#------------------------------------------------------------------------------ #$Date: 2020-02-01 02:10:59 +0200 (Sat, 01 Feb 2020) $ #$Revision: 247419 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/72/1557204.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1557204 loop_ _publ_author_name 'Wang, Rong' 'Fan, Run-Zhu' 'Ni, Fu-Qiang' 'Sang, Jun' 'Xie, Xing-Lin' 'Luo, Si-Yuan' 'Tang, Gui-Hua' 'Yin, Sheng' _publ_section_title ; 19-nor-, 20-nor-, and tetranor-Halimane-Type Furanoditerpenoids from Croton crassifolius ; _journal_name_full 'Journal of Natural Products' _journal_paper_doi 10.1021/acs.jnatprod.9b00634 _journal_year 2020 _chemical_absolute_configuration ad _chemical_formula_moiety 'C24 H26 O10' _chemical_formula_sum 'C24 H26 O10' _chemical_formula_weight 474.45 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2019-03-19 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.77753(5) _cell_length_b 10.89287(6) _cell_length_c 25.97545(15) _cell_measurement_reflns_used 21245 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 76.8390 _cell_measurement_theta_min 3.4080 _cell_volume 2200.63(2) _computing_cell_refinement 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.990 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -28.00 61.00 0.50 0.05 -- 46.62 -30.00 98.00 178 2 \w -173.00 -82.00 0.50 0.05 -- -100.00 -96.00 -81.00 182 3 \w 81.00 178.00 0.50 0.05 -- 107.00 116.00 111.00 194 4 \w 32.00 123.00 0.50 0.05 -- 107.00 -30.00 98.00 182 5 \w -119.00 -71.00 0.50 0.05 -- -46.62-125.00-180.00 96 6 \w -119.00 -71.00 0.50 0.05 -- -46.62-125.00 120.00 96 7 \w -119.00 -71.00 0.50 0.05 -- -46.62-125.00 90.00 96 8 \w 15.00 95.00 0.50 0.05 -- 46.62-125.00 0.00 160 9 \w -117.00 -27.00 0.50 0.05 -- -100.00 61.00 30.00 180 10 \w 34.00 109.00 0.50 0.05 -- 107.00 -96.00 -81.00 150 11 \w 34.00 125.00 0.50 0.05 -- 107.00 -61.00 90.00 182 12 \w 83.00 178.00 0.50 0.05 -- 107.00 77.00 60.00 190 13 \w 34.00 109.00 0.50 0.05 -- 107.00 -94.00-120.00 150 14 \w 34.00 109.00 0.50 0.05 -- 107.00 -94.00 30.00 150 15 \w 34.00 131.00 0.50 0.05 -- 107.00 -77.00 90.00 194 16 \w -119.00 -30.00 0.50 0.05 -- -46.62 -57.00 90.00 178 17 \w -119.00 -52.00 0.50 0.05 -- -46.62 -77.00 -30.00 134 18 \w -119.00 -23.00 0.50 0.05 -- -46.62 -77.00-120.00 192 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.1657865000 _diffrn_orient_matrix_UB_12 0.0545409000 _diffrn_orient_matrix_UB_13 -0.0230687000 _diffrn_orient_matrix_UB_21 -0.0830507000 _diffrn_orient_matrix_UB_22 -0.0005995000 _diffrn_orient_matrix_UB_23 -0.0538504000 _diffrn_orient_matrix_UB_31 -0.0697157000 _diffrn_orient_matrix_UB_32 0.1304375000 _diffrn_orient_matrix_UB_33 0.0093298000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0258 _diffrn_reflns_av_unetI/netI 0.0164 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.990 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 22395 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.983 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 76.996 _diffrn_reflns_theta_min 3.403 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.948 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.77896 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.432 _exptl_crystal_description plate _exptl_crystal_F_000 1000 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.267 _refine_diff_density_min -0.277 _refine_diff_density_rms 0.067 _refine_ls_abs_structure_details ; Flack x determined using 1878 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.03(4) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.159 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 311 _refine_ls_number_reflns 4555 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.159 _refine_ls_R_factor_all 0.0279 _refine_ls_R_factor_gt 0.0267 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0442P)^2^+0.4511P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0723 _refine_ls_wR_factor_ref 0.0795 _reflns_Friedel_coverage 0.729 _reflns_Friedel_fraction_full 0.999 _reflns_Friedel_fraction_max 0.972 _reflns_number_gt 4510 _reflns_number_total 4555 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file np9b00634_si_003.cif _cod_data_source_block liwei_ycyl_18_181219 _cod_database_code 1557204 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_formula CHO _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.911 _shelx_estimated_absorpt_t_min 0.764 _reflns_odcompleteness_completeness 99.76 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 71.98 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C7(H7), C2(H2), C11(H11) 2.b Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C12(H12A,H12B), C9(H9A,H9B), C8(H8A,H8B) 2.c Aromatic/amide H refined with riding coordinates: C18(H18), C15(H15), C17(H17) 2.d Idealised Me refined as rotating group: C34(H34A,H34B,H34C), C23(H23A,H23B,H23C), C31(H31A,H31B,H31C), C28(H28A,H28B, H28C) ; _shelx_res_file ; TITL liwei_ycyl_18_181219_a.res in P2(1)2(1)2(1) liwei_ycyl_18_181219.res created by SHELXL-2016/6 at 10:23:55 on 19-Mar-2019 REM Old TITL liwei_ycyl_18_181219 in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1): R1 0.079, Rweak 0.028, Alpha 0.001 REM 2.633 for 27 systematic absences, Orientation as input REM Flack x = 0.006 ( 0.042 ) from 1866 Parsons' quotients REM Formula found by SHELXT: C24 O10 CELL 1.54184 7.77753 10.892866 25.97545 90 90 90 ZERR 4 0.000045 0.000057 0.000148 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H O UNIT 96 104 40 L.S. 50 PLAN 50 SIZE 0.1 0.2 0.3 BOND $h htab conf acta LIST 6 fmap 2 acta REM REM REM WGHT 0.044200 0.451100 FVAR 0.82984 O14 3 0.064329 0.626651 0.790346 11.00000 0.01650 0.01483 = 0.01848 0.00126 0.00328 0.00103 O20 3 0.244496 0.764233 0.757292 11.00000 0.02065 0.01546 = 0.01904 0.00075 0.00073 -0.00031 O33 3 0.775539 0.617810 0.673555 11.00000 0.01485 0.02599 = 0.02134 -0.00059 0.00206 -0.00041 O32 3 0.542188 0.788593 0.623782 11.00000 0.02464 0.01713 = 0.02064 -0.00140 -0.00119 -0.00147 O25 3 0.340605 0.388016 0.582138 11.00000 0.02673 0.01396 = 0.01517 -0.00124 -0.00290 -0.00152 O22 3 0.680234 0.399713 0.622005 11.00000 0.02158 0.01628 = 0.01890 0.00259 0.00393 0.00452 O30 3 0.508681 0.720561 0.543054 11.00000 0.03103 0.01609 = 0.01633 0.00209 0.00151 -0.00080 O19 3 -0.180393 0.375304 0.906827 11.00000 0.02371 0.02315 = 0.01831 0.00263 0.00318 -0.00265 O24 3 0.720427 0.511826 0.550540 11.00000 0.02758 0.02256 = 0.01833 0.00275 0.00710 0.00560 O27 3 0.227227 0.384957 0.502465 11.00000 0.05902 0.02365 = 0.02388 -0.00201 -0.01848 -0.00049 C29 1 0.519583 0.706463 0.593774 11.00000 0.01387 0.01699 = 0.01510 -0.00072 0.00207 0.00179 C5 1 0.479979 0.568601 0.668457 11.00000 0.01712 0.01311 = 0.01434 -0.00130 -0.00133 0.00217 C10 1 0.333889 0.541570 0.693830 11.00000 0.01579 0.01144 = 0.01718 -0.00073 -0.00167 0.00171 C13 1 0.210539 0.658286 0.765749 11.00000 0.01609 0.01691 = 0.01028 -0.00010 -0.00115 0.00022 C7 1 0.331552 0.521122 0.582372 11.00000 0.02041 0.01326 = 0.01466 0.00049 -0.00132 -0.00170 AFIX 13 H7 2 0.328693 0.551780 0.546912 11.00000 -1.20000 AFIX 0 C3 1 0.616463 0.642490 0.751181 11.00000 0.01539 0.01954 = 0.01629 -0.00180 -0.00246 -0.00020 AFIX 23 H3A 2 0.568917 0.724623 0.753531 11.00000 -1.20000 H3B 2 0.728049 0.642983 0.767860 11.00000 -1.20000 AFIX 0 C2 1 0.497880 0.552705 0.779287 11.00000 0.01558 0.01602 = 0.01539 -0.00013 -0.00046 0.00163 AFIX 13 H2 2 0.550743 0.471193 0.777177 11.00000 -1.20000 AFIX 0 C1 1 0.319812 0.544929 0.752438 11.00000 0.01590 0.01391 = 0.01476 -0.00049 0.00000 0.00051 C12 1 0.212980 0.437844 0.775098 11.00000 0.01822 0.01555 = 0.01517 0.00047 0.00160 0.00049 AFIX 23 H12A 2 0.195476 0.374524 0.749370 11.00000 -1.20000 H12B 2 0.271785 0.401910 0.804380 11.00000 -1.20000 AFIX 0 C16 1 -0.019960 0.458139 0.844450 11.00000 0.01860 0.01526 = 0.01532 0.00042 0.00172 0.00175 C34 1 0.487861 0.587305 0.836053 11.00000 0.02024 0.02448 = 0.01542 -0.00217 -0.00170 0.00317 AFIX 137 H34A 2 0.601376 0.587433 0.850568 11.00000 -1.50000 H34B 2 0.417716 0.528690 0.853958 11.00000 -1.50000 H34C 2 0.438180 0.667587 0.839394 11.00000 -1.50000 AFIX 0 C21 1 0.647376 0.493510 0.590668 11.00000 0.01826 0.01543 = 0.01515 -0.00073 0.00029 -0.00066 C9 1 0.169308 0.512290 0.665473 11.00000 0.01545 0.02175 = 0.01570 -0.00060 -0.00018 -0.00249 AFIX 23 H9A 2 0.073100 0.547990 0.683927 11.00000 -1.20000 H9B 2 0.153169 0.424005 0.664778 11.00000 -1.20000 AFIX 0 C18 1 -0.042589 0.431919 0.929254 11.00000 0.02484 0.02138 = 0.01676 -0.00059 -0.00120 0.00052 AFIX 43 H18 2 -0.021730 0.434321 0.964494 11.00000 -1.20000 AFIX 0 C15 1 -0.162976 0.392773 0.855120 11.00000 0.02111 0.02065 = 0.01604 0.00129 0.00113 -0.00074 AFIX 43 H15 2 -0.239465 0.363537 0.830482 11.00000 -1.20000 AFIX 0 C6 1 0.494209 0.570478 0.610167 11.00000 0.01688 0.01472 = 0.01450 0.00000 0.00150 -0.00011 C4 1 0.638204 0.609009 0.695986 11.00000 0.01629 0.01502 = 0.01854 0.00101 -0.00067 0.00069 C11 1 0.039533 0.492976 0.791842 11.00000 0.01778 0.01412 = 0.01695 -0.00031 0.00023 -0.00035 AFIX 13 H11 2 -0.048854 0.470033 0.766733 11.00000 -1.20000 AFIX 0 C8 1 0.170347 0.560889 0.610526 11.00000 0.01698 0.01908 = 0.01731 -0.00008 -0.00341 -0.00184 AFIX 23 H8A 2 0.070063 0.530453 0.592360 11.00000 -1.20000 H8B 2 0.164305 0.649823 0.611087 11.00000 -1.20000 AFIX 0 C26 1 0.284262 0.331140 0.539009 11.00000 0.02560 0.02088 = 0.01766 -0.00306 -0.00227 -0.00285 C23 1 0.812478 0.315958 0.605054 11.00000 0.02073 0.01560 = 0.02490 0.00143 0.00251 0.00292 AFIX 137 H23A 2 0.765441 0.260359 0.580075 11.00000 -1.50000 H23B 2 0.854876 0.270286 0.634001 11.00000 -1.50000 H23C 2 0.905055 0.361532 0.589814 11.00000 -1.50000 AFIX 0 C17 1 0.058700 0.483686 0.893322 11.00000 0.02177 0.02035 = 0.01975 -0.00114 0.00055 -0.00207 AFIX 43 H17 2 0.159672 0.527370 0.899000 11.00000 -1.20000 AFIX 0 C31 1 0.537916 0.844219 0.524111 11.00000 0.03356 0.01845 = 0.02279 0.00730 0.00342 -0.00019 AFIX 137 H31A 2 0.523606 0.845639 0.487407 11.00000 -1.50000 H31B 2 0.652638 0.869521 0.532678 11.00000 -1.50000 H31C 2 0.456832 0.899258 0.539724 11.00000 -1.50000 AFIX 0 C28 1 0.301534 0.195070 0.544250 11.00000 0.04610 0.01844 = 0.02375 -0.00352 -0.00611 -0.00464 AFIX 137 H28A 2 0.420629 0.174048 0.548323 11.00000 -1.50000 H28B 2 0.256893 0.155925 0.513956 11.00000 -1.50000 H28C 2 0.238173 0.167830 0.573839 11.00000 -1.50000 AFIX 0 HKLF 4 REM liwei_ycyl_18_181219_a.res in P2(1)2(1)2(1) REM R1 = 0.0267 for 4510 Fo > 4sig(Fo) and 0.0279 for all 4555 data REM 311 parameters refined using 0 restraints END WGHT 0.0442 0.4511 REM Instructions for potential hydrogen bonds HTAB C3 O20 EQIV $1 -x+1/2, -y+1, z+1/2 HTAB C18 O30_$1 EQIV $2 -x, y-1/2, -z+3/2 HTAB C15 O20_$2 EQIV $3 -x, y+1/2, -z+3/2 HTAB C8 O19_$3 EQIV $4 -x+1, y-1/2, -z+3/2 HTAB C23 O14_$4 HTAB C31 O19_$3 EQIV $5 x-1/2, -y+1/2, -z+1 HTAB C28 O24_$5 REM Highest difference peak 0.267, deepest hole -0.277, 1-sigma level 0.067 Q1 1 0.3201 0.4748 0.5006 11.00000 0.05 0.27 Q2 1 0.4955 0.4468 0.5180 11.00000 0.05 0.26 Q3 1 -0.3202 0.3755 0.8438 11.00000 0.05 0.25 Q4 1 -0.1579 0.3927 1.0000 11.00000 0.05 0.24 Q5 1 0.1802 0.5063 0.5173 11.00000 0.05 0.24 Q6 1 0.0120 0.4733 1.0176 11.00000 0.05 0.24 Q7 1 -0.0481 0.3813 0.8438 11.00000 0.05 0.23 Q8 1 0.3450 0.3793 0.4995 11.00000 0.05 0.23 Q9 1 0.5441 0.5673 0.6865 11.00000 0.05 0.23 Q10 1 0.1659 0.4910 0.4821 11.00000 0.05 0.22 Q11 1 0.6756 0.9372 0.5852 11.00000 0.05 0.22 Q12 1 0.0072 0.5069 0.9831 11.00000 0.05 0.22 Q13 1 0.1582 0.1482 0.4998 11.00000 0.05 0.22 Q14 1 0.0005 0.4733 0.8138 11.00000 0.05 0.21 Q15 1 0.3310 0.5702 0.5010 11.00000 0.05 0.21 Q16 1 -0.1432 0.4064 0.9652 11.00000 0.05 0.21 Q17 1 0.3318 0.8608 0.5173 11.00000 0.05 0.21 Q18 1 0.0051 0.4592 0.5680 11.00000 0.05 0.21 Q19 1 0.1734 0.5562 0.8616 11.00000 0.05 0.21 Q20 1 0.3263 0.0207 0.5174 11.00000 0.05 0.21 Q21 1 0.6815 0.4770 0.8442 11.00000 0.05 0.21 Q22 1 0.1901 0.4789 0.8973 11.00000 0.05 0.21 Q23 1 0.3402 0.4587 0.4663 11.00000 0.05 0.21 Q24 1 0.9812 0.4343 0.5355 11.00000 0.05 0.20 Q25 1 -0.0348 0.4053 0.9806 11.00000 0.05 0.20 Q26 1 0.4971 0.4565 0.8977 11.00000 0.05 0.20 Q27 1 -0.3236 0.3892 0.9154 11.00000 0.05 0.20 Q28 1 0.5393 0.5919 0.7602 11.00000 0.05 0.20 Q29 1 0.6700 0.4428 0.7762 11.00000 0.05 0.20 Q30 1 0.3555 0.5203 0.5353 11.00000 0.05 0.19 Q31 1 0.5177 0.4202 0.7593 11.00000 0.05 0.19 Q32 1 0.1644 0.4069 0.9657 11.00000 0.05 0.19 Q33 1 0.0230 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4 -8 201.74 6.49 0 4 8 193.98 6.56 0 -4 8 210.11 6.09 0 4 -8 192.81 5.44 0 -4 9 19.36 1.79 0 4 9 16.20 1.95 0 4 -9 18.57 1.87 0 -4 -9 17.03 1.53 0 4 9 17.91 1.89 0 -4 -10 1732.31 31.07 0 4 10 1828.42 32.90 0 4 -10 1817.97 32.93 0 -4 10 1778.79 32.47 0 4 11 785.72 17.61 0 -4 11 770.38 16.66 0 4 11 726.07 16.53 0 -4 -11 775.39 15.16 0 4 -11 782.39 16.95 0 4 12 680.07 16.62 0 4 -12 724.37 16.24 0 -4 12 743.43 16.27 0 4 12 723.38 15.96 0 -4 -12 672.36 13.88 0 4 -12 661.70 16.72 0 4 12 684.51 16.65 0 4 13 852.02 19.21 0 4 13 788.56 17.66 0 -4 13 802.91 18.15 0 4 -13 804.15 18.14 0 4 -13 801.40 19.18 0 4 13 803.30 18.94 0 4 -14 410.17 11.55 0 4 14 398.92 12.08 0 4 14 386.67 10.71 0 4 14 420.59 12.38 0 -4 14 424.29 11.74 0 -4 15 955.80 21.19 0 4 15 930.82 21.70 0 4 15 873.57 20.64 0 4 -15 966.08 22.11 0 4 15 873.45 19.36 0 4 -15 900.68 20.46 0 4 15 916.92 21.57 0 4 15 910.12 21.45 0 -4 -15 906.65 21.01 0 4 16 12.17 2.16 0 -4 16 9.08 1.82 0 4 -16 7.35 1.59 0 4 16 9.57 1.89 0 4 16 9.00 1.92 0 4 16 11.91 2.24 0 -4 16 8.22 1.82 0 4 -16 9.38 2.04 0 -4 -16 8.30 1.75 0 4 16 9.64 1.53 0 4 16 6.33 1.66 0 4 16 9.28 1.89 0 4 17 0.70 1.00 0 -4 17 0.37 0.91 0 4 -17 0.42 1.15 0 4 17 0.63 1.12 0 4 17 0.81 1.14 0 4 -17 2.07 1.10 0 4 17 1.44 1.10 0 -4 -17 0.38 0.96 0 -4 17 0.56 0.94 0 4 17 1.18 1.15 0 4 -18 47.47 3.86 0 -4 18 44.49 3.97 0 4 18 40.46 4.02 0 4 -18 37.29 3.95 0 4 18 33.68 3.49 0 -4 18 42.08 3.92 0 4 18 39.50 3.91 0 4 18 42.43 3.78 0 4 18 41.88 3.90 0 -4 -18 40.88 3.86 0 4 -19 153.66 8.01 0 -4 19 150.97 7.61 0 4 19 146.18 7.72 0 4 -19 143.91 7.06 0 4 19 139.77 7.13 0 -4 -19 148.04 7.58 0 4 19 152.37 7.62 0 4 19 143.61 7.18 0 -4 19 142.74 7.47 0 4 19 145.02 7.80 0 -4 20 285.89 11.00 0 4 -20 279.20 11.35 0 4 -20 273.12 10.19 0 4 20 267.85 11.21 0 4 20 275.69 11.10 0 4 20 290.48 10.68 0 -4 -20 291.58 11.09 0 4 20 278.60 10.79 0 -4 20 281.93 11.05 0 4 21 199.51 9.72 0 4 -21 197.28 8.61 0 4 21 218.36 9.35 0 -4 21 218.13 9.59 0 4 21 217.27 9.16 0 -4 -21 214.78 9.50 0 4 -21 233.41 10.25 0 -4 -22 14.60 2.63 0 4 -22 13.17 2.53 0 4 22 6.71 1.90 0 -4 22 14.61 2.61 0 4 22 12.81 2.62 0 -4 22 12.83 2.52 0 4 22 8.10 2.00 0 4 23 195.26 8.51 0 4 23 196.53 8.65 0 4 -23 212.69 9.77 0 -4 23 200.46 8.78 0 4 24 1.30 1.14 0 -4 24 4.72 1.67 0 4 -24 3.81 1.76 0 4 24 0.56 1.11 0 -4 25 5.12 1.73 0 4 25 3.81 1.37 0 4 25 3.90 1.34 0 4 -25 4.29 1.78 0 4 26 8.45 1.64 0 4 -26 9.17 2.18 0 -4 26 7.26 1.80 0 -4 27 106.89 5.32 0 4 -27 115.38 6.17 0 -4 -27 115.95 6.24 0 4 27 104.35 4.85 0 -4 -28 70.39 4.54 0 -4 28 73.39 3.96 0 4 -28 78.35 4.72 0 4 28 73.10 4.78 0 -4 29 0.09 0.66 0 -4 -29 2.21 0.86 0 4 29 2.71 0.98 0 4 -29 2.85 1.00 0 4 30 69.58 3.80 0 4 -30 63.20 3.48 0 -4 -30 56.41 3.36 0 4 31 1.27 0.66 0 5 0 1.95 0.87 0 5 1 4758.12 76.35 0 5 -1 4545.74 75.98 0 -5 2 5.17 0.58 0 5 -2 6.95 1.23 0 5 2 6.45 1.32 0 5 -3 356.18 9.11 0 5 3 357.86 9.52 0 -5 4 1400.42 23.91 0 5 -4 1445.78 26.19 0 -5 5 28.76 1.70 0 5 -5 27.11 2.12 0 5 -6 1332.40 25.12 0 -5 6 1344.67 24.03 0 5 7 814.85 17.75 0 5 -7 768.77 15.98 0 -5 7 783.66 15.46 0 -5 8 13.15 1.45 0 5 -8 15.38 1.54 0 5 8 14.07 1.88 0 5 -9 36.51 3.09 0 -5 9 35.30 2.45 0 5 9 36.55 2.95 0 5 10 524.10 13.44 0 5 -10 516.36 14.06 0 5 10 487.35 13.38 0 -5 10 540.72 12.47 0 -5 -10 525.22 12.01 0 -5 11 99.98 4.69 0 5 11 104.62 5.24 0 5 -11 106.78 5.70 0 5 11 101.91 5.36 0 -5 -11 121.13 4.60 0 -5 -12 605.67 15.57 0 5 12 591.28 15.67 0 5 12 614.15 15.29 0 -5 12 615.86 14.66 0 5 -12 611.34 16.17 0 5 13 130.28 6.44 0 -5 13 131.43 5.86 0 5 13 135.31 6.08 0 5 13 122.47 6.46 0 5 13 125.16 6.16 0 5 -13 130.54 6.68 0 5 -14 1018.34 23.78 0 5 14 982.48 23.34 0 5 14 1011.01 22.85 0 5 14 1001.48 22.03 0 5 14 1025.51 23.30 0 5 -14 984.87 22.02 0 -5 14 1006.78 22.11 0 5 -15 5.78 1.73 0 5 -15 7.07 1.63 0 5 15 6.65 1.47 0 5 15 9.49 1.97 0 5 15 5.80 1.75 0 5 15 7.56 1.74 0 -5 15 4.79 1.45 0 5 16 1.46 1.30 0 5 -16 1.52 1.30 0 5 16 2.63 1.29 0 5 16 3.54 1.14 0 -5 16 2.31 1.09 0 5 16 1.64 1.25 0 5 -17 115.49 6.82 0 5 17 111.21 5.52 0 5 17 115.29 6.65 0 -5 -17 112.35 6.50 0 -5 17 117.83 6.28 0 5 17 119.19 6.70 0 5 17 120.41 6.52 0 -5 -18 1820.68 37.54 0 5 -18 1837.86 38.37 0 5 18 1793.98 37.65 0 5 18 1792.18 36.79 0 -5 18 1860.48 37.05 0 5 18 1770.41 37.42 0 5 19 466.91 15.01 0 5 19 492.56 15.53 0 5 19 506.98 15.00 0 -5 -19 462.95 15.06 0 -5 19 519.19 15.20 0 5 -19 489.22 15.83 0 -5 20 427.63 13.94 0 5 20 430.66 14.08 0 5 -20 413.04 14.53 0 -5 -20 409.63 13.98 0 5 20 423.17 13.59 0 5 20 437.00 14.43 0 5 -21 4.96 1.58 0 5 21 3.27 1.73 0 -5 -21 2.77 1.44 0 5 21 0.61 1.08 0 5 21 3.07 1.50 0 5 22 180.26 8.35 0 5 -22 183.96 9.08 0 5 22 181.56 8.14 0 5 22 176.42 8.62 0 -5 23 4.75 1.73 0 5 23 1.18 1.18 0 5 -23 1.66 1.59 0 5 23 0.93 1.25 0 5 24 278.08 9.86 0 5 -24 300.60 11.40 0 -5 24 287.68 10.43 0 5 24 293.47 10.28 0 -5 25 432.65 12.81 0 5 25 429.43 12.14 0 5 25 401.19 12.02 0 5 25 452.97 14.31 0 5 -25 440.55 13.94 0 5 26 1.60 0.91 0 -5 26 2.81 1.21 0 5 26 3.34 1.65 0 5 -26 3.56 1.40 0 5 -27 349.92 10.95 0 5 27 358.04 11.35 0 -5 -27 326.42 10.78 0 -5 27 338.64 9.81 0 5 -28 51.28 3.53 0 -5 -28 52.85 3.64 0 5 28 49.56 3.59 0 -5 28 44.80 2.87 0 5 29 0.93 0.88 0 -5 -29 2.53 0.93 0 -5 29 1.55 0.68 0 5 -29 2.54 0.83 0 5 30 25.85 2.00 0 -5 -30 15.90 1.56 0 6 0 85.35 4.47 0 6 -1 3.44 1.16 0 6 1 3.61 1.22 0 6 2 998.51 20.82 0 6 -2 923.79 20.03 0 6 -3 5106.47 85.21 0 6 3 5268.74 86.08 0 6 4 509.28 13.36 0 6 -4 505.42 12.71 0 6 -5 947.81 19.55 0 6 -5 908.38 20.74 0 6 6 249.80 8.50 0 6 -6 254.92 8.99 0 6 -6 253.23 7.87 0 6 7 6.07 1.48 0 6 -7 5.15 1.14 0 6 -7 3.56 1.31 0 6 7 4.91 1.32 0 6 8 255.51 8.93 0 6 -8 252.19 7.80 0 6 -8 244.90 9.18 0 6 9 52.94 3.91 0 6 9 57.42 4.27 0 6 -9 55.84 4.16 0 6 9 51.47 4.08 0 6 9 53.60 3.93 0 6 -9 51.90 4.05 0 6 -9 57.66 3.28 0 6 10 30.00 2.97 0 6 -10 30.95 3.18 0 6 -10 24.75 2.78 0 -6 -10 29.97 2.50 0 6 10 28.11 3.12 0 6 10 29.69 2.98 0 6 10 25.69 2.99 0 6 10 28.56 2.95 0 6 11 0.20 1.16 0 6 11 3.29 1.41 0 -6 -11 1.37 0.78 0 6 11 1.22 1.19 0 6 11 1.56 1.11 0 6 -11 0.38 1.02 0 6 -11 0.52 0.99 0 6 11 0.17 0.90 0 6 12 111.22 6.00 0 6 12 99.56 5.63 0 6 -12 106.92 6.22 0 6 12 101.30 6.17 0 6 12 108.39 5.99 0 -6 -12 121.39 6.25 0 6 12 113.75 6.46 0 6 -12 102.15 5.75 0 6 13 306.33 11.27 0 6 13 322.33 10.72 0 6 -13 300.48 10.56 0 6 13 297.33 10.78 0 6 -13 309.92 11.34 0 6 13 310.51 11.54 0 6 13 285.00 10.47 0 -6 -13 311.91 10.93 0 6 14 97.95 5.90 0 6 -14 100.55 5.76 0 6 14 100.37 6.37 0 6 -14 96.56 6.16 0 -6 -14 101.11 6.04 0 6 14 108.44 5.87 0 6 14 105.21 6.01 0 6 14 103.80 6.38 0 6 -15 9.80 1.96 0 6 15 10.70 2.35 0 6 15 6.56 1.93 0 6 15 11.45 2.26 0 6 15 10.74 2.13 0 6 15 8.73 1.78 0 6 -15 11.35 2.27 0 6 16 563.96 16.40 0 6 16 587.97 17.61 0 6 -16 581.25 15.86 0 6 -16 589.54 17.41 0 6 16 570.52 15.63 0 6 16 587.39 16.90 0 6 16 593.05 17.32 0 6 -17 62.87 5.18 0 6 -17 69.76 4.66 0 6 17 66.75 5.37 0 6 17 57.00 4.61 0 6 17 75.11 5.53 0 6 17 62.82 4.38 0 6 17 66.74 5.15 0 6 18 88.97 5.97 0 -6 -18 73.33 5.45 0 6 18 76.73 5.35 0 6 18 82.45 6.05 0 6 18 70.38 5.43 0 6 -18 82.62 5.96 0 6 19 673.06 18.16 0 -6 -19 641.50 18.64 0 6 19 670.68 18.76 0 6 -19 670.60 19.35 0 6 19 676.18 19.58 0 6 19 653.98 18.66 0 6 20 269.02 10.77 0 6 -20 264.86 11.18 0 6 20 254.60 11.08 0 6 20 249.24 9.93 0 6 20 261.17 10.64 0 6 -21 190.34 9.15 0 6 21 185.08 8.22 0 6 21 189.64 8.83 0 6 21 185.09 9.20 0 6 21 177.21 8.44 0 6 22 78.26 5.48 0 6 22 73.79 4.94 0 6 22 86.18 6.06 0 6 22 82.56 5.44 0 6 -22 83.58 5.85 0 6 23 137.12 6.46 0 6 23 134.18 6.73 0 6 -23 129.52 7.16 0 6 23 130.86 7.36 0 6 -24 -0.20 1.37 0 -6 24 2.33 1.33 0 6 24 1.78 1.16 0 6 24 1.68 1.44 0 6 24 3.45 1.24 0 -6 25 72.12 4.37 0 6 25 73.99 5.00 0 6 -25 75.23 4.94 0 6 25 71.92 4.21 0 6 25 69.52 3.87 0 6 -26 174.72 7.20 0 6 26 169.29 7.32 0 -6 26 168.67 6.40 0 -6 -27 186.62 7.11 0 6 27 188.35 7.26 0 -6 27 183.02 6.19 0 -6 28 30.57 2.04 0 6 -28 38.37 2.72 0 -6 -28 35.80 2.70 0 6 29 72.96 3.40 0 7 0 1.62 1.11 0 7 0 3.49 1.15 0 7 0 1.03 0.88 0 7 1 635.99 16.09 0 7 -1 636.88 16.06 0 7 -1 649.21 16.27 0 7 1 656.39 16.44 0 7 1 670.59 17.10 0 7 -1 648.96 17.06 0 7 -2 24.13 2.81 0 7 -2 25.71 2.69 0 7 -2 27.81 2.97 0 7 2 21.60 2.46 0 7 -2 29.48 2.89 0 7 2 25.95 2.78 0 7 2 24.72 2.81 0 7 2 21.19 2.65 0 7 -3 54.40 4.19 0 7 -3 57.07 4.30 0 7 3 56.84 4.01 0 7 3 61.03 4.25 0 7 3 60.20 4.43 0 7 -3 55.44 3.87 0 7 3 53.90 4.06 0 7 -3 59.87 4.22 0 7 -3 51.88 3.97 0 7 -3 62.58 4.18 0 7 -4 47.54 3.75 0 7 -4 51.03 4.08 0 7 -4 43.22 3.82 0 7 4 50.98 3.95 0 7 4 45.36 3.78 0 7 -4 46.71 3.49 0 7 4 48.58 3.73 0 7 4 45.70 3.92 0 7 4 50.08 3.85 0 7 -5 9.95 1.99 0 7 5 11.17 1.93 0 7 5 7.70 1.67 0 7 -5 6.12 1.69 0 7 5 8.14 1.84 0 7 -5 6.33 1.55 0 7 5 7.77 1.81 0 7 5 9.39 1.92 0 7 -5 9.81 1.96 0 7 -5 9.14 1.63 0 7 -6 3.83 1.33 0 7 6 4.65 1.47 0 7 6 3.11 1.38 0 7 6 3.41 1.33 0 7 -6 3.97 1.48 0 7 -6 10.12 1.95 0 7 -6 4.95 1.47 0 7 6 6.59 1.70 0 7 6 2.67 1.18 0 7 -6 9.91 1.99 0 7 -6 5.22 1.30 0 7 -7 6.63 1.74 0 7 -7 7.58 1.80 0 7 -7 6.97 1.61 0 7 7 8.31 1.88 0 7 7 9.32 1.93 0 7 7 8.04 1.80 0 7 7 7.77 1.87 0 7 -7 8.62 1.54 0 7 7 9.38 2.06 0 7 -7 5.91 1.73 0 7 7 6.99 1.61 0 7 8 520.54 14.83 0 7 -8 497.58 13.88 0 7 8 495.15 15.18 0 7 8 511.04 14.86 0 7 8 534.68 15.47 0 7 8 495.95 14.31 0 7 -8 512.76 14.85 0 7 -8 489.99 12.93 0 7 8 478.65 13.80 0 7 -8 540.95 15.43 0 7 -8 533.35 15.31 0 7 9 433.11 13.57 0 7 9 449.49 13.47 0 7 9 445.51 12.89 0 7 -9 456.82 14.17 0 7 -9 419.81 13.48 0 7 9 443.49 14.19 0 7 9 469.10 14.10 0 7 -9 452.49 12.92 0 7 9 451.36 14.26 0 7 -9 452.54 14.07 0 7 10 640.72 17.17 0 7 10 622.59 17.76 0 7 10 606.96 15.91 0 -7 -10 662.73 15.68 0 7 10 644.16 18.06 0 7 -10 619.02 17.12 0 7 -10 623.14 15.99 0 7 10 650.31 17.34 0 7 -10 627.24 17.56 0 7 10 640.09 17.36 0 7 11 211.24 8.88 0 7 11 211.76 9.49 0 7 11 223.53 9.68 0 7 11 203.49 8.88 0 7 -11 208.70 9.21 0 7 11 204.90 7.91 0 7 11 211.85 8.94 0 7 -11 208.37 8.94 0 -7 -12 915.06 22.69 0 7 -12 952.20 23.23 0 7 12 935.20 22.41 0 7 12 873.50 23.04 0 7 12 885.26 22.89 0 7 -12 925.96 22.31 0 7 12 919.17 22.28 0 7 12 870.12 22.02 0 7 13 361.37 12.47 0 -7 -13 354.43 12.46 0 7 13 375.21 13.37 0 7 13 346.63 12.10 0 7 -13 358.85 12.88 0 7 13 366.48 13.14 0 7 13 357.12 12.34 0 7 -13 367.27 12.36 0 7 -14 1.22 1.32 0 7 -14 3.53 1.72 0 7 14 1.27 1.18 0 7 14 5.96 1.93 0 -7 -14 2.02 1.28 0 7 14 2.69 1.78 0 7 14 3.21 1.54 0 7 14 1.85 1.21 0 7 15 329.89 11.95 0 7 -15 322.18 11.35 0 7 15 315.12 11.60 0 7 15 324.94 12.33 0 7 15 314.99 12.29 0 7 15 312.18 11.22 0 7 -15 306.54 12.01 0 -7 -15 302.40 11.70 0 7 16 75.62 5.46 0 7 -16 71.42 4.98 0 7 16 79.43 5.28 0 7 16 79.32 5.50 0 7 16 74.23 5.74 0 7 -16 73.90 5.61 0 7 16 81.15 5.84 0 -7 -16 78.99 5.70 0 7 17 49.15 4.60 0 7 17 45.41 4.47 0 7 -17 41.99 4.28 0 7 17 44.81 4.22 0 7 17 42.91 4.06 0 7 -17 43.40 3.85 0 7 18 228.15 9.47 0 7 -18 227.83 8.74 0 7 18 215.79 10.01 0 7 18 209.86 9.66 0 7 -18 227.61 10.09 0 7 18 226.68 9.71 0 7 19 7.44 2.13 0 7 19 10.73 2.34 0 7 19 7.78 2.18 0 7 -19 9.06 2.23 0 7 19 6.58 1.92 0 7 20 11.31 2.36 0 7 20 9.23 2.07 0 7 20 8.42 2.29 0 7 20 11.24 2.30 0 7 -20 5.08 1.87 0 7 21 400.74 13.02 0 7 21 383.25 12.87 0 7 21 396.01 12.22 0 7 -21 411.14 13.64 0 7 21 400.38 13.74 0 7 -22 382.99 12.76 0 7 22 372.42 12.27 0 7 22 403.48 13.33 0 7 22 378.45 12.16 0 7 22 388.50 11.56 0 7 23 6.13 1.62 0 7 23 6.94 1.91 0 7 -23 6.99 1.83 0 7 23 7.42 1.53 0 7 -24 128.18 6.15 0 -7 24 112.32 5.39 0 7 24 120.85 5.40 0 7 24 124.53 6.22 0 -7 25 369.04 10.20 0 7 25 394.26 11.56 0 7 -25 393.05 11.26 0 7 25 361.50 9.69 0 7 -26 43.93 3.05 0 7 26 41.98 3.11 0 7 -27 36.57 2.52 0 7 27 40.59 2.74 0 7 28 303.08 7.62 0 8 0 732.65 19.10 0 8 0 746.28 19.64 0 8 0 715.43 19.46 0 8 0 724.99 18.69 0 8 0 746.46 19.02 0 8 0 773.73 20.02 0 8 0 764.13 18.88 0 8 1 625.54 17.14 0 8 -1 610.80 16.84 0 8 1 611.75 17.48 0 8 1 625.80 16.61 0 8 -1 634.91 17.58 0 8 1 652.10 18.01 0 8 -1 643.78 16.86 0 8 1 622.33 16.75 0 8 -1 643.09 17.83 0 8 -1 613.62 17.05 0 8 -1 652.40 17.75 0 8 -1 605.34 16.70 0 8 -2 13.55 2.20 0 8 -2 10.83 2.16 0 8 2 12.24 2.33 0 8 -2 11.58 2.02 0 8 -2 14.92 2.46 0 8 2 13.29 2.16 0 8 -2 10.14 2.19 0 8 2 14.04 2.26 0 8 2 13.14 2.27 0 8 -2 13.63 2.28 0 8 2 14.34 2.37 0 8 -2 12.04 2.35 0 8 -3 166.60 7.51 0 8 3 158.40 7.96 0 8 3 153.56 7.55 0 8 3 160.17 7.41 0 8 -3 148.65 7.38 0 8 -3 144.45 7.42 0 8 -3 154.01 7.74 0 8 3 157.48 7.55 0 8 -3 154.32 7.80 0 8 3 150.45 6.90 0 8 -3 162.10 7.35 0 8 -3 147.64 7.38 0 8 -4 129.44 6.80 0 8 -4 134.14 7.20 0 8 4 129.98 6.82 0 8 -4 133.04 7.03 0 8 -4 127.62 6.87 0 8 4 127.36 6.94 0 8 -4 130.31 7.15 0 8 -4 122.64 6.25 0 8 -4 124.36 6.50 0 8 4 119.90 5.97 0 8 4 125.75 7.14 0 8 4 130.38 6.69 0 8 5 58.77 4.66 0 8 -5 63.51 4.92 0 8 -5 69.08 5.01 0 8 5 63.69 4.74 0 8 5 62.83 4.86 0 8 5 54.84 3.92 0 8 5 63.22 5.05 0 8 -5 53.59 4.40 0 8 5 61.37 4.55 0 8 -5 61.35 4.89 0 8 -5 59.36 4.23 0 8 -5 59.96 4.47 0 8 -6 8.92 1.74 0 8 -6 6.26 1.77 0 8 6 5.06 1.69 0 8 6 6.39 1.94 0 8 -6 5.85 1.64 0 8 -6 4.66 1.82 0 8 6 9.10 2.04 0 8 6 8.28 1.96 0 8 6 7.32 2.04 0 8 -6 5.54 1.86 0 8 7 1896.58 38.28 0 8 -7 1954.49 38.37 0 8 -7 1947.56 39.81 0 8 7 1924.63 39.89 0 8 7 1939.50 39.97 0 8 -7 2050.29 39.57 0 8 -7 1799.75 36.39 0 8 -7 1879.15 38.94 0 8 7 1883.69 38.99 0 8 7 1922.33 38.30 0 8 -8 89.14 5.93 0 8 -8 79.80 5.56 0 8 8 83.03 5.48 0 8 8 76.29 5.16 0 8 -8 74.62 4.52 0 8 -8 80.98 5.80 0 8 8 76.89 5.48 0 8 -8 79.09 5.22 0 8 8 78.98 5.51 0 8 8 81.57 5.83 0 8 8 86.19 6.03 0 8 9 62.88 4.84 0 8 -9 68.10 5.19 0 8 9 71.77 4.94 0 8 -9 67.60 5.25 0 8 9 62.17 5.10 0 8 9 61.91 5.16 0 8 -9 65.09 4.70 0 8 9 59.19 4.87 0 8 9 65.63 5.01 0 8 -9 66.64 5.27 0 8 10 241.93 10.49 0 8 -10 230.63 9.08 0 8 10 241.04 9.27 0 8 10 254.51 10.78 0 8 10 261.39 10.49 0 8 10 246.88 10.15 0 8 -10 248.19 10.58 0 8 10 242.19 9.89 0 8 -10 244.84 10.19 0 8 -11 300.40 11.67 0 8 11 289.37 11.00 0 8 -11 281.52 9.91 0 8 11 286.60 11.30 0 8 11 289.37 11.68 0 8 11 284.01 10.04 0 8 -11 291.62 11.21 0 8 11 283.87 11.06 0 8 11 268.95 11.37 0 8 12 443.83 15.08 0 8 12 435.50 14.41 0 -8 -12 447.11 14.72 0 8 12 453.01 15.20 0 8 12 432.50 12.73 0 8 -12 439.05 14.81 0 8 12 458.36 14.53 0 8 -12 443.94 14.37 0 8 12 452.06 14.40 0 -8 -13 147.69 7.86 0 8 -13 139.92 7.87 0 8 -13 145.40 7.55 0 8 13 135.29 7.34 0 8 13 135.11 7.43 0 8 13 133.15 7.27 0 8 13 148.94 8.21 0 8 13 139.57 7.92 0 8 -14 210.47 9.17 0 8 14 210.55 9.30 0 8 14 206.64 9.75 0 8 14 207.28 9.24 0 -8 -14 209.22 9.62 0 8 14 204.83 9.80 0 8 -14 205.76 9.68 0 8 14 202.75 9.10 0 8 15 83.61 5.68 0 8 15 65.66 5.08 0 8 15 83.66 5.61 0 8 -15 80.40 5.46 0 8 -15 77.79 5.87 0 8 15 73.21 5.78 0 -8 -15 79.21 5.75 0 8 15 81.10 5.97 0 8 16 9.33 2.17 0 8 16 8.50 2.28 0 8 16 9.53 2.35 0 8 -16 6.27 2.07 0 8 -16 10.19 2.14 0 8 16 7.10 1.87 0 8 17 1519.94 32.54 0 8 17 1467.79 31.77 0 8 -17 1590.09 33.69 0 8 -17 1505.80 31.31 0 8 17 1504.50 33.28 0 8 17 1465.28 33.32 0 8 18 530.77 15.10 0 8 18 525.31 16.03 0 8 -18 542.94 16.28 0 8 18 515.03 16.27 0 8 -18 516.07 14.32 0 8 18 511.21 15.37 0 8 19 40.66 4.01 0 8 -19 46.49 3.54 0 8 19 46.82 4.29 0 8 19 39.68 3.78 0 8 -19 48.18 4.30 0 8 19 46.84 3.88 0 8 -20 257.77 10.17 0 8 20 267.29 9.29 0 8 20 248.97 9.79 0 8 20 264.08 9.84 0 8 20 281.84 10.81 0 8 21 27.67 2.97 0 8 -21 24.38 3.00 0 8 21 24.75 2.93 0 8 21 25.64 2.58 0 8 21 22.02 2.90 0 8 22 64.91 4.21 0 8 -22 64.82 4.45 0 8 22 55.88 3.42 0 8 22 70.51 4.75 0 8 23 30.18 2.68 0 -8 23 23.88 2.43 0 8 -23 32.83 3.01 0 8 23 29.95 2.97 0 8 -24 605.79 14.14 0 8 24 602.75 14.39 0 8 -25 41.96 2.85 0 8 25 41.47 2.90 0 8 26 311.85 8.11 0 8 -26 283.92 7.65 0 9 0 0.22 1.12 0 9 0 -0.21 1.12 0 9 0 1.21 1.16 0 9 0 1.91 1.49 0 9 -1 308.49 11.98 0 9 -1 288.89 10.99 0 9 -1 264.24 10.62 0 9 -1 320.64 12.02 0 9 1 305.27 11.07 0 9 -1 287.39 10.77 0 9 1 307.51 12.02 0 9 1 288.56 10.68 0 9 1 291.62 11.68 0 9 1 289.83 11.20 0 9 -1 306.57 11.54 0 9 -2 108.12 6.90 0 9 -2 121.57 6.58 0 9 -2 115.52 6.98 0 9 2 111.36 6.41 0 9 2 113.76 7.04 0 9 2 112.43 7.05 0 9 -2 114.80 6.76 0 9 2 110.11 6.66 0 9 2 125.78 6.60 0 9 -2 112.17 6.63 0 9 -2 108.29 6.37 0 9 -2 111.55 6.94 0 9 -3 5.53 2.06 0 9 3 8.17 2.13 0 9 -3 9.93 2.33 0 9 -3 14.75 2.43 0 9 -3 7.46 1.80 0 9 3 8.82 1.99 0 9 3 8.31 2.08 0 9 -3 10.33 2.27 0 9 3 8.50 1.87 0 9 -3 7.91 2.08 0 9 3 8.61 2.28 0 9 -3 10.52 2.29 0 9 3 7.71 2.09 0 9 4 167.26 7.48 0 9 -4 171.08 7.88 0 9 -4 172.59 8.41 0 9 4 171.03 8.91 0 9 -4 175.59 8.75 0 9 4 185.73 8.43 0 9 4 162.18 8.39 0 9 4 181.45 8.61 0 9 -4 184.67 8.31 0 9 -4 177.58 8.89 0 9 -4 177.12 8.47 0 9 -4 168.08 8.48 0 9 -5 11.94 2.31 0 9 5 13.13 2.67 0 9 5 22.75 3.14 0 9 -5 15.91 2.79 0 9 5 13.54 2.58 0 9 5 14.98 2.49 0 9 -5 14.17 2.69 0 9 -5 26.14 3.24 0 9 -5 13.25 2.23 0 9 5 12.41 2.09 0 9 -5 14.85 2.78 0 9 -6 927.19 24.16 0 9 -6 975.64 24.44 0 9 6 965.34 23.23 0 9 6 954.36 23.42 0 9 -6 883.58 21.63 0 9 -6 938.27 23.19 0 9 6 953.82 24.61 0 9 -6 946.92 22.84 0 9 -7 46.40 4.22 0 9 -7 47.31 4.17 0 9 -7 48.45 4.49 0 9 7 45.78 4.25 0 9 7 47.96 4.71 0 9 -7 42.10 4.41 0 9 7 50.43 4.80 0 9 -7 44.83 4.46 0 9 7 44.03 4.12 0 9 8 0.26 1.57 0 9 8 0.73 1.18 0 9 8 2.13 1.28 0 9 -8 -0.25 1.48 0 9 -8 3.96 1.70 0 9 8 0.84 1.18 0 9 -8 1.21 1.58 0 9 8 1.55 1.41 0 9 -8 1.02 1.32 0 9 -8 1.24 1.24 0 9 -9 495.35 15.68 0 9 9 484.29 14.70 0 9 -9 481.28 14.56 0 9 9 503.70 15.34 0 9 -9 534.33 16.62 0 9 9 524.46 16.65 0 9 -9 487.90 14.83 0 9 9 471.09 16.03 0 9 9 475.88 15.73 0 9 -10 145.30 7.99 0 9 -10 125.20 6.61 0 9 10 130.08 7.73 0 9 10 128.55 6.73 0 9 10 122.88 7.55 0 9 10 139.68 7.81 0 9 -10 133.49 7.01 0 9 10 126.13 7.07 0 9 -10 136.22 7.54 0 9 10 126.45 7.21 0 9 11 60.05 5.23 0 9 -11 63.17 4.75 0 9 11 64.65 5.03 0 9 -11 61.79 4.99 0 9 11 62.32 4.52 0 9 -11 66.75 5.33 0 9 11 62.50 5.39 0 -9 -11 57.93 4.99 0 9 11 59.54 4.74 0 9 11 59.63 5.07 0 9 -11 58.60 4.35 0 9 12 517.56 15.90 0 9 -12 557.54 16.97 0 9 12 531.54 16.87 0 9 12 528.85 15.80 0 9 12 504.38 16.06 0 9 -12 541.59 16.18 0 9 12 512.21 16.72 0 9 12 517.66 14.40 0 9 13 122.89 6.88 0 9 13 118.19 7.30 0 9 13 116.56 5.68 0 9 13 127.79 6.96 0 9 -13 123.71 6.93 0 9 13 111.75 7.14 0 9 -13 120.87 7.27 0 9 14 676.45 18.40 0 9 -14 690.33 18.47 0 9 14 689.16 18.44 0 9 14 679.13 19.45 0 9 14 659.66 19.41 0 9 -14 693.93 19.52 0 9 15 73.36 5.14 0 9 -15 70.96 5.51 0 9 15 83.23 5.98 0 9 15 77.80 5.68 0 9 -15 77.42 5.23 0 9 15 76.10 5.18 0 9 -16 16.85 2.78 0 9 16 16.41 2.78 0 9 16 20.04 3.14 0 9 16 16.40 2.57 0 9 16 19.91 2.83 0 9 -16 17.59 2.55 0 9 17 52.86 4.22 0 9 17 59.77 4.30 0 9 17 59.89 4.79 0 9 -17 52.60 3.98 0 9 -17 63.11 4.87 0 9 17 55.72 4.59 0 9 18 337.32 11.55 0 9 18 328.61 10.47 0 9 -18 347.49 11.72 0 9 -18 332.08 10.23 0 9 18 327.80 11.73 0 9 18 321.89 10.81 0 9 19 99.69 5.70 0 9 19 112.59 6.24 0 9 -19 105.64 4.86 0 9 19 110.51 5.68 0 9 -19 108.06 5.97 0 9 20 320.15 8.69 0 9 20 318.71 9.08 0 9 -20 338.65 9.60 0 9 20 325.08 9.64 0 9 21 2.81 1.34 0 9 -21 0.09 0.23 0 9 21 0.94 1.00 0 9 -21 1.04 1.10 0 9 22 25.30 2.58 0 9 22 24.32 2.27 0 9 -22 23.81 2.37 0 9 23 13.12 1.43 0 9 -23 9.73 1.51 0 9 23 12.90 1.70 0 -9 23 7.92 1.29 0 9 24 27.01 2.07 0 9 -24 27.12 1.97 0 10 0 210.81 9.04 0 10 0 213.90 9.69 0 10 0 217.65 10.12 0 10 0 203.57 8.99 0 10 0 179.78 8.78 0 10 0 225.06 10.12 0 10 1 1.01 1.48 0 10 1 6.19 2.11 0 10 -1 2.59 1.64 0 10 -1 4.49 1.84 0 10 -1 1.54 1.17 0 10 -1 5.90 1.98 0 10 -1 1.24 1.52 0 10 1 1.64 1.31 0 10 -1 4.89 1.53 0 10 1 2.98 1.43 0 10 1 3.25 1.66 0 10 -2 867.01 22.23 0 10 -2 884.57 21.76 0 10 -2 918.71 23.64 0 10 2 826.50 22.31 0 10 -2 913.72 23.30 0 10 2 856.56 21.31 0 10 2 902.05 22.06 0 10 2 918.24 23.91 0 10 2 855.47 23.21 0 10 -2 841.82 21.75 0 10 -2 918.37 23.02 0 10 3 52.99 4.44 0 10 -3 61.20 5.09 0 10 3 48.30 4.50 0 10 -3 63.80 4.72 0 10 -3 63.41 5.01 0 10 3 58.67 4.44 0 10 3 57.58 5.19 0 10 3 58.52 4.96 0 10 -3 57.31 4.83 0 10 -3 49.43 4.32 0 10 3 55.08 5.01 0 10 -3 67.77 5.46 0 10 4 1483.24 31.94 0 10 4 1560.25 34.40 0 10 -4 1519.40 32.85 0 10 -4 1478.81 33.46 0 10 4 1419.77 32.80 0 10 -4 1549.61 31.97 0 10 4 1560.83 33.24 0 10 4 1425.41 30.32 0 10 -4 1544.56 33.01 0 10 -4 1465.46 33.42 0 10 -4 1418.57 31.26 0 10 5 443.16 15.01 0 10 5 521.53 16.52 0 10 5 431.70 12.85 0 10 5 479.99 15.21 0 10 -5 480.98 14.44 0 10 -5 488.78 15.87 0 10 5 461.88 14.50 0 10 -5 488.58 15.30 0 10 -5 455.96 15.47 0 10 -5 474.16 15.04 0 10 6 77.13 5.94 0 10 -6 85.33 6.13 0 10 -6 86.66 6.19 0 10 6 72.24 5.59 0 10 -6 82.96 5.69 0 10 6 82.47 5.71 0 10 6 83.19 5.57 0 10 -6 73.13 5.10 0 10 -7 961.90 22.83 0 10 7 933.67 24.64 0 10 7 990.14 25.05 0 10 -7 957.92 24.65 0 10 -7 935.56 23.26 0 10 -7 958.34 24.58 0 10 7 999.76 23.85 0 10 7 987.63 23.52 0 10 8 245.57 9.84 0 10 -8 226.30 9.96 0 10 -8 242.15 10.52 0 10 8 228.27 10.48 0 10 -8 259.04 9.69 0 10 8 228.86 9.49 0 10 -8 225.23 9.35 0 10 8 232.59 10.50 0 10 -9 62.76 4.98 0 10 9 58.88 4.62 0 10 9 64.57 5.39 0 10 -9 53.81 4.28 0 10 9 57.37 5.04 0 10 9 58.59 4.52 0 10 -9 51.18 4.15 0 10 -9 62.40 5.23 0 10 10 295.94 12.04 0 10 -10 305.69 10.61 0 10 10 310.43 12.21 0 10 -10 313.63 11.62 0 10 10 313.57 10.79 0 10 10 303.99 11.05 0 10 -10 308.75 10.65 0 10 -10 314.16 11.99 0 10 11 3.37 1.75 0 10 11 2.17 1.60 0 10 11 1.34 1.19 0 10 -11 3.69 1.77 0 10 11 5.38 1.75 0 10 -11 1.56 1.22 0 10 -11 2.27 1.23 0 10 -11 3.19 1.70 0 10 12 109.58 6.10 0 10 -12 96.73 5.41 0 10 -12 108.63 6.58 0 10 12 102.67 6.53 0 10 -12 99.10 6.05 0 10 12 112.33 5.54 0 10 12 111.81 6.85 0 10 13 204.37 9.29 0 10 13 200.20 8.36 0 10 -13 211.14 8.85 0 10 13 224.97 9.68 0 10 -13 201.56 7.87 0 10 -13 227.49 9.57 0 10 -14 48.15 4.24 0 10 -14 50.47 3.67 0 10 14 51.93 3.99 0 10 14 50.92 4.43 0 10 -14 52.56 4.12 0 10 14 48.67 4.38 0 10 15 14.03 2.21 0 10 -15 14.93 2.28 0 10 15 12.59 2.43 0 10 -15 13.37 1.91 0 10 -15 13.82 2.40 0 10 15 15.52 2.64 0 10 -16 7.13 1.69 0 10 16 8.37 1.71 0 10 16 11.48 2.21 0 10 -16 11.28 2.12 0 10 16 8.98 1.97 0 10 -17 3.61 1.20 0 10 -17 4.87 1.44 0 10 17 5.30 1.54 0 10 17 3.13 1.17 0 10 17 3.20 1.41 0 10 -17 0.10 0.22 0 10 -18 17.88 1.94 0 10 -18 19.36 2.36 0 10 18 17.98 2.08 0 10 18 16.71 2.34 0 10 18 17.42 2.34 0 10 19 58.41 3.87 0 10 -19 48.13 2.70 0 10 19 55.34 3.63 0 10 -19 55.67 3.66 0 10 -20 30.01 2.55 0 10 20 29.93 2.60 0 10 20 25.49 2.31 0 10 21 52.26 3.12 0 10 -21 56.85 3.14 0 10 21 48.52 2.69 0 -10 22 73.50 3.22 0 10 22 271.45 6.25 0 11 0 1.06 1.21 0 11 0 0.23 1.33 0 11 0 -0.22 1.43 0 11 0 0.19 1.08 0 11 0 1.91 1.43 0 11 1 2.48 1.34 0 11 1 1.99 1.38 0 11 -1 3.07 1.77 0 11 1 4.07 1.75 0 11 -1 4.72 1.47 0 11 1 3.04 1.75 0 11 -1 4.50 1.97 0 11 -1 3.31 1.60 0 11 2 167.20 8.55 0 11 -2 164.39 8.05 0 11 2 165.13 7.44 0 11 -2 170.68 8.59 0 11 2 167.19 7.32 0 11 2 178.55 8.87 0 11 -2 173.62 8.01 0 11 -2 171.73 7.48 0 11 3 320.23 11.56 0 11 -3 306.41 11.79 0 11 -3 305.38 11.12 0 11 -3 314.16 11.46 0 11 -3 296.09 10.22 0 11 3 328.80 12.25 0 11 3 291.76 9.93 0 11 3 300.77 10.48 0 11 3 314.28 12.03 0 11 -4 14.03 2.19 0 11 4 13.70 2.30 0 11 -4 13.90 2.59 0 11 -4 15.36 2.60 0 11 4 9.77 1.80 0 11 4 17.05 2.92 0 11 4 11.07 2.57 0 11 4 17.36 2.81 0 11 -4 15.13 2.54 0 11 -5 4.56 1.45 0 11 -5 2.24 1.61 0 11 -5 6.04 1.85 0 11 5 3.09 1.57 0 11 5 3.30 1.39 0 11 -5 6.13 1.96 0 11 5 7.03 2.17 0 11 6 72.36 4.74 0 11 -6 73.01 4.55 0 11 -6 71.21 4.94 0 11 -6 71.30 5.10 0 11 6 72.06 5.03 0 11 6 78.74 5.68 0 11 7 45.34 4.33 0 11 -7 37.17 3.20 0 11 7 36.68 3.37 0 11 7 34.81 3.50 0 11 -7 32.44 3.35 0 11 -8 171.53 7.46 0 11 8 150.69 6.87 0 11 8 164.92 8.26 0 11 -8 152.19 6.52 0 11 8 165.90 8.22 0 11 8 167.32 7.43 0 11 9 128.95 6.21 0 11 9 152.65 7.63 0 11 9 127.75 7.06 0 11 -9 134.61 6.23 0 11 -9 138.39 6.87 0 11 9 130.91 6.16 0 11 -9 132.03 7.01 0 11 10 56.90 3.85 0 11 10 52.88 4.37 0 11 -10 59.58 3.81 0 11 -10 66.10 4.71 0 11 10 62.66 4.72 0 11 -10 57.28 4.30 0 11 10 53.46 3.71 0 11 11 48.99 3.49 0 11 11 57.43 4.49 0 11 -11 52.79 4.01 0 11 11 52.59 4.27 0 11 -11 51.23 4.08 0 11 12 4.88 1.68 0 11 -12 5.39 1.73 0 11 12 5.25 1.75 0 11 12 3.64 1.21 0 11 -12 5.74 1.71 0 11 13 9.48 1.63 0 11 13 9.46 1.96 0 11 -13 9.25 1.86 0 11 13 10.93 2.01 0 11 -13 8.90 1.77 0 11 -14 87.47 4.96 0 11 14 83.32 4.96 0 11 14 74.55 3.96 0 11 14 80.58 4.90 0 11 -14 85.75 4.63 0 11 15 73.92 4.31 0 11 -15 80.41 4.06 0 11 15 83.02 4.60 0 11 -15 83.27 4.44 0 11 16 0.25 0.30 0 11 -16 2.58 1.01 0 11 16 1.62 1.08 0 11 16 1.95 1.10 0 11 -16 1.43 0.92 0 11 -17 40.38 2.48 0 11 17 48.52 3.25 0 11 -17 44.03 3.01 0 11 17 40.67 2.90 0 11 18 7.59 1.25 0 11 18 6.52 1.27 0 11 -18 8.71 1.29 0 11 19 18.70 1.54 0 11 19 21.21 1.78 0 12 0 252.70 7.58 0 12 0 265.16 8.75 0 12 0 263.57 9.05 0 12 1 112.96 4.95 0 12 -1 106.48 5.08 0 12 1 116.72 6.09 0 12 -1 114.07 5.76 0 12 -1 116.21 6.05 0 12 -2 46.07 3.46 0 12 -2 47.81 3.94 0 12 2 45.51 3.85 0 12 2 42.27 2.96 0 12 -2 47.67 3.79 0 12 3 89.59 3.95 0 12 -3 100.98 5.09 0 12 3 109.61 5.64 0 12 3 107.27 5.79 0 12 -3 104.97 5.47 0 12 4 2.98 1.52 0 12 -4 3.71 1.35 0 12 4 -0.11 0.28 0 12 4 3.88 1.60 0 12 4 1.83 1.39 0 12 -4 2.59 1.29 0 12 -5 100.47 5.09 0 12 5 108.06 5.73 0 12 5 114.60 5.50 0 12 -5 100.31 5.08 0 12 5 106.81 5.71 0 12 6 0.21 0.23 0 12 6 0.18 1.10 0 12 6 1.66 1.22 0 12 -6 0.92 1.26 0 12 -6 2.04 1.26 0 12 -7 583.50 11.93 0 12 7 560.85 12.62 0 12 7 581.83 11.50 0 12 8 0.49 1.24 0 12 8 -0.09 0.23 0 12 9 10.49 2.00 0 12 9 13.19 2.08 0 12 10 117.09 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4909.68 76.65 -1 2 -1 1960.05 30.72 -1 -2 1 1823.95 29.80 1 2 1 1836.96 28.86 -1 2 -1 1929.17 29.83 -1 2 -2 1090.40 18.86 -1 -2 2 1100.81 18.29 1 2 2 1091.48 17.46 1 2 3 2192.37 36.40 -1 2 -3 2233.01 35.82 -1 -2 3 2289.01 35.54 1 2 3 2256.51 35.30 1 2 4 1816.92 29.66 -1 -2 4 1686.38 28.30 1 2 4 1664.63 28.00 -1 -2 4 1763.58 28.91 1 2 4 1823.25 28.65 -1 -2 5 2059.01 32.03 -1 2 -5 1954.02 30.91 1 2 5 1956.49 32.53 -1 -2 5 1943.71 31.39 1 2 5 1751.89 30.96 1 2 5 1854.23 31.46 1 2 6 1355.79 24.13 1 2 6 1313.02 23.29 1 2 6 1319.37 22.97 -1 -2 6 1320.66 23.17 1 -2 -6 1361.71 23.57 1 -2 -7 175.17 5.11 -1 2 -7 167.94 4.43 1 2 7 166.01 4.18 1 -2 -7 180.16 3.46 1 2 7 167.38 4.98 1 2 7 169.74 4.81 -1 -2 7 175.33 4.96 1 2 7 172.28 5.42 1 2 8 485.08 9.24 1 -2 -8 484.10 10.50 1 2 8 457.05 10.26 1 2 8 469.12 10.02 1 2 8 480.33 10.73 -1 -2 8 492.27 10.43 1 -2 -8 449.81 7.80 -1 2 -8 462.09 9.49 -1 2 -9 1246.07 21.20 1 2 9 1312.06 22.88 1 2 9 1240.02 20.79 1 2 9 1265.68 22.34 1 2 9 1211.11 21.87 1 -2 -9 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130.49 5.42 -1 11 14 145.45 6.50 1 11 -14 147.16 6.34 1 11 -14 156.69 6.33 -1 11 13 11.35 2.07 1 11 -13 10.17 1.91 1 11 -13 11.29 1.74 -1 11 13 10.81 1.96 1 11 -13 9.35 1.89 1 11 -12 297.26 9.45 1 11 -12 316.23 10.50 -1 11 12 304.46 10.56 1 11 -12 316.06 10.34 1 11 -11 15.70 2.21 -1 11 11 19.54 2.69 1 11 -11 17.26 2.58 1 11 -11 17.50 2.50 1 11 -11 16.13 1.98 1 11 -10 79.52 4.51 -1 11 10 82.94 5.38 1 11 -10 72.75 4.95 1 11 -10 78.44 4.76 1 11 -9 273.46 9.79 1 11 -9 300.27 9.88 -1 11 9 310.61 11.19 -1 11 9 298.25 11.14 1 11 -8 85.77 5.23 -1 11 8 92.20 5.93 1 11 -8 98.00 5.48 -1 11 8 98.16 6.12 -1 11 7 21.36 2.87 1 11 -7 18.34 2.62 1 11 -7 17.76 2.55 1 11 -7 20.30 2.89 -1 11 7 19.04 2.89 -1 11 7 21.53 3.06 1 11 -6 92.13 5.59 -1 11 6 101.51 6.33 1 11 -6 86.72 5.54 1 11 -6 94.65 5.88 -1 11 6 98.52 5.85 -1 11 6 99.13 6.27 -1 11 5 106.25 6.52 -1 11 5 97.32 5.88 -1 11 5 88.11 5.90 -1 11 5 86.98 4.66 1 11 -5 96.08 5.83 1 11 -5 97.92 5.95 1 11 -5 91.45 5.64 1 11 -4 53.97 4.48 -1 11 4 55.45 4.53 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11 -3 2.89 1.65 1 11 3 5.20 2.06 1 11 3 4.49 1.81 -1 11 -3 5.11 1.73 1 11 4 43.45 3.30 -1 11 -4 53.48 4.58 1 11 4 50.26 4.57 1 11 4 46.06 4.12 1 11 4 53.99 4.51 -1 11 -4 50.03 4.28 -1 11 -4 48.32 4.16 1 11 4 51.13 4.62 1 11 5 104.95 6.53 -1 11 -5 96.76 5.87 1 11 5 89.88 5.72 -1 11 -5 92.91 5.73 1 11 5 106.55 6.61 1 11 5 90.60 5.73 1 11 6 95.33 6.24 -1 11 -6 98.63 5.89 1 11 6 101.85 6.45 1 11 6 91.58 5.76 1 11 6 100.73 6.02 1 11 7 14.84 2.67 1 11 7 15.88 2.51 1 11 7 18.34 2.65 1 11 7 16.12 2.76 -1 11 -7 15.91 2.41 1 11 8 88.17 5.81 -1 11 -8 99.39 5.83 1 11 8 88.05 5.51 1 11 8 94.94 5.51 1 11 8 82.85 5.68 1 11 9 292.35 10.99 1 11 9 306.43 11.22 -1 11 -9 298.76 10.49 1 11 9 306.01 10.63 1 11 9 295.58 10.00 1 11 10 72.73 4.44 1 11 10 87.38 5.56 1 11 10 76.08 5.24 -1 11 -10 80.94 5.24 -1 11 -10 71.63 4.85 1 11 10 78.81 4.98 1 11 11 17.18 2.62 -1 11 -11 19.67 2.60 1 11 11 17.24 2.41 1 11 11 18.40 2.68 -1 11 -11 15.22 2.33 1 11 11 16.61 2.05 -1 11 -12 310.05 10.40 1 11 12 308.72 10.55 1 11 12 298.92 9.89 -1 11 -12 305.06 9.93 1 11 12 304.44 10.42 1 11 12 277.03 8.22 1 11 13 8.01 1.82 -1 11 -13 9.79 1.81 -1 11 -13 11.46 1.94 1 11 13 9.03 1.74 1 11 13 9.89 1.96 1 11 14 145.99 6.13 -1 11 -14 139.55 6.23 1 11 14 143.78 6.48 -1 11 -14 144.58 5.93 1 11 14 147.56 6.42 1 11 15 262.72 8.27 -1 11 -15 266.06 8.62 1 11 15 269.91 8.89 1 11 15 258.53 8.50 -1 11 -15 276.71 8.18 1 11 16 76.36 3.90 -1 11 -16 74.58 3.58 1 11 16 78.72 4.05 1 11 16 83.70 4.40 -1 11 -16 85.29 4.26 1 11 17 13.33 1.58 1 11 17 15.56 1.83 -1 11 -17 15.05 1.43 1 11 17 14.72 1.59 1 11 18 3.27 0.96 1 11 19 94.66 3.61 -1 12 15 88.03 3.61 1 12 -15 81.86 3.14 -1 12 15 78.13 3.31 1 12 -14 28.70 2.04 -1 12 14 32.01 2.26 -1 12 14 25.77 2.13 -1 12 13 90.90 4.17 1 12 -13 88.16 3.97 1 12 -12 56.27 3.30 -1 12 12 55.42 3.42 -1 12 11 30.75 2.68 1 12 -11 28.82 2.54 -1 12 10 103.79 4.86 1 12 -10 113.80 4.90 -1 12 10 114.31 5.14 -1 12 9 9.58 1.82 1 12 -9 8.54 1.38 -1 12 9 9.68 1.81 1 12 -8 148.32 5.69 -1 12 8 154.84 6.74 1 12 -8 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10 3 213.25 9.67 -2 10 3 219.16 8.89 2 10 -3 216.17 9.61 2 10 -2 403.53 13.91 2 10 -2 399.59 14.02 2 10 -2 405.28 13.71 -2 10 2 417.48 14.04 -2 10 2 388.14 12.68 2 10 -2 375.69 13.15 -2 10 2 405.19 13.60 2 10 -1 165.98 8.47 2 10 -1 145.93 7.64 2 10 -1 156.03 8.06 -2 10 1 165.19 8.32 2 10 -1 162.06 8.50 -2 10 1 161.33 7.75 -2 10 1 163.00 8.05 2 10 0 29.32 3.66 2 10 0 38.84 4.14 -2 10 0 38.77 3.99 2 10 0 36.60 3.85 -2 10 0 35.44 3.90 -2 10 0 39.30 3.84 2 10 0 35.74 3.74 -2 10 0 32.71 3.53 -2 10 -1 151.83 7.55 -2 10 -1 173.23 8.34 2 10 1 161.04 8.48 -2 10 -1 159.65 8.20 2 10 1 171.74 8.53 -2 10 -1 168.74 8.05 2 10 1 155.75 7.62 2 10 2 418.41 14.32 -2 10 -2 408.06 13.73 2 10 2 385.95 13.56 -2 10 -2 387.04 12.66 -2 10 -2 392.42 13.52 -2 10 -2 407.29 13.36 2 10 2 371.38 12.27 2 10 2 389.67 14.00 2 10 3 208.09 9.60 2 10 3 207.19 8.42 -2 10 -3 216.50 9.57 2 10 3 206.61 9.56 -2 10 -3 230.69 9.80 2 10 3 218.73 10.00 -2 10 -3 227.96 9.59 -2 10 -3 207.97 8.63 2 10 3 216.61 10.02 -2 10 -4 66.71 5.14 -2 10 -4 61.54 4.93 2 10 4 62.54 5.05 2 10 4 58.94 5.11 2 10 4 65.89 5.23 -2 10 -4 70.80 5.20 2 10 4 60.72 4.19 2 10 4 61.25 5.28 2 10 5 681.60 19.42 -2 10 -5 674.18 18.68 2 10 5 657.41 18.82 2 10 5 664.67 19.30 2 10 5 691.28 19.15 2 10 6 291.74 11.42 2 10 6 289.24 11.65 2 10 6 298.98 11.47 2 10 6 297.47 11.78 2 10 7 100.04 6.47 2 10 7 97.84 6.34 -2 10 -7 101.75 6.28 2 10 7 97.75 6.17 2 10 7 99.66 6.51 -2 10 -7 94.84 5.98 2 10 8 187.66 8.46 2 10 8 185.31 8.93 -2 10 -8 179.17 8.52 2 10 8 173.86 8.51 -2 10 -8 183.54 8.47 2 10 8 186.00 8.91 2 10 9 7.66 2.15 2 10 9 4.58 1.92 2 10 9 5.48 1.71 2 10 9 7.05 2.01 -2 10 -9 6.12 1.89 -2 10 -9 6.53 1.96 -2 10 -10 50.74 4.31 2 10 10 47.40 4.27 2 10 10 46.81 4.42 -2 10 -10 46.26 4.11 2 10 10 45.98 4.19 2 10 10 43.61 3.83 2 10 11 15.68 2.31 2 10 11 14.24 2.69 -2 10 -11 17.67 2.58 2 10 11 14.90 2.54 2 10 11 13.30 2.40 -2 10 -11 15.50 2.52 2 10 12 36.32 3.77 -2 10 -12 36.16 3.49 2 10 12 36.29 3.59 -2 10 -12 39.22 3.56 2 10 12 30.20 2.84 2 10 12 34.79 3.60 -2 10 -13 19.16 2.65 2 10 13 25.10 3.03 2 10 13 23.54 3.01 -2 10 -13 22.02 2.68 2 10 13 24.04 2.92 2 10 14 89.08 5.48 -2 10 -14 95.69 5.38 2 10 14 84.31 5.27 -2 10 -14 96.00 5.12 2 10 14 92.12 5.29 -2 10 -15 124.12 5.95 2 10 15 118.17 6.02 2 10 15 118.72 5.76 2 10 15 122.81 6.30 -2 10 -15 121.00 5.59 -2 10 -16 24.91 2.57 2 10 16 22.72 2.56 2 10 16 27.31 2.87 -2 10 -16 26.45 2.46 2 10 16 24.58 2.48 2 10 17 232.30 8.16 -2 10 -17 215.77 7.46 2 10 17 219.71 7.74 -2 10 -17 203.06 6.50 2 10 17 203.61 6.77 -2 10 -18 98.29 4.48 2 10 18 95.41 4.59 -2 10 -18 83.69 3.42 2 10 18 100.11 4.87 2 10 19 236.18 7.57 -2 10 -19 242.81 7.10 2 10 19 238.00 7.28 2 10 20 15.50 1.55 2 10 20 18.94 1.88 2 -11 18 18.63 1.48 -2 11 17 9.72 1.21 2 11 -17 14.62 1.41 -2 11 16 115.77 4.52 2 11 -16 117.17 4.57 2 11 -16 125.42 4.70 -2 11 15 73.89 3.80 2 11 -15 71.64 3.74 -2 11 15 73.67 4.14 2 11 -15 79.63 3.99 -2 11 14 65.52 4.06 2 11 -14 57.49 3.58 -2 11 14 62.99 3.71 2 11 -14 63.73 3.82 -2 11 13 10.49 1.94 2 11 -13 12.39 1.92 -2 11 13 14.58 1.99 2 11 -13 13.94 2.03 2 11 -12 46.43 3.51 -2 11 12 45.89 3.48 -2 11 12 44.61 3.64 2 11 -12 46.64 3.63 -2 11 11 3.76 1.47 2 11 -11 4.45 1.12 -2 11 11 5.18 1.48 2 11 -11 5.61 1.55 2 11 -11 7.32 1.81 -2 11 10 16.38 2.46 -2 11 10 15.76 2.35 2 11 -10 13.40 2.25 2 11 -10 13.35 1.91 2 11 -10 16.16 2.44 -2 11 9 447.76 13.34 2 11 -9 414.48 12.68 -2 11 9 425.16 12.81 2 11 -9 407.18 11.79 -2 11 8 97.23 5.70 2 11 -8 90.55 5.47 2 11 -8 100.20 5.43 -2 11 8 102.58 5.91 -2 11 7 27.23 3.08 2 11 -7 26.22 3.05 2 11 -7 24.99 2.89 2 11 -7 28.33 3.20 -2 11 7 30.53 3.29 2 11 -6 39.67 3.75 -2 11 6 40.75 3.80 2 11 -6 41.09 3.78 -2 11 6 39.14 2.88 2 11 -6 35.80 3.52 -2 11 6 35.06 3.55 -2 11 5 76.21 5.17 2 11 -5 73.44 5.13 -2 11 5 69.70 4.09 2 11 -5 70.42 4.95 2 11 -5 76.61 5.18 -2 11 5 73.58 5.07 -2 11 4 234.13 8.23 -2 11 4 226.38 9.28 2 11 -4 225.25 9.47 2 11 -4 244.27 9.44 2 11 -4 234.13 9.50 -2 11 4 234.75 9.37 2 11 -3 56.35 4.50 -2 11 3 64.72 4.74 -2 11 3 53.48 3.91 2 11 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3.29 -2 11 -7 31.42 3.30 2 11 7 31.65 3.30 2 11 7 28.71 3.34 2 11 8 107.73 6.13 2 11 8 107.16 5.95 2 11 8 97.06 5.86 -2 11 -8 97.84 5.61 2 11 8 99.42 5.52 2 11 9 404.11 12.53 2 11 9 396.78 12.70 -2 11 -9 424.60 12.44 2 11 9 402.50 11.73 2 11 9 419.60 12.86 2 11 10 12.47 2.20 2 11 10 15.15 2.31 2 11 10 14.80 2.06 -2 11 -10 15.99 2.27 2 11 10 17.26 2.47 2 11 11 6.41 1.66 2 11 11 6.34 1.32 2 11 11 4.29 1.51 2 11 11 5.82 1.66 -2 11 -11 4.16 1.44 2 11 12 46.83 3.59 2 11 12 46.60 3.67 -2 11 -12 45.37 3.40 2 11 12 43.90 3.45 2 11 13 13.77 1.92 2 11 13 12.55 1.87 2 11 13 12.14 1.96 -2 11 -13 13.68 1.89 2 11 14 66.07 3.87 2 11 14 65.86 3.96 -2 11 -14 60.93 3.48 2 11 15 74.00 3.86 -2 11 -15 68.83 3.42 2 11 15 79.64 4.12 -2 11 -16 114.70 4.08 2 11 16 115.31 4.54 2 11 16 123.64 4.94 2 11 17 11.92 1.36 2 11 17 14.36 1.58 -2 12 14 3.47 0.80 2 12 -14 4.13 0.82 -2 12 13 2.36 0.82 -2 12 13 2.90 0.73 2 12 -13 2.71 0.84 2 12 -12 224.42 6.65 -2 12 12 220.02 6.70 -2 12 11 32.93 2.33 2 12 -11 29.81 2.22 2 12 -11 36.36 2.64 -2 12 11 35.08 2.59 -2 12 10 154.14 5.63 2 12 -10 158.68 5.65 -2 12 10 165.00 6.06 -2 12 9 41.40 2.95 2 12 -9 42.63 2.93 2 12 -9 41.23 2.56 -2 12 9 44.13 3.13 -2 12 8 25.82 2.39 2 12 -8 21.20 2.25 2 12 -8 23.03 2.08 2 12 -8 22.65 2.36 -2 12 8 24.39 2.41 -2 12 7 112.12 5.17 -2 12 7 113.59 5.23 2 12 -7 104.70 5.00 2 12 -7 109.66 4.92 2 12 -7 114.67 5.26 2 12 -6 167.63 6.53 -2 12 6 176.31 6.76 -2 12 6 179.40 6.76 2 12 -6 166.47 6.60 2 12 -6 169.23 6.62 2 12 -5 121.04 5.65 -2 12 5 121.29 5.64 2 12 -5 134.09 5.89 2 12 -5 127.92 5.64 -2 12 5 134.45 5.78 2 12 -4 12.37 2.05 -2 12 4 13.52 1.96 2 12 -4 10.65 1.88 2 12 -4 12.72 1.89 -2 12 4 13.88 1.93 2 12 -3 97.68 5.14 -2 12 3 96.95 5.04 -2 12 3 84.18 4.03 2 12 -3 96.29 5.15 2 12 -3 98.40 4.85 2 12 -2 2.41 1.18 -2 12 2 3.78 1.13 2 12 -2 1.42 1.21 -2 12 2 1.23 0.97 2 12 -2 1.88 1.05 -2 12 1 185.44 7.21 2 12 -1 175.33 7.22 -2 12 1 169.94 6.39 2 12 -1 185.77 7.51 2 12 -1 171.24 6.39 -2 12 0 15.72 2.05 2 12 0 15.63 2.15 2 12 0 16.00 2.26 -2 12 0 17.41 2.14 2 12 0 11.62 1.69 2 12 0 18.22 2.45 2 12 1 187.51 7.45 2 12 1 184.70 7.25 -2 12 -1 178.97 6.78 2 12 1 162.54 5.77 2 12 2 3.83 1.18 2 12 2 3.07 1.36 -2 12 -2 1.35 1.25 2 12 3 98.34 5.10 2 12 3 96.12 5.20 -2 12 -3 91.66 4.85 2 12 3 91.73 5.08 2 12 4 11.67 1.96 2 12 4 11.58 1.91 2 12 4 8.48 1.76 -2 12 -4 12.14 1.90 -2 12 -5 139.42 5.94 2 12 5 125.70 5.78 2 12 5 123.87 5.85 2 12 5 135.94 5.99 2 12 6 170.37 6.70 2 12 6 170.30 6.83 2 12 6 169.92 6.62 2 12 7 112.95 5.21 2 12 7 104.65 5.16 2 12 7 105.18 4.86 2 12 8 22.66 2.31 2 12 8 23.02 2.36 2 12 8 26.79 2.28 -2 12 -8 23.58 2.37 2 12 9 39.71 2.89 2 12 9 40.50 3.00 2 12 9 40.11 2.59 -2 12 -9 38.31 2.87 -2 12 -10 163.25 5.79 2 12 10 153.63 5.62 2 12 10 154.45 5.76 2 12 11 33.01 2.48 2 12 11 33.06 2.39 -2 12 -11 34.49 2.49 2 12 12 193.73 6.11 2 12 12 192.98 5.85 -2 12 -12 199.84 6.03 2 12 13 2.19 0.71 -2 12 -13 2.15 0.81 2 13 -7 194.59 5.21 2 13 -6 131.22 4.12 2 13 -5 60.89 2.86 2 13 -5 56.36 2.54 2 13 -4 216.36 6.01 2 13 -4 165.34 4.84 2 13 -3 10.61 1.41 2 13 -2 42.52 2.65 2 13 -1 200.59 6.31 2 13 0 84.87 3.77 -2 13 0 56.95 2.52 -2 13 -1 148.75 4.58 -2 13 -2 31.91 2.03 2 13 3 10.03 1.36 -2 13 -3 10.13 1.24 -2 13 -4 197.22 5.71 2 13 4 205.11 6.05 -2 13 -5 65.06 2.95 2 13 5 61.92 2.90 -2 13 -6 130.52 4.31 -2 13 -7 193.79 5.41 3 0 0 1.04 0.38 -3 0 0 1.23 0.65 -3 0 0 0.43 0.48 -3 0 1 546.11 10.51 -3 0 -1 524.23 11.66 3 0 -1 522.17 10.16 -3 0 1 541.86 10.73 -3 0 -1 528.91 11.08 -3 0 1 533.64 11.76 -3 0 2 87.11 3.14 -3 0 -2 90.85 3.51 3 0 -2 80.76 2.93 -3 0 2 86.48 3.01 -3 0 -2 85.39 3.67 -3 0 2 80.14 3.63 -3 0 3 270.44 6.59 3 0 -3 252.60 6.30 -3 0 3 251.96 5.91 -3 0 -3 254.55 6.93 -3 0 3 266.79 7.40 -3 0 -3 270.70 7.34 -3 0 -4 122.44 4.66 3 0 -4 123.77 4.11 -3 0 4 127.22 4.79 3 0 4 117.31 4.53 -3 0 -4 125.64 4.56 -3 0 4 124.55 3.49 -3 0 4 127.24 4.26 3 0 5 3439.65 55.33 -3 0 5 3362.16 54.50 -3 0 5 3370.27 55.53 3 0 -5 3280.47 54.27 -3 0 5 3244.07 52.31 -3 0 -5 3296.15 55.38 -3 0 6 51.49 3.17 -3 0 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467.21 13.05 -3 0 14 441.81 13.61 -3 0 14 458.00 13.64 -3 0 14 437.07 13.47 -3 0 -14 420.08 11.88 3 0 -14 477.65 13.36 3 0 14 474.76 13.81 -3 0 -14 465.17 13.18 -3 0 15 7.04 1.76 3 0 15 4.37 1.45 -3 0 15 7.37 1.61 3 0 15 4.80 1.40 -3 0 15 5.77 1.69 -3 0 -15 5.37 1.36 3 0 -15 3.78 1.26 3 0 -15 4.51 1.48 3 0 15 6.64 1.80 -3 0 15 6.29 1.77 -3 0 15 4.72 1.61 -3 0 -15 5.77 1.62 -3 0 16 1048.57 24.14 3 0 16 1024.37 23.13 3 0 16 1048.22 23.74 3 0 16 1043.94 24.11 -3 0 16 1021.25 22.70 3 0 16 1001.82 22.90 -3 0 16 1048.32 24.73 -3 0 -16 957.92 22.13 3 0 -16 1030.61 22.47 -3 0 16 1018.53 24.38 -3 0 -16 1025.68 23.41 -3 0 16 1049.78 24.68 3 0 -16 1005.03 23.62 -3 0 17 3263.43 60.08 3 0 17 3361.03 59.34 3 0 17 3217.73 59.61 -3 0 17 3296.49 58.61 -3 0 17 3259.91 60.96 3 0 17 3237.17 58.55 -3 0 -17 3120.45 58.02 3 0 -17 3324.92 58.38 3 0 17 3272.46 60.77 -3 0 17 3238.23 60.77 -3 0 17 3341.25 61.16 3 0 -17 3474.38 60.51 -3 0 18 1347.07 30.39 3 0 18 1465.31 30.09 3 0 18 1368.92 30.08 -3 0 18 1354.94 29.02 -3 0 18 1374.59 31.16 3 0 18 1451.48 31.29 -3 0 -18 1303.34 28.61 3 0 -18 1336.35 28.74 -3 0 18 1352.46 30.78 3 0 -18 1311.04 30.03 -3 0 18 1382.47 31.14 3 0 19 1541.80 33.91 3 0 19 1561.05 32.90 3 0 19 1570.24 33.45 -3 0 -19 1588.15 32.24 -3 0 19 1488.04 31.93 -3 0 19 1594.55 34.45 -3 0 19 1551.44 34.44 3 0 -19 1495.83 31.72 -3 0 19 1498.13 33.91 3 0 -19 1486.89 33.23 3 0 20 107.48 6.44 3 0 20 98.86 6.36 -3 0 20 94.47 5.84 -3 0 20 107.39 6.91 -3 0 20 98.19 6.57 -3 0 -20 92.90 5.73 3 0 -20 109.15 6.75 3 0 -20 96.93 5.81 3 0 20 89.56 6.25 3 0 -21 20.15 2.76 3 0 21 22.33 3.17 -3 0 21 19.42 2.79 3 0 21 17.43 2.96 -3 0 21 22.02 3.31 3 0 21 17.71 2.94 -3 0 21 28.17 3.58 3 0 -21 21.96 3.20 -3 0 -21 19.20 2.72 3 0 22 104.71 6.57 3 0 22 120.07 7.11 -3 0 22 106.27 6.32 -3 0 -22 120.74 6.57 -3 0 22 101.86 6.86 3 0 -22 108.65 6.95 3 0 -22 112.78 6.32 3 0 22 107.31 7.06 -3 0 22 108.77 7.01 3 0 23 622.62 18.07 3 0 -23 591.85 16.61 -3 0 23 607.94 18.10 -3 0 -23 619.27 16.89 -3 0 -24 12.81 2.18 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176.10 7.67 3 10 -8 183.00 8.03 3 10 -7 96.84 5.90 -3 10 7 85.53 5.52 -3 10 7 87.47 4.66 -3 10 7 86.73 5.30 3 10 -7 81.65 5.66 -3 10 6 16.84 2.61 3 10 -6 12.79 2.41 -3 10 6 15.01 2.38 -3 10 6 12.36 2.05 3 10 -6 11.92 2.47 -3 10 5 316.84 11.17 3 10 -5 315.52 11.58 -3 10 5 310.77 10.85 -3 10 5 309.55 10.21 3 10 -5 306.18 11.54 -3 10 4 52.32 4.24 3 10 -4 51.52 4.53 -3 10 4 51.63 4.20 -3 10 4 54.49 4.09 3 10 -4 54.10 4.54 3 10 -3 38.24 3.98 3 10 -3 41.44 3.71 -3 10 3 39.59 3.69 -3 10 3 41.06 3.74 3 10 -3 40.19 3.98 -3 10 3 43.68 3.81 3 10 -2 104.14 6.57 -3 10 2 109.09 6.07 3 10 -2 101.22 5.85 -3 10 2 104.15 5.94 3 10 -2 103.47 6.22 -3 10 2 108.90 5.91 3 10 -1 90.61 5.52 -3 10 1 92.60 5.57 -3 10 1 97.54 5.80 3 10 -1 98.57 6.42 3 10 -1 90.17 5.70 -3 10 1 94.39 5.36 3 10 0 236.20 10.18 -3 10 0 237.80 9.30 3 10 0 234.72 9.29 -3 10 0 256.08 9.78 -3 10 0 230.56 8.38 3 10 0 216.56 9.09 -3 10 0 236.52 8.67 -3 10 -1 99.96 5.74 3 10 1 95.38 5.73 -3 10 -1 84.46 4.93 -3 10 -1 108.20 6.21 3 10 1 94.21 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22.49 1.76 -4 6 -26 25.58 1.80 4 -7 24 18.29 1.51 4 -7 23 310.06 8.20 4 -7 22 10.23 1.61 -4 7 21 99.94 5.33 4 -7 21 92.50 4.63 -4 7 20 94.54 5.48 4 -7 20 104.72 5.18 -4 7 20 88.41 4.90 4 7 -20 95.30 4.55 -4 7 19 207.78 8.65 -4 7 19 185.52 7.15 -4 7 19 180.70 7.59 4 7 -19 194.06 7.44 -4 7 18 1104.66 24.38 -4 7 18 1109.47 25.33 -4 7 17 25.11 3.23 4 -7 17 32.71 3.25 -4 7 17 22.63 2.81 -4 7 17 27.18 3.16 -4 7 16 17.87 2.86 -4 7 16 13.46 2.30 -4 7 16 14.88 2.53 -4 7 15 34.78 3.81 -4 7 15 28.50 3.26 -4 7 15 32.53 3.59 -4 7 14 314.52 11.84 -4 7 14 316.36 11.21 -4 7 14 310.60 11.64 -4 7 13 249.86 10.33 -4 7 13 225.07 9.41 -4 7 13 242.63 10.15 -4 7 12 740.69 20.27 -4 7 12 758.84 19.75 -4 7 12 790.03 20.71 -4 7 11 231.55 9.90 4 7 -11 239.76 9.52 -4 7 11 237.25 9.69 -4 -7 -11 234.67 9.98 4 -7 11 229.18 10.18 -4 7 11 247.00 10.33 -4 7 10 10.16 2.25 -4 7 10 15.55 2.53 4 7 -10 10.49 2.31 -4 -7 -10 10.59 2.29 4 -7 10 11.61 2.43 -4 7 10 13.57 2.58 -4 7 9 176.79 8.41 4 7 -9 187.94 8.65 -4 7 9 168.07 8.06 -4 -7 -9 179.15 8.61 4 -7 9 166.01 8.44 -4 7 9 180.05 8.68 -4 7 8 120.15 6.75 4 7 -8 144.14 7.60 -4 7 8 137.30 7.15 -4 -7 -8 133.50 7.34 4 -7 8 139.14 7.54 -4 7 8 127.17 7.25 -4 7 8 125.09 6.31 -4 7 7 274.27 10.54 4 7 -7 301.13 11.62 -4 7 7 295.54 10.89 -4 -7 -7 300.13 11.37 4 -7 7 279.17 11.11 -4 7 7 290.84 11.38 -4 7 7 281.08 10.01 -4 7 6 123.64 6.60 4 7 -6 133.91 7.47 -4 -7 -6 121.55 7.01 -4 7 6 133.31 7.03 4 7 -6 130.63 7.40 4 -7 6 115.22 6.80 -4 7 6 129.95 7.26 -4 7 6 119.13 6.29 -4 7 5 99.72 5.79 4 7 -5 87.60 6.16 -4 7 5 102.18 6.07 -4 -7 -5 105.76 6.51 4 7 -5 99.19 6.43 4 -7 5 103.73 6.29 -4 7 5 105.32 6.54 -4 7 5 97.39 5.78 -4 7 4 84.99 5.20 4 7 -4 91.22 6.19 -4 7 4 89.77 5.71 4 7 -4 82.14 5.82 4 -7 4 77.64 5.44 -4 7 4 91.44 6.04 -4 7 4 96.51 5.69 4 7 -3 138.40 7.76 -4 7 3 130.41 6.94 4 7 -3 143.44 7.70 4 -7 3 139.12 7.28 -4 7 3 152.05 7.82 -4 7 3 142.74 7.07 4 7 -2 66.75 5.33 -4 7 2 61.34 4.69 4 -7 2 69.22 5.01 -4 -7 -2 57.20 4.71 4 7 -2 58.56 4.84 -4 7 2 54.29 4.71 -4 7 2 61.12 4.65 4 7 -2 53.98 4.31 4 7 -1 468.09 15.40 -4 7 1 475.28 14.27 -4 -7 -1 457.37 14.56 4 7 -1 466.98 14.97 4 -7 1 448.41 14.09 -4 7 1 457.66 14.76 -4 7 1 467.40 14.12 4 7 -1 428.73 13.82 4 7 0 22.37 3.23 -4 7 0 27.24 3.10 -4 -7 0 28.53 3.34 4 7 0 27.69 3.36 4 -7 0 22.91 2.82 -4 7 0 28.85 3.43 -4 7 0 25.65 3.25 4 7 0 17.77 2.65 -4 7 -1 454.99 14.04 4 7 1 438.73 14.19 -4 -7 1 470.55 14.60 4 7 1 466.84 14.89 4 -7 -1 455.43 14.05 -4 7 -1 461.30 14.88 4 7 1 433.28 14.31 4 7 2 59.89 4.72 4 7 2 56.50 4.76 -4 7 -2 68.10 4.89 -4 -7 2 62.07 4.85 4 7 2 61.67 4.95 4 -7 -2 63.98 4.72 -4 7 -2 60.82 4.99 4 7 2 60.87 4.93 4 7 3 132.59 7.21 4 7 3 124.35 7.40 4 7 3 137.06 7.60 -4 7 -3 138.36 7.15 -4 -7 3 138.34 7.23 4 -7 -3 135.00 7.02 4 7 3 129.00 7.31 -4 7 -3 151.48 7.83 -4 7 -3 136.39 7.16 4 7 3 132.00 7.45 4 7 4 86.63 5.83 4 7 4 82.70 6.01 4 7 4 79.58 5.84 -4 7 -4 82.35 5.52 -4 -7 4 92.16 5.82 4 7 4 89.99 6.07 -4 7 -4 91.93 6.07 -4 7 -4 88.19 5.69 4 7 4 82.23 5.88 4 7 5 99.02 6.32 4 7 5 100.28 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7 -12 841.76 21.56 -4 7 -12 799.44 19.60 4 7 13 233.52 10.27 4 7 13 243.03 10.20 -4 7 -13 239.71 10.22 -4 7 -13 241.72 9.26 4 7 14 305.89 11.81 4 7 14 310.52 11.63 -4 7 -14 314.44 11.81 -4 7 -14 300.42 10.31 4 7 15 37.60 3.97 4 7 15 34.55 3.72 -4 7 -15 38.06 3.89 -4 7 -15 31.02 3.03 4 7 16 14.52 2.67 4 7 16 13.94 2.57 -4 7 -16 18.22 2.82 4 7 17 20.74 2.97 4 7 17 26.24 3.11 -4 7 -17 25.50 3.19 4 7 18 1160.01 26.49 4 7 18 1168.41 25.79 -4 7 -18 1193.15 26.36 4 7 19 200.51 8.44 4 7 19 197.09 7.94 -4 7 -19 195.51 8.19 4 7 20 97.99 5.49 4 7 20 101.26 5.24 -4 7 -20 96.80 5.34 4 7 21 92.61 5.10 4 7 21 97.76 4.87 -4 7 -21 96.30 5.06 4 7 22 8.36 1.69 4 7 23 339.23 9.40 4 7 24 21.41 1.91 -4 8 23 113.22 3.96 -4 8 22 4.28 1.02 4 8 -22 5.71 1.13 -4 8 21 43.91 2.99 4 8 -21 48.41 3.07 -4 8 20 84.88 4.53 4 -8 20 80.23 3.90 4 8 -20 89.22 4.53 4 8 -20 75.05 3.44 -4 8 19 396.79 11.56 4 -8 19 388.80 10.60 4 8 -19 400.46 10.50 -4 8 18 71.61 4.61 4 -8 18 76.01 4.25 -4 8 18 66.89 4.01 4 8 -18 74.19 4.30 -4 8 17 200.13 8.22 4 -8 17 205.39 7.55 -4 8 17 187.25 7.37 4 8 -17 204.17 7.95 -4 8 16 405.31 12.74 4 -8 16 413.46 11.90 -4 8 16 385.06 11.82 -4 8 15 11.42 2.25 -4 8 15 10.73 2.11 -4 8 14 14.45 2.46 -4 8 14 13.62 1.99 -4 8 14 16.22 2.48 -4 8 13 164.95 6.97 -4 8 13 175.91 8.03 -4 8 12 18.57 2.81 4 8 -12 26.88 2.90 -4 8 12 21.17 2.60 -4 8 12 18.31 2.80 -4 8 11 122.34 6.80 4 8 -11 117.52 6.21 -4 8 11 108.22 5.78 4 8 -11 112.72 6.83 -4 8 11 113.87 6.53 -4 8 10 66.91 5.04 4 8 -10 74.27 5.17 -4 8 10 69.67 4.65 4 8 -10 78.12 5.72 -4 8 10 71.38 5.21 -4 8 9 174.45 8.32 4 8 -9 195.70 8.77 -4 8 9 186.24 7.89 4 8 -9 193.23 9.19 -4 8 9 200.52 8.95 -4 8 8 723.19 19.02 4 8 -8 729.13 19.68 -4 8 8 699.47 18.01 4 8 -8 744.88 20.29 -4 8 8 745.24 19.66 -4 8 8 692.68 17.48 -4 8 7 433.96 13.72 4 8 -7 435.56 14.58 -4 8 7 443.76 13.27 -4 -8 -7 446.85 14.59 4 8 -7 437.14 14.80 -4 8 7 454.17 14.49 -4 8 7 430.30 12.97 -4 8 6 135.39 6.97 4 8 -6 135.70 7.67 -4 8 6 140.43 6.90 -4 -8 -6 142.38 7.72 4 8 -6 147.61 8.03 -4 8 6 136.56 7.39 -4 8 6 135.20 6.77 -4 8 5 64.92 4.63 4 8 -5 70.64 5.56 -4 8 5 58.24 4.46 4 8 -5 65.14 5.38 -4 -8 -5 59.03 4.99 -4 8 5 78.64 5.58 -4 8 5 64.43 4.69 -4 8 4 298.32 10.43 4 8 -4 296.54 11.96 -4 8 4 293.99 10.50 -4 -8 -4 311.93 11.94 4 8 -4 300.91 11.92 -4 8 4 303.96 11.56 -4 8 4 301.41 10.79 4 8 -3 366.14 13.51 -4 8 3 351.98 11.78 4 8 -3 365.14 13.27 -4 8 3 384.89 13.24 -4 8 3 371.22 12.25 -4 8 2 8.19 1.82 4 8 -2 6.13 2.21 4 8 -2 8.56 2.21 -4 8 2 15.40 2.64 -4 8 2 11.69 2.47 4 8 -1 979.06 25.06 -4 8 1 918.42 22.29 -4 -8 -1 958.25 24.23 4 8 -1 956.58 24.43 -4 8 1 974.35 24.10 -4 8 1 1015.01 23.61 4 8 0 506.68 16.30 -4 8 0 466.96 14.06 -4 -8 0 485.10 15.47 4 8 0 468.58 15.50 -4 8 0 505.17 15.59 -4 8 0 486.02 14.84 4 8 0 462.51 14.84 -4 8 -1 928.60 22.25 -4 -8 1 970.16 24.04 4 8 1 954.37 24.27 -4 8 -1 1002.75 24.23 -4 8 -1 961.14 23.29 4 8 1 897.58 23.32 4 8 2 7.96 2.05 -4 8 -2 8.85 2.07 -4 -8 2 8.96 2.15 4 8 2 8.53 2.26 -4 8 -2 9.40 2.22 4 8 3 369.38 13.54 -4 8 -3 347.14 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73.58 5.48 -4 8 -10 72.05 5.37 -4 8 -10 74.95 5.17 4 8 11 126.15 6.54 4 8 11 117.78 7.00 -4 8 -11 124.67 6.45 4 8 11 127.05 7.19 -4 8 -11 124.00 6.99 -4 8 -11 123.61 6.52 4 8 12 22.59 2.72 4 8 12 24.51 3.28 -4 8 -12 27.18 3.06 4 8 12 25.59 3.27 -4 8 -12 22.83 3.07 -4 8 -12 23.92 2.96 4 8 13 197.33 9.03 -4 8 -13 201.55 8.15 4 8 13 192.43 8.77 -4 8 -13 190.68 8.62 -4 8 -13 182.38 7.74 4 8 14 18.75 2.90 -4 8 -14 14.77 2.31 4 8 14 16.31 2.62 -4 8 -14 16.86 2.65 -4 8 -14 17.39 2.38 4 8 15 13.20 2.52 -4 8 -15 12.52 2.09 4 8 15 15.06 2.54 -4 8 -15 15.08 2.51 -4 8 -15 15.64 2.14 4 8 16 422.34 13.10 -4 8 -16 400.82 11.54 4 8 16 411.24 12.62 -4 8 -16 409.63 12.57 -4 8 -16 380.10 10.53 4 8 17 208.72 8.49 -4 8 -17 190.74 7.16 4 8 17 204.20 8.10 -4 8 -17 207.30 8.16 4 8 18 74.46 4.73 -4 8 -18 63.71 3.71 4 8 18 71.17 4.39 -4 8 -18 72.66 4.47 -4 8 -19 366.21 9.75 4 8 19 385.54 10.95 -4 8 -19 385.99 11.01 4 8 20 83.58 4.47 -4 8 -20 71.57 3.33 4 8 20 81.11 4.14 -4 8 -20 80.48 4.22 4 8 21 46.19 3.09 -4 8 -21 47.78 2.97 4 8 22 6.09 1.17 -4 8 -22 6.14 1.10 4 8 23 110.72 3.90 -4 9 20 69.34 3.21 4 9 -20 65.91 3.26 -4 9 19 56.48 3.15 4 9 -19 61.87 3.34 4 9 -19 53.82 2.55 -4 9 18 66.09 3.71 4 9 -18 67.30 3.76 4 9 -18 63.65 3.30 -4 9 17 118.35 5.37 4 -9 17 111.42 4.58 4 9 -17 121.23 5.54 4 9 -17 120.47 5.23 -4 9 16 129.20 5.53 4 -9 16 119.76 4.60 4 9 -16 127.02 5.66 4 9 -16 126.81 5.47 -4 9 15 598.52 15.17 4 -9 15 568.48 13.74 4 9 -15 602.86 15.52 -4 9 15 538.65 13.28 4 9 -15 633.02 15.59 -4 9 14 59.84 4.18 4 9 -14 61.46 4.40 -4 9 14 55.04 3.56 4 9 -14 58.85 4.31 -4 9 13 8.21 1.88 4 9 -13 8.64 2.09 -4 9 13 7.55 1.65 -4 9 12 233.36 8.91 4 9 -12 233.40 9.41 -4 9 12 219.09 8.20 4 9 -11 23.96 2.65 -4 9 11 28.54 3.11 4 9 -11 28.68 3.38 -4 9 11 26.70 2.96 -4 9 10 100.33 5.79 4 9 -10 107.80 5.77 4 9 -10 108.16 6.46 -4 9 10 102.22 5.66 -4 9 9 359.77 11.81 4 9 -9 366.86 11.99 4 9 -9 370.88 12.85 -4 9 9 362.76 11.73 -4 9 8 98.81 5.72 4 9 -8 97.26 5.97 -4 9 8 97.50 5.74 -4 9 7 41.57 3.74 4 9 -7 48.74 4.30 4 9 -7 49.22 4.54 -4 9 7 50.59 4.21 -4 9 7 49.40 3.74 -4 9 6 196.33 8.17 4 9 -6 209.87 9.35 4 9 -6 204.70 9.44 -4 9 6 212.58 8.81 -4 9 6 211.78 8.21 -4 9 5 73.20 4.70 4 9 -5 70.87 5.38 4 9 -5 74.56 5.64 -4 9 5 72.04 5.08 -4 9 5 67.62 4.63 -4 9 4 89.84 5.15 4 9 -4 93.35 6.32 4 9 -4 85.65 6.06 -4 9 4 94.39 5.84 -4 9 4 93.72 5.57 4 9 -3 8.49 2.19 4 9 -3 2.64 1.70 -4 9 3 4.88 1.80 -4 9 3 4.55 1.74 4 9 -2 13.27 2.56 4 9 -2 13.02 2.62 -4 9 2 13.58 2.47 -4 9 2 13.44 2.39 4 9 -1 182.78 9.18 4 9 -1 199.85 9.42 -4 9 1 187.44 8.58 -4 9 1 211.95 8.87 4 9 0 29.58 3.71 4 9 0 34.89 3.87 -4 9 0 31.12 3.50 -4 9 0 35.01 3.67 4 9 1 209.65 9.69 -4 9 -1 187.52 8.63 -4 9 -1 199.88 8.76 4 9 2 16.66 2.97 -4 9 -2 15.13 2.64 4 9 3 7.82 2.03 4 9 3 3.84 1.75 -4 9 -3 3.57 1.70 4 9 3 3.34 1.34 4 9 4 84.47 6.02 4 9 4 105.17 6.69 -4 9 -4 89.14 5.80 -4 9 -4 88.44 5.77 4 9 5 66.61 5.33 4 9 5 72.67 5.50 -4 9 -5 70.91 5.14 -4 9 -5 71.81 5.26 4 9 6 201.76 9.27 4 9 6 211.65 9.56 -4 9 -6 204.76 8.92 -4 9 -6 214.30 8.99 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5.87 -8 4 13 138.31 4.55 -8 4 13 153.29 5.37 -8 4 12 123.43 4.67 -8 4 12 138.98 5.36 -8 -4 -12 128.03 4.66 -8 4 11 54.33 3.67 -8 4 11 51.58 3.08 -8 4 11 57.91 3.50 -8 -4 -11 52.39 3.07 8 4 -10 31.22 2.52 -8 4 10 40.04 3.32 -8 4 10 38.30 2.78 -8 4 10 38.56 2.98 -8 -4 -10 34.24 2.61 8 4 -9 14.35 1.92 -8 4 9 15.45 2.25 -8 4 9 15.01 1.91 -8 -4 -9 14.61 1.89 -8 4 9 14.91 2.06 8 4 -8 42.73 3.33 -8 4 8 45.60 3.68 -8 4 8 43.15 3.18 -8 -4 -8 42.93 3.14 -8 4 8 38.62 3.17 8 4 -7 52.75 3.89 -8 4 7 54.53 4.09 -8 4 7 51.61 3.58 -8 -4 -7 57.07 3.72 -8 4 7 50.23 3.67 8 4 -6 134.69 6.49 -8 4 6 137.25 6.60 -8 4 6 135.25 5.98 -8 -4 -6 124.45 5.72 -8 4 6 127.05 6.03 8 4 -5 183.34 7.87 -8 4 5 174.10 7.63 -8 4 5 162.30 6.81 -8 -4 -5 166.59 6.81 -8 4 5 166.42 6.99 -8 4 4 8.11 2.02 8 4 -4 8.46 2.05 -8 4 4 5.53 1.53 -8 -4 -4 6.65 1.70 -8 4 4 8.08 1.80 8 4 -3 65.60 4.82 -8 4 3 67.64 4.75 -8 4 3 70.01 4.37 -8 -4 -3 71.75 4.42 -8 4 3 66.40 4.38 8 4 -2 68.50 4.97 -8 4 2 74.30 4.97 -8 4 2 70.73 4.48 -8 -4 -2 74.84 4.55 -8 4 2 72.24 4.55 8 4 -1 38.64 3.77 -8 4 1 33.43 3.46 -8 4 1 35.94 3.20 -8 -4 -1 36.47 3.21 -8 4 1 35.17 3.21 -8 4 0 17.16 2.59 8 4 0 15.37 2.60 -8 -4 0 14.72 2.17 -8 4 0 15.35 2.24 -8 4 0 13.79 2.15 -8 4 -1 37.84 3.59 -8 -4 1 35.72 3.19 -8 4 -1 33.28 3.14 -8 4 -1 32.42 3.10 -8 4 -2 66.07 4.69 -8 -4 2 71.30 4.45 -8 4 -2 64.66 4.27 -8 4 -2 69.87 4.40 8 4 3 73.35 5.05 -8 4 -3 70.39 4.78 -8 -4 3 68.82 4.39 -8 4 -3 68.96 4.33 -8 4 -3 74.65 4.48 -8 4 -4 6.35 1.82 8 4 4 7.39 1.94 -8 -4 4 6.80 1.74 -8 4 -4 7.18 1.72 -8 4 -4 5.70 1.53 8 4 5 175.63 7.69 -8 4 -5 176.01 7.54 -8 -4 5 159.80 6.76 -8 4 -5 167.83 6.82 -8 4 -5 164.63 6.71 8 4 6 128.78 6.40 -8 4 -6 129.28 6.33 -8 -4 6 141.75 6.13 -8 4 -6 124.82 5.70 -8 4 -6 126.17 5.72 8 4 7 57.86 4.10 -8 4 -7 53.93 3.98 -8 -4 7 52.49 3.63 -8 4 -7 52.15 3.55 -8 4 -7 52.74 3.52 8 4 8 43.01 3.39 -8 4 -8 43.17 3.46 -8 -4 8 39.43 3.07 -8 4 -8 36.37 2.91 -8 4 -8 37.91 2.92 8 4 9 14.22 1.98 -8 4 -9 15.32 2.15 -8 -4 9 15.21 1.94 -8 4 -9 12.24 1.73 -8 4 -9 14.09 1.84 8 4 10 34.14 2.63 -8 4 -10 41.00 3.22 -8 -4 10 31.17 2.58 -8 4 -10 32.56 2.53 -8 4 -10 34.87 2.57 -8 4 -11 55.48 3.50 -8 -4 11 50.62 2.97 -8 4 -11 55.61 3.07 -8 4 -11 50.35 2.82 -8 -4 12 131.16 4.80 -8 4 -12 130.11 4.73 -8 4 -12 127.60 4.51 -8 -4 13 129.85 4.46 -8 4 -13 130.30 4.43 -8 4 -14 85.75 3.87 -8 4 -15 29.67 2.06 -8 4 -16 73.01 2.96 -8 5 14 16.10 1.45 -8 5 13 54.05 2.85 -8 5 12 54.79 3.21 -8 5 12 49.94 2.90 -8 5 11 43.44 3.05 -8 5 11 45.50 2.93 -8 5 10 172.92 6.44 -8 5 10 169.15 6.08 8 5 -9 149.56 5.48 -8 5 9 161.67 6.45 -8 5 9 151.26 5.95 8 5 -8 87.20 4.34 -8 5 8 94.75 4.96 -8 5 8 88.21 4.55 8 5 -7 182.56 6.91 -8 5 7 184.58 7.32 -8 5 7 182.72 6.95 8 5 -6 75.34 4.48 -8 5 6 79.18 4.71 -8 5 6 71.10 4.23 8 5 -5 63.73 4.22 -8 5 5 65.23 4.39 -8 5 5 61.37 4.01 8 5 -4 80.89 4.74 -8 5 4 77.82 4.65 -8 5 4 78.37 4.38 8 5 -3 111.18 5.69 -8 5 3 106.48 5.48 -8 5 3 102.24 5.10 -8 5 2 3.17 1.44 8 5 -2 5.26 1.71 -8 5 2 2.34 0.92 -8 5 2 3.85 1.48 8 5 -1 40.81 3.65 -8 5 1 39.50 3.47 -8 5 1 31.85 2.49 -8 5 1 37.55 3.23 -8 5 0 6.53 1.70 8 5 0 6.81 1.93 -8 5 0 2.28 1.00 -8 5 0 5.18 1.58 -8 5 -1 38.71 3.46 -8 5 -1 34.14 2.56 -8 5 -1 38.50 3.20 -8 5 -2 3.80 1.40 -8 5 -2 3.76 1.14 -8 5 -2 3.32 1.36 8 5 3 100.53 5.45 -8 5 -3 115.50 5.73 -8 5 -3 104.14 5.12 8 5 4 83.06 4.85 -8 5 -4 78.24 4.60 -8 5 -4 74.54 4.18 8 5 5 59.70 4.03 -8 5 -5 65.61 4.19 -8 5 -5 62.07 3.75 8 5 6 78.14 4.58 -8 5 -6 79.58 4.62 -8 5 -6 76.53 4.24 8 5 7 187.46 7.05 -8 5 -7 192.69 7.34 -8 5 -7 180.86 6.65 8 5 8 90.36 4.49 -8 5 -8 90.56 4.75 -8 5 -8 87.20 4.28 8 5 9 159.05 5.69 -8 5 -9 163.51 6.38 -8 5 -9 155.20 5.70 -8 5 -10 170.68 6.25 -8 5 -10 164.61 5.57 -8 5 -11 43.03 2.94 -8 5 -11 37.13 2.41 -8 5 -12 54.62 3.14 -8 5 -12 45.49 2.44 -8 5 -13 57.91 3.04 -8 5 -14 15.31 1.49 -8 6 12 4.12 0.87 -8 6 12 3.92 0.83 -8 6 11 219.92 6.37 -8 6 11 216.98 6.26 -8 6 10 82.05 3.80 -8 6 10 82.69 3.72 -8 6 9 36.53 2.63 -8 6 9 35.75 2.52 -8 6 8 10.54 1.62 8 6 -8 8.38 1.25 -8 6 8 11.62 1.69 8 6 -7 34.01 2.53 -8 6 7 38.67 2.92 -8 6 7 35.24 2.73 8 6 -6 74.84 3.97 -8 6 6 77.13 4.07 8 6 -5 1.13 1.10 -8 6 5 1.45 1.04 8 6 -4 83.48 4.49 -8 6 4 71.64 4.13 8 6 -3 48.68 3.53 -8 6 3 42.84 3.21 8 6 -2 135.98 6.06 -8 6 2 133.92 5.78 8 6 -1 32.40 3.03 -8 6 1 32.59 2.82 8 6 0 254.00 8.82 -8 6 0 256.55 8.39 -8 6 -1 39.83 3.08 -8 6 -2 139.39 5.84 8 6 3 45.92 3.43 -8 6 -3 46.08 3.26 8 6 4 80.50 4.44 -8 6 -4 85.74 4.34 8 6 5 1.27 1.02 -8 6 -5 0.69 0.95 8 6 6 78.54 4.05 -8 6 -6 72.52 3.83 8 6 7 34.35 2.55 -8 6 -7 35.62 2.62 8 6 8 10.48 1.35 -8 6 -8 11.76 1.54 -8 6 -9 31.30 2.24 -8 6 -10 70.93 3.19 -8 6 -11 207.08 5.57 -8 7 9 52.04 2.50 -8 7 8 179.03 5.20 -8 7 8 182.13 5.43 -8 7 7 103.57 3.95 -8 7 7 116.88 4.29 8 7 -6 10.02 1.27 -8 7 6 10.10 1.35 -8 7 6 11.49 1.46 8 7 -5 183.62 5.81 -8 7 5 178.69 5.86 -8 7 5 192.79 6.12 8 7 -4 66.23 3.42 -8 7 4 72.99 3.55 -8 7 4 72.61 3.60 8 7 -3 56.07 3.23 -8 7 3 53.12 3.08 -8 7 3 54.90 3.21 -8 7 2 1.39 0.86 8 7 -2 0.97 0.94 -8 7 2 1.11 0.97 8 7 -1 98.16 4.52 -8 7 1 102.96 4.43 -8 7 1 93.21 4.27 8 7 0 258.78 8.01 -8 7 0 266.21 7.84 -8 7 0 275.44 7.94 -8 7 -1 96.80 4.30 -8 7 -1 97.98 4.33 -8 7 -2 1.10 0.86 -8 7 -2 0.49 0.85 8 7 3 56.85 3.24 -8 7 -3 55.98 3.15 -8 7 -3 52.08 3.06 8 7 4 73.60 3.62 -8 7 -4 72.00 3.54 -8 7 -4 72.79 3.56 8 7 5 180.13 5.76 -8 7 -5 189.20 5.94 -8 7 -5 179.97 5.80 8 7 6 8.94 1.21 -8 7 -6 11.76 1.43 -8 7 -6 12.35 1.43 -8 7 -7 110.53 4.11 -8 7 -7 109.16 4.02 -8 7 -8 193.76 5.45 -8 7 -8 179.00 5.21 8 8 0 6.32 0.94 9 0 0 0.32 1.10 -9 0 0 2.05 1.24 9 0 -1 64.14 4.27 -9 0 1 64.47 4.14 -9 0 -1 64.55 4.16 9 0 -2 5.91 1.57 -9 0 2 10.55 1.85 -9 0 -2 7.20 1.66 9 0 3 127.03 6.04 9 0 -3 134.44 6.10 -9 0 3 129.97 5.92 -9 0 -3 132.95 5.97 9 0 4 30.82 2.86 9 0 -4 34.20 2.96 -9 0 4 31.35 2.92 -9 0 -4 30.97 2.84 9 0 5 0.83 1.13 9 0 -5 1.48 1.14 -9 0 5 1.08 1.11 -9 0 -5 1.61 1.13 9 0 6 56.25 3.57 9 0 -6 59.22 3.65 -9 0 6 61.93 3.83 -9 0 -6 66.97 3.98 9 0 -7 11.65 1.63 9 0 7 8.77 1.45 -9 0 7 10.90 1.79 -9 0 -7 10.48 1.75 9 0 8 6.40 1.26 -9 0 8 10.03 1.69 -9 0 -8 8.86 1.55 9 0 -9 3.88 0.87 -9 0 9 4.78 1.24 -9 0 -9 6.08 1.35 -9 0 10 0.60 0.78 -9 0 -10 0.10 0.74 -9 0 11 48.78 2.83 -9 0 -11 50.59 2.88 -9 0 12 114.83 4.23 -9 0 -12 114.99 4.22 -9 0 13 34.77 2.04 -9 0 -13 34.73 2.02 -9 1 12 36.58 2.20 -9 -1 -12 37.95 2.24 -9 1 11 302.98 8.01 -9 -1 -11 305.79 7.98 -9 1 10 17.51 1.82 -9 -1 -10 19.57 1.90 -9 1 9 80.18 3.79 -9 -1 -9 81.96 3.84 9 1 -8 25.79 2.05 -9 1 8 20.09 1.64 -9 1 8 26.42 2.38 -9 -1 -8 28.37 2.43 9 1 -7 187.71 6.26 -9 1 7 194.53 6.73 -9 -1 -7 207.98 6.90 9 1 -6 115.71 5.03 -9 1 6 101.81 4.04 -9 1 6 115.35 5.19 -9 -1 -6 108.69 5.03 -9 1 5 2.35 0.86 9 1 -5 3.55 1.26 9 -1 5 3.13 1.32 -9 1 5 3.14 1.26 -9 -1 -5 2.60 1.30 -9 1 4 158.43 5.47 9 -1 4 159.37 6.68 -9 1 4 157.90 6.46 -9 -1 -4 174.03 6.74 -9 1 3 135.40 5.04 9 1 -3 148.66 6.34 -9 1 3 148.18 6.24 -9 -1 -3 146.29 6.19 -9 1 2 45.61 2.84 9 1 -2 49.77 3.70 -9 -1 -2 46.00 3.48 -9 1 1 76.96 3.73 9 1 -1 88.70 4.97 -9 -1 -1 90.81 4.86 -9 1 0 17.27 1.84 9 1 0 21.46 2.59 -9 -1 0 21.04 2.47 -9 1 -1 75.28 3.65 -9 -1 1 84.46 4.70 -9 1 -2 40.74 2.62 9 -1 -2 45.43 3.56 -9 -1 2 46.41 3.52 9 1 3 157.18 6.61 9 -1 -3 146.37 6.37 -9 -1 3 143.78 6.22 9 1 4 168.96 6.79 9 -1 -4 174.05 6.92 -9 -1 4 167.55 6.67 9 1 5 3.10 1.24 9 -1 -5 2.39 1.17 -9 -1 5 3.67 1.31 9 1 6 105.21 4.94 9 -1 -6 114.18 5.04 -9 -1 6 108.73 5.08 9 1 7 174.76 6.26 9 -1 -7 177.96 6.26 -9 -1 7 198.72 6.88 -9 1 -7 188.67 6.72 9 -1 -8 23.75 2.03 -9 -1 8 28.96 2.51 -9 1 -8 26.11 2.35 -9 -1 9 77.68 3.80 -9 1 -9 78.67 3.78 -9 -1 10 15.28 1.74 -9 1 -10 17.97 1.82 -9 -1 11 306.83 7.98 -9 1 -11 298.70 7.91 -9 -1 12 36.85 2.22 -9 1 -12 38.02 2.24 -9 2 11 14.21 1.36 -9 -2 -11 12.76 1.31 -9 2 10 46.90 2.62 -9 -2 -10 47.69 2.65 -9 2 9 20.91 1.71 -9 2 9 25.69 2.07 -9 -2 -9 23.57 2.00 9 2 -8 132.76 4.42 -9 2 8 139.42 4.54 -9 2 8 153.44 5.19 -9 -2 -8 147.59 5.08 -9 2 7 4.20 1.02 9 2 -7 2.75 0.97 9 -2 7 2.66 1.02 -9 2 7 2.41 0.98 -9 -2 -7 2.00 0.98 9 2 -6 28.75 2.42 -9 2 6 23.49 2.10 9 -2 6 19.73 2.15 -9 2 6 25.36 2.34 -9 -2 -6 26.40 2.39 9 2 -5 78.14 4.16 -9 2 5 76.49 3.73 -9 2 5 80.77 4.16 -9 -2 -5 84.52 4.25 -9 2 4 11.06 1.61 9 2 -4 9.34 1.72 -9 -2 -4 14.44 1.89 -9 2 4 9.81 1.66 9 2 -3 27.09 2.67 -9 2 3 22.60 2.18 -9 2 3 26.63 2.50 -9 -2 -3 27.02 2.54 9 2 -2 42.24 3.32 -9 2 2 41.90 2.88 -9 2 2 42.78 3.17 -9 -2 -2 39.41 3.03 9 2 -1 58.73 3.93 -9 2 1 51.29 3.21 -9 2 1 56.52 3.63 -9 -2 -1 55.18 3.61 9 2 0 138.37 6.14 -9 2 0 131.51 5.24 -9 -2 0 126.69 5.62 -9 2 0 131.07 5.70 -9 2 -1 54.20 3.24 -9 -2 1 61.54 3.83 -9 2 -1 54.18 3.55 -9 2 -2 40.83 2.79 -9 -2 2 41.45 3.12 -9 2 -2 38.18 2.99 9 2 3 27.45 2.72 -9 2 -3 25.68 2.23 -9 -2 3 24.04 2.45 -9 2 -3 26.81 2.52 -9 2 -4 11.38 1.52 9 2 4 8.83 1.70 -9 -2 4 10.12 1.68 -9 2 -4 10.33 1.68 9 2 5 78.29 4.20 -9 2 -5 75.74 3.59 -9 -2 5 79.59 4.16 -9 2 -5 80.95 4.15 9 2 6 29.99 2.49 -9 2 -6 22.83 1.92 9 -2 -6 29.74 2.48 -9 -2 6 26.73 2.43 -9 2 -6 26.42 2.35 -9 2 -7 2.37 0.79 9 2 7 4.73 1.21 9 -2 -7 3.31 1.08 -9 -2 7 3.16 1.06 -9 2 -7 2.19 1.05 9 2 8 110.14 4.32 9 -2 -8 113.52 4.36 -9 2 -8 128.30 4.20 -9 -2 8 144.91 5.20 -9 2 -8 152.46 5.29 -9 -2 9 24.49 2.02 -9 2 -9 20.72 1.88 -9 -2 10 48.31 2.66 -9 2 -10 51.57 2.72 -9 -2 11 14.58 1.40 -9 2 -11 15.05 1.42 -9 3 9 99.19 3.72 -9 3 8 29.91 2.12 -9 3 8 30.79 1.99 -9 -3 -8 30.36 1.97 9 3 -7 116.84 4.15 -9 3 7 112.71 4.20 -9 3 7 108.62 3.92 -9 -3 -7 113.28 3.98 9 3 -6 463.81 10.85 -9 3 6 443.87 10.68 -9 3 6 451.03 10.43 -9 -3 -6 427.90 10.23 9 3 -5 105.97 4.61 -9 3 5 98.16 4.29 -9 3 5 102.83 4.23 -9 -3 -5 97.84 4.16 9 3 -4 357.37 9.87 -9 3 4 361.62 9.46 -9 3 4 350.22 9.14 -9 -3 -4 341.76 9.08 -9 3 3 119.82 4.96 -9 3 3 124.45 4.90 -9 -3 -3 117.34 4.78 9 3 -2 191.76 6.93 -9 3 2 178.69 6.25 -9 3 2 174.91 6.07 -9 -3 -2 180.45 6.17 -9 3 1 5.91 1.29 9 3 -1 7.52 1.63 -9 3 1 8.76 1.38 -9 -3 -1 8.19 1.42 -9 3 0 12.56 1.72 9 3 0 10.25 1.83 -9 3 0 14.47 1.69 -9 3 -1 6.49 1.33 -9 -3 1 6.75 1.27 -9 3 -1 6.88 1.29 -9 3 -2 172.29 6.05 -9 -3 2 165.98 5.92 -9 3 -2 179.45 6.05 9 3 3 134.00 5.58 -9 3 -3 123.08 4.92 -9 -3 3 119.39 4.82 -9 3 -3 114.62 4.70 9 3 4 381.78 10.19 -9 3 -4 352.72 9.32 -9 -3 4 359.18 9.30 -9 3 -4 356.93 9.30 9 3 5 104.00 4.59 -9 3 -5 95.31 4.14 -9 -3 5 100.67 4.22 -9 3 -5 103.47 4.24 9 3 6 435.81 10.76 -9 3 -6 464.85 10.55 -9 -3 6 446.60 10.37 -9 3 -6 428.70 10.24 -9 3 -7 111.03 4.12 -9 -3 7 116.12 4.16 -9 3 -7 108.98 4.06 -9 3 -8 30.57 2.00 -9 -3 8 29.05 1.95 -9 3 -8 32.04 2.01 -9 4 8 109.60 3.89 -9 4 7 100.44 3.87 -9 4 6 1.47 0.80 9 4 -6 1.26 0.70 9 4 -5 30.53 2.20 -9 4 5 29.67 2.20 9 4 -4 16.23 1.73 -9 4 4 18.43 1.82 9 4 -3 42.37 2.80 -9 4 3 39.53 2.64 9 4 -2 40.92 2.83 -9 4 2 41.70 2.73 9 4 -1 9.89 1.53 -9 4 1 7.51 1.32 9 4 0 44.83 2.99 -9 4 0 44.83 2.85 -9 4 -1 9.10 1.37 -9 4 -2 43.05 2.73 9 4 3 43.45 2.86 -9 4 -3 40.02 2.58 9 4 4 17.91 1.86 -9 4 -4 16.79 1.70 9 4 5 30.67 2.20 -9 4 -5 27.57 2.08 -9 4 -6 1.86 0.70 9 4 6 0.98 0.66 -9 4 -7 101.85 3.75 -9 5 5 9.59 1.16 9 5 -4 108.88 3.81 -9 5 4 109.02 3.93 9 5 -3 38.10 2.28 -9 5 3 35.63 2.20 9 5 -2 39.13 2.42 -9 5 2 40.42 2.37 9 5 -1 369.97 8.98 -9 5 1 357.14 8.73 9 5 0 19.11 1.85 -9 5 0 19.01 1.69 -9 5 -1 366.25 8.78 9 5 2 37.77 2.36 -9 5 -2 39.33 2.33 9 5 3 35.05 2.20 -9 5 -3 35.86 2.18 9 5 4 103.65 3.75 -9 5 -4 111.44 3.90 -9 5 -5 11.36 1.21 0 0 0 0.00 0.00 TITL liwei_ycyl_18_181219 in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 7.777530 10.892866 25.975450 90.0000 90.0000 90.0000 ZERR 62.00 0.000045 0.000057 0.000148 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H O UNIT 62.00 62.00 62.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 58073 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.169 _oxdiff_exptl_absorpt_empirical_full_min 0.849 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn O14 O 0.06433(16) 0.62665(11) 0.79035(5) 0.0166(3) Uani 1 1 d . O20 O 0.24450(17) 0.76423(11) 0.75729(5) 0.0184(3) Uani 1 1 d . O33 O 0.77554(16) 0.61781(13) 0.67356(5) 0.0207(3) Uani 1 1 d . O32 O 0.54219(18) 0.78859(12) 0.62378(5) 0.0208(3) Uani 1 1 d . O25 O 0.34061(18) 0.38802(11) 0.58214(5) 0.0186(3) Uani 1 1 d . O22 O 0.68023(18) 0.39971(12) 0.62201(5) 0.0189(3) Uani 1 1 d . O30 O 0.50868(19) 0.72056(12) 0.54305(5) 0.0211(3) Uani 1 1 d . O19 O -0.18039(19) 0.37530(12) 0.90683(5) 0.0217(3) Uani 1 1 d . O24 O 0.72043(19) 0.51183(13) 0.55054(5) 0.0228(3) Uani 1 1 d . O27 O 0.2272(2) 0.38496(14) 0.50247(6) 0.0355(4) Uani 1 1 d . C29 C 0.5196(2) 0.70646(16) 0.59377(7) 0.0153(3) Uani 1 1 d . C5 C 0.4800(2) 0.56860(15) 0.66846(7) 0.0149(3) Uani 1 1 d . C10 C 0.3339(2) 0.54157(15) 0.69383(7) 0.0148(3) Uani 1 1 d . C13 C 0.2105(2) 0.65829(16) 0.76575(6) 0.0144(3) Uani 1 1 d . C7 C 0.3316(2) 0.52112(16) 0.58237(7) 0.0161(3) Uani 1 1 d . H7 H 0.328693 0.551780 0.546912 0.019 Uiso 1 1 calc R C3 C 0.6165(2) 0.64249(17) 0.75118(7) 0.0171(4) Uani 1 1 d . H3A H 0.568917 0.724623 0.753531 0.020 Uiso 1 1 calc R H3B H 0.728049 0.642983 0.767860 0.020 Uiso 1 1 calc R C2 C 0.4979(2) 0.55270(16) 0.77929(7) 0.0157(3) Uani 1 1 d . H2 H 0.550743 0.471193 0.777177 0.019 Uiso 1 1 calc R C1 C 0.3198(2) 0.54493(15) 0.75244(7) 0.0149(3) Uani 1 1 d . C12 C 0.2130(2) 0.43784(16) 0.77510(7) 0.0163(4) Uani 1 1 d . H12A H 0.195476 0.374524 0.749370 0.020 Uiso 1 1 calc R H12B H 0.271785 0.401910 0.804380 0.020 Uiso 1 1 calc R C16 C -0.0200(2) 0.45814(16) 0.84445(7) 0.0164(3) Uani 1 1 d . C34 C 0.4879(3) 0.58730(18) 0.83605(7) 0.0200(4) Uani 1 1 d . H34A H 0.601376 0.587433 0.850568 0.030 Uiso 1 1 calc GR H34B H 0.417716 0.528690 0.853958 0.030 Uiso 1 1 calc GR H34C H 0.438180 0.667587 0.839394 0.030 Uiso 1 1 calc GR C21 C 0.6474(2) 0.49351(16) 0.59067(7) 0.0163(3) Uani 1 1 d . C9 C 0.1693(2) 0.51229(17) 0.66547(7) 0.0176(4) Uani 1 1 d . H9A H 0.073100 0.547990 0.683927 0.021 Uiso 1 1 calc R H9B H 0.153169 0.424005 0.664778 0.021 Uiso 1 1 calc R C18 C -0.0426(3) 0.43192(17) 0.92925(7) 0.0210(4) Uani 1 1 d . H18 H -0.021730 0.434321 0.964494 0.025 Uiso 1 1 calc R C15 C -0.1630(3) 0.39277(17) 0.85512(7) 0.0193(4) Uani 1 1 d . H15 H -0.239465 0.363537 0.830482 0.023 Uiso 1 1 calc R C6 C 0.4942(2) 0.57048(15) 0.61017(7) 0.0154(3) Uani 1 1 d . C4 C 0.6382(2) 0.60901(16) 0.69599(7) 0.0166(4) Uani 1 1 d . C11 C 0.0395(2) 0.49298(16) 0.79184(7) 0.0163(4) Uani 1 1 d . H11 H -0.048854 0.470033 0.766733 0.020 Uiso 1 1 calc R C8 C 0.1703(2) 0.56089(17) 0.61053(7) 0.0178(4) Uani 1 1 d . H8A H 0.070063 0.530453 0.592360 0.021 Uiso 1 1 calc R H8B H 0.164305 0.649823 0.611087 0.021 Uiso 1 1 calc R C26 C 0.2843(3) 0.33114(18) 0.53901(7) 0.0214(4) Uani 1 1 d . C23 C 0.8125(3) 0.31596(16) 0.60505(8) 0.0204(4) Uani 1 1 d . H23A H 0.765441 0.260359 0.580075 0.031 Uiso 1 1 calc GR H23B H 0.854876 0.270286 0.634001 0.031 Uiso 1 1 calc GR H23C H 0.905055 0.361532 0.589814 0.031 Uiso 1 1 calc GR C17 C 0.0587(3) 0.48369(17) 0.89332(7) 0.0206(4) Uani 1 1 d . H17 H 0.159672 0.527370 0.899000 0.025 Uiso 1 1 calc R C31 C 0.5379(3) 0.84422(18) 0.52411(8) 0.0249(4) Uani 1 1 d . H31A H 0.523606 0.845639 0.487407 0.037 Uiso 1 1 calc GR H31B H 0.652638 0.869521 0.532678 0.037 Uiso 1 1 calc GR H31C H 0.456832 0.899258 0.539724 0.037 Uiso 1 1 calc GR C28 C 0.3015(3) 0.19507(18) 0.54425(8) 0.0294(5) Uani 1 1 d . H28A H 0.420629 0.174048 0.548323 0.044 Uiso 1 1 calc GR H28B H 0.256893 0.155925 0.513956 0.044 Uiso 1 1 calc GR H28C H 0.238173 0.167830 0.573839 0.044 Uiso 1 1 calc GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O14 0.0165(6) 0.0148(6) 0.0185(6) 0.0013(5) 0.0033(5) 0.0010(5) O20 0.0207(6) 0.0155(6) 0.0190(6) 0.0008(5) 0.0007(5) -0.0003(5) O33 0.0149(6) 0.0260(7) 0.0213(6) -0.0006(5) 0.0021(5) -0.0004(5) O32 0.0246(7) 0.0171(6) 0.0206(7) -0.0014(5) -0.0012(5) -0.0015(5) O25 0.0267(7) 0.0140(6) 0.0152(6) -0.0012(5) -0.0029(5) -0.0015(5) O22 0.0216(6) 0.0163(6) 0.0189(6) 0.0026(5) 0.0039(5) 0.0045(5) O30 0.0310(7) 0.0161(6) 0.0163(6) 0.0021(5) 0.0015(6) -0.0008(6) O19 0.0237(7) 0.0232(6) 0.0183(6) 0.0026(5) 0.0032(5) -0.0027(6) O24 0.0276(7) 0.0226(7) 0.0183(6) 0.0027(5) 0.0071(5) 0.0056(6) O27 0.0590(11) 0.0237(7) 0.0239(7) -0.0020(6) -0.0185(7) -0.0005(8) C29 0.0139(8) 0.0170(8) 0.0151(8) -0.0007(7) 0.0021(6) 0.0018(7) C5 0.0171(8) 0.0131(7) 0.0143(8) -0.0013(6) -0.0013(7) 0.0022(7) C10 0.0158(8) 0.0114(7) 0.0172(8) -0.0007(6) -0.0017(7) 0.0017(7) C13 0.0161(8) 0.0169(8) 0.0103(7) -0.0001(6) -0.0011(6) 0.0002(7) C7 0.0204(9) 0.0133(8) 0.0147(8) 0.0005(6) -0.0013(7) -0.0017(7) C3 0.0154(8) 0.0195(8) 0.0163(8) -0.0018(7) -0.0025(7) -0.0002(7) C2 0.0156(8) 0.0160(8) 0.0154(8) -0.0001(6) -0.0005(7) 0.0016(7) C1 0.0159(8) 0.0139(7) 0.0148(8) -0.0005(6) 0.0000(7) 0.0005(7) C12 0.0182(9) 0.0155(8) 0.0152(8) 0.0005(7) 0.0016(7) 0.0005(7) C16 0.0186(8) 0.0153(8) 0.0153(8) 0.0004(6) 0.0017(7) 0.0018(7) C34 0.0202(9) 0.0245(9) 0.0154(9) -0.0022(7) -0.0017(7) 0.0032(8) C21 0.0183(8) 0.0154(8) 0.0152(8) -0.0007(6) 0.0003(7) -0.0007(7) C9 0.0155(8) 0.0217(8) 0.0157(8) -0.0006(7) -0.0002(7) -0.0025(7) C18 0.0248(9) 0.0214(9) 0.0168(9) -0.0006(7) -0.0012(8) 0.0005(8) C15 0.0211(9) 0.0206(8) 0.0160(8) 0.0013(7) 0.0011(7) -0.0007(8) C6 0.0169(8) 0.0147(8) 0.0145(8) 0.0000(6) 0.0015(7) -0.0001(7) C4 0.0163(8) 0.0150(8) 0.0185(8) 0.0010(6) -0.0007(7) 0.0007(7) C11 0.0178(8) 0.0141(8) 0.0169(8) -0.0003(6) 0.0002(7) -0.0004(7) C8 0.0170(8) 0.0191(8) 0.0173(8) -0.0001(7) -0.0034(7) -0.0018(7) C26 0.0256(10) 0.0209(9) 0.0177(9) -0.0031(7) -0.0023(8) -0.0028(7) C23 0.0207(9) 0.0156(8) 0.0249(9) 0.0014(7) 0.0025(7) 0.0029(7) C17 0.0218(9) 0.0204(9) 0.0198(9) -0.0011(7) 0.0005(7) -0.0021(7) C31 0.0336(11) 0.0185(9) 0.0228(10) 0.0073(7) 0.0034(8) -0.0002(8) C28 0.0461(13) 0.0184(9) 0.0238(10) -0.0035(7) -0.0061(9) -0.0046(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C13 O14 C11 112.10(13) C26 O25 C7 116.43(14) C21 O22 C23 115.81(14) C29 O30 C31 115.66(15) C15 O19 C18 106.20(15) O32 C29 O30 124.56(16) O32 C29 C6 123.47(16) O30 C29 C6 111.94(15) C10 C5 C6 123.55(16) C10 C5 C4 121.79(16) C4 C5 C6 114.49(16) C5 C10 C1 122.92(16) C5 C10 C9 121.50(16) C9 C10 C1 115.49(15) O14 C13 C1 111.54(14) O20 C13 O14 121.07(16) O20 C13 C1 127.38(16) O25 C7 H7 109.7 O25 C7 C6 107.96(14) O25 C7 C8 109.14(15) C6 C7 H7 109.7 C8 C7 H7 109.7 C8 C7 C6 110.54(14) H3A C3 H3B 107.9 C2 C3 H3A 109.3 C2 C3 H3B 109.3 C4 C3 H3A 109.3 C4 C3 H3B 109.3 C4 C3 C2 111.80(15) C3 C2 H2 107.4 C3 C2 C1 110.99(14) C1 C2 H2 107.4 C34 C2 C3 109.54(15) C34 C2 H2 107.4 C34 C2 C1 113.73(15) C10 C1 C13 106.44(14) C10 C1 C2 112.65(14) C10 C1 C12 113.55(14) C13 C1 C2 110.36(14) C13 C1 C12 102.87(14) C12 C1 C2 110.42(14) C1 C12 H12A 110.4 C1 C12 H12B 110.4 H12A C12 H12B 108.6 C11 C12 C1 106.48(14) C11 C12 H12A 110.4 C11 C12 H12B 110.4 C15 C16 C11 125.31(17) C15 C16 C17 105.77(16) C17 C16 C11 128.92(17) C2 C34 H34A 109.5 C2 C34 H34B 109.5 C2 C34 H34C 109.5 H34A C34 H34B 109.5 H34A C34 H34C 109.5 H34B C34 H34C 109.5 O22 C21 C6 111.39(15) O24 C21 O22 124.48(17) O24 C21 C6 123.97(16) C10 C9 H9A 109.1 C10 C9 H9B 109.1 C10 C9 C8 112.28(15) H9A C9 H9B 107.9 C8 C9 H9A 109.1 C8 C9 H9B 109.1 O19 C18 H18 124.7 C17 C18 O19 110.65(17) C17 C18 H18 124.7 O19 C15 H15 124.5 C16 C15 O19 110.97(17) C16 C15 H15 124.5 C5 C6 C29 107.18(14) C5 C6 C7 113.56(15) C5 C6 C21 112.12(14) C7 C6 C29 107.83(14) C21 C6 C29 109.28(14) C21 C6 C7 106.76(14) O33 C4 C5 121.13(16) O33 C4 C3 122.67(17) C3 C4 C5 116.15(15) O14 C11 C12 105.32(13) O14 C11 C16 108.48(14) O14 C11 H11 109.1 C12 C11 H11 109.1 C16 C11 C12 115.55(15) C16 C11 H11 109.1 C7 C8 C9 110.95(15) C7 C8 H8A 109.4 C7 C8 H8B 109.4 C9 C8 H8A 109.4 C9 C8 H8B 109.4 H8A C8 H8B 108.0 O25 C26 C28 110.46(16) O27 C26 O25 123.41(18) O27 C26 C28 126.12(18) O22 C23 H23A 109.5 O22 C23 H23B 109.5 O22 C23 H23C 109.5 H23A C23 H23B 109.5 H23A C23 H23C 109.5 H23B C23 H23C 109.5 C16 C17 H17 126.8 C18 C17 C16 106.41(17) C18 C17 H17 126.8 O30 C31 H31A 109.5 O30 C31 H31B 109.5 O30 C31 H31C 109.5 H31A C31 H31B 109.5 H31A C31 H31C 109.5 H31B C31 H31C 109.5 C26 C28 H28A 109.5 C26 C28 H28B 109.5 C26 C28 H28C 109.5 H28A C28 H28B 109.5 H28A C28 H28C 109.5 H28B C28 H28C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O14 C13 1.349(2) O14 C11 1.469(2) O20 C13 1.204(2) O33 C4 1.220(2) O32 C29 1.200(2) O25 C7 1.452(2) O25 C26 1.353(2) O22 C21 1.331(2) O22 C23 1.444(2) O30 C29 1.329(2) O30 C31 1.452(2) O19 C18 1.367(2) O19 C15 1.363(2) O24 C21 1.204(2) O27 C26 1.201(3) C29 C6 1.554(2) C5 C10 1.346(3) C5 C6 1.518(2) C5 C4 1.490(2) C10 C1 1.527(2) C10 C9 1.511(2) C13 C1 1.538(2) C7 H7 0.9800 C7 C6 1.553(2) C7 C8 1.515(3) C3 H3A 0.9700 C3 H3B 0.9700 C3 C2 1.530(2) C3 C4 1.489(3) C2 H2 0.9800 C2 C1 1.553(2) C2 C34 1.524(2) C1 C12 1.548(2) C12 H12A 0.9700 C12 H12B 0.9700 C12 C11 1.539(2) C16 C15 1.349(3) C16 C11 1.492(2) C16 C17 1.436(3) C34 H34A 0.9600 C34 H34B 0.9600 C34 H34C 0.9600 C21 C6 1.542(2) C9 H9A 0.9700 C9 H9B 0.9700 C9 C8 1.522(2) C18 H18 0.9300 C18 C17 1.345(3) C15 H15 0.9300 C11 H11 0.9800 C8 H8A 0.9700 C8 H8B 0.9700 C26 C28 1.494(3) C23 H23A 0.9600 C23 H23B 0.9600 C23 H23C 0.9600 C17 H17 0.9300 C31 H31A 0.9600 C31 H31B 0.9600 C31 H31C 0.9600 C28 H28A 0.9600 C28 H28B 0.9600 C28 H28C 0.9600 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion O14 C13 C1 C10 118.28(15) O14 C13 C1 C2 -119.18(15) O14 C13 C1 C12 -1.37(18) O20 C13 C1 C10 -63.0(2) O20 C13 C1 C2 59.6(2) O20 C13 C1 C12 177.39(17) O32 C29 C6 C5 7.4(2) O32 C29 C6 C7 130.05(18) O32 C29 C6 C21 -114.26(19) O25 C7 C6 C29 159.90(13) O25 C7 C6 C5 -81.50(18) O25 C7 C6 C21 42.58(18) O25 C7 C8 C9 58.55(18) O22 C21 C6 C29 149.14(15) O22 C21 C6 C5 30.5(2) O22 C21 C6 C7 -94.49(17) O30 C29 C6 C5 -170.92(14) O30 C29 C6 C7 -48.31(19) O30 C29 C6 C21 67.38(19) O19 C18 C17 C16 -0.1(2) O24 C21 C6 C29 -35.2(2) O24 C21 C6 C5 -153.87(18) O24 C21 C6 C7 81.2(2) C5 C10 C1 C13 107.87(19) C5 C10 C1 C2 -13.2(2) C5 C10 C1 C12 -139.68(17) C5 C10 C9 C8 -20.8(2) C10 C5 C6 C29 111.10(19) C10 C5 C6 C7 -7.9(2) C10 C5 C6 C21 -128.99(18) C10 C5 C4 O33 170.34(17) C10 C5 C4 C3 -12.1(2) C10 C1 C12 C11 -105.88(16) C10 C9 C8 C7 51.2(2) C13 O14 C11 C12 12.56(18) C13 O14 C11 C16 136.84(15) C13 C1 C12 C11 8.71(17) C7 O25 C26 O27 -0.9(3) C7 O25 C26 C28 179.90(18) C3 C2 C1 C10 41.85(19) C3 C2 C1 C13 -76.96(17) C3 C2 C1 C12 169.97(14) C2 C3 C4 O33 -140.75(18) C2 C3 C4 C5 41.8(2) C2 C1 C12 C11 126.49(15) C1 C10 C9 C8 156.12(15) C1 C12 C11 O14 -12.76(17) C1 C12 C11 C16 -132.45(16) C34 C2 C1 C10 165.91(15) C34 C2 C1 C13 47.10(19) C34 C2 C1 C12 -65.97(18) C9 C10 C1 C13 -68.96(19) C9 C10 C1 C2 169.96(15) C9 C10 C1 C12 43.5(2) C18 O19 C15 C16 -0.1(2) C15 O19 C18 C17 0.1(2) C15 C16 C11 O14 125.85(18) C15 C16 C11 C12 -116.2(2) C15 C16 C17 C18 0.0(2) C6 C5 C10 C1 -177.55(15) C6 C5 C10 C9 -0.9(3) C6 C5 C4 O33 -14.2(3) C6 C5 C4 C3 163.32(15) C6 C7 C8 C9 -60.04(19) C4 C5 C10 C1 -2.5(3) C4 C5 C10 C9 174.13(16) C4 C5 C6 C29 -64.27(19) C4 C5 C6 C7 176.76(14) C4 C5 C6 C21 55.6(2) C4 C3 C2 C1 -56.57(19) C4 C3 C2 C34 177.02(15) C11 O14 C13 O20 173.99(16) C11 O14 C13 C1 -7.15(19) C11 C16 C15 O19 179.37(16) C11 C16 C17 C18 -179.28(18) C8 C7 C6 C29 -80.79(17) C8 C7 C6 C5 37.81(19) C8 C7 C6 C21 161.88(14) C26 O25 C7 C6 -141.88(16) C26 O25 C7 C8 97.93(18) C23 O22 C21 O24 -0.5(3) C23 O22 C21 C6 175.15(15) C17 C16 C15 O19 0.0(2) C17 C16 C11 O14 -55.0(2) C17 C16 C11 C12 63.0(2) C31 O30 C29 O32 4.1(3) C31 O30 C29 C6 -177.56(16)