#------------------------------------------------------------------------------ #$Date: 2020-01-30 02:06:39 +0200 (Thu, 30 Jan 2020) $ #$Revision: 247352 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/71/1557184.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557184 loop_ _publ_author_name 'Yang, Yaxi' 'Zhang, Rukang' 'Li, Zhaojun' 'Mei, Lianghe' 'Wan, Shili' 'Ding, Hong' 'Chen, Zhifeng' 'Xing, Jing' 'Feng, Huijin' 'Han, Jie' 'Jiang, Hualiang' 'Zheng, Mingyue' 'Luo, Cheng' 'Zhou, Bing' _publ_section_title ; Discovery of Highly Potent, Selective, and Orally Efficacious p300/CBP Histone Acetyltransferases Inhibitors. ; _journal_name_full 'Journal of medicinal chemistry' _journal_paper_doi 10.1021/acs.jmedchem.9b01721 _journal_year 2020 _chemical_absolute_configuration rmad _chemical_formula_moiety 'C13 H13 N3 O4, H2 O' _chemical_formula_sum 'C13 H15 N3 O5' _chemical_formula_weight 293.28 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2019-05-23 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.4194(2) _cell_length_b 8.5433(2) _cell_length_c 19.1641(5) _cell_measurement_reflns_used 9955 _cell_measurement_temperature 100 _cell_measurement_theta_max 72.293 _cell_measurement_theta_min 2.305 _cell_volume 1378.46(6) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 100.0 _diffrn_measured_fraction_theta_full 0.979 _diffrn_measured_fraction_theta_max 0.981 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0342 _diffrn_reflns_av_unetI/netI 0.0288 _diffrn_reflns_Laue_measured_fraction_full 0.979 _diffrn_reflns_Laue_measured_fraction_max 0.981 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 11510 _diffrn_reflns_point_group_measured_fraction_full 0.983 _diffrn_reflns_point_group_measured_fraction_max 0.984 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 72.286 _diffrn_reflns_theta_min 4.615 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.934 _exptl_absorpt_correction_T_max 0.7536 _exptl_absorpt_correction_T_min 0.5694 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1079 before and 0.0551 after correction. The Ratio of minimum to maximum transmission is 0.7556. The \l/2 correction factor is Not present.' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.413 _exptl_crystal_description block _exptl_crystal_F_000 616 _exptl_crystal_size_max 0.28 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.215 _refine_diff_density_min -0.121 _refine_diff_density_rms 0.030 _refine_ls_abs_structure_details ; Flack x determined using 1102 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.03(5) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.073 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 203 _refine_ls_number_reflns 2683 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.073 _refine_ls_R_factor_all 0.0256 _refine_ls_R_factor_gt 0.0255 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0217P)^2^+0.3067P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0625 _refine_ls_wR_factor_ref 0.0626 _reflns_Friedel_coverage 0.720 _reflns_Friedel_fraction_full 0.988 _reflns_Friedel_fraction_max 0.988 _reflns_number_gt 2665 _reflns_number_total 2683 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL 22019583_0m_a.res in P2(1)2(1)2(1) 22019583_0m.res created by SHELXL-2018/3 at 17:40:16 on 23-May-2019 REM Old TITL 22019583_0m in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.075, Rweak 0.025, Alpha 0.004, Orientation as input REM Flack x = 0.041 ( 0.047 ) from Parsons' quotients REM Formula found by SHELXT: C13 N3 O5 CELL 1.54178 8.4194 8.5433 19.1641 90 90 90 ZERR 4 0.0002 0.0002 0.0005 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 52 60 12 20 EQIV $1 -0.5+X,1.5-Y,1-Z EQIV $2 1-X,-0.5+Y,1.5-Z EQIV $3 0.5-X,1-Y,0.5+Z EQIV $4 0.5+X,1.5-Y,1-Z L.S. 4 PLAN 20 SIZE 0.28 0.15 0.12 TEMP -173.15 HTAB O5 O4_$1 HTAB O5 O2_$2 HTAB N3 O5_$3 HTAB N2 O4_$4 BOND $H list 4 fmap 2 ACTA REM REM REM WGHT 0.021700 0.306700 FVAR 1.62809 O4 4 0.768230 0.872950 0.516231 11.00000 0.01731 0.02117 = 0.02096 0.00026 0.00085 0.00099 O1 4 0.453915 0.460448 0.792226 11.00000 0.02015 0.02301 = 0.02793 0.00335 -0.00138 -0.00289 O3 4 0.850439 0.464310 0.849075 11.00000 0.02252 0.02132 = 0.01766 -0.00197 -0.00480 0.00122 O5 4 0.140005 0.341324 0.457872 11.00000 0.03585 0.01936 = 0.03322 0.00449 -0.01351 -0.00195 O2 4 0.833922 0.584040 0.952601 11.00000 0.04398 0.03122 = 0.02292 -0.00738 -0.01005 0.00380 N3 3 0.612049 0.545126 0.883325 11.00000 0.02659 0.02010 = 0.01907 -0.00076 0.00348 0.00176 AFIX 43 H3 2 0.539404 0.590246 0.909505 11.00000 -1.20000 AFIX 0 N2 3 0.958987 0.689364 0.538085 11.00000 0.01833 0.02402 = 0.02041 -0.00051 0.00337 0.00361 AFIX 43 H2 2 1.045805 0.644690 0.522050 11.00000 -1.20000 AFIX 0 N1 3 0.977343 0.848370 0.442072 11.00000 0.02092 0.02513 = 0.02223 0.00106 0.00328 -0.00155 C10 1 0.896113 0.631180 0.601347 11.00000 0.01432 0.02335 = 0.01774 -0.00038 -0.00159 0.00015 C12 1 0.896633 0.808463 0.499960 11.00000 0.01721 0.01865 = 0.01739 -0.00377 -0.00096 -0.00431 C8 1 0.772843 0.671647 0.713616 11.00000 0.01764 0.01839 = 0.01907 -0.00337 -0.00058 0.00099 AFIX 43 H8 2 0.725246 0.738466 0.747273 11.00000 -1.20000 AFIX 0 C1 1 0.581231 0.475044 0.820616 11.00000 0.02247 0.01382 = 0.01830 0.00412 0.00139 -0.00148 C7 1 0.788079 0.512076 0.726608 11.00000 0.01590 0.01904 = 0.01613 -0.00058 -0.00195 -0.00049 C2 1 0.770081 0.536516 0.900454 11.00000 0.03115 0.01685 = 0.01836 0.00104 -0.00365 0.00041 C9 1 0.827919 0.731870 0.651015 11.00000 0.01821 0.01686 = 0.02088 -0.00091 -0.00095 -0.00002 AFIX 43 H9 2 0.819631 0.840778 0.641692 11.00000 -1.20000 AFIX 0 C11 1 0.908324 0.470636 0.614409 11.00000 0.01855 0.02213 = 0.01890 -0.00543 -0.00103 0.00388 AFIX 43 H11 2 0.953540 0.402771 0.580535 11.00000 -1.20000 AFIX 0 C3 1 0.741739 0.424383 0.791678 11.00000 0.01904 0.01646 = 0.01776 0.00009 -0.00367 -0.00020 C6 1 0.853535 0.411486 0.677534 11.00000 0.01648 0.01793 = 0.02066 -0.00242 -0.00501 0.00225 C4 1 0.754780 0.250895 0.771169 11.00000 0.02617 0.01536 = 0.02265 -0.00153 -0.00232 0.00007 AFIX 23 H4A 2 0.647793 0.205420 0.764209 11.00000 -1.20000 H4B 2 0.809665 0.191039 0.808253 11.00000 -1.20000 AFIX 0 C5 1 0.850941 0.244374 0.702531 11.00000 0.02715 0.01883 = 0.02125 -0.00188 -0.00223 0.00445 AFIX 23 H5A 2 0.959991 0.205491 0.711070 11.00000 -1.20000 H5B 2 0.798498 0.175483 0.667967 11.00000 -1.20000 AFIX 0 C13 1 0.938633 0.990651 0.403992 11.00000 0.03093 0.02644 = 0.02256 0.00367 0.00118 -0.00672 AFIX 137 H13A 2 0.998705 0.993321 0.360208 11.00000 -1.50000 H13B 2 0.966499 1.082015 0.432387 11.00000 -1.50000 H13C 2 0.824618 0.992466 0.393730 11.00000 -1.50000 AFIX 0 H1 2 1.072657 0.808403 0.437211 11.00000 0.03657 H5C 2 0.157217 0.262489 0.485077 11.00000 0.04879 H5D 2 0.196596 0.418006 0.470500 11.00000 0.05064 HKLF 4 REM 22019583_0m_a.res in P2(1)2(1)2(1) REM wR2 = 0.0626, GooF = S = 1.073, Restrained GooF = 1.073 for all data REM R1 = 0.0255 for 2665 Fo > 4sig(Fo) and 0.0256 for all 2683 data REM 203 parameters refined using 0 restraints END WGHT 0.0217 0.3056 REM Highest difference peak 0.215, deepest hole -0.121, 1-sigma level 0.030 Q1 1 0.7566 0.4761 0.7600 11.00000 0.05 0.22 Q2 1 0.6609 0.4407 0.8037 11.00000 0.05 0.18 Q3 1 0.7482 0.3357 0.7836 11.00000 0.05 0.17 Q4 1 0.7861 0.4382 0.8194 11.00000 0.05 0.16 Q5 1 0.8039 0.2461 0.7394 11.00000 0.05 0.15 Q6 1 0.7393 0.5761 0.7134 11.00000 0.05 0.14 Q7 1 0.9178 0.6631 0.5675 11.00000 0.05 0.12 Q8 1 0.8003 0.4611 0.6987 11.00000 0.05 0.12 Q9 1 0.8047 0.5852 0.7271 11.00000 0.05 0.12 Q10 1 0.9519 0.7806 0.5398 11.00000 0.05 0.12 Q11 1 0.8994 0.6739 0.6348 11.00000 0.05 0.12 Q12 1 0.8577 0.3335 0.6865 11.00000 0.05 0.11 Q13 1 0.8420 0.6939 0.6876 11.00000 0.05 0.11 Q14 1 0.8512 0.6740 0.6263 11.00000 0.05 0.11 Q15 1 0.9178 0.4418 0.6522 11.00000 0.05 0.11 Q16 1 0.9301 0.5560 0.6180 11.00000 0.05 0.11 Q17 1 0.5925 0.4531 0.8638 11.00000 0.05 0.10 Q18 1 0.9137 0.7810 0.4528 11.00000 0.05 0.10 Q19 1 0.8284 1.0999 0.3137 11.00000 0.05 0.10 Q20 1 1.0575 1.0599 0.3897 11.00000 0.05 0.10 REM The information below was added by Olex2. REM REM R1 = 0.0255 for 2665 Fo > 4sig(Fo) and 0.0256 for all 11535 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.22, deepest hole -0.12 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0256 REM R1_gt = 0.0255 REM wR_ref = 0.0626 REM GOOF = 1.073 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 11535 REM Reflections_gt = 2665 REM Parameters = n/a REM Hole = -0.12 REM Peak = 0.22 REM Flack = 0.03(5) ; _cod_data_source_file jm9b01721_si_005.cif _cod_data_source_block 22019583_0m _cod_database_code 1557184 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.896 _shelx_estimated_absorpt_t_min 0.780 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C4(H4A,H4B), C5(H5A,H5B) 2.b Aromatic/amide H refined with riding coordinates: N3(H3), N2(H2), C8(H8), C9(H9), C11(H11) 2.c Idealised Me refined as rotating group: C13(H13A,H13B,H13C) ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn O4 O 0.76823(13) 0.87295(13) 0.51623(6) 0.0198(3) Uani 1 1 d . O1 O 0.45392(13) 0.46045(14) 0.79223(6) 0.0237(3) Uani 1 1 d . O3 O 0.85044(13) 0.46431(14) 0.84907(6) 0.0205(3) Uani 1 1 d . O5 O 0.14000(17) 0.34132(16) 0.45787(7) 0.0295(3) Uani 1 1 d . O2 O 0.83392(17) 0.58404(16) 0.95260(7) 0.0327(3) Uani 1 1 d . N3 N 0.61205(18) 0.54513(16) 0.88333(7) 0.0219(3) Uani 1 1 d . H3 H 0.539404 0.590246 0.909505 0.026 Uiso 1 1 calc R N2 N 0.95899(16) 0.68936(17) 0.53808(7) 0.0209(3) Uani 1 1 d . H2 H 1.045805 0.644690 0.522050 0.025 Uiso 1 1 calc R N1 N 0.97734(18) 0.84837(17) 0.44207(8) 0.0228(3) Uani 1 1 d . C10 C 0.89611(19) 0.63118(19) 0.60135(8) 0.0185(3) Uani 1 1 d . C12 C 0.89663(19) 0.80846(19) 0.49996(8) 0.0177(3) Uani 1 1 d . C8 C 0.77284(19) 0.67165(19) 0.71362(8) 0.0184(3) Uani 1 1 d . H8 H 0.725246 0.738466 0.747273 0.022 Uiso 1 1 calc R C1 C 0.58123(19) 0.47504(18) 0.82062(8) 0.0182(3) Uani 1 1 d . C7 C 0.78808(17) 0.51208(19) 0.72661(8) 0.0170(3) Uani 1 1 d . C2 C 0.7701(2) 0.53652(19) 0.90045(8) 0.0221(3) Uani 1 1 d . C9 C 0.82792(19) 0.73187(18) 0.65101(9) 0.0186(3) Uani 1 1 d . H9 H 0.819631 0.840778 0.641692 0.022 Uiso 1 1 calc R C11 C 0.90832(19) 0.47064(19) 0.61441(8) 0.0199(3) Uani 1 1 d . H11 H 0.953540 0.402771 0.580535 0.024 Uiso 1 1 calc R C3 C 0.74174(18) 0.42438(18) 0.79168(8) 0.0178(3) Uani 1 1 d . C6 C 0.85353(18) 0.41149(19) 0.67753(8) 0.0184(3) Uani 1 1 d . C4 C 0.7548(2) 0.25090(19) 0.77117(9) 0.0214(3) Uani 1 1 d . H4A H 0.647793 0.205420 0.764209 0.026 Uiso 1 1 calc R H4B H 0.809665 0.191039 0.808253 0.026 Uiso 1 1 calc R C5 C 0.8509(2) 0.24437(19) 0.70253(9) 0.0224(3) Uani 1 1 d . H5A H 0.959991 0.205491 0.711070 0.027 Uiso 1 1 calc R H5B H 0.798498 0.175483 0.667967 0.027 Uiso 1 1 calc R C13 C 0.9386(2) 0.9907(2) 0.40399(9) 0.0266(4) Uani 1 1 d . H13A H 0.998705 0.993321 0.360208 0.040 Uiso 1 1 calc GR H13B H 0.966499 1.082015 0.432387 0.040 Uiso 1 1 calc GR H13C H 0.824618 0.992466 0.393730 0.040 Uiso 1 1 calc GR H1 H 1.073(3) 0.808(3) 0.4372(12) 0.037(6) Uiso 1 1 d . H5C H 0.157(3) 0.262(4) 0.4851(15) 0.049(8) Uiso 1 1 d . H5D H 0.197(3) 0.418(4) 0.4705(15) 0.051(8) Uiso 1 1 d . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O4 0.0173(5) 0.0212(5) 0.0210(6) 0.0003(4) 0.0009(5) 0.0010(4) O1 0.0201(6) 0.0230(6) 0.0279(6) 0.0034(5) -0.0014(5) -0.0029(5) O3 0.0225(6) 0.0213(5) 0.0177(5) -0.0020(5) -0.0048(4) 0.0012(4) O5 0.0358(7) 0.0194(6) 0.0332(7) 0.0045(6) -0.0135(6) -0.0019(6) O2 0.0440(8) 0.0312(7) 0.0229(6) -0.0074(5) -0.0101(6) 0.0038(6) N3 0.0266(7) 0.0201(7) 0.0191(6) -0.0008(6) 0.0035(6) 0.0018(6) N2 0.0183(6) 0.0240(7) 0.0204(7) -0.0005(6) 0.0034(6) 0.0036(6) N1 0.0209(7) 0.0251(7) 0.0222(7) 0.0011(6) 0.0033(5) -0.0015(6) C10 0.0143(7) 0.0234(7) 0.0177(7) -0.0004(6) -0.0016(6) 0.0002(6) C12 0.0172(7) 0.0187(7) 0.0174(7) -0.0038(6) -0.0010(6) -0.0043(6) C8 0.0176(7) 0.0184(7) 0.0191(8) -0.0034(6) -0.0006(6) 0.0010(6) C1 0.0225(8) 0.0138(6) 0.0183(7) 0.0041(6) 0.0014(6) -0.0015(6) C7 0.0159(7) 0.0190(7) 0.0161(7) -0.0006(6) -0.0019(5) -0.0005(6) C2 0.0311(9) 0.0169(7) 0.0184(8) 0.0010(6) -0.0036(7) 0.0004(7) C9 0.0182(7) 0.0169(7) 0.0209(8) -0.0009(6) -0.0009(6) 0.0000(6) C11 0.0186(7) 0.0221(7) 0.0189(7) -0.0054(6) -0.0010(6) 0.0039(6) C3 0.0190(7) 0.0165(7) 0.0178(7) 0.0001(6) -0.0037(6) -0.0002(6) C6 0.0165(7) 0.0179(7) 0.0207(8) -0.0024(6) -0.0050(6) 0.0023(6) C4 0.0262(8) 0.0154(7) 0.0226(8) -0.0015(6) -0.0023(7) 0.0001(7) C5 0.0272(8) 0.0188(7) 0.0213(8) -0.0019(6) -0.0022(7) 0.0044(7) C13 0.0309(9) 0.0264(8) 0.0226(8) 0.0037(7) 0.0012(7) -0.0067(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C2 O3 C3 109.93(12) H5C O5 H5D 110(3) C1 N3 H3 124.1 C1 N3 C2 111.76(14) C2 N3 H3 124.1 C10 N2 H2 117.3 C12 N2 H2 117.3 C12 N2 C10 125.47(14) C12 N1 C13 120.82(15) C12 N1 H1 116.8(16) C13 N1 H1 118.5(17) C9 C10 N2 121.24(14) C11 C10 N2 118.11(15) C11 C10 C9 120.61(15) O4 C12 N2 121.95(14) O4 C12 N1 121.99(15) N1 C12 N2 116.00(15) C7 C8 H8 120.4 C9 C8 H8 120.4 C9 C8 C7 119.20(14) O1 C1 N3 127.52(15) O1 C1 C3 126.41(14) N3 C1 C3 106.02(13) C8 C7 C3 127.70(15) C6 C7 C8 121.46(15) C6 C7 C3 110.85(14) O3 C2 N3 109.71(13) O2 C2 O3 122.51(16) O2 C2 N3 127.78(16) C10 C9 H9 120.1 C8 C9 C10 119.73(14) C8 C9 H9 120.1 C10 C11 H11 120.4 C6 C11 C10 119.22(15) C6 C11 H11 120.4 O3 C3 C1 102.34(12) O3 C3 C7 110.04(12) O3 C3 C4 111.73(13) C1 C3 C4 115.49(13) C7 C3 C1 112.94(13) C7 C3 C4 104.44(13) C7 C6 C11 119.76(15) C7 C6 C5 111.45(14) C11 C6 C5 128.78(15) C3 C4 H4A 110.4 C3 C4 H4B 110.4 C3 C4 C5 106.84(13) H4A C4 H4B 108.6 C5 C4 H4A 110.4 C5 C4 H4B 110.4 C6 C5 C4 104.13(13) C6 C5 H5A 110.9 C6 C5 H5B 110.9 C4 C5 H5A 110.9 C4 C5 H5B 110.9 H5A C5 H5B 108.9 N1 C13 H13A 109.5 N1 C13 H13B 109.5 N1 C13 H13C 109.5 H13A C13 H13B 109.5 H13A C13 H13C 109.5 H13B C13 H13C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O4 C12 1.253(2) O1 C1 1.209(2) O3 C2 1.345(2) O3 C3 1.4710(18) O5 H5C 0.86(3) O5 H5D 0.85(3) O2 C2 1.205(2) N3 H3 0.8800 N3 C1 1.368(2) N3 C2 1.372(2) N2 H2 0.8800 N2 C10 1.413(2) N2 C12 1.358(2) N1 C12 1.345(2) N1 C13 1.455(2) N1 H1 0.88(3) C10 C9 1.406(2) C10 C11 1.398(2) C8 H8 0.9500 C8 C7 1.392(2) C8 C9 1.385(2) C1 C3 1.524(2) C7 C3 1.506(2) C7 C6 1.388(2) C9 H9 0.9500 C11 H11 0.9500 C11 C6 1.390(2) C3 C4 1.537(2) C6 C5 1.506(2) C4 H4A 0.9900 C4 H4B 0.9900 C4 C5 1.546(2) C5 H5A 0.9900 C5 H5B 0.9900 C13 H13A 0.9800 C13 H13B 0.9800 C13 H13C 0.9800 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag N3 H3 O5 0.88 1.87 2.7360(19) 169.4 2_565 yes N2 H2 O4 0.88 2.02 2.8541(18) 158.5 4_566 yes O5 H5C O2 0.86(3) 1.94(3) 2.797(2) 173(3) 3_646 yes O5 H5D O4 0.85(3) 1.90(3) 2.7149(18) 161(3) 4_466 yes loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 3 0 0 22 2.8 4 0 0 399.16 20.6 -4 0 0 380.56 21.2 5 0 0 7.2 2.9 -6 0 0 895.81 41.7 -6 0 0 915.81 41.7 -6 0 0 969.8 46.3 -7 0 0 -0.1 1.8 -7 0 0 1 1.6 -7 0 0 5.8 3 -8 0 0 536.55 31.2 -8 0 0 566.34 27.8 -8 0 0 607.64 33.3 -8 0 0 568.64 26.9 -9 0 0 1.7 1.4 -9 0 0 0.7 1.8 -10 0 0 835.32 37.3 -10 0 0 715.23 33.1 -3 -1 0 3 1.6 -3 1 0 2.4 0.5 4 1 0 88.29 7.6 -4 1 0 97.29 7.6 5 1 0 2339.87 101.49 -6 -1 0 648.24 30.8 -6 1 0 636.44 30.6 -6 -1 0 706.13 35.7 -6 1 0 675.43 35.2 -6 1 0 685.13 31.3 6 1 0 634.14 36.4 -6 -1 0 639.44 31.4 -7 1 0 1312.77 58.09 -7 -1 0 1303.27 58.59 -7 -1 0 1356.06 57.49 -7 1 0 1262.07 57.59 -7 1 0 1349.96 63.59 -7 -1 0 1346.97 63.59 -8 -1 0 114.49 11.4 -8 1 0 123.29 8.6 -8 1 0 108.99 11.5 -8 -1 0 118.89 8.8 -8 1 0 116.69 8.7 -8 -1 0 111.99 8.1 -8 -1 0 112.59 11.6 -9 1 0 74.19 7.5 -9 -1 0 74.79 6 -9 -1 0 65.89 8.1 -9 1 0 74.29 5 -9 -1 0 74.39 7.8 -9 1 0 77.09 6 -9 1 0 69.79 8.3 -10 -1 0 201.18 11.6 -10 -1 0 193.18 9.4 -10 1 0 195.08 11.3 1 2 0 895.61 39.7 -2 2 0 803.02 34.5 -2 -2 0 854.81 37.2 2 2 0 652.83 37.7 3 2 0 817.02 39.3 -3 2 0 861.91 37.2 4 2 0 434.16 24.2 -4 2 0 439.66 22.1 -5 -2 0 322.57 18.3 5 2 0 295.77 19.7 -6 -2 0 861.01 39.1 -6 2 0 889.71 43 -6 2 0 814.42 37.3 -6 -2 0 808.62 37.4 -6 -2 0 803.02 43 6 2 0 766.82 49.9 -6 -2 0 881.11 43.1 -7 -2 0 1079.09 54.69 -7 -2 0 1086.09 49.9 -7 -2 0 1094.19 54.29 -7 2 0 1114.19 49.2 -7 2 0 1066.39 48.3 -7 2 0 1126.69 54.49 -7 -2 0 1101.39 47.6 -8 2 0 195.08 11.6 -8 -2 0 190.18 9.3 -8 -2 0 196.08 17.5 -9 2 0 87.79 5.9 -9 2 0 82.39 8.9 -9 -2 0 88.29 9 -9 2 0 89.69 6.2 -9 -2 0 71.19 8.2 -9 2 0 88.29 7.7 -9 -2 0 90.59 6.6 -10 -2 0 6.9 2 -10 -2 0 7.5 1.3 0 3 0 5.8 2.1 2 3 0 601.64 30.5 3 3 0 34.4 5.2 -4 3 0 1668.53 72.29 -4 3 0 1679.13 68.79 4 3 0 1659.43 76.19 -5 -3 0 1206.88 52.79 5 3 0 1254.97 60.49 -5 3 0 1191.28 52.09 -5 3 0 1183.48 52.29 -5 -3 0 1280.37 59.09 -5 3 0 1291.97 57.99 -5 -3 0 1172.18 54.29 -6 -3 0 364.16 19.8 -6 -3 0 360.96 23.6 -6 3 0 362.46 22.8 -6 -3 0 346.37 22.5 -6 3 0 364.46 17.7 -6 -3 0 347.77 17.7 -6 3 0 329.07 17.7 -7 -3 0 1031.2 44.7 -7 3 0 1096.59 47.8 -7 -3 0 973.2 51.69 -7 3 0 1055.79 46.4 -7 -3 0 1058.09 48.5 -7 3 0 1068.59 52.59 -7 -3 0 1097.89 53.69 -8 -3 0 524.85 25.8 -8 3 0 531.55 25.4 -8 -3 0 525.45 30 -8 -3 0 449.16 28.1 -8 3 0 496.65 29.3 -8 3 0 557.34 24.7 -9 3 0 1.6 1.4 -9 3 0 -3.1 3.9 -9 -3 0 6.9 2.4 -9 -3 0 3.4 2.2 -9 3 0 0.2 1.6 0 4 0 3047.7 129.69 -1 4 0 14.6 3.5 2 4 0 27.6 5 3 4 0 168.48 14.2 -4 -4 0 217.48 15.9 4 4 0 224.48 18 -4 -4 0 226.98 16.4 -4 -4 0 230.38 13 -4 4 0 220.08 12 -5 4 0 107.79 10.8 -5 -4 0 98.89 7.2 -5 -4 0 105.09 10.9 -5 4 0 101.49 7.2 5 -4 0 98.19 9 -5 -4 0 102.09 8.5 -6 4 0 140.79 8.6 -6 4 0 109.69 8 -6 -4 0 118.09 7.8 -6 -4 0 123.39 9.8 -6 4 0 121.79 11.9 -6 -4 0 154.68 13.8 -7 4 0 80.59 9.6 -7 4 0 98.09 7.7 -7 -4 0 106.79 8.7 -7 -4 0 97.29 10.8 -8 4 0 567.94 32 -8 4 0 654.43 29.3 -8 -4 0 647.64 33.7 -8 -4 0 649.54 29.7 -8 4 0 555.04 31.3 -9 -4 0 34.1 4.8 -9 -4 0 32.7 3.4 -9 4 0 34.5 3.3 0 5 0 9.3 3.8 -2 5 0 5806.22 286.37 -2 5 0 7214.88 274.17 2 5 0 7246.57 283.57 3 -5 0 1162.48 50.89 -3 5 0 1107.59 49.9 -3 5 0 1209.58 56.79 3 5 0 1115.39 59.09 -3 -5 0 1191.48 51.09 -3 -5 0 1175.38 51.29 3 -5 0 1160.88 51.79 -3 -5 0 1151.78 64.69 -4 -5 0 477.75 23.9 -4 -5 0 450.35 27.3 -4 5 0 448.66 22 -4 -5 0 475.85 22.5 4 -5 0 458.45 23.8 -5 -5 0 967.4 48.9 -5 5 0 950.8 42 -5 -5 0 950.4 44.3 -6 -5 0 359.26 24.2 -6 5 0 370.26 17.9 -6 -5 0 348.97 20.1 -6 -5 0 373.46 16.5 -6 5 0 344.07 17.7 6 -5 0 361.26 20.5 -7 5 0 10.8 2.4 -7 -5 0 10.6 4.1 7 -5 0 13.8 3.7 -7 5 0 10 4.1 -8 -5 0 105.09 9.8 -8 5 0 108.59 7.6 -8 -5 0 118.99 8 -9 -5 0 35.4 4.3 -9 5 0 48.9 3.6 -9 -5 0 56.59 5.1 0 -6 0 908.51 41.1 0 -6 0 894.31 41.2 0 -6 0 944.31 41 0 6 0 922.41 49.5 0 6 0 853.41 40.3 0 -6 0 835.62 43.6 1 -6 0 79.09 7 -1 -6 0 71.19 6.6 -1 6 0 65.29 10.4 -1 6 0 72.39 6.4 -1 -6 0 71.49 6.4 -1 -6 0 62.69 8.9 1 6 0 57.19 9.7 1 6 0 67.89 6.4 1 -6 0 63.19 6.6 2 -6 0 2009.8 86.49 2 6 0 1904.01 85.39 -2 -6 0 2065.69 89.89 -2 -6 0 2107.49 85.79 -2 6 0 2049.2 94.49 2 -6 0 1883.61 86.49 -2 6 0 1978.6 84.79 2 -6 0 2063.69 84.99 -2 -6 0 2046.1 85.39 3 -6 0 535.25 26.5 -3 -6 0 547.85 29.9 -3 -6 0 518.95 26 -3 -6 0 519.05 25.2 -3 6 0 509.25 24.7 3 6 0 500.05 25.9 3 -6 0 485.25 28.8 4 6 0 50.99 9.4 -4 -6 0 39 4.8 4 -6 0 44.2 5.9 -4 6 0 49.1 5 -4 -6 0 49.9 5.7 -4 -6 0 44.8 7.7 5 -6 0 2839.72 119.79 -5 -6 0 2915.91 116.49 -5 -6 0 2905.11 119.69 -5 6 0 2810.52 117.19 -5 -6 0 2913.31 125.09 5 6 0 2667.93 118.99 -6 -6 0 559.84 31.8 -6 6 0 530.95 25.1 6 -6 0 574.34 28.4 6 6 0 542.65 27.3 -6 -6 0 583.74 27.9 -6 6 0 539.95 25.2 7 -6 0 431.76 22.5 -7 -6 0 429.96 21.6 -7 -6 0 445.16 25.3 7 6 0 388.36 23.1 -8 -6 0 94.99 6.6 -8 6 0 100.79 6.6 -8 -6 0 105.79 8.6 0 -7 0 3 1.9 0 -7 0 6.9 3.8 1 7 0 1245.68 55.69 -1 -7 0 1191.18 52.99 -1 7 0 1223.08 52.49 -1 -7 0 1155.18 55.89 1 -7 0 1042.6 53.39 1 -7 0 1177.78 53.39 -1 -7 0 1184.68 52.99 -2 -7 0 -0.1 1.5 2 -7 0 1.5 1.9 -2 -7 0 4.1 2.1 -2 7 0 3.5 1.6 -2 -7 0 6.8 3.1 2 7 0 3.6 2.5 3 7 0 49.5 5.9 3 -7 0 52.69 5.8 -3 -7 0 52.89 7.4 -3 -7 0 49.3 5.6 -3 -7 0 37.6 5 -3 7 0 48.5 5 4 -7 0 6.3 2 -4 -7 0 7.1 2.5 -4 -7 0 5 1.8 -4 -7 0 9.3 3.6 4 7 0 3.6 2.4 -4 7 0 2.8 1.4 -5 7 0 3.3 1.6 5 -7 0 0.6 1.8 -5 -7 0 0.4 1.7 -5 7 0 2.9 1.6 -5 -7 0 0.1 1.3 5 7 0 1.4 2.1 -6 -7 0 140.39 12.1 6 7 0 159.88 9.7 6 -7 0 161.18 11.2 -6 7 0 153.38 8.5 -6 -7 0 146.29 10.1 7 -7 0 200.08 11.5 -7 -7 0 177.88 10.6 -7 -7 0 188.38 12.6 -7 7 0 178.28 10.6 0 -8 0 28.5 4.4 0 -8 0 26.8 4.6 1 8 0 339.47 18.5 -1 -8 0 294.47 19.8 -1 8 0 340.77 18.2 -1 -8 0 324.27 18.5 1 -8 0 351.56 19.1 2 -8 0 274.47 16.1 -2 8 0 277.17 15.3 -2 -8 0 247.28 16.1 -2 -8 0 263.47 15.8 -2 -8 0 299.97 25.4 3 -8 0 402.06 20.9 -3 -8 0 386.86 19.4 -3 -8 0 371.16 22.9 3 8 0 380.86 20.4 -3 8 0 399.96 19.7 -3 -8 0 385.46 21 -4 -8 0 37 3.1 -4 -8 0 36.5 6.1 4 8 0 39.7 4.9 4 -8 0 36.9 4.9 -4 8 0 31.4 3.9 -4 -8 0 35.1 5 -5 -8 0 7 2.2 5 8 0 7.3 2.2 -5 -8 0 0.9 3.5 5 -8 0 2.2 2.3 -6 -8 0 21.4 3.9 6 -8 0 20.4 3.2 -6 -8 0 19.4 3 0 -9 0 3.5 1.7 0 9 0 2.2 1.5 1 -9 0 61.89 5.9 -1 9 0 62.59 5.7 1 9 0 56.59 5.9 -1 -9 0 62.99 5.6 -2 -9 0 108.59 9.4 2 -9 0 142.89 9.2 -2 -9 0 136.19 8.1 2 9 0 129.39 8.9 -2 9 0 134.09 8.6 -3 -9 0 134.69 10.3 3 -9 0 161.38 10.1 3 9 0 164.08 9.9 -3 9 0 157.58 9.3 -3 -9 0 166.38 7.3 -4 9 0 33.8 3.3 4 9 0 32.5 3.4 -4 -9 0 33.4 5.6 4 -9 0 32.6 4.1 5 -9 0 234.58 13.4 0 10 0 775.62 34.3 0 -10 0 798.92 34 -1 10 0 67.09 4.9 1 10 0 67.09 4.9 1 -10 0 64.39 4.9 -1 -10 0 66.69 4.1 2 10 0 55.39 4.3 -2 10 0 60.19 4.3 2 -10 0 61.29 4.6 -3 10 0 42.8 3.6 3 10 0 34.7 3 3 -10 0 40.1 3.6 0 0 1 2 0.3 -1 0 -1 28.2 1.7 -1 0 1 30.3 2.4 -1 0 -1 32.1 2 -4 0 1 8411.96 349.27 -4 0 -1 8765.82 348.07 5 0 1 1427.76 64.19 5 0 -1 1448.85 66.19 -6 0 1 706.53 33.4 -6 0 1 701.63 33.3 -6 0 -1 674.13 32.6 -6 0 -1 718.43 33.3 -6 0 -1 743.53 37.2 -6 0 1 736.93 38 -7 0 -1 210.88 15.7 -7 0 -1 196.78 11.9 -7 0 1 191.28 15.9 -7 0 1 194.28 12.4 -7 0 -1 193.58 12.4 -7 0 1 168.28 12.8 -8 0 -1 830.22 37.8 -8 0 1 829.52 37.6 -8 0 -1 814.92 36 -8 0 -1 767.62 41 -8 0 -1 811.72 42.6 -8 0 1 835.42 37.2 -8 0 1 802.32 43 -9 0 -1 79.99 9.1 -9 0 1 85.89 5.5 -9 0 1 98.59 9.2 -9 0 -1 100.29 7.1 -9 0 1 99.19 6.8 -9 0 -1 89.59 8.5 -9 0 1 81.89 9.4 -10 0 -1 127.19 7.8 -10 0 1 131.69 8.5 -10 0 -1 115.09 6.4 -10 0 -1 101.09 8.7 -1 -1 -1 1147.89 46.6 1 1 -1 1090.39 48 1 1 1 1116.19 48 -1 -1 1 1224.38 48.6 -3 1 1 147.39 9.1 -3 -1 -1 136.69 9.7 3 1 -1 133.99 9.3 -3 1 -1 138.49 6.6 3 1 1 131.09 8.8 -3 1 -1 145.29 8.9 -4 1 1 3709.73 154.78 4 1 -1 3684.53 155.08 -4 -1 -1 3632.54 156.68 4 1 1 3728.23 154.18 -4 1 -1 3889.71 153.08 5 1 -1 3374.06 141.59 5 1 1 3264.37 139.69 -6 1 1 1482.95 67.39 -6 1 1 1389.66 61.69 6 1 -1 1399.16 69.19 -6 -1 -1 1421.16 62.69 -6 1 1 1481.75 62.59 -6 -1 -1 1487.35 66.59 -6 -1 -1 1386.36 61.39 -6 -1 1 1483.75 67.49 -6 1 -1 1427.86 61.79 -6 -1 1 1382.06 62.19 6 1 1 1382.56 67.19 -6 -1 1 1423.26 62.59 -6 1 -1 1538.15 66.79 -6 1 -1 1425.16 61.79 -7 1 1 64.59 9 -7 -1 -1 76.49 7.1 -7 1 1 67.29 6.9 -7 1 1 63.89 6.1 -7 -1 -1 62.29 8.3 -7 -1 -1 57.99 5.6 -7 -1 -1 60.09 8 -7 1 -1 62.79 6.2 -7 1 -1 62.29 6.1 -7 1 -1 63.69 8.2 -7 -1 1 72.29 9.4 -7 -1 1 63.59 6.3 -8 -1 -1 263.27 19.3 -8 -1 -1 297.97 19.5 -8 -1 -1 285.17 16.3 -8 1 1 264.37 19.6 -8 1 1 285.07 15.8 -8 1 1 279.67 16.4 -8 -1 1 288.57 15.1 -8 -1 1 264.67 19.7 -8 1 -1 274.67 15 -8 1 -1 273.77 19.4 -8 -1 1 266.17 19 -8 1 -1 256.67 18 -8 -1 1 263.97 15.6 -8 1 -1 277.27 15.5 -9 -1 -1 323.67 19.3 -9 1 1 334.27 19.2 -9 -1 -1 304.07 20 -9 1 1 326.97 15.6 -9 1 1 287.27 19.9 -9 -1 -1 319.07 16.6 -9 1 1 325.47 18.4 -9 1 -1 303.57 20.1 -9 1 -1 320.17 14.6 -9 1 -1 325.67 16.3 -9 -1 1 286.27 19.8 -9 -1 1 329.97 16.3 -9 1 -1 326.67 18.4 -10 -1 -1 125.89 9.4 -10 1 1 112.99 7.4 -10 -1 -1 116.89 6.5 -10 1 -1 97.19 8.4 -10 -1 1 131.19 8.5 0 2 -1 544.05 25 -2 2 1 94.89 7.5 2 2 -1 129.49 8.7 2 2 1 120.89 9.9 -2 -2 1 112.09 9.5 3 2 -1 1932.31 82.39 -3 2 1 1891.91 80.49 3 2 1 1828.52 81.59 -3 2 -1 1963.3 78.79 -4 2 1 1093.89 48.4 -4 2 1 1079.59 42.9 4 2 -1 1059.69 49.99 4 2 1 1023.2 49.2 -4 2 -1 1047.6 43.8 -4 2 -1 1054.69 45.9 5 2 -1 611.54 32.4 -5 -2 -1 580.74 28.1 -5 -2 -1 511.25 30.8 5 2 1 615.64 31.7 6 2 -1 313.67 23.3 -6 -2 -1 291.97 20.8 -6 -2 -1 319.07 16.5 -6 -2 -1 346.97 21.3 -6 2 1 318.47 16.8 -6 -2 -1 332.37 18.4 -6 2 1 357.56 22 -6 -2 1 333.27 18.3 6 2 1 325.27 22.3 -6 -2 1 314.87 17.4 -6 -2 1 322.77 21.4 -6 2 -1 329.27 21 -6 2 -1 305.27 16.6 -7 2 1 174.28 11.5 -7 -2 -1 149.29 11.4 -7 -2 -1 174.48 14.9 -7 2 1 173.38 14.8 -7 -2 -1 159.98 13.9 -7 -2 -1 165.88 9.3 -7 2 1 155.98 10.4 -7 -2 1 169.38 11.7 -7 2 -1 177.38 14.4 -7 -2 1 151.18 14.4 -7 -2 1 173.88 14.6 -7 2 -1 159.18 10.8 -7 2 -1 154.08 10.4 -7 -2 1 164.28 10.6 -8 2 1 394.46 19.4 -8 -2 -1 371.76 32.2 -8 -2 -1 360.96 24.6 -8 2 -1 395.26 20.9 -8 -2 1 385.26 18 -8 -2 1 385.76 21.5 -8 -2 1 359.86 25.4 -8 2 -1 397.26 19.7 -9 2 1 205.08 10.1 -9 2 1 178.78 14.1 -9 -2 -1 187.88 13.6 -9 2 1 196.68 15.3 -9 -2 -1 175.78 13.5 -9 -2 -1 196.98 11.4 -9 2 1 186.98 10.6 -9 2 -1 178.78 14 -9 -2 1 212.68 14.5 -9 2 -1 196.58 10.9 -9 2 -1 188.08 12 -9 -2 1 161.18 13.1 -9 -2 1 200.28 11.1 -10 -2 -1 263.77 14.5 -10 -2 -1 266.17 12.4 -10 -2 1 269.57 14.6 0 3 1 2525.85 103.29 0 3 -1 2347.17 108.99 1 3 -1 106.39 8.6 1 3 1 118.39 9.2 -1 3 -1 115.79 8.4 2 3 -1 103.29 9 2 3 1 104.29 8.9 3 3 -1 745.83 37.1 -3 3 1 730.63 35.4 -3 3 -1 728.13 33.4 3 3 1 718.73 36.7 4 3 -1 1170.18 55.29 -4 3 -1 1158.48 48.2 -4 3 -1 1144.49 49.5 4 3 1 1072.99 54.09 -5 -3 -1 396.46 21 5 3 -1 408.06 25.8 -5 -3 -1 385.46 24.2 -5 3 1 384.06 18.9 -5 -3 -1 366.86 19.2 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562.34 27.7 3 7 3 533.25 27 3 -7 -3 562.44 28.3 -3 7 -3 552.64 26.2 -3 -7 3 514.85 27.1 -4 -7 -3 862.11 44.4 -4 -7 -3 897.01 39.5 -4 7 3 845.92 38 4 -7 3 847.22 39.9 4 7 -3 868.71 39.8 4 -7 -3 851.01 39.8 -4 7 -3 860.61 37.6 -4 -7 3 846.52 38.6 -4 -7 3 828.52 39.7 -4 -7 3 688.83 46.3 -4 7 -3 828.02 40.6 4 7 3 866.11 39.5 -5 7 3 58.79 5.2 -5 -7 -3 57.39 8.1 5 -7 3 46.9 6 5 7 -3 45.2 5.6 -5 -7 -3 54.79 6 -5 -7 3 62.59 6.3 -5 7 -3 58.49 4.7 -5 -7 3 55.99 5 -5 -7 3 63.59 7.6 5 -7 -3 59.89 6.3 6 -7 3 244.48 14.4 -6 7 3 252.27 13.5 -6 -7 -3 242.98 13.9 -6 7 3 260.67 14.6 -6 -7 -3 238.88 17 6 7 -3 250.07 15.8 -6 7 -3 233.08 12.8 -6 -7 3 247.38 14.3 6 -7 -3 245.78 14.8 -6 -7 3 246.08 17.9 -7 7 3 229.68 13.2 -7 -7 -3 246.38 13.1 -7 -7 -3 239.18 15.2 7 7 -3 260.27 12.6 7 -7 -3 253.67 14.1 -7 -7 3 251.87 13.2 -7 7 -3 254.27 13 -7 -7 3 245.78 14.3 -7 7 -3 258.97 13 0 -8 -3 212.98 12.8 0 8 -3 212.08 13.5 0 -8 -3 193.98 14.9 0 8 3 222.68 13.3 0 -8 3 200.08 13.9 -1 8 3 129.99 9.2 -1 -8 -3 118.19 11.6 1 -8 3 129.79 10.4 1 8 -3 137.29 9.9 -1 -8 -3 126.39 8.8 1 -8 -3 134.59 12.1 1 8 3 125.39 9.4 -1 8 -3 128.09 9.5 1 -8 -3 131.69 9.4 -1 -8 3 121.99 10.1 -2 -8 -3 845.72 35 -2 -8 -3 782.72 37 -2 -8 -3 752.72 43.2 2 8 -3 816.92 41.9 2 -8 3 797.72 44 2 -8 -3 757.62 37.3 -2 8 -3 749.23 39.9 2 8 3 812.52 36.9 -3 8 3 28.1 4 3 8 -3 36.4 4.7 -3 -8 -3 19.7 3.7 3 -8 3 32.7 4.7 3 8 3 46.7 5.7 -3 -8 3 29.5 5.5 3 -8 -3 32.9 4.5 -3 -8 3 33.3 4.8 -3 8 -3 29 3.8 -3 -8 3 28.1 4.3 4 8 -3 195.18 11.5 -4 -8 -3 176.88 13.9 -4 -8 -3 186.38 11.6 -4 8 3 186.28 10.7 4 -8 3 194.58 11.7 4 -8 -3 196.48 12.2 -4 8 -3 195.88 10.3 -4 -8 3 172.38 10.6 4 8 3 152.18 11 -4 -8 3 142.19 16.7 -4 -8 3 183.78 12.2 -5 -8 -3 241.18 16.7 5 8 -3 229.58 12.6 5 -8 3 231.88 13.2 -5 8 3 250.57 14.2 -5 -8 -3 246.28 16.1 -5 8 -3 221.38 11.5 -5 8 -3 213.98 10.8 -5 -8 3 219.28 13.8 5 -8 -3 235.68 14 -5 -8 3 221.48 13.4 -6 -8 -3 9.7 2.9 6 -8 3 13.8 2.8 -6 8 3 9.5 1.6 6 8 -3 11.5 2 -6 8 3 6.2 1.6 -6 -8 -3 17 2.6 -6 -8 3 6.3 3.5 6 -8 -3 18.8 3 -6 -8 3 10.7 2.2 0 -9 -3 409.76 19.4 0 9 -3 396.56 20 0 -9 3 369.56 20.3 0 -9 -3 361.36 21.4 0 9 3 405.76 19.7 -1 -9 -3 6.9 1.6 -1 9 3 12.7 2.4 1 9 -3 8.9 2.5 -1 -9 -3 11.1 2.9 1 -9 3 9.8 2.5 1 -9 -3 4.4 2.8 1 9 3 3.2 1.7 -1 -9 3 5.7 2 -1 9 -3 8.9 2.4 1 -9 -3 13.8 2.8 -2 9 3 347.97 17.3 -2 -9 -3 356.66 23.1 2 9 -3 355.16 18.1 2 -9 3 335.07 18 -2 9 -3 341.77 17.1 -2 -9 3 314.87 17.4 2 -9 -3 340.47 17.7 3 9 -3 474.75 25.8 -3 9 3 492.85 21.9 3 -9 3 413.66 25 -3 -9 -3 437.56 24 -3 -9 3 439.46 21.7 3 -9 -3 487.85 22.8 3 9 3 481.35 21.8 -4 9 3 551.44 24.1 -4 -9 -3 489.25 26 4 -9 3 556.44 25 4 9 -3 529.25 24.5 -4 9 3 540.05 25.1 -4 9 -3 530.45 23.1 4 -9 -3 542.45 25.3 5 9 -3 35.4 3 5 -9 3 29.9 3.3 -5 9 3 26.7 4.3 -5 9 3 35.5 2.7 -5 -9 -3 29.4 3.5 5 -9 -3 38.8 3.7 0 10 -3 21 2.7 0 -10 3 21.3 2.7 0 10 3 18.5 2.5 0 -10 -3 17.4 2.5 1 10 -3 157.08 8.8 1 -10 3 153.88 8.8 -1 10 3 154.48 8.6 -1 10 -3 152.58 8.5 1 -10 -3 150.98 8.2 -1 -10 3 166.28 8.5 1 10 3 157.68 8.4 2 10 -3 97.49 6 -2 10 3 87.79 5.7 2 -10 3 98.99 6.2 -2 -10 3 94.19 5 -2 10 -3 95.19 5.6 2 10 3 93.89 5.5 2 -10 -3 97.69 6 3 -10 3 43.7 3.5 -3 10 3 36.5 3.3 3 10 -3 38.5 3.1 3 -10 -3 36.1 3.1 0 0 -4 2128.49 86.29 1 0 -4 1229.48 50.09 1 0 4 1147.29 50.59 1 0 -4 1230.08 52.69 -1 0 -4 1199.78 50.49 -1 0 4 1316.47 52.49 -3 0 -4 3.8 1 3 0 4 3.9 0.8 3 0 -4 2.2 1.7 4 0 4 9837.32 397.16 -4 0 -4 9999 396.76 -5 0 4 59.49 7.9 -5 0 -4 86.29 6.8 -5 0 -4 79.59 11.7 5 0 -4 82.99 9.9 -6 0 4 318.87 21.8 -6 0 4 282.17 16 -6 0 -4 324.27 17.1 -6 0 -4 323.37 19.7 -6 0 4 310.37 17.9 -6 0 4 334.87 18.5 -6 0 -4 275.77 19.4 -6 0 -4 317.67 15.7 -7 0 -4 2329.77 100.79 -7 0 -4 2331.77 96.69 -7 0 4 2160.88 102.99 -7 0 -4 2219.78 93.19 -7 0 -4 2380.66 100.89 -7 0 4 2258.27 95.79 -7 0 4 2246.38 97.29 -8 0 -4 144.39 12.6 -8 0 -4 154.78 12.9 -8 0 4 188.98 14.4 -8 0 -4 166.28 14.7 -8 0 4 129.29 9.2 -8 0 4 135.09 14.2 -9 0 -4 34.4 5.4 -9 0 4 31.5 3.6 -9 0 -4 22 4.5 -9 0 4 25.3 4.8 -9 0 -4 31.2 4.2 -10 0 4 214.28 11.9 -10 0 -4 182.98 12.1 0 1 -4 2012.9 84.99 0 -1 4 2207.58 85.29 0 -1 -4 2055.39 84.09 0 1 -4 2013.3 84.29 -3 -1 -4 5441.36 210.08 3 1 -4 5132.29 209.08 -3 1 -4 5140.79 210.18 3 1 4 5168.18 211.88 -4 -1 -4 377.06 17 -4 1 -4 364.86 16.9 -5 -1 -4 1059.39 48.8 -5 -1 -4 1158.78 61.29 -5 1 4 1072.39 53.89 5 1 -4 1199.98 56.59 -5 1 4 1106.69 49.8 -5 1 -4 1071.99 48.1 -5 1 -4 1137.49 51.69 -5 -1 4 1094.69 57.59 5 1 4 1112.99 49.6 -5 -1 4 1095.69 49.8 -6 -1 -4 797.02 39.2 -6 1 4 775.12 41.8 -6 -1 -4 779.82 40.6 -6 1 4 786.72 37.1 -6 1 4 740.43 34.8 -6 -1 -4 784.32 36.5 6 1 -4 738.73 45 -6 -1 4 793.92 37.1 -6 1 -4 811.12 34.8 -6 1 -4 775.52 35.7 -6 -1 4 755.42 36 -6 -1 4 728.33 41.3 -6 1 -4 822.32 39.6 -7 -1 -4 871.71 45.4 -7 -1 -4 941.71 42.1 -7 1 4 856.41 47.1 -7 -1 -4 944.11 45.4 -7 1 4 924.11 42.5 -7 1 4 861.61 40.3 -7 -1 4 808.42 46.6 -7 1 -4 935.41 41.4 -7 -1 4 929.21 42.2 -7 1 -4 890.51 39.5 -7 1 -4 928.91 45.3 -7 1 -4 890.91 44.2 -7 -1 4 874.01 40.9 -8 -1 -4 290.97 19.2 -8 -1 4 298.87 20.2 -8 1 -4 259.97 12.6 -8 1 -4 276.77 17.8 -8 -1 4 275.57 15.1 -9 1 4 75.49 5.9 -9 -1 -4 63.49 5.8 -9 -1 -4 54.69 7 -9 -1 -4 75.29 8.4 -9 1 -4 60.59 5.3 -9 -1 4 59.09 4.7 -9 1 -4 52.69 6.9 -9 -1 4 56.49 7.1 -10 -1 -4 272.57 13.2 -10 -1 -4 213.18 16.2 -10 1 4 280.07 14.3 -10 -1 4 251.67 13.7 -10 1 -4 244.68 11.6 -10 1 -4 206.08 13.5 -1 -2 -4 432.96 20 1 2 -4 435.26 22.3 -1 -2 4 470.65 23.2 1 -2 -4 442.16 19.9 -1 2 -4 454.75 20.2 -2 -2 -4 1075.79 45.3 2 2 -4 1038.4 48.6 -2 2 4 1093.19 49.5 -2 2 -4 1152.08 45.6 2 2 4 1009.2 47.8 3 2 -4 203.38 10.3 3 2 -4 218.88 14.6 3 2 4 207.68 13.2 -3 2 -4 216.38 11.1 4 2 -4 3724.03 155.58 -4 2 -4 3768.22 149.19 4 2 4 3472.65 152.28 5 2 -4 1035.8 53.99 -5 -2 -4 1051.49 51.49 -5 2 4 1058.19 52.39 -5 2 4 1071.29 46.3 -5 -2 -4 1140.09 50.19 -5 2 -4 1112.79 47.2 -5 -2 4 948.31 51.49 -5 2 -4 1132.49 50.19 -5 2 -4 1026 44.4 5 2 4 1094.69 50.29 -5 -2 4 979.6 51.09 -6 -2 -4 1044.6 47.1 -6 2 4 938.31 49 -6 2 4 937.41 42.2 -6 2 4 964.6 44.2 -6 -2 -4 1000.2 44.2 -6 -2 -4 920.41 48.1 -6 2 -4 950.1 42.5 6 -2 -4 900.81 45.5 -6 -2 4 861.31 48.3 -6 -2 4 941.31 43.9 -6 2 -4 1019.9 47 -6 -2 4 934.31 43.4 -7 2 4 165.98 15.5 -7 2 4 190.08 11 -7 -2 -4 198.18 13 -7 -2 -4 192.38 15.7 -7 2 4 190.28 12.9 -7 -2 -4 203.98 15.1 -7 -2 4 164.78 15.5 -7 2 -4 189.88 15.8 -7 2 -4 209.98 15.4 -7 2 -4 205.18 12.2 -7 -2 4 192.28 12.5 -7 2 -4 192.48 11.3 -7 -2 4 180.48 12 7 -2 -4 148.69 14 -8 2 4 397.76 27 -8 -2 -4 457.75 26.6 -8 -2 -4 468.55 26.6 -8 2 4 467.05 23.8 -8 -2 -4 473.25 23.9 -8 -2 4 453.85 22.5 -8 2 -4 459.85 21.1 -8 2 -4 455.75 26.6 -8 -2 4 450.95 22.4 -8 2 -4 463.05 22.8 -9 2 4 353.46 17.6 -9 -2 -4 331.97 19.5 -9 -2 -4 344.97 17.8 -9 -2 4 354.76 16.2 -9 2 -4 351.46 18.9 -9 2 -4 341.07 20.4 -9 -2 4 331.67 15.2 -9 -2 4 357.76 20.7 -10 2 4 17.4 3.1 -10 -2 -4 21.4 2.3 -10 2 -4 16.8 3.4 -10 -2 4 14.4 3.4 -10 2 -4 11.4 2 0 -3 -4 2790.12 113.69 0 3 -4 2748.02 115.69 -1 -3 -4 283.47 14.2 1 3 -4 262.27 16.2 2 3 -4 3587.14 148.29 -2 -3 -4 3280.57 143.69 2 3 4 3492.35 147.99 -2 3 -4 3707.23 143.09 3 3 -4 299.87 21.3 -3 3 -4 303.17 15.3 3 3 4 302.97 19 4 3 -4 3161.28 136.89 4 3 -4 2873.51 130.79 -4 3 -4 3336.87 129.09 4 3 4 3197.08 135.09 -5 3 4 150.88 9.7 -5 -3 -4 170.28 14.1 5 -3 4 165.98 10.3 5 3 -4 149.59 14.8 -5 -3 -4 163.88 10.9 -5 -3 -4 180.08 12.8 5 -3 -4 128.69 15.3 -5 -3 4 163.68 11 5 3 4 152.38 13.9 -5 3 -4 150.78 9.2 -5 -3 4 150.38 10.7 -5 3 -4 164.28 12.3 -5 -3 4 137.59 14.8 -6 3 4 170.98 12 -6 -3 -4 158.98 15 -6 -3 -4 190.98 14.1 -6 -3 -4 183.08 12.2 -6 -3 4 179.18 14.9 -6 3 -4 183.68 11.4 6 -3 -4 187.48 13.5 -6 -3 4 143.49 14.5 -6 -3 4 174.28 11.9 -7 3 4 246.48 13 -7 3 4 194.18 17 -7 -3 -4 243.88 17 -7 -3 -4 245.28 15 -7 3 4 235.38 14.9 -7 -3 -4 254.97 18.6 -7 -3 4 230.48 14.2 7 -3 -4 209.48 16.2 -7 -3 4 220.48 17.7 -7 3 -4 241.68 17.1 -7 3 -4 245.98 13.7 -7 -3 4 248.98 14.4 -8 -3 -4 23.6 4.1 -8 -3 -4 17.1 4.5 -8 3 4 20.8 3.8 -8 -3 -4 27.2 5.6 -8 3 -4 26.5 5.3 -8 3 -4 30.8 3.8 -8 3 -4 28.3 3.4 -8 -3 4 16.7 3 -8 -3 4 21 3.2 -8 -3 4 29.7 5.6 -9 -3 -4 64.79 6.5 -9 -3 -4 58.49 5.4 -9 3 4 70.39 5.5 -9 -3 -4 52.39 6 -9 3 -4 70.29 5 -9 -3 4 60.59 5 -9 3 -4 55.69 6.4 -9 -3 4 60.59 7 0 4 -4 2957.5 125.59 1 4 -4 4639.94 191.88 -1 4 -4 4658.03 189.58 1 4 4 4460.55 192.68 2 4 -4 119.09 11.5 2 4 4 139.39 12.4 3 4 -4 2030.3 94.99 -3 4 -4 2185.08 87.89 3 4 4 2059.79 94.49 -4 -4 -4 422.96 25.8 4 4 -4 408.26 28.7 -4 -4 -4 435.96 22.4 4 -4 4 423.76 22 -4 4 4 447.56 21 -4 -4 4 433.56 22.3 -4 4 -4 422.96 20.1 -4 -4 4 423.96 22.1 4 -4 -4 466.95 26.2 -4 4 -4 432.26 21.4 4 -4 -4 427.66 22.7 4 4 4 422.16 27.4 5 -4 4 856.81 39.6 -5 -4 -4 873.41 40.6 -5 -4 -4 837.62 44.9 -5 4 4 823.02 38.6 5 -4 -4 847.02 41 -5 -4 4 923.91 45 -5 -4 4 852.01 40.2 -5 4 -4 906.81 42.9 -5 -4 4 877.41 40.2 -6 -4 -4 670.93 32.6 -6 -4 -4 635.34 34.1 -6 -4 -4 652.13 37 -6 4 4 646.04 30.3 -6 4 -4 665.23 34.7 -6 -4 4 649.93 31.9 6 -4 -4 627.14 33.1 -6 4 -4 660.93 30.4 -6 -4 4 658.13 31.5 -6 -4 4 667.73 36.6 -7 -4 -4 173.58 13.6 -7 -4 -4 202.08 21.4 -7 4 4 185.58 17.4 -7 4 4 166.98 10.5 -7 -4 4 209.08 13.2 -7 4 -4 178.58 14.7 7 -4 -4 184.68 13.5 -8 -4 -4 286.47 16.1 -8 4 4 284.77 16.2 -8 -4 -4 288.57 19 -8 4 -4 309.37 14.9 -8 4 -4 270.17 17.8 -8 -4 4 286.57 18.8 -8 -4 4 299.47 15.4 -8 4 -4 282.57 14.9 8 -4 -4 312.27 17.9 -9 -4 -4 15.1 2.6 -9 -4 -4 19.1 3.8 -9 4 4 15.1 2.9 -9 4 4 19.6 2.7 -9 4 -4 11.8 1.8 -9 -4 4 12.2 2.9 -9 -4 4 12.6 1.9 -9 4 -4 10.4 2.7 0 5 4 1870.21 90.09 0 5 -4 2020.3 88.49 1 5 -4 273.07 20.1 1 -5 4 319.87 17.5 -1 5 -4 266.57 15 -1 5 -4 286.97 18.7 1 5 4 259.27 20.5 -1 -5 4 266.77 15.3 1 -5 -4 266.77 15.6 2 5 -4 1328.37 65.39 -2 5 4 1307.27 56.39 -2 -5 -4 1366.86 61.89 2 -5 4 1375.26 60.79 2 -5 -4 1278.47 59.69 -2 5 -4 1212.98 56.29 -2 -5 4 1306.07 58.19 -2 5 -4 1457.65 60.59 -2 -5 4 1237.08 57.89 2 5 4 1327.37 65.89 2 -5 -4 1259.17 57.79 3 -5 4 2288.57 95.09 -3 -5 -4 2214.08 99.39 -3 5 4 2229.38 93.39 3 -5 4 2185.48 95.89 -3 -5 -4 2229.28 94.39 3 5 -4 2270.87 104.79 -3 -5 4 2148.49 97.69 -3 5 -4 2305.57 95.09 3 -5 -4 2217.18 94.69 3 5 4 2250.77 104.29 3 -5 -4 2309.97 96.79 -3 -5 4 2247.48 94.69 -3 -5 4 2250.47 94.89 -3 5 -4 2237.38 93.09 4 -5 4 491.05 26.1 -4 -5 -4 495.35 29.7 -4 -5 -4 508.35 25.6 4 -5 4 509.85 25.4 -4 5 4 492.15 24.1 -4 -5 4 506.05 25.5 -4 -5 4 515.25 25.5 -4 5 -4 491.75 23.4 4 -5 -4 515.95 26.8 4 -5 -4 503.25 25.8 -4 5 -4 513.15 25.3 -4 -5 4 487.65 28.3 5 -5 4 554.54 34.6 -5 -5 -4 662.43 32 -5 5 4 660.53 30.4 -5 -5 -4 681.23 37.1 5 -5 4 703.43 31.6 5 -5 -4 629.24 32.4 -5 5 -4 631.74 28.9 -5 -5 4 650.73 31.4 -5 -5 4 684.03 32.1 -5 -5 4 637.94 35.4 -6 -5 -4 1124.99 54.59 -6 5 4 1032 46.5 -6 -5 -4 1096.29 48.8 -6 5 -4 1044.3 46.5 -6 -5 4 1073.09 48.4 -6 5 -4 1010.2 50.09 -6 -5 4 1074.19 52.69 -6 -5 4 1063.49 47.2 6 -5 -4 1044.9 49.6 -7 5 4 56.89 6 -7 -5 -4 61.89 8.3 -7 -5 -4 66.29 6.2 -7 5 4 54.79 4.9 -7 5 -4 67.59 5.5 -7 -5 4 45.9 4.5 7 -5 -4 60.49 7.1 -7 -5 4 59.99 7.7 -7 5 -4 52.59 7.3 -7 -5 4 50.19 5.6 -8 5 4 137.19 13.1 -8 5 -4 178.28 9.5 -8 -5 4 179.28 12.9 -8 -5 4 192.88 10.3 -8 5 -4 152.38 11.4 8 -5 -4 193.78 12.5 -8 5 -4 188.48 9.8 0 -6 -4 1.4 2.6 0 -6 4 -1.8 1.7 0 6 4 7.8 3 0 -6 4 -0.3 1.8 0 6 4 4.6 5.1 0 -6 -4 3.5 2.9 0 6 -4 9 5.3 0 -6 -4 3 1.7 1 -6 4 1959.3 82.09 -1 6 4 1863.21 80.99 -1 6 4 1960.4 94.79 1 -6 4 1926.51 82.99 -1 -6 -4 1932.51 80.89 1 6 -4 1817.92 81.59 -1 -6 -4 1853.91 85.99 1 6 -4 1810.82 90.99 -1 -6 -4 1976.9 81.39 -1 -6 4 1954.1 81.39 1 -6 -4 1943.31 81.59 -1 -6 4 1957.6 82.49 -1 -6 4 1995.8 82.39 1 -6 -4 1813.02 84.79 -1 6 -4 1864.21 81.19 -1 6 -4 1998.6 89.29 -2 -6 -4 256.77 14.5 -2 6 4 247.28 14.2 2 6 -4 227.28 14.7 -2 -6 -4 249.08 18.3 2 -6 4 257.77 15.1 -2 -6 -4 254.57 13.7 2 -6 4 237.58 15.5 2 -6 -4 267.57 15 -2 -6 4 218.68 17.3 -2 6 -4 270.47 14.6 2 -6 -4 253.97 16.8 -2 -6 4 264.07 15.2 -2 -6 4 245.48 14.3 2 6 4 247.08 15.5 -2 -6 4 266.37 15.4 3 -6 4 1693.43 77.69 -3 -6 -4 1788.12 73.69 -3 6 4 1859.31 77.49 3 -6 4 1668.43 77.79 -3 -6 -4 1823.12 78.59 -3 -6 -4 1768.12 89.99 3 -6 -4 1773.52 78.59 3 -6 -4 1703.23 78.09 -3 6 -4 1713.03 77.59 -3 -6 4 2020 79.79 -3 -6 4 1729.43 79.89 -3 -6 4 1879.51 77.99 -4 -6 -4 90.29 10.7 4 -6 4 104.59 8.9 4 -6 4 112.09 8.6 -4 -6 -4 101.09 8.3 -4 6 4 98.19 7.4 4 -6 -4 95.79 8.8 4 -6 -4 103.19 8.8 -4 -6 4 89.69 9.8 -4 -6 4 94.79 8.3 -4 -6 4 97.29 8 -4 6 -4 95.79 8.5 -4 6 -4 96.89 7 -5 6 4 2934.01 123.19 -5 -6 -4 2986 124.89 -5 -6 -4 3054.99 131.49 5 -6 4 2937.31 124.89 -5 -6 4 2958.3 128.79 -5 -6 4 3046.1 123.99 5 -6 -4 2991.8 125.89 -5 6 -4 2953.4 121.69 -5 -6 4 2961.7 125.09 6 -6 4 173.08 11.8 -6 -6 -4 159.38 14 -6 6 4 138.49 9.4 -6 -6 -4 161.98 11 -6 -6 4 160.08 13.1 -6 -6 4 162.48 9.5 -6 6 -4 160.48 9.6 -6 -6 4 151.18 10.6 6 -6 -4 153.18 11.5 7 6 -4 220.78 12.9 -7 6 4 240.98 13.6 -7 -6 -4 236.88 13.2 -7 6 4 213.98 11.1 -7 -6 4 212.18 12.8 -7 -6 4 236.38 16.4 7 -6 -4 228.28 14.3 -7 6 -4 227.18 12 -8 6 4 82.89 5.9 -8 -6 -4 78.69 7.2 -8 -6 -4 76.69 5.5 8 6 -4 87.39 6.1 -8 6 -4 86.79 6.2 -8 -6 4 79.39 6.9 -8 -6 4 104.69 7.1 8 -6 -4 86.99 7.9 -8 6 -4 71.29 4.9 0 -7 4 123.89 9.3 0 -7 4 120.59 10 0 -7 -4 106.49 11.1 0 7 -4 127.59 9.6 0 -7 -4 130.99 9.2 0 7 4 116.89 9 1 -7 4 120.69 10.5 -1 -7 -4 124.79 12.5 -1 -7 -4 138.59 10.2 -1 7 4 141.99 9.6 -1 -7 -4 138.39 9.2 1 7 -4 133.59 10 -1 -7 4 123.79 10.1 1 -7 -4 135.49 9.8 -1 7 -4 126.49 9.7 -1 -7 4 143.79 10.7 1 7 4 136.79 9.8 1 -7 -4 167.08 12.8 -1 -7 4 139.69 9.5 -2 -7 -4 2091.89 87.79 2 -7 4 1973.4 89.19 -2 7 4 2025.6 86.89 -2 -7 -4 2006.1 92.99 2 7 -4 2137.79 88.49 -2 -7 -4 2138.19 85.89 2 -7 4 2098.79 87.79 2 7 4 2037.3 87.69 -2 -7 4 2068.29 88.89 -2 7 -4 1974.1 86.99 2 -7 -4 2031.5 87.79 2 -7 -4 2123.39 90.49 -2 -7 4 2048.1 88.39 3 -7 4 429.66 22.6 -3 -7 -4 431.16 27.2 -3 -7 -4 456.05 23 3 -7 4 418.16 23.5 3 7 -4 460.85 23.7 -3 7 4 446.46 22.2 -3 -7 -4 457.85 19.3 3 -7 -4 448.46 23.4 -3 -7 4 448.46 23.8 -3 -7 4 473.45 23.5 -3 -7 4 397.96 24.7 3 7 4 427.86 22.7 -3 7 -4 435.96 24.5 3 -7 -4 440.36 23.9 -3 7 -4 450.75 21.9 -4 -7 -4 354.96 23.7 -4 7 4 355.16 18.5 -4 -7 -4 373.16 24.9 -4 -7 4 395.56 20.3 -4 -7 4 341.97 21.6 -4 -7 4 341.47 20 4 -7 -4 350.06 21.3 5 -7 4 168.28 10.9 -5 7 4 136.59 9.2 5 7 -4 150.98 10.5 -5 -7 -4 157.78 10.3 -5 -7 -4 145.49 13.2 5 -7 -4 146.69 10.8 -5 -7 4 148.99 9.4 -5 7 -4 148.69 8.4 -5 -7 4 139.29 11.8 -5 -7 4 156.08 11 -6 7 4 649.74 29.5 -6 -7 -4 550.24 31.1 -6 7 4 570.94 28 6 7 -4 575.84 28.4 -6 -7 -4 564.04 27.4 6 -7 4 580.24 27.9 6 -7 -4 560.64 28.6 -6 7 -4 654.63 28 -6 -7 4 559.24 27.8 -6 -7 4 572.04 24.7 -6 -7 4 571.64 29.5 -7 7 4 144.49 8.9 7 7 -4 136.99 8 -7 -7 -4 136.69 10.3 -7 -7 -4 135.59 8.3 -7 -7 4 129.79 9.1 -7 -7 4 145.39 8.6 -7 7 -4 138.99 7.1 7 -7 -4 149.19 9.2 0 -8 -4 13.5 4.2 0 -8 -4 4.7 1.7 0 8 -4 10.1 2.9 0 8 4 4 2.1 0 -8 4 5.1 3 -1 8 4 285.57 16.5 1 -8 4 252.97 16.6 -1 -8 -4 267.57 20 1 8 -4 279.17 16.3 -1 8 -4 275.47 15.8 1 -8 -4 288.37 15.8 -1 -8 4 272.87 16.7 2 -8 4 803.42 38.5 -2 -8 -4 781.72 41.2 -2 -8 -4 792.22 37.2 -2 -8 -4 831.32 34.6 2 8 -4 801.92 37.7 -2 8 4 852.71 37.1 2 -8 -4 800.72 38.3 -2 8 -4 803.12 36.9 2 -8 -4 782.22 37.3 2 8 4 801.72 37.1 -2 -8 4 768.92 38.3 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59.69 6.4 -6 0 -5 239.58 13.6 -6 0 -5 273.07 15.2 -6 0 5 247.98 14.2 -6 0 5 260.17 16.1 -6 0 -5 246.78 17.5 -6 0 -5 302.37 18.2 -7 0 5 2331.07 97.29 -7 0 -5 2418.86 100.39 -7 0 5 2019.5 102.09 -7 0 -5 2243.88 99.49 -7 0 -5 2335.17 96.19 -7 0 5 2210.38 94.79 -8 0 -5 314.17 22.4 -8 0 5 283.67 26.8 -8 0 -5 300.67 17.8 -8 0 5 330.37 18.9 -8 0 -5 290.67 18.7 -9 0 -5 291.07 16 -9 0 5 272.97 14.7 -9 0 5 269.97 17.5 -9 0 -5 287.97 18.1 -9 0 -5 300.77 15.6 -10 0 -5 214.48 12.8 -10 0 5 252.37 12.8 -10 0 -5 179.98 11.5 1 1 -5 2082.69 88.29 -1 -1 -5 2029.7 88.19 1 -1 5 2224.78 88.09 -1 1 5 2259.27 91.99 1 1 -5 2219.68 90.89 -1 -1 5 2146.99 91.09 -1 1 -5 2151.58 88.69 1 -1 -5 2217.58 87.99 -2 1 5 3285.87 135.79 2 1 -5 3342.47 131.39 -2 -1 -5 3123.39 131.59 2 1 -5 3290.57 135.49 2 1 5 3305.67 133.39 -2 -1 5 3229.58 136.09 -2 1 -5 3350.26 132.19 2 -1 -5 3081.09 130.89 3 1 -5 489.65 26.3 3 1 -5 459.35 20.7 -3 -1 -5 490.25 21.7 -3 1 -5 496.35 22.1 3 1 5 484.85 23 4 1 -5 3664.93 169.88 -4 -1 -5 4032.3 159.28 4 1 5 4078.69 160.88 -5 -1 -5 2291.47 95.19 5 1 -5 2336.67 101.69 -5 1 5 2135.69 91.49 -5 1 5 2112.49 98.19 -5 -1 -5 2222.38 92.29 -5 1 5 2187.68 93.29 -5 1 -5 2193.28 89.49 -5 -1 5 2184.28 93.39 -5 1 -5 2278.37 95.19 -5 1 -5 2167.78 91.39 -5 -1 5 1994.3 97.69 -6 -1 -5 2912.31 117.69 -6 -1 -5 2778.92 119.09 -6 -1 -5 2829.82 114.49 -6 1 5 2790.72 115.49 -6 1 5 2532.45 120.39 -6 1 5 2644.54 112.69 6 -1 -5 2327.87 115.89 -6 -1 5 2626.64 113.59 -6 -1 5 2863.41 115.49 -6 -1 5 2469.95 120.19 -6 1 -5 2838.12 117.69 -6 1 -5 2925.71 117.89 -6 1 -5 2806.52 111.99 -6 1 -5 2761.02 113.49 -7 -1 -5 350.46 21.8 -7 1 5 339.37 19.6 -7 1 5 318.97 23.6 -7 -1 -5 344.77 22.2 -7 -1 -5 354.26 19.4 -7 -1 5 330.67 18.1 -7 1 -5 342.97 16.5 -7 1 -5 350.76 21.8 -7 -1 5 352.16 19.6 -7 1 -5 363.56 19 -7 -1 5 302.47 23.3 -7 1 -5 334.57 20.8 -8 -1 -5 65.39 8.2 -8 -1 -5 71.09 8.2 -8 1 5 63.49 8.8 -8 1 5 70.49 7.1 -8 -1 -5 69.69 6.6 -8 1 -5 64.89 7.8 -8 1 -5 77.39 6.7 -8 1 -5 53.39 8.3 -8 -1 5 67.59 6 -8 -1 5 71.49 6.7 -9 -1 -5 437.46 21.2 -9 -1 -5 414.96 21.9 -9 1 5 431.86 20.8 -9 -1 -5 404.86 23.5 -9 1 -5 424.16 23.8 -9 -1 5 412.16 20 -9 -1 5 423.06 23.8 -9 1 -5 425.76 20.7 -10 -1 -5 8.9 2 -10 -1 -5 14.1 2.9 -10 1 5 15.5 2.8 -10 1 -5 13.5 1.9 -10 -1 5 19 3.1 -10 1 -5 14.8 2.8 -1 -2 -5 56.19 4.3 1 2 -5 54.39 5.6 -1 2 -5 72.49 4.6 -1 2 -5 67.19 4.8 1 -2 -5 65.99 4.4 2 2 -5 5702.43 232.58 2 -2 -5 5855.01 232.48 3 2 -5 1563.84 70.29 3 2 -5 1483.15 64.29 -3 -2 -5 1585.04 65.19 3 2 5 1522.75 68.09 -3 2 -5 1631.54 65.49 4 2 -5 3460.25 149.69 -4 -2 -5 3990.9 152.08 4 2 -5 3653.03 159.08 4 2 5 3713.83 155.38 -4 2 -5 3811.62 151.88 5 2 -5 291.27 22.4 -5 -2 -5 315.67 24.4 -5 2 5 336.87 18.1 -5 -2 -5 347.67 19.3 -5 -2 -5 317.47 17.3 -5 2 5 288.17 18.1 -5 -2 5 303.97 18.1 -5 -2 5 283.27 22.1 -5 2 -5 311.67 16.1 -5 2 -5 320.47 19.2 -5 2 -5 310.67 15 5 2 5 316.87 19 5 -2 -5 265.37 18.1 -5 -2 5 295.97 17.5 -6 2 5 1357.66 58.39 -6 -2 -5 1324.27 64.19 -6 -2 -5 1335.57 59.89 -6 2 5 1241.98 65.09 -6 -2 -5 1423.46 62.69 -6 2 5 1344.17 60.39 6 -2 -5 1323.17 61.89 -6 -2 5 1440.86 60.69 -6 2 -5 1406.36 58.69 -6 -2 5 1371.86 59.29 -6 -2 5 1161.18 64.29 -6 2 -5 1448.46 63.09 -7 -2 -5 23.4 5.7 -7 2 5 22.8 3.6 -7 2 5 20.5 3.9 -7 -2 -5 37.4 5 -7 2 5 20.9 5.7 -7 -2 -5 18.9 5 -7 -2 5 15.5 3.5 -7 2 -5 22.4 3.4 -7 2 -5 27.8 5.5 7 -2 -5 25.6 5.7 -7 -2 5 16.2 5.4 -7 2 -5 26.5 3.9 -8 -2 -5 125.69 11 -8 -2 -5 122.29 11.3 -8 2 5 119.99 9.4 -8 -2 -5 125.19 9.3 -8 2 -5 130.99 11.4 -8 2 -5 115.99 6.7 -8 2 -5 124.39 8.7 -8 -2 5 112.29 8.5 -8 -2 5 121.89 11.5 -8 -2 5 117.99 8.6 -9 2 5 33.4 3.8 -9 -2 -5 28.5 4.6 -9 -2 -5 29.1 4.8 -9 -2 -5 33 4.1 -9 2 -5 39.7 4.8 -9 2 -5 36.1 5.6 -9 -2 5 36.4 5.5 -9 -2 5 29.5 2.9 0 -3 -5 5016.1 205.58 0 -3 5 4972.2 208.78 0 3 -5 5241.58 208.18 -1 3 -5 8317.17 335.57 -2 -3 -5 1827.72 78.09 2 3 -5 1806.92 82.29 -2 3 -5 1937.61 78.09 -2 3 -5 1983.4 76.09 2 3 5 1757.42 81.99 3 3 -5 145.79 12.6 -3 -3 -5 141.19 9.2 3 3 -5 143.19 8.5 3 3 5 139.79 11.7 -3 3 -5 148.89 9.1 -4 -3 -5 525.25 26.7 4 3 -5 559.74 25 -4 3 5 546.35 25.7 4 3 -5 546.75 32.4 -4 -3 -5 532.85 30.2 -4 3 -5 564.14 25.9 4 3 5 571.64 30.8 -4 -3 5 532.05 27.1 4 -3 -5 574.34 28 -5 -3 -5 911.31 41.5 -5 3 5 926.11 40.1 -5 -3 -5 904.91 45.8 -5 3 5 812.12 45.6 5 -3 5 894.21 40.5 -5 -3 -5 887.81 45.6 5 3 -5 909.51 55.79 -5 3 -5 881.71 39.3 5 -3 -5 829.82 42 5 3 5 893.11 45.9 -5 3 -5 960.8 43.9 -5 -3 5 932.51 41.8 -5 -3 5 876.01 41 -6 3 5 354.86 20.2 -6 3 5 321.37 23.3 -6 -3 -5 337.47 23.5 -6 -3 -5 351.76 20 -6 3 5 367.66 18.6 -6 3 -5 347.97 18.4 -6 -3 5 377.76 23.7 -6 3 -5 371.16 22.1 -6 -3 5 353.36 19.9 -6 -3 5 384.66 20.2 -7 -3 -5 753.82 38.2 -7 -3 -5 739.43 40 -7 3 5 756.52 36.3 -7 3 5 757.82 33.5 -7 3 5 625.94 39.3 -7 -3 -5 776.32 36.2 -7 3 -5 789.02 39 -7 -3 5 779.52 35.1 -7 3 -5 740.43 34.3 7 -3 -5 730.93 37.6 -7 -3 5 701.73 39.5 -7 -3 5 760.92 35.3 -8 -3 -5 827.02 41.5 -8 -3 -5 785.72 40.2 -8 3 5 808.52 38.4 -8 -3 -5 849.91 38.5 8 -3 -5 736.33 45.8 -8 -3 5 847.92 36.9 -8 -3 5 824.92 42 -8 3 -5 843.72 41.3 -8 3 -5 825.22 35.6 -8 3 -5 871.71 37.5 -8 -3 5 843.02 36.9 -9 -3 -5 18.8 3.5 -9 -3 -5 11.9 2.4 -9 -3 -5 15.5 5 -9 3 5 18.2 2.6 -9 3 -5 13.9 3.5 -9 3 -5 13.7 2.4 -9 -3 5 17.4 3.8 0 4 -5 75.99 7.9 1 4 -5 1259.37 56.19 -1 4 -5 1084.69 52.49 2 4 -5 1963 91.39 2 4 5 2048.4 92.39 -2 4 -5 2093.89 85.49 -3 -4 -5 629.64 33.5 3 4 -5 639.14 36.3 3 -4 5 622.04 32.1 -3 4 5 612.94 28.6 -3 4 -5 640.84 29.7 3 -4 -5 578.04 29.6 -3 -4 5 599.34 30.1 3 -4 -5 709.83 33.6 3 4 5 636.74 35.6 4 4 -5 1143.69 58.29 4 4 -5 1032.8 48 -4 4 5 1073.89 48.1 -4 -4 -5 1084.29 53.89 4 -4 5 1124.09 49.6 -4 -4 -5 1113.19 49.7 -4 4 -5 1153.68 51.69 -4 -4 5 1102.99 49.4 4 -4 -5 1072.39 49.9 4 -4 -5 1144.69 50.99 -4 -4 5 1126.49 49.99 4 4 5 1074.99 56.09 -4 4 -5 1061.09 47 -4 -4 5 1209.78 55.89 -5 -4 -5 32.9 5 5 -4 5 30 4.5 -5 4 5 29.6 4 -5 -4 -5 35.8 7.3 -5 -4 5 45.7 5.2 -5 -4 5 32.2 4.9 -5 4 -5 24.1 4.8 5 -4 -5 32.5 5.3 -5 -4 5 23.2 5.3 -5 4 -5 31.1 5.7 -6 -4 -5 472.05 24.6 -6 4 5 483.55 24.9 -6 4 5 445.46 22.7 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520.35 24.6 0 3 -7 511.95 25 0 3 -7 537.05 26.7 1 3 -7 1199.88 52.99 -1 -3 -7 1202.88 52.89 1 3 -7 1161.18 56.19 -1 3 -7 1252.97 53.49 -1 3 -7 1313.57 53.29 1 -3 -7 1216.38 52.59 -2 -3 -7 2093.99 90.89 2 3 -7 2081.59 90.59 2 3 -7 2198.98 97.89 2 -3 -7 2212.68 90.69 -2 3 -7 2288.17 91.69 2 3 7 2163.38 95.99 3 3 -7 588.04 27.7 -3 -3 -7 623.34 28.7 3 3 -7 581.24 34 -3 3 -7 606.04 28.7 4 3 -7 688.23 43.5 -4 3 7 566.04 27.3 -4 3 7 575.74 29.6 -4 -3 -7 612.24 29.2 4 3 -7 552.94 26.5 -4 -3 -7 557.54 36.1 4 -3 7 536.65 27.9 4 -3 -7 598.44 29.6 4 3 7 607.94 32.8 -4 -3 7 555.04 27.3 4 -3 -7 595.94 29.6 -4 -3 7 596.44 29.3 -4 -3 7 562.04 27.9 -4 3 -7 573.14 27.9 -4 3 -7 577.24 31.3 -5 -3 -7 566.94 32.3 -5 3 7 575.34 29.4 -5 3 7 568.04 27.3 -5 -3 -7 557.64 28.3 -5 -3 -7 614.64 30.5 5 -3 7 538.55 27.5 -5 -3 7 566.04 26.6 -5 3 -7 607.94 30.8 -5 -3 7 560.04 27.6 -5 3 -7 548.95 27 5 -3 -7 529.15 29.5 -5 -3 7 579.84 29.2 6 -3 7 478.45 24.4 -6 -3 -7 478.95 29.6 -6 -3 -7 487.25 25.7 -6 -3 -7 516.75 27.7 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472.75 27.1 3 4 -7 437.36 22.8 -3 -4 7 439.66 23.2 3 -4 -7 472.85 25 3 -4 -7 436.26 23.3 -3 -4 7 483.35 26.5 3 4 7 435.66 28.5 -3 -4 7 485.75 24.2 -3 4 -7 473.85 23.6 -4 -4 -7 997.9 49.5 -4 -4 -7 978.2 44.4 4 4 -7 866.71 43.5 -4 4 7 993.2 43.5 4 -4 7 968.7 44.5 -4 4 -7 974.7 44.5 -4 -4 7 951.1 44.2 4 -4 -7 958.6 45.4 -4 -4 7 983.7 45.3 -4 -4 7 956.1 47.3 4 -4 -7 1065.19 46.6 4 4 7 908.21 51.19 -4 4 -7 1071.49 47.1 -4 -4 7 969.5 43.1 -5 4 7 223.08 13.5 -5 4 7 227.58 15.1 -5 -4 -7 245.08 18.5 -5 -4 -7 235.28 14.7 5 -4 7 217.48 14 5 -4 -7 224.18 15.5 -5 4 -7 240.98 17.6 -5 -4 7 239.08 17.3 -5 4 -7 232.08 14 -5 -4 7 251.07 15.2 -5 -4 7 228.68 14.2 -6 -4 -7 98.59 10.9 6 -4 7 85.89 7.2 -6 4 7 86.09 8 -6 4 7 82.09 7.2 -6 -4 -7 81.79 7.9 -6 -4 -7 86.79 9.6 -6 4 -7 91.79 9.5 -6 -4 7 91.69 10 6 -4 -7 81.19 8.6 -6 4 -7 100.59 7.4 -6 -4 7 87.99 7.8 -6 -4 7 89.59 8.2 -7 4 7 613.74 30.8 -7 -4 -7 620.14 30.2 -7 4 7 610.14 28.4 -7 -4 -7 626.74 34 -7 -4 -7 577.54 30.8 7 -4 -7 630.34 32 -7 -4 7 599.64 29.6 -7 4 -7 627.34 29.1 -7 -4 7 661.63 29.3 -7 4 -7 645.74 32.6 -7 -4 7 603.64 33.2 -8 4 7 69.09 6.1 -8 -4 -7 59.99 5.7 -8 -4 -7 67.49 7.9 -8 4 -7 64.89 5.6 8 -4 -7 84.49 8.4 -8 4 -7 64.29 6.6 -8 -4 7 69.79 5.8 -8 -4 7 46.4 7.3 -9 -4 -7 38.5 4.4 -9 4 7 47.9 3.7 -9 -4 -7 43.3 3.7 -9 -4 7 32.2 3.6 -9 4 -7 39 3.2 0 5 -7 21.6 4.4 0 5 -7 4.4 2.2 0 -5 -7 4.3 3 -1 5 7 227.48 13.1 1 -5 7 233.78 13.9 1 5 -7 241.78 13.9 1 5 -7 236.28 14.8 1 5 -7 222.88 18.2 -1 -5 -7 219.38 12 1 -5 7 215.68 14.1 -1 -5 -7 199.68 16.2 -1 5 -7 211.78 13 -1 -5 7 228.48 13.7 1 -5 -7 226.58 16.1 -1 -5 7 243.38 14.6 -1 5 -7 243.18 16.1 -1 5 -7 242.78 15 1 -5 -7 268.07 13.7 -1 -5 7 229.18 14.1 1 5 7 242.58 21.3 2 5 -7 403.66 22.6 2 -5 7 437.26 22.2 -2 -5 -7 386.66 20.9 -2 -5 -7 437.66 26 2 -5 7 511.75 27.6 2 5 -7 439.76 29.2 -2 5 7 432.46 21.1 -2 5 -7 461.05 23.5 2 -5 -7 415.06 24.3 2 -5 -7 406.36 21.6 -2 5 -7 408.66 20.9 -2 -5 7 402.16 22.1 -2 -5 7 430.96 22.6 2 5 7 403.66 29.2 -2 -5 7 406.16 21.3 3 5 -7 495.55 26.6 -3 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7 7 688.73 32.5 -1 -7 -7 667.03 37.8 -1 7 -7 687.23 33.1 1 7 7 734.83 33 1 -7 -7 689.83 32.9 -1 7 -7 722.63 36.8 1 -7 -7 701.13 36.8 -1 -7 7 682.33 33 -1 -7 7 716.13 34.6 2 7 -7 824.42 41.8 2 -7 7 805.62 40.5 -2 -7 -7 797.42 43.8 -2 7 7 844.02 38.4 2 -7 7 846.42 39.6 2 7 -7 855.91 39.6 -2 -7 -7 830.92 38.3 -2 -7 7 825.82 39.8 2 -7 -7 864.81 39.4 -2 -7 7 811.12 37.8 2 -7 -7 833.82 41.7 -2 7 -7 890.41 42.5 -2 7 -7 883.91 38.3 -3 7 7 1266.27 53.39 -3 -7 -7 1090.59 57.69 3 -7 7 1262.47 54.49 -3 -7 -7 1189.28 59.49 3 7 -7 1155.68 54.29 3 7 -7 1072.29 56.49 -3 -7 7 1236.28 54.69 3 -7 -7 1325.37 56.49 -3 7 -7 1230.48 56.69 -3 -7 7 1237.78 55.39 3 -7 -7 1268.27 54.99 -4 7 7 201.58 13.4 4 7 -7 178.18 12.2 4 -7 7 184.98 11.7 4 -7 7 202.58 12.4 -4 7 7 173.78 11 -4 -7 -7 173.68 15.2 -4 -7 -7 185.08 11.3 4 -7 -7 180.78 12.4 -4 7 -7 179.78 9.6 -4 -7 7 180.98 11.9 -4 -7 7 172.98 12.3 -5 7 7 93.89 6.9 -5 -7 -7 82.19 9.6 5 7 -7 86.69 7.4 -5 -7 -7 90.29 7 5 -7 7 111.19 7.9 5 -7 -7 95.19 8.2 -5 -7 7 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4.9 0 10 7 736.93 32.5 0 -10 7 841.32 34.5 0 10 -7 737.83 32.3 1 -10 7 401.46 18.3 -1 10 7 379.66 17.8 1 10 -7 384.06 17.8 -1 -10 7 437.76 18.6 -1 10 -7 401.46 17.7 0 0 8 646.64 31.4 0 0 -8 659.93 29.3 -1 0 -8 923.01 39.9 1 0 -8 900.71 39.4 1 0 8 915.31 40.8 -2 0 -8 2358.06 98.69 2 0 8 2442.96 98.09 2 0 -8 2353.46 97.89 -3 0 -8 2296.17 93.19 3 0 -8 2183.18 91.39 -4 0 -8 134.59 8.3 -4 0 -8 111.79 10.5 -4 0 8 119.69 10.7 -5 0 -8 865.01 38.7 -5 0 -8 888.61 43.2 -5 0 8 844.62 39.9 -5 0 8 874.91 42.3 -5 0 -8 996.8 40.5 5 0 -8 809.82 43.1 -6 0 8 2165.68 95.19 6 0 -8 2096.89 96.09 -6 0 -8 2246.58 93.29 -6 0 -8 2256.17 96.69 7 0 -8 135.39 12 -7 0 8 133.39 11.2 -7 0 8 141.29 9 -7 0 -8 148.99 10.5 -7 0 -8 147.99 12.4 -8 0 -8 133.39 11.6 -8 0 8 130.69 10 -8 0 -8 142.49 9.8 -9 0 -8 445.86 20.5 -9 0 8 414.96 22.7 -9 0 -8 394.36 22.3 -9 0 8 411.66 20 0 -1 -8 4487.95 182.28 0 -1 8 4562.64 185.08 0 1 -8 4446.16 182.88 1 1 -8 2034.5 88.19 1 1 -8 1946.41 83.49 -1 -1 -8 1997.4 83.49 1 -1 8 2123.69 84.09 1 1 8 1878.11 87.09 1 -1 -8 1977.4 82.99 -1 1 -8 2128.69 84.39 2 1 -8 1797.12 71.49 2 1 -8 1692.43 77.59 -2 -1 -8 1724.93 71.69 2 -1 -8 1643.44 70.59 2 1 8 1588.04 74.69 -2 1 -8 1808.92 72.49 -3 -1 -8 1290.47 55.09 3 1 -8 1316.97 62.99 3 1 -8 1287.57 54.09 3 -1 -8 1222.78 53.59 3 1 8 1281.17 55.69 -3 1 -8 1336.87 55.79 4 1 -8 1971.9 93.99 -4 -1 -8 1948.8 83.39 -4 1 8 2153.18 84.69 -4 -1 -8 1958.8 88.99 4 1 8 2031.3 82.19 -4 1 -8 2042.2 83.49 -4 1 -8 1916.01 87.09 -4 -1 8 1945.21 89.69 -4 -1 8 1920.61 83.99 -4 1 -8 2055.39 83.79 -5 -1 -8 146.29 11.6 -5 1 8 124.79 9.3 -5 -1 -8 130.89 9.5 -5 -1 -8 170.78 13.8 -5 -1 -8 131.59 8.6 -5 1 8 136.99 10.8 5 1 -8 143.29 16.7 5 1 -8 138.49 14.9 5 -1 -8 123.49 11 -5 -1 8 120.19 10.3 -5 -1 8 126.29 9.1 -5 1 -8 136.89 11.3 -5 1 -8 143.19 9.3 -5 1 -8 124.99 8.5 -6 1 8 211.48 13 -6 -1 -8 213.78 16.8 -6 -1 -8 232.18 16 6 1 -8 181.78 15.3 -6 1 8 215.48 15 -6 -1 -8 221.38 13.8 -6 1 -8 213.18 13.1 -6 -1 8 229.08 15.1 -6 1 -8 216.78 15.6 -7 -1 -8 107.29 11.2 7 1 -8 112.89 10.6 -7 1 8 105.79 9.3 -7 -1 -8 109.49 9.1 -7 1 8 104.19 7.7 -7 -1 -8 115.69 10.8 7 -1 -8 104.19 10.7 -7 1 -8 104.19 8.4 -7 -1 8 109.59 9.5 -7 1 -8 108.79 10.4 -8 -1 -8 150.38 12 -8 -1 -8 137.49 9.8 -8 1 8 158.78 10.8 -8 1 -8 140.79 11.8 8 -1 -8 140.29 12.1 -8 -1 8 136.89 10.1 -8 1 -8 134.09 9.5 -9 -1 -8 362.06 18.1 -9 -1 -8 359.76 20.1 -9 1 8 365.86 18.2 -9 1 -8 360.36 20.3 -9 -1 8 365.16 17.7 -9 -1 8 358.66 20.3 -9 1 -8 388.36 18.2 0 -2 8 126.09 9.6 0 2 -8 116.09 9 0 2 -8 111.49 7.9 0 -2 -8 113.09 7.4 1 2 -8 1995.3 84.99 -1 -2 -8 1974.5 84.49 1 -2 8 2131.59 85.49 1 2 -8 2019.3 88.89 -1 2 -8 2018 85.39 1 -2 -8 2052.09 84.29 2 2 -8 2791.52 115.29 2 2 -8 2828.82 121.39 -2 -2 -8 2665.43 115.19 2 -2 -8 2797.82 114.59 -2 2 -8 2900.21 116.29 -3 -2 -8 1030.8 44.5 3 2 -8 958.1 43.5 3 2 -8 1011.3 51.39 3 -2 -8 1020.8 43.4 3 2 8 1001.6 47.3 -3 2 -8 1022.9 45 4 2 -8 274.87 21.8 -4 -2 -8 273.47 17.2 -4 -2 -8 299.47 15.2 4 2 -8 273.47 13.7 -4 2 8 269.17 17.5 -4 -2 -8 272.37 15.2 -4 2 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5.6 -9 2 -8 57.79 4.8 -9 2 -8 58.29 6.1 0 3 -8 43.8 4.6 0 3 -8 38.5 5 1 3 -8 1401.76 64.49 -1 -3 -8 1379.46 60.29 1 3 -8 1386.76 60.69 1 -3 -8 1384.96 59.99 -1 3 -8 1451.85 60.79 -1 3 -8 1409.86 61.09 2 3 -8 3253.17 128.59 -2 -3 -8 2994.6 128.39 2 3 -8 3105.49 134.49 2 -3 -8 2819.22 127.59 2 3 8 3111.09 136.49 -2 3 -8 3340.87 129.49 3 3 -8 566.94 33.7 3 3 -8 552.04 26.7 -3 3 8 555.64 26.5 -3 -3 -8 582.94 27.6 -3 -3 -8 553.44 34.9 -3 3 -8 592.04 27.9 3 -3 -8 522.55 27.8 -3 -3 8 555.64 28.3 3 3 8 569.34 31.8 -3 -3 8 565.34 26.8 3 -3 -8 589.14 29 -4 -3 -8 111.99 10.2 4 3 -8 133.49 14.8 -4 -3 -8 124.59 9.2 -4 3 8 111.69 8.4 -4 -3 -8 120.99 8.8 -4 -3 -8 119.39 11.8 4 3 -8 111.89 7.9 -4 -3 8 116.29 8.5 -4 -3 8 114.69 8.7 4 3 8 108.49 11.5 -4 -3 8 122.89 9.8 4 -3 -8 132.79 10.3 -4 3 -8 137.49 11.2 -4 3 -8 120.19 8.9 -5 3 8 140.19 11.5 -5 -3 -8 138.19 13.2 5 -3 8 133.69 10.1 -5 -3 -8 133.29 10.2 -5 -3 -8 151.58 11.9 -5 -3 8 156.18 9.7 5 -3 -8 137.89 11.4 -5 3 -8 144.19 12 -5 3 -8 142.89 9.9 -5 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26.5 0 -3 14 449.76 23.9 0 -3 -14 492.65 25.3 1 3 -14 208.68 14.8 -1 -3 -14 227.28 14.8 1 3 -14 205.58 12.3 -1 -3 -14 185.38 15.5 -1 -3 -14 208.38 15.4 -1 3 14 208.58 13.5 1 -3 14 185.68 14.4 -1 -3 14 207.78 14.5 -1 -3 14 227.38 14.4 1 -3 -14 198.88 13.8 -1 3 -14 212.58 15.3 1 -3 -14 222.38 19.2 2 3 -14 257.37 15.1 -2 -3 -14 251.97 16.7 -2 3 14 274.27 16.2 -2 -3 -14 255.67 18.7 -2 -3 -14 244.68 17.9 2 -3 14 249.08 15.2 2 -3 -14 255.37 16.2 -2 3 -14 263.47 18.7 2 -3 -14 290.97 17.4 -2 -3 14 266.17 15.7 2 -3 -14 261.77 18.1 -2 3 -14 255.97 17.4 -3 -3 -14 55.59 8 -3 -3 -14 51.39 6.8 -3 -3 -14 51.79 7.5 -3 3 14 51.99 6.4 3 -3 14 45.8 5.9 3 3 -14 56.19 7.1 3 -3 -14 47.9 6.5 -3 -3 14 46.4 6.8 -3 3 -14 57.89 7.4 -3 -3 14 60.99 6.5 -3 3 -14 61.79 7.9 -4 -3 -14 996.9 47.4 -4 3 14 959.5 45.3 4 -3 14 960.2 44.5 -4 -3 -14 954.6 47.5 -4 -3 14 959.6 44.6 -4 3 -14 937.91 46.2 -4 -3 14 996.3 46.9 -4 3 -14 1009.8 43.7 -4 3 -14 1009.5 48.5 4 -3 -14 996.6 47.3 -5 -3 -14 84.79 7.2 5 -3 14 84.39 7.3 -5 3 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114.69 9.3 -2 -4 -14 107.69 10.7 2 -4 14 110.99 8.8 -2 -4 -14 100.09 10.7 2 4 -14 106.29 8.5 -2 -4 -14 100.49 10 2 4 -14 97.39 10 -2 4 -14 103.09 10.6 -2 4 -14 125.29 11 2 -4 -14 111.29 10 -2 -4 14 112.49 9.1 -2 -4 14 102.89 9.6 2 -4 -14 103.99 9.1 -3 -4 -14 517.15 28.3 3 4 -14 521.35 27 -3 -4 -14 533.65 29.8 -3 -4 -14 500.85 30 3 -4 14 540.45 27.2 -3 4 14 586.74 27.9 -3 4 -14 551.64 29.8 3 -4 -14 545.35 28.6 -3 -4 14 537.05 27.2 -3 -4 14 498.05 28 3 -4 -14 582.84 29.4 -3 4 -14 560.54 30 -4 4 14 550.84 27.2 -4 -4 -14 513.05 29.4 -4 -4 -14 552.04 27.7 4 -4 14 520.75 26.7 -4 -4 14 526.65 28 -4 4 -14 566.24 29.2 -4 4 -14 529.15 25.6 -4 -4 14 534.25 26.4 4 -4 -14 525.45 28.5 -5 -4 -14 561.04 34.5 -5 -4 -14 590.24 31 5 -4 14 595.84 28.4 -5 4 14 580.84 28.9 5 -4 -14 615.04 31 -5 -4 14 599.64 30.3 -5 4 -14 626.04 28.2 -5 4 -14 644.94 31.1 -5 -4 14 601.24 27.8 -6 4 14 710.53 34.8 -6 -4 -14 729.83 36.3 -6 4 14 723.33 33.4 -6 4 -14 828.82 36.8 -6 4 -14 769.62 35.2 -6 -4 14 706.23 34.5 6 -4 -14 730.43 35.5 -7 4 14 97.29 6.9 7 4 -14 101.99 6.7 -7 4 14 101.89 6.4 7 -4 -14 109.79 7.5 -7 4 -14 104.19 6.3 -7 4 -14 101.29 6.8 -7 -4 14 95.99 6.5 0 5 14 18.1 4.3 0 5 -14 14.4 4.2 0 -5 14 17.9 3.6 0 5 -14 15.1 4.6 0 -5 -14 15.1 4.5 1 -5 14 123.49 9.6 -1 5 14 125.39 9.6 -1 -5 -14 110.19 11.4 1 5 -14 115.89 12.8 1 5 -14 118.19 8.5 -1 -5 14 135.19 10.3 -1 5 -14 120.49 11.8 1 -5 -14 114.09 8.1 -1 -5 14 125.69 9.6 1 -5 -14 124.09 11.1 -1 5 -14 115.29 11 2 -5 14 9.1 3 2 5 -14 9.6 4.1 -2 -5 -14 15.6 4.4 2 -5 -14 9.8 3.1 2 -5 -14 9.8 3.1 -2 5 -14 11.9 3.3 -2 -5 14 4.5 2.3 -2 5 -14 2.7 3.7 3 5 -14 752.62 36.6 -3 5 14 806.72 37.3 3 -5 14 792.72 37.4 -3 -5 -14 751.42 40.3 -3 5 -14 841.22 38.6 3 -5 -14 776.92 37.9 3 -5 -14 856.11 39.4 -3 -5 14 780.22 38.1 -3 -5 14 760.62 36.6 -4 5 14 113.19 8.4 -4 -5 -14 96.59 10.1 4 -5 14 117.29 8.6 4 5 -14 113.99 8.7 4 -5 -14 99.19 8.9 -4 5 -14 112.49 10 -4 -5 14 102.39 7.8 -4 -5 14 110.69 9 -4 5 -14 107.19 7.5 -5 -5 -14 523.75 28.8 5 5 -14 614.94 27.8 5 -5 14 561.84 30 -5 5 14 570.44 27.3 -5 -5 14 592.84 25.1 -5 5 -14 573.34 26.4 5 -5 -14 586.04 28.8 -5 5 -14 600.74 27.5 -5 -5 14 550.64 27.9 6 5 -14 448.46 20.5 -6 -5 -14 423.46 20.2 -6 5 14 469.45 23.2 -6 5 14 405.46 19.8 -6 5 -14 411.76 19.6 6 -5 -14 424.56 21.3 -6 -5 14 403.16 20.4 0 6 -14 94.09 7 0 -6 14 91.59 8 0 -6 -14 102.49 9.9 0 6 14 108.69 8.3 0 -6 14 110.39 9.2 1 -6 14 45.7 5.4 1 -6 14 52.19 7.2 1 6 -14 47.4 4.8 -1 6 14 43.9 5.6 -1 -6 -14 41.8 6.6 1 -6 -14 30.5 3.2 -1 -6 14 36.4 5.5 -1 -6 14 42.2 5.1 1 -6 -14 38.5 6 -2 -6 -14 84.19 9.3 2 -6 14 84.99 7.7 -2 6 14 87.59 7.4 2 6 -14 84.99 6.8 -2 -6 14 87.39 7.3 -2 -6 14 78.79 7.5 2 -6 -14 81.29 6.6 2 -6 -14 90.59 8.4 3 6 -14 211.38 12.2 3 -6 14 212.48 12.9 -3 6 14 205.38 12.4 -3 -6 -14 194.28 14.6 -3 -6 14 203.98 11.9 3 -6 -14 213.88 12.7 -3 -6 14 202.58 12.9 4 6 -14 112.19 10.7 4 -6 14 94.49 8 -4 6 14 92.99 7.2 -4 -6 -14 94.89 9.2 -4 -6 14 99.99 6.2 -4 -6 14 93.39 7.6 4 -6 -14 93.29 7.6 -5 6 14 95.69 6.6 5 -6 14 97.29 6.3 -5 -6 -14 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106.59 8.3 0 -3 -20 125.79 11.1 0 -3 20 125.89 8.6 0 3 -20 120.19 10.7 -1 -3 -20 19.8 4.4 -1 3 20 21.8 3.4 1 3 -20 14.8 5.7 1 -3 20 24.6 5 1 -3 -20 13.7 3.6 -1 3 -20 22 5 -1 -3 20 22.2 3.8 2 3 -20 100.39 9.6 -2 3 20 109.39 7.7 2 -3 20 95.09 7.2 -2 -3 -20 114.99 8.7 2 -3 -20 104.39 9.6 -2 -3 20 99.09 7.8 -2 3 -20 115.89 9.4 -3 -3 -20 180.18 14 -3 3 20 146.59 9.2 3 -3 20 144.49 8.6 3 3 -20 146.89 11.2 3 -3 -20 133.89 10.4 -3 3 -20 150.58 10.5 -3 -3 20 138.09 9.1 4 3 -20 13.9 3.1 -4 3 -20 12.8 2.6 -4 -3 20 12 2.1 4 -3 -20 13.8 3.2 0 -4 20 6.8 2 1 4 -20 133.69 9.6 1 -4 20 134.69 8.6 -1 4 20 126.59 8.1 -1 4 -20 132.79 9.2 -1 -4 20 130.09 8.5 2 -4 20 40.5 3.9 2 4 -20 35.5 4.9 -2 4 20 36.9 5.7 -2 -4 20 35.3 3.9 -2 4 -20 37.3 6.1 3 -4 20 359.96 17.1 -3 4 20 398.46 20.8 -3 4 -20 383.46 17.8 -3 -4 20 335.17 17.3 0 -5 20 36.3 3.6 1 -5 20 301.57 14.8 -1 -5 20 302.27 15 2 -5 20 355.06 16.6 -2 -5 20 343.97 16.5 0 0 21 8.9 2.3 1 0 21 4.5 2.6 1 0 -21 4.8 3 -1 0 -21 3.5 2.4 -2 0 21 95.59 8.3 -2 0 -21 99.29 9.5 2 0 -21 94.19 10.1 -3 0 21 756.22 34.2 3 0 -21 737.63 38.7 -3 0 -21 776.22 36.7 -4 0 21 740.53 33.4 -4 0 -21 780.12 35.3 0 1 21 3.8 2.2 0 -1 -21 2.8 2.4 0 1 -21 5.2 2.9 0 -1 21 4.8 1.9 -1 1 21 789.02 34.9 -1 -1 -21 758.02 38.8 1 -1 21 776.82 34.5 1 1 -21 742.63 39.8 1 -1 -21 809.12 40.4 -1 1 -21 796.32 39.4 -1 -1 21 707.53 38.5 2 1 -21 317.47 22.3 -2 1 21 360.06 18.4 -2 -1 21 419.46 23.1 2 -1 -21 366.66 26.1 -2 1 -21 348.87 21.2 3 1 -21 153.88 12.7 -3 -1 -21 164.28 11.3 -3 1 21 157.98 9.6 -3 -1 21 145.29 9.4 3 -1 -21 157.88 12.7 -4 1 21 614.54 27.9 4 1 -21 598.24 31.4 -4 -1 -21 645.64 29.3 4 -1 -21 602.74 31.3 -4 -1 21 619.74 27.9 -4 1 -21 673.03 30 0 -2 21 13.3 2.6 0 2 -21 9 3.4 0 -2 -21 6.6 3.8 1 -2 21 21.8 3.5 -1 2 21 22.6 3.7 -1 -2 -21 30.2 4.8 -1 2 -21 25.9 6.5 1 -2 -21 22.5 4.7 -1 -2 21 20.4 3.8 2 2 -21 386.16 23.4 2 -2 21 393.16 20.9 -2 2 21 405.46 20 -2 -2 -21 417.46 22.1 2 -2 -21 405.36 23.6 -2 -2 21 404.16 20.2 -2 2 -21 440.96 23.1 3 2 -21 500.45 27.3 -3 -2 -21 536.15 25.4 -3 2 21 515.65 24 -3 2 -21 537.85 26.2 -3 -2 21 513.25 24.1 3 -2 -21 492.55 27 -4 2 21 171.28 9.7 -4 -2 -21 187.18 10.1 4 2 -21 194.78 14.1 -4 2 -21 195.98 11.7 4 -2 -21 174.88 11.5 -4 -2 21 171.28 9.6 0 3 -21 225.38 14.4 0 -3 21 218.48 12.3 0 -3 -21 222.68 13.8 1 3 -21 339.17 18.7 1 -3 21 310.87 15.9 -1 -3 -21 322.47 17.7 -1 3 21 294.57 15.3 -1 3 -21 319.37 18.1 -1 -3 21 308.17 16.2 1 -3 -21 321.37 18 -2 3 21 463.65 24.1 -2 -3 -21 467.05 21.8 2 3 -21 459.25 23.7 2 -3 21 432.96 21.7 -2 -3 21 425.96 21.3 -2 3 -21 495.45 23.3 2 -3 -21 399.06 24.9 3 3 -21 332.07 17.3 -3 3 21 300.17 17.1 -3 -3 21 312.87 15.6 3 -3 -21 330.97 16.7 0 -4 21 22.6 3 0 4 -21 22.7 3.6 1 -4 21 117.29 7.4 -1 4 -21 130.59 8.8 -1 -4 21 120.99 7.7 -2 4 21 35.8 4.6 2 -4 21 50.99 3.9 -2 -4 21 49.8 4 0 0 -22 88.79 8.9 0 0 22 95.19 8.1 -1 0 22 79.79 6.1 1 0 -22 79.49 8.6 -1 0 -22 79.79 8 2 0 -22 11.9 3.7 -2 0 22 7.3 1.8 -2 0 -22 3.6 1.9 3 0 -22 25 4.3 -3 0 22 24.8 2.8 -3 0 -22 23.5 3.6 0 -1 22 19 3 0 1 -22 19 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84.39 6 0 0 -23 1.3 1.3 -1 0 23 3.7 1.4 1 0 -23 2.8 1.8 -1 0 -23 5.1 2 -2 0 23 10.9 1.9 -2 0 -23 7.6 2.6 2 0 -23 6.5 2.1 0 -1 23 30.2 3.3 0 1 -23 34.8 4.7 0 -1 -23 32.9 4.4 1 1 -23 49.2 5.6 -1 -1 -23 49.8 5.4 1 -1 -23 51.89 5.5 -1 -1 23 43.6 3.8 -1 1 -23 47.8 5.3 2 1 -23 154.88 13.4 -2 1 23 167.88 8.9 -2 -1 -23 184.08 10.5 2 -1 -23 183.18 11.4 -2 1 -23 173.58 13.6 -2 -1 23 173.18 9.2 0 2 -23 53.79 6.3 0 -2 23 42.8 3.8 0 -2 -23 51.59 4.8 -1 -2 -23 64.89 5.2 1 2 -23 68.79 5.9 -1 -2 23 57.79 4.5 -1 2 -23 72.49 5.8 1 -2 -23 68.99 5.6