.5 H18B C18 H18C 109.5 C20 C19 N1 110.31(18) C20 C19 H19A 109.6 N1 C19 H19A 109.6 C20 C19 H19B 109.6 N1 C19 H19B 109.6 H19A C19 H19B 108.1 C21 C20 C19 179.5(3) C20 C21 H21 180.0 C17 N1 C19 124.92(17) C17 N1 H1N 111.6(19) C19 N1 H1N 123.5(19) C4 O2 H2O 103(2) C6 O3 H3O 107(3) C11 O4 C2 106.28(12) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance C1 C2 1.375(2) C1 C6 1.400(2) C1 C10 1.510(2) C2 O4 1.3921(19) C2 C3 1.400(2) C3 C4 1.426(3) C3 C7 1.463(2) C4 O2 1.344(2) C4 C5 1.396(3) C5 C6 1.393(2) C5 C9 1.498(3) C6 O3 1.349(2) C7 O1 1.238(2) C7 C8 1.486(3) C8 H8A 0.9600 C8 H8B 0.9600 C8 H8C 0.9600 C9 H9A 0.9600 C9 H9B 0.9600 C9 H9C 0.9600 C10 C11 1.493(2) C10 C13 1.514(2) C10 C12 1.553(2) C11 C16 1.324(2) C11 O4 1.379(2) C12 H12A 0.9600 C12 H12B 0.9600 C12 H12C 0.9600 C13 O5 1.243(2) C13 C14 1.440(2) C14 C17 1.424(2) C14 C15 1.461(2) C15 O6 1.245(2) C15 C16 1.471(2) C16 H16 0.9300 C17 N1 1.313(2) C17 C18 1.492(3) C18 H18A 0.9600 C18 H18B 0.9600 C18 H18C 0.9600 C19 C20 1.459(3) C19 N1 1.463(2) C19 H19A 0.9700 C19 H19B 0.9700 C20 C21 1.168(4) C21 H21 0.9300 N1 H1N 0.89(3) O2 H2O 0.77(4) O3 H3O 0.74(4) loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H1N O6 0.89(3) 1.79(3) 2.558(2) 143(3) yes O2 H2O O1 0.77(4) 1.78(4) 2.514(3) 158(3) yes O3 H3O O5 0.74(4) 1.91(4) 2.6440(19) 171(4) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C6 C1 C2 O4 178.82(15) C10 C1 C2 O4 10.45(18) C6 C1 C2 C3 0.8(3) C10 C1 C2 C3 -167.55(15) C1 C2 C3 C4 -0.4(3) O4 C2 C3 C4 -178.17(15) C1 C2 C3 C7 179.59(17) O4 C2 C3 C7 1.8(3) C2 C3 C4 O2 -179.96(16) C7 C3 C4 O2 0.0(3) C2 C3 C4 C5 -0.3(3) C7 C3 C4 C5 179.73(17) O2 C4 C5 C6 -179.78(18) C3 C4 C5 C6 0.5(3) O2 C4 C5 C9 0.8(3) C3 C4 C5 C9 -178.9(2) C4 C5 C6 O3 -179.79(17) C9 C5 C6 O3 -0.4(3) C4 C5 C6 C1 -0.1(3) C9 C5 C6 C1 179.29(19) C2 C1 C6 O3 179.15(16) C10 C1 C6 O3 -15.9(3) C2 C1 C6 C5 -0.5(3) C10 C1 C6 C5 164.47(17) C2 C3 C7 O1 179.8(2) C4 C3 C7 O1 -0.2(3) C2 C3 C7 C8 0.4(3) C4 C3 C7 C8 -179.55(18) C2 C1 C10 C11 -19.23(16) C6 C1 C10 C11 174.39(18) C2 C1 C10 C13 -143.38(14) C6 C1 C10 C13 50.2(3) C2 C1 C10 C12 95.28(16) C6 C1 C10 C12 -71.1(2) C1 C10 C11 C16 -155.12(18) C13 C10 C11 C16 -25.0(2) C12 C10 C11 C16 91.2(2) C1 C10 C11 O4 22.59(16) C13 C10 C11 O4 152.74(13) C12 C10 C11 O4 -91.07(16) C11 C10 C13 O5 -154.13(15) C1 C10 C13 O5 -36.3(2) C12 C10 C13 O5 86.81(17) C11 C10 C13 C14 31.0(2) C1 C10 C13 C14 148.79(14) C12 C10 C13 C14 -88.09(16) O5 C13 C14 C17 -15.2(3) C10 C13 C14 C17 159.22(14) O5 C13 C14 C15 163.74(17) C10 C13 C14 C15 -21.8(2) C17 C14 C15 O6 4.9(3) C13 C14 C15 O6 -174.10(19) C17 C14 C15 C16 -177.89(16) C13 C14 C15 C16 3.1(3) O4 C11 C16 C15 -170.31(16) C10 C11 C16 C15 7.1(3) O6 C15 C16 C11 -177.7(2) C14 C15 C16 C11 5.0(3) C13 C14 C17 N1 168.01(17) C15 C14 C17 N1 -11.0(2) C13 C14 C17 C18 -17.0(3) C15 C14 C17 C18 164.05(18) C14 C17 N1 C19 178.13(19) C18 C17 N1 C19 2.8(3) C20 C19 N1 C17 175.1(2) C16 C11 O4 C2 160.10(17) C10 C11 O4 C2 -17.65(17) C1 C2 O4 C11 4.24(18) C3 C2 O4 C11 -177.76(15)